#------------------------------------------------------------------------------ #$Date: 2021-05-29 08:14:33 +0300 (Sat, 29 May 2021) $ #$Revision: 265609 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243840.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243840 loop_ _publ_author_name 'Sayed, Eman M.' 'Hassanien, Reda' 'Mohamed, Shaaban K.' 'Mague, Joel T.' 'Akkurt, Mehmet' 'Farhan, Nasser' 'Bakhite, Etify A.' 'Al-Waleedy, Safiyyah A. H.' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of 2-{[7-acetyl-4-cyano-6-hydroxy-8-(4-methoxyphenyl)-1,6-dimethyl-5,6,7,8-tetrahydroisoquinolin-3-yl]sulfanyl}-N-phenylacetamide ; _journal_coeditor_code YK2151 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 663 _journal_page_last 667 _journal_paper_doi 10.1107/S2056989021005430 _journal_volume 77 _journal_year 2021 _chemical_formula_moiety 'C29 H29 N3 O4 S' _chemical_formula_sum 'C29 H29 N3 O4 S' _chemical_formula_weight 515.61 _chemical_name_systematic 2-{[7-Acetyl-4-cyano-6-hydroxy-8-(4-methoxyphenyl)-1,6-dimethyl-5,6,7,8-tetrahydroisoquinolin-3-yl]sulfanyl}-N-phenylacetamide _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 99.021(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.4506(16) _cell_length_b 23.112(5) _cell_length_c 13.601(3) _cell_measurement_reflns_used 9458 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 29.0780 _cell_measurement_theta_min 2.3249 _cell_volume 2623.6(10) _computing_cell_refinement ; SAINT (Bruker, 2016) ; _computing_data_collection ; APEX3 (Bruker, 2016) ; _computing_data_reduction ; SAINT (Bruker, 2016) ; _computing_molecular_graphics ; DIAMOND (Brandenburg & Putz, 2012) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker SMART APEX CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0343 _diffrn_reflns_av_unetI/netI 0.0248 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 31 _diffrn_reflns_limit_k_min -31 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 50421 _diffrn_reflns_theta_full 29.000 _diffrn_reflns_theta_max 29.102 _diffrn_reflns_theta_min 1.753 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.164 _exptl_absorpt_correction_T_max 0.98 _exptl_absorpt_correction_T_min 0.89 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.305 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1088 _exptl_crystal_size_max 0.386 _exptl_crystal_size_mid 0.251 _exptl_crystal_size_min 0.138 _refine_diff_density_max 0.489 _refine_diff_density_min -0.196 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.102 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 