#------------------------------------------------------------------------------
#$Date: 2018-10-17 05:48:17 +0300 (Wed, 17 Oct 2018) $
#$Revision: 211493 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/24/26/2242677.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242677
loop_
_publ_author_name
'Hijji, Yousef'
'Benjamin, Ellis'
'Jasinski, Jerry P.'
'Butcher, Ray J.'
_publ_section_title
;
 Crystal structure of the thalidomide analog
 (3a<i>R</i>*,7a<i>S</i>*)-2-(2,6-dioxopiperidin-3-yl)hexahydro-1<i>H</i>-isoindole-1,3(2<i>H</i>)-dione
;
_journal_coeditor_code           LH5881
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              1595
_journal_page_last               1598
_journal_paper_doi               10.1107/S2056989018014317
_journal_volume                  74
_journal_year                    2018
_chemical_formula_iupac          'C13 H16 N2 O4'
_chemical_formula_moiety         'C13 H16 N2 O4'
_chemical_formula_sum            'C13 H16 N2 O4'
_chemical_formula_weight         264.28
_chemical_name_systematic
(3a<i>R</i>*,7a<i>S</i>*)-2-(2,6-Dioxopiperidin-3-yl)hexahydro-1<i>H</i>-isoindole-1,3(2<i>H</i>)-dione
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2018/3
_cell_angle_alpha                90
_cell_angle_beta                 90.475(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.4519(3)
_cell_length_b                   9.2370(3)
_cell_length_c                   11.8727(4)
_cell_measurement_reflns_used    7629
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      77.3360
_cell_measurement_theta_min      3.7200
_cell_volume                     1255.87(7)
_computing_cell_refinement
;
CrysAlisPro (Rigaku OD, 2012)
;
_computing_data_collection
;
CrysAlisPro (Rigaku OD, 2012)
;
_computing_molecular_graphics
;
SHELXTL (Sheldrick, 2008)
;
_computing_publication_material
;
SHELXTL (Sheldrick, 2008)
;
_computing_structure_refinement
;
<i>SHELXL2018/3</i> (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      123(2)
_diffrn_detector_area_resol_mean 10.5081
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type
'Rigaku Oxford Diffraction Xcalibur, Ruby, Gemini'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0241
_diffrn_reflns_av_unetI/netI     0.0202
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            9733
_diffrn_reflns_theta_full        67.679
_diffrn_reflns_theta_max         77.539
_diffrn_reflns_theta_min         3.723
_exptl_absorpt_coefficient_mu    0.873
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.82191
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2012)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.398
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             560
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.34
_exptl_crystal_size_min          0.18
_refine_diff_density_max         0.333
_refine_diff_density_min         -0.349
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.187
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     177
_refine_ls_number_reflns         2626
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.187
_refine_ls_R_factor_all          0.0674
_refine_ls_R_factor_gt           0.0663
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1179P)^2^+1.1244P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2053
_refine_ls_wR_factor_ref         0.2076
_reflns_number_gt                2572
_reflns_number_total             2626
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            lh5881sup1.cif
_cod_data_source_block           I
_cod_database_code               2242677
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
   0   0   1 100.177 17.0311   5
   0   0   2 81602.3 645.132   5
   0   0   3 101.011 35.1078   5
   0   0   4 30932.0 583.724   5
   0   0   5 91.2614 48.9676   5
   0   0   6 25269.9 684.920   5
   0   0   7 68.7199 43.8209   5
   0   0   8 48617.3 1139.46   5
   0   0  -8 47897.3 1153.10   4
   0   0  -9-71.0395 52.2813   4
   0   0   9 42.0431 45.2800   5
   0   0  10 2183.79 149.435  10
   0   0 -10 2161.63 268.632   4
   0   0  10 2215.98 267.400   5
   0   0  11-4.28577 16.6860  13
   0   0  11 66.3523 31.5702  10
   0   0  12 3031.19 164.468  13
   0   0  13 47.2623 23.0872  13
   0   0 -13 17.5689 18.0061  19
   0   0 -14 14992.1 245.059  19
   0  -1   0 548.862 31.9407   1
   0  -1   0 464.360 40.0877   3
   0  -1   1 19097.1 275.403   3
   0  -1  -1 18595.4 281.917   3
   0   1   1 18773.2 166.043   7
   0   1  -1 18673.5 256.287   2
   0  -1  -1 18621.7 206.378   4
   0  -1   2 839986. 2296.25   5
   0   1   2 999999. 2511.22   5
   0  -1   3 16002.2 374.750   5
   0   1   3 15629.1 375.189   5
   0   1   4 13390.8 400.344   5
   0  -1   4 13852.2 402.801   5
   0  -1   5 6846.64 319.042   5
   0   1   5 6551.24 319.856   5
   0  -1   6 4892.34 303.450   5
   0   1   6 5060.59 316.907   5
   0  -1   7 83.2792 41.0939   5
   0  -1  -7 88.0983 51.4656   4
   0  -1  -8 736.513 141.043   4
   0   1   8 570.589 132.936   5
   0  -1   8 1008.83 163.278   5
   0   1   9 554.413 132.259   5
   0  -1   9 298.930 85.2495   5
   0  -1  -9 733.671 147.851   4
   0   1  -9 516.760 131.814   4
   0   1  10 20122.5 455.844  10
   0  -1  10 19250.0 444.029  10
   0  -1 -10 19908.8 407.904  23
   0  -1  10 20445.3 430.322  13
   0   1 -11 6021.61 225.476  19
   0   1  11 6279.36 258.793  10
   0  -1  11 6569.22 248.509  13
   0   1  12 278.735 50.9401  13
   0   1  12 251.069 52.4086  10
   0   1 -12 301.354 50.3977  19
   0  -1 -13 392.168 52.4939  19
   0   1 -13 365.367 47.7593  19
   0   1  13 428.955 56.7369  13
   0   1 -14 21388.8 273.871  19
   0  -1 -14 21370.6 296.795  19
   0   2   0 471074. 1050.50   2
   0  -2   0 459246. 1786.26   3
   0  -2  -1 6813.54 227.864   3
   0  -2   1 6435.89 176.898   1
   0   2   1 6794.21 157.637   7
   0  -2   1 6538.73 217.608   3
   0   2  -1 6353.75 171.129   2
   0  -2  -1 6539.91 173.506   1
   0  -2  -2 140234. 794.442   4
   0  -2   2 139101. 1097.42   3
   0  -2  -2 142149. 973.569   1
   0  -2  -3 229394. 1306.82   4
   0  -2   3 228648. 1572.14   5
   0  -2   4 312849. 2069.65   5
   0  -2  -4 327146. 2061.99   3
   0  -2   5 73400.8 1103.65   5
   0   2   5 74579.7 1164.78   5
   0  -2  -5 73274.5 1077.95   3
   0  -2  -6 228.316 66.2252   4
   0  -2  -6 251.915 75.3551   3
   0   2   6 274.319 82.0351   5
   0  -2   6 208.585 67.5016   5
   0  -2   7 3694.35 292.185   5
   0  -2  -7 4449.21 313.967   4
   0  -2  -7 4197.00 301.851   3
   0  -2  -8 1739.08 213.323   4
   0  -2  -8 1774.51 216.167   3
   0  -2   8 1628.30 208.088   5
   0  -2  -9 5360.06 403.069   4
   0  -2   9 5688.92 414.523   5
   0   2   9 5638.68 216.501   8
   0   2  -9 5678.73 438.806   4
   0  -2  -9 5557.92 211.250  23
   0   2  10 548.057 73.3983   8
   0  -2 -10 539.444 70.9608  23
   0   2 -10 611.057 72.4399  19
   0   2  10 549.005 76.5747  10
   0   2  11 2539.44 164.074  10
   0  -2 -11 2563.29 151.574  23
   0   2 -11 2556.51 144.694  19
   0   2  12 1682.28 127.908  10
   0   2 -12 1849.65 115.929  19
   0   2  13 101.345 30.7838  13
   0   2 -13 83.8322 24.6357  19
   0  -2  13 85.4305 27.6594  27
   0  -2 -14 5595.41 147.905  19
   0   2  14 5722.40 139.732  13
   0  -2  14 5825.20 161.263  27
   0   3   0 56.6727 14.6536   2
   0  -3   0 49.9727 29.8965   3
   0  -3   0 55.7466 22.5771   1
   0  -3   1 126648. 919.812   1
   0  -3  -1 128241. 1220.88   3
   0  -3   1 125735. 1192.41   3
   0  -3  -1 128277. 905.730   1
   0   3   1 127737. 879.263   7
   0  -3  -2 99262.6 898.307   1
   0  -3  -2 99239.9 1116.96   3
   0  -3   2 98263.6 1098.40   3
   0  -3  -3 17923.7 436.533   1
   0  -3  -3 16896.8 499.337   3
   0  -3   3 17082.9 482.662   3
   0  -3   4 1956.14 183.088   5
   0  -3  -4 2161.07 192.718   3
   0  -3  -4 2001.00 166.731   1
   0  -3  -5 120651. 1525.45   3
   0  -3   5 121613. 1526.00   5
   0  -3  -6 158382. 1874.29   3
   0  -3   6 152634. 1840.37   5
   0  -3  -7 225.985 71.0254   4
   0  -3   7 154.698 65.2384   5
   0  -3  -7 193.463 72.7741   3
   0  -3   8 17479.5 696.717   5
   0  -3  -8 18168.8 708.532   3
   0  -3  -8 17483.0 698.344   1
   0  -3  -9 217.897 70.5034   1
   0   3  -9 157.903 32.0220  19
   0  -3  -9 162.753 36.3318  23
   0   3  -9 147.770 72.4497   4
   0   3   9 211.723 49.0084  10
   0   3   9 224.637 45.6201   8
   0  -3   9 197.315 82.7438   5
   0   3 -10 523.821 66.5218  19
   0   3  10 511.174 74.5375  10
   0   3  10 537.941 70.9111   8
   0  -3 -10 524.968 71.3564  23
   0  -3 -11 4647.11 201.641  23
   0   3  11 4812.79 224.548  10
   0   3 -11 5055.63 198.411  19
   0  -3  12 8070.21 269.032  27
   0  -3 -12 7839.40 246.512  23
   0   3 -12 8537.23 234.698  19
   0   3  12 8262.58 271.612  10
   0   3  13 1737.51 106.872  13
   0  -3  13 1739.31 106.651  27
   0   3 -13 1716.59 85.9926  19
   0   3  13 1698.69 103.939  10
   0   3  14 764.185 46.6567  13
   0   3 -14 743.085 44.7572  30
   0  -3 -14 859.831 54.0735  19
   0  -4   0 475105. 1915.25   1
   0  -4   0 444384. 2666.35   3
   0  -4  -1 9571.45 277.381   1
   0  -4   1 9379.16 283.361   1
   0   4   1 9703.21 290.617   7
   0  -4  -1 8579.50 375.045   3
   0  -4   1 8889.26 375.339   3
   0  -4  -2 1339.39 115.350   1
   0   4   2 1507.03 98.6739   7
   0  -4   2 1493.18 160.009   3
   0  -4  -2 1168.69 145.203   3
   0  -4  -3 14121.0 510.102   3
   0  -4   3 14736.2 517.734   3
   0  -4   4 13520.6 526.890   5
   0  -4  -4 12799.9 510.851   3
   0  -4  -4 14221.1 456.532   1
   0  -4  -5 8639.92 446.195   3
   0  -4  -5 9950.25 420.645   1
   0  -4   5 8677.01 450.404   5
   0  -4  -6 3472.04 274.128   1
   0  -4   6 3096.18 278.345   5
   0  -4  -6 3191.73 281.256   3
   0  -4  -7 6333.00 415.575   3
   0  -4  -7 6684.16 408.370   1
   0  -4   7 6104.59 412.973   5
   0  -4  -8 3971.41 338.209   3
   0   4   8 4388.55 186.150   8
   0  -4   8 4229.92 202.090  27
   0   4   8 4334.63 208.004  10
   0   4   8 3951.04 185.486  20
   0   4  -8 4377.71 372.067   4
   0  -4  -8 4130.44 341.552   1
   0  -4   8 4230.70 353.461   5
   0   4   9 57.9988 28.6636   8
   0   4   9 42.1744 30.9607  10
   0   4  -9 7.99390 19.9461  19
   0  -4   9 76.2399 33.0591  27
   0  -4  -9 9.10534 18.7892  23
   0  -4 -10 2818.28 161.068  23
   0   4  10 3063.88 164.990   8
   0   4 -10 3251.21 160.261  19
   0   4  10 3087.11 184.058  10
   0  -4  10 3083.16 179.564  27
   0  -4 -11 5480.57 216.372  23
   0   4 -11 6137.41 208.188  19
   0  -4  11 6167.29 244.386  27
   0   4  11 5945.52 242.731  10
   0  -4  12 15874.8 347.994  27
   0   4  12 15507.9 349.753  10
   0   4 -12 15898.6 288.040  19
   0   4 -13 255.400 36.5176  30
   0   4  13 259.014 40.4416  13
   0   4  13 240.712 36.2052  10
   0  -4  13 244.039 35.8066  27
   0  -4 -14 17.7311 8.63602  19
   0  -5   0 14.6996 29.2004   3
   0  -5  -1 923.889 142.230   3
   0  -5   1 1046.14 150.219   3
   0   5   1 982.834 107.100   7
   0  -5   2 69654.3 1230.40   3
   0  -5  -2 68529.2 1222.76   3
   0  -5  -3 13020.5 550.561   3
   0  -5   3 13439.1 562.260   3
   0  -5   4 6734.41 412.451   3
   0  -5   4 6924.63 421.521   5
   0  -5  -4 6221.80 395.242   3
   0  -5  -5 55.3377 45.8747   3
   0  -5   5-72.9438 49.1223   5
   0  -5   6 2030.56 240.396   5
   0  -5  -6 2066.33 239.513   3
   0   5   7-9.08819 15.4914  20
   0   5   7-19.6287 19.9257  10
   0   5   8 14290.5 336.518   8
   0  -5   8 13957.6 381.080  27
   0   5   8 14252.6 393.233  10
   0   5   8 13371.9 355.085  20
   0   5  -8 14190.7 333.705  19
   0   5   9 8917.88 271.067   8
   0   5  -9 9089.00 267.059  19
   0  -5   9 8800.11 304.849  27
   0   5   9 8753.89 312.388  10
   0  -5  -9 8378.53 276.594  23
   0  -5  10 15891.4 397.455  27
   0   5  10 15885.3 352.905   8
   0   5 -10 16374.3 341.323  19
   0   5  10 15190.1 400.574  10
   0   5 -11 973.301 89.4613  30
   0  -5 -11 1076.20 92.6652  23
   0  -5  11 1252.32 101.706  27
   0   5  11 1126.16 100.790  10
   0   5  12 68.5301 25.8787  10
   0  -5  12 69.5799 21.5909  27
   0   5 -12 46.8374 22.2504  30
   0  -5 -12 78.0493 28.1690  23
   0   5 -13 177.920 25.0821  26
   0   5  13 224.886 33.3874  13
   0   5 -13 186.876 25.3396  30
   0  -6   0 53127.5 1179.88   3
   0  -6  -1 19537.1 725.269   3
   0  -6   1 19405.0 720.380   3
   0  -6  -2 31650.7 937.399   3
   0  -6   2 30799.1 922.738   3
   0  -6  -3 148.528 69.8783   3
   0  -6   3 28.7157 38.5822   3
   0  -6   4 21995.9 816.244   5
   0  -6   4 22723.7 826.655   3
   0  -6  -4 20453.7 782.047   3
   0  -6  -5 1109.87 188.641   3
   0  -6   5 1247.73 194.686   5
   0   6   6 128.729 39.1372  26
   0   6   6 137.616 35.4758  20
   0   6  -6 137.752 39.2734  30
   0  -6   6 166.844 74.9694   5
   0  -6   6 73.5911 31.0395  27
   0  -6  -6 131.976 67.7028   3
   0   6  -7 27382.3 519.703  30
   0  -6   7 29091.6 554.391  27
   0   6   7 27620.9 542.647  10
   0   6   7 27965.6 502.378  20
   0   6   8 6036.48 239.188  20
   0   6   8 6287.09 265.296  10
   0  -6   8 6662.24 264.831  27
   0   6  -8 5889.39 242.016  30
   0  -6  -9 441.139 62.7217  23
   0   6  -9 511.358 71.1599  30
   0   6   9 634.307 83.2864  10
   0  -6   9 519.551 73.3039  27
   0  -6  10-2.06293 26.7833  27
   0   6  10 5.74451 21.6572  10
   0   6 -10 29.4543 21.8363  30
   0  -6 -10 22.5040 19.2789  23
   0   6 -11 8791.92 239.511  26
   0   6  11 8731.55 248.537  10
   0   6 -11 8445.60 235.023  30
   0  -6 -11 8395.29 233.173  23
   0   6  12 3147.93 113.122  10
   0   6 -12 3348.90 117.952  30
   0   6 -12 3321.38 116.287  26
   0  -6 -12 3262.83 121.455  23
   0  -7   0-32.7536 41.7520   3
   0  -7   1 9968.41 562.384   3
   0  -7  -1 9522.16 550.010   3
   0  -7   2 850.681 165.091   3
   0  -7  -2 708.615 149.890   3
   0   7  -3 9733.00 301.061  26
   0   7   3 9891.35 309.461  30
   0   7  -3 10015.8 309.710  30
   0  -7  -3 10035.0 571.137   3
   0   7   3 10498.2 309.911  26
   0  -7   3 10384.6 584.684   3
   0   7   3 10553.8 289.168  20
   0   7  -4 2230.92 147.620  26
   0  -7   4 2543.41 292.167   5
   0   7  -4 2310.23 151.960  30
   0  -7  -4 2511.85 289.536   3
   0   7   4 2582.70 158.621  26
   0   7   4 2478.37 145.042  20
   0   7   5 9396.89 285.653  20
   0   7   5 9261.93 308.109  26
   0   7  -5 9344.71 306.952  26
   0   7  -5 8877.79 300.283  30
   0   7  -6 133.240 39.5308  30
   0   7   6 67.1045 28.6571  26
   0   7   6 121.056 37.3833  20
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   3   1   0 225698. 1030.96   1
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   3   1   7 7571.95 465.194   5
   3   1   8 27.4882 41.7461   5
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   3   1  12 10561.5 327.787  13
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   3   1  13 129.205 35.6924  13
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   3  -2  -1 180673. 969.440   6
   3   2  -1 178601. 772.101   1
   3   2  -1 180101. 1527.85   7
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   3   2   0 10579.9 342.601   6
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   3  -2   7 45303.7 1113.60   5
   3   2   7 47534.3 1213.46   5
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   3  -2  12 12.8810 20.3199  13
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   4   0  -6 2036.25 226.588   1
   4   0  -5 98.0185 62.1149   1
   4   0  -5 118.977 45.3087   7
   4   0  -4 192780. 1855.55   1
   4   0  -4 209583. 1610.08   7
   4   0  -3 31.7543 28.6359   1
   4   0  -3 73.5398 32.5297   7
   4   0  -2 66842.9 898.683   1
   4   0  -2 64431.6 847.770   7
   4   0  -1 55.0277 34.2997   1
   4   0  -1 52.1395 29.2629   7
   4   0   0 23520.0 528.125   7
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   4   0   0 25094.1 492.762   1
   4   0   0 24090.1 524.012   6
   4   0   1 93.7955 41.9447   7
   4   0   1 51.2134 29.1035   1
   4   0   1 57.0247 20.1801   5
   4   0   2 29702.7 585.784   1
   4   0   2 30081.7 533.411   5
   4   0   2 28768.0 645.355   7
   4   0   3 70.1482 36.0980   5
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   4   0   4 14869.9 504.514   5
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   4   0   5 41.2324 36.5668   5
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   4   0   6 4225.97 317.442   5
   4   0   7 27.7879 41.8281   5
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   4   0   9 11.5679 23.6408  13
   4   0   9-41.1302 23.6867   8
   4   0  10 26629.8 555.056  13
   4   0  10 27288.8 499.418   8
   4   0  11 28.7390 26.1942  13
