#------------------------------------------------------------------------------ #$Date: 2020-07-14 08:11:41 +0300 (Tue, 14 Jul 2020) $ #$Revision: 254276 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/10/86/2108643.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108643 loop_ _publ_author_name 'Singla, Labhini' 'Yadav, Hare Ram' 'Roy Choudhury, Angshuman' _publ_section_title ; Evaluation of fluorine-mediated intermolecular interactions in tetrafluorinated tetrahydroisoquinoline derivatives: synthesis and computational studies ; _journal_coeditor_code BM5125SUP1 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first ; ; _journal_paper_doi 10.1107/S2052520620006873 _journal_volume 76 _journal_year 2020 _chemical_formula_moiety 'C22 H17 F4 N O' _chemical_formula_sum 'C22 H17 F4 N O' _chemical_formula_weight 387.36 _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _audit_creation_date 2020-03-09T09:19:26-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _cell_angle_alpha 90 _cell_angle_beta 140.922(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.322(2) _cell_length_b 12.437(2) _cell_length_c 20.012(3) _cell_measurement_reflns_used 4216 _cell_measurement_temperature 100 _cell_measurement_theta_max 27.5 _cell_measurement_theta_min 3.2 _cell_volume 1776.4(6) _computing_cell_refinement ; CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011) ; _computing_data_collection ; CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011) ; _computing_data_reduction ; CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100 _diffrn_detector_area_resol_mean 13.6612 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Rigaku Mercury375R (2x2 bin mode)' _diffrn_measurement_method 'profile data from \w-scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.048 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 17876 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 26 _diffrn_reflns_theta_max 27.519 _diffrn_reflns_theta_min 3.23 _exptl_absorpt_coefficient_mu 0.117 _exptl_absorpt_correction_T_max 1 _exptl_absorpt_correction_T_min 0.853 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Blessing, 1995' _exptl_crystal_colour 'clear light colourless' _exptl_crystal_density_diffrn 1.448 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 800 _exptl_crystal_size_max 0.41 _exptl_crystal_size_mid 0.35 _exptl_crystal_size_min 0.16 _refine_diff_density_max 0.443 _refine_diff_density_min -0.269 _refine_diff_density_rms 0.054 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 321 _refine_ls_number_reflns 4065 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.076 _refine_ls_R_factor_all 0.0704 _refine_ls_R_factor_gt 0.0549 _refine_ls_shift/su_max 0 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0555P)^2^+1.5046P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_ref 0.1459 _reflns_number_gt 3208 _reflns_number_total 4065 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; iq-35-26_100k.res created by SHELXL-2014/7 TITL IQ in P21/c #14 REM reset to P21/c #14 CELL 0.71073 11.3217 12.4373 20.01199 90 140.9222 90 ZERR 4 0.002 0.002 0.00305 0 0.0082 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H F N O UNIT 88 68 16 4 4 L.S. 10 PLAN 30 SIZE 0.35 0.41 0.16 TEMP -173.15 BOND MORE -1 CONF BOND $H fmap 2 53 acta 52 REM REM REM WGHT 0.055500 1.504600 FVAR 0.43464 H4 2 0.974786 0.424002 0.297897 11.00000 0.03202 H6 2 0.740062 0.695456 0.275033 11.00000 0.03945 H7 2 0.686043 0.605509 0.350692 11.00000 0.04023 H1 2 0.832681 0.423511 0.483602 11.00000 0.02914 H2A 2 0.674058 0.219549 0.288278 11.00000 0.03294 H2B 2 0.843143 0.149626 0.392624 11.00000 0.05041 H3A 2 1.063982 0.282298 0.456681 11.00000 0.02416 H3B 2 0.940662 0.251155 0.341590 11.00000 0.04352 H12 2 0.693963 0.071291 0.392898 11.00000 0.03397 H14 2 0.661377 0.047146 0.582613 11.00000 0.03251 H16 2 0.775232 0.335262 0.548845 11.00000 0.02762 H19 2 0.100733 0.394196 0.106671 11.00000 0.04760 H20 2 0.046635 0.502906 0.181439 11.00000 0.04936 H21 2 0.320732 0.559758 0.363268 11.00000 0.04920 H10A 2 0.829279 0.729108 0.142351 11.00000 0.02825 H10B 2 0.869399 0.774741 0.233597 11.00000 0.03016 H10C 2 0.680231 0.713241 0.133830 11.00000 0.03619 C9 1 0.880127 0.403157 0.351647 11.00000 0.02801 0.02234 = 0.02354 -0.00234 0.01976 -0.00222 C4 1 0.913873 0.459265 0.307449 11.00000 0.03056 0.02439 = 0.02779 -0.00277 0.02367 -0.00064 C5 1 0.859727 0.566277 0.276929 11.00000 0.02579 0.02407 = 0.02345 -0.00239 0.01883 -0.00500 C6 1 0.778144 0.619183 0.294955 11.00000 0.02581 0.02193 = 0.02863 0.00051 0.02035 -0.00066 C7 1 0.744125 0.562747 0.338794 11.00000 0.02401 0.02431 = 0.02776 0.00056 0.01959 0.00126 C8 1 0.790315 0.453830 0.365370 11.00000 0.02287 0.02119 = 0.02067 -0.00120 0.01590 -0.00210 C1 1 0.744583 0.395846 0.410581 11.00000 0.02679 0.01885 = 0.02545 0.00019 0.02008 0.00069 C2 1 0.794718 0.226438 0.363786 11.00000 0.04526 0.02062 = 0.03588 -0.00101 0.03326 0.00032 C3 1 0.935609 0.286740 0.382949 11.00000 0.04408 0.02434 = 0.03707 0.00302 0.03456 0.00591 C11 1 0.739156 0.216681 0.460959 11.00000 0.02175 0.02300 = 0.02188 0.00338 0.01517 0.00192 C12 1 0.698892 0.105736 0.438088 11.00000 0.02831 0.02543 = 0.02336 -0.00071 0.01772 -0.00181 C13 1 0.673401 0.046422 0.484544 11.00000 0.03008 0.02093 = 0.02963 0.00152 0.02004 -0.00255 C14 1 0.680863 0.087907 0.551192 11.00000 0.02894 0.02916 = 0.02775 0.00437 0.02026 -0.00176 C15 1 0.716585 0.197166 0.570300 11.00000 0.02334 0.03099 = 0.02289 0.00189 0.01624 0.00004 C16 1 0.745621 0.262386 0.528135 11.00000 0.02395 0.02231 = 0.02440 0.00113 0.01745 -0.00006 C17 1 0.545133 0.425297 0.345766 11.00000 0.02465 0.02306 = 0.02676 0.00407 0.01927 -0.00106 C18 1 0.385400 0.393436 0.240411 11.00000 0.03159 0.03115 = 0.02933 0.00337 0.02373 -0.00395 C19 1 0.205209 0.421398 0.179946 11.00000 0.02527 0.04070 = 0.03180 0.00702 0.01794 -0.00564 C20 1 0.178905 0.483378 0.224823 11.00000 0.03128 0.03919 = 0.04880 0.01737 0.03068 0.00543 C21 1 0.329966 0.517351 0.328160 11.00000 0.04209 0.03032 = 0.05243 0.01093 0.03981 0.00715 C22 1 0.508211 0.488119 0.385097 11.00000 0.03371 0.02657 = 0.03426 0.00554 0.02718 0.00302 C10 1 0.809375 0.715401 0.181420 11.00000 0.03364 0.02956 = 0.03235 0.00448 0.02512 -0.00111 N1 4 0.773653 0.278712 0.419690 11.00000 0.03585 0.01745 = 0.03125 0.00126 0.02747 0.00124 O1 5 0.892396 0.612140 0.229685 11.00000 0.03883 0.02496 = 0.03485 -0.00103 0.03070 -0.00270 F1 3 0.637926 -0.060307 0.461888 11.00000 0.06387 0.02544 = 0.04841 -0.00597 0.04379 -0.01289 F2 3 0.725595 0.243381 0.635471 11.00000 0.04635 0.03319 = 0.03871 0.00281 0.03609 -0.00017 F3 3 0.409318 0.332377 0.195874 11.00000 0.03532 0.04888 = 0.02844 -0.00698 0.02320 -0.01027 F4 3 0.656110 0.524075 0.486265 11.00000 0.03862 0.03908 = 0.03989 -0.00592 0.02994 0.00406 HKLF 4 REM IQ in P21/c #14 REM R1 = 0.0549 for 3208 Fo > 4sig(Fo) and 0.0704 for all 4065 data REM 321 parameters refined using 0 restraints END WGHT 0.0554 1.5076 REM Highest difference peak 0.443, deepest hole -0.269, 1-sigma level 0.054 Q1 1 0.4963 0.2776 0.2195 11.00000 0.05 0.44 Q2 1 0.7787 0.5827 0.2601 11.00000 0.05 0.37 Q3 1 0.7605 0.4193 0.3799 11.00000 0.05 0.34 Q4 1 0.7985 0.4244 0.3414 11.00000 0.05 0.27 Q5 1 0.6436 0.4140 0.3758 11.00000 0.05 0.27 Q6 1 0.7800 0.4965 0.3588 11.00000 0.05 0.25 Q7 1 0.7548 0.2398 0.5034 11.00000 0.05 0.25 Q8 1 0.7367 0.0629 0.5413 11.00000 0.05 0.25 Q9 1 0.6953 0.5403 0.4601 11.00000 0.05 0.25 Q10 1 0.7234 -0.0845 0.4597 11.00000 0.05 0.24 Q11 1 0.7991 0.2580 0.4028 11.00000 0.05 0.24 Q12 1 0.7158 0.2350 0.5388 11.00000 0.05 0.23 Q13 1 0.5366 0.4749 0.3614 11.00000 0.05 0.23 Q14 1 0.8986 0.2633 0.4609 11.00000 0.05 0.22 Q15 1 0.8721 0.4381 0.3828 11.00000 0.05 0.22 Q16 1 0.9097 0.2385 0.3953 11.00000 0.05 0.22 Q17 1 0.8949 0.5240 0.3018 11.00000 0.05 0.21 Q18 1 0.7525 0.2460 0.4420 11.00000 0.05 0.21 Q19 1 1.0192 0.5971 0.2617 11.00000 0.05 0.21 Q20 1 0.4833 0.4208 0.3014 11.00000 0.05 0.21 Q21 1 1.0557 0.2878 0.4204 11.00000 0.05 0.20 Q22 1 0.2293 0.3570 0.1610 11.00000 0.05 0.20 Q23 1 0.9513 0.4352 0.3624 11.00000 0.05 0.19 Q24 1 0.5977 0.2258 0.5629 11.00000 0.05 0.19 Q25 1 0.9210 0.4331 0.3385 11.00000 0.05 0.19 Q26 1 0.8164 0.1395 0.5024 11.00000 0.05 0.18 Q27 1 0.5736 -0.0335 0.4836 11.00000 0.05 0.18 Q28 1 0.8076 0.0851 0.4560 11.00000 0.05 0.18 Q29 1 0.8420 0.5846 0.2437 11.00000 0.05 0.17 Q30 1 0.3054 0.4802 0.2797 11.00000 0.05 0.17 REM The information below was added by Olex2. REM REM R1 = 0.0549 for 3208 Fo > 4sig(Fo) and 0.0704 for all 18332 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.44, deepest hole -0.27 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0704 REM R1_gt = 0.0549 REM wR_ref = 0.1459 REM GOOF = 1.076 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 18332 REM Reflections_gt = 3208 REM Parameters = n/a REM Hole = -0.27 REM Peak = 0.44 REM Flack = n/a ; _cod_data_source_file bm5125sup1.cif _cod_data_source_block 6-34 _cod_original_cell_volume 1776.3(5) _cod_database_code 2108643 _iucr_refine_reflections_details ; 0 0 2 159.56 1.93 0 0 3 0.93 0.66 0 0 3 1.01 0.61 0 0 -3 3.91 1.24 0 0 4 5.48 0.94 0 0 4 5.25 0.69 0 0 -4 7.75 1.27 0 0 5 -0.48 0.61 0 0 5 -0.01 0.34 0 0 -5 0.05 0.79 0 0 6 293.26 7.22 0 0 6 258.88 5.88 0 0 -6 267.55 7.44 0 0 7 -0.20 0.64 0 0 7 1.50 0.78 0 0 -7 0.46 1.19 0 0 8 2.48 0.77 0 0 -8 4.90 1.76 0 0 9 0.52 0.82 0 0 -9 4.01 1.59 0 0 10 35.25 3.06 0 0 10 27.77 2.13 0 0 -10 39.45 3.95 0 0 11 1.98 1.54 0 0 11 0.76 0.74 0 0 -11 14.15 3.16 0 0 12 36.35 3.65 0 0 12 21.15 2.16 0 0 -12 45.21 4.58 0 0 -13 3.48 2.35 0 0 14 4.54 1.84 0 0 -14 10.12 3.16 0 0 15 0.20 1.33 0 0 -15 -1.03 1.39 0 0 16 0.88 1.39 0 0 -16 -0.17 1.52 0 1 2 275.15 4.09 0 -1 2 268.37 3.66 0 -1 2 255.84 3.70 0 1 2 258.56 3.02 0 -1 -2 267.20 3.10 0 -1 -2 257.47 3.90 0 1 -2 266.79 3.95 0 1 3 2012.69 18.93 0 -1 3 1945.31 17.78 0 1 3 1791.54 15.46 0 -1 -3 1872.66 18.02 