data_2239919 _cell_angle_alpha 103.837 _cell_angle_beta 99.173 _cell_angle_gamma 99.772 _cell_length_a 9.7912 _cell_length_b 14.7873 _cell_length_c 16.3592 _exptl_crystal_F_000 996.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file wm5039Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _TransRh2Phen4oPhCNp10Toluene' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 533.24 531.68 15.77 o 3 0 0 4023.15 3864.23 35.26 o 4 0 0 3538.17 3271.50 36.20 o 5 0 0 14273.76 14418.06 157.20 o 6 0 0 9929.58 10276.29 129.09 o 7 0 0 7139.40 7021.79 149.08 o 8 0 0 5009.90 4840.09 196.79 o 9 0 0 2421.08 2424.16 75.97 o 10 0 0 2238.33 2445.29 92.75 o 11 0 0 1706.95 1603.83 79.30 o 12 0 0 834.59 789.77 57.91 o -12 1 0 74.93 75.91 34.36 o -11 1 0 224.36 309.19 96.75 o -10 1 0 5.02 -32.52 40.22 o -9 1 0 505.04 473.13 34.66 o -8 1 0 931.39 945.27 28.97 o -7 1 0 298.30 289.06 21.55 o -6 1 0 7.99 55.57 10.34 o -5 1 0 1974.20 2097.37 30.26 o -4 1 0 1225.81 1179.06 19.36 o -3 1 0 1828.76 1891.05 21.39 o -2 1 0 230.36 231.99 7.34 o 2 1 0 4146.88 4140.25 54.53 o 3 1 0 803.54 871.22 19.86 o 4 1 0 100.59 87.65 12.28 o 5 1 0 520.88 522.08 17.22 o 6 1 0 5.73 -4.20 17.41 o 7 1 0 122.79 136.42 38.07 o 8 1 0 250.27 298.46 30.22 o 9 1 0 226.28 247.95 77.13 o 10 1 0 151.03 143.99 42.03 o 11 1 0 105.34 127.32 59.40 o 12 1 0 35.81 -37.00 43.13 o -12 2 0 515.80 558.70 119.56 o -11 2 0 145.51 96.65 30.11 o -10 2 0 521.70 536.73 38.46 o -9 2 0 1757.05 1887.60 109.14 o -8 2 0 1474.63 1422.43 53.72 o -7 2 0 6598.69 6523.34 92.61 o -6 2 0 11789.28 11897.96 211.22 o -5 2 0 4800.71 4686.14 56.43 o -4 2 0 5642.36 5802.34 100.65 o -3 2 0 2852.61 2684.23 27.75 o -2 2 0 12819.57 13266.93 218.39 o -1 2 0 25574.92 26905.21 414.46 o 1 2 0 33558.01 32649.76 1110.57 o 2 2 0 47187.53 47714.87 441.34 o 3 2 0 26968.61 27420.01 234.17 o 4 2 0 17895.37 18007.79 412.94 o 5 2 0 6929.65 6757.86 114.06 o 6 2 0 5754.62 5601.39 332.10 o 7 2 0 4935.46 4891.77 135.70 o 8 2 0 3766.75 4059.49 135.59 o 9 2 0 3200.77 3065.09 96.66 o 10 2 0 3953.60 3960.14 125.14 o 11 2 0 1532.93 1576.51 77.37 o -12 3 0 110.74 32.85 47.54 o -11 3 0 397.08 351.00 36.53 o -10 3 0 45.11 59.70 17.58 o -9 3 0 23.06 43.94 14.92 o -8 3 0 210.37 236.29 19.22 o -7 3 0 587.46 589.77 24.76 o -6 3 0 2569.13 2683.07 76.58 o -5 3 0 1269.86 1306.83 22.28 o -4 3 0 43.04 124.29 16.93 o -3 3 0 3.44 