#------------------------------------------------------------------------------ #$Date: 2018-10-17 05:47:46 +0300 (Wed, 17 Oct 2018) $ #$Revision: 211492 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/26/2242676.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2242676 loop_ _publ_author_name 'Sapari, Suhaila' 'Wong, Sheryn' 'Ngatiman, Mohammad Fadzlee' 'Misral, Huda' 'Hasbullah, Siti Aishah' _publ_section_title ; Crystal structure and Hirshfeld analysis of 2-[bis(1-methyl-1H-indol-3-yl)methyl]benzoic acid ; _journal_coeditor_code HB7773 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 1580 _journal_page_last 1583 _journal_paper_doi 10.1107/S2056989018014160 _journal_volume 74 _journal_year 2018 _chemical_formula_iupac 'C26 H22 N2 O2' _chemical_formula_moiety 'C26 H22 N2 O2' _chemical_formula_sum 'C26 H22 N2 O2' _chemical_formula_weight 394.45 _chemical_name_systematic ; 2-[Bis(1-methyl-1H-indol-3-yl)methyl]benzoic acid ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 85.85(2) _cell_angle_beta 82.38(2) _cell_angle_gamma 74.57(3) _cell_formula_units_Z 2 _cell_length_a 8.654(5) _cell_length_b 10.923(6) _cell_length_c 10.964(5) _cell_measurement_reflns_used 8410 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 27.33 _cell_measurement_theta_min 2.91 _cell_volume 989.5(9) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; SHELXTL (Sheldrick, 2008) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008), PLATON (Spek, 2009), OLEX2 (Dolomanov et al., 2009) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b), shelXle (H\"ubschle et al., 2011) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker PHOTON 100 CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71076 _diffrn_reflns_av_R_equivalents 0.1007 _diffrn_reflns_av_unetI/netI 0.0532 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 37627 _diffrn_reflns_theta_full 25.243 _diffrn_reflns_theta_max 28.404 _diffrn_reflns_theta_min 2.912 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.084 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5483 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2016) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.324 _exptl_crystal_description block _exptl_crystal_F_000 416 _exptl_crystal_size_max 0.550 _exptl_crystal_size_mid 0.390 _exptl_crystal_size_min 0.300 _refine_diff_density_max 0.724 _refine_diff_density_min -0.349 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 277 _refine_ls_number_reflns 4929 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.1194 _refine_ls_R_factor_gt 0.0692 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0831P)^2^+0.5551P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1621 _refine_ls_wR_factor_ref 0.1904 _reflns_number_gt 3077 _reflns_number_total 4929 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb7773sup1.cif _cod_data_source_block I _cod_original_cell_volume 989.4(9) _cod_database_code 2242676 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.955 _shelx_estimated_absorpt_t_max 0.975 _shelx_hkl_file ; -2 0 0 9.50 2.40 -2 0 0 2.70 1.40 -2 0 0 5.20 1.40 -2 0 0 5.00 1.20 -2 0 0 4.40 1.90 2 0 0 2.40 1.40 2 0 0 5.30 1.70 2 0 0 9.40 2.40 -3 0 0 9.90 2.20 -3 0 0 12.20 2.70 -3 0 0 10.70 3.10 -3 0 0 10.20 1.70 -3 0 0 8.90 2.10 3 0 0 10.90 2.40 3 0 0 12.70 2.00 3 0 0 7.60 2.20 3 0 0 8.40 2.50 -4 0 0 -1.20 1.90 -4 0 0 0.90 1.70 -4 0 0 2.30 2.50 -4 0 0 0.80 2.10 -4 0 0 -0.20 1.50 4 0 0 1.30 2.40 4 0 0 3.00 2.30 4 0 0 0.20 2.30 4 0 0 -1.60 1.90 -5 0 0 15.50 3.60 -5 0 0 15.50 2.90 -5 0 0 16.70 4.40 -5 0 0 9.70 3.30 -5 0 0 13.00 4.00 5 0 0 11.60 3.60 5 0 0 9.20 3.80 5 0 0 12.60 4.50 5 0 0 14.60 3.40 -6 0 0 33.50 4.20 -6 0 0 36.20 7.00 -6 0 0 39.50 6.50 -6 0 0 21.50 4.50 -6 0 0 30.00 5.20 6 0 0 31.20 4.40 6 0 0 36.80 6.50 6 0 0 23.70 5.50 6 0 0 29.80 5.30 -7 0 0 211.18 14.40 -7 0 0 213.58 13.20 -7 0 0 203.38 13.70 -7 0 0 178.98 11.50 -7 0 0 239.38 16.80 7 0 0 173.88 19.20 7 0 0 197.08 13.40 7 0 0 221.98 13.10 7 0 0 223.28 14.40 -8 0 0 206.48 16.20 -8 0 0 205.78 15.70 -8 0 0 214.98 14.20 8 0 0 211.78 13.80 8 0 0 237.78 16.20 8 0 0 210.18 17.00 -9 0 0 -7.00 9.00 -9 0 0 4.80 3.90 -9 0 0 -1.30 4.30 -9 0 0 5.20 7.80 -9 0 0 -2.70 5.80 -9 0 0 5.90 6.90 9 0 0 -1.90 6.80 9 0 0 5.70 5.30 9 0 0 10.20 6.10 9 0 0 2.70 8.80 -10 0 0 -25.90 14.30 -10 0 0 -21.20 11.70 -10 0 0 1.10 10.90 -10 0 0 1.10 5.30 -10 0 0 -0.90 7.40 -10 0 0 4.00 4.60 10 0 0 12.10 8.90 10 0 0 20.60 9.80 10 0 0 -9.90 8.70 10 0 0 -5.00 5.80 -11 0 0 15.00 4.80 -11 0 0 20.20 11.00 -11 0 0 -1.60 6.40 -11 0 0 -6.40 10.80 -11 0 0 19.90 16.70 -11 0 0 -19.60 10.00 11 0 0 4.60 12.30 11 0 0 -5.30 9.80 11 0 0 7.60 7.10 10 -1 0 -2.20 6.00 10 -1 0 4.80 9.90 10 -1 0 -11.30 10.20 10 -1 0 10.00 12.90 -10 1 0 -3.90 5.50 -10 1 0 -1.20 9.20 -10 1 0 -18.30 11.10 -10 1 0 12.70 11.00 -10 1 0 6.80 4.20 9 -1 0 5.10 6.30 9 -1 0 10.50 8.10 9 -1 0 -1.80 6.50 9 -1 0 12.40 7.70 -9 1 0 5.20 4.60 -9 1 0 5.00 9.60 -9 1 0 -4.30 6.10 -9 1 0 7.80 8.00 -9 1 0 7.80 7.40 -9 1 0 2.80 3.40 8 -1 0 23.90 11.00 8 -1 0 14.70 8.30 8 -1 0 12.80 4.40 -8 1 0 13.70 8.50 -8 1 0 7.50 5.90 -8 1 0 5.40 3.20 -8 1 0 4.00 6.00 -8 1 0 7.70 7.10 7 -1 0 41.70 6.70 7 -1 0 30.00 5.60 7 -1 0 32.20 6.10 -7 1 0 19.90 3.90 -7 1 0 30.10 5.80 -7 1 0 32.30 8.10 -7 1 0 40.80 7.60 -7 1 0 36.10 6.00 6 -1 0 53.49 7.30 6 -1 0 51.29 7.00 6 -1 0 69.29 6.60 6 -1 0 62.59 7.90 -6 1 0 54.79 6.30 -6 1 0 62.59 7.20 -6 1 0 58.39 9.30 -6 1 0 49.20 4.70 -6 1 0 58.39 7.50 5 -1 0 635.14 30.30 5 -1 0 631.14 31.50 5 -1 0 596.74 31.50 5 -1 0 653.73 31.10 -5 1 0 602.44 30.90 -5 1 0 637.24 30.60 -5 1 0 688.63 29.80 -5 1 0 608.14 31.60 -5 1 0 607.84 31.20 4 -1 0 104.09 7.40 4 -1 0 106.59 7.60 4 -1 0 96.79 7.10 4 -1 0 106.49 7.00 4 -1 0 104.49 7.20 -4 1 0 119.29 6.10 -4 1 0 99.99 7.30 -4 1 0 103.99 6.90 -4 1 0 102.29 6.80 -4 1 0 101.59 8.20 3 -1 0 11.70 2.30 3 -1 0 9.20 2.30 3 -1 0 8.80 2.10 3 -1 0 13.00 3.20 3 -1 0 8.70 2.40 -3 1 0 8.60 2.20 -3 1 0 15.20 1.90 -3 1 0 13.70 3.10 -3 1 0 7.70 2.50 -3 1 0 10.60 2.20 2 -1 0 54.89 3.90 2 -1 0 61.69 4.40 2 -1 0 57.89 4.50 2 -1 0 55.89 3.80 2 -1 0 61.29 3.80 -2 1 0 60.39 4.40 -2 1 0 56.79 3.90 -2 1 0 55.79 4.30 -2 1 0 58.69 3.90 1 -1 0 208.58 10.40 1 -1 0 190.58 10.10 1 -1 0 227.88 10.90 1 -1 0 234.18 10.60 -1 1 0 224.48 10.60 -1 1 0 224.38 10.80 -1 1 0 242.18 10.50 -2 -1 0 1812.32 82.79 -2 -1 0 1931.11 82.69 -2 -1 0 1794.42 83.19 -2 -1 0 1856.51 83.39 2 1 0 1827.02 83.39 2 1 0 1810.82 83.19 2 1 0 1778.82 82.79 -3 -1 0 1999.00 92.69 -3 -1 0 2181.38 92.29 -3 -1 0 1996.80 93.29 -3 -1 0 1979.40 92.99 3 1 0 1976.30 93.29 3 1 0 2052.89 93.09 3 1 0 2144.39 92.59 3 1 0 1979.40 92.69 -4 -1 0 126.29 6.60 -4 -1 0 113.59 7.80 -4 -1 0 118.19 8.30 -4 -1 0 119.89 7.20 -4 -1 0 111.19 7.00 4 1 0 109.89 7.10 4 1 0 117.09 6.70 4 1 0 114.79 7.80 4 1 0 103.99 7.50 -5 -1 0 13.80 3.20 -5 -1 0 14.80 4.40 -5 -1 0 15.70 3.40 -5 -1 0 18.40 4.20 -5 -1 0 21.10 2.90 5 1 0 13.60 3.40 5 1 0 20.20 3.70 5 1 0 16.00 3.80 5 1 0 17.00 3.40 -6 -1 0 19.80 4.10 -6 -1 0 21.30 5.50 -6 -1 0 26.20 4.70 -6 -1 0 25.10 3.70 -6 -1 0 28.00 5.60 6 1 0 21.20 3.80 6 1 0 25.20 4.60 6 1 0 20.10 5.00 6 1 0 24.50 6.00 -7 -1 0 439.06 20.80 -7 -1 0 429.76 22.00 -7 -1 0 410.96 23.00 -7 -1 0 414.36 24.50 -7 -1 0 398.66 22.10 7 1 0 384.66 24.00 7 1 0 420.46 22.60 7 1 0 396.96 21.20 7 1 0 395.46 23.00 -8 -1 0 72.19 12.30 -8 -1 0 72.09 8.30 -8 -1 0 59.79 8.10 -8 -1 0 61.89 6.10 -8 -1 0 67.79 8.80 8 1 0 69.89 6.90 8 1 0 79.79 11.80 8 1 0 75.79 9.10 -9 -1 0 0.40 8.70 -9 -1 0 -0.40 3.50 -9 -1 0 1.00 4.50 -9 -1 0 -2.00 6.20 -9 -1 0 0.30 6.90 9 1 0 0.20 7.70 9 1 0 -0.90 3.70 9 1 0 3.90 8.30 9 1 0 -2.00 5.60 -10 -1 0 -4.30 7.30 -10 -1 0 2.70 4.20 -10 -1 0 -4.40 5.10 -10 -1 0 -10.50 8.00 -10 -1 0 1.80 7.50 -10 -1 0 -9.20 10.00 10 1 0 -13.90 7.40 10 1 0 -3.80 11.00 10 1 0 3.80 4.60 10 1 0 16.50 8.00 -11 -1 0 -16.30 9.10 -11 -1 0 -14.20 9.70 -11 -1 0 24.30 16.10 -11 -1 0 -6.90 4.20 -11 -1 0 1.10 6.40 -11 -1 0 -2.60 12.20 -11 -1 0 13.30 10.80 11 1 0 -13.30 10.50 11 1 0 30.00 13.60 11 1 0 8.40 7.20 10 -2 0 15.30 10.00 10 -2 0 -10.50 10.00 10 -2 0 1.00 24.20 10 -2 0 -0.10 4.90 -10 2 0 8.30 10.20 -10 2 0 -3.80 3.70 -10 2 0 -19.10 9.90 -10 2 0 -5.60 10.10 -10 2 0 5.70 6.00 -10 2 0 -9.30 8.80 9 -2 0 31.50 5.90 9 -2 0 30.20 9.10 9 -2 0 28.70 11.80 -9 2 0 22.20 7.90 -9 2 0 22.20 8.20 -9 2 0 22.80 4.20 -9 2 0 22.90 9.20 -9 2 0 24.90 5.30 -9 2 0 17.60 8.30 8 -2 0 26.30 6.10 8 -2 0 29.80 6.70 8 -2 0 25.80 8.10 -8 2 0 33.00 8.00 -8 2 0 30.10 8.40 -8 2 0 30.80 4.50 -8 2 0 21.30 7.00 -8 2 0 30.30 7.20 7 -2 0 49.50 8.80 7 -2 0 61.09 7.30 7 -2 0 41.00 7.00 7 -2 0 66.69 9.90 -7 2 0 42.20 5.00 -7 2 0 50.09 8.30 -7 2 0 44.20 7.60 -7 2 0 56.19 8.10 -7 2 0 50.99 11.10 6 -2 0 23.10 4.10 6 -2 0 14.50 4.80 6 -2 0 24.00 5.30 6 -2 0 24.30 6.80 6 -2 0 21.10 6.10 -6 2 0 20.90 5.20 -6 2 0 13.10 4.40 -6 2 0 16.20 5.10 -6 2 0 16.50 3.10 -6 2 0 21.20 4.70 5 -2 0 82.49 8.00 5 -2 0 77.19 6.80 5 -2 0 79.29 8.80 5 -2 0 67.49 6.20 5 -2 0 67.69 6.20 -5 2 0 67.09 8.30 -5 2 0 58.89 7.00 -5 2 0 70.99 6.60 -5 2 0 64.69 6.70 -5 2 0 72.09 5.20 4 -2 0 35.30 4.20 4 -2 0 47.50 4.50 4 -2 0 41.10 4.60 4 -2 0 37.60 6.10 4 -2 0 43.30 5.80 -4 2 0 34.20 4.80 -4 2 0 37.60 4.30 -4 2 0 42.20 5.30 -4 2 0 37.90 4.50 3 -2 0 569.54 27.70 3 -2 0 570.24 28.40 3 -2 0 618.54 27.70 3 -2 0 597.54 27.30 3 -2 0 570.84 28.50 -3 2 0 544.95 28.60 -3 2 0 568.54 27.60 -3 2 0 558.94 28.20 -3 2 0 564.44 27.50 -3 2 0 651.63 27.10 2 -2 0 36.70 3.20 2 -2 0 23.90 2.00 2 -2 0 34.40 3.80 2 -2 0 29.90 2.80 2 -2 0 40.40 4.30 -2 2 0 34.30 2.50 -2 2 0 30.60 3.30 -2 2 0 27.40 2.80 -2 2 0 32.40 3.60 -2 2 0 31.60 3.00 1 -2 0 228.08 11.70 1 -2 0 230.68 11.60 1 -2 0 229.98 11.50 -1 2 0 230.28 10.90 -1 2 0 235.28 11.00 -1 2 0 228.78 11.70 -1 2 0 235.48 11.70 -1 2 0 229.68 11.50 0 -2 0 429.56 19.20 0 -2 0 406.96 19.10 0 -2 0 457.55 19.30 0 -2 0 447.96 18.70 0 2 0 416.86 18.60 0 2 0 362.46 19.10 0 2 0 345.67 18.70 0 2 0 412.76 19.10 0 2 0 394.36 19.20 -1 -2 0 50.39 3.10 -1 -2 0 48.70 2.50 -1 -2 0 39.10 2.70 -1 -2 0 47.00 3.10 -1 -2 0 53.19 3.10 1 2 0 49.10 3.00 1 2 0 39.70 2.60 1 2 0 37.60 3.00 1 2 0 48.50 2.50 -2 -2 0 2616.24 116.09 -2 -2 0 2723.93 115.69 -2 -2 0 2569.94 116.19 -2 -2 0 2604.24 116.39 2 2 0 2563.24 116.19 2 2 0 2164.08 115.89 2 2 0 2660.03 116.39 2 2 0 2598.14 116.09 -3 -2 0 1480.25 67.89 -3 -2 0 1502.75 68.99 -3 -2 0 1444.06 68.69 -3 -2 0 1541.65 67.99 -3 -2 0 1545.35 