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   4   0  13-8.69971 17.5933  13
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   4   1  -9 595.874 74.3584  22
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   4   1  -8 2377.19 266.936   1
   4  -1  -7 14237.3 634.362   1
   4   1  -7 13723.3 601.419   1
   4   1  -6 49153.2 1081.67   1
   4  -1  -6 55436.7 1192.86   1
   4  -1  -5 20447.2 670.016   1
   4   1  -5 20103.1 606.191   7
   4   1  -5 20216.1 622.553   1
   4   1  -4 14602.9 483.660   7
   4   1  -4 14477.8 474.231   1
   4   1  -3 6600.06 295.560   1
   4  -1  -3 6183.54 326.626   1
   4   1  -3 6391.15 316.645   7
   4   1  -2 50466.1 712.623   1
   4  -1  -2 49924.7 859.180   1
   4   1  -2 51870.5 849.855   7
   4  -1  -2 49073.5 678.675   7
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   4   1  -1 16575.1 473.408   6
   4  -1  -1 15616.7 401.258   7
   4   1  -1 16826.3 370.133   1
   4  -1  -1 16749.1 466.994   1
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   4   1  -1 15253.8 459.997   7
   4   1   0 25032.4 424.098   1
   4  -1   0 25766.3 368.754   5
   4   1   0 24149.3 563.336   7
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   4  -1   0 23928.5 517.393   7
   4   1   0 24155.2 558.562   6
   4  -1   0 23876.2 541.739   1
   4  -1   1 78289.1 768.519   5
   4  -1   1 75596.0 982.625   1
   4   1   1 75228.7 1020.39   7
   4   1   1 77964.5 777.133   1
   4  -1   2 112008. 1245.56   1
   4  -1   2 114003. 1094.56   5
   4   1   2 113696. 1062.49   5
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   4   1   2 113003. 1318.31   7
   4  -1   3 41313.3 744.849   5
   4   1   3 42555.8 756.797   5
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   4   1   3 40661.4 824.974   7
   4  -1   3 41107.8 805.114   1
   4   1   4 2574.18 212.116   5
   4  -1   4 2798.53 215.992   5
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   4  -1   5 707.291 122.448   5
   4   1   5 620.066 116.091   5
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   4  -1   6 14441.1 586.654   5
   4   1   6 14514.5 605.388   5
   4  -1   7 4004.51 336.287   5
   4   1   7 4457.32 363.867   5
   4  -1   8 2489.27 279.117   5
   4   1   8 2582.83 293.847   5
   4  -1   9 2325.90 137.270   8
   4   1   9 2297.35 145.804   8
   4  -1   9 2315.58 161.425  13
   4   1  10 198.367 44.2767   8
   4  -1  10 185.416 50.4750  13
   4   1  10 252.609 56.2096  13
   4  -1  11 63.4459 33.9087  13
   4   1  11 108.480 35.9958   8
   4   1  11 54.2972 36.2217  13
   4  -1  12 14414.9 377.217  13
   4   1  12 14534.7 379.952  13
   4  -1  13 81.6459 28.9153  13
   4   1  13 104.684 33.8585  13
   4  -1  13 117.967 34.4536  27
   4  -1  14 3359.97 123.318  27
   4   1  14 3349.72 119.582  13
   4   1  14 3241.11 116.318  27
   4  -1  14 3138.20 108.831  13
   4  -2 -14 176.105 24.1853  19
   4   2 -14 175.307 24.4831  19
   4  -2 -13 970.991 73.8811  19
   4   2 -13 921.576 72.7789  19
   4   2 -12 272.733 40.3763  29
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   4   2 -12 292.690 49.1662  19
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   4  -2 -11 525.341 66.8383  22
   4   2 -11 505.332 68.8905  19
   4   2 -11 535.104 64.3377  29
   4  -2 -10 1917.59 132.838  22
   4  -2 -10 2154.02 133.358  15
   4   2 -10 2021.59 137.851  19
   4   2 -10 1980.25 130.487  29
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   4  -2  -9 1103.13 96.7975  23
   4  -2  -9 1073.94 98.0792  22
   4   2  -9 1149.02 98.1345  29
   4   2  -9 1117.32 102.003  19
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   4  -2  -9 1171.25 99.0405  15
   4   2  -8 1186.96 100.289  19
   4  -2  -8 1024.52 186.596   1
   4   2  -8 1069.77 178.971   1
   4   2  -7 3979.11 328.396   1
   4   2  -7 4102.62 327.041   7
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   4  -3   1 102689. 1384.84   1
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   4  -3   7 26596.3 885.705   5
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   4   3   8 1961.01 135.414  20
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   4   3   8 1892.65 132.951   8
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   4   3   9 7012.20 263.635   8
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   4  -3  11 5865.24 247.845  13
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   4   4   7 14763.8 364.424  20
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   4   4   7 14014.6 356.721   8
   4  -4   8 1367.42 126.713  13
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   4   4   8 1321.85 114.054   8
   4   4   9 36693.1 602.489   8
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   4   4  10 47205.1 672.444   8
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   4   5   2 7587.96 416.452   7
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   4   5   7 5353.39 227.926  20
   4   5   7 5185.83 223.514   8
   4   5   8 2190.42 150.469  20
   4   5   8 2089.37 141.967   8
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   4   5   9 5087.76 220.690   8
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   4  -5  10 785.746 90.5485  13
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   4   5  10 836.554 88.8209   8
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   4   5  11 2425.95 130.867   8
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   4  -5  12 17615.5 330.503  27
   4   5  12 17373.3 308.378  13
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   4   6  -7 23257.0 488.524  30
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   4  -6  -5 59471.9 679.258  16
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   4  -6  -4 22553.8 465.510  18
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   4  -6  -1 2409.16 262.966   3
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   4   6   0 18529.3 710.608   7
   4  -6   0 18396.2 715.730   3
   4  -6   0 18273.8 698.714   1
   4  -6   1 1093.05 176.048   1
   4   6   1 1310.93 181.586   7
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   4  -6   2 9793.10 521.456   1
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   4  -6   3 338.093 107.187   5
   4  -6   4 17670.0 766.210   5
   4   6   4 16673.6 384.271  20
   4  -6   4 18045.9 425.492   9
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   4   6   4 18143.3 389.829  26
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   4   6   5 9665.48 301.205  20
   4  -6   5 10241.6 336.419   9
   4  -6   5 9146.20 339.844  27
   4   6   6 22280.4 463.103  20
   4  -6   6 23414.2 534.434  13
   4  -6   6 22796.0 532.125  27
   4   6   7 163.220 52.3326  20
   4   6   7 171.897 57.7749   8
   4  -6   7 281.130 67.5513  27
   4  -6   7 155.351 50.9709  13
   4   6   8 3286.57 180.908  20
   4   6   8 3366.67 176.146   8
   4  -6   8 3189.20 196.933  27
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   5   0  -6 6729.16 453.156   1
   5   0  -5-37.7093 36.8138   1
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   5   0  -3 16.6818 26.2036   1
   5   0  -3 212.776 63.6700   7
   5   0  -2 146106. 1567.74   6
   5   0  -2 147381. 1497.31   1
   5   0  -2 148299. 1463.48   7
   5   0  -1 28.5473 37.0380   1
   5   0  -1 101.188 40.0047   7
   5   0  -1 59.5778 39.6398   6
   5   0   0 87562.4 1169.36   7
   5   0   0 89269.1 1056.43   1
   5   0   0 88791.7 1152.63   6
   5   0   1 177.581 33.5693   5
   5   0   1 24.2417 18.2440   1
   5   0   2 69093.9 992.223   1
   5   0   2 68916.1 833.390   5
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   5   0   3-6.54841 28.4662   5
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   5   0   5 0.90306 28.6137   5
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   5   0   6 51504.1 1145.52   5
   5   0   7-25.0779 35.6223   5
   5   0   8 12575.6 639.187   5
   5   0   8 12951.3 319.390   8
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   5   0   9 9.01375 15.3587   8
   5   0   9-4.29383 23.6987  13
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   5   0  12 6443.83 247.137  13
   5   0  13 6.83886 12.5622  28
   5   0  13-2.82940 18.0036  27
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   5   1  -8 466.094 64.0725  19
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   5   1  -5 10038.7 453.365   1
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   5  -1  -4 9529.79 469.535   1
   5   1  -4 9751.96 424.401   1
   5   1  -4 10030.0 445.880   7
   5   1  -3 13575.9 446.687   1
   5  -1  -3 12844.6 503.464   1
   5  -1  -3 13654.9 408.023   7
   5   1  -3 12210.9 475.784   7
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   5   1  -2 62285.2 1043.84   7
   5   1  -1 66306.2 1066.25   6
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   5   1  -1 65362.7 1048.82   7
   5  -1  -1 67190.5 1043.12   1
   5  -1  -1 63797.0 950.394   7
   5  -1  -1 66646.0 961.137   6
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   5   1   0 7598.37 352.776   6
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   5  -1   0 7198.35 327.000   7
   5  -1   0 7290.17 335.143   1
   5   1   1 229958. 2036.58   7
   5  -1   1 232454. 1924.63   1
   5  -1   1 244244. 1390.88   5
   5   1   1 241817. 1574.96   1
   5   1   2 117365. 1521.60   7
   5  -1   2 118918. 1417.48   1
   5  -1   3 12165.5 477.022   1
   5  -1   3 12392.2 426.347   5
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   5   1   3 12279.9 419.630   5
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   5   1   3 12801.0 520.150   7
   5  -1   4 34909.6 792.356   5
   5   1   4 35233.6 806.521   5
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   5  -1   5 2326.41 224.467   5
   5   1   5 2155.12 223.392   5
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   5  -1   6 203.024 74.0093   5
   5   1   6 147.348 66.1770   5
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   5  -1   7 2587.13 274.197   5
   5   1   7 2668.91 285.260   5
   5  -1   8 16385.6 722.263   5
   5   1   8 16810.7 754.732   5
   5   1   8 17253.6 383.178   8
   5  -1   8 16646.2 421.217  13
   5   1   8 17099.2 423.448  13
   5   1   9 341.993 59.4797   8
   5  -1   9 270.042 59.9022  13
   5   1   9 253.339 56.5705  13
   5  -1  10 6206.82 272.365  13
   5   1  10 6147.53 240.294   8
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   5   6  -3 22044.4 875.065   7
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   6   0  -3-14.0370 25.7729   1
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   6   0  -1 34.6186 28.2785   1
   6   0  -1-6.16370 25.1222   7
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   6   0   1 20.5925 24.0162   1
   6   0   1 18.9466 30.6615   7
   6   0   2 84822.1 1211.36   1
   6   0   2 83193.1 1375.62   7
   6   0   3 114.255 41.2008   5
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   6   0  12 860.300 79.3955  28
   6   0  12 817.065 83.9381  13
   6   0  12 812.722 77.7830  27
   6   0  13 15.6311 9.80088  28
   6   0  13 8.05885 10.9574  27
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   6   1 -11 870.123 82.2008  29
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   6  -1  -7 5091.26 413.781   1
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   6  -1  -6 1152.44 195.377   1
   6   1  -5 104.152 52.9573   1
   6  -1  -5 80.6636 52.6824   1
   6   1  -5 143.749 56.5014   7
   6   1  -4 9692.32 463.310   7
   6  -1  -4 10161.2 474.106   6
   6   1  -4 9760.50 446.340   1
   6  -1  -4 8885.36 482.275   1
   6  -1  -3 5257.24 330.103   6
   6   1  -3 4358.11 340.881   6
   6   1  -3 5548.50 311.843   1
   6  -1  -3 4695.92 341.076   1
   6   1  -3 4896.43 333.658   7
   6  -1  -3 4756.91 284.979   7
   6   1  -2 1916.45 209.336   6
   6  -1  -2 1909.75 204.935   1
   6   1  -2 1971.71 172.151   1
   6  -1  -2 1775.53 182.002   7
   6   1  -2 1708.62 197.320   7
   6  -1  -2 2013.31 192.971   6
   6   1  -1 79855.6 1294.00   7
   6  -1  -1 81290.1 1212.40   7
   6  -1  -1 81306.7 1262.91   1
   6  -1  -1 83975.6 1207.14   6
   6   1  -1 81830.4 1316.45   6
   6   1   0 291.723 82.4282   6
   6   1   0 450.892 75.6771   1
   6  -1   0 287.469 76.8527   1
   6  -1   0 365.815 89.3579   7
   6   1   1 168421. 1479.44   1
   6  -1   1 157528. 1747.84   1
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   6   1   1 154646. 1868.99   7
   6  -1   2 10718.7 463.572   1
   6   1   2 11371.0 522.848   7
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   6   1   3 31290.8 886.301   7
   6  -1   3 31204.9 828.018   1
   6  -1   4 25837.9 703.638   5
   6   1   4 26308.1 713.298   5
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   6  -1   5 1266.35 173.199   5
   6   1   5 1089.10 160.681   5
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   6  -1   6 11192.0 543.831   5
   6   1   6 11144.1 558.222   5
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   6   1   7 67.7538 40.3965  21
   6  -1   7 134.346 63.4347   5
   6   1   7 132.843 42.6656  13
   6  -1   8 5100.85 240.001  13
   6   1   8 5248.42 213.791   8
   6   1   8 4999.57 231.394  13
   6   1   9 441.636 65.3506   8
   6  -1   9 532.497 79.1924  28
   6  -1   9 477.699 76.2321  13
   6   1   9 432.031 71.6629  13
   6   1  10 27.2110 20.9992   8
   6  -1  10 28.4335 22.6349  28
   6  -1  10 18.3356 26.9357  13
   6   1  10 24.0303 25.0060  13
   6  -1  11 15967.0 408.357  13
   6   1  11 15627.4 397.196  13
   6  -1  11 16343.7 396.197  27
   6  -1  12 3724.30 175.863  13
   6   1  12 3625.40 168.270  28
   6   1  12 3605.01 170.093  13
   6  -1  12 3571.08 163.265  27
   6  -1  12 4015.49 152.267  28
   6  -1  13 3197.46 130.076  13
   6   1  13 3076.48 115.230  28
   6  -1  13 3160.04 118.621  27
   6   1  13 3238.49 129.430  13
   6   2 -13 59.2465 18.2550  19
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   6   2 -12 283.396 40.3449  29
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   6   2  -7 540.688 72.9348  15
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   6   2  -5 18051.0 694.668   7
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   6   2   1 35209.6 929.538   7
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   6  -2   3 34367.9 769.902   5
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   6   2   3 31328.7 921.575   7
   6  -2   4 677.415 119.341   5
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   6  -2   5 17703.6 653.058   5
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   6  -2   6 3020.36 287.555   5
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   6   2   7 9030.64 278.460  11
   6   2   7 8219.63 271.319  21
   6  -2   7 8505.44 291.170  28
   6  -2   7 7893.13 482.722   5
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   6   2   7 8500.40 271.671   8
   6  -2   7 8248.88 299.522  13
   6  -2   7 8651.62 295.791  27
   6   2   8 3260.15 173.874  21
   6   2   8 2939.83 165.482   8
   6  -2   8 2932.49 186.586  13
   6  -2   8 3104.71 181.402  28
   6  -2   8 3061.91 183.835  27
   6   2   8 3141.55 183.415  13
   6   2   9 12039.6 339.754   8
   6  -2   9 13258.9 367.890  28
   6  -2   9 11838.1 377.702  13
   6  -2   9 12145.2 371.970  27
   6   2   9 12201.0 367.591  13
   6   2  10 664.185 78.7946   8
   6  -2  10 636.971 87.6524  13
   6  -2  10 645.740 85.8431  27
   6   2  10 636.383 83.9641  13
   6  -2  10 776.769 85.2775  28
   6   2  11 7311.37 235.963   8
   6  -2  11 6967.88 265.792  13
   6  -2  11 7248.00 262.721  27
   6   2  11 7223.01 261.297  13
   6  -2  12 4000.07 175.394  13
   6   2  12 4021.73 174.876  28
   6  -2  12 4043.17 171.462  27
   6   2  12 4092.60 172.893  13
   6  -2  13 1.35252 8.84665   9
   6   2  13 4.42991 15.1198  28
   6  -2  13-13.3391 12.6670  27
   6  -2  13 18.1891 14.8841  13
   6   2  13 0.54954 13.1328  13
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   6   3 -12 752.133 63.2481  19
   6  -3 -12 689.562 52.4083  19
   6   3 -12 775.891 59.6186  29
   6  -3 -11 293.025 48.2469  22
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   6  -3 -11 276.894 41.0860  19
   6   3 -11 249.263 45.5019  19
   6   3 -11 262.093 43.1345  29
   6  -3 -10 1328.62 109.085  22
   6   3 -10 1255.81 104.135  19
   6  -3 -10 1381.20 106.120  15
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   6   3 -10 1384.85 108.769  29
   6  -3  -9 22158.4 456.678  22
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   6   3  -9 22961.3 454.834  19