23.31 9.77 o -2 3 0 0.40 10.36 10.84 o -1 3 0 15362.18 16156.99 219.45 o 0 3 0 0.61 4.01 9.52 o 1 3 0 381.96 366.50 10.11 o 2 3 0 2607.82 2793.91 25.37 o 3 3 0 270.96 259.16 8.74 o 4 3 0 189.96 183.76 7.76 o 5 3 0 1.02 9.41 7.42 o 6 3 0 8.61 -10.63 17.57 o 7 3 0 64.69 91.01 23.73 o 8 3 0 14.27 15.95 48.53 o 9 3 0 164.65 242.82 34.69 o 10 3 0 13.47 6.30 28.06 o 11 3 0 59.81 30.61 41.29 o -12 4 0 14.94 40.50 47.85 o -11 4 0 107.55 103.99 60.84 o -10 4 0 65.35 42.95 18.11 o -9 4 0 78.83 86.92 35.81 o -8 4 0 540.95 523.20 30.23 o -7 4 0 1731.84 1817.19 53.84 o -6 4 0 1962.84 1890.20 62.81 o -5 4 0 1950.27 2008.36 37.46 o -4 4 0 4431.74 4357.18 61.79 o -3 4 0 2495.99 2396.46 44.48 o -2 4 0 3500.63 3615.47 137.16 o -1 4 0 6.10 13.60 5.74 o 0 4 0 923.94 875.25 14.25 o 1 4 0 39.06 73.18 17.17 o 2 4 0 24208.97 25349.33 284.68 o 3 4 0 30530.37 31653.61 535.62 o 4 4 0 11953.39 11096.09 189.37 o 5 4 0 2760.48 2595.62 59.27 o 6 4 0 2425.87 2582.08 66.97 o 7 4 0 2512.46 2590.86 76.77 o 8 4 0 2320.87 2421.76 84.83 o 9 4 0 3348.58 3501.82 113.70 o 10 4 0 2844.57 2971.01 111.04 o 11 4 0 1060.04 1110.22 73.79 o -12 5 0 3.81 35.73 46.97 o -11 5 0 27.94 55.00 27.30 o -10 5 0 5.86 4.41 28.37 o -9 5 0 51.66 47.21 23.04 o -8 5 0 44.31 47.88 28.05 o -7 5 0 113.03 137.85 21.93 o -6 5 0 1117.67 1136.16 37.51 o -5 5 0 3084.88 3175.36 73.65 o -4 5 0 835.71 988.69 50.63 o -3 5 0 137.96 173.13 16.29 o -2 5 0 268.29 276.83 19.18 o -1 5 0 352.27 347.87 11.39 o 0 5 0 182.65 238.76 28.97 o 1 5 0 0.58 -0.28 10.10 o 2 5 0 64.90 45.99 13.33 o 3 5 0 304.73 342.49 35.77 o 4 5 0 63.85 72.60 10.35 o 5 5 0 468.53 509.36 57.58 o 6 5 0 329.41 357.34 30.44 o 7 5 0 1.00 -22.00 23.64 o 8 5 0 14.07 4.91 24.73 o 9 5 0 4.91 38.18 30.14 o 10 5 0 88.86 107.74 55.52 o 11 5 0 143.85 259.09 176.50 o -12 6 0 11.73 -24.49 46.36 o -11 6 0 8.85 70.35 26.99 o -10 6 0 40.80 77.63 24.98 o -9 6 0 115.42 119.37 21.39 o -8 6 0 2.78 -5.33 12.35 o -7 6 0 47.61 113.20 32.04 o -6 6 0 86.06 151.47 26.13 o -5 6 0 280.99 290.52 21.23 o -4 6 0 1222.51 1146.98 77.44 o -3 6 0 3244.91 3352.86 60.26 o -2 6 0 41.22 58.45 4.83 o -1 6 0 1089.39 1236.13 29.49 o 0 6 0 367.15 337.98 12.95 o 1 6 0 227.48 291.91 13.39 o 2 6 0 1144.80 995.49 23.11 o 3 6 0 549.09 531.44 14.43 o 4 6 0 1808.84 1787.83 48.15 o 5 6 0 3196.12 3251.72 92.77 o 6 6 0 2700.73 2613.94 74.47 o 7 6 0 1590.25 1771.14 