68.59 3 2 0 1416.26 67.89 3 2 0 1504.85 68.99 3 2 0 1545.15 68.19 3 2 0 1471.35 68.69 -4 -2 0 188.38 10.20 -4 -2 0 190.28 9.50 -4 -2 0 176.28 10.40 -4 -2 0 183.78 10.80 -4 -2 0 188.48 9.60 4 2 0 165.88 10.20 4 2 0 176.38 9.60 4 2 0 178.28 10.70 4 2 0 180.18 10.70 -5 -2 0 20.80 4.60 -5 -2 0 20.40 3.00 -5 -2 0 16.10 3.80 -5 -2 0 21.90 4.20 -5 -2 0 15.40 3.00 5 2 0 24.20 4.30 5 2 0 11.80 4.10 5 2 0 16.10 3.20 5 2 0 22.90 3.20 -6 -2 0 1.50 4.80 -6 -2 0 9.00 5.60 -6 -2 0 2.10 2.80 -6 -2 0 -1.10 3.20 -6 -2 0 0.00 3.40 -6 -2 0 4.00 3.10 6 2 0 3.00 3.20 6 2 0 4.30 3.50 6 2 0 4.20 2.90 6 2 0 1.70 3.30 -7 -2 0 15.10 6.50 -7 -2 0 12.90 4.70 -7 -2 0 8.60 4.90 -7 -2 0 10.30 6.90 -7 -2 0 12.30 4.00 -7 -2 0 12.20 3.90 7 2 0 16.40 4.80 7 2 0 9.20 4.70 7 2 0 18.10 4.90 7 2 0 14.80 5.00 -8 -2 0 8.50 5.40 -8 -2 0 2.10 7.00 -8 -2 0 8.30 4.60 -8 -2 0 1.70 3.50 -8 -2 0 1.00 4.90 -8 -2 0 -1.00 4.00 -8 -2 0 3.10 7.70 8 2 0 -2.70 6.70 8 2 0 0.60 3.60 8 2 0 5.10 4.70 8 2 0 8.60 7.00 -9 -2 0 10.40 6.10 -9 -2 0 3.50 5.90 -9 -2 0 -0.30 5.50 -9 -2 0 -1.70 9.50 -9 -2 0 -5.80 4.40 -9 -2 0 3.40 3.60 -9 -2 0 12.00 8.70 9 2 0 -0.20 5.40 9 2 0 -0.10 5.40 9 2 0 3.30 3.70 9 2 0 -1.50 8.00 -10 -2 0 -3.70 5.40 -10 -2 0 4.60 4.30 -10 -2 0 0.30 7.70 -10 -2 0 9.60 9.80 -10 -2 0 -5.20 8.70 -10 -2 0 -1.80 6.30 -10 -2 0 0.20 12.10 10 2 0 -6.30 5.40 10 2 0 2.30 7.00 10 2 0 -0.30 9.40 10 2 0 -2.00 10.50 -11 -2 0 11.10 9.00 -11 -2 0 0.10 5.00 -11 -2 0 -1.60 6.00 -11 -2 0 18.60 17.20 -11 -2 0 6.00 8.80 -11 -2 0 -8.20 10.00 11 2 0 -2.50 5.10 11 2 0 -0.80 10.40 10 -3 0 -10.90 13.20 10 -3 0 14.30 7.40 10 -3 0 -19.80 10.80 -10 3 0 4.40 12.40 -10 3 0 -6.10 10.10 -10 3 0 2.90 14.20 -10 3 0 -8.10 5.90 -10 3 0 2.00 3.80 9 -3 0 0.30 5.80 9 -3 0 -9.70 8.90 9 -3 0 -15.70 10.50 9 -3 0 3.80 7.40 -9 3 0 -6.90 4.80 -9 3 0 4.70 8.70 -9 3 0 2.50 3.20 -9 3 0 5.20 9.60 -9 3 0 7.20 11.30 8 -3 0 6.70 8.90 8 -3 0 2.20 5.10 8 -3 0 1.20 7.50 8 -3 0 8.30 7.50 -8 3 0 8.70 3.00 -8 3 0 2.50 6.00 -8 3 0 7.30 5.60 -8 3 0 2.10 7.20 -8 3 0 -1.40 7.80 7 -3 0 3.40 4.50 7 -3 0 9.50 7.20 7 -3 0 13.40 5.10 7 -3 0 12.00 5.30 7 -3 0 7.40 6.00 -7 3 0 10.70 5.60 -7 3 0 3.90 2.90 -7 3 0 13.40 6.60 -7 3 0 2.50 6.90 -7 3 0 16.90 5.40 6 -3 0 -1.80 4.30 6 -3 0 -3.20 5.10 6 -3 0 2.20 5.70 6 -3 0 4.70 3.20 6 -3 0 -1.50 4.00 -6 3 0 0.80 4.20 -6 3 0 2.40 4.20 -6 3 0 -1.90 4.10 -6 3 0 -2.80 4.80 -6 3 0 -1.20 2.10 5 -3 0 17.60 4.20 5 -3 0 24.50 4.50 5 -3 0 27.00 5.70 5 -3 0 22.20 6.00 5 -3 0 15.40 4.10 -5 3 0 18.80 3.00 -5 3 0 12.80 5.30 -5 3 0 13.20 4.00 -5 3 0 18.70 4.20 -5 3 0 13.60 4.00 4 -3 0 411.56 19.50 4 -3 0 387.06 19.00 4 -3 0 393.86 20.90 4 -3 0 385.96 19.70 4 -3 0 381.46 20.90 -4 3 0 374.96 19.30 -4 3 0 366.96 20.40 -4 3 0 379.86 20.40 -4 3 0 376.06 19.50 3 -3 0 55.89 6.20 3 -3 0 51.49 4.80 3 -3 0 49.40 4.40 3 -3 0 51.99 5.10 -3 3 0 50.99 4.30 -3 3 0 48.40 5.40 -3 3 0 57.39 3.70 -3 3 0 54.59 4.80 -3 3 0 49.99 5.00 2 -3 0 1328.87 61.69 2 -3 0 1432.26 60.59 2 -3 0 1298.47 61.19 2 -3 0 1322.27 61.59 -2 3 0 1286.07 61.19 -2 3 0 1332.77 60.49 -2 3 0 1360.26 61.69 -2 3 0 1260.87 61.49 1 -3 0 179.28 9.90 1 -3 0 176.78 9.70 1 -3 0 177.48 9.50 -1 3 0 173.98 9.80 -1 3 0 197.08 9.00 -1 3 0 174.58 9.70 -1 3 0 182.88 9.90 -1 3 0 184.88 8.70 0 -3 0 2.30 1.70 0 -3 0 1.90 1.00 0 -3 0 -0.40 0.90 0 -3 0 1.70 1.80 0 -3 0 -1.10 1.90 0 3 0 0.00 1.60 0 3 0 1.70 1.60 0 3 0 2.90 0.90 0 3 0 2.10 1.20 -1 -3 0 1617.44 71.59 -1 -3 0 1595.04 70.99 -1 -3 0 1587.64 70.89 1 3 0 1518.05 70.79 1 3 0 1609.64 71.59 1 3 0 1419.86 70.89 1 3 0 1605.74 71.09 -2 -3 0 59.19 4.80 -2 -3 0 63.29 4.10 -2 -3 0 59.69 4.10 -2 -3 0 69.19 4.70 -2 -3 0 61.59 4.80 2 3 0 63.89 4.20 2 3 0 63.39 4.50 2 3 0 54.69 4.80 2 3 0 61.69 3.20 -3 -3 0 528.25 26.10 -3 -3 0 550.44 26.10 -3 -3 0 539.85 26.50 -3 -3 0 548.35 25.40 3 3 0 576.74 25.70 3 3 0 546.35 26.10 3 3 0 542.05 26.60 3 3 0 526.35 24.90 3 3 0 530.65 26.20 -4 -3 0 456.85 22.10 -4 -3 0 444.86 21.20 -4 -3 0 446.76 20.90 -4 -3 0 444.06 22.70 -4 -3 0 448.46 21.20 -4 -3 0 422.36 22.10 4 3 0 434.46 22.20 4 3 0 427.96 20.90 4 3 0 444.36 22.50 4 3 0 458.95 21.70 -5 -3 0 14.50 3.10 -5 -3 0 10.60 3.50 -5 -3 0 10.70 3.60 -5 -3 0 8.80 2.20 -5 -3 0 14.00 4.30 5 3 0 6.30 4.00 5 3 0 8.50 2.50 5 3 0 6.80 3.20 5 3 0 7.70 2.40 -6 -3 0 -2.80 2.40 -6 -3 0 -3.10 3.40 -6 -3 0 -2.90 4.30 -6 -3 0 -2.30 2.20 -6 -3 0 -0.10 2.40 -6 -3 0 7.00 5.10 6 3 0 0.40 2.70 6 3 0 1.90 4.60 6 3 0 2.50 3.50 6 3 0 1.40 3.30 -7 -3 0 28.00 4.60 -7 -3 0 38.20 7.50 -7 -3 0 36.70 6.30 -7 -3 0 35.90 4.90 -7 -3 0 32.30 5.10 -7 -3 0 35.60 6.40 7 3 0 31.00 5.10 7 3 0 30.70 7.20 7 3 0 30.70 6.10 7 3 0 39.20 4.90 -8 -3 0 44.80 6.90 -8 -3 0 76.79 10.80 -8 -3 0 68.89 6.80 -8 -3 0 61.99 8.30 -8 -3 0 65.19 8.10 -8 -3 0 62.59 10.50 -8 -3 0 74.09 7.50 8 3 0 61.49 8.00 8 3 0 66.09 7.50 8 3 0 61.39 10.80 8 3 0 56.99 10.00 -9 -3 0 91.99 10.00 -9 -3 0 76.69 7.30 -9 -3 0 81.59 15.20 -9 -3 0 77.69 8.60 -9 -3 0 78.89 10.70 -9 -3 0 87.29 12.50 9 3 0 79.49 7.70 9 3 0 54.59 9.00 9 3 0 59.59 11.10 9 3 0 77.89 9.70 -10 -3 0 22.90 12.10 -10 -3 0 1.60 11.90 -10 -3 0 10.40 5.80 -10 -3 0 9.50 4.50 -10 -3 0 34.40 11.70 -10 -3 0 28.90 8.50 -10 -3 0 23.10 14.90 10 3 0 8.10 10.50 10 3 0 16.10 6.50 10 3 0 24.20 10.20 10 3 0 16.60 7.30 -11 -3 0 48.60 18.40 -11 -3 0 14.80 10.80 -11 -3 0 18.30 12.70 -11 -3 0 3.90 6.20 -11 -3 0 16.80 7.70 -11 -3 0 16.50 11.30 11 3 0 3.90 9.00 11 3 0 21.30 13.00 11 3 0 -0.20 6.80 9 -4 0 23.40 9.20 9 -4 0 10.50 6.80 9 -4 0 7.60 12.10 9 -4 0 5.60 10.70 -9 4 0 13.10 9.30 -9 4 0 36.50 9.50 -9 4 0 1.10 10.70 -9 4 0 19.20 12.80 -9 4 0 16.10 3.70 8 -4 0 8.40 9.10 8 -4 0 14.70 8.50 8 -4 0 15.40 6.40 8 -4 0 10.40 7.10 -8 4 0 19.90 9.20 -8 4 0 9.40 7.60 -8 4 0 6.60 3.40 -8 4 0 16.00 9.30 -8 4 0 14.80 8.20 7 -4 0 15.80 5.80 7 -4 0 30.30 9.00 7 -4 0 21.60 5.50 7 -4 0 20.60 5.70 7 -4 0 -0.20 7.40 -7 4 0 31.60 7.10 -7 4 0 21.40 6.20 -7 4 0 10.10 3.40 -7 4 0 20.60 6.20 -7 4 0 19.40 7.40 6 -4 0 3.90 4.50 6 -4 0 -0.10 4.20 6 -4 0 6.60 4.50 6 -4 0 0.00 6.50 -6 4 0 5.60 5.70 -6 4 0 6.10 4.80 -6 4 0 -1.00 4.10 -6 4 0 3.70 4.70 -6 4 0 5.10 2.60 5 -4 0 5.70 5.50 5 -4 0 -4.20 3.30 5 -4 0 0.70 5.80 5 -4 0 3.60 3.80 5 -4 0 1.20 3.80 -5 4 0 1.80 3.50 -5 4 0 4.00 4.30 -5 4 0 1.00 5.30 -5 4 0 -2.00 3.50 -5 4 0 -1.10 2.10 4 -4 0 81.19 7.50 4 -4 0 75.89 6.80 4 -4 0 79.99 6.20 4 -4 0 81.69 8.80 -4 4 0 72.39 6.10 -4 4 0 69.79 7.60 -4 4 0 71.69 8.10 -4 4 0 71.59 6.80 -4 4 0 69.69 5.00 3 -4 0 7.80 3.30 3 -4 0 12.10 4.20 3 -4 0 5.30 1.60 3 -4 0 10.80 4.10 -3 4 0 5.90 2.20 -3 4 0 12.60 3.60 -3 4 0 7.10 3.40 -3 4 0 7.10 3.50 2 -4 0 35.60 4.90 2 -4 0 31.20 4.20 2 -4 0 28.40 4.00 -2 4 0 30.40 2.80 -2 4 0 31.70 4.30 -2 4 0 23.80 3.60 -2 4 0 24.60 4.50 1 -4 0 974.20 44.80 1 -4 0 921.41 44.50 1 -4 0 930.61 44.80 -1 4 0 939.01 44.70 -1 4 0 950.60 43.40 -1 4 0 1028.00 43.90 -1 4 0 936.71 43.30 -1 4 0 938.41 44.60 -1 4 0 894.11 44.60 -1 4 0 1022.00 43.90 0 -4 0 105.09 6.60 0 -4 0 97.89 6.20 0 -4 0 103.29 5.00 0 -4 0 95.09 6.10 0 4 0 76.99 5.30 0 4 0 98.19 6.00 0 4 0 95.69 6.10 0 4 0 97.69 5.00 -1 -4 0 314.77 14.30 -1 -4 0 249.88 13.80 -1 -4 0 310.87 15.10 -1 -4 0 310.57 14.10 1 4 0 248.68 14.00 1 4 0 303.07 15.10 1 4 0 297.07 14.20 1 4 0 302.97 14.10 -2 -4 0 1.00 0.90 -2 -4 0 3.20 2.30 -2 -4 0 4.80 2.00 -2 -4 0 2.40 2.60 -2 -4 0 3.20 1.90 2 4 0 5.00 2.00 2 4 0 2.70 1.00 2 4 0 2.10 1.90 2 4 0 5.30 1.50 -3 -4 0 600.74 29.00 -3 -4 0 575.94 28.50 -3 -4 0 607.54 28.80 -3 -4 0 553.84 28.50 -3 -4 0 597.64 28.00 3 4 0 603.54 28.70 3 4 0 579.74 28.50 3 4 0 630.64 28.10 3 4 0 608.54 29.00 3 4 0 578.14 27.00 3 4 0 587.64 27.00 -4 -4 0 205.48 10.90 -4 -4 0 203.48 12.30 -4 -4 0 203.88 11.90 -4 -4 0 202.18 10.60 -4 -4 0 204.18 11.70 4 4 0 199.18 12.20 4 4 0 194.88 11.50 4 4 0 213.28 10.90 4 4 0 193.18 9.70 -5 -4 0 122.89 8.60 -5 -4 0 115.89 8.50 -5 -4 0 124.59 7.80 -5 -4 0 127.69 9.80 -5 -4 0 117.09 7.80 5 4 0 117.69 8.60 5 4 0 120.99 9.70 5 4 0 117.69 6.80 5 4 0 118.39 7.60 -6 -4 0 101.69 7.80 -6 -4 0 108.89 8.70 -6 -4 0 110.69 7.50 -6 -4 0 87.49 6.40 -6 -4 0 108.99 8.70 -6 -4 0 104.99 10.10 6 4 0 95.69 6.70 6 4 0 113.09 7.90 6 4 0 101.19 8.80 6 4 0 97.59 8.30 -7 -4 0 3.00 3.30 -7 -4 0 2.20 5.00 -7 -4 0 5.70 6.70 -7 -4 0 4.70 3.90 -7 -4 0 1.90 9.90 -7 -4 0 3.80 2.60 7 4 0 8.20 3.50 7 4 0 3.20 5.80 7 4 0 -0.50 4.30 7 4 0 5.40 3.50 -8 -4 0 4.20 3.50 -8 -4 0 4.50 5.20 -8 -4 0 6.60 5.80 -8 -4 0 3.70 4.90 -8 -4 0 5.10 4.80 -8 -4 0 1.80 3.60 -8 -4 0 4.40 5.90 8 4 0 7.70 6.60 8 4 0 3.80 5.30 8 4 0 5.40 3.80 8 4 0 5.40 3.70 -9 -4 0 4.40 3.90 -9 -4 0 3.70 6.10 -9 -4 0 -6.50 4.10 -9 -4 0 16.60 6.60 -9 -4 0 3.90 8.70 -9 -4 0 2.80 5.30 -9 -4 0 0.90 10.50 9 4 0 7.30 6.10 9 4 0 3.60 4.50 9 4 0 -4.20 3.60 9 4 0 -0.30 5.80 -10 -4 0 5.30 5.70 -10 -4 0 8.30 11.60 -10 -4 0 13.70 5.10 -10 -4 0 15.90 5.50 -10 -4 0 2.20 8.10 -10 -4 0 -2.30 7.10 -10 -4 0 31.20 9.20 10 4 0 11.80 6.20 10 4 0 24.00 7.10 10 4 0 4.50 9.10 10 4 0 7.10 10.60 -11 -4 0 -7.60 15.00 -11 -4 0 29.60 10.80 -11 -4 0 8.90 5.90 -11 -4 0 16.50 11.30 -11 -4 0 8.90 7.10 11 4 0 5.40 8.10 11 4 0 46.20 14.40 11 4 0 8.90 5.30 9 -5 0 4.50 6.30 9 -5 0 -8.00 13.30 -9 5 0 4.20 5.60 -9 5 0 10.90 3.80 -9 5 0 -7.00 10.10 -9 5 0 14.00 9.50 -9 5 0 19.70 10.40 8 -5 0 -2.90 6.00 8 -5 0 8.00 7.00 8 -5 0 3.10 9.10 8 -5 0 -16.60 9.70 -8 5 0 -2.80 8.50 -8 5 0 -9.40 7.90 -8 5 0 -10.10 9.40 -8 5 0 2.80 3.10 7 -5 0 17.30 9.90 7 -5 0 16.60 4.70 7 -5 0 10.00 11.00 7 -5 0 -1.50 8.50 -7 5 0 12.90 8.40 -7 5 0 9.00 6.10 -7 5 0 6.60 7.80 -7 5 0 5.90 6.60 -7 5 0 11.70 3.20 6 -5 0 3.10 3.40 6 -5 0 5.20 7.00 6 -5 0 0.90 5.60 6 -5 0 1.70 4.70 -6 5 0 -2.20 4.20 -6 5 0 3.10 5.00 -6 5 0 1.20 2.50 -6 5 0 7.20 6.30 -6 5 0 -1.10 5.30 5 -5 0 44.40 7.90 5 -5 0 36.80 5.50 5 -5 0 42.20 8.30 5 -5 0 42.90 6.90 -5 5 0 36.50 6.40 -5 5 0 26.60 3.80 -5 5 0 43.70 6.70 -5 5 0 39.60 5.90 -5 5 0 37.40 7.50 4 -5 0 107.59 9.20 4 -5 0 89.89 8.30 4 -5 0 96.89 8.90 -4 5 0 98.79 8.60 -4 5 0 105.99 8.40 -4 5 0 106.39 9.30 -4 5 0 88.39 6.20 -4 5 0 97.49 7.00 3 -5 0 6.50 3.50 3 -5 0 3.70 4.30 3 -5 0 4.20 1.50 3 -5 0 6.30 3.60 -3 5 0 2.50 2.20 -3 5 0 6.60 3.90 -3 5 0 3.30 3.80 -3 5 0 2.80 2.90 -3 5 0 0.90 2.10 2 -5 0 515.85 25.40 2 -5 0 480.05 24.80 2 -5 0 496.85 25.30 -2 5 0 464.15 24.90 -2 5 0 485.65 24.70 -2 5 0 491.25 25.10 -2 5 0 531.55 23.60 -2 5 0 489.05 23.10 1 -5 0 105.79 7.10 1 -5 0 111.19 7.60 1 -5 0 103.59 7.80 -1 5 0 104.79 7.30 -1 5 0 103.69 5.50 -1 5 0 116.99 6.50 -1 5 0 104.79 5.40 -1 5 0 98.99 8.10 -1 