#------------------------------------------------------------------------------ #$Date: 2017-01-07 04:25:21 +0200 (Sat, 07 Jan 2017) $ #$Revision: 190001 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/20/2242006.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242006 _cell_angle_alpha 75.040 _cell_angle_beta 82.162 _cell_angle_gamma 86.007 _cell_length_a 7.8740 _cell_length_b 8.9716 _cell_length_c 24.2325 _exptl_crystal_F_000 864.00 _reflns_d_resolution_high 0.7712 _cod_data_source_file hb76311-Brsup3.hkl _cod_data_source_block 1-Br _shelx_title ' fr1318' _shelx_refln_list_code 4 _shelx_f_calc_maximum 253.99 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 165.18 175.79 7.21 o 3 0 0 748.62 738.04 12.34 o 4 0 0 302.98 302.17 11.38 o 5 0 0 2184.62 2098.42 37.72 o 6 0 0 30.81 25.21 6.00 o 7 0 0 17.64 53.57 20.28 o 8 0 0 1389.03 1665.60 63.76 o 9 0 0 486.96 378.86 44.15 o 10 0 0 31.27 42.88 27.55 o -10 1 0 72.64 54.04 20.47 o -9 1 0 0.76 51.45 14.94 o -8 1 0 1.94 9.94 9.52 o -7 1 0 450.02 442.84 50.90 o -6 1 0 218.31 169.55 16.00 o -5 1 0 560.62 581.63 26.42 o -4 1 0 267.98 265.55 10.38 o -3 1 0 10464.94 10105.14 97.58 o -2 1 0 860.50 863.76 13.02 o -1 1 0 4088.35 4091.68 43.88 o 1 1 0 2782.62 2804.49 28.43 o 2 1 0 14398.65 15225.54 78.63 o 3 1 0 70.60 91.74 5.31 o 4 1 0 4245.67 4472.75 54.28 o 5 1 0 10.97 22.82 6.56 o 6 1 0 596.42 542.84 27.11 o 7 1 0 2174.97 2307.57 55.24 o 8 1 0 1029.31 1073.14 74.79 o 9 1 0 0.36 15.67 14.63 o 10 1 0 2.13 53.30 15.39 o -9 2 0 499.66 489.82 75.83 o -8 2 0 52.50 26.54 8.70 o -7 2 0 23.78 29.33 9.18 o -6 2 0 2020.28 1910.10 79.41 o -5 2 0 1511.80 1688.79 38.20 o -4 2 0 935.46 860.82 22.82 o -3 2 0 1766.29 1690.39 22.79 o -2 2 0 573.96 489.23 21.10 o -1 2 0 22907.08 24992.19 147.31 o 0 2 0 85.75 107.33 10.58 o 1 2 0 17082.36 13446.34 193.78 o 2 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178.07 23.52 o 2 3 28 27.23 28.29 10.43 o 3 3 28 266.43 258.94 38.03 o 4 3 28 180.79 149.68 22.62 o 5 3 28 34.06 37.17 9.55 o -3 4 28 253.11 255.25 45.70 o -2 4 28 419.78 328.82 58.18 o -1 4 28 537.25 535.04 70.99 o 0 4 28 441.78 366.32 42.55 o 1 4 28 12.27 10.63 13.21 o 2 4 28 7.19 43.92 16.86 o 3 4 28 41.22 43.31 12.50 o 4 4 28 0.34 30.27 12.33 o 5 4 28 185.25 180.76 33.18 o -2 5 28 81.68 70.99 16.60 o -1 5 28 161.19 147.75 26.49 o 0 5 28 64.37 63.61 18.94 o 1 5 28 185.33 164.94 24.58 o 2 5 28 74.49 64.86 14.31 o 3 5 28 38.15 27.55 13.32 o 4 5 28 888.81 818.58 105.24 o 5 5 28 316.21 235.84 84.94 o -2 6 28 202.26 155.73 72.68 o -1 6 28 254.51 185.51 33.06 o 0 6 28 166.38 142.47 26.39 o 1 6 28 485.85 398.23 65.91 o 2 6 28 340.63 269.51 40.23 o 3 6 28 354.75 352.70 53.57 o 4 6 28 102.09 70.26 25.24 o -1 7 28 5.48 18.44 29.89 o 0 7 28 432.40 606.37 72.33 o 1 7 28 2.03 28.77 44.69 o 2 7 28 67.42 104.14 23.28 o 3 7 28 722.67 707.33 78.52 o 0 -1 29 184.13 211.57 39.35 o 1 -1 29 211.01 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