67.24 o 8 6 0 1351.70 1279.47 61.57 o 9 6 0 306.82 319.97 41.23 o 10 6 0 767.81 795.23 61.18 o -12 7 0 121.37 139.92 59.83 o -11 7 0 265.50 298.97 37.92 o -10 7 0 667.96 680.20 44.72 o -9 7 0 76.21 83.92 24.83 o -8 7 0 276.39 245.07 27.68 o -7 7 0 11.30 32.52 29.54 o -6 7 0 569.78 552.99 30.43 o -5 7 0 182.50 212.55 22.29 o -4 7 0 1.49 -3.21 21.80 o -3 7 0 1318.11 1535.43 39.23 o -2 7 0 15.34 29.35 8.57 o -1 7 0 61.79 46.38 10.71 o 0 7 0 15.57 17.32 12.68 o 1 7 0 4.92 14.78 10.23 o 2 7 0 409.48 401.17 20.98 o 3 7 0 281.31 290.06 13.36 o 4 7 0 81.12 76.22 21.56 o 5 7 0 89.32 78.25 24.10 o 6 7 0 37.18 64.42 25.54 o 7 7 0 43.66 46.71 27.87 o 8 7 0 211.62 249.01 76.10 o 9 7 0 1.13 26.67 30.16 o 10 7 0 3.57 62.32 35.94 o -12 8 0 202.71 187.51 41.45 o -11 8 0 360.22 366.70 42.01 o -10 8 0 241.65 275.27 35.79 o -9 8 0 119.63 170.94 28.70 o -8 8 0 301.16 343.26 62.87 o -7 8 0 940.20 971.80 44.84 o -6 8 0 302.73 428.83 59.48 o -5 8 0 1086.76 939.54 47.70 o -4 8 0 1596.43 1668.38 46.56 o -3 8 0 745.81 787.17 35.47 o -2 8 0 330.80 356.30 12.62 o -1 8 0 117.34 100.96 9.76 o 0 8 0 692.10 725.36 34.07 o 1 8 0 22.61 44.16 19.50 o 2 8 0 104.60 106.18 12.69 o 3 8 0 142.73 160.86 27.65 o 4 8 0 310.89 263.52 28.94 o 5 8 0 29.07 33.34 23.06 o 6 8 0 210.56 277.35 32.88 o 7 8 0 291.15 247.00 35.33 o 8 8 0 99.60 89.05 35.60 o 9 8 0 209.36 319.21 73.76 o -12 9 0 796.65 756.85 93.82 o -11 9 0 651.65 608.65 52.86 o -10 9 0 601.15 560.78 44.82 o -9 9 0 966.47 965.01 173.00 o -8 9 0 909.93 844.14 46.78 o -7 9 0 1042.51 997.31 47.06 o -6 9 0 380.60 359.51 31.82 o -5 9 0 313.77 278.48 25.27 o -4 9 0 320.18 286.89 26.36 o -3 9 0 771.69 750.17 34.27 o -2 9 0 1451.59 1487.38 43.68 o -1 9 0 3.75 22.55 12.52 o 0 9 0 174.77 228.23 38.71 o 1 9 0 1.25 -12.17 16.92 o 2 9 0 10.18 24.67 19.92 o 3 9 0 368.64 350.60 27.21 o 4 9 0 133.79 124.91 24.21 o 5 9 0 4.98 -2.19 21.88 o 6 9 0 28.22 73.47 27.81 o 7 9 0 0.30 21.74 69.13 o 8 9 0 6.75 -12.16 29.77 o 9 9 0 3.13 12.10 31.81 o -11 10 0 347.96 465.21 48.07 o -10 10 0 580.94 600.71 50.37 o -9 10 0 1417.20 1471.12 92.48 o -8 10 0 445.85 602.48 45.45 o -7 10 0 495.29 438.04 36.38 o -6 10 0 1140.45 1104.52 59.22 o -5 10 0 625.06 595.26 36.25 o -4 10 0 1866.38 1902.26 110.66 o -3 10 0 1714.79 1771.43 55.77 o -2 10 0 801.77 694.40 31.22 o -1 10 0 1112.06 1146.85 42.22 o 0 10 0 170.77 168.77 14.41 o 1 