#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:07:34 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180965 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/45/2204578.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204578_Fobs loop_ _publ_author_name 'He, Xiang' 'Lu, Can-Zhong' 'Yu, Ya-Qin' 'Chen, Shu-Mei' 'Wu, Xiao-Yuan' 'Liu, Jiu-Hui' _publ_section_title ; trans-Tetrakis(3-aminopyridine)dichlorocadmium(II) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1639 _journal_page_last m1640 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.159 _cell_angle_beta 69.668 _cell_angle_gamma 67.949 _cell_length_a 7.7792 _cell_length_b 8.7583 _cell_length_c 10.2481 _exptl_crystal_F_000 282.00 _reflns_d_resolution_high 0.8388 _cod_data_source_file wk6033Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' d in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 108.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2221.61 2090.57 30.30 o 2 0 0 9.88 9.28 0.40 o 3 0 0 2296.55 2153.76 31.44 o 4 0 0 435.69 382.89 6.27 o 5 0 0 515.61 538.60 18.75 o 6 0 0 1176.22 1213.45 32.27 o 7 0 0 283.89 272.83 8.76 o 8 0 0 19.02 14.10 2.46 o -7 1 0 16.43 17.64 1.99 o -6 1 0 262.86 257.18 10.35 o -5 1 0 336.02 335.36 6.96 o -4 1 0 5.44 9.78 3.24 o -3 1 0 1968.58 2014.57 29.49 o -2 1 0 2673.94 2755.39 71.10 o -1 1 0 1116.59 1056.71 18.99 o 0 1 0 2957.17 2926.48 73.41 o 1 1 0 340.45 356.76 9.24 o 2 1 0 180.20 161.18 2.55 o 3 1 0 435.93 373.73 6.31 o 4 1 0 2439.37 2369.69 34.67 o 5 1 0 460.59 436.42 7.51 o 6 1 0 326.37 322.43 9.69 o 7 1 0 423.60 425.34 12.59 o 8 1 0 162.49 147.92 5.68 o -7 2 0 3.54 2.14 1.80 o -6 2 0 245.08 248.39 9.60 o -5 2 0 569.82 555.77 10.99 o -4 2 0 16.82 17.69 0.94 o -3 2 0 462.10 476.66 9.19 o -2 2 0 3382.42 3448.64 61.62 o -1 2 0 3782.64 3733.19 66.45 o 0 2 0 238.52 251.16 6.76 o 1 2 0 2799.84 2896.46 56.29 o 2 2 0 482.52 473.96 10.57 o 3 2 0 314.08 300.99 4.71 o 4 2 0 4031.24 4165.77 60.63 o 5 2 0 469.64 481.41 28.85 o 6 2 0 4.37 4.57 1.00 o 7 2 0 150.12 143.34 5.17 o 8 2 0 211.34 215.35 7.38 o -7 3 0 99.07 85.41 4.03 o -6 3 0 17.43 15.18 1.71 o -5 3 0 170.03 163.11 3.30 o -4 3 0 530.90 522.11 10.34 o -3 3 0 7.33 7.00 