   6   3  -9 23153.6 466.404  29
   6  -3  -8 261.864 55.1779  22
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   6   3  -8 241.343 49.7077  19
   6   3  -8 209.395 50.0740  29
   6  -3  -8 311.201 59.6999  15
   6  -3  -7 78.4925 42.4557  22
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   6   3  -7 73.1713 34.6841  19
   6  -3  -7 166.977 47.0983  16
   6   3  -7 85.8968 42.9567  29
   6  -3  -6 31586.2 527.688  22
   6   3  -6 30973.3 492.493  19
   6  -3  -6 31036.0 511.809  16
   6   3  -6 31339.4 523.076  29
   6   3  -6 30508.4 962.202   7
   6  -3  -5 24633.8 903.472   1
   6   3  -5 25412.2 877.716   7
   6  -3  -4 13431.4 639.504   1
   6   3  -4 12249.5 621.110   7
   6   3  -3 4238.12 336.315   6
   6  -3  -3 4164.62 351.475   1
   6   3  -3 4001.74 341.013   7
   6   3  -2 39777.8 1013.76   6
   6  -3  -2 41137.9 1051.39   1
   6   3  -2 41351.6 1062.12   7
   6   3  -1 16595.3 663.065   7
   6   3  -1 15847.5 626.437   6
   6  -3  -1 17456.0 682.492   1
   6  -3   0 22016.6 752.490   1
   6   3   0 21396.3 750.760   7
   6   3   0 20970.0 711.135   6
   6  -3   1 70793.2 1375.51   1
   6   3   1 71227.8 1377.41   7
   6  -3   2 5926.89 333.778   5
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   6   3   2 6731.54 430.556   7
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   6  -3   2 6402.15 415.515   1
   6  -3   3 21547.7 664.733   5
   6  -3   3 19567.8 741.300   1
  -6   3  -3 18726.5 724.539   2
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   6   3   3 21218.0 774.827   7
   6  -3   4 37614.8 934.345   5
  -6   3  -4 34955.7 1042.01   2
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   6   3   4 36500.6 1040.55   7
   6  -3   5 46539.2 1094.02   5
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  -6   3  -5 43769.1 1210.46   2
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   6  -3   6 576.171 127.718   5
   6  -3   6 564.248 84.5660  13
   6  -3   6 562.393 79.5848  27
   6   3   7 10464.9 304.886  21
   6   3   7 11281.6 309.737  20
   6   3   7 9941.19 304.847   8
   6  -3   7 10064.1 340.987  13
   6  -3   7 10382.3 338.295  27
   6   3   8 13654.5 362.892   8
   6  -3   8 13577.2 404.002  13
   6  -3   8 13693.3 398.388  27
   6   3   9 11081.7 327.875   8
   6  -3   9 10776.8 358.404  13
   6  -3   9 10804.4 352.779  27
   6   3   9 11463.6 350.392  13
   6  -3  10 1422.01 126.605  13
   6   3  10 1420.10 113.441   8
   6  -3  10 1471.59 125.985  27
   6   3  10 1512.00 123.628  13
   6  -3  11 5376.07 222.883  13
   6   3  11 5304.20 197.952   8
   6  -3  11 5573.23 224.617  27
   6   3  11 5410.31 214.075  13
   6  -3  12 17.2478 18.0688  27
   6  -3  12 27.5340 17.0513  13
   6   3  12 18.4136 14.6278  13
   6   3  13 7287.07 153.566  28
   6  -3  13 7025.66 151.627  13
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   6   4 -12 182.922 27.8016  30
   6  -4 -11 7300.60 208.460  22
   6   4 -11 7579.96 211.934  29
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   6   4 -11 7231.31 212.886  19
   6  -4 -11 7488.21 178.542  19
   6   4 -10 2558.02 141.599  29
   6  -4 -10 2537.36 140.611  22
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   6   4 -10 2480.71 140.334  19
   6  -4 -10 2630.18 132.295  15
   6  -4  -9 157.243 43.0763  22
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   6   4  -9 142.005 39.9138  19
   6  -4  -9 134.385 39.1775  15
   6   4  -9 130.049 39.9098  29
   6  -4  -8 8167.21 281.602  22
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   6   4  -8 8067.50 274.577  19
   6   4  -8 8133.60 280.795  29
   6  -4  -7 1456.76 122.955  22
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   6   4  -7 1336.37 112.177  19
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   6   4  -7 1262.14 116.431  29
   6  -4  -6 1704.47 128.398  22
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   6   4  -6 1651.70 121.249  19
   6   4  -6 1741.13 129.717  29
   6  -4  -6 1663.71 120.830  16
   6   4  -6 2131.35 269.700   7
   6   4  -5 6085.07 453.216   6
   6   4  -5 5059.92 203.742  19
   6  -4  -5 5832.17 448.898   1
   6  -4  -5 6194.09 229.158  16
   6   4  -5 5455.97 223.039  29
   6   4  -5 6201.94 463.828   7
   6   4  -4 3313.22 321.911   6
   6  -4  -4 3179.90 325.031   1
   6   4  -4 3541.35 345.156   7
   6   4  -3 1435.47 209.943   6
   6  -4  -3 1296.64 202.928   1
   6   4  -3 1442.22 219.774   7
   6   4  -2 40290.9 1054.03   6
   6   4  -2 39922.9 1107.04   7
   6  -4  -2 40528.0 1092.91   1
   6  -4  -1 1702.58 224.583   1
   6   4  -1 1710.90 228.821   7
   6   4  -1 1605.39 202.800   6
   6  -4   0 3093.86 299.777   1
   6   4   0 2959.20 293.494   7
   6  -4   1 10235.7 547.221   1
   6   4   1 9599.23 525.682   7
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   6  -4   2 25861.0 872.738   1
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   6  -4   2 27750.7 787.636   5
   6   4   2 26113.4 873.852   7
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   6  -4   3 6269.14 387.817   5
   6  -4   3 5521.40 414.905   1
   6   4   3 5982.76 426.953   7
   6  -4   4 9909.85 512.693   5
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   6   4   4 10026.1 548.157   7
   6   4   5 14291.4 355.175  11
   6  -4   5 13989.3 628.718   5
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   6  -4   5 14167.8 392.643  13
   6  -4   5 13990.1 381.135  27
   6  -4   6 2078.81 155.912  13
   6   4   6 2068.05 132.505  21
   6  -4   6 2144.52 250.956   5
   6   4   6 2275.60 140.721  20
   6  -4   6 2112.26 154.438  27
   6  -4   7 18956.1 478.516  13
   6   4   7 19161.3 432.824   8
   6  -4   7 18851.3 472.117  27
   6  -4   8 6839.19 288.547  13
   6   4   8 7037.21 262.825   8
   6  -4   8 7003.30 288.831  27
   6  -4   9 4665.88 231.163  13
   6   4   9 4411.29 204.434   8
   6  -4   9 4589.51 228.833  27
   6   4   9 4987.60 221.260  13
   6  -4  10 6388.41 254.661  13
   6   4  10 6160.52 226.818   8
   6  -4  10 6474.55 254.306  27
   6   4  10 6406.24 235.536  13
   6   4  11 40.6587 21.9665   8
   6  -4  11 39.0497 25.9767  27
   6  -4  11 42.6490 25.4260  13
   6   4  11 50.6011 25.9168  13
   6  -4  12 1253.22 80.2256   9
   6   4  12 1204.40 78.2096  28
   6   4  12 1134.99 70.2972  13
   6  -4  12 1244.37 80.9041  13
   6   5 -12 2221.12 82.4895  12
   6  -5 -11 6718.34 169.973  22
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   6   5 -11 6869.79 176.447  30
   6  -5 -10 9461.55 246.250  22
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   6   5 -10 9955.29 254.391  30
   6   5 -10 9802.64 258.741  29
   6   5  -9 15879.4 366.578  29
   6  -5  -9 15891.9 358.502  22
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   6   5  -9 16781.4 365.050  30
   6  -5  -8 3875.66 188.862  22
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   6   5  -8 3695.26 184.401  19
   6   5  -8 4265.73 193.626  30
   6   5  -8 3927.28 194.371  29
   6   5  -7 820.963 91.9637  29
   6  -5  -7 821.463 90.8261  22
  -6   5   7 838.154 92.2267  10
   6   5  -7 766.388 87.4258  19
   6  -5  -7 888.046 89.7634  16
   6   5  -7 892.145 90.2277  30
   6  -5  -6 7292.21 267.188  22
  -6   5   6 7577.82 270.397  10
   6  -5  -6 7306.36 257.634  16
   6   5  -6 7009.40 266.882  29
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   6   5  -5 9422.95 282.140  17
   6   5  -5 9741.55 321.596  29
   6   5  -4 14143.6 669.898   6
   6  -5  -4 12818.8 357.718  18
   6   5  -4 14943.8 353.897  17
   6   5  -4 13430.3 352.366  29
   6  -5  -4 13613.2 677.626   1
   6   5  -4 13145.2 680.869   7
   6   5  -3 2419.05 271.658   6
   6  -5  -3 2279.42 150.688   9
   6  -5  -3 2409.69 151.507  18
   6   5  -3 2457.33 144.844  29
   6   5  -3 2368.49 289.826   7
   6  -5  -3 2240.45 271.437   1
   6  -5  -2 26060.4 912.049   1
   6   5  -2 24999.7 915.559   7
   6   5  -2 25472.5 855.203   6
   6  -5  -1 9201.79 546.437   1
   6   5  -1 9323.43 547.289   7
   6   5  -1 8592.94 490.023   6
   6   5   0 7855.06 495.573   7
   6  -5   0 8249.55 514.750   1
  -6   5  -1 52246.7 1232.18   2
   6   5   1 52031.2 1267.33   7
   6  -5   1 52421.5 1289.14   1
  -6  -5  -1 53486.3 1120.67   3
   6  -5   2 26869.2 928.384   1
   6   5   2 27001.1 911.286   7
  -6   5  -2 26254.7 893.950   2
  -6  -5  -2 25930.8 824.429   3
   6  -5   3 2016.24 237.762   5
   6  -5   3 1893.05 140.138   9
   6   5   3 1861.11 126.229  17
  -6   5  -3 1895.99 251.116   2
   6   5   3 1885.39 242.548   7
  -6  -5  -3 1906.29 234.612   3
   6   5   3 2083.49 136.010  12
   6   5   4 583.371 79.0563  20
  -6  -5  -4 825.570 157.915   3
   6  -5   4 367.106 104.541   5
   6  -5   4 697.949 106.245   9
   6  -5   4 718.712 90.6694  13
  -6   5  -4 1005.74 181.901   2
   6   5   5 89571.5 873.725  21
   6  -5   5 84629.8 1011.17  13
   6   5   5 89872.6 882.101  20
   6  -5   5 85032.3 967.142   9
   6  -5   5 86030.7 1003.54  27
   6   5   6 1672.78 124.691  20
   6  -5   6 1674.25 141.333   9
   6  -5   6 1585.21 142.015  13
   6  -5   6 1597.11 140.294  27
   6   5   7 2737.80 160.874  20
   6   5   7 2505.56 157.213   8
   6  -5   7 2472.72 175.872  13
   6  -5   7 2577.53 176.306  27
   6   5   8 1982.01 134.628  20
   6   5   8 1889.13 134.969   8
   6  -5   8 1878.44 150.608  13
   6  -5   8 1922.92 151.471  27
   6  -5   9 3435.68 185.512   9
   6   5   9 3378.93 171.446   8
   6  -5   9 3523.15 194.218  13
   6  -5   9 3450.80 191.915  27
   6  -5  10 2958.52 156.342   9
   6   5  10 2896.83 144.552   8
   6  -5  10 3049.04 164.495  13
   6  -5  10 3012.95 163.171  27
   6   5  10 3041.88 142.682  13
   6  -5  11 1287.99 88.2244   9
   6   5  11 1234.02 79.6278   8
   6   5  11 1245.79 83.8687  28
   6   5  11 1211.48 75.1119  13
  -6   5 -11 1204.60 71.1542  26
   6  -5  12 2758.07 90.2640   9
   6   6 -11 3070.37 103.714  12
  -6   6  11 4484.21 114.947  10
   6  -6 -10 589.486 52.0381  22
  -6   6  10 701.761 62.9305  10
   6   6 -10 618.673 54.6329  30
   6  -6  -9 6420.93 203.883  22
  -6   6   9 6291.99 214.419  10
   6   6  -9 6718.38 206.961  30
   6  -6  -8 542.509 68.7424  22
  -6   6   8 546.644 70.0458  10
   6   6  -8 527.524 64.8409  30
   6  -6  -8 654.620 67.1205  15
   6   6  -8 546.388 70.7823  29
   6  -6  -7 1804.16 128.695  22
  -6   6   7 1831.05 132.043  10
   6  -6  -7 1950.71 125.019  16
   6   6  -7 1923.23 127.232  30
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   6  -6  -6 107.620 40.3489  22
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   6   7   3 2771.87 160.300  20
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   6   7   6 512.895 69.9596   8
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   6   7   7 37.9194 24.9563   8
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   6   7   9 677.054 59.1494   8
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   6   8  -7 117.343 25.7989  30
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   6   8  -1 12278.9 333.557  20
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   6   8   0 18925.4 409.882  20
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   6   8   0 19368.8 420.556  12
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   6   8   1 4400.18 200.409  12
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   6   8   4 10363.0 287.296  20
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   6   8   5 1130.36 94.0059  20
   6  -8   5 1136.39 96.7410   9
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   6   8   6 5771.12 198.018  20
   6  -8   6 5940.05 203.229   9
   6   8   6 6103.66 201.147   8
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   6   8   7 21799.2 348.667  20
   6  -8   7 22447.9 355.718   9
   6   8   7 22596.9 347.850   8
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   6  -8   8 3427.99 115.074   9
   6   8   8 3614.84 118.334   8
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   6   9  -7 18.4061 10.8836  20
   6  -9  -6 684.427 50.9140  22
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   6   9  -6 629.445 53.7192  20
   6   9  -6 584.306 45.2039  12
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   6   9  -5 1866.32 103.346  20
   6   9  -5 2084.19 102.020  12
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   6   9  -4 2381.88 123.853  20
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   6   9  -3 5482.08 187.681  12
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   6   9  -1 5926.39 203.801  12
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   6   9   4 76.6440 34.2591  20
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   6  -9   4 43.2219 34.2702   9
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   6  -9   5 18945.5 329.896  18
   6   9   5 19895.5 300.407   8
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   6   9   6 1777.81 87.4043  20
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   6   9   6 1868.31 79.0051   8
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   6 -10  -4 1004.43 51.4468  22
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   6 -10  -2 1751.52 69.3447  16
   6  10  -1 611.736 53.9132  20
   6 -10  -1 622.020 48.1413  16
   6  10   0 12.2723 12.9070  20
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   6 -10   1 163.587 31.4316  18
   6  10   2 1088.48 70.1998  20
   6 -10   2 1083.50 70.6057  18
   6  10   3 11795.5 212.345  20
   6 -10   3 11581.4 209.338  18
   6  10   4 189.955 26.7624  20
   6 -10   4 172.052 24.4071  18
   7   0 -12 876.635 61.8616  19
   7   0 -12 966.724 69.7303  29
   7   0 -11 30.2317 19.2817  19
   7   0 -11-0.28366 16.4862  29
   7   0 -10 6513.74 240.323  22
   7   0 -10 7394.38 229.652  19
   7   0  -9-0.98000 20.9003  22
   7   0  -9 12.1349 19.8639  19
   7   0  -9 15.6354 28.0594  15
   7   0  -8 29192.5 528.059  22
   7   0  -8 34362.8 509.147  19
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   7   0  -8 28973.0 532.716  15
   7   0  -7 10.4976 17.7870  22
   7   0  -7 23.8062 27.3699  15
   7   0  -6 3696.00 329.341   1
   7   0  -6 4161.27 192.551  15
   7   0  -5 65.9926 49.7887   6
   7   0  -5 169.920 72.5816   1
   7   0  -4 24748.7 852.120   6
   7   0  -4 22062.5 776.523   1
   7   0  -3 27.2840 37.1849   6
   7   0  -3-11.6687 26.3162   1
   7   0  -2 25042.1 766.686   7
   7   0  -2 25816.3 740.205   1
   7   0  -2 25276.5 786.023   6
   7   0  -1 122.857 57.7669   6
   7   0  -1 32.5335 39.5844   1
   7   0  -1 144.384 63.0453   7
   7   0   0 2697.10 230.468   1
   7   0   0 2339.91 243.625   7
   7   0   1 34.0938 31.1509   1
   7   0   1 44.7803 43.2929   7
   7   0   2 72307.7 1212.96   1
  -7   0  -3 57.1085 40.9173   2
  -7   0  -4 148852. 2042.63   2
  -7   0  -5 116.053 64.5634   2
   7   0   6 4739.68 214.872  21
  -7   0  -6 4899.02 395.791   2
   7   0   6 4933.16 229.078  28
   7   0   7-1.47484 18.8672  28
   7   0   7 88.4959 33.4114  13
   7   0   8 18447.2 468.653  28
   7   0   8 18885.0 456.652  13
   7   0   9 9.88836 25.8925  28
   7   0   9 43.5277 26.7335  13
   7   0  10 69.1742 41.9284  28
   7   0  10 39.6631 28.5457  27
   7   0  10 69.0514 36.2451  13
   7   0  11 20.5912 21.5904  28
   7   0  11 20.2712 20.8479  27
   7   0  11 16.6243 23.5301  13
   7   0  12 5472.59 189.928  13
   7   0  12 5877.68 182.687  28
   7   0  12 5526.23 159.808  27
   7   0  13 1.74232 8.24594  13
   7   1 -12 655.279 56.8756  29
   7   1 -12 653.076 54.7765  19
   7  -1 -12 656.066 50.6395  19
   7  -1 -12 676.524 58.0219  29
   7   1 -11 671.541 69.0502  29
   7   1 -11 590.213 61.8594  19
   7  -1 -11 546.048 56.3509  19
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   7   1 -10 13923.6 341.183  29
   7   1 -10 14434.4 326.504  19
   7  -1 -10 14505.9 310.909  19
   7  -1 -10 14006.5 349.989  15
   7   1  -9 2497.35 153.367  22
   7  -1  -9 2496.48 154.788  22
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   7   1  -9 2489.72 153.546  29
   7   1  -9 2690.30 148.156  19
   7  -1  -9 2883.97 145.298  19
   7  -1  -9 2604.17 160.045  15
   7   1  -8 1524.73 120.989  22
   7  -1  -8 1820.77 131.506  22
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   7   1  -8 1802.21 120.487  19
   7   1  -8 1532.47 124.725  15
   7  -1  -8 1685.68 130.130  15
   7   1  -7 368.861 60.7751  22
   7  -1  -7 404.118 63.2662  22
   7   1  -7 429.999 57.9468  19
   7   1  -7 459.317 71.6047  15
   7  -1  -7 466.273 75.1335  15
   7   1  -6 971.614 101.633  22
   7  -1  -6 901.128 93.2411  22
   7  -1  -6 826.743 214.339   1