5 0 106.09 6.30 -1 5 0 98.49 7.50 0 -5 0 90.49 6.40 0 -5 0 83.19 6.20 0 -5 0 94.99 6.90 0 5 0 82.99 6.00 0 5 0 85.29 4.80 0 5 0 85.89 6.20 0 5 0 97.49 5.40 -1 -5 0 135.59 7.50 -1 -5 0 146.59 8.10 -1 -5 0 145.19 9.20 -1 -5 0 148.99 7.70 -1 -5 0 150.88 8.90 1 5 0 149.19 7.80 1 5 0 135.49 7.90 1 5 0 164.68 8.10 1 5 0 138.29 8.70 -2 -5 0 -3.80 2.80 -2 -5 0 3.00 2.10 -2 -5 0 -0.50 1.20 -2 -5 0 2.60 2.10 -2 -5 0 -3.00 2.30 2 5 0 1.50 2.00 2 5 0 2.50 1.30 2 5 0 -1.50 2.90 2 5 0 1.80 2.00 -3 -5 0 370.66 19.20 -3 -5 0 370.66 18.80 -3 -5 0 368.36 18.30 -3 -5 0 384.66 18.20 -3 -5 0 372.16 19.30 3 5 0 349.87 17.10 3 5 0 377.76 18.50 3 5 0 358.96 18.70 3 5 0 386.16 19.30 -4 -5 0 164.88 10.70 -4 -5 0 186.48 10.90 -4 -5 0 184.18 9.90 -4 -5 0 177.48 9.90 -4 -5 0 176.98 10.60 4 5 0 175.28 9.80 4 5 0 169.58 10.40 4 5 0 174.68 10.80 4 5 0 160.48 8.10 4 5 0 173.18 10.80 -5 -5 0 2.70 3.10 -5 -5 0 2.20 3.90 -5 -5 0 2.10 4.30 -5 -5 0 2.90 4.00 -5 -5 0 4.80 3.30 5 5 0 2.60 1.20 5 5 0 -0.60 3.20 5 5 0 2.10 4.10 5 5 0 1.90 4.00 -6 -5 0 0.90 3.50 -6 -5 0 2.70 3.70 -6 -5 0 -3.20 4.00 -6 -5 0 4.10 5.30 -6 -5 0 3.40 5.30 6 5 0 1.70 4.70 6 5 0 -0.90 4.60 6 5 0 -3.30 2.40 6 5 0 2.20 1.80 -7 -5 0 13.00 5.00 -7 -5 0 20.90 5.90 -7 -5 0 13.70 7.00 -7 -5 0 10.20 3.60 -7 -5 0 12.80 6.70 7 5 0 10.20 3.70 7 5 0 8.60 10.60 7 5 0 15.30 3.00 7 5 0 16.30 5.40 -8 -5 0 47.20 7.60 -8 -5 0 38.40 7.40 -8 -5 0 45.00 6.30 -8 -5 0 34.40 5.90 -8 -5 0 40.00 9.40 8 5 0 48.40 9.00 8 5 0 41.90 5.80 8 5 0 41.50 6.70 8 5 0 44.80 9.10 -9 -5 0 48.40 7.40 -9 -5 0 45.20 6.80 -9 -5 0 76.69 10.30 -9 -5 0 43.50 11.00 -9 -5 0 71.39 9.80 9 5 0 55.39 7.30 9 5 0 55.09 8.00 9 5 0 43.40 10.30 9 5 0 52.49 10.40 -10 -5 0 12.90 7.90 -10 -5 0 9.50 6.40 -10 -5 0 4.10 5.00 -10 -5 0 5.10 8.70 -10 -5 0 -6.20 12.00 -10 -5 0 5.30 10.60 10 5 0 11.10 7.50 10 5 0 12.80 10.60 10 5 0 6.30 5.70 10 5 0 11.10 6.40 -11 -5 0 21.70 6.20 -11 -5 0 31.30 7.90 -11 -5 0 20.00 17.00 -11 -5 0 38.40 11.20 -11 -5 0 51.39 12.00 11 5 0 35.90 14.10 11 5 0 33.30 6.80 11 5 0 28.10 8.00 8 -6 0 3.80 13.40 8 -6 0 17.10 12.30 8 -6 0 5.00 6.50 8 -6 0 21.30 8.50 -8 6 0 8.60 9.60 -8 6 0 18.00 10.90 -8 6 0 4.20 3.30 -8 6 0 8.60 8.50 -8 6 0 18.00 14.40 7 -6 0 9.60 7.30 7 -6 0 9.00 10.20 7 -6 0 16.60 5.00 7 -6 0 -0.50 10.20 -7 6 0 6.70 3.30 -7 6 0 11.30 8.60 -7 6 0 9.30 9.10 -7 6 0 11.30 8.10 -7 6 0 22.90 6.50 6 -6 0 61.49 11.20 6 -6 0 39.40 12.70 6 -6 0 83.79 7.20 6 -6 0 64.19 11.20 -6 6 0 69.29 8.10 -6 6 0 74.89 9.80 -6 6 0 72.59 9.60 -6 6 0 56.69 5.50 -6 6 0 79.99 12.30 5 -6 0 4.80 8.40 5 -6 0 17.50 5.80 5 -6 0 10.20 5.10 5 -6 0 13.90 4.70 -5 6 0 6.60 3.80 -5 6 0 6.10 6.30 -5 6 0 -2.40 6.10 -5 6 0 14.00 5.50 -5 6 0 6.30 2.70 4 -6 0 9.10 5.20 4 -6 0 0.50 1.90 4 -6 0 -0.50 5.50 4 -6 0 10.60 5.10 -4 6 0 2.10 2.60 -4 6 0 4.40 3.00 -4 6 0 7.70 5.00 -4 6 0 3.70 4.10 -4 6 0 3.50 6.80 3 -6 0 140.99 10.90 3 -6 0 123.79 10.00 3 -6 0 134.49 9.90 -3 6 0 129.69 7.80 -3 6 0 121.99 7.30 -3 6 0 122.09 10.30 -3 6 0 121.49 10.20 -3 6 0 123.99 9.80 2 -6 0 78.79 7.80 2 -6 0 76.59 8.00 2 -6 0 72.69 6.50 -2 6 0 72.39 4.40 -2 6 0 72.59 7.40 -2 6 0 73.59 7.40 -2 6 0 71.29 4.50 -2 6 0 74.29 5.40 -2 6 0 74.69 6.50 1 -6 0 40.30 6.10 1 -6 0 38.50 5.50 1 -6 0 39.00 4.90 1 -6 0 31.00 3.00 -1 6 0 36.60 5.70 -1 6 0 42.10 5.20 -1 6 0 38.70 2.70 -1 6 0 38.00 4.70 -1 6 0 36.50 2.80 -1 6 0 45.60 4.20 0 -6 0 6.40 3.00 0 -6 0 1.30 2.60 0 -6 0 0.70 1.60 0 -6 0 -4.40 2.90 0 6 0 0.90 2.50 0 6 0 2.10 2.50 0 6 0 0.40 1.30 -1 -6 0 0.70 1.70 -1 -6 0 -0.20 2.40 -1 -6 0 0.50 1.80 -1 -6 0 -0.30 3.00 -1 -6 0 4.80 3.70 1 6 0 0.20 1.70 1 6 0 -2.30 2.30 1 6 0 -2.80 1.80 -2 -6 0 2.50 1.80 -2 -6 0 6.90 2.30 -2 -6 0 8.30 2.50 -2 -6 0 5.40 3.10 -2 -6 0 2.10 2.80 2 6 0 4.50 2.30 2 6 0 3.10 1.90 2 6 0 2.80 3.70 2 6 0 2.70 2.20 -3 -6 0 284.67 14.00 -3 -6 0 267.47 14.20 -3 -6 0 278.67 14.80 -3 -6 0 279.47 15.70 -3 -6 0 280.57 15.70 3 6 0 275.47 15.20 3 6 0 297.37 14.40 3 6 0 273.07 14.70 3 6 0 256.77 13.10 -4 -6 0 6.30 4.00 -4 -6 0 4.60 2.40 -4 -6 0 5.90 2.50 -4 -6 0 5.40 4.20 -4 -6 0 4.90 3.60 4 6 0 5.20 3.70 4 6 0 4.60 2.40 4 6 0 3.50 4.00 -5 -6 0 206.28 13.50 -5 -6 0 211.18 13.00 -5 -6 0 209.48 11.70 -5 -6 0 192.68 12.40 -5 -6 0 182.78 11.40 5 6 0 195.38 12.70 5 6 0 193.48 12.70 5 6 0 197.98 13.40 5 6 0 197.58 11.30 -6 -6 0 13.40 5.70 -6 -6 0 13.30 3.70 -6 -6 0 10.50 5.60 -6 -6 0 27.30 6.10 -6 -6 0 12.70 4.40 6 6 0 12.10 4.50 6 6 0 13.70 1.50 6 6 0 12.50 4.80 6 6 0 12.70 2.20 6 6 0 18.50 4.10 -7 -6 0 0.00 5.50 -7 -6 0 -1.60 4.10 -7 -6 0 -1.10 6.60 -7 -6 0 1.80 3.30 -7 -6 0 6.60 7.60 7 6 0 -4.20 4.00 7 6 0 -0.40 1.70 7 6 0 1.50 6.00 7 6 0 -8.10 5.90 -8 -6 0 114.79 8.90 -8 -6 0 149.09 14.60 -8 -6 0 111.59 9.10 -8 -6 0 81.09 17.30 8 6 0 107.59 8.90 8 6 0 109.19 7.40 8 6 0 129.19 13.60 8 6 0 140.39 13.10 -9 -6 0 6.50 7.20 -9 -6 0 6.10 7.00 -9 -6 0 2.90 5.80 -9 -6 0 3.10 9.10 -9 -6 0 -7.60 4.40 9 6 0 -1.50 3.20 9 6 0 2.50 5.70 9 6 0 -11.90 6.10 9 6 0 -8.40 5.10 -10 -6 0 -3.10 4.30 -10 -6 0 3.30 12.10 -10 -6 0 17.30 9.10 -10 -6 0 6.70 12.00 -10 -6 0 -10.50 8.60 -10 -6 0 -3.10 5.80 10 6 0 5.30 10.40 10 6 0 29.60 10.90 10 6 0 -11.90 5.30 10 6 0 -2.00 4.10 -11 -6 0 23.20 13.80 -11 -6 0 23.80 8.20 -11 -6 0 41.40 12.50 -11 -6 0 35.60 12.50 11 6 0 27.70 10.90 11 6 0 33.20 7.00 8 -7 0 13.00 6.90 8 -7 0 9.10 14.80 8 -7 0 13.70 10.00 -8 7 0 21.40 13.70 -8 7 0 -11.40 10.10 7 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0 135.09 7.20 -1 7 0 144.59 10.00 -1 7 0 136.89 9.80 -1 7 0 160.18 8.90 -1 7 0 142.79 10.00 0 -7 0 0.90 3.10 0 -7 0 2.00 3.00 0 -7 0 -1.70 1.90 0 -7 0 5.20 4.50 0 7 0 7.20 3.50 0 7 0 0.00 2.60 0 7 0 -0.30 2.80 0 7 0 2.30 1.50 -1 -7 0 25.60 3.20 -1 -7 0 29.50 5.10 -1 -7 0 28.80 5.00 -1 -7 0 18.50 3.40 -1 -7 0 26.10 4.20 1 7 0 23.70 3.70 1 7 0 29.30 3.80 1 7 0 24.40 3.30 1 7 0 26.40 5.30 -2 -7 0 169.48 9.30 -2 -7 0 166.48 10.50 -2 -7 0 167.28 9.10 -2 -7 0 157.58 11.20 -2 -7 0 158.38 9.30 2 7 0 147.79 9.00 2 7 0 177.58 9.60 2 7 0 159.18 10.60 2 7 0 158.68 9.30 -3 -7 0 6.90 3.20 -3 -7 0 0.30 2.30 -3 -7 0 4.40 3.30 -3 -7 0 2.60 3.50 -3 -7 0 1.20 1.60 -3 -7 0 5.70 3.00 3 7 0 -0.40 3.00 3 7 0 1.60 3.00 3 7 0 5.00 1.70 3 7 0 7.30 3.10 -4 -7 0 2.00 3.50 -4 -7 0 0.00 3.50 -4 -7 0 4.70 2.80 -4 -7 0 -4.90 3.30 -4 -7 0 1.50 4.30 4 7 0 1.90 3.80 4 7 0 0.10 3.30 4 7 0 -4.50 3.90 -5 -7 0 -1.50 3.70 -5 -7 0 1.60 3.50 -5 -7 0 0.30 4.60 -5 -7 0 1.10 3.90 -5 -7 0 -1.90 3.30 5 7 0 -0.40 2.50 5 7 0 -0.60 4.70 5 7 0 4.50 4.50 -6 -7 0 12.60 4.70 -6 -7 0 12.60 4.80 -6 -7 0 11.30 5.80 -6 -7 0 16.30 4.80 -6 -7 0 20.90 6.30 6 7 0 12.50 3.80 6 7 0 8.10 6.00 6 7 0 11.60 4.60 -7 -7 0 9.90 4.60 -7 -7 0 15.00 6.80 -7 -7 0 5.00 7.90 -7 -7 0 0.10 4.90 -7 -7 0 3.90 8.40 7 7 0 10.90 8.60 7 7 0 21.30 11.20 7 7 0 1.60 4.70 -8 -7 0 21.00 5.40 -8 -7 0 28.70 8.20 -8 -7 0 37.20 9.30 -8 -7 0 24.80 6.20 -8 -7 0 37.60 9.40 8 7 0 22.90 6.90 8 7 0 28.60 9.20 8 7 0 29.40 6.50 -9 -7 0 6.30 8.20 -9 -7 0 0.30 5.70 -9 -7 0 -2.50 6.70 -9 -7 0 8.80 5.10 -9 -7 0 8.80 10.70 9 7 0 -2.00 5.50 9 7 0 0.50 8.90 9 7 0 -4.00 9.20 -10 -7 0 -8.40 10.10 -10 -7 0 6.90 5.60 -10 -7 0 -8.80 11.90 -10 -7 0 6.10 11.90 -10 -7 0 11.70 7.00 10 7 0 1.40 10.50 10 7 0 8.50 10.10 10 7 0 6.40 2.70 10 7 0 3.70 6.70 -11 -7 0 11.60 12.00 -11 -7 0 4.80 6.30 -11 -7 0 7.50 5.70 -11 -7 0 10.80 13.10 -11 -7 0 -15.70 17.00 11 7 0 -6.10 16.20 11 7 0 -9.10 7.80 7 -8 0 -12.40 13.30 7 -8 0 -0.70 9.80 7 -8 0 -9.20 13.80 7 -8 0 5.10 6.30 -7 8 0 20.90 6.70 -7 8 0 10.00 3.50 -7 8 0 20.20 10.60 -7 8 0 10.30 10.30 6 -8 0 17.20 9.90 6 -8 0 25.20 6.50 6 -8 0 13.60 11.90 6 -8 0 7.90 8.60 -6 8 0 22.40 8.70 -6 8 0 21.50 3.90 -6 8 0 20.20 9.10 -6 8 0 22.80 10.10 -6 8 0 29.70 5.40 5 -8 0 7.50 7.00 5 -8 0 4.30 9.40 5 -8 0 9.00 8.10 -5 8 0 6.00 7.00 -5 8 0 8.30 3.40 -5 8 0 -8.10 7.60 -5 8 0 0.90 7.50 -5 8 0 0.80 3.40 4 -8 0 1.80 2.30 4 -8 0 10.20 7.60 4 -8 0 6.60 6.30 4 -8 0 7.90 5.60 -4 8 0 -0.60 6.60 -4 8 0 7.20 2.50 -4 8 0 11.30 5.80 -4 8 0 6.20 2.80 -4 8 0 -0.20 6.60 3 -8 0 41.70 7.40 3 -8 0 24.80 3.00 3 -8 0 36.10 9.80 3 -8 0 30.30 10.00 -3 8 0 27.70 3.00 -3 8 0 21.90 6.20 -3 8 0 23.40 2.70 -3 8 0 30.20 7.10 -3 8 0 22.40 5.80 2 -8 0 -1.40 2.00 2 -8 0 4.00 4.20 2 -8 0 -0.70 5.20 2 -8 0 3.60 5.70 -2 8 0 0.60 1.00 -2 8 0 -4.10 5.30 -2 8 0 0.60 1.10 -2 8 0 -1.10 4.30 -2 8 0 -1.90 3.50 1 -8 0 24.50 5.70 1 -8 0 18.50 2.90 1 -8 0 22.80 6.40 1 -8 0 26.50 5.60 -1 8 0 19.30 4.70 -1 8 0 18.80 2.00 -1 8 0 29.10 4.30 -1 8 0 23.00 6.20 -1 8 0 20.90 2.00 0 -8 0 -3.40 3.70 0 -8 0 6.80 5.30 0 -8 0 -3.10 4.70 0 8 0 4.70 3.40 0 8 0 1.50 1.60 0 8 0 -0.40 3.60 0 8 0 -0.70 2.80 -1 -8 0 13.30 2.60 -1 -8 0 14.50 3.80 -1 -8 0 9.60 5.50 -1 -8 0 7.20 2.70 -1 -8 0 10.80 5.00 1 8 0 11.80 5.30 1 8 0 17.70 3.40 1 8 0 11.80 2.70 1 8 0 13.20 3.50 -2 -8 0 0.30 2.50 -2 -8 0 6.10 2.90 -2 -8 0 1.00 2.50 -2 -8 0 -0.50 4.30 -2 -8 0 4.10 4.20 2 8 0 -1.40 3.40 2 8 0 -2.00 2.80 2 8 0 5.20 2.70 2 8 0 2.90 2.90 -3 -8 0 55.49 5.60 -3 -8 0 51.59 7.70 -3 -8 0 49.90 5.10 -3 -8 0 47.10 6.70 -3 -8 0 51.69 5.50 3 8 0 46.20 7.50 3 8 0 50.19 5.80 3 8 0 53.09 4.40 3 8 0 59.39 5.70 -4 -8 0 -3.40 2.80 -4 -8 0 1.10 3.40 -4 -8 0 0.10 5.50 -4 -8 0 2.10 3.70 -4 -8 0 7.70 4.00 4 8 0 0.30 4.70 4 8 0 2.60 4.10 4 8 0 3.70 3.50 4 8 0 0.40 1.10 -5 -8 0 79.79 9.80 -5 -8 0 77.59 8.80 -5 -8 0 90.49 7.80 -5 -8 0 72.59 7.60 -5 -8 0 81.89 9.90 5 8 0 71.99 7.20 5 8 0 62.09 7.70 5 8 0 89.59 8.70 -6 -8 0 40.40 6.00 -6 -8 0 38.80 8.50 -6 -8 0 35.90 5.70 -6 -8 0 38.20 7.20 -6 -8 0 27.50 7.60 6 8 0 37.10 5.90 6 8 0 31.10 6.00 6 8 0 34.10 7.50 -7 -8 0 4.50 5.50 -7 -8 0 1.90 3.70 -7 -8 0 3.20 6.90 -7 -8 0 7.90 7.30 -7 -8 0 6.10 4.80 7 8 0 9.90 4.10 7 8 0 7.30 6.70 7 8 0 0.20 6.40 -8 -8 0 -0.10 3.90 -8 -8 0 3.80 7.80 -8 -8 0 -8.60 7.70 -8 -8 0 3.90 5.20 -8 -8 0 3.00 8.20 8 8 0 0.80 5.90 8 8 0 0.10 4.50 8 8 0 1.10 7.00 -9 -8 0 8.60 10.10 -9 -8 0 -5.70 9.10 -9 -8 0 4.30 8.80 -9 -8 0 20.50 5.60 -9 -8 0 6.50 5.40 9 8 0 1.20 10.20 9 8 0 12.50 5.00 9 8 0 11.80 8.90 -10 -8 0 0.00 5.90 -10 -8 0 16.70 7.40 -10 -8 0 -16.90 12.80 -10 -8 0 2.70 12.90 -10 -8 0 26.20 12.00 10 8 0 0.20 6.60 10 8 0 7.20 9.50 10 8 0 0.80 12.70 6 -9 0 2.70 10.80 6 -9 0 14.60 6.50 6 -9 0 0.40 9.20 6 -9 0 15.10 10.40 -6 9 0 14.50 10.50 -6 9 0 14.60 3.80 -6 9 0 20.70 11.90 -6 9 0 10.50 4.60 -6 9 0 7.40 7.60 5 -9 0 7.90 10.20 5 -9 0 -9.90 9.80 5 -9 0 9.60 8.90 -5 9 0 15.40 3.20 -5 9 0 6.30 6.40 -5 9 0 11.50 2.80 -5 9 0 5.90 9.10 -5 9 0 7.60 9.60 4 -9 0 39.70 10.70 4 -9 0 88.99 14.40 