0.72 o -2 3 0 456.65 391.31 6.79 o -1 3 0 3490.00 3502.00 62.53 o 0 3 0 184.07 200.13 3.94 o 1 3 0 219.47 216.81 4.24 o 2 3 0 2580.62 2648.07 38.58 o 3 3 0 134.03 109.56 5.88 o 4 3 0 42.52 41.02 2.40 o 5 3 0 1366.16 1349.21 24.79 o 6 3 0 227.83 232.54 5.06 o 7 3 0 93.49 97.87 7.77 o 8 3 0 173.56 183.78 6.42 o -6 4 0 61.68 59.62 2.34 o -5 4 0 133.61 124.00 2.82 o -4 4 0 833.19 886.80 17.02 o -3 4 0 365.02 399.52 8.12 o -2 4 0 616.18 677.59 12.87 o -1 4 0 1643.48 1678.94 30.27 o 0 4 0 820.27 770.25 14.20 o 1 4 0 311.02 339.47 6.55 o 2 4 0 2455.87 2507.89 36.65 o 3 4 0 1706.40 1854.72 27.28 o 4 4 0 207.38 206.69 11.21 o 5 4 0 1030.56 1096.54 20.40 o 6 4 0 272.14 272.45 14.47 o 7 4 0 78.59 78.12 2.35 o 8 4 0 127.52 132.31 4.88 o -5 5 0 2.50 8.24 2.05 o -4 5 0 227.99 236.17 11.34 o -3 5 0 602.24 596.12 11.78 o -2 5 0 115.83 136.16 6.90 o -1 5 0 131.62 114.77 2.61 o 0 5 0 1753.11 1828.38 33.07 o 1 5 0 392.84 426.17 8.23 o 2 5 0 502.28 507.32 12.51 o 3 5 0 2134.61 2233.37 32.83 o 4 5 0 733.48 801.41 23.18 o 5 5 0 89.24 101.42 6.98 o 6 5 0 671.04 667.79 20.42 o 7 5 0 362.92 362.16 19.45 o 8 5 0 54.90 53.33 3.08 o -5 6 0 31.42 36.47 3.27 o -4 6 0 14.42 18.40 1.70 o -3 6 0 325.03 323.60 9.90 o -2 6 0 501.55 486.30 13.95 o -1 6 0 156.23 161.96 5.45 o 0 6 0 380.43 343.15 6.88 o 1 6 0 350.80 316.59 21.43 o 2 6 0 100.92 108.32 3.78 o 3 6 0 621.83 622.70 13.21 o 4 6 0 1373.27 1392.54 25.63 o 5 6 0 32.06 25.72 1.87 o 6 6 0 170.72 168.79 5.85 o 7 6 0 204.65 205.85 7.00 o 8 6 0 44.47 56.64 3.35 o -4 7 0 10.23 17.51 2.54 o -3 7 0 40.74 36.45 2.63 o -2 7 0 138.30 130.43 5.09 o -1 7 0 1.06 -1.08 1.08 o 0 7 0 23.07 18.96 1.61 o 1 7 0 1042.35 990.88 35.49 o 2 7 0 322.86 314.92 6.52 o 3 7 0 105.66 97.39 3.67 o 4 7 0 451.79 458.29 13.23 o 5 7 0 43.83 31.17 2.12 o 6 7 0 43.56 41.64 2.67 o 7 7 0 231.15 212.72 7.40 o -2 8 0 104.48 82.55 3.69 o -1 8 0 160.86 139.10 5.19 o 0 8 0 41.90 37.30 2.33 o 1 8 0 258.94 225.46 16.36 o 2 8 0 446.97 417.28 15.79 o 3 8 0 106.05 108.01 4.20 o 4 8 0 6.83 0.23 1.67 o 5 8 0 121.95 110.13 4.47 o 6 8 0 106.61 111.39 4.62 o -1 9 0 224.15 183.20 6.57 o 0 9 0 136.04 120.27 4.71 o 1 9 0 29.73 18.81 2.20 o 2 9 0 165.85 164.67 5.62 o 3 9 0 116.45 126.27 