   7   1  -5 1717.43 250.516   6
   7  -1  -5 1783.45 253.009   1
   7  -1  -4 1032.30 165.687   6
   7   1  -4 799.323 168.395   6
   7  -1  -4 732.565 144.264   1
   7   1  -4 831.513 157.507   7
   7   1  -3 27764.9 883.777   6
   7  -1  -3 28444.5 859.736   1
   7   1  -3 28158.3 846.101   7
   7  -1  -3 28749.4 812.494   6
   7   1  -2 11734.3 553.171   6
   7  -1  -2 11408.6 525.302   1
   7  -1  -2 12508.6 507.554   7
   7   1  -2 11483.2 544.893   7
   7  -1  -2 11417.1 501.172   6
   7  -1  -1 2044.59 217.549   1
   7  -1  -1 2254.47 223.253   7
   7   1  -1 2101.72 237.767   7
   7   1  -1 1937.05 220.628   6
   7  -1   0 10311.5 480.929   1
   7   1   0 10108.2 517.203   7
   7  -1   1 833.594 138.644   1
   7   1   1 540.377 127.608   7
   7  -1   2 6031.08 375.448   1
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   7   1   2 5924.77 413.831   7
  -7   1  -3 3513.43 321.996   2
  -7  -1  -3 3713.19 307.986   2
  -7  -1  -3 3846.32 290.337   3
  -7   1  -4 6339.29 433.849   2
  -7  -1  -4 7366.81 432.689   2
  -7   1  -5 16016.2 720.365   2
  -7  -1  -5 16659.5 674.875   2
   7   1   6 25027.5 489.328  21
   7  -1   6 26551.9 528.446  28
  -7   1  -6 23979.2 903.420   2
   7  -1   6 27163.0 512.043  13
   7   1   7 6749.44 261.928  21
   7   1   7 7810.12 253.264   8
   7  -1   7 7159.96 284.776  28
   7  -1   7 7351.16 281.047  13
   7   1   7 7615.09 275.616  13
   7   1   8 1400.01 113.655  11
   7   1   8 1429.78 110.705   8
   7  -1   8 1316.86 125.198  28
   7  -1   8 1212.82 119.029  13
   7  -1   8 1339.95 116.788  27
   7   1   8 1367.11 121.304  13
   7  -1   9 20092.1 474.273  28
   7   1   9 21563.6 424.498   8
   7  -1   9 19588.9 474.538  13
   7  -1   9 21697.9 467.292  27
   7   1   9 20637.0 473.085  13
   7  -1  10 14545.3 379.708  28
   7   1  10 14992.9 333.636   8
   7   1  10 13840.4 392.475  28
   7  -1  10 14320.2 393.890  13
   7   1  10 14086.6 381.168  13
   7  -1  10 14922.1 372.654  27
   7  -1  11 745.132 84.3781  13
   7  -1  11 783.489 78.7635  28
   7   1  11 774.475 86.4967  28
   7   1  11 713.842 80.3154  13
   7  -1  11 793.448 79.6483  27
   7   1  11 817.904 73.1475  27
   7   1  12 46.5636 20.2239  28
   7  -1  12 27.0945 12.3356   9
   7  -1  12 65.4141 21.8769  27
   7  -1  12 3.39237 15.6760  13
   7   1  12 7.11836 15.8080  13
   7  -1  13 9007.81 170.227  13
   7   2 -12 160.664 28.8096  29
   7   2 -12 152.126 27.0897  19
   7  -2 -12 123.071 20.1764  19
   7  -2 -12 180.022 29.4260  29
   7  -2 -11 4957.60 187.705  22
   7   2 -11 5189.31 177.847  19
   7  -2 -11 5387.06 158.722  19
   7   2 -11 5277.38 187.485  29
   7  -2 -10 1113.79 98.1206  22
  -7   2  10 1218.95 100.144  10
   7   2 -10 1187.02 94.6756  19
   7  -2 -10 1320.71 89.0284  19
   7  -2 -10 1212.97 101.162  15
   7   2 -10 1200.60 99.3674  29
   7  -2  -9 1762.37 127.937  22
  -7   2   9 1902.83 131.455  10
   7   2  -9 1788.74 121.574  19
   7  -2  -9 1729.00 128.779  15
   7   2  -9 1783.72 129.150  29
   7  -2  -8 98.6426 35.9071  22
  -7   2   8 148.096 42.0946  10
   7   2  -8 103.315 33.3114  19
   7  -2  -8 101.633 26.6927  15
   7   2  -8 65.6091 29.9687  29
   7  -2  -7 1059.57 111.731  22
   7   2  -7 806.078 83.2436  19
   7   2  -7 930.243 97.2277  29
   7  -2  -6 1189.80 200.964   1
   7   2  -6 1007.55 91.1650  22
   7  -2  -6 1147.34 100.578  22
   7   2  -6 1095.18 90.3481  19
   7  -2  -6 1152.53 102.419  16
   7   2  -6 1218.13 104.201  15
   7   2  -6 1160.60 102.515  29
   7   2  -5 28926.0 977.106   6
   7  -2  -5 30362.5 995.112   1
   7   2  -5 29725.2 918.326   7
   7   2  -4 22578.7 844.093   6
   7  -2  -4 21472.3 823.092   1
   7   2  -4 22120.9 793.998   7
   7  -2  -3 16777.5 697.736   1
   7   2  -3 16599.4 704.179   6
   7   2  -3 16068.6 673.431   7
   7   2  -2 2781.88 285.503   6
   7   2  -2 3033.05 292.186   7
   7  -2  -2 3089.66 294.257   1
   7  -2  -1 17037.4 669.805   1
   7   2  -1 16287.5 677.415   7
   7   2  -1 15843.7 656.373   6
   7  -2   0 1358.51 189.797   1
   7   2   0 1266.49 190.473   7
   7  -2   1 51132.1 1159.29   1
   7   2   1 51552.9 1229.71   7
   7  -2   2 9721.61 507.041   1
   7   2   2 9970.66 549.453   7
  -7   2  -3 6063.07 425.328   2
  -7  -2  -3 7034.80 397.872   3
   7   2   3 7195.34 480.238   7
   7  -2   3 7089.81 447.940   1
  -7   2  -4 21398.1 828.623   2
  -7  -2  -4 22152.5 763.616   3
  -7  -2  -5 852.292 158.257   3
  -7   2  -5 1934.22 259.115   2
   7   2   6 887.230 93.1959  11
   7   2   6 825.332 90.5638  21
  -7  -2  -6 769.182 161.293   3
   7   2   6 928.117 89.8385   8
   7  -2   6 903.534 97.3566  13
  -7   2  -6 743.442 161.400   2
   7  -2   6 993.492 102.590  28
   7   2   7 69478.7 811.251  11
   7  -2   7 68638.8 870.775  28
   7   2   7 65757.0 807.837  21
   7   2   7 68928.0 782.568   8
   7  -2   7 66347.1 865.100  13
   7  -2   7 72619.7 858.003  27
   7   2   7 71198.4 823.607  13
   7  -2   8 942.752 103.360  28
   7   2   8 1108.16 99.3758  11
   7   2   8 929.699 94.0646   8
   7  -2   8 891.858 103.648  13
   7  -2   8 944.742 101.210  27
   7   2   8 909.369 98.1525  13
   7   2   9 1304.92 109.026   8
   7  -2   9 1356.12 118.045  28
   7  -2   9 1221.00 119.680  13
   7  -2   9 1294.42 116.291  27
   7   2   9 1371.21 120.009  13
   7  -2  10 1214.72 114.233  13
   7   2  10 1253.47 99.7890   8
   7  -2  10 1413.34 109.593  28
   7   2  10 1196.89 115.764  28
   7  -2  10 1369.38 114.380  27
   7   2  10 1243.85 109.768  13
   7   2  11 20116.0 420.104  28
   7  -2  11 21052.4 424.266  13
   7  -2  11 21254.6 401.714  27
   7   2  11 20642.3 399.681  13
   7  -2  12 1960.51 91.9296   9
   7  -2  12 1969.08 109.795  13
   7   2  12 1987.10 102.696  13
   7  -2  12 1926.52 97.3223  27
   7   2  12 2002.11 109.098  28
   7   3 -12 49.4743 14.3627  29
   7  -3 -12 69.0402 16.8057  29
   7   3 -12 52.7589 13.7743  30
   7  -3 -11 31.8987 17.9883  22
  -7   3  11 53.8663 21.8241  10
   7   3 -11 27.6418 19.2220  19
   7   3 -11 75.7576 24.5815  29
   7  -3 -10 18.5051 18.0987  22
  -7   3  10 63.9375 26.8129  10
   7   3 -10 18.9683 17.2179  19
   7  -3 -10 39.8282 22.5261  15
   7   3 -10 75.7305 32.0220  29
   7  -3  -9 34.6279 33.2502  22
  -7   3   9 27.0365 24.4865  10
   7   3  -9 40.9791 27.1439  19
   7  -3  -9 23.5311 29.9628  15
   7   3  -9 34.0899 28.0915  29
   7  -3  -8 28.9081 26.7745  22
   7   3  -8 74.5585 36.8208  29
  -7   3   8 138.297 40.9953  10
   7   3  -8 51.3491 24.5026  19
   7  -3  -8 29.3971 29.9922  15
   7  -3  -7 43773.0 651.753  22
   7   3  -7 44321.5 615.607  19
   7   3  -7 43872.0 650.931  29
   7  -3  -6 305.443 54.7704  22
   7   3  -6 326.193 58.3266  29
   7   3  -6 349.673 55.8473  19
   7  -3  -6 432.104 65.4497  16
   7   3  -6 221.880 86.8958   7
   7   3  -5 19494.5 813.294   6
   7  -3  -5 19538.0 415.988  22
   7   3  -5 18719.7 373.545  19
   7  -3  -5 18638.6 405.586  16
   7  -3  -5 19798.9 826.362   1
   7   3  -5 19211.1 783.695   7
   7   3  -5 19279.7 409.096  29
   7   3  -4 8315.96 532.901   6
   7   3  -4 9337.98 548.229   7
   7  -3  -4 8172.05 522.417   1
   7   3  -3 1304.61 202.869   6
   7  -3  -3 1621.57 227.831   1
   7   3  -3 1452.75 218.001   7
   7   3  -2 17768.5 744.603   7
   7  -3  -2 18022.6 742.978   1
   7   3  -2 17819.6 723.075   6
   7  -3  -1 3498.70 323.533   1
   7   3  -1 3322.72 323.518   7
   7   3  -1 3307.84 308.231   6
   7   3   0 577.806 136.095   7
   7  -3   0 563.724 130.808   1
   7  -3   1 17525.6 720.883   1
   7   3   1 17449.0 743.444   7
   7  -3   2 11926.3 596.069   1
  -7   3  -2 10548.7 572.499   2
   7   3   2 12142.4 627.389   7
  -7   3  -3 3780.70 348.212   2
   7  -3   3 3971.55 352.537   1
   7   3   3 4308.08 376.701   7
  -7  -3  -3 4472.02 336.365   3
   7   3   4 73422.8 1558.49   7
  -7  -3  -4 75308.8 1452.16   3
   7   3   5 24301.6 482.927  11
   7   3   5 23480.7 464.707  21
   7   3   5 24399.4 441.384  17
  -7   3  -5 23516.5 910.461   2
  -7  -3  -5 23612.5 860.204   3
   7  -3   5 24867.3 496.512  28
   7  -3   5 23984.9 498.820  13
   7  -3   5 25471.0 489.863  27
   7   3   6 206.635 47.8745  11
   7   3   6 257.068 53.9582  21
   7  -3   6 246.537 52.1798  28
   7  -3   6 306.014 56.5555  27
   7  -3   6 180.703 43.5697  13
   7   3   7 3679.91 185.715  11
   7   3   7 3412.17 184.115  21
   7   3   7 3276.68 179.131   8
   7  -3   7 3036.57 189.888  13
   7  -3   7 3639.81 194.708  28
   7  -3   7 3360.69 192.025  27
   7   3   8 5865.68 229.978  21
   7   3   8 5447.00 227.583   8
   7  -3   8 6085.53 242.165  28
   7  -3   8 5253.77 248.321  13
   7  -3   8 5536.49 246.765  27
   7   3   8 6138.23 244.205  13
   7   3   9 14179.5 357.421   8
   7  -3   9 14377.2 401.460  13
   7  -3   9 14846.1 394.454  27
   7   3   9 15266.8 378.153  13
   7   3  10 603.762 68.8943   8
   7  -3  10 662.263 82.7501  13
   7   3  10 676.887 84.3475  28
   7  -3  10 679.043 80.1041  27
   7   3  10 628.383 73.5184  13
   7  -3  11 91.1210 28.7148   9
   7   3  11 92.9963 27.2391   8
   7   3  11 110.255 32.3435  28
   7  -3  11 110.121 31.6109  27
   7  -3  11 139.375 36.3150  13
   7   3  11 78.9667 25.7498  13
   7  -3  12 1445.20 74.9215   9
   7  -3  12 1554.16 89.7476  13
   7   3  12 1528.68 86.5831  28
   7   3  12 1410.62 72.6909  13
   7   4 -12 516.985 38.6961  12
   7  -4 -11 1996.02 100.727  22
  -7   4  11 1969.40 94.5127  10
   7   4 -11 1876.21 84.2448  30
   7   4 -11 2049.37 101.369  29
   7  -4 -10 10439.1 269.726  22
  -7   4  10 10717.8 264.522  10
   7  -4 -10 10568.3 254.874  15
   7   4 -10 11411.1 252.302  30
   7   4 -10 10587.7 272.786  29
   7  -4  -9 10664.3 300.817  22
  -7   4   9 11788.0 307.299  10
   7   4  -9 10971.0 293.258  19
   7  -4  -9 11299.2 300.398  15
   7   4  -9 10884.3 304.465  29
   7  -4  -8 1991.17 138.025  22
  -7   4   8 2137.45 139.232  10
   7   4  -8 1875.62 128.213  19
   7  -4  -8 2011.70 137.706  15
   7   4  -8 1824.95 134.402  29
   7  -4  -7 3070.23 174.050  22
  -7   4   7 3602.35 182.351  10
   7   4  -7 3074.69 175.229  29
   7   4  -7 2997.62 163.946  19
   7  -4  -7 3020.77 169.337  16
   7  -4  -6 6322.21 249.761  22
   7   4  -6 6272.48 234.696  19
   7   4  -6 6404.40 251.380  29
   7  -4  -6 6333.68 246.092  16
   7  -4  -5 42727.7 626.705  16
   7   4  -5 43159.7 637.560  29
   7   4  -4 9674.98 574.593   6
   7   4  -4 9626.16 579.769   7
   7  -4  -4 9226.42 301.070  18
   7  -4  -4 9375.61 292.940  16
   7   4  -4 9289.82 288.288  29
   7  -4  -4 9561.02 579.779   1
   7   4  -3 24310.0 884.277   6
   7  -4  -3 23973.9 480.465   9
   7   4  -3 24203.8 911.739   7
   7  -4  -3 25169.2 924.647   1
   7  -4  -2 11652.8 626.533   1
   7   4  -2 10887.2 579.810   6
   7   4  -2 11365.8 620.465   7
   7  -4  -1 7214.26 486.572   1
   7   4  -1 6888.03 479.519   7
   7   4  -1 6892.11 453.680   6
   7  -4   0 20594.5 822.364   1
   7   4   0 19799.8 808.100   7
   7   4   1 5195.08 417.006   7
  -7   4  -1 4801.69 389.331   2
   7  -4   1 4948.12 398.749   1
   7  -4   2 38499.9 1122.27   1
  -7   4  -2 37326.7 1092.81   2
   7   4   2 40770.1 1166.57   7
   7   4   3 25613.8 469.932  24
   7   4   3 26598.3 502.361  11
   7  -4   3 25247.9 498.920   9
   7   4   3 25328.3 455.956  17
  -7   4  -3 24384.0 911.874   2
   7   4   3 27147.9 955.455   7
  -7  -4  -3 26312.4 828.279   3
   7  -4   3 26775.8 950.451   1
   7   4   3 26171.5 476.487  12
   7   4   4 22788.4 440.495  24
   7   4   4 22895.7 472.786  11
   7   4   4 22616.3 459.719  21
   7  -4   4 22128.5 477.527   9
   7   4   4 22191.4 435.083  17
  -7   4  -4 23138.9 901.266   2
   7   4   4 23788.3 889.577   7
  -7  -4  -4 23755.9 830.495   3
   7  -4   4 22940.6 496.805  13
   7  -4   4 22972.9 480.698  27
   7   4   5 23035.3 483.771  11
   7   4   5 22273.4 462.127  21
   7  -4   5 21164.6 481.239   9
   7  -4   5 21804.5 499.013  13
   7  -4   5 21885.0 485.910  27
   7   4   6 11872.3 337.254  11
   7   4   6 10999.4 322.647  21
   7  -4   6 10457.3 341.036   9
   7  -4   6 10768.4 356.361  13
   7  -4   6 11324.9 355.926  27
   7   4   7 2804.84 158.054  11
   7   4   7 2567.82 152.369  21
   7   4   7 2292.25 150.058   8
   7  -4   7 2296.97 166.242  13
   7  -4   7 2334.08 163.557  27
   7   4   8 2529.69 154.583   8
   7  -4   8 2584.49 173.830  13
   7  -4   8 2714.20 173.584  27
   7   4   8 3015.66 160.684  13
   7  -4   9 2842.62 167.075   9
   7   4   9 2719.13 152.729   8
   7  -4   9 2684.75 170.211  13
   7  -4   9 2847.97 169.570  27
   7   4   9 3077.84 157.034  13
   7  -4  10 4168.26 184.261   9
   7   4  10 3922.84 166.373   8
   7  -4  10 3944.04 188.143  13
   7   4  10 4044.81 184.488  28
   7  -4  10 4127.21 185.578  27
   7   4  10 4171.90 165.799  13
   7  -4  11 2896.39 130.064   9
   7   4  11 2672.71 114.639   8
   7  -4  11 2700.54 133.971  13
   7   4  11 2581.69 125.352  28
   7   4  11 2598.25 107.226  13
  -7   4 -11 2450.43 89.6434  26
   7   4  12 15.8384 9.53787  28
   7   5 -11 4.90814 12.2979  12
  -7   5  11 22.3591 9.51204  10
   7  -5 -11 31.3157 12.9387  22
   7  -5 -10 226.960 37.9210  22
   7   5 -10 223.236 31.4041  30
  -7   5  10 216.408 34.5549  10
   7  -5 -10 195.325 29.6902  15
   7   5 -10 218.858 38.1810  29
   7  -5  -9 204.499 42.5597  22
  -7   5   9 195.934 38.0140  10
   7   5  -9 221.426 42.1729  29
   7  -5  -9 217.276 39.0105  15
   7   5  -9 222.328 38.2344  30
   7  -5  -8 1545.00 118.184  22
  -7   5   8 1762.69 120.030  10
   7  -5  -8 1655.04 119.025  15
   7   5  -8 1463.45 116.441  29
   7  -5  -7 19378.7 427.862  22
   7  -5  -7 20087.8 423.849  16
   7   5  -7 19160.1 432.107  29
   7  -5  -6 6462.15 261.002  22
   7  -5  -6 6795.56 253.950  16
   7   5  -6 6217.28 252.605  29
   7   5  -5 2834.11 161.692  17
   7  -5  -5 2541.88 153.983  16
   7   5  -5 2621.31 161.725  29
   7  -5  -4 1259.12 127.291  18
   7  -5  -4 1277.32 114.831  16
   7   5  -4 1234.46 113.086  29
   7   5  -3 270.924 53.1475  12
   7   5  -3 128.799 36.2762  24
   7   5  -3 49.2257 50.7839   6
   7  -5  -3 165.902 45.8599  18
   7   5  -3 181.820 45.8813  17
   7   5  -3 144.700 38.7678  29
   7   5  -2 28027.9 521.708  12
   7   5  -2 28042.3 499.142  24
   7  -5  -2 29454.2 1014.24   1
   7  -5  -2 27362.2 528.919   9
   7  -5  -2 28675.4 529.896  18
   7   5  -2 28602.8 514.435  17
   7   5  -2 27841.1 478.525  29
   7   5  -2 28111.7 996.495   7
   7   5  -2 29117.1 952.760   6
   7   5  -1 102.409 29.8560  12
   7  -5  -1 70.9749 60.3277   1
   7   5  -1 84.4062 32.2905  24
   7  -5  -1 131.225 39.0634  18
   7  -5  -1 63.8523 30.1753   9
   7   5  -1 123.299 35.5552  17
   7   5  -1 205.232 88.0593   7
   7   5   0 532.488 70.7288  24
   7  -5   0 605.125 143.953   1
   7  -5   0 531.615 72.1342   9
  -7   5   0 441.375 121.545   2
   7   5   0 508.279 68.6149  17
   7   5   0 657.702 152.363   7
   7   5   0 499.825 67.0709  12
   7   5   1 49.6956 28.0859  12
   7   5   1 34.5423 30.4626  24
   7  -5   1 41.5215 27.3894   9
   7   5   1 24.8959 24.4227  17
   7  -5   1 78.6297 52.9418   1
  -7   5  -1 11.5509 31.7539   2
   7   5   1 39.0483 46.1598   7
   7   5   2 9476.33 302.447  24
   7  -5   2 10278.1 601.790   1
   7  -5   2 9066.29 308.761   9
   7   5   2 9069.15 287.190  17
  -7   5  -2 8588.47 543.431   2
   7   5   2 10169.9 588.759   7
   7   5   2 9408.54 296.142  12
   7   5   3 157.922 42.3065  12
   7  -5   3 176.246 46.7968   9
   7   5   3 199.615 43.5042  17
   7   5   3 91.9030 63.7192   7
   7   5   4 12550.2 345.423  21
   7  -5   4 12733.8 371.848   9
   7   5   4 11927.0 336.091  17
   7   5   5 256.524 57.2582  21
   7   5   5 224.475 48.4605  20
   7  -5   5 272.995 64.6229   9
   7  -5   5 186.149 54.0698  13
   7  -5   6 29081.4 596.019  13
   7   5   6 30543.2 513.561  21
   7   5   6 32407.9 527.102  20
   7  -5   6 27720.1 556.128   9
   7   5   6 33020.4 563.279  28
   7   5   7 31972.9 517.126  20
   7  -5   7 28582.6 556.091   9
   7   5   7 28259.1 515.170   8
   7  -5   7 28577.5 582.608  13
   7   5   7 30686.1 544.320  28
  -7   5  -7 31185.3 471.953  26
   7  -5   8 13851.0 372.194   9
   7   5   8 13155.0 336.458   8
   7  -5   8 13819.7 387.593  13
   7   5   8 14229.0 358.983  28
  -7   5  -8 14753.7 313.056  26
   7  -5   9 2218.25 138.730   9
   7   5   9 2168.58 128.210   8
   7   5   9 2235.75 133.220  28
   7  -5   9 2109.00 141.972  13
  -7   5  -9 2257.82 111.571  26
   7  -5  10 415.058 54.2072   9
   7   5  10 483.005 54.2907   8
   7   5  10 464.846 54.5198  28
  -7   5 -10 453.164 42.5665  26