338 _refine_ls_number_reflns 7039 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.102 _refine_ls_R_factor_all 0.0530 _refine_ls_R_factor_gt 0.0433 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0798P)^2^+0.1546P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1214 _refine_ls_wR_factor_ref 0.1262 _reflns_number_gt 5632 _reflns_number_total 7039 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yk2151sup1.cif _cod_data_source_block I _cod_original_cell_volume 2623.5(9) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2243840 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.940 _shelx_estimated_absorpt_t_max 0.978 _shelx_hkl_file ; -1 0 0 1.70 0.30 1 0 0 1.00 0.20 -1 0 0 1.60 0.30 -1 0 0 1.70 0.30 2 0 0 4939.31 200.38 2 0 0 5470.65 200.58 -2 0 0 4873.71 200.28 -2 0 0 4603.04 200.28 -2 0 0 4673.73 200.38 -3 0 0 -0.20 0.50 3 0 0 0.00 0.50 -3 0 0 0.30 0.70 -3 0 0 0.40 0.60 3 0 0 0.20 0.70 3 0 0 -0.10 0.30 -4 0 0 5.90 0.90 -4 0 0 0.50 0.90 4 0 0 0.90 0.40 4 0 0 0.20 0.80 -4 0 0 0.60 1.00 -4 0 0 0.20 0.80 4 0 0 1.00 0.70 -5 0 0 -0.30 1.10 -5 0 0 0.30 1.20 5 0 0 0.30 0.50 -5 0 0 -0.20 1.10 -5 0 0 0.20 0.50 -5 0 0 0.10 1.00 5 0 0 -0.30 1.20 5 0 0 -0.80 0.90 -6 0 0 455.15 19.50 -6 0 0 455.15 19.60 -6 0 0 455.45 19.80 6 0 0 483.55 19.60 -7 0 0 -0.30 1.60 -7 0 0 0.20 1.90 -7 0 0 0.20 1.50 7 0 0 0.60 1.50 8 0 0 127.79 6.70 -8 0 0 128.59 6.90 -8 0 0 120.09 6.30 -8 0 0 128.49 7.10 9 0 0 -0.50 2.30 -9 0 0 0.00 2.60 -9 0 0 -0.80 1.90 -9 0 0 -0.80 2.60 -10 0 0 33.60 3.40 -10 0 0 23.60 4.10 -11 0 0 1.10 4.50 -11 0 0 0.70 3.00 -1 -1 0 568.24 22.50 -1 -1 0 566.24 22.50 -1 -1 0 546.45 22.50 1 -1 0 532.25 22.50 1 1 0 528.65 22.50 -1 1 0 576.74 22.60 1 1 0 530.35 22.50 -1 1 0 554.04 22.50 -1 1 0 544.45 22.50 2 -1 0 156.88 6.50 -2 -1 0 155.08 6.60 -2 -1 0 145.49 6.60 -2 -1 0 162.98 6.70 -2 -1 0 155.48 6.60 2 1 0 161.58 6.60 -2 1 0 150.18 6.50 2 1 0 148.29 6.60 2 1 0 161.88 6.50 -2 1 0 161.58 6.60 -2 1 0 152.48 6.60 3 -1 0 90.79 4.10 -3 -1 0 90.89 4.20 -3 -1 0 87.29 4.10 -3 -1 0 86.99 4.10 3 -1 0 94.49 4.00 -3 1 0 94.09 4.10 3 1 0 84.39 4.10 -3 1 0 90.69 4.20 3 1 0 94.79 4.10 3 1 0 95.39 3.90 -3 1 0 83.19 4.10 4 -1 0 267.97 11.30 -4 -1 0 265.27 11.30 4 -1 0 286.87 11.40 -4 -1 0 255.57 11.40 -4 -1 0 275.97 11.40 -4 -1 0 268.17 11.50 -4 1 0 259.57 11.50 4 1 0 270.97 11.10 -4 1 0 251.07 11.30 -4 1 0 251.47 11.40 4 1 0 279.87 11.40 4 1 0 268.47 11.30 -5 -1 0 367.06 16.50 -5 -1 0 398.26 16.60 -5 -1 0 386.66 16.70 5 -1 0 401.96 16.50 5 -1 0 396.26 16.50 5 1 0 408.36 16.50 -5 1 0 367.16 16.60 -5 1 0 376.66 16.40 -5 1 0 