4 -9 0 42.80 9.80 4 -9 0 52.49 4.30 -4 9 0 72.49 10.10 -4 9 0 53.79 4.50 -4 9 0 65.39 3.80 -4 9 0 69.39 11.20 -4 9 0 47.90 9.40 3 -9 0 8.60 5.40 3 -9 0 4.80 2.60 3 -9 0 -2.80 7.10 3 -9 0 0.30 8.00 -3 9 0 2.90 6.00 -3 9 0 0.10 4.80 -3 9 0 2.80 7.10 2 -9 0 9.10 4.70 2 -9 0 -1.80 2.40 2 -9 0 3.90 6.90 2 -9 0 1.80 6.40 -2 9 0 5.10 5.70 -2 9 0 6.00 7.40 1 -9 0 40.50 6.70 1 -9 0 54.19 10.00 1 -9 0 53.59 9.30 -1 9 0 64.39 9.40 -1 9 0 71.49 6.30 -1 9 0 64.99 7.90 0 -9 0 3.10 4.60 0 -9 0 -0.30 5.80 0 -9 0 -0.90 2.60 0 9 0 -0.70 4.40 0 9 0 1.50 1.60 0 9 0 -2.40 3.90 0 9 0 3.00 3.10 -1 -9 0 0.10 2.20 -1 -9 0 8.40 5.80 -1 -9 0 -5.70 5.30 -1 -9 0 7.90 4.40 -1 -9 0 7.90 2.90 1 9 0 -6.20 5.80 1 9 0 6.50 2.60 1 9 0 2.40 3.40 1 9 0 5.80 3.70 -2 -9 0 1.00 5.30 -2 -9 0 4.20 2.80 -2 -9 0 1.00 3.20 -2 -9 0 8.00 3.10 -2 -9 0 4.00 5.70 2 9 0 4.10 3.10 2 9 0 6.80 3.30 2 9 0 3.00 5.80 2 9 0 3.00 3.30 -3 -9 0 3.50 5.30 -3 -9 0 0.30 2.30 -3 -9 0 5.90 3.60 -3 -9 0 4.70 3.50 3 9 0 4.70 3.70 3 9 0 0.40 2.40 3 9 0 -8.50 5.10 3 9 0 2.60 3.40 -4 -9 0 20.60 4.60 -4 -9 0 18.30 7.20 -4 -9 0 21.10 4.90 -4 -9 0 22.60 5.60 -4 -9 0 14.10 4.90 4 9 0 19.60 5.10 4 9 0 21.10 2.60 4 9 0 18.50 4.70 4 9 0 27.00 7.30 -5 -9 0 8.50 4.40 -5 -9 0 -5.00 7.50 -5 -9 0 1.10 4.50 -5 -9 0 1.50 5.70 -5 -9 0 6.40 4.40 5 9 0 0.40 3.10 5 9 0 4.10 4.90 5 9 0 2.70 4.80 -6 -9 0 -1.60 4.80 -6 -9 0 11.50 5.20 -6 -9 0 -1.40 6.80 -6 -9 0 5.10 5.60 6 9 0 1.70 4.50 6 9 0 -2.50 5.60 6 9 0 -1.40 6.60 -7 -9 0 28.40 9.10 -7 -9 0 34.80 6.70 -7 -9 0 41.00 9.20 -7 -9 0 33.40 6.40 -7 -9 0 46.60 9.90 7 9 0 34.30 6.70 7 9 0 48.30 8.80 -8 -9 0 11.30 8.50 -8 -9 0 5.90 6.70 -8 -9 0 11.70 9.30 -8 -9 0 7.40 6.10 -8 -9 0 8.80 4.60 8 9 0 16.30 8.60 8 9 0 13.70 6.00 -9 -9 0 44.50 8.30 -9 -9 0 52.49 12.90 -9 -9 0 52.39 12.00 -9 -9 0 34.10 11.60 -9 -9 0 37.90 6.90 9 9 0 43.70 12.20 9 9 0 36.20 11.90 9 9 0 35.50 7.80 -10 -9 0 17.60 7.10 -10 -9 0 12.10 12.70 -10 -9 0 14.40 11.20 -10 -9 0 12.60 15.70 10 9 0 -7.40 9.50 10 9 0 6.20 7.10 10 9 0 4.10 10.80 5 -10 0 23.40 13.80 5 -10 0 37.00 11.80 5 -10 0 30.50 10.90 -5 10 0 6.60 11.50 -5 10 0 27.10 11.00 -5 10 0 28.00 10.40 4 -10 0 5.30 8.00 4 -10 0 -17.70 8.80 4 -10 0 -7.20 8.50 -4 10 0 9.50 8.30 -4 10 0 8.90 8.90 -4 10 0 -11.50 6.30 3 -10 0 11.70 2.90 3 -10 0 -2.30 9.30 3 -10 0 15.60 8.90 -3 10 0 4.50 5.90 -3 10 0 11.20 7.80 -3 10 0 14.30 8.30 2 -10 0 2.50 7.50 2 -10 0 -11.90 4.30 2 -10 0 7.70 6.70 2 -10 0 -2.40 7.40 -2 10 0 6.80 6.20 -2 10 0 -3.00 7.40 1 -10 0 20.40 6.30 1 -10 0 24.30 8.60 1 -10 0 8.10 12.50 1 -10 0 18.60 3.60 -1 10 0 25.10 5.00 -1 10 0 19.50 6.60 -1 10 0 19.50 6.30 0 -10 0 15.00 7.50 0 -10 0 4.70 4.70 0 -10 0 5.60 3.10 0 -10 0 -0.30 12.30 0 10 0 8.00 4.90 0 10 0 10.70 2.10 0 10 0 14.20 5.90 0 10 0 11.70 4.20 0 10 0 9.80 1.50 -1 -10 0 -3.30 7.10 -1 -10 0 -2.90 5.70 -1 -10 0 -0.90 2.80 -1 -10 0 -2.20 4.20 1 10 0 0.20 4.80 1 10 0 -3.70 3.50 1 10 0 -2.20 2.30 -2 -10 0 17.90 4.00 -2 -10 0 23.20 6.70 -2 -10 0 21.50 8.30 -2 -10 0 11.80 3.50 -2 -10 0 10.20 4.30 2 10 0 22.70 7.50 2 10 0 18.80 4.40 2 10 0 21.50 3.90 2 10 0 14.10 4.30 -3 -10 0 0.80 6.20 -3 -10 0 8.50 5.30 -3 -10 0 6.80 3.70 -3 -10 0 2.00 3.60 -3 -10 0 8.90 3.60 -3 -10 0 13.70 6.10 3 10 0 -2.50 3.70 3 10 0 8.10 6.40 3 10 0 11.10 4.20 -4 -10 0 30.00 5.40 -4 -10 0 49.50 6.50 -4 -10 0 46.40 8.80 -4 -10 0 40.40 6.50 -4 -10 0 44.60 9.20 4 10 0 51.89 7.60 4 10 0 55.19 9.70 4 10 0 41.90 4.00 4 10 0 48.80 6.60 -5 -10 0 6.40 4.80 -5 -10 0 0.50 11.50 -5 -10 0 12.60 5.10 -5 -10 0 5.00 4.00 -5 -10 0 16.50 8.30 5 10 0 5.80 4.50 5 10 0 0.90 7.20 5 10 0 4.00 5.50 -6 -10 0 66.09 11.90 -6 -10 0 56.29 10.10 -6 -10 0 60.59 7.80 -6 -10 0 52.29 7.40 6 10 0 53.39 10.40 6 10 0 67.69 9.40 6 10 0 65.69 7.70 -7 -10 0 9.50 5.90 -7 -10 0 14.00 9.70 -7 -10 0 12.20 6.10 -7 -10 0 4.90 7.40 -7 -10 0 9.60 9.40 7 10 0 5.50 4.20 7 10 0 21.20 7.80 -8 -10 0 -5.50 9.20 -8 -10 0 -0.50 4.10 -8 -10 0 5.70 5.60 -8 -10 0 -16.10 10.20 8 10 0 7.40 6.30 8 10 0 8.60 9.40 -9 -10 0 28.20 13.40 -9 -10 0 -2.50 12.00 -9 -10 0 5.80 7.10 -9 -10 0 -2.70 5.90 -9 -10 0 -4.40 11.60 9 10 0 -17.90 10.00 9 10 0 7.50 6.10 -10 -10 0 17.20 6.20 -10 -10 0 17.80 7.80 -10 -10 0 26.40 15.00 10 10 0 43.40 14.50 4 -11 0 37.20 14.90 4 -11 0 27.00 12.40 4 -11 0 11.70 10.80 -4 11 0 30.70 12.20 -4 11 0 35.80 11.20 -4 11 0 15.80 9.20 3 -11 0 8.80 10.60 3 -11 0 21.20 10.00 3 -11 0 1.90 10.70 -3 11 0 21.00 8.30 -3 11 0 -5.70 8.20 2 -11 0 7.40 10.30 2 -11 0 -0.70 7.20 2 -11 0 -9.60 9.20 -2 11 0 -1.50 6.70 -2 11 0 -0.90 7.60 1 -11 0 11.10 8.80 1 -11 0 -6.30 8.00 1 -11 0 9.20 3.30 1 -11 0 0.80 6.40 -1 11 0 4.10 6.30 -1 11 0 17.40 8.90 0 -11 0 7.30 7.90 0 -11 0 -0.10 3.20 0 -11 0 -4.60 8.10 0 -11 0 20.60 6.60 0 11 0 13.30 6.40 0 11 0 7.40 4.70 0 11 0 9.70 10.00 -1 -11 0 21.90 9.40 -1 -11 0 29.30 6.20 -1 -11 0 20.60 3.90 -1 -11 0 37.80 8.90 1 11 0 26.40 3.70 1 11 0 23.60 4.90 1 11 0 30.10 7.10 1 11 0 22.30 5.80 -2 -11 0 283.67 20.00 -2 -11 0 329.67 27.00 -2 -11 0 272.67 18.70 -2 -11 0 244.28 15.30 2 11 0 291.97 19.60 2 11 0 280.87 15.10 2 11 0 281.07 16.50 2 11 0 300.47 16.40 -3 -11 0 11.70 4.40 -3 -11 0 18.60 7.90 -3 -11 0 24.10 4.90 -3 -11 0 13.10 5.50 -3 -11 0 9.00 9.00 3 11 0 20.00 4.80 3 11 0 17.20 4.60 3 11 0 29.10 8.90 3 11 0 15.00 3.90 -4 -11 0 38.50 10.10 -4 -11 0 22.20 6.10 -4 -11 0 20.30 5.10 -4 -11 0 24.00 7.40 -4 -11 0 27.80 5.50 4 11 0 36.80 8.90 4 11 0 27.20 5.60 4 11 0 20.70 3.30 4 11 0 21.30 5.50 -5 -11 0 13.10 8.70 -5 -11 0 31.90 6.10 -5 -11 0 29.00 9.80 -5 -11 0 9.30 5.50 -5 -11 0 21.80 5.10 5 11 0 29.90 7.00 5 11 0 21.20 7.20 5 11 0 18.10 5.70 -6 -11 0 3.70 6.90 -6 -11 0 16.70 5.00 -6 -11 0 10.00 5.70 -6 -11 0 15.30 9.40 -6 -11 0 13.40 8.10 6 11 0 3.80 6.80 6 11 0 -11.30 12.80 6 11 0 9.50 6.20 -7 -11 0 7.00 4.60 -7 -11 0 -7.40 9.40 -7 -11 0 -4.90 7.80 -7 -11 0 -0.50 4.40 -7 -11 0 9.10 8.50 7 11 0 -4.60 5.40 7 11 0 2.10 7.80 7 11 0 12.00 7.10 -8 -11 0 -0.30 9.10 -8 -11 0 -7.00 6.00 -8 -11 0 7.50 10.20 -8 -11 0 0.00 6.40 8 11 0 0.00 4.50 8 11 0 -2.10 9.00 -9 -11 0 -20.60 13.90 -9 -11 0 9.60 14.80 -9 -11 0 -5.60 4.70 -9 -11 0 0.80 11.70 9 11 0 -6.10 12.50 9 11 0 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36.80 6.70 2 -8 3 43.80 8.00 -3 8 -3 6.40 6.10 -3 8 -3 1.90 3.50 -3 8 -3 0.80 4.90 -3 8 -3 0.30 4.20 -3 8 -3 -4.20 3.50 3 -8 3 6.00 4.80 3 -8 3 -0.90 5.40 3 -8 3 2.70 2.60 3 -8 3 -0.90 6.40 -4 8 -3 63.19 7.90 -4 8 -3 76.19 11.40 -4 8 -3 69.99 9.70 -4 8 -3 55.09 7.40 -4 8 -3 46.20 8.80 4 -8 3 57.99 6.20 4 -8 3 45.00 5.50 4 -8 3 74.69 11.60 4 -8 3 66.59 11.80 4 -8 3 52.89 10.50 -5 8 -3 8.60 6.70 -5 8 -3 10.30 4.50 -5 8 -3 5.30 9.20 -5 8 -3 -1.30 5.30 -5 8 -3 -6.10 8.30 5 -8 3 4.70 8.40 5 -8 3 8.70 8.30 5 -8 3 -2.10 2.90 5 -8 3 -1.20 7.50 5 -8 3 -2.30 4.10 -6 8 -3 1.90 8.70 -6 8 -3 3.00 6.10 -6 8 -3 -7.20 6.90 -6 8 -3 4.10 6.60 6 -8 3 -10.60 9.90 6 -8 3 -5.90 5.10 6 -8 3 1.70 9.50 6 -8 3 11.40 11.20 6 -8 3 5.10 3.80 -7 8 -3 12.80 9.90 -7 8 -3 0.30 10.40 7 -8 3 27.00 13.40 7 -8 3 1.40 6.00 7 -8 3 -2.90 13.30 7 -8 3 -14.50 11.20 10 7 -3 16.40 6.00 10 7 -3 26.20 10.30 10 7 -3 15.90 6.60 10 7 -3 5.40 6.20 10 7 -3 7.00 12.90 -10 -7 3 -15.70 13.10 -10 -7 3 2.60 6.50 -10 -7 3 -14.30 9.60 -10 -7 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3.60 -1 3 -3 328.97 16.10 -1 3 -3 308.47 16.40 -1 3 -3 332.67 15.40 -1 3 -3 305.67 16.50 1 -3 3 307.87 16.30 1 -3 3 336.47 15.50 1 -3 3 313.47 15.30 1 -3 3 315.97 16.50 1 -3 3 324.97 15.00 -2 3 -3 612.74 30.70 -2 3 -3 637.04 29.60 -2 3 -3 616.54 30.40 2 -3 3 608.44 29.60 2 -3 3 632.74 28.60 2 -3 3 631.04 28.60 2 -3 3 620.94 30.60 2 -3 3 601.14 30.40 2 -3 3 663.73 29.20 -3 3 -3 64.79 6.60 -3 3 -3 60.39 5.60 -3 3 -3 62.99 5.80 -3 3 -3 61.39 5.60 3 -3 3 60.89 4.30 3 -3 3 65.49 5.90 3 -3 3 67.09 4.70 3 -3 3 66.89 5.70 3 -3 3 58.69 5.50 -4 3 -3 5.60 3.60 -4 3 -3 9.60 3.60 -4 3 -3 3.60 3.70 -4 3 -3 4.10 4.20 4 -3 3 7.80 2.50 4 -3 3 7.80 2.70 4 -3 3 -2.00 3.40 4 -3 3 12.10 4.60 4 -3 3 7.40 3.90 -5 3 -3 31.80 6.00 -5 3 -3 30.90 6.00 -5 3 -3 40.70 7.10 -5 3 -3 35.30 5.90 5 -3 3 32.00 6.20 5 -3 3 46.30 7.40 5 -3 3 35.90 4.90 5 -3 3 30.20 5.90 5 -3 3 28.70 3.80 -6 3 -3 -4.20 5.20 -6 3 -3 4.80 5.90 -6 3 -3 2.00 5.60 -6 3 -3 0.30 9.50 -6 3 -3 2.20 1.40 6 -3 3 -0.10 3.60 6 -3 3 3.50 3.80 6 -3 3 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1.50 7.60 -9 -2 3 -12.00 8.30 8 2 -3 37.00 8.90 8 2 -3 33.10 6.70 8 2 -3 32.60 6.60 8 2 -3 30.30 7.50 -8 -2 3 25.30 5.80 -8 -2 3 32.50 5.10 -8 -2 3 34.80 5.20 -8 -2 3 28.70 4.80 -8 -2 3 37.60 9.50 -8 -2 3 26.50 5.10 -8 -2 3 28.50 8.40 7 2 -3 32.40 6.10 7 2 -3 34.10 6.90 7 2 -3 36.40 6.60 7 2 -3 30.90 6.10 -7 -2 3 29.70 5.30 -7 -2 3 32.90 8.20 -7 -2 3 29.20 5.50 -7 -2 3 33.50 5.30 -7 -2 3 33.10 4.80 -7 -2 3 31.80 4.80 6 2 -3 73.79 6.90 6 2 -3 56.49 8.70 6 2 -3 46.90 6.70 6 2 -3 60.39 7.00 -6 -2 3 56.89 6.10 -6 -2 3 49.40 5.20 -6 -2 3 55.59 6.60 -6 -2 3 47.90 5.20 -6 -2 3 52.29 4.80 -6 -2 3 61.19 8.20 -6 -2 3 49.60 8.90 5 2 -3 29.60 4.90 5 2 -3 26.70 5.30 5 2 -3 23.80 5.30 5 2 -3 25.60 3.80 -5 -2 3 22.20 3.70 -5 -2 3 22.50 3.60 -5 -2 3 23.60 4.20 -5 -2 3 27.30 5.60 -5 -2 3 22.60 5.20 4 2 -3 23.10 3.40 4 2 -3 28.60 4.00 4 2 -3 21.80 4.30 4 2 -3 25.10 4.10 -4 -2 3 22.80 3.90 -4 -2 3 21.00 4.00 -4 -2 3 23.00 3.10 -4 -2 3 20.00 3.60 -4 -2 3 23.20 3.30 3 2 -3 613.14 27.20 3 2 -3 586.84 27.80 3 2 -3 564.44 28.00 3 2 -3 587.74 27.90 3 2 -3 607.14 26.90 -3 -2 3 560.84 26.80 -3 -2 3 567.84 27.80 -3 -2 3 550.14 27.80 -3 -2 3 505.15 27.40 -3 -2 3 587.44 27.20 2 2 -3 453.05 24.40 2 2 -3 564.34 25.00 2 2 -3 563.04 24.70 2 2 -3 515.25 25.30 -2 -2 3 515.35 24.50 -2 -2 3 527.85 24.70 -2 -2 3 511.15 25.30 -2 -2 3 549.15 24.60 -2 -2 3 515.55 24.80 1 2 -3 192.88 10.30 1 2 -3 183.98 9.70 1 2 -3 192.88 10.30 1 2 -3 204.08 9.30 -1 -2 3 186.78 9.40 -1 -2 3 184.58 9.70 -1 -2 3 187.48 9.20 -1 -2 3 188.68 9.50 -1 -2 3 179.58 10.00 0 2 -3 333.57 16.30 0 2 -3 327.57 16.20 0 2 -3 335.97 16.60 0 -2 3 342.47 15.70 0 -2 3 325.67 16.20 0 -2 3 344.57 15.60 0 -2 3 311.17 16.40 0 -2 3 323.57 16.30 -1 2 -3 2125.99 91.99 -1 2 -3 1992.80 91.99 -1 2 -3 1786.12 90.89 -1 2 -3 2085.99 92.39 1 -2 3 2083.39 90.79 1 -2 3 2168.28 91.29 1 -2 3 1987.10 92.19 1 -2 3 1981.10 91.99 1 -2 3 1920.81 90.99 -2 2 -3 2007.80 92.79 -2 2 -3 2029.60 93.79 -2 2 -3 2016.80 93.59 2 -2 3 2172.78 92.59 2 -2 3 2034.50 93.79 2 -2 3 1935.31 92.79 2 -2 3 1978.80 93.49 2 -2 3 2153.18 92.09 2 -2 3 2040.60 91.79 -3 2 -3 274.87 14.40 -3 2 -3 