#------------------------------------------------------------------------------ #$Date: 2020-07-16 07:52:49 +0300 (Thu, 16 Jul 2020) $ #$Revision: 254334 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/86/2108645.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108645 _cell_angle_alpha 90.000 _cell_angle_beta 119.896 _cell_angle_gamma 90.000 _cell_length_a 15.5993 _cell_length_b 49.0620 _cell_length_c 15.6099 _exptl_crystal_F_000 4512.00 _reflns_d_resolution_high 0.7824 _cod_data_source_file dk5096Isup2.hkl _cod_data_source_block I _shelx_title ' B21 in B21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 491.28 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' 'x+1/2, y, z+1/2' '-x+1/2, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -62 0 726.67 819.55 63.26 o 2 -61 0 342.88 402.64 29.22 o 0 -60 0 4.71 8.77 24.23 o 2 -60 0 275.74 304.68 19.78 o 4 -60 0 209.28 175.68 15.43 o 2 -59 0 1270.50 1321.83 50.44 o 4 -59 0 873.59 938.03 36.54 o 0 -58 0 57.52 59.17 15.83 o 2 -58 0 118.64 127.94 16.23 o 4 -58 0 387.84 457.22 34.32 o 6 -58 0 117.72 122.52 15.67 o 2 -57 0 298.20 295.13 24.80 o 4 -57 0 979.29 974.92 48.58 o 6 -57 0 506.40 623.30 51.48 o 0 -56 0 61.63 98.40 28.58 o 2 -56 0 372.14 430.06 29.78 o 4 -56 0 689.90 701.36 42.30 o 6 -56 0 486.96 519.63 33.20 o 2 -55 0 178.34 162.09 16.49 o 4 -55 0 663.98 706.42 44.88 o 6 -55 0 482.73 464.60 35.38 o 0 -54 0 425.52 410.43 30.90 o 2 -54 0 319.15 307.72 20.73 o 4 -54 0 305.49 372.22 34.55 o 6 -54 0 303.37 304.91 31.07 o 8 -54 0 312.55 356.81 35.23 o 2 -53 0 853.81 765.36 31.36 o 4 -53 0 1129.38 1257.74 44.92 o 6 -53 0 543.08 547.25 31.77 o 8 -53 0 1249.21 1369.53 59.89 o 0 -52 0 141.67 172.80 25.72 o 2 -52 0 999.59 830.59 32.11 o 4 -52 0 1461.50 1514.31 65.78 o 6 -52 0 304.96 332.80 23.72 o 8 -52 0 559.09 539.53 37.36 o 2 -51 0 850.31 778.51 31.11 o 4 -51 0 495.12 527.99 27.30 o 6 -51 0 236.09 319.22 24.15 o 8 -51 0 1297.64 1492.47 62.63 o 0 -50 0 3094.17 2784.05 109.19 o 2 -50 0 986.65 949.79 37.14 o 4 -50 0 1528.68 1435.84 41.60 o 6 -50 0 876.84 959.81 36.17 o 8 -50 0 743.81 791.27 33.15 o 2 -49 0 480.47 529.31 25.90 o 4 -49 0 693.21 713.28 26.72 o 6 -49 0 1690.70 1700.55 58.43 o 8 -49 0 1059.16 1023.54 38.80 o 10 -49 0 259.88 292.58 49.08 o 0 -48 0 21621.48 20192.71 583.00 o 2 -48 0 783.07 784.22 30.77 o 4 -48 0 917.84 1074.06 36.75 o 6 -48 0 801.44 833.46 33.53 o 8 -48 0 1578.20 1757.83 53.14 o 10 -48 0 937.75 914.73 53.58 o 2 -47 0 1263.43 1122.93 41.41 o 4 -47 0 4068.29 3758.77 92.48 o 6 -47 0 654.95 569.47 29.99 o 8 -47 0 906.38 1040.58 39.30 o 10 -47 0 509.26 485.75 30.36 o 0 -46 0 417.33 384.65 39.42 o 2 -46 0 1116.94 1100.49 43.50 o 4 -46 0 2569.74 2507.04 59.99 o 6 -46 0 666.42 675.75 32.16 o 8 -46 0 1511.48 1509.19 87.76 o 10 -46 0 952.13 929.78 40.73 o 2 -45 0 2574.83 2202.15 67.40 o 4 -45 0 2010.35 1846.41 48.50 o 6 -45 0 698.28 746.06 38.52 o 8 -45 0 224.67 254.97 25.32 o 10 -45 0 1499.49 1705.80 59.02 o 0 -44 0 6262.43 5982.66 215.43 o 2 -44 0 7237.23 6319.63 146.65 o 4 -44 0 2516.22 2276.30 56.54 o 6 -44 0 1984.96 1910.75 56.52 o 8 -44 0 1596.56 1743.30 58.19 o 10 -44 0 517.22 535.89 32.43 o 12 -44 0 225.38 272.15 42.39 o 2 -43 0 2011.16 1838.66 61.93 o 4 -43 0 6789.36 6135.37 128.53 o 6 -43 0 3676.07 3779.04 94.00 o 8 -43 0 792.43 759.87 35.14 o 10 -43 0 832.55 875.55 45.67 o 12 -43 0 792.04 706.64 59.88 o 0 -42 0 29104.65 27422.37 877.09 o 2 -42 0 3622.80 3117.33 79.83 o 4 -42 0 4871.26 4388.62 113.56 o 6 -42 0 1103.01 1083.18 38.49 o 8 -42 0 2197.60 2541.84 67.78 