   7   5  11 84.7687 19.7282   8
   7   5  11 114.891 20.2934  28
   7   6 -10 1591.46 84.4459  12
  -7   6  10 1609.50 65.9794  10
   7   6  -9 25.5112 22.8027  12
   7  -6  -9 17.4697 19.6501  22
  -7   6   9 31.8875 17.8813  10
   7  -6  -9 30.9123 16.2222  15
   7   6  -8 3291.67 164.624  12
   7  -6  -8 3377.98 157.734  22
  -7   6   8 3614.15 152.832  10
   7  -6  -8 3563.58 149.546  15
   7   6  -8 3387.96 161.636  29
   7   6  -7 800.943 87.7570  12
   7  -6  -7 711.737 78.1345  22
  -7   6   7 875.547 82.7477  10
   7  -6  -7 790.483 78.0347  16
   7   6  -7 788.380 85.5906  29
   7   6  -6 6617.10 258.566  12
   7  -6  -6 6586.09 247.627  22
  -7   6   6 7382.55 244.824  10
   7  -6  -6 6681.44 237.962  16
   7   6  -6 6455.91 251.248  29
   7   6  -5 178.900 58.6988  12
   7   6  -5 197.926 53.6731  17
   7  -6  -5 331.744 71.1833  16
   7   6  -5 190.380 62.3460  29
   7   6  -4 360.866 62.2796  12
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   7   6   8 189.759 41.3156   8
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   7   7   0 5083.20 222.649  12
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   7  -7   1 18078.4 435.371   9
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   7   7   1 18205.7 417.591  12
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   7   7   4 55.9782 31.7651  21
   7   7   4 51.9697 25.3548  20
   7   7   5 16873.2 360.234  20
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   7   7   6 5139.50 190.339  20
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   7   7   6 4976.84 199.052   8
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   7  -7   8 4133.20 156.716   9
   7   7   8 4090.21 149.016   8
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   7  -7   9 480.512 44.3492   9
   7   7   9 482.100 42.7758   8
   7   8  -8 56.9494 14.2437  12
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   7  -8  -6 1836.88 102.595  22
   7   8  -6 1710.70 102.146  12
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   7   8  -1 1348.06 103.257  20
   7  -8  -1 1343.01 114.236  18
   7   8  -1 1399.53 112.432  12
   7   8   0 52.5203 26.1051  12
   7   8   0 37.1454 20.4630  20
   7  -8   0 34.7433 26.0789   9
   7  -8   0 12.1092 23.0211  18
   7   8   1 6322.47 220.288  20
   7  -8   1 6556.70 242.289   9
   7  -8   1 6270.52 242.989  18
   7   8   1 6575.11 236.914  12
   7   8   2 3101.61 152.149  20
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   7  -8   2 2972.36 166.133  18
   7   8   3 1562.06 107.886  21
   7   8   3 1259.24 97.0844  20
   7  -8   3 1353.96 113.513   9
   7   8   4 5132.56 185.377  20
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   7   8   5 1709.72 101.707  20
   7  -8   5 1706.59 112.971   9
   7   8   5 1745.60 112.173   8
   7   8   6 3405.54 130.370  20
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   7   8   6 3414.58 137.669   8
   7  -8   7 6001.34 162.414   9
   7   8   7 6158.71 162.041   8
   7   8   8 2627.83 81.3404   8
   7  -9  -6 167.459 22.7568  22
   7  -9  -5 1251.21 70.5298  22
   7   9  -5 1091.49 63.3731  12
   7  -9  -4 1613.66 91.5215  22
   7   9  -4 1465.20 80.3346  20
   7  -9  -4 1419.28 72.3396  16
   7   9  -4 1610.77 87.6158  12
   7  -9  -3 5837.55 166.846  16
   7   9  -3 5550.94 175.853  12
   7   9  -2 73.5369 25.5041  12
   7   9  -2 15.9268 13.7156  20
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   7   9  -1 9405.32 230.945  20
   7  -9  -1 9133.45 250.362  18
   7   9  -1 9594.71 243.416  12
   7   9   0 6000.54 185.022  20
   7  -9   0 5844.59 201.926  18
   7   9   1 3765.27 145.950  20
   7  -9   1 3700.82 161.875  18
   7   9   2 180.953 28.5172  21
   7   9   2 234.009 37.8117  20
   7  -9   2 185.266 37.7363  18
   7   9   3 10550.8 228.669  20
   7  -9   3 11070.8 241.194   9
   7  -9   3 10633.1 255.964  18
   7   9   4 1938.56 92.0604  20
   7  -9   4 2005.64 95.2293   9
   7  -9   4 1970.72 103.989  18
   7   9   4 2021.60 96.6143   8
   7   9   5 2134.83 85.2049  20
   7  -9   5 2136.31 84.1402   9
   7  -9   5 2376.39 102.994  18
   7   9   5 2300.41 90.3063   8
   7  -9   6 8694.96 163.036  18
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   7 -10   0 7350.06 143.992  16
   7  10   1 866.418 48.5329  20
   7 -10   1 802.745 49.4663  16
   7 -10   2 2838.47 91.6113  18
   8   0 -12 1048.13 62.7291  29
   8   0 -11 13.3133 11.8986  19
   8   0 -11-10.1433 18.2860  29
   8   0 -10 41489.1 472.542  19
   8   0 -10 38267.5 538.869  29
   8   0  -9 52.5989 31.7684  22
   8   0  -9 76.7273 32.2628  15
   8   0  -8 4593.05 205.858  22
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   8   0  -7 15.0236 18.7737  22
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   8   0  -6 10721.4 300.663  22
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   8   0  -5 34.6011 19.6106  22
   8   0  -5 19.1092 19.5123  15
   8   0  -4 4684.07 379.448   6
   8   0  -4 4918.16 364.893   1
   8   0  -3 0.31570 24.4304   6
   8   0  -3-27.7387 34.3667   1
   8   0  -2 41315.1 989.178   1
   8   0  -2 39622.4 1049.33   7
   8   0  -2 38384.6 1037.23   6
   8   0  -1 42.9598 38.0445   1
   8   0  -1-19.4668 32.3709   7
   8   0   0 68314.5 1226.92   1
   8   0   0 61785.1 1341.10   7
   8   0   1-16.8454 28.9593   1
   8   0   1 93.4373 59.3505   7
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   8   0   5-13.4134 23.3170  21
   8   0   5-6.82224 25.6943  28
   8   0   6 16970.4 424.159  21
   8   0   6 17821.8 455.477  28
   8   0   7 3.24429 19.2224  28
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   8   0   8 10102.8 325.720  13
   8   0   9-4.86602 17.5665  11
   8   0   9 2.16030 24.7845  28
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   8   0  10 68254.2 808.951  28
   8   0  10 69668.8 791.012  13
   8   0  10 73048.1 704.296  25
   8   0  11 64.5913 28.2590  28
   8   0  11 13.1394 19.3524  13
   8   0  12 10108.2 202.403  13
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   8   1  -9 244.767 43.3696  19
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   8   1  -9 175.970 44.4697  29
   8   1  -8 12126.8 330.786  22
   8  -1  -8 12441.9 338.530  22
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   8   1  -7 39202.7 590.388  22
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   8   1  -7 39849.5 619.910  15
   8  -1  -7 40849.0 638.210  15
   8   1  -6 359.811 57.9403  22
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   8   1  -5 1044.11 186.610   6
   8  -1  -5 435.083 76.4251  22
   8  -1  -5 1138.92 189.207   1
   8  -1  -5 490.751 77.8635  16
   8   1  -5 1076.85 108.670  15
   8   1  -4 36640.3 1089.89   6
   8  -1  -4 37992.6 1072.38   1
   8   1  -3 2644.98 282.032   7
   8  -1  -3 2315.96 267.070   1
   8  -1  -3 2645.17 264.460   6
   8   1  -3 2364.24 274.451   6
   8  -1  -2 4269.41 343.378   1
   8   1  -2 4256.79 357.576   7
   8   1  -2 4226.70 360.167   6
   8  -1  -1 1247.61 182.700   1
   8   1  -1 1256.72 199.859   7
   8  -1   0 12080.6 563.665   1
   8   1   0 11515.5 600.299   7
   8   1   1 4180.03 367.545   7
   8  -1   1 4089.70 325.672   1
   8  -1   2 6283.07 409.141   1
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   8   1   2 6452.52 463.677   7
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   8   1   4 3325.64 178.477  21
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   8   1   5 11979.6 344.241  11
   8  -1   5 11389.0 340.555  21
   8   1   5 11772.2 342.546  21
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   8   1   5 11971.4 360.294  28
   8   1   6 1454.68 121.955  11
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   8  -1   6 1669.07 139.852  28
   8   1   6 1615.61 138.898  28
   8  -1   6 1747.28 132.077  13
   8   1   7 1706.81 134.490  11
   8   1   7 1734.36 141.978  21
   8  -1   7 1808.39 153.035  28
   8   1   7 1611.28 146.776  28
   8  -1   7 1728.48 137.457  13
   8   1   8 355.246 60.0880  11
   8   1   8 465.650 80.8936  28
   8  -1   8 417.407 69.4518  13
   8   1   8 407.888 65.7084  13
   8  -1   8 401.505 72.3292  28
   8  -1   8 454.874 66.3492  25
   8  -1   9 329.944 63.7694  28
   8   1   9 351.949 66.8640  28
   8   1   9 479.694 70.4644  13
   8  -1   9 297.609 60.1348  13
   8  -1  10 14715.7 304.555  11
   8  -1  10 14520.1 356.542  28
   8   1  10 13708.9 366.107  28
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   8  -1  11 10731.0 253.550  28
   8   1  11 9955.74 271.217  28
   8  -1  11 10146.1 265.022  13
   8   1  11 10258.2 254.529  13
   8   1  11 10297.6 221.434  25
   8  -1  12 4823.48 141.810  13
   8   1  12 4933.86 142.759  28
   8   2 -12 608.742 43.4936  29
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   8   2 -11 94.2798 25.6214  29
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   8   2 -10 1112.71 81.2049  19
   8  -2 -10 951.451 85.0992  15
   8   2 -10 1069.93 89.3861  29
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   8  -2  -9 6998.78 249.969  15
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   8  -2  -8 47.8367 25.7401  22
   8   2  -8 90.4991 26.3579  19
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   8   2  -7 4360.41 204.812  29
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   8   2  -6 23239.6 463.623  15
   8   2  -6 23980.6 469.343  29
   8   2  -5 19381.3 823.282   6
   8  -2  -5 19632.1 409.418  22
   8  -2  -5 19452.9 421.761  16
   8   2  -5 18691.4 399.730  15
   8  -2  -5 18223.5 793.914   1
   8   2  -5 19820.6 414.244  29
   8   2  -4 15884.1 737.427   6
   8   2  -4 16865.7 366.975  24
   8  -2  -4 15628.9 351.923  22
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   8   2  -4 16667.6 362.243  14
   8  -2  -4 14559.0 698.185   1
   8   2  -4 16261.4 356.795  29
   8   2  -4 15407.7 694.031   7
   8   2  -3 10842.6 589.304   7
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   8   2  -3 11740.0 620.974   6
   8  -2  -2 40106.2 1111.15   1
   8   2  -2 39212.0 1125.71   7
   8   2  -2 40462.9 1130.00   6
   8  -2  -1 6617.78 451.106   1
   8   2  -1 6640.12 465.512   7
   8  -2   0 2701.13 289.957   1
   8   2   0 2698.69 302.749   7
   8   2   1 7488.51 505.399   7
   8  -2   1 7579.03 478.972   1
   8  -2   2 11855.6 598.290   1
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   8   2   2 12351.6 657.826   7
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   8   2   3 2435.28 289.235   7
   8   2   4 8056.14 248.696  24
   8   2   4 6690.15 258.377  11
   8   2   4 6805.68 256.994  21
   8  -2   4 7295.49 253.138   9
   8   2   4 7716.68 237.157  17
   8  -2   4 7161.09 261.296  25
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   8  -2   4 6896.27 272.796  28
   8   2   4 7212.33 270.551  28
   8   2   5 4093.58 206.260  11
   8   2   5 3942.56 204.366  21
   8  -2   5 4229.62 199.460   9
   8  -2   5 4167.78 219.215  28
   8  -2   5 4406.78 208.561  25
   8  -2   5 4246.60 206.241  13
   8   2   5 4894.51 233.025  28
   8   2   6 24211.0 499.330  11
   8   2   6 24035.4 501.305  21
   8  -2   6 25949.8 502.660   9
   8   2   6 26983.5 482.147   8
   8  -2   6 24429.1 534.063  28
   8  -2   6 25125.5 515.188  13
   8   2   6 24428.2 531.468  28
   8  -2   6 26023.6 495.451  25
   8   2   7 46140.8 672.662  11
   8   2   7 44722.6 683.755  21
   8  -2   7 46024.4 721.529  28
   8  -2   7 45885.4 710.566  13
   8   2   8 4831.13 206.534  11
   8   2   8 5041.01 206.914   8
   8  -2   8 4703.39 226.326  28
   8  -2   8 4668.97 226.778  13
   8   2   8 4503.05 231.708  28
   8   2   8 5225.72 219.269  13
   8  -2   9 191.900 44.5803   9
   8   2   9 178.268 41.7323   8
   8  -2   9 168.510 45.3686  28
   8   2   9 234.881 57.0267  28
   8  -2   9 180.221 42.7037  27
   8  -2   9 186.807 49.8206  13
   8   2   9 192.628 46.2369  13
   8  -2  10 1560.75 104.864   9
   8   2  10 1505.79 94.9471   8
   8  -2  10 1527.54 117.179  13
   8   2  10 1447.76 117.076  28
   8  -2  10 1623.93 106.897  27
   8   2  10 1525.21 106.333  13
   8  -2  11 73.7763 23.3358   9
   8   2  11 57.6400 24.9591  28
   8  -2  11 53.1614 20.9941  27
   8  -2  11 68.4657 25.3941  13
   8   2  11 54.9292 17.1058  13
   8   2  12 199.780 28.6711  28
   8  -2  12 199.452 28.0676  13
   8  -3 -11 1844.35 95.4298  22
   8   3 -11 2027.03 98.4376  29
   8  -3 -10 692.157 69.2492  22
   8  -3 -10 693.220 69.5990  15
   8   3 -10 682.225 68.5423  29
   8  -3  -9 2153.07 132.957  22
   8   3  -9 2203.20 122.647  19
   8  -3  -9 2205.40 135.622  15
   8   3  -9 2199.25 135.470  29
   8  -3  -8 152.353 46.0409  22
   8   3  -8 180.463 39.5434  19
   8  -3  -8 177.208 45.8707  15
   8   3  -8 162.458 44.2267  29
   8   3  -7 41096.7 626.165  29
   8  -3  -7 39565.6 615.638  22
   8  -3  -6 9775.08 305.175  22
   8   3  -6 10486.2 285.320  19
   8  -3  -6 9312.20 301.374  16
   8   3  -6 9781.78 304.083  29
   8  -3  -5 20395.5 434.727  22
   8  -3  -5 20210.8 436.865  16
   8   3  -5 19708.6 423.595  29
   8   3  -4 36193.6 1119.00   6
   8   3  -4 38108.1 559.748  24
   8  -3  -4 35068.2 551.469  22
   8   3  -4 35905.5 549.972  29
   8  -3  -4 34416.9 552.792  16
   8   3  -4 35968.6 551.617  14
   8   3  -4 35476.0 1093.31   7
   8  -3  -4 36090.4 1129.54   1
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   8  -3  -3 12305.4 322.029  18
   8  -3  -3 11611.6 317.334  16
   8   3  -3 11992.4 324.140  14
   8   3  -3 11949.8 641.563   7
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   8   3  -3 11348.7 621.961   6
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   8   3   1 34141.0 1109.12   7
   8  -3   1 34260.9 1059.71   1
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   8   3   2 2287.40 148.871  11
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   8   3   3 22475.4 440.157  24
   8   3   3 22365.1 473.672  11
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   8   3   3 22537.6 425.808  17
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   8   3   3 23469.9 445.376  14
   8   3   3 23247.1 925.700   7
   8   3   3 24821.9 480.080  28
   8  -3   3 23657.0 472.707  25
   8   3   4 13908.5 342.047  24
   8   3   4 11851.2 355.784  11
   8   3   4 11442.0 342.838  21
   8  -3   4 11538.3 339.931   9
   8   3   4 12985.4 330.017  17
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   8  -3   4 11951.7 349.709  13
   8   3   4 12896.5 361.502  28
   8  -3   4 13023.2 349.403  25
   8   3   5 28454.6 544.686  11
   8   3   5 28523.5 538.425  21
   8   3   5 29827.7 501.198  17
   8  -3   5 29061.0 547.089   9
   8  -3   5 29402.9 557.994  13
   8   3   5 30010.2 568.266  28
   8  -3   6 5734.41 253.176  13
   8   3   6 5869.24 245.151  11
   8   3   6 5674.13 243.617  21
   8  -3   6 5900.78 249.752   9
   8   3   6 5864.22 233.281   8
   8   3   6 5844.28 257.431  28
   8   3   7 5231.55 222.948  11
   8   3   7 4887.85 221.736  21
   8  -3   7 5099.37 232.041   9
   8   3   7 5144.95 217.556   8
   8  -3   7 4975.42 239.183  13
   8   3   7 5202.16 246.635  28
   8  -3   7 5669.21 237.491  27
   8  -3   8 481.028 74.4294  13
   8   3   8 572.153 69.5148  11
   8  -3   8 624.984 79.8756   9
   8   3   8 534.464 67.6445   8
   8   3   8 612.795 85.4647  28
   8  -3   8 568.163 74.3984  27
   8  -3   9 5871.39 226.901   9
   8   3   9 5712.59 208.037   8
   8   3   9 5663.88 237.426  28
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   8   3   9 6250.60 213.294  13
   8  -3   9 5680.08 236.946  13
   8  -3  10 2517.04 132.199   9
   8   3  10 2520.63 121.961   8
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   8   3  10 2488.96 142.605  28
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   8   3  10 2704.11 124.882  13
   8  -3  11 108.842 19.2762  11
   8  -3  11 138.410 26.6072   9
   8   3  11 144.938 32.8833  28
   8  -3  11 171.263 34.3193  13
   8   3  11 120.718 21.7612  13
   8   4 -11 876.323 57.0640  29
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   8  -4 -10 50.2215 22.3299  22
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   8   4 -10 22.9170 21.0279  29
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   8  -4  -8 2593.79 149.536  22
   8   4  -8 2989.19 147.328  17
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   8   4  -6 9095.14 295.744  29
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   8   4  -5 3356.15 184.474  29
   8   4  -4 104.358 35.3309  12
   8   4  -4 63.9573 26.0020  24
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   8  -4  -3 1000.48 101.161  18