273.77 14.80 -3 2 -3 266.37 14.60 -3 2 -3 258.27 14.10 3 -2 3 254.17 14.50 3 -2 3 287.97 13.40 3 -2 3 259.87 14.10 3 -2 3 259.27 14.50 3 -2 3 275.07 13.00 -4 2 -3 119.09 8.60 -4 2 -3 126.29 8.80 -4 2 -3 122.69 9.10 -4 2 -3 125.59 9.00 4 -2 3 142.89 7.40 4 -2 3 112.09 8.60 4 -2 3 122.39 8.70 4 -2 3 123.29 9.10 4 -2 3 127.09 7.30 -5 2 -3 3.90 1.20 -5 2 -3 5.10 3.40 -5 2 -3 4.90 4.80 -5 2 -3 6.80 4.30 -5 2 -3 4.20 3.60 5 -2 3 1.80 4.30 5 -2 3 6.40 3.10 5 -2 3 4.00 3.10 5 -2 3 6.70 4.50 5 -2 3 2.70 2.60 -6 2 -3 6.00 5.90 -6 2 -3 6.20 1.50 -6 2 -3 7.80 4.40 -6 2 -3 3.70 4.80 -6 2 -3 6.40 5.60 6 -2 3 6.30 3.50 6 -2 3 2.90 4.90 6 -2 3 3.30 5.00 6 -2 3 9.50 3.20 6 -2 3 2.30 4.60 6 -2 3 8.40 5.60 -7 2 -3 144.49 14.30 -7 2 -3 164.38 13.40 -7 2 -3 164.78 15.00 7 -2 3 160.58 13.20 7 -2 3 156.48 10.60 7 -2 3 165.38 14.30 -8 2 -3 21.50 7.10 -8 2 -3 26.80 8.80 -8 2 -3 25.10 9.10 -8 2 -3 12.40 8.40 8 -2 3 24.80 7.30 8 -2 3 30.60 8.40 8 -2 3 11.00 5.30 8 -2 3 17.60 7.00 -9 2 -3 3.40 8.70 -9 2 -3 1.00 10.70 -9 2 -3 13.30 9.10 -9 2 -3 13.00 9.40 9 -2 3 23.30 10.60 9 -2 3 17.70 8.30 9 -2 3 9.90 5.30 9 -2 3 33.80 9.40 -10 2 -3 10.60 12.70 -10 2 -3 12.20 10.60 -10 2 -3 0.50 11.50 -10 2 -3 -15.60 11.90 10 -2 3 19.30 10.90 10 -2 3 4.30 13.80 10 -2 3 3.40 6.10 10 1 -3 22.10 13.80 10 1 -3 -10.70 10.40 10 1 -3 9.20 9.50 10 1 -3 -2.30 6.80 -10 -1 3 11.20 11.50 -10 -1 3 -2.10 5.10 -10 -1 3 5.30 5.50 -10 -1 3 3.60 6.00 -10 -1 3 0.70 5.40 -10 -1 3 -3.30 13.10 -10 -1 3 5.90 8.40 9 1 -3 6.30 4.70 9 1 -3 9.50 7.70 9 1 -3 -9.80 6.80 9 1 -3 1.10 7.00 -9 -1 3 -2.70 4.60 -9 -1 3 1.60 4.70 -9 -1 3 8.60 6.90 -9 -1 3 -5.40 8.80 -9 -1 3 -8.90 4.40 -9 -1 3 10.70 4.60 -9 -1 3 14.20 9.00 8 1 -3 2.40 5.00 8 1 -3 4.50 8.10 8 1 -3 1.60 6.00 8 1 -3 13.60 6.20 -8 -1 3 3.10 4.00 -8 -1 3 0.10 3.80 -8 -1 3 -2.70 5.70 -8 -1 3 1.20 3.80 -8 -1 3 -4.20 6.40 7 1 -3 180.58 13.60 7 1 -3 173.88 11.40 7 1 -3 196.28 13.30 -7 -1 3 168.78 10.60 -7 -1 3 186.78 10.50 -7 -1 3 183.78 12.90 -7 -1 3 158.38 12.50 -7 -1 3 169.88 10.30 -7 -1 3 187.98 11.50 -7 -1 3 168.28 13.30 6 1 -3 26.60 5.50 6 1 -3 21.00 4.90 6 1 -3 17.60 5.90 6 1 -3 20.90 5.10 -6 -1 3 18.10 3.10 -6 -1 3 14.30 5.20 -6 -1 3 19.60 6.20 -6 -1 3 17.30 3.80 -6 -1 3 20.30 4.30 -6 -1 3 20.20 4.60 -6 -1 3 19.30 3.30 5 1 -3 20.30 4.30 5 1 -3 27.60 5.60 5 1 -3 28.60 4.50 5 1 -3 29.10 5.20 -5 -1 3 20.90 2.90 -5 -1 3 18.90 3.00 -5 -1 3 25.00 4.30 -5 -1 3 23.60 4.20 -5 -1 3 23.20 4.10 -5 -1 3 26.30 5.60 -5 -1 3 23.00 3.50 4 1 -3 119.39 8.70 4 1 -3 116.69 7.90 4 1 -3 117.19 8.10 4 1 -3 110.79 7.10 -4 -1 3 112.69 7.00 -4 -1 3 110.29 7.20 -4 -1 3 114.09 8.10 -4 -1 3 113.89 8.00 -4 -1 3 107.59 7.90 -4 -1 3 125.29 6.30 -4 -1 3 115.59 6.30 3 1 -3 1138.69 50.59 3 1 -3 1105.79 51.39 3 1 -3 1120.19 51.39 3 1 -3 1070.79 51.29 -3 -1 3 1074.39 49.80 -3 -1 3 1138.29 50.19 -3 -1 3 1041.70 51.09 -3 -1 3 1043.10 51.19 -3 -1 3 1139.59 50.59 2 1 -3 3.70 1.90 2 1 -3 2.30 1.60 2 1 -3 1.90 2.30 2 1 -3 -0.70 1.80 2 1 -3 1.40 1.10 -2 -1 3 3.00 1.00 -2 -1 3 1.10 1.20 -2 -1 3 1.20 1.80 -2 -1 3 2.80 2.10 1 1 -3 158.48 7.80 1 1 -3 155.48 8.50 1 1 -3 157.08 7.90 -1 -1 3 153.48 7.80 -1 -1 3 151.88 7.90 -1 -1 3 156.48 7.70 -1 -1 3 150.98 8.50 -1 -1 3 161.98 8.00 0 1 -3 444.16 21.60 0 1 -3 446.46 20.50 0 1 -3 447.66 21.30 0 1 -3 458.55 21.90 0 -1 3 433.86 21.50 0 -1 3 438.46 21.30 0 -1 3 472.85 21.00 0 -1 3 464.95 20.90 -1 1 -3 54.19 3.20 -1 1 -3 52.59 4.20 -1 1 -3 47.90 4.00 1 -1 3 53.39 2.40 1 -1 3 45.40 3.90 1 -1 3 47.10 3.00 1 -1 3 50.39 3.30 1 -1 3 39.80 4.10 1 -1 3 49.20 2.70 -2 1 -3 1401.06 63.79 -2 1 -3 1335.87 63.79 -2 1 -3 1389.16 63.09 -2 1 -3 1429.06 63.69 2 -1 3 1438.06 62.39 2 -1 3 1306.07 63.49 2 -1 3 1336.27 63.69 2 -1 3 1315.37 62.99 2 -1 3 1466.75 62.89 -3 1 -3 20.80 3.80 -3 1 -3 18.90 3.30 -3 1 -3 20.80 3.90 -3 1 -3 22.70 3.60 3 -1 3 18.40 3.50 3 -1 3 22.40 3.50 3 -1 3 21.20 2.80 3 -1 3 25.40 2.70 3 -1 3 18.70 3.50 -4 1 -3 120.79 8.40 -4 1 -3 132.69 8.70 -4 1 -3 132.89 9.00 -4 1 -3 128.79 8.90 4 -1 3 131.49 7.50 4 -1 3 124.19 8.50 4 -1 3 134.49 7.30 4 -1 3 129.09 8.30 4 -1 3 123.89 8.30 4 -1 3 122.59 8.80 -5 1 -3 103.69 9.00 -5 1 -3 113.99 9.70 -5 1 -3 111.89 9.00 -5 1 -3 97.19 7.90 5 -1 3 112.19 7.10 5 -1 3 114.79 8.70 5 -1 3 98.99 8.50 5 -1 3 119.49 7.20 5 -1 3 101.59 8.80 5 -1 3 105.49 8.50 -6 1 -3 6.70 5.40 -6 1 -3 0.20 4.20 -6 1 -3 -1.80 3.70 -6 1 -3 0.50 1.50 -6 1 -3 1.10 3.80 6 -1 3 -0.40 4.40 6 -1 3 0.40 3.50 6 -1 3 2.60 3.30 6 -1 3 0.70 2.70 6 -1 3 1.30 4.20 -7 1 -3 21.50 2.90 -7 1 -3 20.00 6.90 -7 1 -3 18.70 6.10 -7 1 -3 21.60 6.70 -7 1 -3 26.00 7.50 7 -1 3 29.20 8.20 7 -1 3 23.20 4.90 7 -1 3 21.10 6.30 7 -1 3 27.60 6.50 -8 1 -3 215.98 15.50 -8 1 -3 235.88 16.70 -8 1 -3 169.58 17.70 8 -1 3 219.68 21.90 8 -1 3 232.08 17.30 8 -1 3 220.38 13.30 8 -1 3 169.88 15.00 -9 1 -3 45.90 10.40 -9 1 -3 41.10 10.20 -9 1 -3 28.70 8.10 -9 1 -3 23.20 8.80 -9 1 -3 33.90 4.00 9 -1 3 53.19 11.00 9 -1 3 42.90 9.50 9 -1 3 39.70 9.60 9 -1 3 46.20 7.00 -10 1 -3 11.10 9.60 -10 1 -3 -6.80 12.10 -10 1 -3 10.00 3.30 -10 1 -3 1.90 11.10 -10 1 -3 6.70 13.30 10 -1 3 4.80 9.40 10 -1 3 3.60 6.00 10 -1 3 27.00 10.60 10 -1 3 36.50 10.80 10 0 -3 34.30 11.30 10 0 -3 -15.20 10.90 10 0 -3 7.90 6.10 10 0 -3 -9.10 12.50 -10 0 3 4.30 6.00 -10 0 3 2.00 5.20 -10 0 3 1.50 5.60 -10 0 3 -6.20 12.70 -10 0 3 3.20 11.10 -10 0 3 15.40 6.20 -10 0 3 2.00 9.00 9 0 -3 2.30 8.80 9 0 -3 6.60 10.50 9 0 -3 8.00 7.60 9 0 -3 21.60 6.70 -9 0 3 21.20 5.30 -9 0 3 17.50 5.10 -9 0 3 7.10 6.60 -9 0 3 15.90 10.20 -9 0 3 13.10 4.80 -9 0 3 14.90 9.20 -9 0 3 15.70 5.10 8 0 -3 -13.50 7.30 8 0 -3 -2.00 5.40 8 0 -3 6.60 6.40 8 0 -3 3.50 7.00 -8 0 3 8.10 6.70 -8 0 3 8.10 3.70 -8 0 3 0.80 5.40 -8 0 3 6.50 4.80 -8 0 3 -1.00 4.10 -8 0 3 0.10 3.40 -8 0 3 -7.50 7.30 7 0 -3 71.59 8.00 7 0 -3 75.09 7.00 7 0 -3 66.49 9.30 7 0 -3 69.49 9.10 -7 0 3 75.09 8.90 -7 0 3 84.39 6.40 -7 0 3 70.29 6.90 -7 0 3 66.89 5.90 -7 0 3 73.39 13.30 -7 0 3 78.39 6.20 6 0 -3 103.39 9.10 6 0 -3 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7.90 11.90 5 12 -4 18.20 9.10 5 12 -4 19.40 9.90 5 12 -4 25.60 6.30 5 12 -4 27.60 6.00 -5 -12 4 23.10 9.80 -5 -12 4 34.50 10.50 -5 -12 4 28.20 7.60 -5 -12 4 11.40 13.20 -5 -12 4 33.60 9.70 -5 -12 4 32.00 6.30 4 12 -4 16.50 4.90 4 12 -4 11.80 10.50 4 12 -4 6.30 8.70 4 12 -4 29.00 6.70 -4 -12 4 16.40 5.40 -4 -12 4 16.60 7.80 -4 -12 4 15.70 9.00 -4 -12 4 17.40 5.70 -4 -12 4 12.60 12.20 3 12 -4 -0.80 4.20 3 12 -4 1.70 6.40 3 12 -4 -3.20 7.90 3 12 -4 30.00 11.50 -3 -12 4 0.40 5.70 -3 -12 4 2.30 7.50 -3 -12 4 0.50 4.80 -3 -12 4 -6.80 11.10 -3 -12 4 17.40 12.20 -3 -12 4 -5.30 6.20 2 12 -4 5.20 6.80 2 12 -4 0.50 6.90 2 12 -4 9.40 4.50 2 12 -4 23.00 10.50 -2 -12 4 10.80 7.80 -2 -12 4 -4.90 4.50 -2 -12 4 -1.50 7.70 -2 -12 4 6.10 3.90 -2 -12 4 4.10 10.50 -2 -12 4 16.90 9.00 1 12 -4 -3.20 7.20 1 12 -4 -10.00 6.00 1 12 -4 13.00 9.60 1 12 -4 2.80 4.20 -1 -12 4 -13.70 7.20 -1 -12 4 5.00 5.40 -1 -12 4 -3.10 6.70 -1 -12 4 2.60 4.70 -1 -12 4 -2.30 7.60 -1 -12 4 -1.30 8.10 0 12 -4 -6.20 8.80 0 12 -4 15.10 11.70 0 12 -4 5.40 6.30 0 -12 4 8.20 8.90 0 -12 4 12.40 5.90 0 -12 4 14.90 5.10 0 -12 4 -2.20 8.10 0 -12 4 31.40 8.80 -1 12 -4 19.50 9.40 -1 12 -4 -3.90 5.90 -1 12 -4 -10.50 9.30 -1 12 -4 -0.20 6.30 1 -12 4 4.20 4.50 1 -12 4 2.40 5.40 1 -12 4 10.00 9.40 1 -12 4 -2.70 12.10 -2 12 -4 -4.40 6.50 -2 12 -4 7.10 11.40 -2 12 -4 -10.00 13.40 2 -12 4 -4.20 10.30 2 -12 4 -8.20 4.60 2 -12 4 5.70 6.00 8 11 -4 9.50 7.00 8 11 -4 7.90 13.20 -8 -11 4 -16.20 13.30 -8 -11 4 -14.20 11.70 -8 -11 4 -0.50 7.00 -8 -11 4 -15.40 14.20 -8 -11 4 0.30 7.00 7 11 -4 18.70 11.40 7 11 -4 10.40 11.20 7 11 -4 2.90 4.20 7 11 -4 0.40 3.80 7 11 -4 10.30 6.00 -7 -11 4 -5.70 10.40 -7 -11 4 2.20 10.30 -7 -11 4 1.00 10.00 -7 -11 4 2.50 5.20 6 11 -4 1.40 9.30 6 11 -4 -0.60 9.50 6 11 -4 2.60 4.10 6 11 -4 -7.90 4.20 6 11 -4 3.10 5.50 -6 -11 4 -7.30 9.60 -6 -11 4 13.90 6.00 -6 -11 4 7.70 6.00 -6 -11 4 2.00 8.60 -6 -11 4 3.70 9.30 5 11 -4 56.19 8.40 5 11 -4 64.49 10.80 5 11 -4 54.79 7.70 5 11 -4 34.40 10.40 -5 -11 4 62.09 11.70 -5 -11 4 84.69 9.00 -5 -11 4 69.99 12.40 -5 -11 4 70.49 7.60 -5 -11 4 57.79 10.20 4 11 -4 12.70 7.30 4 11 -4 -1.70 4.50 4 11 -4 10.90 8.90 -4 -11 4 15.90 10.00 -4 -11 4 -1.60 6.70 -4 -11 4 8.20 6.90 -4 -11 4 4.80 5.30 -4 -11 4 2.70 5.10 -4 -11 4 8.40 7.10 3 11 -4 11.40 6.00 3 11 -4 18.80 7.30 3 11 -4 29.60 9.00 3 11 -4 14.60 4.00 -3 -11 4 10.90 5.80 -3 -11 4 21.40 6.50 -3 -11 4 14.90 6.80 -3 -11 4 16.00 5.00 -3 -11 4 8.80 9.70 2 11 -4 53.29 10.60 2 11 -4 41.80 5.80 2 11 -4 57.99 9.50 2 11 -4 40.30 8.00 -2 -11 4 59.59 7.30 -2 -11 4 52.89 7.30 -2 -11 4 40.10 7.10 -2 -11 4 65.89 10.20 -2 -11 4 55.69 8.50 -2 -11 4 63.19 11.60 1 11 -4 50.99 9.50 1 11 -4 27.40 4.70 1 11 -4 48.60 8.30 1 11 -4 36.70 7.40 -1 -11 4 40.70 11.00 -1 -11 4 45.30 6.80 -1 -11 4 43.10 7.80 -1 -11 4 39.50 5.40 -1 -11 4 33.00 11.20 0 11 -4 4.10 6.80 0 11 -4 9.50 4.00 0 11 -4 6.80 7.10 0 11 -4 4.00 5.10 0 -11 4 13.90 10.20 0 -11 4 11.80 4.90 0 -11 4 7.30 5.10 0 -11 4 9.40 6.80 0 -11 4 11.80 6.60 -1 11 -4 -3.10 7.50 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5.20 4.30 6 10 -4 5.80 4.00 6 10 -4 4.40 8.20 6 10 -4 4.30 8.80 6 10 -4 10.50 5.30 -6 -10 4 11.80 7.90 -6 -10 4 2.20 5.90 -6 -10 4 1.30 4.30 -6 -10 4 1.40 8.60 -6 -10 4 -1.70 7.70 5 10 -4 25.20 5.20 5 10 -4 31.70 8.20 5 10 -4 26.60 5.60 5 10 -4 18.40 8.10 -5 -10 4 22.70 7.10 -5 -10 4 20.20 8.60 -5 -10 4 28.20 6.60 -5 -10 4 18.30 6.90 -5 -10 4 32.60 6.60 4 10 -4 -1.80 10.00 4 10 -4 12.10 7.60 4 10 -4 3.60 4.30 4 10 -4 1.90 4.40 -4 -10 4 9.50 4.90 -4 -10 4 -1.70 5.30 -4 -10 4 10.80 8.60 -4 -10 4 -0.40 5.80 -4 -10 4 -2.50 5.60 3 10 -4 5.70 4.80 3 10 -4 10.30 7.10 3 10 -4 -8.70 3.40 3 10 -4 -3.40 5.50 -3 -10 4 10.30 8.60 -3 -10 4 1.10 4.30 -3 -10 4 1.30 4.80 -3 -10 4 -0.30 5.10 -3 -10 4 -6.30 4.10 -3 -10 4 7.30 9.20 2 10 -4 -11.00 5.20 2 10 -4 -0.90 3.00 2 10 -4 -4.70 5.10 2 10 -4 -1.50 6.80 -2 -10 4 -3.30 4.10 -2 -10 4 -3.10 3.80 -2 -10 4 -6.50 4.90 -2 -10 4 8.50 4.40 -2 -10 4 -6.20 4.90 -2 -10 4 5.30 7.80 -2 -10 4 -7.40 4.30 1 10 -4 -1.30 5.80 1 10 -4 9.60 5.40 1 10 -4 13.80 8.00 1 10 -4 3.30 3.00 -1 -10 4 4.50 4.30 -1 -10 4 6.50 5.20 -1 -10 4 4.50 4.70 -1 -10 4 15.60 5.70 -1 -10 4 5.50 4.00 -1 -10 4 1.90 7.60 0 10 -4 -3.30 4.60 0 10 -4 1.70 6.50 0 10 -4 0.20 3.10 0 10 -4 14.50 8.30 0 -10 4 -0.20 4.40 0 -10 4 1.80 5.10 0 -10 4 9.40 6.50 0 -10 4 5.90 6.30 0 -10 4 5.40 4.20 -1 10 -4 2.50 4.50 -1 10 -4 