4.73 o 4 9 0 33.96 41.07 2.67 o 5 9 0 515.76 510.21 15.01 o -4 -9 1 110.70 120.89 5.05 o -3 -9 1 123.26 141.75 5.39 o -2 -9 1 106.44 120.16 4.69 o -1 -9 1 3.90 -1.65 1.67 o 0 -9 1 154.33 138.46 5.28 o -6 -8 1 96.06 108.84 5.07 o -5 -8 1 147.83 130.60 5.26 o -4 -8 1 2.04 7.87 1.85 o -3 -8 1 29.11 29.56 2.08 o -2 -8 1 385.19 348.49 7.66 o -1 -8 1 87.66 91.09 3.94 o 0 -8 1 66.76 59.24 3.16 o 1 -8 1 80.12 62.30 3.16 o 2 -8 1 2.74 -1.53 1.53 o -7 -7 1 52.60 60.26 3.71 o -6 -7 1 31.44 33.29 2.61 o -5 -7 1 848.40 812.86 22.50 o -4 -7 1 257.48 240.58 7.80 o -3 -7 1 32.14 30.22 2.04 o -2 -7 1 285.90 281.45 6.00 o -1 -7 1 420.96 399.61 8.12 o 0 -7 1 84.51 73.37 3.35 o 1 -7 1 121.50 111.53 4.43 o 2 -7 1 244.33 218.04 7.23 o 3 -7 1 28.01 18.83 2.08 o -7 -6 1 302.54 307.33 9.88 o -6 -6 1 232.31 235.58 7.84 o -5 -6 1 325.63 342.66 10.39 o -4 -6 1 223.28 220.95 7.12 o -3 -6 1 316.81 304.59 12.22 o -2 -6 1 106.63 98.72 2.50 o -1 -6 1 726.71 685.48 13.07 o 0 -6 1 380.77 398.24 20.82 o 1 -6 1 86.04 76.08 3.31 o 2 -6 1 465.23 459.56 13.32 o 3 -6 1 344.82 342.49 7.36 o 4 -6 1 3.49 7.13 9.82 o 5 -6 1 30.84 26.08 2.61 o -8 -5 1 73.45 72.11 3.75 o -7 -5 1 534.90 534.28 15.41 o -6 -5 1 674.59 682.29 19.06 o -5 -5 1 0.85 1.32 1.17 o -4 -5 1 776.17 832.84 15.63 o -3 -5 1 1400.55 1460.69 21.70 o -2 -5 1 316.05 335.48 5.37 o -1 -5 1 2178.78 2341.90 61.31 o 0 -5 1 1560.13 1568.52 28.54 o 1 -5 1 104.59 112.16 2.66 o 2 -5 1 232.07 251.09 5.43 o 3 -5 1 718.44 709.66 23.31 o 4 -5 1 81.47 85.65 4.85 o 5 -5 1 51.47 57.10 2.51 o -7 -4 1 113.93 110.07 12.60 o -6 -4 1 714.85 770.72 25.19 o -5 -4 1 0.63 -2.20 2.57 o -4 -4 1 137.03 135.35 5.24 o -3 -4 1 1044.76 1027.98 21.15 o -2 -4 1 1290.63 1271.84 18.83 o -1 -4 1 290.32 297.69 8.11 o 0 -4 1 707.15 685.70 12.76 o 1 -4 1 1041.32 968.11 14.48 o 2 -4 1 173.61 161.44 3.65 o 3 -4 1 301.86 291.25 11.88 o 4 -4 1 517.82 548.00 19.58 o 5 -4 1 65.42 67.62 4.33 o 6 -4 1 66.20 72.17 9.31 o -8 -3 1 127.10 142.41 5.45 o -7 -3 1 23.72 21.78 8.58 o -6 -3 1 258.15 253.46 13.26 o -5 -3 1 462.55 481.79 9.43 o -4 -3 1 162.43 140.40 5.99 o -3 -3 1 1197.70 1183.29 17.55 o -2 -3 1 2546.06 2523.27 36.81 o -1 -3 1 113.15 98.42 1.72 o 0 -3 1 1117.41 1123.76 20.37 