o 10 -42 0 494.79 543.20 35.64 o 12 -42 0 538.73 487.81 54.42 o 2 -41 0 2498.90 2322.76 68.53 o 4 -41 0 4303.97 3954.48 84.10 o 6 -41 0 2430.48 2629.01 68.34 o 8 -41 0 1479.00 1415.07 55.17 o 10 -41 0 1131.15 1178.64 46.88 o 12 -41 0 822.67 750.81 51.86 o 0 -40 0 300.22 232.95 29.66 o 2 -40 0 10847.51 9654.90 203.68 o 4 -40 0 10399.43 9233.19 177.70 o 6 -40 0 3108.76 2972.60 74.30 o 8 -40 0 1051.41 1153.49 43.46 o 10 -40 0 1046.95 1095.89 46.29 o 12 -40 0 390.24 434.21 30.79 o 2 -39 0 1233.30 1040.67 38.28 o 4 -39 0 367.85 389.64 20.24 o 6 -39 0 1673.57 1457.09 58.29 o 8 -39 0 1625.04 1625.03 46.96 o 10 -39 0 1209.50 1299.25 42.05 o 12 -39 0 830.92 827.43 52.64 o 0 -38 0 553.43 540.33 41.98 o 2 -38 0 2656.26 2614.91 78.61 o 4 -38 0 4476.50 4158.94 86.14 o 6 -38 0 8688.81 7981.06 168.90 o 8 -38 0 1503.52 1390.62 42.85 o 10 -38 0 316.45 298.67 22.11 o 12 -38 0 245.93 206.87 25.51 o 2 -37 0 2170.44 1873.24 54.18 o 4 -37 0 1207.62 1126.45 36.03 o 6 -37 0 2012.42 1804.25 45.09 o 8 -37 0 1195.07 1268.14 39.88 o 10 -37 0 553.40 578.18 31.64 o 12 -37 0 736.73 703.82 42.61 o 0 -36 0 7593.51 8154.60 277.31 o 2 -36 0 2427.78 2170.53 57.28 o 4 -36 0 3197.46 2801.23 77.96 o 6 -36 0 10782.38 10277.97 195.84 o 8 -36 0 2876.88 2678.35 63.43 o 10 -36 0 430.78 455.38 25.67 o 12 -36 0 1670.33 1707.77 61.55 o 14 -36 0 242.26 113.65 27.50 o 2 -35 0 2402.54 2399.00 68.41 o 4 -35 0 11618.66 10472.89 231.44 o 6 -35 0 4918.88 4674.88 90.98 o 8 -35 0 4261.93 4178.00 87.85 o 10 -35 0 3099.87 3102.52 111.60 o 12 -35 0 272.00 239.34 22.35 o 14 -35 0 965.90 1033.78 81.00 o 0 -34 0 36.21 38.88 22.01 o 2 -34 0 17008.43 15270.15 437.76 o 4 -34 0 2269.60 2087.11 55.77 o 6 -34 0 2214.52 1965.40 44.26 o 8 -34 0 6759.45 6491.43 144.44 o 10 -34 0 2560.50 2368.00 63.28 o 12 -34 0 2060.76 2008.42 96.46 o 14 -34 0 294.73 226.68 40.84 o 2 -33 0 1878.77 1876.26 53.84 o 4 -33 0 7192.30 6848.06 175.01 o 6 -33 0 1198.90 1131.96 32.00 o 8 -33 0 5959.05 5782.41 141.13 o 10 -33 0 307.54 271.59 19.78 o 12 -33 0 490.45 228.54 37.71 o 14 -33 0 370.08 360.95 50.77 o 0 -32 0 1793.04 1473.73 139.35 o 2 -32 0 9389.32 8976.90 268.25 o 4 -32 0 3860.61 3394.05 93.65 o -1 -62 1 54.73 49.03 14.83 o -1 -61 1 302.88 258.41 29.57 o -1 -60 1 133.28 164.64 13.93 o -1 -59 1 48.94 49.41 13.40 o -1 -58 1 360.24 364.33 27.84 o -1 -57 1 9.35 14.64 11.16 o -1 -56 1 93.29 94.90 14.79 o -1 -55 1 114.63 113.49 15.28 o -1 -54 1 56.14 83.53 15.71 o -1 -53 1 151.73 140.08 17.28 o -1 -52 1 236.63 188.57 16.24 o -1 -51 1 64.34 79.99 15.67 o -1 -50 1 347.45 313.35 24.92 o -1 -49 1 715.14 669.98 30.61 o -1 -48 1 72.76 63.67 17.41 o -1 -47 1 1502.72 1285.44 46.09 o -1 -46 1 6315.47 5290.82 125.37 o -1 -45 1 278.04 273.62 20.35 o -1 -44 1 1203.24 1001.85 39.57 o -1 -43 1 763.00 741.92 39.47 o -1 -42 1 871.15 793.53 31.66 o -1 -41 1 2720.53 2457.51 65.66 o -1 -40 1 2351.47 2020.29 60.04 o -1 -39 1 3015.17 2606.96 74.16 o -1 -38 1 850.66 725.31 49.26 o -1 -37 1 127.08 133.57 20.77 o -1 -36 1 146.47 149.50 19.48 o -1 -35 1 1029.17 907.82 44.46 o -1 -34 1 279.52 290.96 24.25 o -1 -33 1 763.19 744.43 32.95 o -1 -32 1 2296.43 2081.08 58.89 o -3 -61 3 126.87 107.91 16.18 o -3 -60 3 435.18 368.46 20.45 o -3 -59 3 23.46 29.99 13.94 o -3 -58 3 255.96 245.38 20.22 o -3 -57 3 226.88 221.65 24.60 o -3 -56 3 346.67 341.14 31.48 o -3 -55 3 36.06 26.67 17.44 o -3 -54 3 324.74 308.06 21.68 o -3 -53 3 330.36 279.38 18.71 o -3 -52 3 118.72 120.71 15.22 o -3 -51 3 420.27 351.88 19.50 o -3 -50 3 1173.66 1051.06 34.34 o -3 -49 3 110.08 107.61 15.51 o -3 -48 3 351.96 308.72 18.61 o -3 -47 3 722.29 608.98 26.12 o -3 -46 3 681.02 593.26 27.08 o -3 -45 3 593.88 495.03 27.21 o -3 -44 3 343.21 361.19 23.20 o -3 -43 3 1083.60 918.67 36.41 o -3 -42 3 1032.06 871.91 33.50 o -3 -41 3 463.43 372.46 21.05 o -3 -40 3 261.96 226.78 18.40 o -3 -39 3 505.75 443.90 21.23 o -3 -38 3 2744.15 2396.37 62.23 o -3 -37 3 820.42 754.54 29.40 o -3 -36 3 414.15 401.69 23.08 o -3 -35 3 2371.08 1906.68 57.51 o -3 -34 3 163.74 125.83 17.03 o -3 -33 3 4209.83 3643.81 99.91 o -3 -32 3 775.94 677.57 33.94 o -5 -59 5 186.25 193.12 20.66 o -5 -58 5 597.19 518.12 25.19 o -5 -57 5 293.66 326.63 34.63 o -5 -56 5 757.13 661.08 39.15 o -5 -55 5 192.17 168.13 23.86 o -5 -54 5 545.51 511.42 35.23 o -5 -53 5 173.12 179.55 22.21 o -5 -52 5 265.23 275.63 21.67 o -5 -51 5 473.39 436.82 30.29 o -5 -50 5 712.30 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630.70 33.51 o 14 -31 0 448.60 414.92 37.98 o 0 -30 0 5432.47 4676.89 275.15 o 2 -30 0 3435.00 3067.56 91.24 o 4 -30 0 5261.94 5011.88 115.44 o 6 -30 0 2063.16 2155.07 62.90 o 8 -30 0 5459.34 5304.81 103.96 o 10 -30 0 856.94 882.99 34.84 o 12 -30 0 830.19 746.38 36.48 o 14 -30 0 755.52 757.52 43.43 o 2 -29 0 1969.33 1912.82 75.13 o 4 -29 0 2163.61 1911.34 54.08 o 6 -29 0 3686.33 3371.27 69.97 o 8 -29 0 5241.97 5366.33 100.20 o 10 -29 0 2853.73 2913.54 68.09 o 12 -29 0 876.53 949.19 40.24 o 14 -29 0 325.31 274.47 24.76 o 0 -28 0 922.68 1010.28 69.62 o 2 -28 0 2977.80 2631.63 112.44 o 4 -28 0 4432.00 4038.99 105.87 o 6 -28 0 3308.11 3095.62 76.05 o 8 -28 0 5614.69 5296.83 96.02 o 10 -28 0 2386.83 2282.02 55.85 o 12 -28 0 1133.20 1208.13 44.72 o 14 -28 0 817.62 853.81 45.72 o 4 -27 0 193.02 136.29 16.56 o 6 -27 0 723.25 722.49 25.83 o 8 -27 0 751.65 767.76 27.81 o 10 -27 0 3029.65 3609.31 85.52 o 12 -27 0 976.73 985.78 40.25 o 14 -27 0 326.18 329.26 29.27 o 0 -26 0 10.30 12.98 19.46 o 2 -26 0 19844.73 17981.81 514.77 o 4 -26 0 5648.12 5762.40 147.08 o 6 -26 0 5100.40 4626.50 93.16 o 8 -26 0 3448.46 3431.58 67.28 o 10 -26 0 4437.67 4983.03 136.03 o 12 -26 0 790.61 739.56 37.30 o 14 -26 0 285.47 256.46 25.83 o 2 -25 0 37510.76 36477.24 938.62 o 4 -25 0 1006.33 963.39 41.05 o 6 -25 0 4164.41 3910.47 79.83 o 8 -25 0 2246.60 2017.95 51.07 o 10 -25 0 2500.25 2415.19 92.21 o 12 -25 0 1168.78 1209.58 76.72 o 14 -25 0 978.62 883.07 58.96 o 0 -24 0 7098.91 7195.80 335.62 o 2 -24 0 9693.72 9746.65 239.19 o 4 -24 0 8645.89 8447.94 209.18 o 6 -24 0 11076.11 11709.62 238.92 o 8 -24 0 2628.65 2669.21 69.86 o 10 -24 0 3456.12 3562.69 79.61 o 12 -24 0 3537.54 3432.39 91.14 o 14 -24 0 925.18 674.94 44.72 o 2 -23 0 15941.82 15322.20 370.70 o 4 -23 0 2341.17 2277.39 69.76 o 6 -23 0 3375.49 3429.95 71.02 o 8 -23 0 2923.36 2934.33 84.55 o 10 -23 0 1953.31 1919.30 48.63 o 12 -23 0 822.45 848.65 34.75 o 14 -23 0 259.21 266.76 20.39 o 0 -22 0 592.42 121.05 30.73 o 2 -22 0 7224.34 6828.08 158.83 o 4 -22 0 4166.42 3963.28 112.05 o 6 -22 0 5887.59 6217.75 127.68 o 8 -22 0 374.18 361.21 17.02 o 10 -22 0 428.04 410.02 19.64 o 12 -22 0 1392.11 1336.20 37.72 o 14 -22 0 582.95 595.18 27.80 o 16 -22 0 443.66 224.06 35.13 o 2 -21 0 17381.71 15550.70 375.05 o 4 -21 0 20867.24 20565.37 587.29 o 6 -21 0 2604.43 2661.32 56.55 o 8 -21 0 5990.82 5665.95 105.40 o 10 -21 0 2820.13 2631.40 51.74 o 12 -21 0 1088.27 939.51 30.31 o 14 -21 0 377.86 387.17 22.69 o 16 -21 0 482.08 324.81 39.39 o 0 -20 0 6845.72 5928.53 226.57 o 2 -20 0 15928.57 15445.64 441.95 o 4 -20 0 7303.50 6983.02 206.28 o 6 -20 0 13787.95 13979.62 271.36 o 8 -20 