0 1 4 126.90 3.28 0 -1 4 128.34 2.98 0 1 4 110.45 2.14 0 -1 4 101.51 2.56 0 -1 -4 124.01 3.38 0 1 -4 129.17 3.46 0 1 5 41.70 2.21 0 -1 5 41.88 2.07 0 1 5 37.05 1.51 0 -1 5 33.29 1.77 0 -1 -5 37.70 2.31 0 1 -5 41.30 2.50 0 1 6 314.23 7.74 0 -1 6 313.37 7.47 0 1 6 282.50 6.03 0 -1 6 271.23 6.39 0 -1 -6 316.44 8.32 0 1 -6 319.85 8.51 0 1 7 657.09 13.78 0 -1 7 677.86 13.80 0 1 7 604.47 11.39 0 -1 7 604.11 11.99 0 -1 -7 637.69 13.95 0 1 -7 647.57 14.12 0 1 8 8.65 1.69 0 -1 8 10.72 1.90 0 1 8 6.69 1.06 0 -1 8 6.97 1.24 0 -1 -8 7.24 1.89 0 1 -8 9.91 2.14 0 1 9 27.52 2.72 0 -1 9 27.38 2.50 0 -1 9 20.99 1.88 0 -1 -9 36.39 3.40 0 1 -9 37.88 3.75 0 1 10 6.90 1.97 0 -1 10 7.57 1.76 0 1 10 2.77 0.94 0 -1 10 3.92 1.22 0 -1 -10 6.92 2.14 0 1 -10 6.32 2.11 0 1 11 27.75 2.97 0 -1 11 26.47 2.72 0 -1 11 25.49 2.23 0 -1 -11 44.23 4.49 0 1 -11 48.84 4.66 0 1 12 0.48 1.14 0 -1 12 2.27 1.47 0 -1 -12 4.39 2.06 0 1 -12 2.05 2.16 0 1 13 10.50 2.66 0 -1 13 11.47 2.10 0 -1 -13 13.25 3.00 0 1 -13 13.37 3.29 0 1 14 5.88 2.27 0 -1 14 6.30 2.45 0 -1 -14 7.93 3.13 0 1 -14 4.72 2.52 0 1 15 2.15 1.90 0 -1 15 3.27 1.89 0 -1 -15 1.98 1.65 0 1 -15 -0.56 1.36 0 1 16 2.33 2.12 0 -1 16 -0.75 1.26 0 -1 -16 6.06 3.34 0 1 -16 1.80 2.59 0 2 0 831.26 8.36 0 -2 0 845.85 8.61 0 -2 0 852.43 7.95 0 2 0 850.18 7.94 0 2 -1 346.65 4.34 0 2 1 390.86 5.14 0 -2 1 364.04 4.97 0 -2 -1 358.00 4.40 0 2 -1 379.94 4.50 0 2 -2 109.00 2.25 0 2 2 119.44 2.83 0 -2 2 112.38 2.79 0 -2 -2 106.80 1.99 0 -2 -2 109.30 2.56 0 2 -2 118.73 2.56 0 2 3 654.47 8.56 0 -2 3 649.56 7.64 0 -2 3 650.54 8.23 0 -2 -3 659.64 6.91 0 -2 -3 643.11 8.26 0 2 -3 666.47 8.35 0 2 4 698.89 9.49 0 -2 4 694.16 8.59 0 -2 4 644.61 8.54 0 -2 -4 676.00 7.26 0 -2 -4 668.58 9.22 0 2 -4 685.54 9.29 0 2 5 91.52 3.44 0 -2 5 87.24 2.81 0 2 5 79.71 3.24 0 -2 5 75.15 2.74 0 -2 -5 82.11 3.32 0 2 -5 84.02 3.24 0 2 6 226.02 6.56 0 -2 6 231.99 6.06 0 -2 6 213.38 5.75 0 -2 -6 231.73 6.85 0 2 -6 249.18 7.25 0 2 7 7.44 1.63 0 -2 7 7.38 1.41 0 2 7 3.46 0.81 0 -2 7 4.68 1.14 0 -2 -7 8.32 1.89 0 2 -7 9.31 1.87 0 2 8 21.79 2.31 0 -2 8 21.55 2.04 0 -2 8 20.04 1.93 0 -2 -8 20.93 2.51 0 2 -8 18.01 2.39 0 2 9 19.22 2.62 0 -2 9 13.54 1.88 0 2 9 16.32 1.53 0 -2 9 18.20 1.88 0 -2 -9 17.51 2.86 0 2 -9 22.19 2.95 0 2 10 4.09 1.74 0 -2 10 2.14 1.18 0 2 10 2.02 0.73 0 -2 10 1.11 0.80 0 -2 -10 9.89 2.76 0 2 -10 5.32 1.81 0 2 11 7.05 1.96 0 -2 11 5.49 1.60 0 -2 11 5.76 1.55 0 -2 -11 7.76 3.00 0 2 -11 11.20 2.96 0 2 12 18.02 2.68 0 -2 12 22.39 2.83 0 -2 12 17.69 2.24 0 -2 -12 16.96 3.38 0 2 -12 17.39 3.02 0 2 13 1.88 1.92 0 -2 13 -0.17 1.14 0 -2 13 -0.32 0.74 0 -2 -13 -0.54 1.40 0 2 -13 1.39 1.51 0 2 14 1.27 1.29 0 -2 14 0.61 1.21 0 -2 -14 0.69 1.71 0 2 -14 0.93 1.53 0 2 15 3.62 2.39 0 -2 15 4.63 2.15 0 -2 -15 2.60 1.79 0 2 -15 3.82 2.32 0 2 16 2.56 2.38 0 -2 16 5.32 2.45 0 -2 -16 3.84 3.17 0 2 -16 3.80 2.36 0 3 0 2.55 1.21 0 -3 0 2.19 0.93 0 3 0 1.52 0.75 0 3 -1 671.47 7.84 0 3 1 758.66 9.00 0 -3 1 721.31 8.87 0 -3 -1 718.47 8.23 0 -3 -1 689.65 7.63 0 3 -1 729.36 7.82 0 3 -2 28.78 1.46 0 3 2 29.93 1.82 0 -3 2 31.09 1.83 0 -3 -2 33.16 1.47 0 -3 -2 30.30 1.68 0 3 -2 31.58 1.51 0 3 -3 669.76 8.21 0 3 3 724.24 9.70 0 -3 3 683.14 9.17 0 -3 -3 693.16 7.80 0 -3 -3 706.07 9.03 0 3 -3 713.92 8.89 0 3 4 3.21 1.00 0 -3 4 4.97 0.91 0 -3 4 4.40 1.16 0 -3 -4 3.45 0.75 0 -3 -4 3.87 1.22 0 3 -4 4.55 1.12 0 3 5 237.67 6.59 0 -3 5 234.51 5.80 0 -3 5 218.45 5.96 0 -3 -5 236.58 5.11 0 -3 -5 243.53 6.61 0 3 -5 239.38 6.42 0 3 6 530.73 11.90 0 -3 6 503.39 10.56 0 3 6 474.93 9.01 0 -3 6 488.31 10.72 0 -3 -6 485.32 11.14 0 3 -6 496.38 11.17 0 3 7 10.37 1.85 0 -3 7 9.84 1.40 0 3 7 7.85 1.51 0 -3 7 8.47 1.47 0 -3 -7 10.27 2.09 0 3 -7 9.13 1.85 0 3 8 -0.02 0.97 0 -3 8 -0.39 0.69 0 3 8 0.65 0.44 0 -3 8 1.00 1.07 0 -3 -8 -0.73 0.93 0 3 -8 1.06 1.07 0 3 9 1.40 1.12 0 -3 9 3.64 1.35 0 3 9 2.43 0.76 0 -3 9 2.09 0.95 0 -3 -9 4.80 1.91 0 3 -9 2.98 1.58 0 3 10 4.89 1.57 0 -3 10 5.14 1.55 0 -3 10 3.48 1.19 0 -3 -10 2.48 1.41 0 3 -10 5.12 2.09 0 3 11 2.57 1.66 0 -3 11 0.75 0.88 0 -3 -11 1.98 1.65 0 3 -11 2.11 1.35 0 3 12 15.91 2.92 0 -3 12 11.87 2.22 0 -3 12 12.09 2.24 0 -3 -12 12.89 2.90 0 3 -12 15.02 2.90 0 3 13 0.55 1.34 0 -3 13 2.68 1.30 0 -3 13 1.97 1.29 0 -3 -13 0.86 1.55 0 3 -13 3.02 2.12 0 3 14 4.05 2.37 0 -3 14 -0.35 1.10 0 -3 -14 4.35 2.50 0 3 -14 -0.61 1.43 0 3 15 7.58 2.19 0 -3 15 6.36 2.33 0 -3 -15 9.34 3.04 0 3 -15 8.26 3.18 0 3 16 55.14 5.18 0 -3 -16 54.17 6.27 0 3 -16 46.77 5.24 0 4 0 1058.72 11.91 0 -4 0 1059.70 12.11 0 4 0 1058.25 10.82 0 4 -1 57.40 2.14 0 4 1 58.09 2.43 0 -4 1 57.66 2.45 0 -4 -1 57.03 2.19 0 -4 -1 53.51 2.22 0 4 -1 54.76 1.83 0 4 -2 705.63 8.82 0 4 2 705.49 9.68 0 -4 2 714.17 9.81 0 -4 -2 708.83 8.76 0 -4 -2 676.01 8.46 0 4 -2 711.15 8.53 0 4 -3 92.56 2.74 0 4 3 85.32 3.23 0 -4 3 91.64 3.28 0 -4 -3 89.24 2.53 0 -4 -3 88.16 2.98 0 4 -3 90.36 2.79 0 4 -4 216.44 6.49 0 4 4 227.79 5.64 0 -4 4 215.10 5.34 0 -4 -4 214.37 3.74 0 -4 -4 211.31 4.80 0 4 -4 220.83 4.96 0 4 -5 50.68 2.50 0 4 5 51.99 3.05 0 -4 5 46.03 2.77 0 -4 -5 48.49 1.93 0 -4 -5 53.69 2.94 0 4 -5 50.55 2.72 0 4 6 348.58 9.30 0 -4 6 354.42 8.53 0 -4 6 342.68 8.91 0 -4 -6 342.45 7.39 0 -4 -6 338.30 9.00 0 4 -6 347.39 9.02 0 4 7 98.93 4.44 0 -4 7 101.46 3.75 0 -4 7 87.21 3.84 0 -4 -7 97.69 2.71 0 -4 -7 92.66 4.27 0 4 -7 100.97 4.34 0 4 8 154.16 6.50 0 -4 8 155.82 5.76 0 4 8 137.03 5.36 0 -4 8 152.61 6.14 0 -4 -8 166.21 6.93 0 4 -8 162.64 6.72 0 4 9 106.79 5.18 0 -4 9 103.89 4.34 0 4 9 90.26 2.86 0 -4 9 97.05 4.39 0 -4 -9 82.21 4.70 0 4 -9 102.75 4.90 0 4 10 5.10 2.13 0 -4 10 4.23 1.49 0 -4 10 4.24 1.55 0 -4 -10 8.21 2.37 0 4 -10 5.85 2.11 0 4 11 -1.45 1.11 0 -4 11 -0.67 0.96 0 -4 -11 2.77 2.03 0 4 -11 1.60 1.98 0 4 12 19.75 3.46 0 -4 12 12.65 2.05 0 -4 12 12.48 2.22 0 -4 -12 18.06 3.56 0 4 -12 17.74 3.18 0 4 13 1.07 1.35 0 -4 13 0.41 1.04 0 -4 13 -0.13 0.89 0 -4 -13 0.39 1.40 0 4 -13 2.52 2.42 0 4 14 2.34 2.12 0 -4 14 1.04 1.26 0 -4 -14 1.43 1.79 0 4 -14 0.81 1.42 0 4 15 27.03 3.91 0 -4 -15 29.93 4.66 0 4 -15 25.16 4.25 0 5 0 0.64 0.66 0 -5 0 0.18 0.76 0 5 0 -0.55 0.42 0 5 -1 87.39 2.90 0 5 1 88.45 3.15 0 -5 1 89.16 3.28 0 -5 -1 87.62 3.07 0 -5 -1 86.15 5.33 0 5 -1 86.33 2.44 0 5 -2 36.90 1.99 0 5 2 41.83 2.33 0 -5 2 41.41 2.53 0 -5 -2 39.96 2.06 0 -5 -2 37.23 3.37 0 5 -2 38.21 1.80 0 5 -3 533.67 10.72 0 5 3 625.66 13.04 0 -5 3 577.11 12.31 0 -5 -3 566.09 11.11 0 -5 -3 554.85 11.17 0 5 -3 576.98 11.31 0 5 -4 136.24 3.69 0 5 4 156.06 5.33 0 -5 4 148.56 5.24 0 -5 -4 149.59 4.28 0 -5 -4 145.55 4.23 0 5 -4 146.42 4.05 0 5 -5 9.76 2.17 0 5 5 8.09 1.45 0 -5 5 9.00 1.55 0 -5 -5 9.23 1.14 0 -5 -5 6.91 1.44 0 5 -5 7.89 1.29 0 5 -6 47.33 3.03 0 5 6 49.29 3.39 0 -5 6 38.06 2.78 0 -5 -6 51.24 2.25 0 -5 -6 49.42 3.13 0 5 -6 54.36 3.22 0 5 -7 8.22 1.57 0 5 7 6.32 1.81 0 -5 7 3.14 1.19 0 -5 -7 6.85 0.98 0 -5 -7 5.98 1.70 0 5 -7 3.53 1.23 0 5 8 56.39 3.82 0 -5 8 55.87 3.10 0 -5 8 57.34 3.60 0 -5 -8 52.88 2.37 0 -5 -8 52.51 3.63 0 5 -8 52.67 3.61 0 5 9 18.50 2.85 0 -5 9 15.36 2.05 0 -5 9 13.47 2.01 0 -5 -9 13.33 2.56 0 5 -9 15.38 2.60 0 5 10 22.11 3.17 0 -5 10 19.46 2.20 0 -5 10 21.19 2.58 0 -5 -10 16.07 2.74 0 5 -10 25.42 3.17 0 5 11 1.88 1.36 0 -5 11 0.13 0.97 0 -5 11 2.65 1.74 0 -5 -11 2.81 1.99 0 5 -11 0.90 1.18 0 5 12 14.04 3.14 0 -5 12 12.12 2.09 0 -5 12 12.85 2.34 0 -5 -12 12.15 3.17 0 5 -12 13.45 2.92 0 5 13 5.95 2.36 0 -5 13 4.78 2.00 0 -5 13 5.87 2.16 0 -5 -13 5.35 2.67 0 5 -13 6.46 2.65 0 5 14 39.56 4.62 0 -5 14 31.52 3.69 0 -5 14 36.68 3.85 0 -5 -14 39.84 5.31 0 5 -14 34.64 4.19 0 5 15 8.94 3.49 0 -5 -15 3.32 2.63 0 5 -15 7.79 2.73 0 6 0 2544.82 17.89 0 -6 0 2558.30 17.08 0 6 0 2475.16 40.52 0 -6 1 142.59 4.40 0 -6 -1 151.35 4.83 0 -6 -1 139.07 5.25 0 6 -1 148.29 3.42 0 6 -2 25.19 2.42 0 6 2 26.14 3.04 0 -6 2 17.19 1.91 0 -6 -2 17.90 1.73 0 -6 -2 16.59 3.53 0 6 -2 16.06 1.41 0 6 -3 25.77 1.90 0 6 3 29.60 2.42 0 -6 3 26.43 2.35 0 -6 -3 26.62 1.94 0 -6 -3 23.28 1.76 0 6 -3 26.26 1.80 0 6 -4 82.41 3.11 0 6 4 81.45 3.77 0 -6 4 85.56 3.90 0 -6 -4 82.42 3.01 0 -6 -4 83.62 3.42 0 6 -4 84.14 3.14 0 6 -5 43.82 2.62 0 6 5 46.65 3.33 0 -6 5 42.62 3.15 0 -6 -5 44.64 2.31 0 -6 -5 44.49 2.90 0 6 -5 48.11 2.75 0 6 -6 2.25 0.59 0 6 6 0.36 1.00 0 -6 6 3.07 1.27 0 -6 -6 0.87 0.82 0 -6 -6 0.44 0.84 0 6 -6 1.02 0.86 0 6 -7 69.23 4.22 0 6 7 84.22 4.74 0 -6 7 79.37 4.28 0 -6 -7 79.22 2.95 0 -6 -7 78.64 4.12 0 6 -7 76.77 3.91 0 6 -8 6.95 2.50 0 6 8 8.15 1.87 0 -6 8 8.23 2.11 0 -6 -8 7.84 1.14 0 -6 -8 8.62 2.23 0 6 -8 14.09 2.24 0 6 9 89.77 5.16 0 -6 9 76.76 4.59 0 -6 -9 77.43 4.78 0 6 -9 95.30 5.01 0 6 -10 214.68 11.58 0 6 10 253.71 8.59 0 -6 10 249.43 7.89 0 -6 -10 237.06 8.29 0 6 -10 266.21 8.39 0 6 -11 0.17 0.83 0 6 11 -0.87 1.33 0 -6 11 1.82 1.51 0 -6 -11 -0.07 1.21 0 6 -11 -0.01 1.07 0 6 -12 0.49 0.83 0 6 12 5.71 2.16 0 -6 -12 0.22 1.33 0 6 -12 0.37 1.20 0 6 -13 95.96 5.43 0 6 13 124.17 7.42 0 -6 13 92.93 5.64 0 -6 -13 99.62 6.97 0 6 -13 118.74 7.11 0 6 14 4.38 2.32 0 -6 -14 0.91 1.52 0 6 -14 0.38 1.46 0 6 15 3.62 2.58 0 -6 -15 2.16 2.66 0 6 -15 2.13 2.36 0 7 0 7.33 2.13 0 -7 0 0.60 0.85 0 7 0 0.23 0.55 0 7 -1 173.30 5.58 0 7 1 197.69 6.55 0 -7 1 167.12 5.76 0 -7 -1 172.52 5.60 0 -7 -1 162.43 9.63 0 7 -1 173.16 4.80 0 7 -2 66.27 3.01 0 7 2 60.88 3.33 0 -7 2 65.38 3.55 0 -7 -2 67.88 3.16 0 -7 -2 66.61 6.38 0 7 -2 64.81 2.61 0 7 -3 227.54 6.55 0 7 3 247.41 7.70 0 -7 3 241.28 7.65 0 -7 -3 239.21 6.80 0 -7 -3 224.59 6.36 0 7 -3 231.51 6.26 0 7 -4 14.43 1.70 0 7 4 14.47 2.02 0 -7 4 14.40 2.20 0 -7 -4 12.00 1.55 0 -7 -4 12.49 1.72 0 7 -4 12.88 1.56 0 7 -5 19.57 1.91 0 7 5 20.05 2.45 0 -7 5 19.84 2.52 0 -7 -5 21.03 1.90 0 -7 -5 20.30 2.20 0 7 -5 20.93 1.99 0 7 -6 113.58 4.16 0 7 6 127.03 5.55 0 -7 6 124.68 5.39 0 -7 -6 120.66 3.95 0 -7 -6 118.17 4.64 0 7 -6 124.39 4.60 0 7 -7 4.76 1.19 0 7 7 8.39 1.89 0 -7 7 7.19 1.90 0 -7 -7 5.41 1.23 0 -7 -7 6.15 1.79 0 7 -7 7.38 1.76 0 7 8 22.49 3.19 0 -7 8 17.31 2.64 0 -7 -8 16.35 1.65 0 -7 -8 17.01 2.71 0 7 -8 20.45 2.59 0 7 -9 24.33 6.09 0 7 9 25.36 