o 1 -3 1 929.30 864.77 12.87 o 2 -3 1 101.09 101.06 1.81 o 3 -3 1 7.25 2.30 1.92 o 4 -3 1 618.75 668.24 30.79 o 5 -3 1 182.11 208.53 4.88 o 6 -3 1 12.21 17.37 3.15 o 7 -3 1 105.26 93.77 4.41 o -8 -2 1 264.83 260.68 8.54 o -7 -2 1 78.18 82.14 3.60 o -6 -2 1 73.39 64.73 6.56 o -5 -2 1 1095.92 1048.77 19.40 o -4 -2 1 1183.88 1149.88 17.15 o -3 -2 1 644.50 709.15 10.67 o -2 -2 1 3413.54 3423.70 49.76 o -1 -2 1 617.32 607.05 9.01 o 0 -2 1 890.04 979.15 17.68 o 1 -2 1 360.68 341.73 8.99 o 2 -2 1 4135.77 4278.46 76.28 o 3 -2 1 485.45 551.67 10.53 o 4 -2 1 477.05 558.04 17.93 o 5 -2 1 588.58 584.65 11.50 o 6 -2 1 37.84 37.76 1.37 o 7 -2 1 21.41 17.64 2.38 o -8 -1 1 96.90 96.33 4.37 o -7 -1 1 575.23 556.86 15.92 o -6 -1 1 331.39 347.26 10.35 o -5 -1 1 1200.89 1195.69 17.93 o -4 -1 1 1805.52 1758.16 28.85 o -3 -1 1 410.95 389.78 9.72 o -2 -1 1 1235.32 1264.23 18.56 o -1 -1 1 6483.80 6783.39 98.11 o 0 -1 1 335.73 295.58 4.41 o 1 -1 1 2808.27 2848.21 41.33 o 2 -1 1 2464.55 2464.41 44.04 o 3 -1 1 1327.53 1273.46 18.76 o 4 -1 1 408.85 478.20 20.14 o 5 -1 1 243.48 226.73 10.62 o 6 -1 1 278.29 263.38 5.80 o 7 -1 1 49.09 45.36 2.78 o 8 -1 1 75.67 83.16 4.14 o -8 0 1 31.01 37.98 2.74 o -7 0 1 317.19 329.02 10.30 o -6 0 1 232.29 224.34 7.31 o -5 0 1 17.31 19.13 1.02 o -4 0 1 2185.82 2299.89 33.76 o -3 0 1 1831.87 1813.30 26.60 o -2 0 1 28.24 35.53 2.58 o -1 0 1 3792.61 3767.68 54.59 o 0 0 1 4965.95 4961.59 87.89 o 1 0 1 6401.85 5763.61 181.29 o 2 0 1 2419.34 2380.74 81.92 o 3 0 1 3212.04 3261.81 84.03 o 4 0 1 164.88 146.35 7.13 o 5 0 1 342.36 337.60 6.81 o 6 0 1 1910.43 1916.18 49.91 o 7 0 1 448.58 427.77 12.85 o 8 0 1 1.14 -1.48 1.80 o -7 1 1 35.36 38.61 2.67 o -6 1 1 335.28 338.59 7.19 o -5 1 1 150.90 151.55 3.60 o -4 1 1 421.54 451.48 7.09 o -3 1 1 2394.79 2442.64 35.74 o -2 1 1 2022.01 2129.60 31.10 o -1 1 1 537.46 595.89 10.87 o 0 1 1 1175.08 1215.68 30.66 o 1 1 1 2290.30 2127.06 37.76 o 2 1 1 460.65 461.46 8.41 o 3 1 1 2831.05 2725.24 48.62 o 4 1 1 856.79 751.39 11.30 o 5 1 1 174.12 173.42 2.99 o 6 1 1 139.31 138.55 4.92 o 7 1 1 246.58 213.14 7.13 o 8 1 1 31.33 44.99 2.84 o -7 2 1 0.22 1.65 1.89 o -6 2 1 270.60 274.57 6.13 o -5 2 1 622.97 705.42 13.70 o -4 2 1 