0 2013.21 2027.18 49.71 o 10 -20 0 3837.08 3757.98 69.36 o 12 -20 0 3223.32 3504.60 79.61 o 14 -20 0 322.72 337.01 24.19 o 16 -20 0 132.52 157.80 33.76 o 2 -19 0 29580.01 27309.77 650.86 o 4 -19 0 9491.28 8729.42 254.57 o 6 -19 0 7012.95 7109.97 157.12 o 8 -19 0 2939.56 2870.25 59.41 o 10 -19 0 2135.61 2014.22 42.20 o 12 -19 0 2827.48 2715.81 65.14 o 14 -19 0 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9904.66 197.59 o 4 32 0 3863.21 3748.27 90.34 o 6 32 0 3367.74 3349.62 80.17 o 8 32 0 2791.13 3023.47 79.33 o 10 32 0 1306.12 1216.56 36.52 o 12 32 0 1208.88 1146.49 37.19 o 2 33 0 1868.58 2140.92 50.29 o 4 33 0 7162.49 7656.35 163.44 o 6 33 0 1217.10 1233.80 37.87 o 8 33 0 6021.70 6341.95 175.61 o 10 33 0 306.87 222.74 30.29 o 12 33 0 490.01 560.36 33.16 o 0 34 0 37.20 66.12 14.70 o 2 34 0 16968.75 17838.13 332.78 o 4 34 0 2244.98 2298.08 53.40 o 6 34 0 2210.29 2174.64 54.90 o 8 34 0 6719.69 6967.70 176.61 o 10 34 0 2561.21 2494.60 69.46 o 12 34 0 2038.12 1936.17 63.95 o 2 35 0 2411.03 2631.96 58.92 o 4 35 0 11647.51 11776.43 233.00 o 6 35 0 4956.17 5156.67 110.69 o 8 35 0 4261.29 4471.31 127.66 o 10 35 0 3078.25 3103.54 91.28 o 12 35 0 272.22 306.19 25.70 o 0 36 0 7558.92 8655.64 257.53 o 2 36 0 2427.21 2451.74 50.95 o 4 36 0 3205.87 3183.26 63.05 o 6 36 0 10825.31 11549.34 241.07 o 8 36 0 2862.71 2768.39 77.12 o 10 36 0 425.62 434.72 23.59 o 12 36 0 1674.27 1705.88 114.87 o 2 37 0 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1160.99 35.17 o -11 -7 3 3113.13 3471.63 67.84 o -9 -7 3 232.19 271.05 13.31 o -7 -7 3 595.50 603.72 24.30 o -5 -7 3 1475.38 1439.59 40.36 o -3 -7 3 475.53 434.31 15.76 o -1 -7 3 62.43 67.01 9.90 o 1 -7 3 3207.20 3064.29 91.86 o 3 -7 3 2328.70 2300.12 65.60 o 3 -7 3 3447.39 3091.40 86.12 o 5 -7 3 1449.94 1541.46 62.39 o 7 -7 3 377.45 410.11 26.55 o 9 -7 3 1235.06 1298.71 36.75 o 11 -7 3 713.16 762.83 27.53 o 13 -7 3 83.49 39.59 11.96 o 15 -7 3 20.39 3.14 11.61 o -15 -6 3 548.39 596.40 28.89 o -13 -6 3 495.13 377.34 48.89 o -11 -6 3 300.93 322.19 17.85 o -9 -6 3 1985.37 2147.73 45.73 o -7 -6 3 695.64 694.91 23.05 o -5 -6 3 241.57 246.29 11.84 o -3 -6 3 1353.36 1338.94 34.72 o -1 -6 3 1013.90 985.14 32.03 o 1 -6 3 1055.96 1025.07 36.14 o 3 -6 3 1117.61 1108.19 35.58 o 3 -6 3 1654.48 1521.95 48.12 o 5 -6 3 341.86 410.80 49.92 o 7 -6 3 324.49 356.70 26.90 o 9 -6 3 223.67 171.64 16.45 o 11 -6 3 201.09 165.17 14.69 o 13 -6 3 381.98 427.73 38.74 o 15 -6 3 83.38 29.72 15.79 o -17 -5 3 21.05 12.72 12.95 o -15 -5 3 601.90 681.56 38.22 o -13 -5 3 10.99 4.33 11.09 o -11 -5 3 360.34 369.62 17.64 o -9 -5 3 163.16 168.16 12.70 o -7 -5 3 382.62 403.67 19.39 o -5 -5 3 396.03 406.99 15.67 o -3 -5 3 95.02 118.72 9.39 o -1 -5 3 1072.31 1044.60 33.11 o 1 -5 3 7049.72 6923.43 197.90 o 3 -5 3 5526.47 5600.42 162.96 o 3 -5 3 8180.43 7379.09 179.90 o 5 -5 3 874.71 962.15 43.25 o 7 -5 3 146.20 111.08 16.40 o 9 -5 3 1658.87 1886.83 55.06 o 11 -5 3 1034.17 1186.23 45.37 o 13 -5 3 29.18 12.39 12.73 o 15 -5 3 142.12 -0.47 15.05 o -17 -4 3 33.88 3.88 12.74 o -15 -4 3 1093.02 1045.58 60.87 o -13 -4 3 1529.14 1726.76 45.12 o -11 -4 3 515.49 570.12 19.52 o -9 -4 3 1575.70 1656.40 37.04 o -7 -4 3 590.90 591.61 24.93 o -5 -4 3 353.42 372.99 15.72 o -3 -4 3 219.00 213.27 11.34 o -1 -4 3 709.49 732.30 27.34 o 1 -4 3 1918.05 1941.10 61.24 o 3 -4 3 558.78 436.78 19.19 o 3 -4 3 377.67 334.06 19.36 o 5 -4 3 1576.55 1649.20 57.49 o 7 -4 3 1437.80 1644.66 55.39 o 9 -4 3 1532.13 1643.62 58.78 o 11 -4 3 29.95 22.88 12.29 o 13 -4 3 227.51 96.26 12.86 o 15 -4 3 51.92 12.86 10.24 o -17 -3 3 296.79 85.43 16.90 o -15 -3 3 49.30 30.41 13.78 o -13 -3 3 2398.16 2700.36 71.24 o -11 -3 3 102.26 113.01 10.39 o -9 -3 3 15.55 23.02 7.88 o -7 -3 3 214.50 192.39 13.47 o -5 -3 3 655.88 607.72 19.73 o -3 -3 3 664.20 640.68 18.38 o -1 -3 3 1160.49 1161.29 38.21 o 1 -3 3 6338.11 6013.47 224.20 o 3 -3 3 2040.97 2092.04 74.73 o 3 -3 3 3020.16 2666.36 61.28 o 5 -3 3 423.38 427.50 25.86 o 7 -3 3 2311.02 2424.03 76.97 o 9 -3 3 2012.42 2061.88 70.30 o 11 -3 3 512.72 415.80 36.78 o 13 -3 3 125.74 58.45 12.92 o -17 -2 3 29.05 6.01 12.93 o -15 -2 3 69.65 46.51 14.11 o -13 -2 3 157.64 108.27 14.68 o -11 -2 3 731.63 849.73 26.25 o -9 -2 3 78.04 62.05 8.22 o -7 -2 3 332.69 333.16 16.98 o -5 -2 3 183.41 173.89 10.49 o -3 -2 3 52.30 57.62 6.66 o -1 -2 3 445.58 418.58 18.96 o 1 -2 3 2965.42 2913.70 96.53 o 3 -2 3 8.89 3.56 12.41 o 3 -2 3 13.16 13.08 9.41 o 5 -2 3 235.59 204.50 25.05 o 7 -2 3 1481.89 1633.88 46.38 o 9 -2 3 490.69 638.46 49.72 o 11 -2 3 439.63 387.87 35.12 o 13 -2 3 136.75 81.22 12.94 o 15 -2 3 174.97 22.97 12.50 o -17 -1 3 71.71 40.75 13.08 o -15 -1 3 1124.44 1141.29 41.27 o -13 -1 3 1220.74 1287.97 39.45 o -11 -1 3 640.54 709.70 25.41 o -9 -1 3 65.25 72.29 9.67 o -7 -1 3 750.67 763.51 35.17 o -5 -1 3 906.46 845.43 23.81 o -3 -1 3 1543.26 1466.06 36.65 o -1 -1 3 202.36 214.42 14.01 o 1 -1 3 2885.89 2898.35 96.00 o 3 -1 3 3137.54 3316.69 111.99 o 3 -1 3 4643.51 4078.80 103.18 o 5 -1 3 2214.49 2323.54 75.18 o 7 -1 3 707.34 821.90 29.28 o 9 -1 3 281.60 208.94 20.01 o 11 -1 3 1347.82 1471.23 45.69 o 13 -1 3 175.37 84.58 14.74 o 15 -1 3 8.19 1.09 10.68 o -17 0 3 49.27 18.10 12.88 o -15 0 3 688.47 772.16 31.35 o -13 0 3 3.34 7.47 13.04 o -11 0 3 9.97 9.00 9.68 o -9 0 3 1351.67 1459.94 34.16 o -7 0 3 39.97 64.61 8.88 o -5 0 3 219.49 178.48 10.42 o -3 0 3 77.17 82.94 7.56 o -1 0 3 1029.64 999.76 29.86 o 1 0 3 3147.82 3360.62 163.69 o 3 0 3 26.19 3.03 8.47 o 3 0 3 17.62 15.15 12.35 o 5 0 3 733.62 856.51 36.55 o 7 0 3 72.22 67.37 14.15 o 9 0 3 32.69 52.17 17.87 o 11 0 3 1313.89 1564.52 43.23 o 13 0 3 37.95 31.96 12.63 o 15 0 3 475.08 52.96 17.99 o -17 1 3 71.79 14.47 12.52 o -15 1 3 1123.39 1198.94 43.10 o -13 1 3 1212.19 1285.32 38.70 o -11 1 3 643.20 716.76 25.22 o -9 1 3 63.93 81.94 8.45 o -7 1 3 752.90 786.69 29.54 o -5 1 3 895.29 814.14 24.05 o -3 1 3 1542.08 1422.57 37.83 o -1 1 3 202.72 215.63 13.84 o 1 1 3 2895.75 2930.42 113.13 o 3 1 3 3132.58 3260.06 110.03 o 3 1 3 4636.16 4081.09 102.69 o 5 1 3 2221.00 2367.01 84.70 o 7 1 3 705.85 744.38 30.05 o 9 1 3 283.41 218.09 22.39 o 11 1 3 1343.22 1537.85 44.72 o 13 1 3 175.61 92.67 13.63 o 15 1 3 7.84 5.13 10.96 o -17 2 3 30.25 16.72 12.01 o -15 2 3 70.68 30.40 15.14 o -13 2 3 161.06 127.09 14.52 o -11 2 3 739.22 810.96 28.46 o -9 2 3 76.49 71.84 10.06 o -7 2 3 332.49 345.38 19.73 o -5 2 3 183.11 176.69 10.34 o -3 2 3 51.80 55.24 6.06 o -1 2 3 449.22 411.81 18.48 o 1 2 3 2955.35 2994.14 99.06 o 3 2 3 12.42 5.43 7.85 o 3 2 3 8.39 18.51 10.15 o 5 2 3 239.48 269.15 23.55 o 7 2 3 1501.49 1635.28 47.75 o 9 2 3 488.53 461.71 48.36 o 11 2 3 444.46 489.34 34.16 o 13 2 3 133.48 94.82 13.35 o 15 2 3 175.71 41.14 11.33 o -17 3 3 290.01 70.64 14.69 o -15 3 3 48.76 35.18 15.16 o -13 3 3 2386.22 2703.14 77.10 o -11 3 3 101.18 96.82 13.33 o -9 3 3 15.94 14.31 8.28 o -7 3 3 213.28 197.53 14.26 o -5 3 3 655.77 601.37 20.40 o -3 3 3 663.44 652.51 18.76 o -1 3 3 1158.00 1191.39 38.57 o 1 3 3 6333.13 6442.76 206.09 o 3 3 3 3013.53 2719.17 84.37 o 3 3 3 2036.49 2086.04 74.34 o 5 3 3 428.12 425.74 