3.37 0 -7 9 28.17 3.24 0 -7 -9 23.92 2.91 0 7 -9 26.89 2.89 0 7 -10 32.96 4.48 0 7 10 43.73 4.27 0 -7 10 36.18 3.82 0 -7 -10 45.56 4.41 0 7 -10 42.83 4.02 0 7 -11 0.93 0.70 0 7 11 0.55 1.37 0 -7 11 0.75 1.24 0 -7 -11 0.41 1.22 0 7 -11 1.21 1.23 0 7 -12 13.43 3.77 0 7 12 21.71 3.80 0 -7 12 15.28 3.08 0 -7 -12 18.38 3.18 0 7 -12 22.18 3.66 0 7 13 66.77 5.66 0 -7 13 58.60 4.84 0 -7 -13 59.32 5.52 0 7 -13 74.95 5.97 0 7 14 21.59 4.42 0 -7 14 15.83 3.48 0 -7 -14 24.46 4.50 0 7 -14 20.91 3.55 0 8 0 0.87 0.95 0 -8 0 0.58 0.83 0 8 0 0.92 0.85 0 8 -1 19.55 1.98 0 8 1 15.65 2.21 0 -8 1 18.04 2.28 0 -8 -1 17.63 2.09 0 -8 -1 17.11 4.62 0 8 -1 17.01 1.64 0 8 -2 38.35 2.62 0 8 2 41.40 2.96 0 -8 2 41.94 3.12 0 -8 -2 41.02 2.81 0 -8 -2 37.47 4.49 0 8 -2 42.61 2.26 0 8 -3 227.33 7.52 0 8 3 203.78 7.55 0 -8 3 214.94 7.94 0 -8 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9.97 2.77 0 -9 9 8.32 2.55 0 -9 -9 7.44 2.03 0 9 -9 6.11 1.89 0 9 10 8.10 2.75 0 -9 10 10.51 2.92 0 -9 -10 6.48 2.14 0 9 -10 8.62 2.46 0 9 11 122.69 7.74 0 -9 11 112.59 6.54 0 -9 -11 125.54 6.83 0 9 -11 109.82 6.42 0 9 12 -1.11 1.57 0 -9 12 -0.73 1.47 0 -9 -12 1.45 1.57 0 9 -12 -0.20 1.24 0 9 13 23.41 3.98 0 -9 -13 27.75 4.44 0 9 -13 28.48 4.12 0 10 0 32.75 3.70 0 -10 0 19.68 2.58 0 10 -1 52.92 3.95 0 10 1 49.49 3.93 0 -10 1 49.18 3.72 0 -10 -1 42.00 3.43 0 -10 -1 40.48 4.62 0 10 -1 43.38 2.57 0 10 -2 14.43 2.65 0 10 2 11.25 2.04 0 -10 2 15.61 2.54 0 -10 -2 12.60 2.02 0 -10 -2 11.37 3.98 0 10 -2 11.64 1.48 0 10 -3 3.97 2.02 0 10 3 0.59 1.14 0 -10 3 -0.81 1.06 0 -10 -3 1.17 1.04 0 -10 -3 0.64 0.68 0 10 -3 -0.76 0.64 0 10 4 1.27 1.07 0 -10 4 4.79 2.08 0 -10 -4 0.93 1.17 0 10 -4 1.66 1.27 0 10 -5 4.91 1.56 0 10 5 7.17 2.38 0 -10 5 4.44 1.76 0 -10 -5 3.12 1.45 0 10 -5 5.58 1.54 0 10 6 210.03 7.92 0 -10 6 213.01 8.10 0 -10 -6 206.56 6.33 0 10 -6 202.01 6.31 0 10 -7 321.00 8.24 0 10 7 361.31 10.57 0 -10 7 321.06 9.93 0 -10 -7 329.95 7.77 0 10 -7 332.35 8.31 0 10 -8 9.87 2.15 0 10 8 12.54 3.07 0 -10 8 10.66 2.47 0 -10 -8 9.71 1.78 0 10 -8 11.96 2.22 0 10 9 19.55 3.62 0 -10 9 13.03 3.01 0 10 -9 18.55 2.82 0 10 -10 3.56 1.87 0 10 10 4.26 2.54 0 -10 10 1.28 1.46 0 10 -10 6.00 2.17 0 10 11 5.99 2.63 0 -10 11 3.51 2.04 0 10 -11 2.26 1.30 0 10 12 24.94 4.20 0 -10 12 21.51 3.64 0 10 -12 17.53 3.24 0 11 0 -0.76 1.38 0 -11 0 -0.26 1.02 0 -11 0 0.38 0.49 0 11 -1 -0.04 1.36 0 11 1 1.04 1.29 0 -11 1 1.11 1.20 0 -11 -1 1.07 1.18 0 -11 -1 1.62 0.94 0 11 -1 0.63 0.90 0 11 -2 158.77 6.10 0 11 2 183.12 7.08 0 -11 2 177.55 7.08 0 -11 -2 172.51 6.41 0 -11 -2 168.94 5.40 0 11 -2 168.51 5.09 0 11 -3 2.74 1.61 0 11 3 3.32 1.72 0 -11 3 3.99 2.28 0 -11 -3 1.34 1.44 0 -11 -3 1.68 0.93 0 11 -3 2.69 1.08 0 11 -4 8.18 2.26 0 11 4 4.97 2.12 0 -11 4 5.28 2.48 0 -11 -4 5.81 1.62 0 -11 -4 5.52 1.65 0 11 -4 4.06 1.34 0 11 5 2.45 1.96 0 -11 5 3.29 2.26 0 -11 -5 2.69 1.41 0 -11 -5 1.41 1.42 0 11 -5 0.50 0.80 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3 -6 35.69 2.08 -2 3 5 5.39 0.98 -2 -3 5 4.92 1.10 2 -3 -5 5.16 0.99 2 -3 -5 6.52 0.91 2 3 -5 4.82 1.06 -2 3 4 1105.59 12.57 2 3 -4 1121.50 10.40 -2 -3 4 1177.02 13.11 2 -3 -4 1195.73 13.22 2 -3 -4 1164.90 10.62 2 3 -4 1122.79 12.63 -2 3 3 200.55 4.05 2 3 -3 200.86 3.01 -2 -3 3 195.12 3.69 2 -3 -3 204.27 4.09 2 3 -3 198.62 3.93 -2 3 2 2.07 0.83 2 3 -2 0.29 0.55 -2 -3 2 1.76 0.71 2 -3 -2 2.37 0.79 -2 3 2 1.09 0.20 2 3 -2 0.80 0.72 2 -3 -1 425.37 6.72 -2 -3 1 471.31 7.26 -2 3 1 474.22 5.26 -2 3 0 17.53 3.04 2 3 0 18.60 1.73 -2 -3 0 15.50 0.89 2 -3 0 15.35 1.49 -2 -3 0 16.52 4.33 -2 3 0 18.59 1.22 2 3 1 62.78 2.87 2 -3 1 65.04 2.79 2 -3 1 55.04 2.49 -2 -3 -1 53.12 1.18 -2 -3 -1 60.27 2.93 -2 3 -1 57.74 2.25 2 3 2 247.35 6.89 2 -3 2 258.09 6.88 2 -3 2 205.77 5.59 -2 -3 -2 241.26 6.86 -2 3 -2 244.69 6.35 2 3 3 159.92 5.04 2 -3 3 157.83 4.72 2 -3 3 144.82 4.63 -2 -3 -3 155.82 5.58 -2 3 -3 159.90 5.45 2 3 4 278.51 8.37 2 -3 4 262.85 7.69 2 -3 4 225.78 6.42 -2 3 -4 271.35 7.77 2 3 5 38.30 3.18 2 -3 5 34.98 2.68 2 -3 5 34.33 2.32 -2 -3 -5 32.07 2.97 -2 3 -5 39.06 3.03 2 3 6 302.26 8.15 2 -3 6 298.47 7.58 2 -3 6 242.37 5.83 -2 3 -6 305.51 7.89 2 3 7 47.94 3.70 2 -3 7 47.34 3.48 -2 -3 -7 47.41 4.15 -2 3 -7 48.12 3.72 2 3 8 12.49 2.71 2 -3 8 11.61 2.29 2 -3 8 12.17 1.74 -2 -3 -8 10.39 2.73 -2 3 -8 9.95 2.30 2 3 9 25.56 3.64 2 -3 9 19.32 2.80 -2 -3 -9 21.55 3.86 -2 3 -9 17.62 2.88 2 3 10 31.63 3.74 2 -3 10 29.63 3.49 -2 -3 -10 27.90 3.98 -2 3 -10 32.17 3.97 2 3 11 16.53 3.22 2 -3 11 16.29 3.16 -2 -3 -11 15.80 3.40 -2 3 -11 23.28 4.09 2 3 12 0.19 1.43 2 -3 12 1.00 1.46 -2 -3 -12 -0.24 1.49 -2 3 -12 2.14 2.03 2 3 13 0.13 1.53 2 -3 13 0.79 1.55 -2 -3 -13 1.50 1.79 -2 3 -13 0.54 1.45 -2 4 18 54.87 5.07 2 -4 -18 64.95 6.62 2 4 -18 71.30 6.22 -2 4 17 1.31 1.39 2 -4 -17 1.76 1.59 2 4 -17 2.66 2.35 -2 4 16 0.43 1.18 -2 -4 16 2.09 1.49 2 -4 -16 2.27 2.24 2 4 -16 2.07 2.00 -2 4 15 0.37 1.17 -2 -4 15 -0.21 0.79 2 -4 -15 0.46 1.39 2 4 -15 1.06 1.88 -2 4 14 12.68 2.64 -2 -4 14 12.36 2.24 -2 4 14 7.92 1.63 -2 -4 14 10.30 2.14 2 -4 -14 9.35 2.62 2 4 -14 13.03 2.66 -2 4 13 14.27 2.90 -2 -4 13 11.67 1.83 -2 4 13 11.75 1.73 -2 -4 13 11.22 2.20 2 -4 -13 10.15 2.48 2 4 -13 11.94 2.63 -2 4 12 52.94 3.81 -2 -4 12 47.76 2.75 -2 4 12 48.08 3.37 -2 -4 12 53.97 3.94 2 -4 -12 49.63 4.18 2 4 -12 51.43 3.91 -2 4 11 290.46 7.55 -2 -4 11 296.34 5.59 -2 4 11 250.62 12.32 -2 -4 11 289.89 7.59 2 -4 -11 280.02 7.57 2 4 -11 302.20 8.03 -2 4 10 110.19 5.06 -2 -4 10 119.15 4.20 -2 -4 10 121.04 5.49 2 -4 -10 118.65 4.64 2 -4 -10 118.88 5.43 2 4 -10 123.99 5.67 -2 4 9 65.55 3.38 -2 -4 9 59.10 3.38 2 -4 -9 63.14 2.96 2 -4 -9 62.32 3.29 2 4 -9 72.75 3.74 2 4 -8 647.75 11.78 -2 4 8 675.58 14.23 -2 -4 8 704.47 14.84 2 -4 -8 715.99 14.05 2 -4 -8 700.86 14.14 2 4 -8 721.78 15.02 2 4 -7 47.62 1.63 -2 4 7 53.52 2.81 -2 -4 7 50.83 2.89 2 -4 -7 54.45 2.56 2 4 -7 51.38 2.88 2 4 -6 181.28 2.78 -2 4 6 198.23 4.93 -2 -4 6 197.56 4.96 2 -4 -6 201.72 4.54 2 -4 -6 193.06 4.08 2 4 -6 195.96 4.76 2 4 -5 337.15 4.57 -2 4 5 366.07 6.90 -2 -4 5 359.31 6.83 2 -4 -5 376.88 6.66 2 -4 -5 370.87 5.23 2 4 -5 361.36 6.58 -2 4 4 340.04 6.44 2 4 -4 334.90 4.80 -2 -4 4 358.91 6.53 2 -4 -4 361.95 6.48 2 -4 -4 363.29 4.38 2 4 -4 344.63 6.20 -2 4 3 70.68 2.81 2 4 -3 73.26 2.26 -2 -4 3 74.00 2.65 2 -4 -3 76.77 2.90 2 -4 -3 70.99 0.95 2 4 -3 67.50 2.60 -2 4 2 148.43 3.92 2 4 -2 156.94 3.48 -2 -4 2 159.61 3.55 2 -4 -2 154.64 4.04 -2 4 2 141.64 1.27 2 4 -2 156.92 3.85 -2 4 1 84.85 3.12 2 4 -1 97.36 3.13 -2 -4 1 90.95 2.53 2 -4 -1 99.41 3.42 -2 4 1 94.88 1.82 -2 4 0 398.93 8.19 2 4 0 402.11 7.20 -2 -4 0 360.06 5.21 2 -4 0 383.57 7.05 -2 -4 0 408.97 9.44 -2 4 0 405.89 5.63 -2 4 -1 12.47 2.55 2 4 1 14.75 1.73 2 -4 1 12.08 1.45 -2 -4 -1 11.59 0.90 -2 -4 -1 12.05 1.82 -2 4 -1 14.10 1.40 -2 4 -2 138.94 4.32 2 4 2 151.92 4.84 2 -4 2 124.87 4.11 -2 -4 -2 142.47 4.65 2 4 3 3.02 1.19 2 -4 3 4.15 1.34 2 -4 3 1.86 0.84 -2 -4 -3 2.59 1.11 -2 4 -3 2.04 0.95 2 4 4 40.06 3.25 2 -4 4 38.75 3.00 2 -4 4 29.56 2.46 -2 -4 -4 33.48 2.99 -2 4 -4 38.22 2.72 2 4 5 39.26 3.27 2 -4 5 39.79 2.94 2 -4 5 36.76 2.65 -2 -4 -5 30.60 3.00 -2 4 -5 39.78 3.07 2 4 6 79.72 4.78 2 -4 6 73.12 4.18 2 -4 6 60.95 3.40 -2 -4 -6 64.73 4.24 -2 4 -6 68.80 4.16 2 4 7 1.18 1.29 2 -4 7 0.72 1.43 2 -4 7 0.56 0.79 -2 -4 -7 1.39 1.73 -2 4 -7 0.38 1.05 2 4 8 -0.63 1.20 2 -4 8 1.72 1.18 2 -4 8 0.52 0.78 -2 -4 -8 0.87 1.34 -2 4 -8 0.21 1.10 2 4 9 -0.47 1.31 2 -4 9 0.33 1.12 2 -4 9 0.27 0.77 -2 -4 -9 3.38 2.44 -2 4 -9 1.38 1.29 2 4 10 14.15 3.13 2 -4 10 14.86 2.60 2 -4 10 10.27 2.19 -2 -4 -10 12.63 3.07 -2 4 -10 16.39 3.10 2 4 11 6.21 2.39 2 -4 11 9.86 2.70 -2 -4 -11 5.31 1.99 -2 4 -11 4.91 2.09 2 4 12 8.59 2.84 2 -4 12 9.01 3.32 -2 -4 -12 9.99 3.12 -2 4 -12 7.10 2.43 -2 5 18 1.57 1.61 2 -5 -18 -0.62 1.48 2 5 -18 2.21 1.84 -2 5 17 -0.22 1.15 -2 -5 17 3.03 1.94 2 -5 -17 3.44 2.22 2 5 -17 3.15 2.96 -2 5 16 6.41 2.43 -2 -5 16 8.13 2.17 2 -5 -16 6.23 2.26 2 5 -16 8.91 2.85 -2 5 15 61.51 5.07 -2 -5 15 55.90 4.51 2 -5 -15 49.58 4.73 2 5 -15 61.04 5.34 -2 5 14 4.73 1.79 -2 -5 14 3.81 1.53 -2 -5 14 2.97 1.65 2 -5 -14 11.24 2.88 2 5 -14 6.81 2.52 -2 5 13 0.46 1.14 -2 -5 13 0.97 1.12 -2 5 13 0.55 0.55 -2 -5 13 0.49 1.17 2 -5 -13 3.73 2.27 2 5 -13 0.26 1.24 -2 5 12 17.25 2.82 -2 5 12 8.04 4.04 -2 -5 12 14.85 2.58 2 -5 -12 31.70 4.02 2 5 -12 17.68 2.73 2 5 -11 1.01 0.56 -2 5 11 3.15 1.77 2 -5 -11 0.95 0.88 2 -5 -11 8.29 2.55 2 5 -10 19.07 4.52 -2 5 10 29.73 2.91 -2 -5 10 32.54 3.08 2 -5 -10 27.42 2.16 2 -5 -10 28.65 2.82 2 5 -10 29.47 2.83 -2 5 9 17.07 2.14 -2 -5 9 15.91 2.23 2 -5 -9 16.14 1.67 2 -5 -9 16.34 1.99 2 5 -9 18.08 2.21 2 5 -8 26.89 1.57 -2 5 8 33.46 2.71 -2 -5 8 31.40 2.68 2 -5 -8 32.46 2.29 2 -5 -8 29.81 2.32 2 5 -8 30.50 2.43 2 5 -7 130.85 2.93 -2 5 7 125.95 4.65 -2 -5 7 144.84 4.85 2 -5 -7 146.19 4.24 2 -5 -7 152.50 4.75 2 5 -7 137.11 4.42 2 5 -6 7.02 2.08 -2 -5 6 2.55 1.13 2 -5 -6 2.03 1.07 2 -5 -6 2.40 1.22 2 5 -6 3.91 1.13 2 5 -5 1029.85 18.81 -2 5 5 968.76 18.86 -2 -5 5 1005.01 19.04 2 -5 -5 1036.37 19.23 2 -5 -5 1018.39 17.45 2 5 -5 981.99 18.34 -2 5 4 210.32 5.43 2 5 -4 213.81 4.55 -2 -5 4 207.49 5.02 2 -5 -4 208.99 5.19 2 -5 -4 198.88 2.76 2 5 -4 212.38 5.06 -2 5 3 2.66 0.99 2 5 -3 2.99 0.80 -2 -5 3 4.53 1.05 2 -5 -3 2.96 1.18 2 -5 -3 2.65 0.42 2 5 -3 2.73 0.95 -2 5 2 10.27 1.50 2 5 -2 12.16 1.34 -2 -5 2 12.22 1.70 2 -5 -2 12.79 1.74 -2 5 2 10.59 0.63 2 5 -2 10.90 1.34 -2 5 1 17.37 1.80 2 5 -1 21.10 1.88 -2 -5 1 12.59 1.24 2 -5 -1 14.52 1.79 -2 5 1 17.00 0.96 2 5 -1 17.86 1.75 -2 5 0 6.93 1.36 2 5 0 6.28 1.38 -2 -5 0 6.34 1.03 -2 5 0 6.42 0.86 -2 5 -1 154.29 5.51 2 5 1 166.65 5.57 2 -5 1 151.58 5.23 -2 -5 -1 145.74 3.85 -2 -5 -1 159.50 5.36 -2 5 -1 162.94 4.36 -2 5 -2 638.06 16.53 2 5 2 618.06 14.08 2 -5 2 608.95 13.71 -2 -5 -2 579.48 11.05 -2 -5 -2 646.28 14.44 -2 5 -2 646.69 13.24 -2 5 -3 180.84 6.74 2 5 3 197.08 6.81 2 -5 3 181.43 6.15 -2 -5 -3 192.20 4.34 -2 -5 -3 193.66 6.82 -2 5 -3 199.00 6.02 -2 5 -4 31.15 2.72 2 5 4 37.41 3.27 2 -5 4 34.46 