8.52 7.56 1.45 o -3 2 1 316.01 284.82 5.81 o -2 2 1 683.51 643.10 9.79 o -1 2 1 709.36 712.10 13.05 o 0 2 1 11878.16 11969.30 299.79 o 1 2 1 4943.06 4602.20 81.60 o 2 2 1 112.49 101.97 3.08 o 3 2 1 515.72 504.64 9.25 o 4 2 1 981.23 870.10 21.62 o 5 2 1 703.53 724.86 13.67 o 6 2 1 151.31 162.59 10.63 o 7 2 1 184.65 203.98 6.91 o 8 2 1 155.55 163.23 5.96 o -6 3 1 68.76 68.45 9.48 o -5 3 1 696.23 687.63 32.96 o -4 3 1 203.78 193.29 4.43 o -3 3 1 27.68 26.04 2.12 o -2 3 1 885.66 819.39 15.25 o -1 3 1 2613.93 2490.88 44.66 o 0 3 1 1475.82 1484.74 37.83 o 1 3 1 874.77 820.39 21.01 o 2 3 1 2306.56 2421.05 43.15 o 3 3 1 102.79 137.79 6.10 o 4 3 1 332.21 300.53 8.54 o 5 3 1 1290.33 1306.91 24.06 o 6 3 1 209.96 217.27 8.89 o 7 3 1 47.58 52.41 1.79 o 8 3 1 430.38 413.69 12.57 o -6 4 1 50.28 45.52 2.10 o -5 4 1 233.22 222.69 5.27 o -4 4 1 451.49 437.63 9.03 o -3 4 1 171.66 177.21 6.96 o -2 4 1 343.74 362.74 7.34 o -1 4 1 4378.43 4482.18 113.25 o 0 4 1 903.73 984.24 25.53 o 1 4 1 1354.36 1377.49 35.16 o 2 4 1 2657.71 2697.74 48.18 o 3 4 1 588.79 570.65 10.53 o 4 4 1 1321.00 1414.72 36.49 o 5 4 1 1230.98 1262.12 23.33 o 6 4 1 489.33 503.42 10.04 o 7 4 1 182.52 173.85 12.35 o 8 4 1 307.94 328.83 10.16 o -5 5 1 5.03 7.74 3.03 o -4 5 1 234.61 230.33 11.22 o -3 5 1 423.01 436.25 9.51 o -2 5 1 145.71 157.97 5.34 o -1 5 1 1854.01 2173.01 55.91 o 0 5 1 745.34 771.35 20.46 o 1 5 1 1.89 3.14 0.64 o 2 5 1 355.51 346.35 11.69 o 3 5 1 1986.51 1875.09 33.72 o 4 5 1 273.25 323.74 15.54 o 5 5 1 465.44 505.82 16.31 o 6 5 1 750.57 766.31 14.78 o 7 5 1 262.91 253.35 5.67 o 8 5 1 48.04 51.53 4.51 o -4 6 1 60.90 61.48 2.39 o -3 6 1 292.90 274.78 8.76 o -2 6 1 308.91 312.15 9.58 o -1 6 1 155.40 160.68 5.32 o 0 6 1 535.44 476.87 9.22 o 1 6 1 234.91 221.31 6.62 o 2 6 1 50.78 41.97 1.33 o 3 6 1 1014.05 1036.04 21.96 o 4 6 1 1022.69 1029.47 19.18 o 5 6 1 418.22 419.25 8.48 o 6 6 1 155.29 157.17 3.83 o 7 6 1 203.10 210.87 9.10 o 8 6 1 17.72 16.22 2.14 o -4 7 1 17.62 7.04 2.33 o -3 7 1 117.91 118.63 4.56 o -2 7 1 155.09 135.69 5.03 o -1 7 1 45.72 44.72 2.33 o 0 7 1 82.08 69.27 3.03 o 1 7 1 703.13 678.03 14.37 o 2 7 1 215.31 192.86 9.48 o 3 7 1 181.85 184.13 12.22 o 4 7 1 468.15 477.09 24.84 