5.30 6.70 -1 10 -4 11.40 8.40 1 -10 4 9.90 8.70 1 -10 4 0.80 4.10 1 -10 4 5.90 3.50 1 -10 4 2.70 5.50 1 -10 4 -0.30 6.30 -2 10 -4 59.39 8.30 -2 10 -4 60.19 8.30 -2 10 -4 52.19 11.30 -2 10 -4 64.69 9.60 2 -10 4 63.89 7.00 2 -10 4 69.99 11.60 2 -10 4 52.39 9.90 2 -10 4 36.10 8.90 2 -10 4 51.89 6.70 -3 10 -4 -2.70 9.20 -3 10 -4 3.60 7.40 -3 10 -4 -0.60 5.10 -3 10 -4 -5.70 5.50 3 -10 4 6.60 10.50 3 -10 4 -6.00 4.00 3 -10 4 -2.70 8.80 3 -10 4 -2.60 8.00 3 -10 4 3.30 4.40 -4 10 -4 9.20 6.30 -4 10 -4 -16.70 10.30 -4 10 -4 1.30 5.60 4 -10 4 2.20 4.20 4 -10 4 -0.60 10.40 4 -10 4 4.40 4.80 4 -10 4 -6.30 4.60 4 -10 4 -8.50 8.60 4 -10 4 6.20 10.10 -5 10 -4 -1.50 7.90 -5 10 -4 12.20 10.10 -5 10 -4 -7.50 13.60 -5 10 -4 -0.40 7.10 5 -10 4 28.70 16.80 5 -10 4 23.60 13.80 5 -10 4 -5.90 5.60 5 -10 4 0.90 4.20 5 -10 4 -2.30 5.30 5 -10 4 -21.80 10.90 9 9 -4 12.10 11.50 9 9 -4 7.70 5.70 9 9 -4 5.00 13.30 9 9 -4 5.80 7.30 9 9 -4 12.10 6.40 -9 -9 4 -11.40 13.50 -9 -9 4 21.50 10.80 -9 -9 4 24.40 7.30 -9 -9 4 5.70 9.50 8 9 -4 -1.30 4.20 8 9 -4 21.40 9.40 8 9 -4 3.30 4.60 8 9 -4 5.30 4.20 8 9 -4 -6.60 10.10 -8 -9 4 7.50 6.40 -8 -9 4 -1.20 7.70 -8 -9 4 2.70 8.70 -8 -9 4 2.10 6.10 -8 -9 4 0.30 10.10 7 9 -4 -7.00 4.10 7 9 -4 -4.80 4.70 7 9 -4 -6.60 8.30 7 9 -4 1.20 7.30 7 9 -4 0.40 4.10 -7 -9 4 -10.90 7.90 -7 -9 4 7.40 4.60 -7 -9 4 0.90 5.70 -7 -9 4 2.30 6.70 6 9 -4 86.79 8.30 6 9 -4 97.99 10.80 6 9 -4 103.49 8.40 6 9 -4 112.79 9.40 6 9 -4 75.79 10.90 -6 -9 4 105.99 12.90 -6 -9 4 75.39 12.00 -6 -9 4 97.89 8.40 -6 -9 4 100.09 9.50 5 9 -4 11.90 4.50 5 9 -4 -2.60 6.60 5 9 -4 -3.20 4.00 -5 -9 4 4.00 5.10 -5 -9 4 4.90 5.60 -5 -9 4 14.70 6.30 -5 -9 4 1.80 5.00 -5 -9 4 5.60 6.40 4 9 -4 2.40 8.70 4 9 -4 -1.60 5.50 4 9 -4 -2.70 3.50 4 9 -4 1.00 4.30 -4 -9 4 -1.70 4.80 -4 -9 4 0.90 5.30 -4 -9 4 -7.40 6.80 -4 -9 4 6.50 5.80 -4 -9 4 1.80 3.30 3 9 -4 12.50 4.70 3 9 -4 12.80 8.10 3 9 -4 9.20 3.50 3 9 -4 9.10 5.30 -3 -9 4 19.60 7.80 -3 -9 4 8.80 5.10 -3 -9 4 12.70 4.90 -3 -9 4 20.40 5.10 -3 -9 4 10.80 4.90 2 9 -4 65.99 7.80 2 9 -4 58.09 8.40 -2 -9 4 65.39 6.50 -2 -9 4 61.59 7.50 -2 -9 4 56.89 7.70 -2 -9 4 61.19 6.80 -2 -9 4 69.19 7.60 -2 -9 4 56.99 8.10 1 9 -4 33.90 7.90 1 9 -4 30.10 5.50 1 9 -4 34.20 6.20 1 9 -4 24.70 4.00 -1 -9 4 30.40 8.00 -1 -9 4 32.50 5.60 -1 -9 4 29.60 5.30 -1 -9 4 21.90 4.70 -1 -9 4 25.30 4.70 -1 -9 4 19.00 5.20 -1 -9 4 20.20 5.00 0 9 -4 -1.50 2.80 0 9 -4 1.90 3.90 0 9 -4 -2.30 4.70 0 9 -4 4.60 5.10 0 -9 4 -0.40 4.00 0 -9 4 0.30 3.80 0 -9 4 -9.60 6.50 0 -9 4 0.80 4.70 0 -9 4 2.10 3.60 -1 9 -4 7.40 6.00 -1 9 -4 4.60 4.10 -1 9 -4 14.60 5.70 1 -9 4 12.20 4.00 1 -9 4 11.60 7.50 1 -9 4 -0.90 5.40 1 -9 4 1.50 3.50 1 -9 4 7.30 5.00 -2 9 -4 49.40 7.30 -2 9 -4 57.29 10.20 -2 9 -4 53.19 8.50 -2 9 -4 43.60 7.60 2 -9 4 44.40 8.50 2 -9 4 50.19 7.80 2 -9 4 58.99 6.10 2 -9 4 38.90 8.00 2 -9 4 42.00 5.40 -3 9 -4 7.50 5.10 -3 9 -4 7.80 6.10 -3 9 -4 7.50 6.60 -3 9 -4 -4.00 4.60 3 -9 4 -7.40 8.10 3 -9 4 3.80 3.50 3 -9 4 3.40 3.70 3 -9 4 -2.70 7.50 3 -9 4 -5.90 6.00 -4 9 -4 -3.70 6.80 -4 9 -4 0.20 5.30 -4 9 -4 1.10 5.90 -4 9 -4 0.10 5.40 -4 9 -4 0.50 9.00 4 -9 4 2.50 4.00 4 -9 4 8.50 9.00 4 -9 4 6.40 3.80 4 -9 4 6.60 3.30 4 -9 4 -8.70 8.70 4 -9 4 -10.00 9.30 -5 9 -4 0.30 7.20 -5 9 -4 6.30 6.50 -5 9 -4 3.10 7.30 -5 9 -4 7.10 8.10 -5 9 -4 -8.70 11.40 5 -9 4 -4.40 4.20 5 -9 4 -8.10 8.50 5 -9 4 3.30 3.90 5 -9 4 -0.60 7.70 5 -9 4 -11.00 4.70 5 -9 4 5.40 8.50 -6 9 -4 22.20 10.60 -6 9 -4 23.80 8.30 -6 9 -4 40.80 14.00 6 -9 4 40.60 13.40 6 -9 4 42.30 14.60 6 -9 4 26.60 5.00 6 -9 4 16.10 13.40 6 -9 4 20.80 6.50 9 8 -4 -4.20 11.20 9 8 -4 10.00 5.60 9 8 -4 4.80 6.00 9 8 -4 -0.10 11.80 9 8 -4 9.30 6.60 -9 -8 4 4.30 7.60 -9 -8 4 10.00 12.20 -9 -8 4 9.20 5.40 -9 -8 4 -13.60 11.30 -9 -8 4 10.30 9.60 8 8 -4 12.50 5.10 8 8 -4 0.20 9.00 8 8 -4 18.90 6.60 8 8 -4 20.40 9.80 8 8 -4 6.60 5.30 -8 -8 4 15.80 6.50 -8 -8 4 12.60 6.40 -8 -8 4 11.20 10.30 -8 -8 4 21.90 9.80 -8 -8 4 19.50 8.10 7 8 -4 0.60 4.10 7 8 -4 2.60 4.10 7 8 -4 1.70 6.00 7 8 -4 1.60 7.10 7 8 -4 0.40 5.20 7 8 -4 -0.50 6.50 -7 -8 4 -7.70 12.90 -7 -8 4 -2.10 3.90 -7 -8 4 1.60 7.70 -7 -8 4 7.70 5.80 -7 -8 4 3.60 7.70 6 8 -4 7.70 4.10 6 8 -4 4.10 3.90 6 8 -4 2.70 5.50 6 8 -4 -3.10 6.70 6 8 -4 4.00 5.00 -6 -8 4 5.10 4.00 -6 -8 4 -0.50 11.50 -6 -8 4 -0.10 6.60 -6 -8 4 3.90 5.10 -6 -8 4 0.60 6.10 5 8 -4 7.70 5.70 5 8 -4 3.50 3.70 5 8 -4 11.80 4.60 5 8 -4 9.90 4.20 -5 -8 4 4.50 5.70 -5 -8 4 12.00 5.30 -5 -8 4 13.20 5.40 -5 -8 4 3.60 5.90 -5 -8 4 6.30 3.70 4 8 -4 133.59 9.60 4 8 -4 163.98 10.80 4 8 -4 153.28 11.30 4 8 -4 130.39 11.80 -4 -8 4 152.48 11.40 -4 -8 4 160.58 12.60 -4 -8 4 165.58 11.60 -4 -8 4 158.98 9.90 -4 -8 4 161.68 10.80 3 8 -4 42.90 6.70 3 8 -4 38.00 6.70 3 8 -4 35.80 4.70 3 8 -4 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111.09 8.90 -6 -3 4 107.69 11.10 -6 -3 4 116.99 7.80 5 3 -4 29.50 6.20 5 3 -4 27.10 5.40 5 3 -4 38.30 5.50 5 3 -4 38.60 5.40 -5 -3 4 27.20 4.10 -5 -3 4 28.80 5.50 -5 -3 4 35.00 5.50 -5 -3 4 30.90 4.50 -5 -3 4 30.00 4.30 4 3 -4 10.30 3.40 4 3 -4 8.70 3.70 4 3 -4 6.70 4.30 4 3 -4 10.10 2.70 4 3 -4 14.90 3.70 -4 -3 4 10.20 2.80 -4 -3 4 9.00 3.90 -4 -3 4 8.30 3.50 -4 -3 4 9.50 3.30 -4 -3 4 11.10 3.80 3 3 -4 5.40 2.40 3 3 -4 4.90 2.50 3 3 -4 6.30 2.90 3 3 -4 3.10 2.70 -3 -3 4 4.60 2.80 -3 -3 4 4.40 2.10 -3 -3 4 3.60 3.40 -3 -3 4 8.60 2.60 -3 -3 4 9.30 3.00 2 3 -4 -2.00 1.80 2 3 -4 -2.50 2.10 2 3 -4 -3.50 1.90 2 3 -4 0.30 1.70 2 3 -4 0.00 2.00 -2 -3 4 2.50 2.00 -2 -3 4 0.10 2.20 -2 -3 4 -0.20 1.90 -2 -3 4 2.30 1.80 -2 -3 4 1.90 1.80 1 3 -4 191.58 11.10 1 3 -4 201.38 11.00 1 3 -4 194.18 10.60 -1 -3 4 187.28 9.30 -1 -3 4 190.38 11.00 -1 -3 4 187.38 10.00 -1 -3 4 194.38 10.60 -1 -3 4 195.68 10.60 0 3 -4 90.89 6.20 0 3 -4 92.39 6.50 0 3 -4 89.89 6.50 0 -3 4 90.79 6.40 0 -3 4 87.39 6.40 0 -3 4 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9.70 8.30 -6 -10 5 18.50 5.20 5 10 -5 52.89 8.50 5 10 -5 35.80 6.00 5 10 -5 57.79 10.10 5 10 -5 42.30 9.50 -5 -10 5 67.99 11.00 -5 -10 5 26.80 8.50 -5 -10 5 53.49 11.20 -5 -10 5 47.40 7.20 -5 -10 5 66.99 8.60 4 10 -5 25.90 4.80 4 10 -5 23.50 8.20 4 10 -5 31.10 6.50 4 10 -5 28.40 8.70 -4 -10 5 21.00 7.40 -4 -10 5 13.30 5.70 -4 -10 5 29.20 9.40 -4 -10 5 23.10 6.70 -4 -10 5 21.70 6.20 3 10 -5 64.19 11.40 3 10 -5 69.79 7.10 3 10 -5 94.49 9.90 3 10 -5 79.29 12.20 -3 -10 5 75.79 10.00 -3 -10 5 98.69 9.00 -3 -10 5 84.39 12.50 -3 -10 5 101.49 8.60 -3 -10 5 87.09 9.90 2 10 -5 26.00 9.10 2 10 -5 40.90 7.50 2 10 -5 24.60 4.30 -2 -10 5 36.70 6.00 -2 -10 5 32.70 5.80 -2 -10 5 24.80 7.10 -2 -10 5 39.30 6.20 -2 -10 5 41.90 8.00 -2 -10 5 29.00 6.40 -2 -10 5 38.50 9.90 1 10 -5 22.40 8.70 1 10 -5 39.50 7.90 1 10 -5 38.30 7.10 1 10 -5 19.80 4.20 -1 -10 5 33.00 9.30 -1 -10 5 31.40 5.80 -1 -10 5 41.10 6.00 -1 -10 5 28.60 6.00 -1 -10 5 38.60 6.00 -1 -10 5 16.80 6.50 0 10 -5 47.40 10.30 0 10 -5 38.40 8.70 0 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7.30 4.80 -1 -6 6 17.10 3.60 0 6 -6 18.80 5.00 0 6 -6 4.50 5.50 0 6 -6 9.70 4.80 0 6 -6 6.40 1.50 0 -6 6 15.10 4.60 0 -6 6 13.90 3.60 0 -6 6 12.00 3.50 0 -6 6 7.60 4.70 -1 6 -6 8.50 3.80 -1 6 -6 8.70 6.00 -1 6 -6 10.70 6.10 1 -6 6 5.30 1.80 1 -6 6 4.20 2.70 1 -6 6 7.30 5.70 1 -6 6 11.40 3.10 1 -6 6 4.20 5.20 1 -6 6 7.90 1.60 -2 6 -6 239.48 16.80 -2 6 -6 255.27 17.20 -2 6 -6 268.87 16.00 2 -6 6 245.78 13.40 2 -6 6 263.07 14.10 2 -6 6 245.38 16.10 2 -6 6 238.28 13.00 2 -6 6 251.87 16.70 -3 6 -6 47.00 7.70 -3 6 -6 58.79 8.10 -3 6 -6 39.50 7.20 -3 6 -6 28.00 4.50 3 -6 6 42.90 4.00 3 -6 6 46.10 8.70 3 -6 6 37.80 6.80 3 -6 6 39.50 5.10 3 -6 6 36.80 5.90 -4 6 -6 13.80 7.50 -4 6 -6 13.40 4.50 -4 6 -6 19.80 6.20 -4 6 -6 14.00 6.20 -4 6 -6 10.80 9.60 4 -6 6 1.40 6.70 4 -6 6 7.70 4.70 4 -6 6 9.80 2.90 4 -6 6 17.30 4.10 4 -6 6 11.50 5.60 4 -6 6 15.90 2.00 -5 6 -6 4.30 6.60 -5 6 -6 0.40 7.90 -5 6 -6 7.80 11.40 -5 6 -6 10.50 5.10 -5 6 -6 -8.10 7.10 5 -6 6 4.20 5.40 5 -6 6 5.20 5.40 5 -6 6 -1.70 3.50 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4.90 8.80 5 -5 9 17.50 5.10 5 -5 9 21.00 5.10 -6 5 -9 3.40 11.70 -6 5 -9 2.60 6.00 -6 5 -9 -0.20 11.80 -6 5 -9 8.30 10.50 -6 5 -9 -2.70 10.10 6 -5 9 0.90 8.00 6 -5 9 -9.70 4.30 6 -5 9 4.50 6.10 -7 5 -9 -0.20 15.60 -7 5 -9 -8.20 12.20 -7 5 -9 -24.30 13.70 -7 5 -9 14.50 8.60 7 -5 9 -16.30 8.70 7 -5 9 -5.30 4.80 8 4 -9 -1.70 13.10 7 4 -9 -3.80 8.80 7 4 -9 0.30 6.40 7 4 -9 24.70 10.40 7 4 -9 -9.40 12.00 -7 -4 9 14.40 9.00 -7 -4 9 7.50 5.70 -7 -4 9 -15.90 8.30 6 4 -9 10.10 10.00 6 4 -9 -0.50 8.20 6 4 -9 -0.70 5.50 6 4 -9 2.50 7.00 6 4 -9 8.90 7.50 -6 -4 9 11.30 7.00 -6 -4 9 -1.10 3.80 -6 -4 9 0.00 4.40 -6 -4 9 6.00 6.60 5 4 -9 2.80 4.60 5 4 -9 -5.90 8.60 5 4 -9 4.70 7.30 5 4 -9 12.40 7.40 5 4 -9 -3.80 5.30 -5 -4 9 3.30 4.70 -5 -4 9 9.40 5.30 -5 -4 9 6.00 7.80 -5 -4 9 0.20 2.90 -5 -4 9 -4.70 4.40 4 4 -9 12.50 4.30 4 4 -9 26.90 7.40 4 4 -9 13.30 7.10 4 4 -9 10.60 4.60 4 4 -9 10.20 4.70 4 4 -9 6.00 7.90 -4 -4 9 12.40 5.00 -4 -4 9 15.00 4.40 -4 -4 9 12.60 3.70 -4 -4 9 14.90 4.90 -4 -4 9 8.40 6.90 3 4 -9 10.40 4.40 3 4 -9 25.80 7.50 3 4 -9 13.50 3.00 3 4 -9 14.40 5.80 3 4 -9 11.30 4.00 -3 -4 9 12.60 4.50 -3 -4 9 14.60 6.60 -3 -4 9 17.70 4.90 -3 -4 9 13.80 4.10 -3 -4 9 12.60 2.90 2 4 -9 -1.10 5.90 2 4 -9 -4.80 5.60 2 4 -9 1.70 3.70 2 4 -9 -4.50 4.10 -2 -4 9 2.00 2.90 -2 -4 9 2.40 5.40 -2 -4 9 -3.00 4.00 -2 -4 9 4.60 3.60 1 4 -9 0.20 2.40 1 4 -9 0.40 6.00 1 4 -9 7.50 5.00 1 4 -9 1.60 4.70 -1 -4 9 4.40 3.40 -1 -4 9 3.60 4.10 -1 -4 9 0.20 4.20 0 4 -9 9.80 6.60 0 4 -9 21.50 6.60 0 4 -9 1.40 4.90 0 -4 9 16.80 3.60 0 -4 9 13.40 5.10 0 -4 9 13.90 3.50 -1 4 -9 58.89 10.90 -1 4 -9 74.39 10.50 -1 4 -9 40.80 8.10 1 -4 9 64.79 5.40 1 -4 9 71.79 8.50 1 -4 9 60.39 5.80 -2 4 -9 3.90 11.90 -2 4 -9 0.30 6.50 -2 4 -9 3.70 6.30 2 -4 9 -0.70 5.70 2 -4 9 -0.70 5.70 2 -4 9 6.30 2.60 2 -4 9 3.00 2.90 -3 4 -9 -5.00 6.90 -3 4 -9 -4.60 7.20 -3 4 -9 -4.80 4.90 3 -4 9 -1.70 3.60 3 -4 9 4.60 1.90 3 -4 9 0.10 5.90 3 -4 9 2.90 4.90 -4 4 -9 -2.80 8.10 -4 4 -9 3.40 6.00 -4 4 -9 19.00 6.90 -4 4 -9 14.80 8.10 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20.70 7.00 -5 -3 9 33.60 5.80 -5 -3 9 36.40 6.70 -5 -3 9 39.70 8.80 -5 -3 9 26.60 5.90 4 3 -9 0.50 7.10 4 3 -9 -3.50 4.10 4 3 -9 10.30 6.50 4 3 -9 0.80 6.40 4 3 -9 -0.90 2.60 4 3 -9 2.60 4.50 -4 -3 9 4.80 4.20 -4 -3 9 -1.30 6.00 -4 -3 9 1.50 2.50 -4 -3 9 -7.10 3.80 -4 -3 9 -1.30 4.10 3 3 -9 134.69 12.30 3 3 -9 129.09 12.80 3 3 -9 138.79 12.70 -3 -3 9 134.59 