2.65 -2 -5 -4 38.61 3.34 -2 5 -4 38.74 2.69 2 5 5 39.83 3.41 2 -5 5 34.94 2.96 2 -5 5 33.04 2.84 -2 -5 -5 27.48 2.89 -2 5 -5 31.01 2.65 2 5 6 -0.31 1.27 2 -5 6 -0.24 0.94 2 -5 6 0.60 0.83 -2 -5 -6 0.58 1.22 -2 5 -6 0.41 0.95 2 5 7 60.41 4.59 2 -5 7 54.45 3.86 2 -5 7 64.49 3.94 -2 -5 -7 58.15 4.51 -2 5 -7 59.45 4.17 2 5 8 37.49 4.00 2 -5 8 32.46 3.22 -2 -5 -8 37.71 3.90 -2 5 -8 37.15 3.90 2 5 9 174.01 7.82 2 -5 9 168.68 6.92 2 -5 9 146.97 5.94 -2 -5 -9 153.15 7.78 -2 5 -9 171.80 7.43 2 5 10 4.06 2.56 2 -5 10 2.12 1.82 2 -5 10 2.15 1.52 -2 -5 -10 0.53 1.54 -2 5 -10 2.24 1.91 2 5 11 9.44 3.24 2 -5 11 8.97 2.70 -2 -5 -11 12.38 3.47 -2 5 -11 12.26 3.30 2 5 12 -0.50 1.57 2 -5 12 0.75 1.39 -2 -5 -12 1.36 2.19 -2 5 -12 1.36 1.53 -2 6 17 20.15 3.55 -2 -6 17 14.99 2.88 2 -6 -17 15.49 4.05 2 6 -17 20.10 3.82 -2 6 16 11.10 3.08 2 -6 -16 13.57 3.32 2 6 -16 8.78 2.99 -2 6 15 39.66 4.52 -2 -6 15 33.56 3.94 2 -6 -15 38.18 4.82 2 6 -15 37.91 4.37 -2 6 14 6.10 2.24 -2 -6 14 7.78 2.46 2 -6 -14 5.80 2.29 2 6 -14 7.27 2.49 -2 6 13 144.42 6.86 -2 -6 13 151.26 6.76 2 -6 -13 125.11 6.38 2 6 -13 148.65 6.77 -2 6 12 77.30 4.81 -2 -6 12 75.52 4.74 2 -6 -12 71.65 3.50 2 -6 -12 67.19 4.50 2 6 -12 79.35 4.76 2 6 -11 16.91 5.64 -2 6 11 27.29 3.24 -2 -6 11 28.83 3.22 2 -6 -11 24.03 2.22 2 -6 -11 22.72 2.89 2 6 -11 31.00 3.25 2 6 -10 2.52 0.95 -2 6 10 2.79 1.63 -2 -6 10 1.19 1.20 2 -6 -10 2.41 1.13 2 -6 -10 3.84 1.61 2 6 -10 3.19 1.35 2 6 -9 7.14 1.11 -2 6 9 8.19 1.95 -2 -6 9 6.44 1.70 2 -6 -9 9.96 1.67 2 -6 -9 10.42 1.82 2 6 -9 8.78 1.80 2 6 -8 3.18 0.82 -2 6 8 3.47 1.30 -2 -6 8 4.69 1.46 2 -6 -8 5.46 1.36 2 -6 -8 3.74 1.23 2 6 -8 3.72 1.15 2 6 -7 13.35 1.25 -2 6 7 17.87 2.23 -2 -6 7 16.22 2.11 2 -6 -7 16.32 1.91 2 -6 -7 17.46 1.74 2 6 -7 17.54 2.00 2 6 -6 30.92 1.73 -2 -6 6 33.58 2.62 2 -6 -6 31.04 2.29 2 -6 -6 32.01 1.85 2 6 -6 33.65 2.39 -2 6 5 133.65 5.38 2 6 -5 131.80 3.35 -2 -6 5 144.51 4.73 2 -6 -5 139.45 4.35 2 -6 -5 139.76 3.12 2 6 -5 139.61 4.30 -2 6 4 58.86 4.82 2 6 -4 35.14 2.64 -2 -6 4 44.08 2.66 2 -6 -4 39.28 2.59 2 -6 -4 41.16 1.55 2 6 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2 7 9 49.92 4.83 2 -7 9 50.73 4.21 -2 -7 -9 40.04 4.21 -2 7 -9 47.52 4.37 -2 7 -10 4.75 2.32 2 7 10 14.55 3.63 2 -7 10 8.15 2.51 -2 -7 -10 4.45 2.53 -2 7 -10 11.15 2.77 2 7 11 11.17 2.86 -2 -7 -11 13.85 3.80 -2 7 -11 12.87 3.02 -2 8 16 18.96 3.96 -2 -8 16 12.68 3.13 2 -8 -16 11.55 3.26 2 8 -16 10.19 3.34 -2 8 15 5.42 2.68 -2 -8 15 1.77 1.62 2 -8 -15 3.76 1.87 2 8 -15 4.22 2.35 -2 8 14 19.22 3.63 -2 -8 14 13.92 2.88 2 -8 -14 17.87 3.36 2 8 -14 15.73 3.10 -2 8 13 11.34 2.75 -2 -8 13 9.74 2.66 2 -8 -13 4.32 1.49 2 -8 -13 9.38 2.59 2 8 -13 11.89 2.85 -2 8 12 51.90 4.36 -2 -8 12 55.04 4.50 2 -8 -12 54.06 3.52 2 -8 -12 59.29 4.45 2 8 -12 53.43 4.26 2 8 -11 0.40 0.77 -2 8 11 2.65 1.74 -2 -8 11 4.29 2.09 2 -8 -11 1.86 1.07 2 -8 -11 5.76 1.91 2 8 -11 4.37 1.95 -2 8 10 11.33 2.66 -2 -8 10 7.78 2.35 2 -8 -10 5.57 1.56 2 -8 -10 3.34 1.46 2 8 -10 11.30 2.21 2 8 -9 350.24 6.81 -2 8 9 350.27 9.41 -2 -8 9 389.36 10.03 2 -8 -9 383.94 8.38 2 8 -9 382.10 9.07 2 8 -8 95.84 3.61 -2 8 8 99.48 5.22 -2 -8 8 95.40 5.03 2 -8 -8 100.40 4.47 2 8 -8 102.87 4.61 -2 8 7 90.84 4.73 -2 -8 7 82.31 4.53 2 -8 -7 83.40 3.97 2 8 -7 81.62 4.02 2 8 -6 5.02 1.35 -2 8 6 10.63 2.53 -2 -8 6 7.13 1.96 2 -8 -6 6.95 1.58 2 8 -6 6.00 1.44 2 8 -5 1.75 1.23 -2 8 5 6.07 2.13 -2 -8 5 -0.09 0.97 2 -8 -5 0.08 0.88 2 -8 -5 0.28 0.39 2 8 -5 0.36 0.75 -2 8 4 14.75 2.39 2 8 -4 14.12 1.69 -2 -8 4 16.28 2.13 2 -8 -4 11.74 1.85 2 -8 -4 15.72 1.31 2 8 -4 13.93 1.83 -2 8 3 45.98 3.38 2 8 -3 47.71 2.94 -2 -8 3 49.22 3.37 2 -8 -3 47.77 3.33 2 -8 -3 41.45 1.77 2 8 -3 48.36 2.99 -2 8 2 34.87 2.75 2 8 -2 38.27 2.62 -2 -8 2 37.73 2.79 2 -8 -2 37.20 2.92 2 8 -2 33.84 2.44 -2 8 1 11.74 1.94 2 8 -1 10.99 1.58 -2 -8 1 11.26 1.71 2 -8 -1 15.19 2.17 -2 -8 1 11.32 1.89 -2 8 1 10.61 1.04 -2 8 0 18.96 2.27 2 8 0 18.79 2.33 -2 -8 0 19.74 2.05 2 -8 0 22.53 2.57 -2 -8 0 17.09 1.94 -2 8 0 18.90 1.42 -2 8 -1 17.23 2.24 2 8 1 19.15 2.50 2 -8 1 17.08 2.47 -2 -8 -1 15.01 1.74 -2 -8 -1 18.75 4.51 -2 8 -1 18.25 1.50 -2 8 -2 3.01 1.52 2 8 2 1.33 1.12 2 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3.10 2.18 2 9 -15 0.73 1.25 -2 9 14 0.66 1.47 -2 -9 14 0.82 1.40 2 -9 -14 0.92 1.54 2 9 -14 4.30 2.30 -2 9 13 6.17 2.78 -2 -9 13 3.36 2.04 2 -9 -13 3.13 2.01 2 9 -13 4.79 1.88 -2 9 12 15.44 3.23 -2 -9 12 9.08 3.04 2 -9 -12 7.09 1.82 2 -9 -12 5.00 1.57 2 9 -12 6.35 1.89 -2 9 11 312.60 10.24 -2 -9 11 314.04 9.97 2 -9 -11 306.73 8.08 2 -9 -11 308.33 8.77 2 9 -11 313.97 9.22 2 9 -10 13.46 1.93 -2 9 10 16.21 2.91 -2 -9 10 18.56 3.01 2 -9 -10 17.32 2.32 2 -9 -10 15.68 2.57 2 9 -10 18.41 2.63 2 9 -9 12.35 1.91 -2 9 9 15.04 2.74 -2 -9 9 19.73 3.21 2 -9 -9 19.62 2.59 2 -9 -9 15.65 2.37 2 9 -9 19.36 2.75 -2 9 8 4.57 1.78 -2 -9 8 5.76 1.98 2 -9 -8 3.47 1.31 2 -9 -8 7.09 1.62 2 9 -8 4.99 1.79 2 9 -7 3.38 1.17 -2 9 7 6.04 2.15 -2 -9 7 6.63 2.16 2 -9 -7 5.16 1.44 2 -9 -7 7.08 1.30 2 9 -7 8.01 1.99 2 9 -6 2.30 1.26 -2 9 6 5.05 2.01 -2 -9 6 1.27 1.24 2 -9 -6 0.83 0.95 2 -9 -6 0.96 0.71 2 9 -6 0.11 0.83 -2 9 5 27.06 3.08 2 9 -5 32.01 2.43 -2 -9 5 32.21 3.00 2 -9 -5 31.14 2.94 2 -9 -5 30.76 1.92 2 9 -5 33.44 2.73 -2 9 4 18.64 2.66 2 9 -4 21.84 2.19 -2 -9 4 25.96 2.74 2 -9 -4 22.66 2.73 2 -9 -4 20.39 1.54 2 9 -4 20.12 2.21 -2 9 3 135.52 5.49 2 9 -3 146.58 4.90 -2 -9 3 152.27 5.55 2 -9 -3 150.36 5.64 2 -9 -3 137.67 3.21 2 9 -3 151.82 5.07 -2 9 2 6.85 1.91 2 9 -2 7.46 1.74 -2 -9 2 6.16 1.77 2 -9 -2 6.27 1.72 2 -9 -2 4.74 0.91 2 9 -2 7.60 1.59 -2 9 1 24.95 2.64 2 9 -1 31.23 2.84 -2 -9 1 27.58 2.64 2 -9 -1 26.21 2.93 -2 -9 1 26.51 5.26 -2 9 1 24.12 1.55 -2 9 0 15.89 2.22 2 9 0 13.19 2.05 -2 -9 0 14.61 1.90 2 -9 0 14.30 2.36 -2 -9 0 15.47 3.41 -2 9 0 14.09 1.32 -2 9 -1 2.12 1.31 2 9 1 1.80 1.54 2 -9 1 3.09 1.87 -2 -9 -1 3.22 1.21 -2 -9 -1 1.34 0.81 -2 9 -1 2.70 0.89 -2 9 -2 16.32 2.30 2 9 2 21.36 2.65 2 -9 2 19.03 2.80 -2 -9 -2 15.18 1.75 -2 -9 -2 17.82 2.36 -2 9 -2 18.29 1.78 -2 9 -3 12.44 2.19 2 9 3 13.46 2.40 2 -9 3 13.02 2.59 -2 -9 -3 10.45 1.61 -2 -9 -3 12.93 2.22 -2 9 -3 11.33 1.61 -2 9 -4 2.78 1.52 2 9 4 2.39 1.31 2 -9 4 0.47 1.21 -2 -9 -4 3.07 1.19 -2 -9 -4 2.93 1.71 -2 9 -4 2.78 1.21 -2 9 -5 2.58 1.41 2 9 5 3.24 2.17 2 -9 5 1.34 1.35 -2 -9 -5 0.92 1.20 -2 9 -5 1.42 0.74 -2 9 -6 2.23 1.42 2 9 6 1.26 1.47 2 -9 6 1.00 1.73 -2 -9 -6 1.08 1.25 -2 9 -6 2.91 1.44 -2 9 -7 71.14 4.94 2 9 7 80.45 5.96 2 -9 7 76.70 5.25 -2 -9 -7 77.15 5.39 -2 9 -7 70.69 4.45 -2 9 -8 17.61 2.98 2 9 8 21.24 3.94 2 -9 8 18.28 3.17 -2 -9 -8 15.30 2.98 -2 9 -8 16.92 2.79 -2 9 -9 1.44 1.21 2 9 9 6.84 2.96 -2 -9 -9 7.17 2.84 -2 9 -9 3.21 1.98 2 9 10 14.78 3.67 2 -9 10 12.72 3.33 -2 -9 -10 14.77 3.77 -2 9 -10 14.76 3.27 -2 10 15 35.41 5.09 -2 -10 15 26.37 4.57 2 -10 -15 27.10 3.92 2 10 -15 30.47 3.98 -2 10 14 1.20 1.80 -2 -10 14 1.79 2.42 2 -10 -14 0.02 1.37 2 10 -14 1.03 1.32 -2 10 13 1.93 1.70 -2 -10 13 -0.13 1.32 2 -10 -13 -0.68 1.13 2 10 -13 0.30 1.14 -2 10 12 1.92 2.11 -2 -10 12 0.03 1.32 2 -10 -12 1.49 1.21 2 -10 -12 2.52 2.04 2 10 -12 0.83 1.20 -2 10 11 72.49 5.66 -2 -10 11 85.15 5.82 2 -10 -11 78.54 4.49 2 -10 -11 71.15 4.63 2 10 -11 76.06 4.87 -2 10 10 11.69 2.80 -2 -10 10 8.63 2.71 2 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0.71 0.83 2 -10 0 1.03 1.19 -2 -10 0 1.96 1.07 -2 10 0 2.29 0.96 -2 10 -1 83.86 4.82 2 10 1 74.05 4.53 -2 -10 -1 76.57 3.92 2 -10 1 78.38 4.89 -2 -10 -1 78.76 4.37 -2 10 -1 73.52 2.97 -2 10 -2 2.66 1.19 2 10 2 6.08 2.41 2 -10 2 5.92 2.11 -2 -10 -2 4.06 1.39 -2 -10 -2 3.68 1.62 -2 10 -2 1.14 0.69 -2 10 -3 3.20 1.59 2 10 3 6.73 2.03 2 -10 3 9.16 2.51 -2 -10 -3 4.51 1.38 -2 -10 -3 4.68 1.66 -2 10 -3 5.08 1.36 -2 10 -4 53.29 3.92 2 10 4 57.59 4.71 2 -10 4 49.52 4.38 -2 -10 -4 51.56 3.23 -2 -10 -4 46.71 4.01 -2 10 -4 47.28 3.14 -2 10 -5 64.37 4.46 2 10 5 74.03 5.50 2 -10 5 66.97 5.10 -2 -10 -5 64.69 5.02 -2 10 -5 70.66 4.14 2 10 6 26.75 4.02 2 -10 6 20.40 3.38 -2 -10 -6 21.97 3.63 -2 10 -6 22.19 2.63 -2 10 -7 5.79 2.47 2 10 7 6.59 2.57 2 -10 7 5.43 2.11 -2 -10 -7 10.14 2.92 -2 10 -7 4.21 1.74 -2 10 -8 18.65 3.20 2 10 8 21.65 3.68 2 -10 8 24.29 3.85 -2 -10 -8 24.68 4.25 -2 10 -8 22.65 3.17 -2 10 -9 19.19 3.28 2 10 9 33.36 4.95 2 -10 9 30.27 4.07 -2 -10 -9 34.92 4.60 -2 11 14 23.92 4.18 -2 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4.90 1.88 2 -11 -3 4.85 1.94 2 11 -3 6.76 1.69 -2 11 2 51.73 4.37 2 11 -2 60.84 4.05 -2 -11 2 49.39 3.68 2 -11 -2 59.74 4.25 -2 11 1 -0.08 1.19 2 11 -1 4.51 1.89 -2 -11 1 0.91 1.01 2 -11 -1 1.30 1.34 -2 -11 1 1.30 0.89 -2 11 0 7.94 2.29 2 11 0 5.29 2.04 2 -11 0 5.50 2.04 -2 -11 0 5.82 1.45 -2 -11 0 4.56 0.89 -2 11 -1 14.38 2.55 2 11 1 17.18 2.83 2 -11 1 11.07 2.47 -2 -11 -1 13.41 2.23 -2 -11 -1 16.54 2.48 -2 11 -2 10.01 2.25 2 11 2 10.16 2.41 2 -11 2 10.43 2.84 -2 -11 -2 12.79 2.08 -2 -11 -2 10.63 2.10 -2 11 -3 15.83 2.56 2 11 3 16.15 3.17 2 -11 3 17.32 3.38 -2 -11 -3 15.03 2.42 -2 -11 -3 15.38 2.77 -2 11 -4 10.17 2.40 2 11 4 11.35 2.99 2 -11 4 15.21 3.40 -2 -11 -4 13.05 2.82 2 11 5 1.21 2.07 2 -11 5 1.74 1.49 -2 -11 -5 0.17 1.23 -2 11 -6 0.02 1.02 2 11 6 6.58 2.76 2 -11 6 0.43 1.39 -2 -11 -6 1.52 1.70 -2 11 -7 0.04 1.13 2 11 7 1.32 1.54 2 -11 7 -0.54 1.34 -2 -11 -7 -0.29 1.20 2 11 8 1.23 1.68 2 -11 8 2.18 1.56 -2 -11 -8 3.49 2.14 2 11 9 7.93 3.57 2 -11 9 9.86 3.76 -2 -11 -9 4.47 2.56 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0 2.24 0.99 -4 -3 0 2.23 1.41 -4 3 0 3.13 1.13 4 3 1 28.90 2.68 4 -3 1 33.19 2.94 4 -3 1 29.18 2.24 -4 -3 -1 30.54 3.29 -4 3 -1 27.83 2.47 4 3 2 12.49 2.16 4 -3 2 22.22 2.62 4 -3 2 11.40 1.60 -4 -3 -2 17.39 2.77 -4 3 -2 16.00 2.22 4 3 3 21.01 2.78 4 -3 3 23.60 2.76 4 -3 3 21.00 2.03 -4 -3 -3 21.79 2.80 -4 3 -3 22.32 2.47 4 3 4 164.97 7.00 4 -3 4 155.74 6.62 4 -3 4 127.27 4.52 -4 -3 -4 141.95 6.59 -4 3 -4 151.62 6.26 4 3 5 136.85 6.84 4 -3 5 115.60 5.85 -4 -3 -5 124.20 6.51 -4 3 -5 130.14 6.20 4 3 6 8.58 2.67 4 -3 6 7.22 2.44 -4 -3 -6 7.42 2.61 -4 3 -6 10.44 2.70 4 3 7 5.91 2.29 4 -3 7 7.45 2.53 -4 -3 -7 1.09 1.48 -4 3 -7 3.70 2.16 4 3 8 38.86 4.42 4 -3 8 36.11 4.37 -4 -3 -8 30.12 4.08 -4 3 -8 31.04 3.83 4 3 9 4.08 2.68 4 -3 9 1.63 1.65 -4 -3 -9 3.58 2.22 -4 3 -9 2.23 2.18 -4 -3 -10 16.94 4.00 -4 3 -10 19.51 4.09 -4 4 20 0.65 1.20 -4 -4 20 2.49 1.86 4 -4 -20 2.58 2.15 4 4 -20 4.81 2.45 -4 4 19 16.37 3.17 4 -4 -19 16.61 3.34 4 4 -19 17.99 3.61 -4 4 18 19.15 3.11 -4 4 18 8.15 1.69 -4 -4 18 13.53 2.97 4 -4 -18 13.61 3.21 4 4 -18 13.40 2.76 -4 4 17 8.42 2.40 -4 4 17 5.16 1.64 -4 -4 17 10.16 2.77 4 -4 -17 9.43 2.59 4 4 -17 9.27 2.76 -4 4 16 12.48 2.38 -4 -4 16 13.62 2.62 4 -4 -16 4.41 2.12 4 4 -16 9.11 2.39 -4 4 15 0.58 1.03 -4 4 15 1.22 0.76 -4 -4 15 0.66 1.13 4 -4 -15 0.55 1.15 4 4 -15 3.28 1.83 -4 4 14 11.45 2.07 -4 4 14 5.08 2.39 -4 -4 14 14.06 2.60 4 -4 -14 2.00 1.46 4 4 -14 12.57 2.25 -4 4 13 22.34 2.51 -4 -4 13 16.64 2.36 4 -4 -13 17.16 2.15 4 4 -13 17.86 2.50 -4 4 12 41.35 3.03 -4 -4 12 31.29 2.95 4 -4 -12 35.84 2.70 4 -4 -12 39.33 2.77 4 4 -12 33.25 2.89 -4 4 11 31.12 2.48 -4 -4 11 32.99 2.82 4 -4 -11 27.15 2.36 4 -4 -11 25.73 2.21 4 4 -11 31.38 2.78 -4 4 10 223.63 6.83 -4 -4 10 208.39 6.87 4 -4 -10 222.25 6.81 4 -4 -10 233.03 6.32 4 4 -10 210.48 6.89 -4 4 9 40.92 3.10 -4 -4 9 48.16 2.92 4 -4 -9 46.49 2.84 4 -4 -9 38.99 1.96 4 4 -9 41.06 2.77 4 4 -8 229.34 4.07 -4 -4 8 240.01 6.91 4 -4 -8 247.26 6.98 4 -4 -8 219.11 5.00 4 4 -8 231.21 6.77 -4 4 7 591.14 12.59 4 4 -7 562.11 9.89 -4 -4 7 554.74 11.86 4 -4 -7 573.36 12.37 4 -4 -7 529.91 9.38 4 4 -7 545.32 11.91 -4 4 6 106.07 3.80 4 4 -6 119.16 2.77 -4 -4 6 115.61 3.73 4 -4 -6 122.94 4.23 4 4 -6 112.61 3.98 4 -4 -6 111.56 1.55 -4 4 5 86.70 3.47 4 4 -5 82.63 2.72 -4 -4 5 84.99 3.02 4 -4 -5 89.10 3.60 4 4 -5 88.87 3.59 -4 4 4 296.95 7.80 4 4 -4 311.13 7.33 -4 -4 4 314.82 7.16 4 -4 -4 298.18 7.70 -4 4 4 297.48 5.43 4 4 -4 316.26 8.14 -4 4 3 19.83 4.00 4 4 -3 18.54 1.85 -4 -4 3 19.26 1.34 4 -4 -3 16.87 1.76 -4 -4 3 19.85 2.27 -4 4 3 23.50 1.29 -4 4 2 100.13 5.56 4 4 -2 101.48 3.91 -4 -4 2 83.82 2.40 4 -4 -2 88.75 3.60 -4 -4 2 105.68 7.33 -4 4 2 98.78 2.75 -4 4 1 119.69 4.95 4 4 -1 140.46 5.36 -4 -4 1 113.91 2.92 4 -4 -1 119.41 4.54 -4 -4 1 125.33 7.92 -4 4 1 125.35 4.15 4 4 0 274.05 8.36 4 -4 0 277.98 8.40 4 -4 0 230.24 6.87 -4 -4 0 271.02 8.40 -4 4 0 269.53 7.20 4 4 1 9.76 1.88 4 -4 1 10.10 2.02 4 -4 1 8.40 1.50 -4 -4 -1 10.60 2.26 -4 4 -1 9.29 1.77 4 4 2 2.78 2.13 4 -4 2 1.82 1.57 4 -4 2 0.09 0.61 -4 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15 84.73 5.06 -4 -5 15 76.14 4.81 4 -5 -15 83.62 4.85 4 5 -15 87.67 5.36 -4 5 14 58.55 4.06 -4 -5 14 53.89 4.23 4 -5 -14 49.18 3.42 4 5 -14 58.04 4.26 -4 5 13 159.66 5.89 -4 -5 13 166.12 6.39 4 -5 -13 154.36 5.38 4 -5 -13 161.37 5.53 4 5 -13 157.32 6.27 -4 5 12 22.65 2.60 -4 -5 12 23.89 2.77 4 -5 -12 24.73 2.63 4 -5 -12 23.24 2.21 4 5 -12 23.21 2.85 -4 5 11 134.75 5.72 -4 -5 11 118.06 5.66 4 -5 -11 126.48 5.52 4 -5 -11 135.93 5.22 4 5 -11 120.07 5.70 -4 5 10 23.40 2.41 -4 -5 10 24.60 2.45 4 -5 -10 26.88 2.37 4 -5 -10 25.72 1.85 4 5 -10 25.77 2.45 -4 5 9 2.15 0.95 -4 -5 9 3.34 1.30 4 -5 -9 4.53 1.24 4 -5 -9 3.20 0.79 4 5 -9 4.84 1.29 -4 5 8 15.62 1.93 4 5 -8 16.48 0.97 -4 -5 8 16.93 1.84 4 -5 -8 17.55 2.02 4 -5 -8 15.58 1.17 4 5 -8 15.41 1.79 -4 5 7 9.05 2.03 4 5 -7 10.33 1.03 -4 -5 7 9.81 1.46 4 -5 -7 12.02 1.99 4 -5 -7 9.09 0.71 4 5 -7 9.20 1.62 -4 5 6 75.34 3.61 4 5 -6 80.18 2.54 -4 -5 6 81.80 3.41 4 -5 -6 78.71 3.58 4 5 -6 77.84 3.46 -4 5 5 45.35 2.89 4 5 -5 51.77 2.33 -4 -5 5 51.38 2.70 4 -5 -5 53.93 3.11 4 5 -5 49.22 2.90 -4 5 4 107.56 4.27 4 5 -4 109.57 3.58 -4 -5 4 110.49 3.50 4 -5 -4 111.50 4.17 4 5 -4 108.40 4.21 -4 5 3 0.10 0.80 4 5 -3 0.63 0.70 -4 -5 3 0.79 0.72 4 -5 -3 0.09 0.78 -4 -5 3 1.74 1.09 -4 5 3 0.68 0.40 -4 5 2 26.97 7.52 4 5 -2 26.68 2.47 -4 -5 2 20.56 1.43 4 -5 -2 21.83 2.18 -4 -5 2 23.12 6.29 -4 5 2 22.94 1.44 -4 5 1 13.72 4.06 4 5 -1 12.14 1.91 -4 -5 1 12.78 1.12 4 -5 -1 13.52 1.96 -4 -5 1 12.93 4.08 -4 5 1 11.40 1.21 -4 5 0 2.93 1.06 4 5 0 2.13 1.30 4 -5 0 2.80 1.17 -4 -5 0 4.04 1.68 -4 5 0 2.16 0.79 -4 5 -1 59.24 3.94 4 5 1 59.64 3.92 4 -5 1 67.84 3.70 -4 -5 -1 54.30 3.99 -4 5 -1 71.22 3.39 4 5 2 4.32 1.84 4 -5 2 2.23 1.02 -4 -5 -2 3.77 1.90 -4 5 -2 4.59 1.28 4 5 3 17.76 2.51 4 -5 3 17.33 2.55 4 -5 3 18.66 2.24 -4 -5 -3 20.65 2.99 -4 5 -3 17.77 2.34 4 5 4 53.06 4.59 4 -5 4 49.75 3.98 4 -5 4 47.04 3.25 -4 -5 -4 46.91 4.21 -4 5 -4 54.46 3.85 4 5 5 13.40 2.97 4 -5 5 9.01 2.27 4 -5 5 11.01 2.05 -4 -5 -5 11.53 3.22 -4 5 -5 12.41 2.44 4 5 6 1.62 1.59 4 -5 6 4.09 2.26 4 -5 6 3.52 1.68 -4 -5 -6 1.52 2.09 -4 5 -6 3.33 1.79 4 5 7 15.52 3.63 4 -5 7 15.49 3.36 -4 -5 -7 16.53 3.92 -4 5 -7 14.61 3.02 4 5 8 12.99 3.24 4 -5 8 12.55 2.96 -4 -5 -8 10.22 3.47 -4 5 -8 11.41 2.64 4 5 9 1.79 2.39 4 -5 9 1.04 1.47 -4 -5 -9 0.54 1.64 -4 5 -9 0.57 1.41 -4 6 20 2.11 2.27 -4 -6 20 1.56 1.39 4 -6 -20 4.34 2.31 4 6 -20 1.67 1.74 -4 6 19 1.44 1.41 -4 -6 19 1.09 2.05 4 -6 -19 0.81 1.45 4 6 -19 1.39 1.69 -4 6 18 26.35 3.97 -4 -6 18 21.45 3.76 4 -6 -18 25.97 3.62 4 6 -18 28.78 4.44 -4 6 17 14.78 2.89 -4 6 17 8.05 3.46 -4 -6 17 12.82 2.80 4 -6 -17 13.35 3.41 4 6 -17 11.09 3.00 -4 6 16 0.55 1.22 -4 6 16 0.31 0.43 -4 -6 16 1.57 1.45 4 -6 -16 0.53 1.51 4 6 -16 3.37 1.85 -4 6 15 24.33 2.94 -4 -6 15 26.94 3.49 4 -6 -15 25.74 2.71 4 -6 -15 19.62 2.74 4 6 -15 27.96 3.33 -4 6 14 3.28 1.84 -4 -6 14 3.22 1.72 4 -6 -14 3.42 1.40 4 6 -14 2.01 1.30 -4 6 13 10.48 2.27 -4 -6 13 8.04 2.20 4 -6 -13 10.12 1.94 4 -6 -13 16.10 2.47 4 6 -13 9.64 2.04 -4 6 12 72.53 4.40 -4 -6 12 75.59 4.62 4 -6 -12 74.26 4.02 4 -6 -12 86.26 3.93 4 6 -12 69.14 4.20 -4 6 11 2.07 1.58 -4 -6 11 0.58 1.06 4 -6 -11 1.64 1.38 4 -6 -11 0.98 0.66 4 6 -11 0.35 0.97 -4 6 10 -0.03 0.90 -4 -6 10 2.57 1.37 4 -6 -10 2.74 1.39 4 -6 -10 1.13 0.62 4 6 -10 2.43 1.24 -4 6 9 6.02 1.77 4 6 -9 4.04 0.63 -4 -6 9 5.48 1.67 4 -6 -9 6.51 1.70 4 6 -9 4.65 1.39 -4 6 8 203.16 6.85 -4 -6 8 206.25 6.97 4 -6 -8 211.38 6.92 4 6 -8 204.61 6.82 -4 6 7 82.51 4.08 4 6 -7 83.69 2.59 -4 -6 7 90.60 3.95 4 -6 -7 94.39 4.18 4 6 -7 83.74 3.84 -4 6 6 500.02 12.25 4 6 -6 485.10 10.30 -4 -6 6 483.32 11.46 4 -6 -6 499.12 12.22 4 6 -6 486.63 11.81 -4 6 5 13.42 2.23 4 6 -5 11.84 1.49 -4 -6 5 10.86 1.65 4 -6 -5 13.71 1.97 4 6 -5 12.85 1.80 -4 6 4 74.72 3.89 4 6 -4 73.74 3.17 -4 -6 4 71.59 3.18 4 -6 -4 84.51 4.11 4 6 -4 70.64 3.61 -4 6 3 10.49 1.65 4 6 -3 10.30 1.56 -4 -6 3 11.75 1.48 4 -6 -3 10.63 1.81 -4 -6 3 10.94 1.94 -4 6 3 10.49 0.68 -4 6 2 -0.21 0.81 4 6 -2 0.89 0.87 -4 -6 2 0.08 0.43 4 -6 -2 1.54 0.98 -4 -6 2 -0.43 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-3 0.96 1.13 -5 -4 3 1.40 0.57 5 -4 -3 1.17 1.06 -5 -4 3 4.06 1.38 -5 4 3 2.93 0.90 -5 4 2 2.48 1.48 5 4 -2 1.42 0.85 -5 -4 2 1.16 0.44 5 -4 -2 0.56 0.66 -5 -4 2 2.56 1.38 -5 4 2 1.21 0.68 5 4 -1 6.64 1.80 5 -4 -1 2.28 1.35 5 -4 -1 3.37 1.27 -5 -4 1 3.88 1.77 -5 4 1 4.34 1.33 5 4 0 2.53 1.44 5 -4 0 2.11 1.81 5 -4 0 3.77 1.30 -5 -4 0 2.80 1.63 -5 4 0 0.86 0.62 5 4 1 55.15 4.02 5 -4 1 62.37 4.32 5 -4 1 53.11 3.17 -5 -4 -1 67.83 4.70 -5 4 -1 61.10 3.68 5 4 2 9.29 2.47 5 -4 2 22.33 3.22 5 -4 2 7.46 1.67 -5 -4 -2 12.90 2.70 -5 4 -2 10.59 2.01 5 4 3 14.11 2.86 5 -4 3 12.97 2.67 5 -4 3 11.63 1.81 -5 -4 -3 10.83 2.92 -5 4 -3 13.87 2.61 5 4 4 1.00 1.47 5 -4 4 -0.11 1.21 5 -4 4 0.05 0.68 -5 -4 -4 1.15 2.03 -5 4 -4 0.57 1.00 5 4 5 1.43 1.60 5 -4 5 1.54 1.54 -5 -4 -5 4.44 2.80 -5 4 -5 1.63 1.46 5 4 6 2.28 1.75 5 -4 6 0.45 1.46 -5 4 -6 -0.33 1.17 5 4 7 0.77 1.62 5 -4 7 1.37 1.67 -5 -4 -7 1.58 1.60 -5 4 -7 0.56 1.26 5 4 8 -0.01 1.52 5 -4 8 1.26 1.67 -5 -4 -8 2.35 2.34 -5 4 -8 1.81 1.58 -5 5 21 0.81 1.30 5 -5 -21 1.27 1.86 5 5 -21 1.29 1.63 -5 5 20 5.73 2.54 -5 -5 20 2.36 1.64 5 -5 -20 6.08 2.35 5 5 -20 5.60 2.24 -5 5 19 15.47 2.79 -5 -5 19 14.02 3.24 5 -5 -19 14.59 2.93 5 5 -19 17.92 3.74 -5 5 18 50.46 4.27 -5 5 18 40.38 3.66 -5 -5 18 52.68 4.67 5 -5 -18 54.32 4.61 5 5 -18 57.69 4.94 -5 5 17 35.49 3.29 -5 -5 17 36.98 4.09 5 -5 -17 38.04 3.77 5 5 -17 36.40 4.15 -5 5 16 70.27 4.50 -5 5 16 52.85 7.47 -5 -5 16 70.22 4.98 5 -5 -16 60.47 4.02 5 5 -16 63.53 4.67 -5 5 15 18.92 2.54 -5 -5 15 20.65 2.65 5 -5 -15 17.97 2.45 5 -5 -15 17.54 2.28 5 5 -15 20.59 3.08 -5 5 14 29.28 2.93 -5 -5 14 26.90 2.99 5 -5 -14 24.81 2.57 5 -5 -14 26.70 2.54 5 5 -14 22.32 2.75 -5 5 13 1.75 1.23 -5 -5 13 1.54 1.07 5 -5 -13 1.23 1.20 5 -5 -13 1.84 0.92 5 5 -13 2.14 1.39 -5 5 12 24.11 2.49 -5 -5 12 21.11 2.52 5 -5 -12 24.73 2.60 5 -5 -12 16.88 1.76 5 5 -12 21.38 2.49 -5 5 11 3.68 1.44 -5 -5 11 5.05 1.76 5 -5 -11 4.49 1.62 5 -5 -11 3.58 0.92 5 5 -11 4.13 1.50 -5 5 10 25.52 2.38 -5 -5 10 27.39 2.57 5 -5 -10 27.23 2.50 5 -5 -10 23.19 1.49 5 5 -10 27.91 2.63 -5 5 9 203.16 6.71 -5 -5 9 201.22 6.69 5 -5 -9 217.79 7.13 5 5 -9 206.62 6.96 -5 5 8 37.31 2.67 5 5 -8 37.45 1.71 -5 -5 8 38.67 2.86 5 -5 -8 40.13 3.07 5 5 -8 36.78 2.83 -5 5 7 13.31 1.99 5 5 -7 11.48 1.31 -5 -5 7 15.64 1.98 5 -5 -7 11.34 1.99 5 5 -7 11.99 1.90 -5 5 6 44.75 3.02 5 5 -6 48.41 2.58 -5 -5 6 44.49 2.60 5 -5 -6 45.89 3.15 5 5 -6 44.56 2.96 -5 5 5 179.87 6.45 5 5 -5 200.56 6.10 -5 -5 5 193.73 5.70 5 -5 -5 193.05 6.58 5 5 -5 193.70 6.70 -5 5 4 98.43 4.96 5 5 -4 95.09 3.86 -5 -5 4 97.60 3.18 5 -5 -4 98.13 4.31 -5 -5 4 106.73 4.62 -5 5 4 102.16 2.35 -5 5 3 20.48 4.46 5 5 -3 21.11 2.21 -5 -5 3 22.56 1.63 5 -5 -3 21.76 2.26 -5 -5 3 22.20 5.52 -5 5 3 19.33 1.47 -5 5 2 32.73 3.93 5 5 -2 33.03 3.02 -5 -5 2 26.55 1.48 5 -5 -2 31.18 2.73 -5 -5 2 35.45 6.50 -5 5 2 31.26 2.02 -5 5 1 7.41 1.73 5 5 -1 3.49 1.63 5 -5 -1 4.13 1.32 -5 -5 1 10.64 2.48 -5 5 1 5.37 1.19 -5 5 0 245.01 7.69 5 5 0 250.53 7.73 5 -5 0 230.60 6.53 -5 -5 0 249.60 7.91 -5 5 0 252.28 6.17 5 5 1 11.80 2.20 5 -5 1 15.01 2.17 -5 -5 -1 15.38 3.06 -5 5 -1 12.20 1.90 5 5 2 56.19 4.59 5 -5 2 62.80 4.71 -5 -5 -2 52.76 4.53 -5 5 -2 58.66 3.91 5 5 3 11.30 2.72 5 -5 3 8.72 2.17 5 -5 3 11.34 2.29 -5 -5 -3 12.23 3.01 -5 5 -3 6.84 1.70 5 5 4 0.92 1.44 5 -5 4 2.21 1.96 5 -5 4 -0.36 0.87 -5 -5 -4 0.27 