o 5 7 1 2.57 0.26 1.51 o 6 7 1 16.43 14.35 1.74 o 7 7 1 359.46 317.81 9.99 o 8 7 1 120.69 109.56 4.71 o -2 8 1 314.62 306.80 9.84 o -1 8 1 295.28 316.87 10.01 o 0 8 1 52.13 37.32 2.29 o 1 8 1 250.34 230.28 10.27 o 2 8 1 392.21 375.90 7.67 o 3 8 1 72.62 66.94 2.90 o 4 8 1 388.55 384.96 11.45 o 5 8 1 261.02 265.14 8.48 o 6 8 1 72.11 73.35 3.48 o 7 8 1 73.92 58.86 3.63 o -1 9 1 121.06 107.40 4.54 o 0 9 1 20.47 11.94 1.85 o 1 9 1 81.61 54.71 2.86 o 2 9 1 258.22 220.65 6.96 o 3 9 1 132.36 126.00 4.62 o 4 9 1 127.47 127.54 4.83 o 5 9 1 261.43 258.56 8.42 o 6 9 1 189.75 186.22 6.70 o 3 10 1 327.36 292.49 9.08 o 4 10 1 3.92 -1.04 1.76 o -3 -9 2 172.97 185.68 6.51 o -2 -9 2 67.37 68.68 3.35 o -1 -9 2 29.82 39.52 2.95 o -5 -8 2 68.40 65.16 3.56 o -4 -8 2 54.88 57.14 3.22 o -3 -8 2 147.19 147.37 5.45 o -2 -8 2 267.76 244.59 5.53 o -1 -8 2 71.14 65.31 3.22 o 0 -8 2 38.75 45.67 2.86 o 1 -8 2 80.27 68.85 3.63 o 2 -8 2 0.13 -1.42 1.87 o -6 -7 2 41.95 46.69 3.03 o -5 -7 2 407.98 405.08 12.34 o -4 -7 2 497.83 526.71 15.22 o -3 -7 2 57.33 52.39 2.74 o -2 -7 2 338.98 327.27 25.16 o -1 -7 2 62.71 63.32 2.01 o 0 -7 2 8.70 13.82 1.70 o 1 -7 2 440.91 467.13 13.74 o 2 -7 2 313.32 294.72 9.50 o 3 -7 2 6.83 0.34 1.91 o -7 -6 2 200.46 203.29 7.17 o -6 -6 2 112.85 122.47 4.92 o -5 -6 2 444.07 462.95 13.61 o -4 -6 2 664.62 699.36 19.46 o -3 -6 2 94.95 98.86 2.64 o -2 -6 2 229.43 217.16 5.78 o -1 -6 2 553.51 543.88 12.62 o 0 -6 2 371.66 387.14 16.66 o 1 -6 2 124.31 124.74 4.62 o 2 -6 2 295.00 293.23 9.24 o 3 -6 2 116.70 119.47 4.75 o 4 -6 2 36.71 25.47 2.29 o -7 -5 2 284.37 266.62 8.65 o -6 -5 2 110.81 109.24 4.41 o -5 -5 2 479.61 514.12 14.70 o -4 -5 2 517.44 532.99 15.06 o -3 -5 2 437.72 462.99 20.88 o -2 -5 2 113.80 130.14 3.12 o -1 -5 2 1063.31 1105.37 20.46 o 0 -5 2 1632.60 1707.32 31.10 o 1 -5 2 97.36 99.16 3.89 o 2 -5 2 317.38 320.40 6.78 o 3 -5 2 711.84 686.48 13.39 o 4 -5 2 86.36 91.31 2.66 o 5 -5 2 116.51 122.93 3.65 o -7 -4 2 148.40 113.95 4.41 o -6 -4 2 700.04 689.77 19.10 o -5 -4 2 337.76 333.99 9.99 o -4 -4 2 19.73 15.48 1.15 o -3 -4 2 563.74 559.89 9.78 o -2 -4 2 215.70 209.12 3.48 o -1 -4 2 270.94 288.06 6.39 o 0 -4 2 1663.31 1682.94 30.51 o 1 -4 2 344.59 327.37 