   8   4  -3 1033.52 103.339  17
   8  -4  -3 942.216 96.6133  16
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   8  -4  -2 5846.40 242.566   9
   8  -4  -2 6278.12 240.097  18
   8   4  -2 5891.86 237.677  17
   8   4  -2 6091.83 240.597  12
   8   4  -2 5619.54 230.515  14
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   8  -4  -1 6607.19 488.439   1
   8  -4  -1 6169.20 233.703  18
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   8   4  -1 5994.04 468.648   7
   8   4  -1 6081.61 235.333  12
   8   4   0 1989.42 137.578  24
   8  -4   0 2027.06 139.836   9
   8  -4   0 1954.00 130.564  18
   8   4   0 1914.54 131.768  17
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   8   4   0 1857.81 133.755  14
   8   4   0 1888.96 264.530   7
   8   4   0 2015.11 134.197  12
   8   4   1 11803.4 335.389  24
   8  -4   1 12007.6 342.114   9
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   8   4   1 11523.2 316.379  17
   8   4   1 11480.9 329.361  14
   8   4   1 12264.6 677.825   7
   8  -4   1 12465.0 657.626   1
   8   4   1 12120.3 328.008  12
   8   4   2 3122.12 171.663  24
   8   4   2 3287.27 182.575  11
   8  -4   2 3416.42 344.024   1
   8  -4   2 2870.90 171.499   9
   8   4   2 3035.22 164.626  17
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   8   4   2 3146.47 170.195  14
   8   4   2 3535.02 359.738   7
   8   4   2 3210.11 171.891  12
   8   4   3 2370.40 150.248  24
   8   4   3 2461.04 161.393  11
   8   4   3 2401.28 156.570  21
   8  -4   3 2390.73 157.699   9
   8   4   3 2432.29 147.768  17
   8   4   3 2520.14 148.645  14
   8   4   3 2499.01 153.408  12
   8   4   4 466.093 69.4950  24
   8   4   4 309.397 58.5889  11
   8   4   4 226.214 47.2656  21
   8  -4   4 351.223 61.0453   9
   8   4   4 331.812 56.0007  17
   8  -4   4 314.185 59.7768  13
   8   4   5 32387.9 580.543  11
   8   4   5 31661.0 564.533  21
   8  -4   5 31683.6 583.352   9
   8  -4   5 33198.5 617.290  13
   8   4   6 5946.14 242.766  11
   8   4   6 5857.69 237.731  21
   8  -4   6 5772.73 250.406   9
   8  -4   6 5633.87 255.987  13
   8   4   6 6207.20 255.857  28
   8   4   7 8773.01 278.112  21
   8  -4   7 8654.56 300.004   9
   8   4   7 8469.89 277.272   8
   8  -4   7 8379.99 307.077  13
   8   4   7 8820.56 302.990  28
   8  -4   8 155.387 39.7688   9
   8   4   8 173.383 37.7399   8
   8   4   8 170.994 46.5423  28
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   8  -4   9 2994.45 155.357   9
   8   4   9 2933.27 143.742   8
   8  -4   9 2991.28 165.433  13
   8   4   9 3025.97 159.313  28
   8  -4  10 1882.24 106.884   9
   8   4  10 1776.87 96.1516   8
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   8   4  10 1691.49 104.408  28
   8  -4  11 2649.03 93.6437   9
   8   4  11 2643.68 99.9367  28
   8   5 -10 1566.28 83.6325  12
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   8  -5  -8-1.71646 15.6524  15
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   8   5  -7 1816.15 112.889  17
   8   5  -7 1590.72 119.980  29
   8   5  -6 545.505 76.5222  12
   8  -5  -6 495.676 71.1277  22
   8   5  -6 554.284 70.5102  17
   8  -5  -6 543.001 75.4213  16
   8   5  -6 545.335 74.3186  29
   8   5  -5 23.3202 20.6835  12
   8  -5  -5 10.9744 21.6197  22
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   8   5  -4 1573.92 143.857  17
   8  -5  -4 2169.32 151.007  16
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   8   5  -3 923.487 99.8321  12
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   8   5  -2 3061.58 171.657  24
   8  -5  -2 2906.48 176.857   9
   8  -5  -2 2947.92 174.687  18
   8   5  -2 2946.29 172.731  17
   8   5  -2 2849.30 170.016  12
   8   5  -1 18354.4 427.053  24
   8  -5  -1 18946.2 447.403   9
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   8   5  -1 18504.0 423.552  17
   8   5  -1 18621.4 427.877  12
   8   5   0 50709.2 716.946  24
   8  -5   0 52451.9 741.759   9
   8   5   0 51133.7 693.681  17
   8   5   0 52902.6 712.342  12
   8   5   1 9164.17 306.181  24
   8  -5   1 9176.81 310.882   9
   8   5   1 8738.45 289.322  17
   8   5   1 9180.47 297.639  12
   8   5   2 4176.17 206.990  24
   8  -5   2 4455.60 218.990   9
   8   5   2 4242.56 201.779  17
   8   5   2 4269.64 203.960  12
   8   5   3 1141.26 109.671  21
   8  -5   3 1114.86 111.876   9
   8   5   3 1137.17 105.257  17
   8   5   4 17442.6 413.249  21
   8  -5   4 17342.6 431.973   9
   8   5   4 16923.5 399.555  17
   8   5   5 228.517 47.0152  21
   8  -5   5 220.878 49.9212   9
   8   5   6 2184.59 136.927  21
   8  -5   6 2209.63 152.289   9
   8   5   7 4079.06 172.658  21
   8  -5   7 3948.20 194.291   9
   8   5   7 3788.91 179.952   8
   8   5   7 4163.87 185.813  28
   8  -5   8 780.007 82.6202   9
   8   5   8 770.151 76.5208   8
   8   5   8 810.470 77.9875  28
   8  -5   9 587.795 65.0781   9
   8   5   9 593.685 60.3255   8
   8   5   9 662.482 63.3342  28
   8  -5  10 284.678 37.5493   9
   8   5  10 285.673 34.6701   8
   8   5  10 244.941 30.8688  28
   8   6  -9 811.634 61.6775  12
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   8   6  -8 58.2441 28.3825  12
   8  -6  -8 53.9446 24.3085  22
   8  -6  -8 68.0097 25.1372  15
   8   6  -7 1107.35 93.9549  12
   8  -6  -7 1149.00 93.0569  22
   8   6  -6 1697.03 127.495  12
   8  -6  -6 1745.50 127.865  22
   8  -6  -6 1890.76 125.822  16
   8   6  -5 1771.05 133.611  12
   8  -6  -5 1905.10 132.955  22
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   8  -6  -5 1765.66 126.011  16
   8   6  -4 20263.1 447.527  12
   8  -6  -4 19537.1 420.000  16
   8  -6  -3 13355.9 370.538  18
   8   6  -3 14050.2 354.792  17
   8  -6  -3 12855.0 344.841  16
   8   6  -3 13543.3 367.951  12
   8  -6  -2 24140.3 498.581  18
   8   6  -2 23904.6 489.474  12
   8  -6  -1 4570.82 224.430   9
   8  -6  -1 4716.01 222.754  18
   8   6  -1 4568.78 209.699  17
   8   6  -1 4390.95 213.192  12
   8  -6   0 5658.20 245.546   9
   8  -6   0 5860.95 244.442  18
   8   6   0 5875.14 235.955  17
   8   6   0 5501.86 232.645  12
   8  -6   1 27137.2 538.965   9
   8  -6   1 28242.0 532.373  18
   8   6   1 27131.3 509.576  17
   8   6   1 27243.6 514.703  12
   8  -6   2 3627.75 203.141   9
   8   6   2 3830.62 192.952  17
   8   6   2 3807.39 193.538  12
   8   6   3 4784.97 217.819  21
   8  -6   3 4217.03 215.178   9
   8   6   3 4849.28 215.866  17
   8   6   4 2015.72 143.073  21
   8  -6   4 1131.17 127.720   9
   8   6   5 2968.77 154.327  21
   8  -6   5 2733.51 164.539   9
   8  -6   6 10886.6 315.695   9
   8   6   6 10297.1 291.903   8
   8  -6   7 74.8281 29.8627   9
   8   6   7 95.9757 32.6593   8
   8  -6   8 12400.0 287.588   9
   8   6   8 12317.9 269.115   8
   8  -6   9 516.311 50.8083   9
   8   6   9 488.493 46.6978   8
   8  -7  -8 362.034 37.5192  22
   8   7  -8 299.759 36.8376  12
   8  -7  -7 3366.26 134.564  22
   8  -7  -7 3388.63 123.508  15
   8   7  -7 3088.96 134.497  12
   8  -7  -6 6202.65 201.532  22
   8  -7  -6 6008.69 189.477  16
   8   7  -6 6090.24 206.597  12
   8  -7  -5 5441.21 203.629  22
   8  -7  -5 5475.20 195.548  16
   8   7  -5 5425.11 209.020  12
   8   7  -4 2693.17 130.630  17
   8  -7  -4 2542.39 141.201  16
   8   7  -4 2466.17 147.906  12
   8   7  -3 345.644 50.1071  20
   8   7  -3 293.817 46.9035  17
   8  -7  -3 299.385 51.5631  16
   8   7  -3 353.860 58.6348  12
   8   7  -2 227.219 45.6658  20
   8  -7  -2 367.470 67.4503  18
   8   7  -2 380.179 67.3029  17
   8   7  -2 262.485 62.4514  12
   8  -7  -1 21280.0 455.753  18
   8   7  -1 22447.3 435.584  17
   8   7  -1 20876.6 439.477  12
   8   7   0 2420.30 131.884  20
   8  -7   0 2311.03 152.377   9
   8  -7   0 2154.33 145.085  18
   8   7   0 2266.22 141.951  17
   8   7   0 2068.22 137.583  12
   8  -7   1 12603.8 354.154   9
   8  -7   1 13045.9 353.164  18
   8   7   1 13680.7 347.642  17
   8   7   1 12902.6 341.870  12
   8   7   2 2621.83 135.775  20
   8  -7   2 2335.93 151.360   9
   8  -7   2 2423.30 151.810  18
   8   7   3 83.7106 32.7643  21
   8   7   3 32.6821 23.7811  20
   8  -7   3 30.3398 26.9347   9
   8   7   4 2067.43 121.510  21
   8   7   4 2073.79 116.419  20
   8  -7   4 1927.01 133.463   9
   8   7   5 4700.89 163.656  21
   8   7   5 4472.12 160.194  20
   8   7   6 532.631 51.6490  20
   8  -7   6 552.296 67.1113   9
   8   7   6 576.838 66.6305   8
   8  -7   7 474.479 54.7833   9
   8   7   7 431.364 49.1883   8
   8  -7   8-3.47678 12.1019   9
   8   7   8 0.76189 12.5640   8
   8  -8  -7 1495.00 62.9559  22
   8   8  -7 1014.53 53.2032  12
   8   8  -6 148.834 32.3201  12
   8  -8  -6 150.100 32.4749  22
   8  -8  -5 5370.90 169.134  22
   8  -8  -5 5367.08 155.868  16
   8   8  -5 5238.22 170.271  12
   8  -8  -4 938.155 82.4510  22
   8   8  -4 524.202 49.0341  20
   8  -8  -4 890.602 77.1199  16
   8   8  -4 601.588 76.6336  12
   8   8  -3 112.456 38.9910  12
   8   8  -3 104.329 27.4272  20
   8  -8  -3 113.481 35.8772  16
   8   8  -2 744.859 65.9699  20
   8  -8  -2 748.472 78.0883  18
   8  -8  -2 753.403 75.0752  16
   8   8  -2 740.093 79.3514  12
   8   8  -1 1007.55 78.1389  20
   8  -8  -1 1143.58 97.4839  18
   8   8  -1 990.032 92.4412  12
   8   8   0 10451.5 246.582  20
   8  -8   0 9896.60 283.957  18
   8   8   0 9550.45 270.740  12
   8   8   1 5434.72 177.879  20
   8  -8   1 5404.40 207.768   9
   8  -8   1 5054.81 201.528  18
   8   8   2 1727.55 106.388  21
   8   8   2 1666.72 96.2712  20
   8  -8   2 1666.70 114.200   9
   8  -8   2 1606.99 112.101  18
   8   8   3 1182.91 81.4531  21
   8   8   3 1235.20 80.1247  20
   8  -8   3 1186.09 93.8571   9
   8  -8   3 1174.43 93.2444  18
   8   8   4 5370.96 155.540  20
   8  -8   4 5049.71 180.980   9
   8  -8   4 5044.72 181.660  18
   8   8   5 749.139 52.4817  20
   8  -8   5 751.478 70.2676   9
   8  -8   5 828.320 69.7846  18
   8   8   5 886.619 72.7624   8
   8  -8   6 10504.8 212.517   9
   8  -8   6 10741.6 214.433  18
   8   8   6 10459.0 206.383   8
   8   8   7 523.241 37.9699   8
   8  -9  -4 3517.93 111.510  22
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   8   9   3 3003.10 108.077   8
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   8   9   4 22596.1 259.234   8
   9   0 -11 11.0848 12.6908  29
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   9   0   9 6.27620 27.4925  28
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   9   0  11-4.67122 10.6328  13
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   9   1  -3 26050.0 906.726   7
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   9   1   0 19263.7 818.669   7
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   9   1   0 18438.4 428.047  25
   9   1   1 6707.13 245.055  11
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   9  -1   5 829.533 82.8151  14
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   9   1   6 17449.8 425.194  11
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   9   1   6 17599.6 460.789  28
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   9   1   7 5260.97 229.649  11
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   9  -2   1 23450.2 865.815   1
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   9   2   1 22937.5 480.748  25
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   9   2   2 4541.04 212.945  21
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   9   2   2 4752.09 194.384  17
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   9   2   3 211.231 50.8514  11
   9   2   3 178.755 42.1912  21
   9   2   3 157.306 35.1867  17
   9   2   3 149.422 39.1937  14
   9   2   3 168.572 49.6875  28
   9  -2   4 30.7300 28.3343  25
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   9   2   4 40.6647 28.5147  11
   9   2   4 57.4395 33.7619  21
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   9   2   4 72.0946 22.7958  14
   9   2   4 93.4948 36.9736  28
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   9   2   5 6520.03 279.147  28
   9  -2   5 6085.67 254.549  25
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   9  -2   6 96.4070 38.3705   9
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   9   2   8 13796.4 330.683  11
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   9   2   9 13362.5 274.700  11
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   9   2  11 63.3576 20.3081  28
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   9  -3  -1 6635.05 249.781   9
   9   3  -1 6355.79 244.784  17
   9   3  -1 6266.65 250.852  14
   9   3  -1 7163.38 249.255  12
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   9   3   0 1379.14 112.994  17
   9   3   0 1387.59 117.624  14
   9   3   0 1616.98 117.669  12
   9   3   0 1508.64 120.006  25
   9   3   1 33654.9 571.215  24
   9   3   1 33360.7 580.301  11
   9  -3   1 36190.2 575.356   9
   9   3   1 34225.3 553.780  17
   9   3   1 34045.5 577.426  14
   9  -3   1 34283.0 607.973  25
   9   3   1 35649.5 596.078  25
   9   3   2 1571.55 124.440  24
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   9  -3   2 1271.54 112.406   9
   9   3   2 1412.41 110.911  17
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   9   3   2 1463.51 113.582  12
   9  -3   2 1430.96 125.212  25
   9   3   3 3253.79 172.369  24
   9   3   3 3000.42 178.632  11
   9   3   3 3095.24 179.682  21
   9  -3   3 3078.07 171.317   9
   9   3   3 3074.71 161.760  17
   9   3   3 3228.01 172.670  14
   9   3   3 3526.22 187.178  28
   9  -3   3 3058.54 178.711  25
   9   3   4 5352.42 218.535  24
   9   3   4 5005.76 231.577  11
   9   3   4 4899.90 229.895  21
   9  -3   4 4808.02 218.049   9
   9   3   4 5367.02 214.335  17
   9   3   4 5961.05 222.424  14
   9   3   4 5529.20 244.083  28
   9  -3   4 5165.12 227.998  25
   9  -3   5 188.674 48.7943  25
   9   3   5 156.119 48.2091  11
   9   3   5 266.262 60.5914  21
   9  -3   5 166.576 44.6934   9
   9   3   5 288.009 60.0289  28
   9  -3   5 190.712 44.7830  13
   9   3   6 1213.05 111.424  11
   9   3   6 1300.09 116.836  21
   9  -3   6 1308.03 112.571   9
   9   3   6 1434.56 111.576   8
   9  -3   6 1350.71 118.762  13
   9   3   6 1370.54 123.165  28
   9   3   7 298.324 53.4585  11
   9   3   7 339.288 59.4452  21
   9  -3   7 303.439 57.8897   9
   9   3   7 341.749 54.9478   8
   9  -3   7 410.442 66.2242  13
   9   3   7 314.028 64.1666  28
   9   3   8 1931.69 116.235  11
   9  -3   8 2030.97 127.020   9
   9   3   8 1967.05 117.946   8
   9  -3   8 1863.79 131.795  13
   9   3   8 1769.09 131.281  28
   9  -3   9 12098.8 273.159   9
   9   3   9 12133.1 255.357   8
   9  -3   9 11846.4 302.526  13
   9   3   9 11288.9 303.455  28
   9  -3  10 917.364 63.8930  11
   9  -3  10 915.947 59.9664   9
   9   3  10 887.579 74.2158  28
   9  -4 -10 471.166 44.6158  22
   9   4 -10 450.207 44.1931  29
   9   4  -9 2249.19 110.094  12
   9  -4  -9 2771.96 126.619  22
   9   4  -9 2191.71 91.8994  17
   9  -4  -9 2749.25 125.935  15
   9   4  -9 2947.53 131.397  29
   9   4  -8 3112.14 148.412  12
   9  -4  -8 3195.72 150.429  22
   9   4  -8 3266.02 141.693  17
   9  -4  -8 3491.56 161.548  15
   9   4  -8 3354.32 156.529  29
   9   4  -7 367.351 56.6690  12
   9  -4  -7 393.664 59.5922  22
   9   4  -7 426.464 59.4633  17
   9  -4  -7 387.573 60.2144  15
   9   4  -7 403.936 60.2453  29
   9   4  -6 2082.97 138.161  12
   9  -4  -6 1877.87 128.419  22
   9   4  -6 2080.66 137.305  17
   9  -4  -6 1917.85 134.523  16
   9   4  -6 1947.00 130.271  29
   9   4  -5 7068.67 261.424  12
   9  -4  -5 6581.63 245.166  22
   9   4  -5 6614.71 253.265  17
   9  -4  -5 6534.72 250.000  16
   9   4  -5 6602.51 241.201  29
   9   4  -4 24615.7 488.249  12
   9   4  -4 24995.4 458.658  24
   9  -4  -4 22038.8 444.808  22
   9   4  -4 23130.0 477.193  17
   9  -4  -4 22075.1 455.410  16
   9   4  -4 23735.1 446.504  29
   9   4  -3 17949.2 408.953  24
   9   4  -3 16617.6 414.478  17
   9  -4  -3 16311.7 391.284  16
   9   4  -3 16676.1 401.819  14
   9   4  -3 17940.4 417.473  12
   9   4  -2 33175.5 569.197  24
   9  -4  -2 34873.9 562.465  18
   9   4  -2 32035.4 566.000  17
   9  -4  -2 31058.2 533.122  16
   9   4  -2 31195.5 556.905  14
   9   4  -2 34934.3 575.871  12
   9   4  -1 15570.1 396.851  24
   9  -4  -1 15956.4 403.853   9
   9   4  -1 14892.8 385.954  17
   9   4  -1 15199.3 395.156  14
   9   4  -1 16458.4 391.225  12
   9   4   0 8696.49 298.595  24
   9  -4   0 9159.84 302.476   9
   9   4   0 8738.13 289.251  17