29.00 o 7 3 3 2318.83 2417.81 80.26 o 9 3 3 2006.11 2152.08 97.28 o 11 3 3 512.19 390.87 30.72 o 13 3 3 127.86 68.61 12.80 o 15 3 3 300.86 45.31 12.14 o -17 4 3 33.27 12.51 13.99 o -15 4 3 1084.17 1211.65 50.82 o -13 4 3 1536.75 1718.13 52.77 o -11 4 3 515.18 530.87 25.61 o -9 4 3 1583.75 1613.74 40.28 o -7 4 3 592.00 636.32 25.69 o -5 4 3 351.28 358.88 13.14 o -3 4 3 218.36 209.63 9.32 o -1 4 3 709.05 739.73 26.91 o 1 4 3 1904.96 1980.21 68.10 o 3 4 3 377.96 341.38 27.02 o 3 4 3 559.22 454.02 23.04 o 5 4 3 1577.45 1635.91 70.93 o 7 4 3 1425.85 1650.91 55.59 o 9 4 3 1528.06 1683.96 71.71 o 11 4 3 29.87 33.28 14.50 o 13 4 3 227.17 115.14 13.65 o 15 4 3 52.06 -0.27 10.21 o -17 5 3 21.63 9.59 14.28 o -15 5 3 603.61 692.17 31.72 o -13 5 3 11.64 -0.08 13.39 o -11 5 3 359.11 296.63 23.06 o -9 5 3 163.68 188.14 12.43 o -7 5 3 385.51 434.04 20.09 o -5 5 3 395.35 402.41 13.38 o -3 5 3 94.07 118.16 7.21 o -1 5 3 1072.63 1067.75 35.75 o 1 5 3 7074.21 7400.02 236.28 o 3 5 3 5511.55 5902.35 222.36 o 3 5 3 8158.34 7056.09 186.23 o 5 5 3 876.50 1036.93 46.88 o 3 -12 5 6451.43 5987.11 120.25 o 3 -11 5 5223.74 5107.21 98.96 o 3 -10 5 1201.38 1082.45 30.67 o 3 -9 5 1629.43 1593.62 37.72 o 3 -8 5 9156.21 8920.18 173.82 o 3 -7 5 825.21 862.35 28.63 o 3 -6 5 425.84 404.79 19.57 o 3 -5 5 1815.94 1744.37 49.30 o 3 -4 5 2808.19 2562.55 60.66 o 3 -3 5 341.62 387.71 17.02 o 3 -2 5 2087.58 1808.31 44.58 o 3 -1 5 25.36 15.82 7.07 o 3 0 5 699.76 643.59 18.91 o 3 1 5 25.41 28.09 6.92 o 3 2 5 2083.84 1817.82 41.78 o 3 3 5 340.04 387.67 17.25 o 3 4 5 2831.77 2786.27 83.73 o 3 5 5 1809.02 1725.27 47.77 o 3 -12 7 2826.08 2793.96 58.71 o 3 -11 7 658.12 717.45 18.82 o 3 -10 7 968.94 1062.07 31.22 o 3 -9 7 518.46 553.28 17.98 o 3 -8 7 1771.13 1816.71 35.69 o 3 -7 7 443.89 489.02 17.97 o 3 -6 7 605.05 637.98 17.72 o 3 -5 7 771.90 787.36 20.56 o 3 -4 7 1064.62 1045.07 26.40 o 3 -3 7 469.52 500.50 21.84 o 3 -2 7 630.71 650.21 26.99 o 3 -1 7 1367.98 1349.10 32.43 o 3 0 7 999.95 1019.93 28.38 o 3 1 7 1362.28 1409.55 42.45 o 3 2 7 637.26 656.71 20.01 o 3 3 7 468.62 535.69 22.35 o 3 4 7 1049.70 1052.91 29.80 o 3 5 7 779.57 746.52 24.20 o 3 -12 9 250.57 310.12 15.75 o 3 -11 9 4387.52 4676.22 104.66 o 3 -10 9 784.36 768.24 24.83 o 3 -9 9 88.67 91.06 12.72 o 3 -8 9 739.63 820.11 25.53 o 3 -7 9 210.47 245.89 15.09 o 3 -6 9 379.18 464.52 27.70 o 3 -5 9 481.40 494.26 22.42 o 3 -4 9 1480.63 1346.35 38.67 o 3 -3 9 597.30 570.17 22.51 o 3 -2 9 2658.86 2650.82 60.71 o 3 -1 9 222.20 262.03 16.26 o 3 0 9 335.84 422.14 19.63 o 3 1 9 224.14 261.73 17.26 o 3 2 9 2660.81 2642.59 61.55 o 3 3 9 600.29 653.27 25.24 o 3 4 9 1473.23 1388.66 37.65 o 3 5 9 488.71 469.08 21.25 o 3 -12 11 1200.83 1224.88 35.88 o 3 -11 11 53.01 79.83 15.25 o 3 -10 11 5750.57 5777.26 137.60 o 3 -9 11 1560.54 1631.68 42.38 o 3 -8 11 1206.24 1210.77 34.95 o 3 -7 11 2898.27 2990.29 65.90 o 3 -6 11 3844.91 4024.98 84.63 o 3 -5 11 394.12 407.56 20.75 o 3 -4 11 1731.51 1763.48 46.75 o 3 -3 11 128.90 138.13 17.33 o 3 -2 11 553.67 552.70 25.15 o 3 -1 11 240.90 233.32 18.23 o 3 0 11 46.81 63.00 15.33 o 3 1 11 244.67 228.75 17.91 o 3 2 11 542.77 557.56 25.97 o 3 3 11 129.68 144.35 19.00 o 3 4 11 1721.34 1746.24 48.17 o 3 5 11 398.50 429.56 22.54 o 3 -12 13 203.44 224.02 16.60 o 3 -11 13 136.48 120.90 15.54 o 3 -10 13 1161.84 1095.05 38.58 o 3 -9 13 56.70 47.03 14.68 o 3 -8 13 488.40 474.48 24.43 o 3 -7 13 1962.19 1994.69 54.00 o 3 -6 13 548.49 560.20 23.91 o 3 -5 13 379.54 443.99 23.44 o 3 -4 13 145.91 149.38 17.94 o 3 -3 13 408.82 447.42 