396.96 16.70 5 1 0 410.56 16.10 5 1 0 382.96 16.50 -6 -1 0 16.40 2.00 6 -1 0 20.00 2.00 -6 -1 0 24.60 2.30 -6 -1 0 19.70 1.90 -6 1 0 15.60 1.70 -6 1 0 11.40 1.90 -6 1 0 16.90 2.10 6 1 0 20.10 2.00 7 -1 0 0.90 1.70 -7 -1 0 3.10 1.70 -7 -1 0 2.00 1.50 -7 -1 0 2.70 1.90 -7 1 0 3.20 2.00 -7 1 0 1.00 1.40 7 1 0 3.00 1.70 -7 1 0 0.70 1.70 -8 -1 0 18.10 2.90 8 -1 0 19.70 2.60 -8 -1 0 23.20 2.60 -8 -1 0 21.70 2.80 -8 1 0 16.60 2.80 8 1 0 19.20 2.70 -8 1 0 15.80 2.90 -8 1 0 18.60 2.30 9 -1 0 46.80 4.00 -9 -1 0 32.60 4.20 -9 -1 0 36.90 3.70 -9 -1 0 41.80 4.10 -9 1 0 32.30 3.10 -9 1 0 39.30 4.00 -9 1 0 34.30 4.00 9 1 0 38.40 3.70 10 -1 0 0.40 3.10 -10 -1 0 2.70 2.50 10 -1 0 2.10 3.40 -10 -1 0 -1.90 3.60 -10 1 0 0.60 3.20 -10 1 0 1.20 3.60 -10 1 0 0.80 2.30 -11 -1 0 2.30 3.00 -11 -1 0 3.00 4.20 -11 1 0 2.10 2.90 -11 1 0 0.90 4.60 0 -2 0 1165.68 48.90 0 2 0 1222.48 48.90 0 2 0 1166.38 48.90 0 2 0 1234.98 48.90 -1 -2 0 395.56 16.10 1 -2 0 386.76 16.00 -1 -2 0 395.76 16.10 -1 -2 0 376.16 16.10 -1 -2 0 389.86 16.10 -1 2 0 410.16 16.10 -1 2 0 373.66 16.00 1 2 0 401.16 16.10 1 2 0 396.06 16.10 -1 2 0 391.56 16.10 -2 -2 0 2412.06 96.49 -2 -2 0 2303.47 96.59 -2 -2 0 2355.76 96.49 -2 -2 0 2406.36 96.49 2 -2 0 2261.97 96.39 2 2 0 2438.06 96.39 -2 2 0 2341.67 96.59 2 2 0 2447.56 96.49 2 2 0 2328.07 96.49 -2 2 0 2336.07 96.39 -2 2 0 2355.86 96.59 -3 -2 0 17.70 1.30 3 -2 0 17.10 1.10 -3 -2 0 15.80 1.30 -3 -2 0 17.30 1.30 -3 -2 0 15.50 1.20 3 2 0 16.20 1.20 3 2 0 16.20 1.00 -3 2 0 16.00 1.30 -3 2 0 15.80 1.30 3 2 0 14.40 1.20 -3 2 0 15.60 1.10 -4 -2 0 503.35 20.50 4 -2 0 488.75 20.50 4 -2 0 482.05 20.40 -4 -2 0 495.75 20.60 -4 -2 0 484.05 20.50 -4 -2 0 489.95 20.50 -4 2 0 470.85 20.40 4 2 0 508.65 20.30 4 2 0 499.35 20.50 -4 2 0 486.35 20.60 -4 2 0 494.65 20.60 4 2 0 490.75 20.50 5 -2 0 65.99 3.40 5 -2 0 58.19 3.30 -5 -2 0 63.19 3.30 -5 -2 0 66.79 3.60 -5 -2 0 59.99 3.40 -5 2 0 62.29 3.30 5 2 0 67.59 3.40 -5 2 0 57.89 3.50 5 2 0 71.59 3.00 -5 2 0 67.59 3.60 5 2 0 63.09 3.50 -6 -2 0 74.19 4.10 6 -2 0 85.59 4.20 -6 -2 0 87.89 4.50 -6 -2 0 77.49 4.30 6 2 0 88.89 5.10 6 2 0 75.99 4.20 -6 2 0 79.49 4.40 -6 2 0 78.29 4.10 -6 2 0 85.99 4.50 -7 -2 0 37.50 3.00 -7 -2 0 27.70 2.80 -7 -2 0 31.30 3.20 7 -2 0 38.70 3.10 -7 2 0 36.70 3.30 7 2 0 35.90 3.10 -7 2 0 39.60 3.20 -7 2 0 36.50 2.80 -8 -2 0 207.58 9.90 8 -2 0 199.78 9.60 -8 -2 0 191.48 9.50 -8 -2 0 209.98 10.00 -8 2 0 211.88 10.00 -8 2 0 215.18 10.00 -8 2 0 202.58 9.40 8 2 0 211.58 9.80 -9 -2 0 12.40 2.50 9 -2 0 9.30 2.70 9 -2 0 7.20 3.00 -9 -2 0 7.80 2.90 -9 -2 0 11.70 3.10 -9 2 0 6.00 2.80 9 2 0 7.30 