10 0 932.71 942.34 26.11 o 2 10 0 1118.24 1045.84 43.41 o 3 10 0 169.21 179.45 31.62 o 4 10 0 26.69 42.73 33.39 o 5 10 0 416.00 441.66 37.87 o 6 10 0 112.87 86.27 35.03 o 7 10 0 22.38 19.99 46.82 o 8 10 0 3.82 95.07 57.54 o -11 11 0 778.68 871.52 63.71 o -10 11 0 880.09 812.85 57.26 o -9 11 0 900.33 1076.12 104.88 o -8 11 0 1449.18 1505.57 153.45 o -7 11 0 2063.89 2171.39 154.09 o -6 11 0 2281.29 2485.25 155.09 o -5 11 0 1167.67 1148.19 52.85 o -4 11 0 329.08 297.62 30.38 o -3 11 0 1474.81 1458.20 94.39 o -2 11 0 4679.96 4399.20 255.30 o -1 11 0 1082.51 1068.45 35.69 o 0 11 0 653.56 606.20 37.77 o 1 11 0 2.51 -12.55 15.62 o 2 11 0 656.16 643.60 31.78 o 3 11 0 93.51 136.75 30.94 o 4 11 0 277.88 264.92 40.48 o 5 11 0 244.31 296.27 75.49 o 6 11 0 135.78 197.62 35.88 o 7 11 0 18.53 51.28 49.53 o 8 11 0 29.67 19.40 34.70 o -11 12 0 316.89 313.32 47.30 o -10 12 0 256.14 283.74 41.61 o -9 12 0 497.74 550.12 52.09 o -8 12 0 671.04 754.03 53.12 o -7 12 0 1738.26 1902.65 77.90 o -6 12 0 1358.14 1375.19 74.09 o -5 12 0 1981.74 1914.65 73.01 o -4 12 0 1192.36 1203.75 54.78 o -3 12 0 518.52 621.05 41.27 o -2 12 0 696.73 683.19 41.26 o -1 12 0 1293.98 1207.19 34.44 o 0 12 0 2207.99 2211.22 49.71 o 1 12 0 857.07 867.95 35.05 o 2 12 0 1369.66 1443.46 43.32 o 3 12 0 1415.00 1430.06 52.21 o 4 12 0 742.87 713.82 51.98 o 5 12 0 1022.88 912.95 56.12 o 6 12 0 303.79 268.63 79.01 o 7 12 0 144.37 116.06 38.31 o -10 13 0 457.70 473.64 84.61 o -9 13 0 1692.60 1874.68 93.22 o -8 13 0 1601.91 1684.81 79.51 o -7 13 0 1593.33 1661.11 75.20 o -6 13 0 2304.11 2514.26 204.23 o -5 13 0 2198.22 2146.80 84.76 o -4 13 0 1205.76 1205.08 59.84 o -3 13 0 679.89 618.09 44.20 o -2 13 0 1178.54 1202.70 56.97 o -1 13 0 1196.54 1072.04 42.91 o 0 13 0 1163.12 1153.40 55.20 o 1 13 0 1230.08 1180.19 37.25 o 2 13 0 442.95 432.28 25.03 o 3 13 0 9.58 1.21 49.97 o 4 13 0 103.72 136.98 77.04 o 5 13 0 177.61 159.47 46.03 o 6 13 0 114.86 175.14 70.37 o -10 14 0 327.84 474.23 194.87 o -9 14 0 439.55 440.71 52.92 o -8 14 0 282.68 336.91 46.60 o -7 14 0 1243.73 1154.47 93.55 o -6 14 0 1079.30 1260.97 70.61 o -5 14 0 1145.76 1259.98 94.41 o -4 14 0 1215.54 1261.28 153.34 o -3 14 0 212.63 247.58 35.46 o -2 14 0 1288.11 1296.13 59.37 o -1 14 0 2246.52 2349.75 77.96 o 0 14 0 1057.04 951.18 48.93 o 1 14 0 1629.21 1598.08 99.96 o 2 14 0 1651.97 1652.57 112.01 o 3 