5.25 o 2 -4 2 1.04 1.44 2.69 o 3 -4 2 583.89 555.51 12.25 o 4 -4 2 258.20 238.31 7.35 o 5 -4 2 6.00 2.69 1.05 o 6 -4 2 56.67 53.89 3.98 o -7 -3 2 23.74 20.07 1.40 o -6 -3 2 567.37 575.78 11.28 o -5 -3 2 67.97 60.14 1.80 o -4 -3 2 126.86 137.58 5.92 o -3 -3 2 1558.35 1574.27 23.25 o -2 -3 2 1154.53 1258.40 18.60 o -1 -3 2 998.58 1028.24 15.22 o 0 -3 2 624.15 582.45 11.48 o 1 -3 2 1153.24 1140.79 16.92 o 2 -3 2 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1.89 o 5 8 9 49.26 53.44 3.01 o 6 8 9 172.61 173.81 6.62 o 3 9 9 215.56 243.51 8.61 o 4 9 9 100.56 88.93 4.31 o 5 9 9 4.54 2.52 2.18 o -1 -2 10 110.25 102.08 4.94 o 0 -2 10 29.39 21.71 2.74 o 1 -2 10 64.36 78.82 3.97 o 2 -2 10 184.25 199.85 7.38 o 3 -2 10 80.70 89.33 4.54 o -1 -1 10 89.90 76.31 3.96 o 0 -1 10 263.05 258.50 8.72 o 1 -1 10 26.69 26.04 2.44 o 2 -1 10 88.67 74.15 3.71 o 3 -1 10 223.67 244.50 8.36 o 4 -1 10 50.56 74.79 3.99 o 5 -1 10 17.68 23.96 2.73 o -2 0 10 142.53 133.80 5.19 o -1 0 10 20.63 22.18 2.37 o 0 0 10 277.08 278.64 9.24 o 1 0 10 231.62 238.95 8.14 o 2 0 10 208.59 194.25 6.93 o 3 0 10 262.29 249.00 8.23 o 4 0 10 409.41 428.69 13.04 o 5 0 10 62.09 72.12 3.79 o 6 0 10 50.51 66.43 3.61 o -2 1 10 190.92 175.55 6.40 o -1 1 10 72.81 59.75 3.20 o 0 1 10 66.78 70.46 3.24 o 1 1 10 410.66 417.60 12.59 o 2 1 10 113.92 104.09 4.41 o 3 1 10 47.34 48.15 2.84 o 4 1 10 351.62 340.18 10.54 o 5 1 10 53.14 65.16 3.37 o -2 2 10 75.84 73.96 3.67 o -1 2 10 174.60 172.64 6.25 o 0 2 10 1.14 3.29 1.61 o 1 2 10 511.79 458.67 13.55 o 2 2 10 372.38 385.17 11.62 o 3 2 10 30.04 31.25 2.31 o 4 2 10 95.88 95.00 3.96 o 5 2 10 309.46 357.19 10.84 o 7 2 10 23.54 39.40 3.22 o -2 3 10 28.61 25.78 2.69 o -1 3 10 80.01 71.16 3.56 o 0 3 10 54.55 44.99 2.67 o 1 3 10 207.23 179.17 6.17 o 2 3 10 332.91 332.47 11.49 o 3 3 10 220.41 220.55 19.87 o 4 3 10 1.93 8.78 3.60 o 5 3 10 95.26 83.79 4.35 o 6 3 10 108.35 80.00 3.77 o 7 3 10 11.34 12.26 2.23 o -1 4 10 235.81 239.10 8.29 o 0 4 10 1110.69 1145.60 31.04 o 1 4 10 88.08 93.03 4.38 o 2 4 10 39.20 38.79 3.85 o 3 4 10 405.45 387.67 8.08 o 4 4 10 65.08 66.93 2.25 o 5 4 10 278.31 254.92 8.31 o 6 4 10 549.37 539.73 15.80 o 7 4 10 62.95 48.22 3.07 o -1 5 10 49.56 46.14 