3.40 -9 2 0 7.30 2.90 -9 2 0 7.50 2.10 -10 -2 0 56.49 4.60 10 -2 0 56.89 5.40 -10 -2 0 51.49 5.50 10 -2 0 49.60 4.60 -10 2 0 51.59 4.30 -10 2 0 55.59 5.40 -10 2 0 45.70 4.90 -11 -2 0 17.60 3.70 -11 -2 0 12.50 4.60 -11 2 0 12.40 3.00 -11 2 0 11.50 4.30 0 -3 0 0.10 0.20 0 -3 0 0.40 0.30 0 3 0 0.60 0.20 0 3 0 0.80 0.30 0 3 0 0.10 0.30 -1 -3 0 4039.40 161.38 1 -3 0 3872.61 161.38 1 -3 0 3867.11 161.28 -1 -3 0 4046.50 161.28 -1 -3 0 3812.72 161.48 -1 3 0 3962.70 161.28 -1 3 0 4019.10 161.28 1 3 0 3910.01 161.28 -1 3 0 3944.21 161.28 1 3 0 4066.39 161.38 -1 3 0 3938.61 161.28 -2 -3 0 227.88 9.60 2 -3 0 229.98 9.50 -2 -3 0 223.48 9.60 -2 -3 0 236.68 9.60 -2 -3 0 229.68 9.60 -2 3 0 226.78 9.50 -2 3 0 220.88 9.70 -2 3 0 233.18 9.70 2 3 0 224.68 9.60 2 3 0 231.78 9.60 2 3 0 230.48 9.50 3 -3 0 244.88 10.70 -3 -3 0 248.78 10.80 -3 -3 0 254.57 10.80 -3 -3 0 251.07 10.90 -3 -3 0 260.97 10.80 3 3 0 261.97 10.80 -3 3 0 254.57 10.90 -3 3 0 249.08 10.90 -3 3 0 252.77 10.70 3 3 0 269.07 10.70 3 3 0 266.27 10.80 4 -3 0 422.16 16.80 -4 -3 0 399.66 16.90 -4 -3 0 419.26 16.90 -4 -3 0 406.56 17.00 -4 -3 0 379.06 16.90 -4 3 0 408.56 17.00 -4 3 0 407.06 16.80 4 3 0 375.06 16.80 -4 3 0 401.76 17.00 4 3 0 401.56 16.70 4 3 0 405.06 16.90 -5 -3 0 3.80 1.10 -5 -3 0 3.60 1.30 -5 -3 0 1.90 1.30 -5 -3 0 1.70 1.20 5 -3 0 2.60 1.00 5 -3 0 3.90 1.60 5 3 0 4.00 0.90 5 3 0 5.00 1.20 -5 3 0 2.60 0.90 5 3 0 2.30 1.20 -5 3 0 3.30 1.30 -5 3 0 2.10 1.20 -6 -3 0 86.19 4.70 6 -3 0 88.49 4.70 -6 -3 0 93.99 4.90 -6 -3 0 101.29 5.10 -6 3 0 104.89 5.10 -6 3 0 95.39 4.60 6 3 0 100.19 5.00 6 3 0 100.39 4.80 -6 3 0 91.49 5.00 -7 -3 0 493.95 20.80 7 -3 0 474.95 20.70 -7 -3 0 496.85 21.00 -7 -3 0 482.55 20.70 7 3 0 485.65 20.80 -7 3 0 485.55 21.00 -7 3 0 469.05 20.50 -7 3 0 503.45 21.00 8 -3 0 36.00 3.60 -8 -3 0 36.70 3.50 8 -3 0 40.60 3.40 -8 -3 0 34.30 3.60 -8 -3 0 37.20 3.40 -8 3 0 36.20 3.70 -8 3 0 30.80 2.90 -8 3 0 34.30 3.70 8 3 0 37.10 3.40 9 -3 0 40.50 4.30 -9 -3 0 49.00 4.50 -9 -3 0 40.20 3.90 9 -3 0 48.70 4.40 -9 3 0 43.90 4.40 -9 3 0 44.20 3.50 -9 3 0 45.00 4.30 10 -3 0 6.70 3.90 -10 -3 0 1.80 2.70 10 -3 0 2.40 3.00 -10 -3 0 6.90 3.90 -10 3 0 3.90 3.40 -10 3 0 2.30 3.30 -10 3 0 4.70 2.20 -11 -3 0 4.10 3.40 -11 -3 0 7.70 4.90 -11 3 0 6.20 4.20 -11 3 0 4.00 2.60 0 -4 0 6.40 0.60 0 -4 0 4.80 0.40 0 4 0 5.70 0.40 0 4 0 4.40 0.50 0 4 0 6.10 0.60 1 -4 0 608.04 25.00 1 -4 0 605.34 25.20 -1 -4 0 602.44 25.20 -1 -4 0 607.04 25.10 -1 4 0 588.54 25.00 -1 4 0 617.14 25.20 -1 4 0 607.54 25.10 -1 4 0 613.54 25.00 1 4 0 612.54 25.20 -1 4 0 662.33 25.20 2 -4 0 541.15 22.90 -2 -4 0 