11.70 -3 -3 9 121.59 9.40 -3 -3 9 120.99 8.40 -3 -3 9 127.39 9.40 -3 -3 9 125.89 8.30 2 3 -9 1.30 2.10 2 3 -9 0.00 3.70 2 3 -9 4.20 4.70 2 3 -9 4.40 4.50 2 3 -9 -0.60 3.20 -2 -3 9 6.10 3.90 -2 -3 9 1.90 3.90 -2 -3 9 6.10 3.70 -2 -3 9 5.70 3.40 1 3 -9 3.50 6.50 1 3 -9 9.80 4.70 1 3 -9 7.00 3.20 -1 -3 9 7.50 3.20 -1 -3 9 12.00 4.00 -1 -3 9 13.30 4.40 -1 -3 9 6.50 3.40 0 3 -9 30.50 5.90 0 3 -9 30.80 9.20 0 3 -9 39.20 8.00 0 -3 9 39.70 5.20 0 -3 9 40.20 6.70 0 -3 9 37.50 4.50 -1 3 -9 22.20 5.80 -1 3 -9 10.00 11.10 -1 3 -9 17.20 5.80 1 -3 9 18.70 5.30 1 -3 9 11.00 4.00 1 -3 9 15.90 3.20 -2 3 -9 54.99 9.90 -2 3 -9 55.29 9.20 -2 3 -9 60.99 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73.69 14.50 4 -7 10 71.09 9.00 4 -7 10 68.09 15.00 -5 7 -10 37.50 13.90 5 -7 10 4.10 6.20 6 6 -10 -18.60 13.70 6 6 -10 7.90 6.10 6 6 -10 2.70 7.20 6 6 -10 8.90 11.40 6 6 -10 28.20 11.70 -6 -6 10 0.40 5.80 -6 -6 10 16.70 7.00 -6 -6 10 26.40 7.40 -6 -6 10 9.70 5.20 5 6 -10 3.60 6.20 5 6 -10 -2.70 12.20 5 6 -10 4.50 8.20 5 6 -10 -2.60 5.30 5 6 -10 9.00 9.70 -5 -6 10 -0.70 4.40 -5 -6 10 -2.90 5.60 -5 -6 10 3.70 4.30 -5 -6 10 8.20 5.40 -5 -6 10 26.90 11.50 4 6 -10 11.30 6.40 4 6 -10 2.30 10.30 4 6 -10 23.80 9.50 4 6 -10 6.00 4.40 4 6 -10 -0.10 7.80 -4 -6 10 -7.90 5.00 -4 -6 10 5.60 6.30 -4 -6 10 -3.90 6.10 -4 -6 10 -1.70 5.00 3 6 -10 2.90 6.60 3 6 -10 2.90 8.30 3 6 -10 -8.00 4.00 3 6 -10 6.30 6.50 -3 -6 10 -0.50 4.60 -3 -6 10 8.90 6.40 -3 -6 10 6.20 8.00 -3 -6 10 2.60 3.70 2 6 -10 4.70 3.30 2 6 -10 2.20 6.60 2 6 -10 0.30 6.00 2 6 -10 19.80 8.50 -2 -6 10 2.70 7.50 -2 -6 10 8.80 7.80 -2 -6 10 6.20 4.20 -2 -6 10 2.40 4.20 1 6 -10 2.70 6.90 1 6 -10 -4.60 6.50 1 6 -10 12.90 6.50 -1 -6 10 2.40 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11.40 5 5 -10 31.50 9.30 5 5 -10 12.50 9.20 -5 -5 10 15.10 5.80 -5 -5 10 10.40 4.40 -5 -5 10 5.90 5.70 -5 -5 10 16.10 5.50 -5 -5 10 19.80 7.90 4 5 -10 3.30 3.10 4 5 -10 15.60 7.90 4 5 -10 0.60 5.10 4 5 -10 -9.80 9.40 4 5 -10 6.30 7.30 4 5 -10 13.40 5.60 -4 -5 10 3.20 5.20 -4 -5 10 -0.10 4.70 -4 -5 10 -15.70 7.60 -4 -5 10 3.50 3.20 -4 -5 10 2.80 4.70 3 5 -10 3.70 6.90 3 5 -10 5.00 5.80 3 5 -10 -8.60 7.80 -3 -5 10 -6.90 4.10 -3 -5 10 0.10 4.80 -3 -5 10 -6.20 6.60 -3 -5 10 -2.30 4.70 2 5 -10 -8.80 7.60 2 5 -10 -0.90 5.20 2 5 -10 5.60 3.60 2 5 -10 -5.40 5.20 -2 -5 10 -6.60 6.30 -2 -5 10 2.40 4.20 -2 -5 10 -1.50 5.10 -2 -5 10 -4.00 4.10 1 5 -10 12.50 7.80 1 5 -10 -0.50 5.50 1 5 -10 8.60 8.20 -1 -5 10 10.20 10.00 -1 -5 10 4.40 4.70 -1 -5 10 13.10 4.40 0 5 -10 51.49 13.80 0 5 -10 82.79 12.40 0 5 -10 89.09 11.00 0 -5 10 76.99 6.90 0 -5 10 89.69 7.20 0 -5 10 73.59 9.70 -1 5 -10 -8.10 6.90 -1 5 -10 9.60 8.50 -1 5 -10 -10.40 7.30 1 -5 10 5.60 3.50 1 -5 10 3.60 4.50 1 -5 10 3.70 6.70 -2 5 -10 3.50 9.00 -2 5 -10 3.20 8.90 -2 5 -10 -5.10 7.90 2 -5 10 12.80 4.80 2 -5 10 27.90 8.20 2 -5 10 13.60 3.40 -3 5 -10 12.30 7.40 -3 5 -10 13.20 9.60 -3 5 -10 25.20 9.80 3 -5 10 25.30 8.90 3 -5 10 28.90 4.00 3 -5 10 17.10 5.10 3 -5 10 31.40 8.80 -4 5 -10 17.20 10.50 -4 5 -10 11.70 10.80 -4 5 -10 5.70 8.00 -4 5 -10 20.00 9.10 4 -5 10 8.00 9.30 4 -5 10 7.10 8.60 4 -5 10 15.70 5.00 -5 5 -10 15.40 11.80 -5 5 -10 -20.30 11.40 -5 5 -10 20.00 11.40 -5 5 -10 0.10 3.20 -5 5 -10 15.10 11.80 5 -5 10 1.70 7.60 5 -5 10 0.00 4.80 5 -5 10 4.20 10.80 -6 5 -10 33.00 10.60 -6 5 -10 19.10 14.70 -6 5 -10 33.20 6.70 -6 5 -10 37.60 12.60 6 -5 10 28.70 6.40 6 -5 10 18.70 6.20 6 -5 10 38.70 11.10 7 4 -10 9.70 6.60 7 4 -10 11.90 10.90 7 4 -10 -0.90 11.80 7 4 -10 -25.50 14.80 7 4 -10 43.90 14.50 -7 -4 10 13.50 6.70 -7 -4 10 15.00 6.30 -7 -4 10 12.40 9.90 6 4 -10 12.50 12.20 6 4 -10 -1.90 9.00 6 4 -10 3.70 5.40 6 4 -10 6.20 10.80 6 4 -10 24.20 10.50 -6 -4 10 -4.50 5.70 -6 -4 10 -0.10 5.20 -6 -4 10 7.00 11.20 -6 -4 10 20.10 8.00 5 4 -10 0.40 10.30 5 4 -10 0.70 6.00 5 4 -10 15.30 9.00 5 4 -10 6.80 5.60 5 4 -10 26.00 9.40 -5 -4 10 18.30 6.20 -5 -4 10 12.40 4.60 -5 -4 10 25.50 9.60 -5 -4 10 10.20 5.30 4 4 -10 7.50 4.30 4 4 -10 8.30 9.10 4 4 -10 18.00 8.20 4 4 -10 13.60 8.20 4 4 -10 8.00 4.30 4 4 -10 8.10 4.80 -4 -4 10 7.20 4.90 -4 -4 10 -0.40 7.80 -4 -4 10 10.50 4.20 -4 -4 10 4.90 3.80 -4 -4 10 5.80 3.70 3 4 -10 19.40 5.30 3 4 -10 16.40 4.60 3 4 -10 22.40 7.90 3 4 -10 9.80 6.60 3 4 -10 11.40 2.50 -3 -4 10 16.40 4.60 -3 -4 10 8.40 4.70 -3 -4 10 12.90 7.00 -3 -4 10 10.10 5.00 2 4 -10 -4.30 7.20 2 4 -10 -1.40 6.70 2 4 -10 2.50 4.70 -2 -4 10 0.10 4.20 -2 -4 10 -1.50 4.40 -2 -4 10 2.80 4.10 -2 -4 10 4.60 4.40 1 4 -10 7.00 5.30 1 4 -10 8.20 8.00 1 4 -10 9.70 2.80 1 4 -10 7.20 6.80 -1 -4 10 3.40 3.30 -1 -4 10 8.20 5.10 -1 -4 10 10.80 3.70 0 4 -10 -3.30 5.60 0 4 -10 7.10 7.60 0 4 -10 16.90 7.60 0 -4 10 9.20 5.60 0 -4 10 2.60 3.30 0 -4 10 4.70 4.30 -1 4 -10 4.40 7.10 -1 4 -10 -7.40 7.50 -1 4 -10 1.90 6.30 1 -4 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-4 -14 25.90 13.40 -2 -4 -14 10.80 10.90 -2 -4 -14 3.60 12.00 2 4 14 12.20 5.10 2 4 14 16.40 5.20 -3 -4 -14 -4.10 11.00 -3 -4 -14 -16.80 11.00 -3 -4 -14 -14.80 11.70 -3 -4 -14 11.70 10.30 -3 -4 -14 -14.00 12.00 -3 -4 -14 19.70 10.60 -3 -4 -14 10.40 10.10 -3 -4 -14 7.60 12.30 3 4 14 6.90 4.90 3 4 14 1.50 4.40 -4 -4 -14 11.40 10.50 -4 -4 -14 21.70 11.60 -4 -4 -14 18.80 11.40 -4 -4 -14 -7.60 8.40 -4 -4 -14 12.80 12.50 -4 -4 -14 -21.70 12.40 -4 -4 -14 -18.40 14.40 -4 -4 -14 -2.90 11.40 4 4 14 1.50 4.60 4 4 14 5.40 4.70 -2 -5 -14 15.00 10.80 -2 -5 -14 25.10 12.00 -2 -5 -14 1.60 12.60 -2 -5 -14 -0.50 11.40 -2 -5 -14 16.00 13.20 -2 -5 -14 0.70 11.80 -2 -5 -14 -7.90 9.50 2 5 14 0.70 4.50 2 5 14 -6.20 4.90 -3 -5 -14 8.70 11.20 -3 -5 -14 -6.30 11.50 -3 -5 -14 5.60 12.70 -3 -5 -14 -17.40 9.50 -3 -5 -14 11.70 11.50 3 5 14 -0.20 4.60 3 5 14 -3.00 4.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 74863 _shelx_res_file ; TITL PX1Me_2MW_0m_a.res in P-1 PX1Me_2MW_0m.res created by SHELXL-2016/6 at 12:25:26 on 30-Jul-2018 CELL 0.71076 8.6538 10.9227 10.9636 85.850 82.381 74.571 ZERR 2.00 0.0048 0.0063 0.0054 0.023 0.020 0.029 LATT 1 SFAC C H N O UNIT 52 44 4 4 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP 20.000 SIZE 0.300 0.390 0.550 ACTA L.S. 20 FMAP 2 PLAN 5 0 0.00 HTAB BOND $H CONF DFIX 0.81 0.01 O3 H3O WGHT 0.083100 0.555100 FVAR 0.85059 O1 4 0.128601 0.946768 0.878621 11.00000 0.06929 0.06177 = 0.06981 -0.02665 0.02495 -0.02524 C1 1 0.063498 0.862628 0.884597 11.00000 0.03431 0.04980 = 0.03813 0.00484 -0.00230 -0.00797 H3O 2 -0.070090 0.924967 1.005327 11.00000 0.19815 C26 1 0.821918 0.801609 0.364341 11.00000 0.03937 0.06835 = 0.06072 0.00224 0.01289 -0.01728 AFIX 137 H26A 2 0.840826 0.738582 0.303606 11.00000 -1.50000 H26B 2 0.901263 0.775487 0.420976 11.00000 -1.50000 H26C 2 0.829479 0.881343 0.324457 11.00000 -1.50000 AFIX 0 C25 1 0.489264 0.929444 0.270499 11.00000 0.06087 0.04234 = 0.03865 0.00284 -0.00303 -0.01997 AFIX 43 H25 2 0.573439 0.932437 0.209051 11.00000 -1.20000 AFIX 0 C24 1 0.331526 0.980771 0.250397 11.00000 0.06976 0.05169 = 0.04771 0.01352 -0.02133 -0.01707 AFIX 43 H24 2 0.308350 1.019279 0.174135 11.00000 -1.20000 AFIX 0 N1 3 0.615222 0.642872 0.972019 11.00000 0.04143 0.05823 = 0.03155 -0.00066 -0.00585 -0.01792 N2 3 0.662636 0.815779 0.430549 11.00000 0.03172 0.04492 = 0.04270 0.00248 0.00254 -0.01188 C2 1 0.100183 0.758698 0.793702 11.00000 0.02809 0.03866 = 0.03438 0.00658 -0.00518 -0.00529 C14 1 0.725768 0.367186 0.718184 11.00000 0.05513 0.04354 = 0.05405 -0.00730 -0.00381 -0.00875 AFIX 43 H14 2 0.748386 0.307509 0.657587 11.00000 -1.20000 AFIX 0 C3 1 -0.016792 0.692399 0.792240 11.00000 0.02896 0.05033 = 0.04401 0.00447 0.00061 -0.00973 AFIX 43 H3 2 -0.109288 0.711578 0.848612 11.00000 -1.20000 AFIX 0 O3 4 -0.053757 0.857058 0.972101 11.00000 0.06141 0.07001 = 0.05434 -0.01367 0.02010 -0.02088 C4 1 0.001239 0.599550 0.709657 11.00000 0.03785 0.05172 = 0.05351 0.00563 -0.00739 -0.02372 AFIX 43 H4 2 -0.076746 0.554773 0.711828 11.00000 -1.20000 AFIX 0 C5 1 0.135304 0.573227 0.623767 11.00000 0.04281 0.05178 = 0.04477 -0.00670 -0.00325 -0.01824 AFIX 43 H5 2 0.147565 0.512118 0.565909 11.00000 -1.20000 AFIX 0 C6 1 0.251833 0.638637 0.624317 11.00000 0.03271 0.05424 = 0.03943 -0.00405 0.00130 -0.01435 AFIX 43 H6 2 0.341532 0.621037 0.565193 11.00000 -1.20000 AFIX 0 C7 1 0.240202 0.729245 0.709388 11.00000 0.02870 0.04112 = 0.03291 0.00504 -0.00553 -0.01044 C21 1 0.393904 0.867260 0.480344 11.00000 0.03480 0.02900 = 0.03796 -0.00015 -0.00401 -0.00888 C8 1 0.384163 0.784928 0.711880 11.00000 0.02746 0.03723 = 0.03510 -0.00337 -0.00035 -0.00959 AFIX 13 H8 2 0.341561 0.869135 0.746666 11.00000 -1.20000 AFIX 0 C22 1 0.234466 0.921165 0.455896 11.00000 0.03727 0.04107 = 0.04949 0.00162 -0.00797 -0.00466 AFIX 43 H22 2 0.148793 0.919612 0.516422 11.00000 -1.20000 AFIX 0 C9 1 0.493927 0.704788 0.799529 11.00000 0.02925 0.04416 = 0.03264 -0.00161 0.00007 -0.01473 C23 1 0.206189 0.976156 0.341900 11.00000 0.04856 0.04997 = 0.06231 0.00712 -0.02088 -0.00490 AFIX 43 H23 2 0.100327 1.011219 0.325564 11.00000 -1.20000 AFIX 0 C10 1 0.513464 0.739743 0.912345 11.00000 0.03751 0.04961 = 0.03833 -0.00381 0.00027 -0.01544 AFIX 43 H10 2 0.464125 0.819036 0.944587 11.00000 -1.20000 AFIX 0 C11 1 0.662816 0.540814 0.897861 11.00000 0.03257 0.04634 = 0.03406 0.00225 -0.00077 -0.01740 C13 1 0.625944 0.486242 0.697177 11.00000 0.04196 0.04392 = 0.04161 -0.00238 -0.00596 -0.01271 AFIX 43 H13 2 0.582726 0.506790 0.622801 11.00000 -1.20000 AFIX 0 C12 1 0.590323 0.575522 0.788235 11.00000 0.02903 0.04218 = 0.03229 -0.00028 -0.00006 -0.01442 C19 1 0.629417 0.775476 0.550536 11.00000 0.03228 0.04153 = 0.03690 0.00161 -0.00217 -0.01055 AFIX 43 H19 2 0.707140 0.734204 0.601145 11.00000 -1.20000 AFIX 0 C15 1 0.792790 0.334744 0.827204 11.00000 0.05284 0.04385 = 0.05888 0.00724 -0.00371 -0.00423 AFIX 43 H15 2 0.858248 0.253282 0.839323 11.00000 -1.20000 AFIX 0 C17 1 0.665285 0.645574 1.092607 11.00000 0.06981 0.08739 = 0.03495 -0.00323 -0.01298 -0.02987 AFIX 137 H17A 2 0.769095 0.663417 1.083578 11.00000 -1.50000 H17B 2 0.672004 0.564573 1.134905 11.00000 -1.50000 H17C 2 0.587916 0.710521 1.139210 11.00000 -1.50000 REM ##### REM ##### REM ##### AFIX 0 C16 1 0.764207 0.421298 0.918555 11.00000 0.04622 0.05712 = 0.04332 0.01407 -0.00845 -0.01388 AFIX 43 H16 2 0.811197 0.400285 0.991351 11.00000 -1.20000 AFIX 0 C20 1 0.519314 0.872837 0.385568 11.00000 0.03808 0.03211 = 0.03993 -0.00165 -0.00211 -0.01247 C18 1 