3.12 o 0 5 10 358.11 381.63 11.85 o 1 5 10 66.64 65.95 3.37 o 2 5 10 31.66 22.45 1.50 o 3 5 10 210.50 195.70 4.65 o 4 5 10 384.10 375.67 7.94 o 5 5 10 213.69 213.80 7.49 o 6 5 10 233.16 229.45 7.89 o 7 5 10 204.01 181.06 6.66 o 0 6 10 57.16 47.20 3.14 o 1 6 10 168.02 166.62 6.25 o 2 6 10 112.48 99.27 5.25 o 3 6 10 157.43 156.26 4.02 o 4 6 10 690.73 682.33 19.34 o 5 6 10 89.40 93.94 4.16 o 6 6 10 4.14 7.49 2.06 o 7 6 10 191.02 184.73 7.06 o 1 7 10 59.27 43.21 3.08 o 2 7 10 173.78 177.04 6.66 o 3 7 10 21.56 23.50 6.83 o 4 7 10 87.10 86.05 4.05 o 5 7 10 270.84 292.91 9.56 o 6 7 10 41.09 38.95 3.22 o 3 8 10 125.65 130.47 5.60 o 4 8 10 44.20 33.37 2.74 o 5 8 10 209.34 225.93 7.99 o 1 -1 11 23.37 21.93 2.63 o 2 -1 11 142.30 155.43 6.11 o 3 -1 11 217.99 213.10 7.74 o 0 0 11 92.23 91.03 4.30 o 1 0 11 135.37 126.70 5.24 o 2 0 11 74.88 65.52 3.52 o 3 0 11 135.78 126.82 5.20 o 4 0 11 135.69 141.62 5.60 o 0 1 11 135.91 136.15 5.39 o 1 1 11 136.34 134.80 5.41 o 2 1 11 21.41 37.68 2.76 o 3 1 11 21.15 21.61 2.35 o 4 1 11 244.12 254.49 8.57 o 5 1 11 116.61 128.63 5.17 o 0 2 11 0.84 -1.32 1.32 o 1 2 11 101.55 93.30 3.97 o 3 2 11 45.08 45.65 2.91 o 4 2 11 171.21 179.85 6.40 o 5 2 11 189.62 197.75 6.91 o 0 3 11 36.40 26.93 2.21 o 1 3 11 113.31 106.06 4.39 o 2 3 11 344.61 325.65 10.12 o 3 3 11 147.49 150.55 5.56 o 4 3 11 77.32 72.56 3.50 o 5 3 11 51.86 65.73 3.27 o 0 4 11 178.61 184.90 6.74 o 1 4 11 173.45 153.73 5.73 o 2 4 11 179.60 168.07 6.04 o 3 4 11 231.37 225.07 5.21 o 4 4 11 47.06 49.12 8.24 o 5 4 11 161.16 161.89 5.94 o 6 4 11 632.43 591.51 17.17 o 1 5 11 189.33 184.20 13.48 o 2 5 11 52.24 53.66 2.19 o 3 5 11 311.56 313.94 6.93 o 4 5 11 147.25 143.14 9.37 o 5 5 11 29.36 30.77 2.67 o 6 5 11 152.97 125.68 5.28 o 2 6 11 18.28 23.85 2.46 o 3 6 11 120.73 113.52 7.84 o 4 6 11 196.35 196.95 7.00 o 5 6 11 92.62 105.05 4.54 o 6 6 11 74.25 66.35 3.65 o 3 7 11 0.57 -1.68 1.68 o 4 7 11 80.71 70.99 3.73 o 5 7 11 210.74 208.57 7.42 o 2 2 12 191.04 183.08 6.85 o 3 2 12 23.22 18.41 2.40 o 2 3 12 213.11 219.46 7.61 o 3 3 12 14.17 19.59 2.35 o 4 3 12 53.87 56.30 3.39 o 2 4 12 182.96 183.90 6.57 o 3 4 12 104.60 102.76 4.39 o 4 4 12 38.99 40.67 2.97 o 4 5 12 199.73 220.78 7.48 o