14 0 1832.22 1924.25 81.02 o 4 14 0 1199.77 1219.25 65.45 o 5 14 0 572.13 606.18 129.07 o 6 14 0 295.92 290.27 94.01 o -9 15 0 643.54 479.81 58.56 o -8 15 0 985.04 1120.67 74.13 o -7 15 0 916.21 865.57 66.87 o -6 15 0 1263.05 1419.12 75.22 o -5 15 0 1487.66 1568.60 103.11 o -4 15 0 1821.94 1882.42 106.19 o -3 15 0 1925.56 2142.31 91.75 o -2 15 0 633.73 568.24 46.15 o -1 15 0 281.56 354.20 36.17 o 0 15 0 742.49 699.00 43.01 o 1 15 0 1419.51 1452.73 104.10 o 2 15 0 1225.48 1235.66 62.27 o 3 15 0 1262.55 1185.47 63.54 o 4 15 0 366.94 357.88 69.72 o 5 15 0 39.92 18.62 54.04 o -8 16 0 146.22 185.63 81.29 o -7 16 0 116.38 100.36 40.21 o -6 16 0 257.36 334.35 48.05 o -5 16 0 633.69 688.13 59.30 o -4 16 0 1430.91 1499.04 80.80 o -3 16 0 1902.98 2039.96 157.87 o -2 16 0 1106.52 1228.51 188.99 o -1 16 0 293.89 358.52 42.89 o 0 16 0 218.18 197.36 37.26 o 1 16 0 952.97 966.50 58.09 o 2 16 0 1776.78 1543.15 116.60 o 3 16 0 1001.57 839.85 79.80 o -7 17 0 201.37 170.17 45.58 o -6 17 0 531.74 735.63 130.25 o -5 17 0 935.50 1037.04 73.58 o -4 17 0 788.04 1001.95 68.71 o -3 17 0 1690.08 1766.92 93.54 o -2 17 0 1018.57 1044.98 64.71 o -1 17 0 185.70 208.72 42.20 o 0 17 0 414.90 382.75 40.07 o 1 17 0 1115.76 1262.04 109.12 o 2 17 0 1182.57 936.29 99.81 o -5 18 0 182.27 119.54 44.29 o -4 18 0 276.26 381.60 158.48 o -3 18 0 288.54 303.76 47.83 o -2 18 0 260.70 258.12 82.55 o -1 18 0 318.94 303.33 49.01 o 0 18 0 367.07 403.35 75.36 o -1 -18 1 165.73 86.69 55.50 o 0 -18 1 176.07 214.62 65.04 o 1 -18 1 189.98 178.01 38.14 o 2 -18 1 221.76 326.32 60.29 o 3 -18 1 446.20 538.52 55.41 o 4 -18 1 484.40 458.79 54.90 o 5 -18 1 245.72 291.30 49.80 o 6 -18 1 74.10 140.22 57.34 o -2 -17 1 712.69 717.95 83.89 o -1 -17 1 715.66 785.70 86.60 o 0 -17 1 146.74 153.47 70.61 o 1 -17 1 49.91 89.64 35.02 o 2 -17 1 268.31 186.10 38.76 o 3 -17 1 408.52 525.67 115.27 o 4 -17 1 254.08 329.23 69.13 o 5 -17 1 153.09 263.00 48.79 o 6 -17 1 115.57 128.11 44.71 o 7 -17 1 105.23 135.09 56.77 o -4 -16 1 300.27 248.89 47.72 o -3 -16 1 954.37 920.62 59.09 o -2 -16 1 1228.64 1262.62 63.47 o -1 -16 1 960.89 965.55 154.23 o 0 -16 1 535.49 479.92 84.09 o 1 -16 1 297.53 442.55 96.83 o 2 -16 1 1470.12 1347.19 76.85 o 3 -16 1 1071.65 1000.59 78.55 o 4 -16 1 813.72 1016.60 64.66 o 5 -16 1 1212.94 1379.45 75.25 o 6 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