21.27 o 3 -2 13 431.65 496.87 22.46 o 3 -1 13 482.09 475.53 22.44 o 3 0 13 71.68 75.49 14.83 o 3 1 13 491.39 544.05 23.27 o 3 2 13 435.87 464.98 25.34 o 3 3 13 410.19 432.06 30.53 o 3 4 13 143.86 132.89 16.12 o 3 5 13 380.32 452.48 22.99 o 3 -12 15 103.00 34.92 29.73 o 3 -11 15 150.33 126.63 24.08 o 3 -10 15 1.55 -12.63 17.60 o 3 -9 15 99.61 101.49 16.60 o 3 -8 15 39.51 37.43 15.95 o 3 -7 15 62.35 54.63 17.95 o 3 -6 15 131.66 105.82 18.50 o 3 -5 15 92.74 76.71 18.09 o 3 -4 15 22.88 14.60 15.41 o 3 -3 15 134.80 119.20 26.02 o 3 -2 15 148.87 113.54 15.70 o 3 -1 15 162.11 146.50 17.45 o 3 0 15 42.63 20.13 14.64 o 3 1 15 160.42 140.84 16.33 o 3 2 15 148.36 167.42 20.30 o 3 3 15 135.31 123.05 15.99 o 3 4 15 22.11 22.11 12.88 o 3 5 15 92.27 70.09 14.60 o 3 5 -17 106.66 143.19 13.73 o 3 6 -17 596.12 602.86 24.52 o 3 7 -17 810.01 863.33 27.54 o 3 8 -17 261.40 217.70 15.40 o 3 9 -17 1193.71 1207.43 41.37 o 3 10 -17 165.67 184.27 15.13 o 3 11 -17 242.79 231.64 16.33 o 3 12 -17 259.05 237.92 15.34 o 3 13 -17 371.69 340.76 21.67 o 3 14 -17 269.22 282.01 22.51 o 3 15 -17 67.19 70.21 12.25 o 3 16 -17 16.49 13.70 11.66 o 3 17 -17 87.90 88.20 13.49 o 3 18 -17 350.88 361.46 24.54 o 3 19 -17 359.43 346.52 39.29 o 3 20 -17 21.42 17.19 15.11 o 3 21 -17 159.46 128.58 23.32 o 3 22 -17 117.14 138.05 30.97 o 3 5 -15 136.70 139.20 14.18 o 3 6 -15 529.65 521.62 21.14 o 3 7 -15 727.31 718.85 27.87 o 3 8 -15 177.63 172.82 14.91 o 3 9 -15 439.05 420.19 20.59 o 3 10 -15 312.57 358.35 17.91 o 3 11 -15 895.98 877.80 29.56 o 3 12 -15 423.02 403.54 20.17 o 3 13 -15 524.94 489.06 22.09 o 3 14 -15 561.41 529.85 23.41 o 3 15 -15 281.71 336.49 18.15 o 3 16 -15 743.05 762.72 30.35 o 3 17 -15 391.30 368.30 19.64 o 3 18 -15 806.16 724.55 25.32 o 3 19 -15 95.89 107.05 12.87 o 3 20 -15 196.43 236.54 14.74 o 3 21 -15 127.82 162.27 15.46 o 3 22 -15 17.30 12.08 11.75 o 3 23 -15 900.96 839.16 29.22 o 3 5 -13 399.71 449.27 23.02 o 3 6 -13 1948.29 1824.25 49.71 o 3 7 -13 680.96 656.21 32.75 o 3 8 -13 1964.39 1916.85 53.98 o 3 9 -13 727.84 685.64 31.01 o 3 10 -13 1568.92 1523.57 46.99 o 3 11 -13 305.19 352.33 21.98 o 3 12 -13 431.03 407.80 27.33 o 3 13 -13 65.78 110.33 14.94 o 3 14 -13 1577.03 1542.11 41.26 o 3 15 -13 50.33 37.05 14.72 o 3 16 -13 44.31 34.30 14.85 o 3 17 -13 650.02 663.27 25.74 o 3 18 -13 310.02 314.90 20.16 o 3 19 -13 113.66 147.87 15.62 o 3 20 -13 2004.08 1995.59 82.46 o 3 21 -13 2041.31 1876.57 53.76 o 3 22 -13 190.19 250.48 17.41 o 3 23 -13 51.87 71.80 13.32 o 3 5 -11 1344.01 1323.13 47.91 o 3 6 -11 154.98 131.70 19.09 o 3 7 -11 586.35 625.44 30.80 o 3 8 -11 14.70 4.90 16.07 o 3 9 -11 466.24 439.93 30.70 o 3 10 -11 963.50 1039.85 41.83 o 3 11 -11 140.75 171.11 20.98 o 3 12 -11 327.87 367.38 24.37 o 3 13 -11 334.56 405.14 26.96 o 3 14 -11 922.10 943.25 39.57 o 3 15 -11 1764.77 1852.87 57.24 o 3 16 -11 1439.47 1427.36 43.30 o 3 17 -11 555.72 558.09 25.61 o 3 18 -11 415.20 484.46 23.15 o 3 19 -11 812.38 958.79 34.83 o 3 20 -11 73.59 74.59 13.61 o 3 21 -11 3212.25 3266.38 140.02 o 3 22 -11 788.08 796.74 34.07 o 3 23 -11 41.71 56.20 11.31 o 3 5 -9 175.16 218.47 18.54 o 3 6 -9 8237.88 8648.19 305.56 o 3 7 -9 2425.63 2664.85 127.52 o 3 8 -9 308.39 391.92 32.42 o 3 9 -9 238.30 291.45 28.80 o 3 10 -9 869.18 1038.82 51.97 o 3 11 -9 2463.71 2776.53 112.66 o 3 12 -9 237.50 271.08 16.60 o 3 13 -9 3172.10 3471.31 185.61 o 3 14 -9 565.07 710.39 41.27 o 3 15 -9 650.31 743.88 40.85 o 3 16 -9 201.72 259.76 19.53 o 3 17 -9 868.14 860.51 43.50 o 3 18 -9 712.93 738.08 50.40 o 3 19 -9 1008.00 1034.08 