571.14 22.80 2 -4 0 557.24 22.80 -2 -4 0 570.24 22.90 -2 -4 0 545.95 22.80 -2 -4 0 551.84 22.90 -2 4 0 548.15 23.00 -2 4 0 521.05 22.70 2 4 0 560.04 22.80 2 4 0 566.34 22.90 -2 4 0 556.64 22.70 -2 4 0 560.24 22.70 2 4 0 558.74 22.80 -2 4 0 548.95 22.90 -3 -4 0 256.97 10.80 -3 -4 0 262.37 11.00 3 -4 0 256.77 10.80 -3 -4 0 241.98 10.90 -3 -4 0 245.78 10.80 3 4 0 256.47 10.80 3 4 0 261.47 10.90 -3 4 0 261.97 11.00 3 4 0 250.47 10.90 -3 4 0 274.37 10.70 -3 4 0 255.47 10.70 -3 4 0 257.67 11.00 -4 -4 0 884.71 35.90 4 -4 0 873.01 35.90 -4 -4 0 863.91 36.00 -4 -4 0 848.22 36.10 -4 -4 0 896.71 35.90 4 4 0 870.01 35.80 4 4 0 876.31 35.90 -4 4 0 875.11 36.10 4 4 0 842.12 35.90 -4 4 0 875.11 35.80 -4 4 0 856.41 36.10 -4 4 0 879.31 35.80 -5 -4 0 27.30 2.30 -5 -4 0 30.70 2.30 5 -4 0 30.80 2.10 -5 -4 0 27.70 2.10 -5 -4 0 31.50 2.40 -5 4 0 28.80 2.30 5 4 0 28.00 1.90 -5 4 0 30.40 1.90 5 4 0 31.20 2.20 -5 4 0 27.90 2.30 5 4 0 28.70 2.30 -6 -4 0 17.00 1.90 -6 -4 0 16.80 2.00 6 -4 0 14.00 1.70 -6 -4 0 18.80 2.20 6 4 0 14.80 2.00 -6 4 0 15.40 2.10 -6 4 0 14.30 1.60 -6 4 0 18.40 2.20 6 4 0 18.70 2.00 -7 -4 0 6.20 2.10 7 -4 0 3.10 1.60 -7 -4 0 4.70 1.80 -7 -4 0 3.20 2.00 -7 4 0 3.00 1.40 -7 4 0 4.10 2.00 7 4 0 2.00 1.70 -7 4 0 5.20 2.30 -8 -4 0 -1.30 2.30 8 -4 0 -0.10 1.80 -8 -4 0 -0.70 2.20 8 -4 0 -2.30 2.50 -8 -4 0 -0.70 1.90 -8 4 0 2.00 2.30 8 4 0 2.30 2.30 -8 4 0 0.50 2.30 -8 4 0 0.80 1.50 9 -4 0 14.00 2.80 -9 -4 0 9.50 3.00 -9 -4 0 7.70 2.40 9 -4 0 8.20 3.10 -9 4 0 8.80 2.90 -9 4 0 15.70 3.20 -9 4 0 8.50 2.00 -10 -4 0 99.29 7.50 10 -4 0 94.99 6.90 -10 -4 0 110.49 6.50 10 -4 0 107.69 6.70 -10 4 0 97.29 7.00 -10 4 0 117.09 7.10 -10 4 0 99.29 5.80 -11 -4 0 0.00 3.40 11 -4 0 -3.50 6.10 -11 -4 0 -1.10 4.20 -11 4 0 -2.20 2.40 -11 4 0 0.90 4.20 0 -5 0 0.00 0.40 0 -5 0 0.20 0.30 0 5 0 0.10 0.40 0 5 0 0.30 0.30 0 5 0 0.40 0.40 1 -5 0 87.99 4.10 -1 -5 0 91.39 4.00 -1 -5 0 99.59 4.10 -1 -5 0 94.69 4.10 1 -5 0 92.49 3.90 1 -5 0 90.99 4.00 -1 5 0 93.99 4.10 -1 5 0 92.89 4.20 1 5 0 97.79 4.00 -1 5 0 91.69 3.90 -1 5 0 95.69 4.00 1 5 0 94.49 4.10 2 -5 0 182.68 7.90 -2 -5 0 190.68 7.80 -2 -5 0 188.58 7.90 -2 -5 0 189.68 7.90 -2 -5 0 186.78 7.80 -2 5 0 173.78 7.90 -2 5 0 181.98 7.70 2 5 0 174.48 7.80 -2 5 0 184.08 7.70 -2 5 0 194.08 7.70 -2 5 0 180.48 7.90 2 5 0 186.18 7.80 -3 -5 0 600.94 25.60 3 -5 0 630.04 25.70 -3 -5 0 622.84 25.60 3 -5 0 612.54 25.50 -3 -5 0 618.84 25.70 -3 5 0 642.74 25.40 -3 5 0 643.14 25.50 3 5 0 603.34 25.60 3 5 0 623.54 25.60 -3 5 0 624.94 25.80 -3 5 0 617.94 25.50 -3 5 0 582.34 25.70 3 5 0 622.14 25.60 4 -5 0 39.60 2.50 -4 -5 0 