   9   4   0 8690.05 297.902  14
   9   4   0 9480.28 296.262  12
   9   4   1 3830.42 197.444  24
   9  -4   1 3959.77 199.797   9
   9  -4   1 4609.73 198.716  18
   9   4   1 3874.15 189.446  17
   9   4   1 3922.08 198.688  14
   9   4   1 4079.84 193.277  12
   9   4   1 4408.98 203.645  25
   9   4   2 5383.23 232.511  24
   9   4   2 5332.12 241.533  21
   9  -4   2 4755.16 224.503   9
   9   4   2 5129.62 220.744  17
   9   4   2 5690.37 235.030  14
   9   4   2 5638.71 229.246  12
   9   4   3 23202.6 473.171  24
   9   4   3 23505.8 503.243  11
   9   4   3 23047.4 492.727  21
   9  -4   3 23365.1 486.733   9
   9   4   3 22771.2 453.960  17
   9   4   3 24746.2 474.112  14
   9   4   4 2152.42 156.390  11
   9   4   4 2279.62 162.236  21
   9   4   4 2451.77 152.394  17
   9   4   4 2424.87 142.499  14
   9   4   5 5499.70 238.137  11
   9   4   5 5533.46 235.670  21
   9  -4   5 5653.03 238.087   9
   9   4   6 2936.28 165.116  21
   9  -4   6 3082.20 173.177   9
   9   4   6 3143.78 163.437   8
   9   4   6 3160.55 175.065  28
   9   4   7 494.027 65.8464  21
   9  -4   7 506.293 68.4593   9
   9   4   7 507.285 64.1316   8
   9   4   7 445.085 64.5212  28
   9  -4   8 1927.25 120.457   9
   9   4   8 1941.91 113.481   8
   9   4   8 2000.67 125.862  28
   9  -4   9 5808.94 181.311   9
   9   4   9 5725.46 167.114   8
   9   4   9 5671.67 186.406  28
   9  -4  10 4879.86 127.898  11
   9  -4  10 4904.98 124.279   9
   9   4  10 4869.59 135.253  28
   9   4  10 5071.52 149.678  25
   9   5  -9 45.0604 18.4912  12
   9  -5  -9 32.4077 14.4318  22
   9  -5  -9 43.4415 17.2738  15
   9   5  -8 626.738 61.6602  12
   9  -5  -8 690.870 64.6015  22
   9  -5  -8 703.743 65.7880  15
   9   5  -8 744.847 68.5811  29
   9   5  -7 1901.15 119.029  12
   9  -5  -7 1815.78 114.588  22
   9   5  -7 1944.06 107.347  17
   9  -5  -7 1898.43 119.966  15
   9   5  -7 1950.47 118.815  29
   9   5  -6 558.515 72.0230  12
   9  -5  -6 475.708 63.6688  22
   9   5  -6 561.185 66.5366  17
   9  -5  -6 447.875 61.9514  16
   9   5  -6 529.515 65.1841  29
   9   5  -5 1632.48 124.047  12
   9  -5  -5 1722.94 122.494  22
   9   5  -5 1815.58 125.846  17
   9  -5  -5 1656.86 122.711  16
   9   5  -5 1620.90 117.359  29
   9  -5  -4 9328.03 290.903  22
   9   5  -4 9547.06 300.705  17
   9  -5  -4 9228.83 293.348  16
   9   5  -4 9419.99 281.320  29
   9   5  -4 9452.26 300.354  12
   9   5  -3 1310.61 115.894  24
   9   5  -3 1102.41 110.700  17
   9  -5  -3 1314.23 114.583  16
   9   5  -3 1114.55 102.970  29
   9   5  -3 1195.42 114.304  12
   9   5  -2 5861.12 237.912  24
   9  -5  -2 5872.24 238.232  18
   9   5  -2 5564.23 234.312  17
   9  -5  -2 5531.86 226.113  16
   9   5  -2 5569.06 233.584  12
   9   5  -1 407.297 65.7859  24
   9  -5  -1 395.931 61.2606  18
   9  -5  -1 323.880 61.4241   9
   9   5  -1 335.560 59.1783  17
   9   5  -1 378.310 62.7255  12
   9   5   0 6119.47 251.994  24
   9  -5   0 6224.49 254.790   9
   9  -5   0 6659.26 249.647  18
   9   5   0 5892.63 238.905  17
   9   5   0 6235.84 244.628  12
   9   5   1 478.881 72.3977  24
   9  -5   1 450.518 69.7898   9
   9  -5   1 471.854 67.4816  18
   9   5   1 525.079 73.1820  17
   9   5   1 508.042 70.5673  12
   9   5   2 9501.92 309.713  24
   9   5   2 9654.31 316.845  21
   9  -5   2 9563.58 314.428   9
   9   5   2 9457.57 296.157  17
   9   5   2 9821.93 304.455  12
   9   5   3 9048.39 300.729  21
   9  -5   3 9303.54 309.196   9
   9   5   3 8753.53 282.701  17
   9   5   4 15744.8 386.777  21
   9  -5   4 15403.2 390.912   9
   9   5   5 2384.57 145.254  21
   9  -5   5 2317.99 149.475   9
   9   5   6 285.038 49.9226  21
   9  -5   6 333.119 57.0230   9
   9   5   6 313.282 51.9410   8
   9   5   7 1366.56 93.3629  21
   9  -5   7 1325.76 101.889   9
   9   5   7 1295.41 95.0115   8
   9  -5   8 1234.54 89.2338   9
   9   5   8 1207.55 82.2032   8
   9   5   8 1280.75 78.5888  28
   9  -5   9 1781.95 88.3814   9
   9   5   9 1726.87 80.5356   8
   9  -6  -9 750.047 42.4399  22
   9  -6  -8 4828.99 141.454  22
   9  -6  -8 4658.52 130.485  15
   9  -6  -7 1309.36 86.9717  22
   9  -6  -7 1371.23 90.5873  15
   9   6  -7 1124.71 82.4959  12
   9   6  -6 44.6883 25.8369  12
   9  -6  -6 69.9706 27.7681  22
   9   6  -6 43.8112 23.6829  17
   9  -6  -5 432.542 59.3540  22
   9   6  -5 419.752 53.1774  17
   9  -6  -5 358.476 54.1573  16
   9   6  -5 391.956 59.1013  12
   9  -6  -4 18211.1 381.538  22
   9  -6  -4 18411.1 386.425  16
   9   6  -4 18791.8 401.700  12
   9   6  -3 4904.30 203.714  17
   9  -6  -3 4453.78 197.548  16
   9   6  -3 4692.92 208.042  12
   9  -6  -2 15409.2 377.199  18
   9   6  -2 16484.1 378.665  17
   9  -6  -2 15246.3 361.811  16
   9   6  -2 15749.4 378.897  12
   9  -6  -1 4951.58 215.368  18
   9   6  -1 4905.96 211.224  17
   9   6  -1 4772.94 210.253  12
   9   6   0 29.2242 23.2812  12
   9  -6   0 73.2401 27.0754  18
   9  -6   0 21.0652 23.0838   9
   9   6   0 29.8584 22.5689  17
   9  -6   1 1905.86 138.172   9
   9  -6   1 1867.49 131.130  18
   9   6   1 1863.11 129.480  17
   9   6   1 1830.77 130.313  12
   9   6   2 3124.52 174.127  21
   9  -6   2 3278.88 182.571   9
   9  -6   2 2944.88 163.125  18
   9   6   2 3336.05 174.078  17
   9   6   3 4128.97 192.455  21
   9  -6   3 3937.32 194.827   9
   9   6   4 2325.65 142.817  21
   9  -6   4 1361.10 119.094   9
   9   6   5 124.229 33.5970  21
   9  -6   5 138.685 38.6335   9
   9   6   6 2404.21 116.132  21
   9  -6   6 2139.23 126.187   9
   9   6   6 2261.84 123.333   8
   9  -6   7 13026.1 280.530   9
   9   6   7 12881.3 264.091   8
   9  -6   8 5008.22 149.418   9
   9   6   8 4945.11 139.683   8
   9   6   8 4754.61 140.033  25
   9  -7  -7 562.647 45.5992  22
   9  -7  -7 488.915 37.6017  15
   9   7  -7 412.359 40.4879  12
   9   7  -6 22.9517 18.4321  12
   9  -7  -6 20.7097 17.1649  22
   9   7  -5 111.690 29.5986  12
   9  -7  -5 112.895 27.5917  22
   9  -7  -5 152.193 32.9057  16
   9  -7  -4 304.474 51.5661  22
   9   7  -4 218.682 41.6772  17
   9  -7  -4 297.241 52.1047  16
   9   7  -4 223.875 48.2447  12
   9   7  -3 2865.25 133.828  17
   9  -7  -3 2564.79 135.118  16
   9   7  -3 2686.19 143.777  12
   9  -7  -2 11586.3 293.144  16
   9   7  -2 11729.0 304.293  12
   9  -7  -1 833.039 83.8378  18
   9   7  -1 704.050 75.7989  17
   9   7  -1 677.033 78.8060  12
   9  -7   0 614.746 71.8960  18
   9   7   0 752.794 77.4035  17
   9   7   0 638.608 73.3784  12
   9  -7   1 3347.74 171.741   9
   9  -7   1 3374.00 165.540  18
   9   7   1 3501.16 165.918  17
   9   7   2 2169.33 130.953  21
   9  -7   2 2023.27 134.621   9
   9  -7   2 1724.27 120.484  18
   9   7   3 1461.68 100.990  21
   9  -7   3 1367.00 106.255   9
   9  -7   3 1379.54 101.373  18
   9   7   4 2048.34 109.434  21
   9  -7   4 2071.33 123.008   9
   9  -7   4 2091.57 117.703  18
   9   7   5 5.05818 12.3141  21
   9  -7   5 27.7902 17.7248  18
   9  -7   5 5.38977 15.2802   9
   9   7   5-2.29242 15.6834   8
   9  -7   6 732.261 63.9309   9
   9  -7   6 818.442 60.2588  18
   9   7   6 766.179 61.3829   8
   9  -7   7 7123.34 163.602   9
   9   7   7 7286.09 157.664   8
   9  -8  -5 2230.63 87.4927  22
   9   8  -5 1968.33 85.2888  12
   9   8  -4 125.903 28.5775  12
   9  -8  -4 157.735 28.5590  22
   9  -8  -4 125.460 27.3672  16
   9  -8  -3 306.965 40.7280  22
   9  -8  -3 283.481 38.8543  16
   9   8  -3 338.971 44.8099  12
   9  -8  -2 1550.97 91.2064  16
   9   8  -2 1476.48 94.0199  12
   9  -8  -1 3221.84 134.467  16
   9   8  -1 3277.59 141.491  12
   9   8   0 53.6142 22.2249  21
   9  -8   0 19.1923 15.4103  18
   9   8   1 854.445 71.0145  21
   9  -8   1 826.029 72.5432  18
   9   8   2 625.086 58.2898  21
   9  -8   2 498.649 55.8298  18
   9   8   3 136.348 26.1554  21
   9  -8   3 158.290 32.0409  18
   9  -8   3 119.503 30.9034   9
   9  -8   4 433.314 46.7234   9
   9  -8   4 423.815 44.6019  18
   9   8   4 418.924 45.0043   8
   9  -8   5 3373.24 111.112   9
   9  -8   5 3426.46 104.957  18
   9   8   5 3540.21 109.709   8
   9   9  -2 117.314 19.8769  21
   9  -9  -2 143.500 22.2347  16
   9  -9  -1 1673.93 65.4254  22
   9   9  -1 1868.58 74.3158  21
   9  -9  -1 1917.19 73.5976  16
   9   9   0 14.0442 7.93320  21
   9  -9   0 16.1499 12.6164  16
   9  -9   1 672.088 43.9519  16
   9  -9   2 1367.41 57.2601  16
   9   9   2 1310.68 57.4632   8
  10   0 -10 5174.97 150.203  29
  10   0  -9 3.70582 14.2980  29
  10   0  -8 14540.7 331.477  15
  10   0  -8 14887.8 322.306  29
  10   0  -7 1.11796 14.2339  22
  10   0  -7 3.96283 20.7914  15
  10   0  -7 31.8322 23.1094  29
  10   0  -6 2754.76 155.820  15
  10   0  -6 2710.14 147.227  29
  10   0  -5 13.7586 19.7041  15
  10   0  -4 60157.3 716.189  15
  10   0  -4 68041.6 753.848  14
  10   0  -3-0.09564 20.4994  14
  10   0  -2 51701.7 694.152  14
  10   0  -1 23.3683 30.2913  14
  10   0  -1 25.7987 29.4535  25
  10   0   0 6744.32 241.189  11
  10   0   0 6012.53 242.167  14
  10   0   0 6456.94 269.340  25
  10   0   1 10.9559 20.0381  25
  10   0   1-0.30490 18.2717  11
  10   0   1 29.3576 22.3354  21
  10   0   1 33.7463 23.6278  14
  10   0   2 18445.3 404.171  24
  10   0   2 18150.6 421.809  11
  10   0   2 19129.6 433.915  21
  10   0   2 18254.4 421.584  14
  10   0   2 17331.1 445.937  25
  10   0   3 22.9566 31.4453  25
  10   0   3 7.81371 16.3595  24
  10   0   3-0.96319 20.3818  11
  10   0   3-53.3442 31.0419  21
  10   0   3 5.02891 17.6880  14
  10   0   4 18375.3 441.414  11
  10   0   4 19800.6 465.899  21
  10   0   4 18837.2 467.997  25
  10   0   5 19.6445 25.7415  25
  10   0   5 53.5004 33.6463  11
  10   0   5 117.056 52.0173  21
  10   0   5 55.2893 25.0843  14
  10   0   6 3048.83 174.756  11
  10   0   6 2973.95 186.733  28
  10   0   6 3145.89 184.519  25
  10   0   7 24.1341 26.3093  25
  10   0   7 20.2239 19.8208  11
  10   0   7 9.60867 21.8138  28
  10   0   8 12832.2 312.047  11
  10   0   8 13316.8 360.000  28
  10   0   8 13626.9 333.591  25
  10   0   9 25.3798 18.7409  25
  10   0   9-10.2591 14.0984  11
  10   0  10 3292.55 91.3679  11
  10   1 -10 1402.87 77.7627  29
  10  -1 -10 1379.57 76.8705  29
  10  -1  -9 5862.86 192.093  15
  10   1  -9 5777.04 184.342  29
  10  -1  -9 5891.26 183.593  29
  10  -1  -8 176.298 36.8586  22
  10  -1  -8 229.156 47.5162  15
  10   1  -8 130.967 33.6100  29
  10  -1  -7 1796.89 114.333  22
  10  -1  -7 1961.33 128.961  15
  10   1  -7 1800.94 119.323  29
  10   1  -6 6070.89 209.366  24
  10  -1  -6 6373.11 216.411  22
  10   1  -6 6032.49 224.253  15
  10  -1  -6 6120.21 234.132  15
  10   1  -6 6282.71 224.604  29
  10   1  -5 588.561 70.2958  24
  10   1  -5 579.875 70.3605  15
  10  -1  -5 572.275 74.9554  15
  10   1  -5 618.132 68.7029  14
  10   1  -5 627.786 71.8004  29
  10   1  -4 17832.7 393.266  14
  10  -1  -4 18317.1 388.700  14
  10   1  -3 3308.46 176.625  14
  10  -1  -3 3395.47 177.505  14
  10   1  -2 48659.6 677.056  14
  10  -1  -2 49604.9 682.519  14
  10   1  -1 3097.79 161.502  11
  10   1  -1 3023.78 164.492  17
  10   1  -1 2897.91 168.224  14
  10  -1  -1 2800.64 165.369  14
  10  -1  -1 2901.23 183.883  25
  10   1  -1 3016.44 185.214  25
  10   1   0 16105.1 392.158  24
  10   1   0 17510.6 398.937  11
  10   1   0 17601.4 397.623  21
  10   1   0 17929.1 391.689  17
  10   1   0 16397.2 398.933  14
  10  -1   0 16348.9 399.914  14
  10  -1   0 16573.9 435.874  25
  10   1   0 16920.3 431.642  25
  10   1   1 10740.4 318.371  24
  10   1   1 11034.6 326.691  11
  10  -1   1 11959.6 327.082  11
  10   1   1 11245.8 330.118  21
  10   1   1 10562.5 320.588  14
  10  -1   1 11039.8 328.433  14
  10  -1   1 10465.0 347.169  25
  10   1   1 11031.8 350.898  25
  10   1   2 13181.4 345.809  24
  10   1   2 12547.3 355.949  11
  10  -1   2 11455.8 335.217  11
  10  -1   2 13478.5 359.397  21
  10   1   2 12990.7 364.974  21
  10   1   2 12528.1 348.609  14
  10  -1   2 12527.7 351.671  14
  10  -1   2 12090.1 374.085  25
  10   1   2 12249.4 372.859  25
  10   1   3 8069.08 264.379  24
  10  -1   3 8245.11 254.826  24
  10   1   3 7451.14 277.910  11
  10  -1   3 7706.83 279.579  21
  10   1   3 7506.09 282.072  21
  10   1   3 7732.08 266.548  14
  10  -1   3 7575.80 267.599  14
  10  -1   3 7306.11 288.581  25
  10   1   3 7488.70 292.592  25
  10   1   4 9451.81 274.007  24
  10   1   4 7716.68 285.026  11
  10   1   4 8184.95 299.957  21
  10   1   4 9111.54 278.274  14
  10  -1   4 8872.79 280.364  14
  10   1   4 8706.33 320.561  28
  10  -1   4 8202.03 304.141  25
  10   1   4 7636.20 297.039  25
  10  -1   5 43.6039 33.1332  25
  10   1   5 33.6205 25.5284  25
  10   1   5 18.4217 20.7564  11
  10   1   5 50.1784 31.6079  21
  10  -1   5 47.0841 24.3594  14
  10   1   5 11.1062 20.4569  28
  10   1   6 2230.54 148.830  11
  10   1   6 2302.73 158.653  21
  10   1   6 2283.72 163.341  28
  10  -1   6 2272.17 152.884  25
  10   1   6 2161.09 155.477  25
  10   1   7 934.560 92.5182  11
  10  -1   7 1000.95 96.5095  11
  10   1   7 1121.97 113.785  28
  10  -1   7 874.982 89.3444  25
  10   1   7 985.103 101.142  25
  10   1   8 3498.45 159.741  11
  10  -1   8 3616.75 167.523  11
  10   1   8 3563.43 186.432  28
  10  -1   8 4038.16 168.396  25
  10   1   8 3605.12 177.223  25
  10   1   9 23.1329 15.8043  11
  10  -1   9 22.9854 19.1799  11
  10   1   9 47.6412 30.4696  28
  10  -1  10 1117.52 57.5761  11
  10   1  10 1086.08 60.9315  25
  10   2 -10 439.296 42.3693  29
  10  -2 -10 394.707 39.2659  29
  10  -2  -9 83.0219 23.6096  22
  10  -2  -9 58.5677 26.9438  15
  10   2  -9 99.1155 27.6475  29
  10  -2  -9 99.3188 26.2956  29
  10  -2  -8 12841.8 286.643  22
  10  -2  -8 13152.3 310.813  15
  10   2  -8 13037.3 293.742  29
  10  -2  -7 449.682 58.6637  22
  10  -2  -7 485.335 64.5791  15
  10   2  -7 519.825 64.7542  29
  10  -2  -6 5289.04 199.954  22
  10  -2  -6 5386.75 223.340  15
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  10  -8   0 63.5074 18.5893  16
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  11   5   5 2420.42 101.576   8
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  13   1  -2 446.399 48.8650  17
  13   1  -2 393.086 52.3716  14
  13  -1  -2 393.757 51.6929  14
  13   1  -1 32.7533 24.0495  24
  13  -1  -1 28.7119 18.9967  24
  13   1  -1 35.1412 19.2317  17
  13   1  -1 23.7978 19.9543  14
  13  -1  -1 31.3820 19.1389  14
  13   1   0 949.518 80.5935  24
  13  -1   0 908.070 77.8535  24
  13   1   0 896.311 79.3449  14
  13  -1   0 866.592 76.3007  14
  13   1   1 190.398 36.8663  24
  13  -1   1 152.940 32.5450  24
  13   1   1 125.943 33.8126  14
  13  -1   1 147.752 35.3005  14
  13   1   2 2729.60 123.400  24
  13  -1   2 2780.25 119.050  24
  13  -1   2 2920.30 120.001  11
  13   1   2 2739.49 129.025  14
  13  -1   2 2694.19 128.669  14
  13   1   2 2793.83 144.138  25
  13   1   3 3429.00 123.407  24
  13  -1   3 3539.29 134.800  11
  13   1   3 3327.51 130.406  14
  13  -1   3 3248.11 132.150  14
  13   1   3 3387.95 154.635  25
  13  -1   4 8584.52 204.898  11
  13   1   4 8441.65 173.863  14
  13  -1   4 8539.52 185.093  14
  13   1   4 8395.60 230.515  25
  13  -1   5 897.785 63.1385  11
  13   1   5 890.555 69.3687  25
  13  -1   6 589.868 44.4908  11
  13   1   6 599.911 48.5734  25
  13   2  -6 116.664 18.9138  17
  13  -2  -5 997.703 58.6760  24
  13   2  -5 282.368 34.6578  17
  13   2  -4 252.983 34.8472  24
  13  -2  -4 284.949 38.4791  24
  13   2  -4 171.243 32.7204  17
  13   2  -3 692.595 59.4069  24
  13  -2  -3 675.621 61.5849  24
  13   2  -3 683.254 58.2733  17
  13  -2  -3 724.380 56.1662  14
  13   2  -2 5926.08 184.158  24
  13  -2  -2 5829.19 183.215  24
  13   2  -2 5683.73 180.662  14
  13  -2  -2 5783.30 174.605  14
  13   2  -1 1295.32 89.5585  24
  13  -2  -1 1349.60 89.9353  24
  13   2  -1 1171.04 76.5054  17
  13   2  -1 1282.89 89.8359  14
  13  -2  -1 1295.18 87.7834  14
  13   2   0 9.52872 16.5748  24
  13  -2   0-11.6205 16.1127  24
  13   2   0 54.4055 26.2789  21
  13   2   0-9.18128 12.6256  17
  13   2   0 19.3316 19.4285  14
  13  -2   0 2.90399 17.5677  14
  13   2   1 458.004 53.9911  24
  13  -2   1 445.776 49.6024  24
  13   2   1 516.450 56.5422  21
  13   2   1 399.287 39.8070  17
  13   2   1 469.171 55.6864  14
  13  -2   1 452.817 55.4930  14
  13   2   2 5235.68 166.179  24
  13  -2   2 5212.71 148.902  24
  13   2   2 5335.33 175.774  21
  13   2   2 5146.36 169.132  14
  13  -2   2 5224.79 173.466  14
  13   2   2 5242.12 184.647  25