0.467729 0.804120 0.585087 11.00000 0.02928 0.03040 = 0.03634 -0.00177 -0.00089 -0.00816 REM ##### HKLF 4 1 1 0 0 0 1 0 0 0 1 REM PX1Me_2MW_0m_a.res in P-1 REM R1 = 0.0692 for 3077 Fo > 4sig(Fo) and 0.1194 for all 4929 data REM 277 parameters refined using 1 restraints END WGHT 0.0851 0.5545 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y+2, -z+2 HTAB O3 O1_$1 REM Highest difference peak 0.724, deepest hole -0.349, 1-sigma level 0.060 Q1 1 0.2983 0.8682 0.7837 11.00000 0.05 0.72 Q2 1 0.1490 0.8535 0.8197 11.00000 0.05 0.39 Q3 1 0.1766 0.7358 0.7627 11.00000 0.05 0.27 Q4 1 0.3198 0.7449 0.7151 11.00000 0.05 0.24 Q5 1 0.2939 0.5543 0.6339 11.00000 0.05 0.23 ; _shelx_res_checksum 7918 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.1286(3) 0.9468(2) 0.8786(2) 0.0672(6) Uani d 1 C C1 0.0635(3) 0.8626(2) 0.8846(2) 0.0418(6) Uani d 1 H H3O -0.070(8) 0.925(3) 1.005(6) 0.20(3) Uiso d 1 C C26 0.8219(3) 0.8016(3) 0.3643(3) 0.0575(7) Uani d 1 H H26A 0.840826 0.738582 0.303606 0.086 Uiso calc 1 H H26B 0.901263 0.775487 0.420976 0.086 Uiso calc 1 H H26C 0.829479 0.881343 0.324457 0.086 Uiso calc 1 C C25 0.4893(3) 0.9294(2) 0.2705(2) 0.0465(6) Uani d 1 H H25 0.573439 0.932437 0.209051 0.056 Uiso calc 1 C C24 0.3315(4) 0.9808(3) 0.2504(3) 0.0556(7) Uani d 1 H H24 0.308350 1.019279 0.174135 0.067 Uiso calc 1 N N1 0.6152(2) 0.6429(2) 0.97202(18) 0.0427(5) Uani d 1 N N2 0.6626(2) 0.81578(19) 0.43055(18) 0.0403(5) Uani d 1 C C2 0.1002(3) 0.7587(2) 0.7937(2) 0.0346(5) Uani d 1 C C14 0.7258(3) 0.3672(3) 0.7182(3) 0.0517(7) Uani d 1 H H14 0.748386 0.307509 0.657587 0.062 Uiso calc 1 C C3 -0.0168(3) 0.6924(2) 0.7922(2) 0.0420(6) Uani d 1 H H3 -0.109288 0.711578 0.848612 0.050 Uiso calc 1 O O3 -0.0538(3) 0.8571(2) 0.97210(19) 0.0631(6) Uani d 1 C C4 0.0012(3) 0.5995(2) 0.7097(2) 0.0456(6) Uani d 1 H H4 -0.076746 0.554773 0.711828 0.055 Uiso calc 1 C C5 0.1353(3) 0.5732(3) 0.6238(2) 0.0452(6) Uani d 1 H H5 0.147565 0.512118 0.565909 0.054 Uiso calc 1 C C6 0.2518(3) 0.6386(2) 0.6243(2) 0.0419(6) Uani d 1 H H6 0.341532 0.621037 0.565193 0.050 Uiso calc 1 C C7 0.2402(3) 0.7292(2) 0.7094(2) 0.0341(5) Uani d 1 C C21 0.3939(3) 0.8673(2) 0.4803(2) 0.0339(5) Uani d 1 C C8 0.3842(3) 0.7849(2) 0.7119(2) 0.0332(5) Uani d 1 H H8 0.341561 0.869135 0.746666 0.040 Uiso calc 1 C C22 0.2345(3) 0.9212(2) 0.4559(2) 0.0436(6) Uani d 1 H H22 0.148793 0.919612 0.516422 0.052 Uiso calc 1 C C9 0.4939(3) 0.7048(2) 0.7995(2) 0.0347(5) Uani d 1 C C23 0.2062(3) 0.9762(3) 0.3419(3) 0.0543(7) Uani d 1 H H23 0.100327 1.011219 0.325564 0.065 Uiso calc 1 C C10 0.5135(3) 0.7397(2) 0.9123(2) 0.0414(6) Uani d 1 H H10 0.464125 0.819036 0.944587 0.050 Uiso calc 1 C C11 0.6628(3) 0.5408(2) 0.8979(2) 0.0368(5) Uani d 1 C C13 0.6259(3) 0.4862(2) 0.6972(2) 0.0421(6) Uani d 1 H H13 0.582726 0.506790 0.622801 0.050 Uiso calc 1 C C12 0.5903(3) 0.5755(2) 0.7882(2) 0.0339(5) Uani d 1 C C19 0.6294(3) 0.7755(2) 0.5505(2) 0.0371(5) Uani d 1 H H19 0.707140 0.734204 0.601145 0.044 Uiso calc 1 C C15 0.7928(3) 0.3347(3) 0.8272(3) 0.0542(7) Uani d 1 H H15 0.858248 0.253282 0.839323 0.065 Uiso calc 1 C C17 0.6653(4) 0.6456(3) 1.0926(2) 0.0616(8) Uani d 1 H H17A 0.769095 0.663417 1.083578 0.092 Uiso calc 1 H H17B 0.672004 0.564573 1.134905 0.092 Uiso calc 1 H H17C 0.587916 0.710521 1.139210 0.092 Uiso calc 1 C C16 0.7642(3) 0.4213(3) 0.9186(2) 0.0493(6) Uani d 1 H H16 0.811197 0.400285 0.991351 0.059 Uiso calc 1 C C20 0.5193(3) 0.8728(2) 0.3856(2) 0.0363(5) Uani d 1 C C18 0.4677(3) 0.8041(2) 0.5851(2) 0.0322(5) Uani d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0693(14) 0.0618(13) 0.0698(14) -0.0252(11) 0.0249(11) -0.0267(11) C1 0.0343(12) 0.0498(15) 0.0381(13) -0.0080(11) -0.0023(10) 0.0048(11) C26 0.0394(14) 0.0683(19) 0.0607(18) -0.0173(13) 0.0129(12) 0.0022(14) C25 0.0609(16) 0.0423(13) 0.0386(13) -0.0200(12) -0.0030(12) 0.0028(11) C24 0.0698(19) 0.0517(16) 0.0477(16) -0.0171(14) -0.0213(14) 0.0135(12) N1 0.0414(11) 0.0582(13) 0.0315(10) -0.0179(10) -0.0058(8) -0.0007(9) N2 0.0317(10) 0.0449(11) 0.0427(11) -0.0119(8) 0.0025(8) 0.0025(9) C2 0.0281(10) 0.0387(12) 0.0344(11) -0.0053(9) -0.0052(9) 0.0066(9) C14 0.0551(16) 0.0435(14) 0.0540(16) -0.0087(12) -0.0038(13) -0.0073(12) C3 0.0290(11) 0.0503(14) 0.0440(13) -0.0097(10) 0.0006(10) 0.0045(11) O3 0.0614(13) 0.0700(14) 0.0543(12) -0.0209(11) 0.0201(10) -0.0137(11) C4 0.0379(13) 0.0517(15) 0.0535(15) -0.0237(11) -0.0074(11) 0.0056(12) C5 0.0428(13) 0.0518(15) 0.0448(14) -0.0182(11) -0.0032(11) -0.0067(11) C6 0.0327(12) 0.0542(15) 0.0394(13) -0.0144(11) 0.0013(10) -0.0040(11) C7 0.0287(10) 0.0411(12) 0.0329(11) -0.0104(9) -0.0055(9) 0.0050(9) C21 0.0348(11) 0.0290(11) 0.0380(12) -0.0089(9) -0.0040(9) -0.0002(9) C8 0.0275(10) 0.0372(12) 0.0351(12) -0.0096(9) -0.0004(9) -0.0034(9) C22 0.0373(12) 0.0411(13) 0.0495(15) -0.0047(10) -0.0080(11) 0.0016(11) C9 0.0292(11) 0.0442(13) 0.0326(11) -0.0147(9) 0.0001(9) -0.0016(9) C23 0.0486(15) 0.0500(16) 0.0623(18) -0.0049(12) -0.0209(13) 0.0071(13) C10 0.0375(12) 0.0496(14) 0.0383(13) -0.0154(11) 0.0003(10) -0.0038(11) C11 0.0326(11) 0.0463(13) 0.0341(12) -0.0174(10) -0.0008(9) 0.0023(10) C13 0.0420(13) 0.0439(14) 0.0416(13) -0.0127(11) -0.0060(10) -0.0024(11) C12 0.0290(10) 0.0422(12) 0.0323(11) -0.0144(9) -0.0001(9) -0.0003(9) C19 0.0323(11) 0.0415(13) 0.0369(12) -0.0106(10) -0.0022(9) 0.0016(10) C15 0.0528(16) 0.0438(15) 0.0589(17) -0.0042(12) -0.0037(13) 0.0072(13) C17 0.0698(19) 0.087(2) 0.0350(14) -0.0299(17) -0.0130(13) -0.0032(14) C16 0.0462(14) 0.0571(16) 0.0433(14) -0.0139(12) -0.0085(11) 0.0141(12) C20 0.0381(12) 0.0321(11) 0.0399(12) -0.0125(9) -0.0021(10) -0.0017(9) C18 0.0293(10) 0.0304(11) 0.0363(12) -0.0082(9) -0.0009(9) -0.0018(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 C1 O3 120.9(2) O1 C1 C2 124.9(2) O3 C1 C2 114.1(2) N2 C26 H26A 109.5 N2 C26 H26B 109.5 H26A C26 H26B 109.5 N2 C26 H26C 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 C24 C25 C20 117.9(2) C24 C25 H25 121.1 C20 C25 H25 121.1 C25 C24 C23 121.0(3) C25 C24 H24 119.5 C23 C24 H24 119.5 C11 N1 C10 108.1(2) C11 N1 C17 125.0(2) C10 N1 C17 126.9(2) C20 N2 C19 108.30(19) C20 N2 C26 126.1(2) C19 N2 C26 125.6(2) C3 C2 C7 119.2(2) C3 C2 C1 116.8(2) C7 C2 C1 123.9(2) C13 C14 C15 121.4(3) C13 C14 H14 119.3 C15 C14 H14 119.3 C4 C3 C2 121.6(2) C4 C3 H3 119.2 C2 C3 H3 119.2 C1 O3 H3O 102(5) C3 C4 C5 119.5(2) C3 C4 H4 120.2 C5 C4 H4 120.2 C4 C5 C6 119.2(2) C4 C5 H5 120.4 C6 C5 H5 120.4 C5 C6 C7 122.6(2) C5 C6 H6 118.7 C7 C6 H6 118.7 C6 C7 C2 117.7(2) C6 C7 C8 118.5(2) C2 C7 C8 123.7(2) C22 C21 C20 118.0(2) C22 C21 C18 134.8(2) C20 C21 C18 107.2(2) C9 C8 C18 114.13(18) C9 C8 C7 108.83(18) C18 C8 C7 112.70(18) C9 C8 H8 106.9 C18 C8 H8 106.9 C7 C8 H8 106.9 C23 C22 C21 119.3(2) C23 C22 H22 120.3 C21 C22 H22 120.3 C10 C9 C12 105.5(2) C10 C9 C8 125.6(2) C12 C9 C8 128.7(2) C22 C23 C24 121.6(3) C22 C23 H23 119.2 C24 C23 H23 119.2 C9 C10 N1 111.3(2) C9 C10 H10 124.4 N1 C10 H10 124.4 N1 C11 C16 129.4(2) N1 C11 C12 108.1(2) C16 C11 C12 122.5(2) C14 C13 C12 119.5(2) C14 C13 H13 120.2 C12 C13 H13 120.2 C13 C12 C11 118.0(2) C13 C12 C9 135.0(2) C11 C12 C9 107.0(2) C18 C19 N2 110.8(2) C18 C19 H19 124.6 N2 C19 H19 124.6 C14 C15 C16 121.0(2) C14 C15 H15 119.5 C16 C15 H15 119.5 N1 C17 H17A 109.5 N1 C17 H17B 109.5 H17A C17 H17B 109.5 N1 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C15 C16 C11 117.6(2) C15 C16 H16 121.2 C11 C16 H16 121.2 N2 C20 C25 130.2(2) N2 C20 C21 107.6(2) C25 C20 C21 122.2(2) C19 C18 C21 106.1(2) C19 C18 C8 126.7(2) C21 C18 C8 126.96(19) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C1 1.193(3) C1 O3 1.311(3) C1 C2 1.507(4) C26 N2 1.445(3) C26 H26A 0.9600 C26 H26B 0.9600 C26 H26C 0.9600 C25 C24 1.371(4) C25 C20 1.389(3) C25 H25 0.9300 C24 C23 1.385(4) C24 H24 0.9300 N1 C11 1.368(3) N1 C10 1.371(3) N1 C17 1.449(3) N2 C20 1.370(3) N2 C19 1.375(3) C2 C3 1.395(3) C2 C7 1.402(3) C14 C13 1.379(4) C14 C15 1.380(4) C14 H14 0.9300 C3 C4 1.373(4) C3 H3 0.9300 O3 H3O 0.820(10) C4 C5 1.374(3) C4 H4 0.9300 C5 C6 1.383(3) C5 H5 0.9300 C6 C7 1.384(3) C6 H6 0.9300 C7 C8 1.529(3) C21 C22 1.402(3) C21 C20 1.410(3) C21 C18 1.431(3) C8 C9 1.507(3) C8 C18 1.507(3) C8 H8 0.9800 C22 C23 1.370(4) C22 H22 0.9300 C9 C10 1.365(3) C9 C12 1.441(3) C23 H23 0.9300 C10 H10 0.9300 C11 C16 1.388(4) C11 C12 1.410(3) C13 C12 1.394(3) C13 H13 0.9300 C19 C18 1.358(3) C19 H19 0.9300 C15 C16 1.380(4) C15 H15 0.9300 C17 H17A 0.9600 C17 H17B 0.9600 C17 H17C 0.9600 C16 H16 0.9300 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O3 H3O O1 2_577 0.82(4) 1.89(5) 2.679(3) 163(6) y C8 H8 O1 . 0.98 2.20 2.945(4) 132 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C20 C25 C24 C23 -0.1(4) O1 C1 C2 C3 -161.0(3) O3 C1 C2 C3 16.6(3) O1 C1 C2 C7 16.6(4) O3 C1 C2 C7 -165.8(2) C7 C2 C3 C4 -0.5(3) C1 C2 C3 C4 177.2(2) C2 C3 C4 C5 -1.9(4) C3 C4 C5 C6 1.7(4) C4 C5 C6 C7 0.8(4) C5 C6 C7 C2 -3.1(4) C5 C6 C7 C8 172.9(2) C3 C2 C7 C6 2.9(3) C1 C2 C7 C6 -174.7(2) C3 C2 C7 C8 -172.9(2) C1 C2 C7 C8 9.5(3) C6 C7 C8 C9 -90.0(2) C2 C7 C8 C9 85.8(3) C6 C7 C8 C18 37.6(3) C2 C7 C8 C18 -146.6(2) C20 C21 C22 C23 0.4(3) C18 C21 C22 C23 179.7(3) C18 C8 C9 C10 125.1(2) C7 C8 C9 C10 -108.1(2) C18 C8 C9 C12 -59.5(3) C7 C8 C9 C12 67.3(3) C21 C22 C23 C24 -0.6(4) C25 C24 C23 C22 0.4(4) C12 C9 C10 N1 0.4(3) C8 C9 C10 N1 176.70(19) C11 N1 C10 C9 -0.7(3) C17 N1 C10 C9 179.4(2) C10 N1 C11 C16 -179.6(2) C17 N1 C11 C16 0.3(4) C10 N1 C11 C12 0.7(2) C17 N1 C11 C12 -179.4(2) C15 C14 C13 C12 -0.7(4) C14 C13 C12 C11 1.9(3) C14 C13 C12 C9 -179.8(2) N1 C11 C12 C13 178.30(19) C16 C11 C12 C13 -1.4(3) N1 C11 C12 C9 -0.5(2) C16 C11 C12 C9 179.8(2) C10 C9 C12 C13 -178.4(2) C8 C9 C12 C13 5.4(4) C10 C9 C12 C11 0.1(2) C8 C9 C12 C11 -176.1(2) C20 N2 C19 C18 0.3(3) C26 N2 C19 C18 179.6(2) C13 C14 C15 C16 -1.0(4) C14 C15 C16 C11 1.5(4) N1 C11 C16 C15 -179.9(2) C12 C11 C16 C15 -0.2(4) C19 N2 C20 C25 179.3(2) C26 N2 C20 C25 0.1(4) C19 N2 C20 C21 -0.2(3) C26 N2 C20 C21 -179.4(2) C24 C25 C20 N2 -179.5(2) C24 C25 C20 C21 -0.1(4) C22 C21 C20 N2 179.5(2) C18 C21 C20 N2 0.0(2) C22 C21 C20 C25 0.0(3) C18 C21 C20 C25 -179.5(2) N2 C19 C18 C21 -0.3(3) N2 C19 C18 C8 -174.8(2) C22 C21 C18 C19 -179.2(3) C20 C21 C18 C19 0.2(2) C22 C21 C18 C8 -4.7(4) C20 C21 C18 C8 174.7(2) C9 C8 C18 C19 -11.6(3) C7 C8 C18 C19 -136.4(2) C9 C8 C18 C21 175.0(2) C7 C8 C18 C21 50.2(3) _cod_database_fobs_code 2242676