1.41 -5 5 -4 0.39 0.99 5 -5 5 3.09 2.17 -5 -5 -5 2.02 1.85 -5 5 -5 3.55 2.00 5 5 6 -0.58 1.43 5 -5 6 -1.20 1.47 -5 -5 -6 4.15 2.62 -5 5 -6 0.01 1.23 5 5 7 36.48 4.89 5 -5 7 24.02 4.16 -5 -5 -7 25.45 4.06 -5 5 -7 21.49 3.61 -5 6 21 1.61 2.11 -5 -6 21 0.90 2.11 5 6 -21 0.66 1.51 -5 6 20 -0.07 1.37 -5 -6 20 1.69 1.44 5 6 -20 3.10 2.18 -5 6 19 0.70 1.31 -5 6 19 1.46 0.97 -5 -6 19 3.39 2.18 5 6 -19 1.60 1.61 -5 6 18 1.31 1.21 -5 6 18 0.76 0.98 -5 -6 18 2.85 2.09 -5 6 17 10.00 2.27 -5 6 17 8.15 3.21 -5 -6 17 11.36 3.05 5 6 -17 11.44 2.86 -5 6 16 7.16 1.93 -5 -6 16 4.77 2.33 5 -6 -16 5.53 1.67 5 6 -16 2.85 1.86 -5 6 15 9.27 2.16 -5 -6 15 11.53 2.74 5 -6 -15 10.20 2.16 5 6 -15 9.55 2.37 -5 6 14 2.76 1.24 -5 -6 14 2.62 1.82 5 -6 -14 2.12 1.61 5 -6 -14 1.67 0.94 5 6 -14 5.47 2.23 -5 6 13 8.96 2.09 -5 -6 13 8.05 2.23 5 -6 -13 5.56 1.70 5 -6 -13 7.20 1.50 5 6 -13 9.10 2.19 -5 6 12 26.97 2.73 -5 -6 12 27.24 2.90 5 -6 -12 27.60 2.89 5 -6 -12 24.11 2.00 5 6 -12 29.78 2.91 -5 6 11 6.63 1.86 -5 -6 11 7.54 1.90 5 -6 -11 4.30 1.62 5 -6 -11 5.59 1.01 5 6 -11 7.33 2.04 -5 6 10 27.32 2.74 -5 -6 10 25.10 2.61 5 -6 -10 27.28 2.71 5 -6 -10 26.74 1.62 5 6 -10 23.63 2.53 -5 6 9 221.53 7.93 5 6 -9 222.73 5.93 -5 -6 9 234.21 8.21 5 -6 -9 224.19 8.04 5 6 -9 225.15 8.09 -5 6 8 12.36 2.04 -5 -6 8 7.65 1.60 5 -6 -8 9.30 1.85 5 6 -8 9.06 1.79 -5 6 7 22.03 2.41 5 6 -7 19.47 1.65 -5 -6 7 20.63 2.12 5 -6 -7 23.37 2.58 5 6 -7 19.29 2.35 -5 6 6 2.13 1.41 5 6 -6 1.20 0.75 -5 -6 6 1.86 0.88 5 -6 -6 2.32 1.24 5 6 -6 1.80 1.18 -5 6 5 38.15 3.03 5 6 -5 38.33 2.56 -5 -6 5 32.28 2.30 5 -6 -5 31.83 2.83 5 6 -5 38.22 3.03 -5 6 4 0.36 0.94 5 6 -4 0.73 1.15 -5 -6 4 -0.01 0.50 5 -6 -4 1.62 1.43 -5 -6 4 0.45 0.95 -5 6 3 11.43 3.51 5 6 -3 13.51 2.09 -5 -6 3 8.92 1.30 5 -6 -3 10.83 1.91 -5 -6 3 10.72 2.23 -5 6 3 10.72 1.08 -5 6 2 9.56 2.41 5 6 -2 7.30 1.97 -5 -6 2 6.65 1.08 5 -6 -2 9.69 2.11 -5 -6 2 6.80 2.06 -5 6 2 8.65 1.31 -5 6 1 20.99 5.07 5 6 -1 21.09 2.63 5 -6 -1 21.23 2.50 -5 -6 1 23.39 3.27 -5 6 1 21.54 1.86 -5 6 0 23.36 6.02 5 6 0 24.24 3.08 5 -6 0 24.02 2.61 -5 -6 0 20.80 2.81 -5 6 0 25.34 2.26 -5 6 -1 3.80 1.27 5 6 1 3.48 1.92 5 -6 1 1.60 1.26 -5 -6 -1 5.49 2.40 -5 6 -1 2.98 1.48 -5 6 -2 1.58 0.95 5 6 2 -0.37 1.27 -5 -6 -2 1.43 1.51 -5 6 -2 0.16 0.72 -5 6 -3 2.28 1.78 5 6 3 2.64 1.59 5 -6 3 4.41 1.72 -5 -6 -3 2.74 1.66 -5 6 -3 1.67 1.27 -5 6 -4 8.13 2.51 5 6 4 11.01 2.68 5 -6 4 7.28 2.04 -5 -6 -4 11.96 3.26 -5 6 -4 8.75 2.26 -5 6 -5 3.60 1.95 5 6 5 3.00 2.29 -5 -6 -5 7.21 3.06 -5 6 -5 3.44 1.77 -5 6 -6 0.07 1.27 5 6 6 2.33 1.71 -5 -6 -6 2.28 2.22 -5 6 -6 0.65 1.16 -5 6 -7 8.92 2.71 5 6 7 9.36 3.42 -5 -6 -7 10.04 3.63 -5 6 -7 6.06 2.40 -5 7 20 -0.05 1.34 -5 -7 20 -0.57 1.55 5 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-7 9 30.57 2.92 5 -7 -9 29.49 3.04 5 7 -9 27.03 2.72 -5 7 8 0.81 1.09 5 7 -8 0.19 0.45 -5 -7 8 1.23 0.93 5 -7 -8 1.43 1.02 5 7 -8 1.09 1.04 -5 7 7 42.82 3.37 5 7 -7 41.85 2.53 -5 -7 7 45.93 3.38 5 -7 -7 50.20 3.89 5 7 -7 40.20 3.14 -5 7 6 0.80 1.09 5 7 -6 1.72 1.04 -5 -7 6 0.57 0.77 5 -7 -6 0.16 0.99 5 7 -6 0.71 1.01 -5 7 5 105.29 4.96 5 7 -5 106.65 4.16 -5 -7 5 107.80 4.12 5 -7 -5 102.37 4.95 5 7 -5 103.74 4.82 -5 7 4 20.45 5.89 5 7 -4 22.44 2.31 -5 -7 4 18.70 1.81 5 -7 -4 21.07 2.69 -5 -7 4 25.51 3.01 -5 7 3 184.58 6.53 5 7 -3 189.50 6.13 -5 -7 3 173.56 4.50 5 -7 -3 182.66 6.42 -5 -7 3 168.58 8.60 -5 7 2 4.55 1.88 5 7 -2 3.48 1.65 -5 -7 2 2.19 0.80 5 -7 -2 0.62 1.08 -5 -7 2 3.62 0.97 -5 7 2 0.81 0.43 -5 7 1 25.91 6.95 5 7 -1 28.46 3.12 5 -7 -1 24.48 2.89 -5 -7 1 24.82 3.07 -5 7 1 21.04 1.85 -5 7 0 6.61 1.35 5 7 0 4.76 2.08 5 -7 0 4.93 1.61 -5 -7 0 6.23 2.14 -5 7 0 5.62 1.44 -5 7 -1 3.72 2.30 5 7 1 3.56 2.02 5 -7 1 6.01 2.05 -5 -7 -1 8.21 2.58 -5 7 -1 5.59 1.53 -5 7 -2 -0.01 0.63 5 7 2 -0.43 1.30 5 -7 2 2.05 1.11 -5 -7 -2 -0.57 1.34 -5 7 -2 0.96 1.09 -5 7 -3 0.08 0.98 5 7 3 -0.06 1.41 5 -7 3 1.78 1.60 -5 -7 -3 -0.01 1.56 -5 7 -3 0.26 0.84 -5 7 -4 3.79 1.16 5 7 4 1.24 1.68 5 -7 4 5.06 1.99 -5 -7 -4 4.67 2.29 -5 7 -4 6.76 2.35 -5 7 -5 2.35 1.25 5 7 5 1.45 1.58 5 -7 5 0.85 1.17 -5 -7 -5 0.51 1.46 -5 7 -5 0.59 1.04 -5 7 -6 -0.08 0.78 5 7 6 2.03 1.89 -5 -7 -6 0.04 1.40 -5 7 -6 -0.02 1.11 -5 8 19 1.37 1.44 -5 -8 19 0.48 1.25 -5 8 18 -0.20 1.33 -5 8 18 0.05 0.80 -5 -8 18 1.65 1.56 5 8 -18 -0.93 1.36 -5 8 17 8.34 2.63 -5 -8 17 9.03 3.06 5 -8 -17 7.17 2.01 5 8 -17 9.26 2.97 -5 8 16 15.77 2.94 -5 -8 16 12.68 2.96 5 -8 -16 13.41 2.52 5 8 -16 12.08 3.04 -5 8 15 1.98 1.69 -5 -8 15 5.12 2.42 5 -8 -15 4.17 1.72 5 8 -15 4.33 2.26 -5 8 14 4.57 1.76 -5 -8 14 3.75 1.95 5 -8 -14 6.16 2.08 5 8 -14 9.43 2.47 -5 8 13 4.32 1.96 -5 -8 13 9.11 2.15 5 -8 -13 7.89 2.18 5 8 -13 10.20 2.44 -5 8 12 38.82 3.79 -5 -8 12 38.20 3.83 5 -8 -12 35.12 3.28 5 8 -12 29.90 3.02 -5 8 11 45.10 3.81 -5 -8 11 59.38 4.28 5 -8 -11 58.48 4.21 5 8 -11 57.12 4.09 -5 8 10 1.28 1.27 -5 -8 10 1.69 1.06 5 -8 -10 1.62 1.62 5 8 -10 1.78 1.21 -5 8 9 9.53 2.21 5 8 -9 8.03 1.33 -5 -8 9 8.48 2.14 5 -8 -9 11.35 2.52 5 8 -9 9.65 2.18 -5 8 8 96.87 4.99 5 8 -8 108.88 3.80 -5 -8 8 112.24 5.09 5 -8 -8 117.05 5.41 5 8 -8 109.67 5.17 -5 8 7 0.26 1.13 -5 -8 7 1.21 0.90 5 -8 -7 1.13 1.17 5 8 -7 3.34 1.70 -5 8 6 30.79 3.22 5 8 -6 35.56 2.60 -5 -8 6 35.26 2.97 5 -8 -6 30.13 3.11 5 8 -6 31.36 3.02 -5 8 5 301.27 8.45 5 8 -5 315.29 7.24 -5 -8 5 300.45 6.97 5 -8 -5 311.03 8.63 5 8 -5 293.54 8.07 -5 8 4 120.19 5.51 5 8 -4 139.56 5.33 -5 -8 4 125.40 4.48 5 -8 -4 123.54 5.78 -5 -8 4 111.92 6.54 5 8 -3 1.63 1.56 -5 -8 3 1.52 0.90 5 -8 -3 1.73 1.24 -5 -8 3 4.05 1.35 -5 8 2 3.75 1.71 5 8 -2 3.89 1.55 -5 -8 2 4.76 1.26 5 -8 -2 7.17 2.28 -5 -8 2 4.51 1.54 -5 8 1 9.41 2.50 5 8 -1 7.82 2.08 5 -8 -1 5.66 1.96 -5 -8 1 5.82 2.34 -5 8 0 7.74 2.32 5 8 0 8.45 2.30 5 -8 0 12.85 2.56 -5 -8 0 10.03 2.33 -5 8 -1 14.24 4.65 5 8 1 18.61 3.49 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1.51 1.45 7 -5 -19 1.22 1.44 7 5 -19 1.72 1.48 -7 5 18 112.15 5.47 -7 -5 18 108.58 6.07 7 -5 -18 102.46 5.53 7 -5 -18 113.35 5.33 7 5 -18 108.85 6.22 -7 5 17 10.71 2.00 -7 -5 17 13.95 3.05 7 -5 -17 8.63 2.34 7 -5 -17 9.85 1.86 7 5 -17 7.86 2.42 -7 5 16 3.85 1.59 -7 -5 16 5.81 2.12 7 -5 -16 1.26 1.26 7 -5 -16 4.25 1.40 7 5 -16 3.61 1.93 -7 5 15 15.26 2.48 -7 -5 15 19.03 2.82 7 -5 -15 16.20 2.53 7 -5 -15 14.14 1.70 7 5 -15 14.25 2.63 -7 5 14 21.13 2.48 -7 -5 14 18.41 2.61 7 -5 -14 18.78 2.83 7 -5 -14 18.14 1.79 7 5 -14 18.30 2.64 -7 5 13 3.19 1.47 -7 -5 13 2.45 1.14 7 -5 -13 3.74 1.48 7 -5 -13 2.16 0.86 7 5 -13 4.67 1.71 -7 5 12 9.07 1.87 -7 -5 12 12.33 2.05 7 -5 -12 10.73 2.21 7 5 -12 10.12 2.07 7 -5 -12 7.62 1.05 -7 5 11 15.42 2.18 7 5 -11 12.08 1.11 -7 -5 11 16.24 2.18 7 -5 -11 17.53 2.43 7 5 -11 13.86 2.08 -7 5 10 3.46 1.63 7 5 -10 1.05 0.66 -7 -5 10 4.00 1.46 7 -5 -10 2.32 1.50 7 5 -10 1.78 1.43 -7 5 9 13.34 2.19 7 5 -9 13.05 1.60 -7 -5 9 14.08 1.89 7 -5 -9 15.62 2.42 7 5 -9 12.46 2.19 -7 5 8 5.89 1.70 7 5 -8 7.87 1.40 -7 -5 8 8.22 1.63 7 -5 -8 6.95 1.83 7 5 -8 9.15 2.00 -7 5 7 1.22 1.61 7 5 -7 0.53 0.74 -7 -5 7 0.56 0.64 7 -5 -7 0.63 0.92 -7 5 7 0.21 0.28 7 5 -7 -0.15 0.93 -7 5 6 45.64 5.56 7 5 -6 47.44 3.24 -7 -5 6 45.97 2.58 7 -5 -6 43.40 3.44 -7 -5 6 38.84 5.42 -7 5 6 44.05 2.25 -7 5 5 0.44 0.52 -7 -5 5 0.32 0.42 7 -5 -5 0.71 0.91 -7 -5 5 0.63 0.71 -7 5 5 1.09 0.79 -7 5 4 79.77 11.04 7 5 -4 86.34 4.66 7 -5 -4 83.97 4.47 -7 -5 4 86.32 10.50 -7 5 4 88.71 3.77 -7 5 3 23.89 7.14 7 5 -3 28.93 3.11 7 -5 -3 26.23 2.64 -7 -5 3 30.89 3.76 -7 5 3 28.58 2.47 -7 5 2 75.17 10.43 7 5 -2 74.70 5.05 -7 -5 2 80.43 5.67 -7 5 2 76.35 4.18 -7 5 1 30.73 4.09 7 5 -1 33.18 3.90 7 -5 -1 26.69 2.88 -7 -5 1 31.60 4.37 -7 5 1 30.98 3.17 -7 5 0 7.67 2.44 7 5 0 11.79 3.01 -7 -5 0 10.40 3.08 -7 5 0 11.98 2.64 7 5 1 77.40 6.21 7 -5 1 55.09 4.92 -7 -5 -1 68.22 5.72 -7 5 -1 73.29 4.85 7 5 2 8.29 2.90 7 -5 2 7.96 3.12 -7 -5 -2 11.58 3.15 -7 5 -2 6.86 2.32 7 5 3 2.72 2.42 7 -5 3 0.48 1.77 -7 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7 6 0 2.63 2.18 7 -6 0 1.56 1.19 -7 -6 0 2.08 2.21 -7 6 0 0.41 0.87 -7 6 -1 1.96 1.17 7 6 1 0.80 1.66 7 -6 1 -0.43 0.97 -7 -6 -1 4.92 2.67 -7 6 -1 1.32 1.34 -7 6 -2 2.06 1.41 7 6 2 2.39 2.11 -7 -6 -2 1.70 2.21 -7 6 -2 0.95 1.16 -7 6 -3 13.91 5.62 7 6 3 26.96 3.97 -7 -6 -3 18.50 3.69 -7 7 22 2.52 1.99 -7 -7 22 5.93 2.53 7 7 -22 7.02 2.64 -7 7 21 1.45 1.50 -7 7 21 -0.88 1.04 -7 -7 21 2.39 1.90 7 7 -21 2.14 2.09 -7 7 20 1.31 1.42 -7 -7 20 3.41 2.25 7 -7 -20 0.61 1.20 7 7 -20 2.88 1.68 -7 7 19 6.60 2.28 -7 -7 19 3.20 2.19 7 -7 -19 1.52 1.54 7 -7 -19 0.18 0.88 7 7 -19 0.39 1.40 -7 7 18 52.79 4.47 -7 -7 18 49.27 4.70 7 -7 -18 48.05 4.29 7 -7 -18 41.11 3.45 7 7 -18 54.90 4.81 -7 7 17 33.10 3.75 -7 -7 17 37.91 4.52 7 -7 -17 29.45 3.36 7 -7 -17 25.69 2.65 7 7 -17 31.04 3.73 -7 7 16 19.09 3.00 -7 -7 16 23.13 3.11 7 -7 -16 19.24 2.96 7 7 -16 19.99 3.15 -7 7 15 80.01 4.97 -7 -7 15 84.28 5.43 7 -7 -15 86.54 5.16 7 7 -15 85.96 5.20 -7 7 14 27.63 3.27 -7 -7 14 44.52 4.30 7 -7 -14 35.68 3.65 7 7 -14 38.49 3.64 -7 7 13 17.57 3.01 -7 -7 13 7.87 2.15 7 -7 -13 7.82 2.15 7 7 -13 7.67 2.17 -7 7 12 -0.06 1.16 -7 -7 12 2.39 1.26 7 -7 -12 1.88 1.62 7 7 -12 1.47 1.59 -7 7 11 1.10 1.45 -7 -7 11 2.96 1.64 7 7 -11 2.37 1.19 -7 7 10 10.01 2.15 7 7 -10 6.28 1.39 -7 -7 10 11.02 2.18 7 -7 -10 7.59 2.12 7 7 -10 10.32 2.09 -7 7 9 44.93 3.79 7 7 -9 33.42 2.51 -7 -7 9 45.39 3.56 7 -7 -9 38.23 3.74 7 7 -9 40.25 3.56 -7 7 8 66.83 4.39 -7 -7 8 68.00 3.62 7 -7 -8 71.85 4.65 7 7 -8 68.72 4.55 -7 7 7 42.77 5.99 7 7 -7 46.95 3.24 -7 -7 7 42.60 2.98 7 -7 -7 46.72 3.90 7 7 -7 46.05 3.80 -7 7 6 146.44 6.73 7 7 -6 161.01 5.94 -7 -7 6 150.63 4.89 7 -7 -6 166.82 6.75 -7 -7 6 149.19 7.89 -7 7 5 201.34 7.81 7 7 -5 215.91 7.14 -7 -7 5 200.81 5.26 7 -7 -5 219.26 7.75 -7 -7 5 213.96 15.47 -7 7 4 144.85 13.38 7 7 -4 152.66 6.47 7 -7 -4 151.27 6.43 -7 -7 4 137.62 13.59 -7 7 3 15.40 3.21 7 7 -3 17.86 2.94 7 -7 -3 18.63 2.85 -7 -7 3 16.75 3.18 -7 7 2 80.79 8.45 7 7 -2 74.32 5.30 7 -7 -2 72.25 4.76 -7 -7 2 85.58 6.26 -7 7 1 7.60 3.12 7 7 -1 9.24 2.74 7 -7 -1 7.38 2.43 -7 -7 1 7.06 2.63 -7 7 0 2.89 1.35 7 7 0 2.25 1.98 7 -7 0 1.11 1.47 -7 -7 0 3.01 1.77 -7 7 -1 0.71 1.00 7 7 1 -0.68 1.66 7 -7 1 0.52 1.44 -7 -7 -1 -0.56 1.37 -7 7 -2 -0.23 0.77 7 7 2 1.88 1.55 -7 -7 -2 1.68 1.79 -7 8 21 1.32 1.58 -7 8 21 0.39 0.53 -7 -8 21 0.60 1.48 7 8 -21 1.46 2.16 -7 8 20 2.63 2.05 -7 -8 20 2.87 2.22 7 -8 -20 2.02 1.95 7 8 -20 2.51 2.25 -7 8 19 20.54 3.40 -7 -8 19 25.25 3.92 7 -8 -19 23.11 3.26 7 8 -19 24.77 3.93 -7 8 18 14.44 3.16 -7 -8 18 18.49 3.88 7 -8 -18 16.52 2.86 7 8 -18 18.28 3.28 -7 8 17 4.09 1.96 -7 -8 17 2.01 1.63 7 -8 -17 2.15 1.67 7 8 -17 5.58 2.50 -7 8 16 0.44 1.20 -7 -8 16 0.33 1.43 7 -8 -16 2.00 2.01 7 8 -16 1.84 1.49 -7 8 15 17.09 2.89 -7 -8 15 13.78 3.08 7 -8 -15 15.21 3.00 7 8 -15 11.81 2.46 -7 8 14 33.59 3.88 -7 -8 14 32.25 3.54 7 -8 -14 32.38 3.56 7 8 -14 28.46 3.31 -7 8 13 9.67 2.54 -7 -8 13 12.86 2.74 7 -8 -13 11.73 2.89 7 8 -13 8.91 2.16 -7 8 12 50.63 4.15 -7 -8 12 59.18 4.51 7 -8 -12 56.42 4.22 7 8 -12 62.33 4.37 -7 8 11 68.55 4.59 -7 -8 11 72.17 4.63 7 -8 -11 66.23 4.52 7 8 -11 70.25 4.64 -7 8 10 1.78 1.38 -7 -8 10 -0.44 0.98 7 -8 -10 2.29 1.68 7 8 -10 -0.07 1.20 -7 8 9 6.70 2.03 7 8 -9 10.51 1.78 -7 -8 9 7.81 1.76 7 -8 -9 7.58 2.25 7 8 -9 10.59 2.24 -7 8 8 6.65 2.38 7 8 -8 1.53 0.99 -7 -8 8 5.45 1.68 7 -8 -8 5.18 2.08 7 8 -8 4.31 1.75 -7 8 7 53.02 4.20 -7 -8 7 60.26 3.50 7 -8 -7 64.51 4.52 -7 8 6 47.52 4.10 7 8 -6 43.67 3.41 -7 -8 6 43.45 3.01 7 -8 -6 46.51 4.11 -7 -8 6 36.26 4.67 -7 8 5 226.75 8.54 7 8 -5 215.18 7.36 -7 -8 5 201.90 5.53 7 -8 -5 204.62 7.76 -7 -8 5 193.46 16.99 -7 8 4 5.67 2.53 7 8 -4 8.67 2.36 7 -8 -4 10.59 2.31 -7 -8 4 8.32 3.25 -7 8 3 0.74 1.50 7 8 -3 1.73 1.75 7 -8 -3 2.65 1.87 -7 -8 3 1.70 1.56 -7 8 2 21.30 6.36 7 8 -2 18.55 3.34 7 -8 -2 16.40 3.21 -7 -8 2 19.39 3.49 -7 8 1 2.39 0.96 7 8 -1 2.63 2.05 -7 -8 1 1.12 1.60 -7 8 0 2.35 1.40 7 8 0 4.59 2.55 7 -8 0 0.69 1.27 -7 -8 0 1.59 2.11 -7 8 -1 0.18 0.77 7 8 1 0.39 1.80 -7 -8 -1 2.10 1.64 -7 8 -2 1.67 1.48 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1.17 8 -4 -9 8.11 2.14 -8 4 9 4.26 0.95 8 4 -9 5.95 1.84 -8 4 8 9.26 3.00 8 4 -8 8.56 1.75 -8 -4 8 8.56 1.52 8 -4 -8 7.61 2.10 -8 -4 8 9.31 2.61 -8 4 8 6.71 1.24 -8 4 7 0.11 0.61 8 4 -7 -0.41 0.74 -8 -4 7 0.28 0.52 8 -4 -7 -0.06 0.77 -8 -4 7 -0.43 1.00 -8 4 7 0.17 0.53 -8 4 6 2.64 2.61 8 4 -6 3.75 1.51 -8 -4 6 2.98 1.06 8 -4 -6 4.44 1.41 -8 -4 6 5.41 2.48 -8 4 6 9.45 1.60 -8 4 5 112.51 14.19 8 4 -5 123.02 5.80 8 -4 -5 129.36 5.21 -8 -4 5 116.61 6.05 -8 4 5 124.70 4.77 -8 4 4 15.21 3.01 8 4 -4 14.49 2.86 8 -4 -4 13.39 2.16 -8 -4 4 15.16 3.16 -8 4 4 13.43 2.09 8 4 -3 35.85 4.10 8 -4 -3 32.27 3.04 -8 -4 3 39.41 4.39 -8 4 3 41.75 3.47 8 4 -2 12.34 3.24 8 -4 -2 6.85 2.40 8 -4 -2 7.56 1.98 -8 -4 2 10.93 2.86 -8 4 2 10.53 2.24 8 4 -1 11.04 2.91 8 -4 -1 14.51 3.78 -8 -4 1 13.98 3.50 -8 4 1 11.53 2.43 8 4 0 6.38 2.83 8 -4 0 8.14 3.05 -8 -4 0 7.28 3.25 -8 4 0 4.82 1.95 8 4 1 5.81 2.95 8 -4 1 9.65 3.13 -8 -4 -1 4.81 2.95 -8 4 -1 8.07 2.50 8 4 2 69.78 6.15 8 -4 2 73.53 6.28 -8 -4 -2 70.05 6.35 -8 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3.52 -8 6 13 8.23 2.59 -8 -6 13 3.71 1.55 8 -6 -13 3.86 1.96 8 6 -13 6.07 2.20 -8 6 12 6.69 2.31 -8 -6 12 2.92 1.58 8 -6 -12 1.98 1.72 8 6 -12 1.36 1.30 -8 6 11 7.21 2.17 8 6 -11 5.97 1.38 -8 -6 11 9.80 2.20 8 -6 -11 6.46 1.96 8 6 -11 7.43 1.90 -8 6 10 1.00 1.22 8 6 -10 1.00 1.03 -8 -6 10 1.34 1.19 8 -6 -10 -0.35 1.15 8 6 -10 1.07 1.24 -8 6 9 43.62 3.70 -8 -6 9 42.76 3.07 8 -6 -9 47.22 3.75 8 6 -9 46.05 3.85 -8 6 8 6.54 2.18 8 6 -8 9.81 1.98 -8 -6 8 8.10 1.60 8 -6 -8 10.13 2.49 -8 -6 8 8.96 2.41 -8 6 7 22.86 3.31 8 6 -7 15.48 2.37 -8 -6 7 23.98 2.50 8 -6 -7 12.91 2.64 -8 -6 7 19.46 6.97 -8 6 6 1.95 1.15 8 6 -6 1.29 1.39 8 -6 -6 2.00 1.56 -8 -6 6 2.42 1.05 -8 6 5 4.07 1.79 8 6 -5 4.13 2.03 8 -6 -5 5.95 1.84 -8 -6 5 5.31 3.15 -8 6 4 99.67 13.94 8 6 -4 96.02 5.69 8 -6 -4 99.69 5.30 -8 -6 4 96.76 6.31 -8 6 3 45.43 14.14 8 6 -3 58.19 4.73 8 -6 -3 54.68 4.12 -8 -6 3 71.56 5.75 -8 6 2 44.96 14.15 8 6 -2 54.20 5.14 8 -6 -2 48.79 4.14 -8 -6 2 42.33 5.00 -8 6 1 1.94 1.69 8 6 -1 0.05 1.34 8 -6 -1 2.24 1.67 -8 -6 1 0.58 1.47 -8 6 0 7.72 2.11 8 6 0 10.76 3.40 -8 -6 0 9.84 3.33 -8 6 -1 19.40 8.60 8 6 1 33.95 4.48 -8 -6 -1 31.60 4.52 -8 7 22 2.30 1.78 -8 7 22 3.69 1.47 -8 -7 22 2.50 2.27 8 7 -22 1.06 2.52 -8 -7 21 2.89 2.14 8 7 -21 1.41 1.56 -8 7 20 3.72 2.17 -8 -7 20 7.36 2.73 8 -7 -20 3.81 1.95 8 7 -20 2.09 2.04 -8 7 19 2.11 1.74 -8 -7 19 1.25 1.61 8 -7 -19 0.06 1.20 8 7 -19 -0.04 1.43 -8 7 18 1.22 1.56 -8 -7 18 0.74 1.39 8 -7 -18 0.26 1.24 8 7 -18 -0.55 1.30 -8 7 17 9.37 2.68 -8 -7 17 9.91 2.88 8 -7 -17 8.30 2.61 8 7 -17 10.90 2.73 -8 7 16 1.74 1.37 -8 -7 16 2.24 1.42 8 -7 -16 2.95 1.77 8 7 -16 3.67 1.94 -8 7 15 0.49 1.23 -8 -7 15 2.22 1.62 8 -7 -15 1.89 1.71 8 7 -15 0.57 1.31 -8 7 14 3.51 1.99 -8 -7 14 4.46 1.91 8 -7 -14 3.75 1.99 8 7 -14 3.05 2.02 -8 7 13 11.54 2.46 -8 -7 13 14.93 2.46 8 -7 -13 12.66 2.54 8 7 -13 15.84 3.05 -8 7 12 51.09 4.05 -8 -7 12 45.38 3.70 8 -7 -12 52.34 4.22 8 7 -12 45.40 3.92 -8 7 11 157.56 6.76 -8 -7 11 165.01 6.24 8 -7 -11 176.17 7.15 8 7 -11 157.86 6.79 -8 7 10 21.04 3.17 8 7 -10 17.83 2.17 -8 -7 10 19.55 2.48 8 -7 -10 18.56 3.09 -8 7 9 23.57 3.33 8 7 -9 17.10 2.34 -8 -7 9 17.39 2.35 8 -7 -9 24.73 3.38 8 7 -9 20.28 3.01 -8 7 8 13.93 2.86 -8 -7 8 9.51 1.82 8 -7 -8 11.28 2.42 -8 -7 8 11.23 2.77 -8 7 7 1.41 1.40 8 7 -7 1.96 1.33 -8 -7 7 0.92 0.70 8 -7 -7 3.40 1.62 -8 -7 7 0.83 1.27 -8 7 6 9.35 2.45 8 7 -6 12.87 2.66 8 -7 -6 7.95 2.31 -8 -7 6 9.02 3.17 -8 7 5 32.42 10.60 8 7 -5 34.73 3.68 8 -7 -5 31.72 3.57 -8 -7 5 35.43 9.74 -8 7 4 0.35 0.99 8 7 -4 1.95 1.65 8 -7 -4 2.84 1.78 -8 -7 4 3.71 2.25 -8 7 3 30.36 6.36 8 7 -3 32.66 4.02 -8 -7 3 33.22 4.75 -8 7 2 53.00 11.94 8 7 -2 47.99 4.63 8 -7 -2 52.25 4.58 -8 -7 2 58.62 5.33 -8 7 1 8.28 2.81 8 7 -1 7.43 2.90 -8 -7 1 15.32 3.77 -8 7 0 24.79 8.85 8 7 0 36.08 4.74 -8 -7 0 39.73 5.14 -8 8 22 0.51 1.50 -8 8 22 3.69 1.90 -8 -8 22 0.70 1.46 8 8 -22 1.74 1.69 -8 8 21 11.00 3.26 -8 -8 21 12.05 3.27 8 -8 -21 5.71 2.44 8 8 -21 10.67 3.09 -8 8 20 2.81 2.02 -8 -8 20 1.94 1.63 8 -8 -20 1.28 1.76 8 8 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2.91 2.13 13 -5 -15 4.46 2.18 -13 -5 15 5.17 2.25 -13 5 14 66.97 5.97 -13 -5 14 61.55 8.58 -13 5 13 2.26 1.70 13 -5 -13 2.22 2.00 -13 -5 13 0.33 1.21 -13 6 22 27.48 3.93 -13 -6 22 33.15 4.27 13 -6 -22 34.84 4.73 13 6 -22 35.86 4.76 -13 6 21 7.17 2.27 -13 -6 21 12.04 3.17 13 -6 -21 9.24 3.13 13 6 -21 7.83 3.29 -13 6 20 1.51 2.04 -13 -6 20 -0.39 1.30 13 -6 -20 1.31 1.56 13 6 -20 2.53 1.87 -13 6 19 1.02 1.45 -13 -6 19 2.82 2.13 13 -6 -19 1.21 1.67 13 6 -19 2.55 2.59 -13 6 18 8.41 2.93 -13 -6 18 8.37 2.80 13 -6 -18 7.30 3.14 13 6 -18 11.07 3.12 -13 6 17 0.48 1.31 -13 -6 17 1.94 1.70 13 -6 -17 0.91 1.42 13 6 -17 0.97 1.68 -13 6 16 3.16 2.12 13 -6 -16 1.50 1.70 -13 -6 16 4.06 3.09 -13 6 15 2.10 1.82 13 -6 -15 1.04 1.34 -13 -6 15 0.63 1.03 -13 6 14 3.38 2.40 13 -6 -14 2.62 2.27 -13 -6 14 3.12 2.16 -13 7 20 0.19 1.62 -13 -7 20 0.15 1.29 13 -7 -20 -0.63 1.38 13 7 -20 2.77 2.72 -13 7 19 27.18 4.32 -13 -7 19 28.02 4.45 13 -7 -19 20.95 4.12 13 7 -19 27.62 4.34 -13 7 18 1.85 1.57 -13 -7 18 1.87 1.86 13 -7 -18 4.37 2.63 13 7 -18 6.05 2.48 -13 7 17 -0.48 1.32 -13 -7 17 1.45 1.72 13 -7 -17 -0.06 1.57 13 7 -17 0.33 1.46 -13 7 16 1.91 2.37 13 -7 -16 -0.42 1.39 -13 -7 16 1.71 1.85 -14 0 24 -0.32 1.46 -14 0 23 0.95 1.33 -14 0 22 4.46 2.48 -14 0 21 -0.26 1.41 14 0 -21 1.34 1.76 -14 0 20 16.35 4.74 -14 0 19 0.96 0.91 -14 0 18 0.84 1.20 -14 0 18 0.00 1.05 -14 0 17 0.28 0.67 -14 0 17 1.34 1.08 -14 0 17 0.92 0.95 -14 0 16 32.46 9.81 -14 0 16 37.27 13.02 -14 0 16 31.47 12.12 -14 0 15 0.24 0.51 -14 0 15 0.79 1.48 -14 1 24 0.92 0.79 -14 -1 24 0.32 1.58 14 1 -24 -0.10 1.40 -14 1 23 1.03 1.28 -14 -1 23 2.89 2.38 14 1 -23 2.71 2.40 -14 1 22 0.28 1.00 -14 -1 22 0.47 1.47 14 1 -22 0.32 1.22 -14 1 21 0.74 1.59 -14 -1 21 0.38 1.48 14 1 -21 3.48 2.19 -14 1 20 0.58 0.86 -14 -1 20 1.43 1.59 14 1 -20 2.58 1.76 -14 1 19 12.62 6.01 -14 -1 19 15.23 5.20 14 1 -19 22.36 3.68 -14 1 18 1.25 1.98 -14 1 18 1.55 0.96 -14 -1 18 0.28 1.32 -14 -1 18 0.48 1.12 -14 1 17 12.72 2.71 -14 1 17 14.21 4.20 -14 -1 17 11.93 3.53 -14 -1 17 13.40 4.96 -14 -1 16 4.27 2.63 -14 1 16 3.57 3.19 -14 1 16 3.74 1.29 -14 -1 16 4.54 2.71 -14 -1 16 4.66 1.66 -14 -1 15 -0.13 1.08 -14 1 15 -0.85 1.39 -14 -1 15 0.00 1.10 -14 2 23 2.54 1.36 -14 -2 23 3.06 1.74 -14 2 22 2.04 1.31 -14 2 21 6.44 2.61 -14 -2 21 13.12 3.20 -14 2 20 0.51 0.79 -14 -2 20 4.09 2.05 -14 2 19 22.95 3.49 -14 2 19 14.66 6.78 -14 -2 19 24.43 3.90 -14 2 18 32.45 4.03 -14 2 18 23.49 8.79 -14 -2 18 32.64 4.17 -14 -2 18 29.87 4.01 -14 2 17 2.20 1.95 -14 2 17 2.16 2.05 -14 -2 17 1.37 1.70 -14 -2 17 4.91 2.39 -14 2 16 7.03 2.65 -14 2 16 3.37 1.82 -14 -2 16 7.57 2.61 -14 -2 15 0.43 1.29 -14 2 15 0.88 1.10 -14 2 15 3.23 1.51 -14 -2 15 1.19 1.38 -14 3 23 1.14 1.09 -14 -3 23 3.88 2.71 14 3 -23 1.62 1.57 -14 -3 22 2.85 2.31 14 3 -22 0.11 1.37 -14 3 21 1.73 1.05 -14 -3 21 2.77 1.95 14 3 -21 1.20 1.48 -14 3 20 1.02 1.33 -14 3 20 1.45 1.31 -14 -3 20 1.21 1.36 14 3 -20 0.17 1.30 -14 3 19 0.01 1.18 -14 3 19 -0.22 1.28 -14 -3 19 1.61 1.91 14 3 -19 1.54 2.06 -14 3 18 -0.97 1.26 -14 -3 18 2.51 2.01 -14 -3 18 2.25 1.86 -14 3 17 0.85 1.41 -14 -3 17 -0.71 1.18 -14 3 16 8.80 3.20 14 -3 -16 7.07 2.74 -14 -3 16 5.38 2.00 -14 4 22 0.54 1.77 -14 -4 22 0.42 1.48 -14 4 21 2.12 2.24 -14 -4 21 0.18 1.37 14 4 -21 3.16 2.39 -14 4 20 15.59 3.28 -14 -4 20 11.85 2.80 14 -4 -20 14.12 3.54 14 4 -20 12.39 3.59 -14 4 19 3.91 2.05 -14 -4 19 1.24 1.47 14 -4 -19 2.37 1.90 14 4 -19 4.80 2.73 -14 4 18 3.00 2.23 -14 -4 18 2.11 1.80 14 -4 -18 8.27 3.00 -14 4 17 2.16 2.24 14 -4 -17 3.49 2.33 -14 -4 17 0.69 1.18 0 0 0 0.00 0.00 ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_type_symbol H4 0.975(3) 0.424(2) 0.2979(19) 0.032(6) Uiso d 1 . . H H6 0.740(4) 0.695(2) 0.275(2) 0.039(7) Uiso d 1 . . H H7 0.686(4) 0.606(2) 0.351(2) 