41.10 2.40 -4 -5 0 41.70 2.50 4 -5 0 45.90 2.30 -4 -5 0 40.50 2.50 -4 -5 0 43.00 2.60 4 5 0 37.90 2.30 4 5 0 43.00 2.30 -4 5 0 42.00 2.20 -4 5 0 39.00 2.60 -4 5 0 41.70 2.60 -4 5 0 42.80 2.20 -5 -5 0 665.83 27.60 -5 -5 0 677.03 27.40 5 -5 0 642.94 27.30 5 -5 0 666.23 27.60 -5 -5 0 712.93 27.50 -5 -5 0 628.64 27.50 -5 5 0 656.83 27.60 -5 5 0 648.94 27.60 5 5 0 675.23 27.20 5 5 0 639.54 27.40 5 5 0 623.94 27.40 -5 5 0 656.03 27.20 6 -5 0 30.70 2.80 -6 -5 0 36.00 2.80 -6 -5 0 32.70 2.60 -6 -5 0 30.00 2.60 6 -5 0 32.60 2.50 -6 5 0 29.70 2.80 -6 5 0 34.80 2.80 6 5 0 35.60 2.90 -6 5 0 37.30 2.30 6 5 0 31.00 2.60 7 -5 0 49.99 3.40 -7 -5 0 54.59 3.70 -7 -5 0 44.60 3.60 7 -5 0 49.40 4.10 -7 -5 0 53.09 3.80 -7 5 0 42.10 4.00 -7 5 0 49.30 3.10 7 5 0 60.49 3.80 -7 5 0 54.59 3.90 -8 -5 0 64.99 4.40 -8 -5 0 59.19 4.50 8 -5 0 65.49 4.20 8 -5 0 53.59 4.50 -8 -5 0 68.99 6.30 -8 5 0 58.39 4.50 -8 5 0 57.59 3.60 -8 5 0 56.49 4.50 9 -5 0 103.99 6.30 -9 -5 0 91.89 6.20 9 -5 0 108.99 5.90 -9 -5 0 86.69 5.90 -9 5 0 90.19 5.10 -9 5 0 91.99 6.20 -9 5 0 101.09 6.30 -10 -5 0 4.50 3.50 10 -5 0 4.00 3.00 -10 -5 0 -0.60 2.70 10 -5 0 1.10 4.00 -10 5 0 1.90 2.00 -10 5 0 2.20 4.00 -10 5 0 0.90 3.30 -11 -5 0 4.80 3.70 -11 -5 0 5.20 4.90 11 -5 0 5.10 4.10 11 -5 0 2.40 4.50 -11 5 0 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13.00 2.30 -8 7 0 8.70 3.00 -8 7 0 12.50 2.90 -8 7 0 8.20 1.50 -9 -7 0 182.78 8.80 -9 -7 0 170.58 9.40 9 -7 0 173.88 9.20 -9 7 0 171.18 8.10 -9 7 0 179.18 9.20 -9 7 0 173.98 9.60 -10 -7 0 4.40 3.30 -10 -7 0 6.90 3.60 10 -7 0 4.70 3.80 10 -7 0 1.10 3.20 -10 7 0 4.70 2.10 -10 7 0 5.60 3.80 -10 7 0 5.60 3.80 11 -7 0 18.50 5.80 -11 -7 0 25.50 4.50 11 -7 0 18.60 4.50 -11 -7 0 19.30 4.90 -11 7 0 17.20 5.60 -11 7 0 16.50 2.70 -11 7 0 19.50 5.10 0 -8 0 501.05 21.10 0 -8 0 491.15 21.00 0 8 0 513.05 21.30 0 8 0 504.45 21.00 0 8 0 517.25 21.20 0 8 0 535.65 21.00 -1 -8 0 2391.36 95.79 -1 -8 0 2287.17 95.89 1 -8 0 2340.27 95.89 1 -8 0 2405.86 95.69 -1 -8 0 2388.56 95.79 1 -8 0 2349.46 95.69 -1 8 0 2370.66 95.79 1 8 0 2282.07 95.79 -1 8 0 2391.86 95.59 -1 8 0 2268.27 95.99 1 8 0 2382.76 95.89 1 8 0 2294.37 95.99 -1 8 0 2316.17 95.59 -2 -8 0 620.44 25.50 -2 -8 0 607.74 25.60 -2 -8 0 642.34 25.60 -2 -8 0 640.54 25.50 2 -8 0 603.44 25.30 2 -8 0 606.74 25.60 2 -8 0 624.64 25.30 -2 8 0 605.74 25.70 -2 8 0 618.04 25.60 2 8 0 584.74 25.40 2 8 0 651.23 25.60 2 8 0 601.84 25.50 -2 8 0 608.94 25.20 -2 8 0 627.24 25.40 -2 8 0 602.44 25.20 3 -8 0 42.00 2.10 3 -8 0 35.40 2.10 -3 -8 0 41.00 2.20 -3 -8 0 39.20 2.40 -3 -8 0 37.80 2.30 -3 -8 0 40.90 2.50 3 -8 0 35.60 2.40 -3 8 0 39.40 2.50 -3 8 0 38.80 1.90 3 8 0 42.10 2.40 3 8 0 38.90 2.30 3 8 0 34.60 2.20 -3 8 0 41.90 1.90 -3 8 0 41.00 2.10 -3 8 0 42.20 2.50 -4 -8 0 33.70 2.30 -4 -8 0 41.20 2.60 4 -8 0 39.20 2.60 -4 -8 0 37.20 2.50 -4 8 0 42.00 1.90 4 8 0 34.70 2.30 -4 8 0 30.50 2.50 4 8 0 32.20 2.30 -4 8 0 37.10 1.90 4 8 0 34.00 2.30 -4 8 0 35.00 2.60 -4 8 0 36.40 1.90 -5 -8 0 2.20 1.50 5 -8 0 1.70 0.90 5 -8 0 2.10 1.20 -5 -8 0 1.60 1.40 -5 -8 0 0.80 1.20 -5 -8 0 0.10 1.20 5 8 0 0.20 1.20 5 8 0 1.60 1.40 -5 8 0 0.20 1.00 -5 8 0 1.20 0.80 5 8 0 1.90 1.20 -5 8 0 0.70 1.40 -5 8 0 1.00 1.40 -6 -8 0 24.50 2.50 6 -8 0 28.30 2.90 -6 -8 0 32.70 2.90 6 -8 0 30.00 2.50 -6 -8 0 29.10 2.90 6 8 0 27.40 2.60 6 8 0 27.60 2.50 -6 8 0 31.60 3.00 -6 8 0 34.90 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620.24 26.10 -1 9 0 650.03 26.10 -1 9 0 634.64 26.40 2 -9 0 73.59 3.90 -2 -9 0 81.69 3.80 -2 -9 0 85.69 4.00 2 -9 0 74.39 3.60 2 -9 0 83.09 3.70 -2 -9 0 85.59 3.80 -2 -9 0 77.99 3.90 -2 9 0 86.09 3.50 2 9 0 81.99 3.80 -2 9 0 82.69 3.80 -2 9 0 80.19 3.40 -2 9 0 84.49 4.10 2 9 0 76.79 3.90 3 -9 0 769.72 32.80 3 -9 0 768.02 32.50 -3 -9 0 780.82 32.70 -3 -9 0 812.72 32.60 -3 -9 0 800.92 32.90 3 -9 0 792.52 32.50 -3 -9 0 766.82 32.70 -3 9 0 782.32 32.40 -3 9 0 804.52 32.90 -3 9 0 811.02 32.40 -3 9 0 835.92 32.90 3 9 0 784.22 32.70 3 9 0 780.32 32.70 -3 9 0 809.42 32.50 3 9 0 755.02 32.70 4 -9 0 267.37 11.50 -4 -9 0 278.47 11.70 4 -9 0 253.67 11.90 -4 -9 0 269.27 11.80 -4 -9 0 273.97 11.60 -4 -9 0 268.37 11.90 -4 9 0 274.17 11.30 -4 9 0 260.57 11.90 4 9 0 261.17 11.70 -4 9 0 288.47 11.40 4 9 0 273.67 11.70 -4 9 0 280.77 11.30 4 9 0 262.17 11.70 -4 9 0 277.37 12.00 -5 -9 0 72.39 4.00 -5 -9 0 68.89 3.90 -5 -9 0 72.89 3.90 -5 -9 0 59.79 3.60 5 -9 0 64.09 3.90 -5 9 0 68.09 3.20 5 9 0 65.79 3.80 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2.30 1 10 0 35.80 2.00 -1 10 0 39.50 1.80 -1 10 0 41.20 1.80 -1 10 0 37.70 2.30 -1 10 0 41.20 2.20 2 -10 0 253.37 10.60 -2 -10 0 248.18 10.90 -2 -10 0 250.47 10.70 -2 -10 0 256.07 10.80 2 -10 0 241.98 10.90 -2 -10 0 254.67 10.70 2 -10 0 248.58 10.60 2 10 0 246.98 10.80 -2 10 0 257.97 11.00 -2 10 0 257.57 10.40 -2 10 0 248.78 10.40 -2 10 0 256.47 10.70 2 10 0 250.37 10.70 -3 -10 0 20.80 2.00 -3 -10 0 20.30 1.90 3 -10 0 20.80 1.60 -3 -10 0 19.60 1.70 -3 -10 0 21.10 1.80 3 -10 0 21.20 1.90 3 -10 0 20.40 1.50 3 10 0 22.70 1.90 -3 10 0 23.20 1.10 -3 10 0 22.10 1.70 -3 10 0 23.60 1.90 -3 10 0 22.80 1.10 3 10 0 18.20 1.80 -3 10 0 21.10 2.00 3 10 0 22.50 1.70 4 -10 0 34.00 2.60 -4 -10 0 31.70 2.50 4 -10 0 