  13  -2   3 781.304 57.3595  11
  13   2   3 789.488 60.5773  14
  13  -2   3 831.401 65.1821  14
  13   2   3 778.946 70.4787  25
  13  -2   4 2697.91 104.918  11
  13  -2   4 2724.11 100.439  14
  13   2   4 2742.88 123.904  25
  13  -2   5 13734.5 218.717  11
  13   2   5 13596.4 249.983  25
  13   2   6 2293.04 84.8032  25
  13  -3  -5 104.968 17.5457  24
  13   3  -5 140.818 22.0220  17
  13  -3  -4 1655.02 79.6373  24
  13   3  -4 2095.75 88.9648  17
  13   3  -3 1303.20 73.6688  24
  13  -3  -3 1358.23 79.6622  24
  13   3  -3 1259.71 75.2586  17
  13  -3  -3 1192.61 63.3957  14
  13   3  -2 5435.67 163.683  24
  13  -3  -2 5428.69 165.272  24
  13   3  -2 5089.31 153.137  17
  13  -3  -2 5170.53 150.572  14
  13   3  -1 149.403 33.8350  24
  13  -3  -1 179.810 32.1197  24
  13   3  -1 126.549 27.1785  17
  13  -3  -1 150.600 31.0377  14
  13   3   0 758.667 65.8985  24
  13  -3   0 709.649 59.9881  24
  13   3   0 685.631 56.2979  21
  13   3   0 679.065 56.0648  17
  13  -3   0 716.675 62.4570  14
  13   3   1 180.805 35.1361  24
  13  -3   1 146.218 26.5334  24
  13   3   1 128.132 28.0815  21
  13   3   1 126.009 25.1288  17
  13  -3   1 141.043 30.6428  14
  13   3   2 16374.9 292.591  21
  13  -3   2 16964.6 291.550  14
  13   3   3 7686.28 196.264  21
  13  -3   3 7714.89 180.173  14
  13   3   3 7528.05 186.905  25
  13  -3   4 878.964 47.7677  11
  13  -3   4 1043.04 55.3729  14
  13   3   4 1079.48 67.3274  25
  13   3   5 80.2351 17.0875  25
  13  -4  -4 655.139 41.4573  24
  13   4  -4 374.511 33.6482  17
  13  -4  -3 708.467 49.9301  24
  13   4  -3 849.612 53.3321  17
  13  -4  -2 4.65838 11.5760  24
  13   4  -2 7.87762 11.2228  17
  13  -4  -2 9.76514 9.38882  14
  13  -4  -1 328.276 36.5846  24
  13   4  -1 343.657 37.9880  17
  13  -4  -1 346.127 38.4594  14
  13  -4   0 6.60660 9.79523  24
  13   4   0-27.6407 16.8703  21
  13   4   0-0.93673 11.2851  17
  13  -4   0 6.83858 13.7528  14
  13   4   1 773.462 57.6037  21
  13  -4   1 852.623 60.9481  14
  13   4   2 53.8696 20.5462  21
  13  -4   2 62.9864 18.8555  14
  13   4   3 332.913 41.8636  21
  13  -4   3 157.509 23.5169  14
  13  -5   0 2969.02 87.2248  14
  13  -5   1 592.303 39.9604  14
  14   0  -3 1.80481 8.70639  24
  14   0  -2 722.505 52.9248  24
  14   0  -2 642.283 47.2854  14
  14   0  -1 13.2656 13.0394  24
  14   0  -1 12.3988 13.3455  14
  14   0   0 3870.45 121.773  24
  14   0   0 4007.21 129.100  14
  14   0   1 2.54713 9.89710  24
  14   0   1 19.6898 13.8500  14
  14   0   2 3496.13 108.588  14
  14   1  -3 103.767 18.1074  24
  14  -1  -3 113.231 19.7752  24
  14   1  -2 1910.34 81.2404  24
  14  -1  -2 1980.41 83.6894  24
  14  -1  -2 2075.23 79.1687  14
  14   1  -1 924.817 59.8470  24
  14  -1  -1 875.962 57.4826  24
  14   1  -1 992.887 62.6814  14
  14  -1  -1 974.400 60.6007  14
  14   1   0 3516.82 115.082  24
  14  -1   0 3348.93 108.929  24
  14   1   0 3744.35 121.825  14
  14  -1   0 3677.31 121.206  14
  14   1   1 182.515 26.7973  24
  14  -1   1 147.805 22.1389  24
  14   1   1 235.085 32.5452  14
  14  -1   1 236.821 31.9552  14
  14   1   2 3234.50 100.307  14
  14  -1   2 3330.72 104.941  14
  14  -2  -3 27.3941 11.7640  24
  14   2  -2 639.746 43.2688  24
  14  -2  -2 611.539 42.9587  24
  14   2  -1 1559.48 72.0283  24
  14  -2  -1 1673.06 72.4691  14
  14   2   0 72.3019 19.5731  24
  14  -2   0 34.7883 11.6622  24
  14  -2   0 54.1210 17.3972  14
  14  -2   1 1291.49 66.4164  14
  14  -2   2 1367.40 62.2259  14
  14  -3   0-3.24774 9.29621  14
;
_shelx_hkl_checksum              6717
_shelx_res_file
;
TITL hijji131
    shelx.res
    created by SHELXL-2018/3 at 12:25:04 on 17-Aug-2018
CELL 1.54178  11.4519   9.2370  11.8727  90.0000  90.4750  90.0000
ZERR      4   0.0003   0.0003   0.0004    0.000    0.003    0.000
LATT  1
SYMM -x,1/2+y,1/2-z
SFAC C H N O
UNIT   52 64 8 16
temp -150
l.s. 15
acta
conf
bond $h
htab
EQIV $1 -x+1, -y+2, -z+1
HTAB N2 O3_$1
EQIV $2 -x+1, y-1/2, -z+3/2
HTAB C7 O4_$2
EQIV $3 -x+1, -y+1, -z+1
HTAB C9 O1_$3
HTAB C12 O2_$2
HTAB C13 O2
HTAB C13 O2_$2
omit    -1   2   1
omit    -6   0   2
omit     4   5   2
omit    -3   3   1
omit     2   2   1
omit     6   3   2
omit    -2   3   6
omit    -7   2   7
omit    -6   5   1
omit    -4   1   1
omit    -5   2   2
omit    11   2   1
omit     1   5   1
omit    -5   4   1
omit    -6   2   3
omit    -4   4   9
omit     6   2   2
omit    -9   3   1
omit     1   2   2
omit     2   3   9
omit    -2   3   3
omit     9   4   2
twin 1 0 0 0 -1 0 0 0 -1
WGHT    0.117900    1.124400
BASF   0.04425
FVAR       7.50302
O1    4    0.669601    0.430900    0.564016    11.00000    0.02976    0.01994 =
         0.03743   -0.00427   -0.00505   -0.00112
O2    4    0.671114    0.849856    0.766062    11.00000    0.03055    0.02004 =
         0.04073   -0.00590   -0.00277    0.00012
O3    4    0.583917    0.844762    0.518624    11.00000    0.02805    0.02694 =
         0.03469    0.00548    0.00057    0.00417
O4    4    0.217205    0.900037    0.645777    11.00000    0.02658    0.02735 =
         0.04779   -0.00185   -0.00307    0.00518
N1    3    0.642536    0.637323    0.669007    11.00000    0.02260    0.01639 =
         0.02941    0.00025   -0.00615    0.00039
N2    3    0.400796    0.868487    0.585375    11.00000    0.02602    0.01894 =
         0.03375    0.00228   -0.00439    0.00430
H2N   2    0.392562    0.951974    0.550042    11.00000    0.04307
C1    1    0.709969    0.531706    0.616013    11.00000    0.02655    0.01729 =
         0.02587    0.00244   -0.00486    0.00173
C2    1    0.836777    0.576201    0.628327    11.00000    0.02451    0.01771 =
         0.02973    0.00017   -0.00391    0.00048
AFIX  13
H2A   2    0.886927    0.491448    0.648892    11.00000   -1.20000
AFIX   0
C3    1    0.871286    0.638780    0.512354    11.00000    0.02974    0.02757 =
         0.02909   -0.00189   -0.00084   -0.00266
AFIX  23
H3A   2    0.893112    0.558146    0.461791    11.00000   -1.20000
H3B   2    0.802837    0.688401    0.478581    11.00000   -1.20000
AFIX   0
C4    1    0.972864    0.745436    0.520129    11.00000    0.03059    0.03193 =
         0.03086    0.00111   -0.00080   -0.00464
AFIX  23
H4A   2    1.043151    0.695475    0.549779    11.00000   -1.20000
H4B   2    0.990952    0.783222    0.444218    11.00000   -1.20000
AFIX   0
C5    1    0.940666    0.870409    0.597871    11.00000    0.02858    0.02517 =
         0.03454    0.00271   -0.00350   -0.00504
AFIX  23
H5A   2    1.003226    0.944367    0.597275    11.00000   -1.20000
H5B   2    0.867389    0.916344    0.571200    11.00000   -1.20000
AFIX   0
C6    1    0.924796    0.812775    0.717127    11.00000    0.02499    0.02754 =
         0.03092   -0.00058   -0.00450   -0.00534
AFIX  23
H6A   2    0.899178    0.893048    0.766341    11.00000   -1.20000
H6B   2    1.001037    0.777727    0.746054    11.00000   -1.20000
AFIX   0
C7    1    0.835645    0.689471    0.723952    11.00000    0.02397    0.02156 =
         0.02532    0.00136   -0.00393   -0.00198
AFIX  13
H7A   2    0.850009    0.636936    0.796398    11.00000   -1.20000
AFIX   0
C8    1    0.710327    0.741210    0.724148    11.00000    0.02497    0.01948 =
         0.02585    0.00167   -0.00435   -0.00096
C9    1    0.518635    0.658424    0.646037    11.00000    0.02190    0.01705 =
         0.03187   -0.00047   -0.00701    0.00147
AFIX  13
H9A   2    0.491323    0.576348    0.597625    11.00000   -1.20000
AFIX   0
C10   1    0.506072    0.798031    0.577565    11.00000    0.02532    0.01800 =
         0.02828   -0.00057   -0.00540    0.00206
C11   1    0.304749    0.826064    0.648087    11.00000    0.02421    0.02131 =
         0.03355   -0.00534   -0.00545    0.00065
C12   1    0.317131    0.688939    0.715259    11.00000    0.02446    0.02171 =
         0.03926    0.00008   -0.00170   -0.00164
AFIX  23
H12A  2    0.288711    0.606388    0.669460    11.00000   -1.20000
H12B  2    0.267804    0.695498    0.783153    11.00000   -1.20000
AFIX   0
C13   1    0.443484    0.660763    0.751201    11.00000    0.02388    0.02180 =
         0.03218    0.00301   -0.00341   -0.00074
AFIX  23
H13A  2    0.470638    0.737979    0.802975    11.00000   -1.20000
H13B  2    0.449314    0.566826    0.790999    11.00000   -1.20000
AFIX   0
HKLF 4
REM  hijji131
REM wR2 = 0.2076, GooF = S = 1.187, Restrained GooF = 1.187 for all data
REM R1 = 0.0663 for 2572 Fo > 4sig(Fo) and 0.0674 for all 2626 data
REM 177 parameters refined using 0 restraints
END
WGHT      0.1212      1.0954
REM Instructions for potential hydrogen bonds
HTAB N2 O3_$1
HTAB C7 O4_$2
HTAB C9 O1_$3
HTAB C12 O2_$2
HTAB C13 O2
HTAB C13 O2_$2
REM Highest difference peak  0.333,  deepest hole -0.349,  1-sigma level  0.079
Q1    1   0.8412  0.6272  0.6855  11.00000  0.05    0.33
Q2    1   0.6993  0.5129  0.5365  11.00000  0.05    0.31
Q3    1   0.6910  0.4436  0.6398  11.00000  0.05    0.30
Q4    1   0.6741  0.4281  0.4768  11.00000  0.05    0.27
Q5    1   0.8428  0.6741  0.8051  11.00000  0.05    0.27
Q6    1   0.8439  0.6443  0.4210  11.00000  0.05    0.26
Q7    1   0.6795  0.8529  0.8547  11.00000  0.05    0.25
Q8    1   0.5505  0.8515  0.4355  11.00000  0.05    0.24
Q9    1   0.5769  0.6533  0.6558  11.00000  0.05    0.24
Q10   1   0.9350  0.8226  0.8027  11.00000  0.05    0.24
Q11   1   0.5210  0.6556  0.5594  11.00000  0.05    0.24
Q12   1   0.6998  0.8747  0.8448  11.00000  0.05    0.24
Q13   1   0.8597  0.6174  0.5819  11.00000  0.05    0.24
Q14   1   0.4836  0.5247  0.5217  11.00000  0.05    0.24
Q15   1   0.7714  0.7064  0.7170  11.00000  0.05    0.23
Q16   1   0.4312  0.8730  0.6621  11.00000  0.05    0.23
Q17   1   0.8928  0.7436  0.8687  11.00000  0.05    0.23
Q18   1   0.4147  0.9424  0.6563  11.00000  0.05    0.22
Q19   1   0.4550  0.6359  0.9125  11.00000  0.05    0.22
Q20   1   0.3799  0.8641  0.4991  11.00000  0.05    0.22
;
_shelx_res_checksum              4777
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
O O1 0.66960(17) 0.4309(2) 0.56402(17) 0.0291(4) Uani d 1
O O2 0.67111(18) 0.8499(2) 0.76606(18) 0.0305(5) Uani d 1
O O3 0.58392(17) 0.8448(2) 0.51862(17) 0.0299(5) Uani d 1
O O4 0.21720(17) 0.9000(2) 0.64578(19) 0.0339(5) Uani d 1
N N1 0.64254(19) 0.6373(2) 0.66901(18) 0.0228(5) Uani d 1
N N2 0.4008(2) 0.8685(2) 0.58537(19) 0.0263(5) Uani d 1
H H2N 0.393(4) 0.952(5) 0.550(3) 0.043(10) Uiso d 1
C C1 0.7100(2) 0.5317(3) 0.6160(2) 0.0233(5) Uani d 1
C C2 0.8368(2) 0.5762(3) 0.6283(2) 0.0240(5) Uani d 1
H H2A 0.886927 0.491448 0.648892 0.029 Uiso calc 1
C C3 0.8713(2) 0.6388(3) 0.5124(2) 0.0288(6) Uani d 1
H H3A 0.893112 0.558146 0.461791 0.035 Uiso calc 1
H H3B 0.802837 0.688401 0.478581 0.035 Uiso calc 1
C C4 0.9729(2) 0.7454(3) 0.5201(2) 0.0311(6) Uani d 1
H H4A 1.043151 0.695475 0.549779 0.037 Uiso calc 1
H H4B 0.990952 0.783222 0.444218 0.037 Uiso calc 1
C C5 0.9407(2) 0.8704(3) 0.5979(2) 0.0295(6) Uani d 1
H H5A 1.003226 0.944367 0.597275 0.035 Uiso calc 1
H H5B 0.867389 0.916344 0.571200 0.035 Uiso calc 1
C C6 0.9248(2) 0.8128(3) 0.7171(2) 0.0278(6) Uani d 1
H H6A 0.899178 0.893048 0.766341 0.033 Uiso calc 1
H H6B 1.001037 0.777727 0.746054 0.033 Uiso calc 1
C C7 0.8356(2) 0.6895(3) 0.7240(2) 0.0236(5) Uani d 1
H H7A 0.850009 0.636936 0.796398 0.028 Uiso calc 1
C C8 0.7103(2) 0.7412(3) 0.7241(2) 0.0235(5) Uani d 1
C C9 0.5186(2) 0.6584(3) 0.6460(2) 0.0236(5) Uani d 1
H H9A 0.491323 0.576348 0.597625 0.028 Uiso calc 1
C C10 0.5061(2) 0.7980(3) 0.5776(2) 0.0239(5) Uani d 1
C C11 0.3047(2) 0.8261(3) 0.6481(2) 0.0264(5) Uani d 1
C C12 0.3171(2) 0.6889(3) 0.7153(2) 0.0285(6) Uani d 1
H H12A 0.288711 0.606388 0.669460 0.034 Uiso calc 1
H H12B 0.267804 0.695498 0.783153 0.034 Uiso calc 1
C C13 0.4435(2) 0.6608(3) 0.7512(2) 0.0260(5) Uani d 1
H H13A 0.470638 0.737979 0.802975 0.031 Uiso calc 1
H H13B 0.449314 0.566826 0.790999 0.031 Uiso calc 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O1 0.0298(9) 0.0199(9) 0.0374(10) -0.0011(7) -0.0051(8) -0.0043(7)
O2 0.0306(10) 0.0200(9) 0.0407(11) 0.0001(7) -0.0028(8) -0.0059(7)
O3 0.0280(10) 0.0269(10) 0.0347(10) 0.0042(7) 0.0006(8) 0.0055(7)
O4 0.0266(9) 0.0273(10) 0.0478(12) 0.0052(8) -0.0031(8) -0.0019(9)
N1 0.0226(10) 0.0164(9) 0.0294(10) 0.0004(8) -0.0062(8) 0.0003(8)
N2 0.0260(11) 0.0189(10) 0.0337(11) 0.0043(8) -0.0044(9) 0.0023(9)
C1 0.0265(12) 0.0173(11) 0.0259(11) 0.0017(9) -0.0049(9) 0.0024(9)
C2 0.0245(11) 0.0177(11) 0.0297(12) 0.0005(9) -0.0039(9) 0.0002(9)
C3 0.0297(13) 0.0276(13) 0.0291(13) -0.0027(10) -0.0008(10) -0.0019(10)
C4 0.0306(13) 0.0319(14) 0.0309(13) -0.0046(11) -0.0008(10) 0.0011(10)
C5 0.0286(13) 0.0252(13) 0.0345(14) -0.0050(10) -0.0035(10) 0.0027(10)
C6 0.0250(12) 0.0275(12) 0.0309(13) -0.0053(10) -0.0045(10) -0.0006(10)
C7 0.0240(11) 0.0216(11) 0.0253(11) -0.0020(9) -0.0039(9) 0.0014(9)
C8 0.0250(11) 0.0195(11) 0.0258(11) -0.0010(9) -0.0043(9) 0.0017(9)
C9 0.0219(11) 0.0170(11) 0.0319(12) 0.0015(8) -0.0070(9) -0.0005(9)
C10 0.0253(11) 0.0180(11) 0.0283(11) 0.0021(9) -0.0054(9) -0.0006(9)
C11 0.0242(12) 0.0213(12) 0.0336(13) 0.0007(9) -0.0054(10) -0.0053(10)
C12 0.0245(12) 0.0217(12) 0.0393(14) -0.0016(9) -0.0017(10) 0.0001(10)
C13 0.0239(12) 0.0218(12) 0.0322(13) -0.0007(9) -0.0034(10) 0.0030(9)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C8 N1 C1 112.6(2)
C8 N1 C9 122.3(2)
C1 N1 C9 123.4(2)
C10 N2 C11 127.0(2)
C10 N2 H2N 118(3)
C11 N2 H2N 115(3)
O1 C1 N1 123.9(2)
O1 C1 C2 128.4(2)
N1 C1 C2 107.5(2)
C1 C2 C7 103.9(2)
C1 C2 C3 105.49(19)
C7 C2 C3 113.9(2)
C1 C2 H2A 111.1
C7 C2 H2A 111.1
C3 C2 H2A 111.1
C4 C3 C2 112.8(2)
C4 C3 H3A 109.0
C2 C3 H3A 109.0
C4 C3 H3B 109.0
C2 C3 H3B 109.0
H3A C3 H3B 107.8
C5 C4 C3 109.7(2)
C5 C4 H4A 109.7
C3 C4 H4A 109.7
C5 C4 H4B 109.7
C3 C4 H4B 109.7
H4A C4 H4B 108.2
C6 C5 C4 109.2(2)
C6 C5 H5A 109.8
C4 C5 H5A 109.8
C6 C5 H5B 109.8
C4 C5 H5B 109.8
H5A C5 H5B 108.3
C5 C6 C7 113.2(2)
C5 C6 H6A 108.9
C7 C6 H6A 108.9
C5 C6 H6B 108.9
C7 C6 H6B 108.9
H6A C6 H6B 107.8
C8 C7 C6 113.4(2)
C8 C7 C2 103.24(19)
C6 C7 C2 117.1(2)
C8 C7 H7A 107.5
C6 C7 H7A 107.5
C2 C7 H7A 107.5
O2 C8 N1 123.9(2)
O2 C8 C7 128.2(2)
N1 C8 C7 107.8(2)
N1 C9 C13 113.9(2)
N1 C9 C10 107.4(2)
C13 C9 C10 111.9(2)
N1 C9 H9A 107.8
C13 C9 H9A 107.8
C10 C9 H9A 107.8
O3 C10 N2 121.2(2)
O3 C10 C9 122.6(2)
N2 C10 C9 116.2(2)
O4 C11 N2 119.1(2)
O4 C11 C12 124.1(3)
N2 C11 C12 116.8(2)
C11 C12 C13 112.1(2)
C11 C12 H12A 109.2
C13 C12 H12A 109.2
C11 C12 H12B 109.2
C13 C12 H12B 109.2
H12A C12 H12B 107.9
C9 C13 C12 108.3(2)
C9 C13 H13A 110.0
C12 C13 H13A 110.0
C9 C13 H13B 110.0
C12 C13 H13B 110.0
H13A C13 H13B 108.4
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
O1 C1 1.207(3)
O2 C8 1.208(3)
O3 C10 1.217(3)
O4 C11 1.213(3)
N1 C8 1.394(3)
N1 C1 1.397(3)
N1 C9 1.456(3)
N2 C10 1.374(3)
N2 C11 1.390(4)
N2 H2N 0.88(5)
C1 C2 1.515(3)
C2 C7 1.544(3)
C2 C3 1.548(4)
C2 H2A 1.0000
C3 C4 1.527(4)
C3 H3A 0.9900
C3 H3B 0.9900
C4 C5 1.525(4)
C4 H4A 0.9900
C4 H4B 0.9900
C5 C6 1.525(4)
C5 H5A 0.9900
C5 H5B 0.9900
C6 C7 1.532(3)
C6 H6A 0.9900
C6 H6B 0.9900
C7 C8 1.513(3)
C7 H7A 1.0000
C9 C13 1.522(4)
C9 C10 1.531(3)
C9 H9A 1.0000
C11 C12 1.503(4)
C12 C13 1.528(4)
C12 H12A 0.9900
C12 H12B 0.9900
C13 H13A 0.9900
C13 H13B 0.9900
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N2 H2N O3 3_676 0.88(5) 2.07(5) 2.928(3) 165(4) yes
C7 H7A O4 2_646 1.00 2.42 3.150(3) 129.2 yes
C9 H9A O1 3_666 1.00 2.65 3.385(3) 130.4 yes
C12 H12A O2 2_646 0.99 2.53 3.143(3) 119.8 yes
C13 H13A O2 . 0.99 2.56 3.142(3) 117.5 yes
C13 H13B O2 2_646 0.99 2.52 3.163(3) 122.3 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C8 N1 C1 O1 179.5(2)
C9 N1 C1 O1 -15.2(4)
C8 N1 C1 C2 -5.3(3)
C9 N1 C1 C2 160.0(2)
O1 C1 C2 C7 -167.9(2)
N1 C1 C2 C7 17.2(2)
O1 C1 C2 C3 72.0(3)
N1 C1 C2 C3 -102.9(2)
C1 C2 C3 C4 155.2(2)
C7 C2 C3 C4 41.9(3)
C2 C3 C4 C5 -58.7(3)
C3 C4 C5 C6 64.9(3)
C4 C5 C6 C7 -55.2(3)
C5 C6 C7 C8 -80.1(3)
C5 C6 C7 C2 40.0(3)
C1 C2 C7 C8 -21.7(2)
C3 C2 C7 C8 92.6(2)
C1 C2 C7 C6 -147.1(2)
C3 C2 C7 C6 -32.8(3)
C1 N1 C8 O2 172.5(2)
C9 N1 C8 O2 6.9(4)
C1 N1 C8 C7 -9.4(3)
C9 N1 C8 C7 -174.9(2)
C6 C7 C8 O2 -34.8(4)
C2 C7 C8 O2 -162.5(3)
C6 C7 C8 N1 147.1(2)
C2 C7 C8 N1 19.4(3)
C8 N1 C9 C13 -67.6(3)
C1 N1 C9 C13 128.4(2)
C8 N1 C9 C10 56.9(3)
C1 N1 C9 C10 -107.1(3)
C11 N2 C10 O3 179.1(2)
C11 N2 C10 C9 -0.4(4)
N1 C9 C10 O3 25.9(3)
C13 C9 C10 O3 151.6(2)
N1 C9 C10 N2 -154.6(2)
C13 C9 C10 N2 -28.9(3)
C10 N2 C11 O4 -179.6(2)
C10 N2 C11 C12 0.4(4)
O4 C11 C12 C13 -151.1(3)
N2 C11 C12 C13 28.9(3)
N1 C9 C13 C12 178.0(2)
C10 C9 C13 C12 55.9(3)
C11 C12 C13 C9 -56.1(3)

_cod_database_fobs_code 2242677