0.040(7) Uiso d 1 . . H H1 0.833(3) 0.4235(19) 0.4836(19) 0.029(6) Uiso d 1 . . H H2A 0.674(4) 0.220(2) 0.288(2) 0.033(6) Uiso d 1 . . H H2B 0.843(4) 0.150(2) 0.393(2) 0.050(8) Uiso d 1 . . H H3A 1.064(3) 0.2823(18) 0.4567(19) 0.024(6) Uiso d 1 . . H H3B 0.941(4) 0.251(2) 0.342(2) 0.044(7) Uiso d 1 . . H H12 0.694(3) 0.071(2) 0.393(2) 0.034(6) Uiso d 1 . . H H14 0.661(3) 0.047(2) 0.5826(19) 0.033(6) Uiso d 1 . . H H16 0.775(3) 0.335(2) 0.5488(18) 0.028(6) Uiso d 1 . . H H19 0.101(4) 0.394(2) 0.107(2) 0.048(8) Uiso d 1 . . H H20 0.047(4) 0.503(2) 0.181(2) 0.049(8) Uiso d 1 . . H H21 0.321(4) 0.560(2) 0.363(2) 0.049(8) Uiso d 1 . . H H10A 0.829(3) 0.7291(19) 0.1424(19) 0.028(6) Uiso d 1 . . H H10B 0.869(3) 0.775(2) 0.234(2) 0.030(6) Uiso d 1 . . H H10C 0.680(4) 0.713(2) 0.134(2) 0.036(7) Uiso d 1 . . H C9 0.8801(3) 0.40316(16) 0.35165(15) 0.0250(4) Uani d 1 . . C C4 0.9139(3) 0.45927(17) 0.30745(16) 0.0263(4) Uani d 1 . . C C5 0.8597(3) 0.56628(16) 0.27693(15) 0.0248(4) Uani d 1 . . C C6 0.7781(3) 0.61918(17) 0.29495(16) 0.0265(4) Uani d 1 . . C C7 0.7441(3) 0.56275(17) 0.33879(16) 0.0260(4) Uani d 1 . . C C8 0.7903(3) 0.45383(16) 0.36537(15) 0.0229(4) Uani d 1 . . C C1 0.7446(3) 0.39585(16) 0.41058(16) 0.0240(4) Uani d 1 . . C C2 0.7947(3) 0.22644(17) 0.36379(19) 0.0316(5) Uani d 1 . . C C3 0.9356(3) 0.28674(17) 0.38295(19) 0.0312(5) Uani d 1 . . C C11 0.7392(3) 0.21668(16) 0.46096(15) 0.0245(4) Uani d 1 . . C C12 0.6989(3) 0.10574(17) 0.43809(17) 0.0287(4) Uani d 1 . . C C13 0.6734(3) 0.04642(17) 0.48454(17) 0.0310(5) Uani d 1 . . C C14 0.6809(3) 0.08791(18) 0.55119(17) 0.0309(5) Uani d 1 . . C C15 0.7166(3) 0.19717(18) 0.57030(16) 0.0280(4) Uani d 1 . . C C16 0.7456(3) 0.26239(17) 0.52814(16) 0.0253(4) Uani d 1 . . C C17 0.5451(3) 0.42530(16) 0.34577(16) 0.0257(4) Uani d 1 . . C C18 0.3854(3) 0.39344(18) 0.24041(17) 0.0306(5) Uani d 1 . . C C19 0.2052(3) 0.4214(2) 0.17995(19) 0.0381(6) Uani d 1 . . C C20 0.1789(3) 0.4834(2) 0.2248(2) 0.0403(6) Uani d 1 . . C C21 0.3300(4) 0.5174(2) 0.3282(2) 0.0375(5) Uani d 1 . . C C22 0.5082(3) 0.48812(17) 0.38510(18) 0.0305(5) Uani d 1 . . C C10 0.8094(3) 0.71540(18) 0.18142(19) 0.0325(5) Uani d 1 . . C N1 0.7737(3) 0.27871(13) 0.41969(14) 0.0263(4) Uani d 1 . . N O1 0.8924(2) 0.61214(12) 0.22969(12) 0.0301(3) Uani d 1 . . O F1 0.6379(2) -0.06031(11) 0.46189(12) 0.0456(4) Uani d 1 . . F F2 0.72560(19) 0.24338(10) 0.63547(10) 0.0354(3) Uani d 1 . . F F3 0.40932(18) 0.33238(12) 0.19587(10) 0.0396(3) Uani d 1 . . F F4 0.65611(19) 0.52408(11) 0.48627(11) 0.0399(3) Uani d 1 . . F loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C9 0.0280(10) 0.0223(10) 0.0235(9) -0.0022(8) 0.0198(9) -0.0023(8) C4 0.0306(11) 0.0244(10) 0.0278(10) -0.0006(8) 0.0237(10) -0.0028(8) C5 0.0258(10) 0.0241(10) 0.0235(9) -0.0050(8) 0.0188(9) -0.0024(8) C6 0.0258(10) 0.0219(10) 0.0286(10) -0.0007(8) 0.0204(9) 0.0005(8) C7 0.0240(10) 0.0243(10) 0.0278(10) 0.0013(8) 0.0196(9) 0.0006(8) C8 0.0229(9) 0.0212(9) 0.0207(9) -0.0021(7) 0.0159(8) -0.0012(7) C1 0.0268(10) 0.0188(9) 0.0254(10) 0.0007(7) 0.0201(9) 0.0002(8) C2 0.0453(13) 0.0206(10) 0.0359(12) 0.0003(9) 0.0333(12) -0.0010(9) C3 0.0441(13) 0.0243(11) 0.0371(12) 0.0059(9) 0.0346(12) 0.0030(9) C11 0.0218(9) 0.0230(10) 0.0219(9) 0.0019(7) 0.0152(9) 0.0034(7) C12 0.0283(10) 0.0254(10) 0.0234(10) -0.0018(8) 0.0177(9) -0.0007(8) C13 0.0301(11) 0.0209(10) 0.0296(11) -0.0026(8) 0.0200(10) 0.0015(8) C14 0.0289(11) 0.0292(11) 0.0277(11) -0.0018(8) 0.0203(10) 0.0044(8) C15 0.0233(10) 0.0310(11) 0.0229(10) 0.0000(8) 0.0162(9) 0.0019(8) C16 0.0239(10) 0.0223(10) 0.0244(10) -0.0001(8) 0.0174(9) 0.0011(8) C17 0.0247(10) 0.0231(10) 0.0268(10) -0.0011(8) 0.0193(9) 0.0041(8) C18 0.0316(11) 0.0312(11) 0.0293(11) -0.0040(9) 0.0237(10) 0.0034(9) C19 0.0253(11) 0.0407(13) 0.0318(12) -0.0056(9) 0.0179(10) 0.0070(10) C20 0.0313(12) 0.0392(13) 0.0488(15) 0.0054(10) 0.0307(12) 0.0174(11) C21 0.0421(13) 0.0303(12) 0.0524(15) 0.0071(10) 0.0398(13) 0.0109(10) C22 0.0337(11) 0.0266(11) 0.0343(11) 0.0030(9) 0.0272(10) 0.0055(9) C10 0.0336(12) 0.0296(12) 0.0323(11) -0.0011(9) 0.0251(11) 0.0045(9) N1 0.0359(10) 0.0174(8) 0.0312(9) 0.0012(7) 0.0275(9) 0.0013(7) O1 0.0388(8) 0.0250(7) 0.0349(8) -0.0027(6) 0.0307(8) -0.0010(6) F1 0.0639(10) 0.0254(7) 0.0484(9) -0.0129(6) 0.0438(8) -0.0060(6) F2 0.0464(8) 0.0332(7) 0.0387(7) -0.0002(6) 0.0361(7) 0.0028(5) F3 0.0353(7) 0.0489(8) 0.0284(7) -0.0103(6) 0.0232(6) -0.0070(6) F4 0.0386(8) 0.0391(8) 0.0399(8) 0.0041(6) 0.0299(7) -0.0059(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 C9 C8 120.04(19) . . ? C4 C9 C3 120.92(19) . . ? C8 C9 C3 119.02(18) . . ? C9 C4 H4 119.6(15) . . ? C5 C4 H4 119.5(15) . . ? C5 C4 C9 120.87(19) . . ? C6 C5 C4 119.57(19) . . ? O1 C5 C4 115.81(18) . . ? O1 C5 C6 124.63(18) . . ? C5 C6 H6 121.3(15) . . ? C5 C6 C7 119.32(19) . . ? C7 C6 H6 119.4(15) . . ? C6 C7 H7 115.7(15) . . ? C6 C7 C8 121.55(19) . . ? C8 C7 H7 122.7(15) . . ? C9 C8 C7 118.53(18) . . ? C9 C8 C1 122.55(17) . . ? C7 C8 C1 118.91(17) . . ? C8 C1 H1 107.0(14) . . ? C8 C1 C17 109.79(16) . . ? C17 C1 H1 107.4(14) . . ? N1 C1 H1 106.7(14) . . ? N1 C1 C8 113.21(16) . . ? N1 C1 C17 112.35(16) . . ? H2A C2 H2B 106(2) . . ? C3 C2 H2A 111.6(14) . . ? C3 C2 H2B 108.6(16) . . ? N1 C2 H2A 111.1(14) . . ? N1 C2 H2B 108.4(16) . . ? N1 C2 C3 110.49(18) . . ? H3A C3 H3B 105(2) . . ? C9 C3 H3A 109.4(14) . . ? C9 C3 H3B 111.2(16) . . ? C9 C3 C2 110.63(19) . . ? C2 C3 H3A 113.0(13) . . ? C2 C3 H3B 107.6(16) . . ? C16 C11 C12 117.90(19) . . ? N1 C11 C12 121.23(19) . . ? N1 C11 C16 120.87(18) . . ? C11 C12 H12 120.5(15) . . ? C13 C12 H12 120.3(15) . . ? C13 C12 C11 119.1(2) . . ? C14 C13 C12 124.5(2) . . ? F1 C13 C12 117.3(2) . . ? F1 C13 C14 118.14(19) . . ? C13 C14 H14 124.6(15) . . ? C13 C14 C15 115.0(2) . . ? C15 C14 H14 120.4(15) . . ? C16 C15 C14 124.4(2) . . ? F2 C15 C14 118.03(19) . . ? F2 C15 C16 117.59(19) . . ? C11 C16 H16 123.0(14) . . ? C15 C16 H16 117.9(14) . . ? C15 C16 C11 119.04(19) . . ? C18 C17 C1 122.53(19) . . ? C22 C17 C1 123.26(19) . . ? C22 C17 C18 114.18(19) . . ? C19 C18 C17 123.4(2) . . ? F3 C18 C17 117.91(19) . . ? F3 C18 C19 118.7(2) . . ? C18 C19 H19 117.8(16) . . ? C20 C19 H19 123.0(16) . . ? C20 C19 C18 119.2(2) . . ? C19 C20 H20 119.7(16) . . ? C21 C20 H20 119.9(16) . . ? C21 C20 C19 120.4(2) . . ? C20 C21 H21 124.2(18) . . ? C20 C21 C22 118.2(2) . . ? C22 C21 H21 117.6(18) . . ? C17 C22 C21 124.7(2) . . ? F4 C22 C17 117.85(19) . . ? F4 C22 C21 117.5(2) . . ? H10A C10 H10B 108.3(19) . . ? H10A C10 H10C 110(2) . . ? H10B C10 H10C 110(2) . . ? O1 C10 H10A 104.8(14) . . ? O1 C10 H10B 113.6(14) . . ? O1 C10 H10C 110.3(16) . . ? C2 N1 C1 119.84(16) . . ? C11 N1 C1 118.93(17) . . ? C11 N1 C2 119.68(16) . . ? C5 O1 C10 116.63(17) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C9 C4 . 1.393(3) ? C9 C8 . 1.393(3) ? C9 C3 . 1.507(3) ? C4 H4 . 0.95(2) ? C4 C5 . 1.392(3) ? C5 C6 . 1.391(3) ? C5 O1 . 1.378(2) ? C6 H6 . 0.99(3) ? C6 C7 . 1.391(3) ? C7 H7 . 1.01(3) ? C7 C8 . 1.400(3) ? C8 C1 . 1.528(3) ? C1 H1 . 0.99(2) ? C1 C17 . 1.539(3) ? C1 N1 . 1.473(2) ? C2 H2A . 0.98(3) ? C2 H2B . 1.03(3) ? C2 C3 . 1.518(3) ? C2 N1 . 1.465(3) ? C3 H3A . 0.98(2) ? C3 H3B . 0.98(3) ? C11 C12 . 1.413(3) ? C11 C16 . 1.408(3) ? C11 N1 . 1.389(3) ? C12 H12 . 0.96(3) ? C12 C13 . 1.381(3) ? C13 C14 . 1.370(3) ? C13 F1 . 1.359(2) ? C14 H14 . 0.96(3) ? C14 C15 . 1.384(3) ? C15 C16 . 1.382(3) ? C15 F2 . 1.355(2) ? C16 H16 . 0.94(2) ? C17 C18 . 1.397(3) ? C17 C22 . 1.384(3) ? C18 C19 . 1.384(3) ? C18 F3 . 1.349(3) ? C19 H19 . 0.99(3) ? C19 C20 . 1.380(4) ? C20 H20 . 1.02(3) ? C20 C21 . 1.374(4) ? C21 H21 . 0.95(3) ? C21 C22 . 1.390(3) ? C22 F4 . 1.356(3) ? C10 H10A . 0.98(2) ? C10 H10B . 1.00(2) ? C10 H10C . 0.94(3) ? C10 O1 . 1.434(3) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C9 C4 C5 C6 2.8(3) . . . . ? C9 C4 C5 O1 -177.11(18) . . . . ? C9 C8 C1 C17 -136.73(19) . . . . ? C9 C8 C1 N1 -10.3(3) . . . . ? C4 C9 C8 C7 -3.1(3) . . . . ? C4 C9 C8 C1 178.31(18) . . . . ? C4 C9 C3 C2 -145.1(2) . . . . ? C4 C5 C6 C7 -2.9(3) . . . . ? C4 C5 O1 C10 169.60(18) . . . . ? C5 C6 C7 C8 0.1(3) . . . . ? C6 C5 O1 C10 -10.3(3) . . . . ? C6 C7 C8 C9 3.0(3) . . . . ? C6 C7 C8 C1 -178.43(18) . . . . ? C7 C8 C1 C17 44.7(2) . . . . ? C7 C8 C1 N1 171.18(17) . . . . ? C8 C9 C4 C5 0.3(3) . . . . ? C8 C9 C3 C2 33.5(3) . . . . ? C8 C1 C17 C18 67.4(2) . . . . ? C8 C1 C17 C22 -110.5(2) . . . . ? C8 C1 N1 C2 -15.0(3) . . . . ? C8 C1 N1 C11 179.24(17) . . . . ? C1 C17 C18 C19 -178.27(19) . . . . ? C1 C17 C18 F3 1.6(3) . . . . ? C1 C17 C22 C21 179.1(2) . . . . ? C1 C17 C22 F4 -0.8(3) . . . . ? C3 C9 C4 C5 178.9(2) . . . . ? C3 C9 C8 C7 178.25(19) . . . . ? C3 C9 C8 C1 -0.3(3) . . . . ? C3 C2 N1 C1 48.2(3) . . . . ? C3 C2 N1 C11 -146.16(19) . . . . ? C11 C12 C13 C14 1.3(3) . . . . ? C11 C12 C13 F1 -178.97(19) . . . . ? C12 C11 C16 C15 1.3(3) . . . . ? C12 C11 N1 C1 157.14(19) . . . . ? C12 C11 N1 C2 -8.6(3) . . . . ? C12 C13 C14 C15 0.1(3) . . . . ? C13 C14 C15 C16 -0.7(3) . . . . ? C13 C14 C15 F2 179.92(18) . . . . ? C14 C15 C16 C11 0.0(3) . . . . ? C16 C11 C12 C13 -1.9(3) . . . . ? C16 C11 N1 C1 -23.7(3) . . . . ? C16 C11 N1 C2 170.58(19) . . . . ? C17 C1 N1 C2 110.1(2) . . . . ? C17 C1 N1 C11 -55.7(2) . . . . ? C17 C18 C19 C20 -0.4(3) . . . . ? C18 C17 C22 C21 1.0(3) . . . . ? C18 C17 C22 F4 -178.79(18) . . . . ? C18 C19 C20 C21 0.3(3) . . . . ? C19 C20 C21 C22 0.4(3) . . . . ? C20 C21 C22 C17 -1.2(3) . . . . ? C20 C21 C22 F4 178.67(19) . . . . ? C22 C17 C18 C19 -0.2(3) . . . . ? C22 C17 C18 F3 179.68(18) . . . . ? N1 C1 C17 C18 -59.6(2) . . . . ? N1 C1 C17 C22 122.6(2) . . . . ? N1 C2 C3 C9 -55.7(2) . . . . ? N1 C11 C12 C13 177.27(19) . . . . ? N1 C11 C16 C15 -177.87(18) . . . . ? O1 C5 C6 C7 176.93(18) . . . . ? F1 C13 C14 C15 -179.68(19) . . . . ? F2 C15 C16 C11 179.35(18) . . . . ? F3 C18 C19 C20 179.66(19) . . . . ? _cod_database_fobs_code 2108643