51.94 o 3 20 -9 1667.24 1735.27 72.61 o 3 21 -9 198.35 193.18 15.41 o 3 22 -9 287.48 356.46 17.72 o 3 23 -9 46.14 35.07 10.44 o 3 24 -9 1131.63 1190.88 50.73 o 3 6 -7 359.32 309.15 37.42 o 3 8 -7 1581.45 1903.10 111.53 o 3 9 -7 216.09 275.29 26.44 o 3 10 -7 2378.57 2595.29 89.70 o 3 11 -7 243.39 310.37 21.47 o 3 12 -7 847.15 819.36 29.82 o 3 13 -7 3449.00 3516.78 168.06 o 3 14 -7 1230.17 1201.97 40.15 o 3 15 -7 835.89 857.17 28.57 o 3 16 -7 42.96 35.60 7.81 o 3 17 -7 4525.90 4931.67 134.02 o 3 18 -7 475.02 475.02 18.73 o 3 19 -7 2815.27 3005.95 81.42 o 3 20 -7 1466.54 1660.54 54.73 o 3 21 -7 199.57 231.61 15.73 o 3 22 -7 1356.32 1432.09 36.75 o 3 23 -7 1453.26 1546.95 42.70 o 3 24 -7 2072.36 2180.38 52.49 o 3 6 -5 7322.38 7709.14 244.99 o 3 7 -5 1103.56 1183.53 39.50 o 3 8 -5 2202.23 2251.87 68.94 o 3 9 -5 6015.26 6010.55 173.27 o 3 10 -5 2261.93 2455.97 86.23 o 3 11 -5 903.92 925.68 39.98 o 3 12 -5 100.52 98.55 14.35 o 3 13 -5 492.24 535.77 25.27 o 3 14 -5 101.74 118.51 14.25 o 3 15 -5 2958.08 2896.58 83.40 o 3 16 -5 516.83 470.22 22.41 o 3 17 -5 4708.29 4772.58 131.53 o 3 18 -5 5552.67 5857.61 136.60 o 3 19 -5 242.33 272.18 15.91 o 3 20 -5 692.00 843.99 30.27 o 3 21 -5 1060.87 982.12 31.14 o 3 22 -5 244.73 292.81 14.75 o 3 23 -5 315.69 345.36 17.09 o 3 24 -5 1150.98 1262.42 33.10 o 3 6 -3 2006.74 1982.68 61.28 o 3 7 -3 706.44 659.46 26.54 o 3 8 -3 552.64 512.44 23.56 o 3 9 -3 477.77 474.36 22.83 o 3 10 -3 4970.90 4609.20 146.58 o 3 11 -3 1451.35 1425.93 48.33 o 3 12 -3 2827.77 2628.30 81.38 o 3 13 -3 346.75 317.89 16.46 o 3 14 -3 541.73 539.59 22.49 o 3 15 -3 669.37 703.34 23.84 o 3 16 -3 2258.12 2184.63 55.41 o 3 17 -3 4088.31 4111.39 97.80 o 3 18 -3 8284.87 8143.01 186.19 o 3 19 -3 158.84 165.18 15.33 o 3 20 -3 1228.84 1208.35 47.48 o 3 21 -3 2903.26 2823.98 70.43 o 3 22 -3 340.13 370.50 17.49 o 3 23 -3 5038.52 4987.86 104.97 o 3 24 -3 672.83 791.18 29.41 o 3 6 -1 17.32 14.35 6.17 o 3 7 -1 1336.66 1122.78 31.47 o 3 8 -1 1092.32 1023.42 28.24 o 3 9 -1 778.61 727.35 30.12 o 3 10 -1 843.21 705.81 21.34 o 3 11 -1 2848.39 2499.70 75.22 o 3 12 -1 1171.09 1074.88 30.00 o 3 13 -1 1746.12 1472.35 43.72 o 3 14 -1 24.24 18.28 7.15 o 3 15 -1 468.66 401.63 18.66 o 3 16 -1 2918.55 2591.21 63.00 o 3 17 -1 4942.54 4545.44 130.21 o 3 18 -1 964.78 846.17 23.15 o 3 19 -1 1033.98 991.57 28.33 o 3 20 -1 1390.49 1381.90 43.04 o 3 21 -1 68.01 49.76 6.87 o 3 22 -1 318.77 322.87 16.08 o 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972.98 28.34 o -5 8 3 2361.60 2387.92 68.97 o -3 8 3 372.20 357.49 12.56 o -1 8 3 952.77 865.90 31.68 o 1 8 3 4990.82 5276.85 171.07 o 3 8 3 1114.14 991.31 41.50 o 3 8 3 752.56 735.51 33.85 o 5 8 3 664.60 763.96 37.58 o 7 8 3 829.38 1056.67 72.42 o 9 8 3 417.48 349.27 40.34 o 11 8 3 999.61 1096.18 36.32 o 13 8 3 219.24 132.94 14.26 o 15 8 3 299.42 33.33 14.79 o -17 9 3 2.40 -2.06 14.90 o -15 9 3 202.98 129.85 17.09 o -13 9 3 117.65 96.73 14.67 o -11 9 3 111.24 108.74 13.28 o -9 9 3 312.84 343.01 17.06 o -7 9 3 355.62 407.47 17.01 o -5 9 3 2231.52 2223.09 57.81 o -3 9 3 321.68 345.98 12.60 o -1 9 3 426.29 382.96 20.29 o 1 9 3 3941.26 4056.16 120.56 o 3 9 3 105.09 104.26 9.24 o 3 9 3 70.95 68.25 13.90 o 5 9 3 420.20 496.19 26.69 o 7 9 3 1369.91 1550.84 64.02 o 9 9 3 1227.07 1367.97 58.07 o 11 9 3 192.62 140.03 15.35 o 13 9 3 220.13 94.08 12.90 o 15 9 3 146.65 10.37 9.77 o -17 10 3 63.85 19.23 14.37 o -15 10 3 116.45 90.93 16.61 o -13 10 3 574.70 683.67 48.71 o -11 10 3 213.49 242.48 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