35.00 2.10 -4 -10 0 36.30 2.40 -4 -10 0 29.90 2.50 -4 -10 0 30.80 2.20 -4 10 0 36.80 1.70 -4 10 0 35.40 1.70 -4 10 0 33.60 2.00 4 10 0 28.80 2.30 4 10 0 28.50 2.20 -4 10 0 35.00 2.60 -4 10 0 27.40 2.50 -5 -10 0 398.26 16.80 5 -10 0 395.16 16.60 -5 -10 0 393.16 16.90 -5 -10 0 410.56 16.70 -5 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3.00 2.10 5 -15 0 5.30 1.40 -5 -15 0 7.10 2.00 -5 15 0 5.90 2.20 5 15 0 3.60 1.70 5 15 0 5.40 1.90 6 -15 0 7.10 1.70 6 -15 0 7.00 2.60 -6 -15 0 7.80 2.50 -6 15 0 10.10 2.70 6 15 0 8.00 2.00 6 15 0 8.60 2.30 7 -15 0 5.10 1.90 -7 -15 0 3.80 2.70 7 -15 0 6.20 2.80 -7 15 0 3.30 2.80 7 15 0 2.50 2.40 8 -15 0 7.80 2.40 -8 -15 0 4.70 3.10 8 -15 0 10.20 3.40 8 15 0 10.80 3.00 -8 15 0 11.90 3.50 -9 -15 0 33.90 4.80 9 -15 0 38.30 5.10 9 -15 0 29.40 3.70 -9 15 0 28.40 4.70 10 -15 0 -0.40 5.00 10 -15 0 0.00 3.60 -10 -15 0 1.70 5.00 -10 15 0 -0.80 5.50 0 -16 0 6.80 1.50 0 -16 0 7.40 1.10 0 -16 0 7.00 1.60 0 16 0 6.10 1.70 0 16 0 6.80 0.80 0 16 0 7.70 1.50 0 16 0 8.30 0.90 -1 -16 0 128.49 5.80 1 -16 0 117.69 6.00 -1 -16 0 126.19 6.20 1 -16 0 122.49 5.70 -1 -16 0 126.19 6.00 -1 16 0 126.89 5.30 1 16 0 132.59 5.60 1 16 0 121.99 6.20 1 16 0 123.49 6.10 -1 16 0 126.49 6.30 -1 16 0 126.79 6.00 -1 16 0 126.69 5.30 -2 -16 0 342.47 14.50 -2 -16 0 339.97 14.80 2 -16 0 339.17 14.30 2 -16 0 335.77 14.80 -2 -16 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1.50 1 -20 0 38.20 3.40 -1 -20 0 33.90 3.50 -1 -20 0 37.90 3.30 1 -20 0 36.60 3.20 -1 -20 0 33.80 2.80 1 -20 0 37.40 2.60 -1 20 0 26.90 2.90 1 20 0 41.80 3.30 1 20 0 37.00 2.20 1 20 0 39.30 3.40 -1 20 0 40.50 3.50 2 -20 0 203.78 9.10 -2 -20 0 186.18 8.80 2 -20 0 182.78 8.40 -2 -20 0 178.68 9.00 -2 -20 0 182.28 8.60 -2 20 0 184.28 9.10 -2 20 0 189.98 8.80 2 20 0 197.98 8.30 2 20 0 170.38 8.90 3 -20 0 22.00 3.00 -3 -20 0 24.20 3.10 3 -20 0 19.40 2.00 -3 -20 0 26.90 2.60 -3 20 0 31.60 3.40 3 20 0 27.60 3.20 3 20 0 29.20 2.40 -3 20 0 24.10 2.80 4 -20 0 -0.50 1.30 -4 -20 0 0.90 2.00 4 -20 0 0.40 2.40 -4 -20 0 2.20 2.30 4 20 0 -0.50 2.10 4 20 0 -0.10 1.50 -4 20 0 -0.40 2.40 5 -20 0 8.50 2.80 5 -20 0 4.00 1.60 -5 -20 0 5.50 2.70 -5 -20 0 4.00 2.50 -5 20 0 2.70 2.80 5 20 0 2.60 1.80 5 20 0 6.60 2.60 6 -20 0 22.20 3.70 6 -20 0 24.50 2.70 -6 -20 0 22.60 3.70 -6 20 0 32.80 4.20 6 20 0 25.30 2.80 6 20 0 23.80 3.60 7 -20 0 10.40 3.70 7 -20 0 8.20 2.40 -7 -20 0 9.10 3.50 7 20 0 7.00 3.40 -7 20 0 4.10 3.60 7 20 0 6.10 2.80 8 -20 0 -0.90 4.10 8 -20 0 2.90 2.80 -8 -20 0 2.20 4.00 8 20 0 0.00 3.20 -8 20 0 3.00 4.20 0 -21 0 1.10 1.90 0 -21 0 1.50 2.00 0 -21 0 1.00 1.40 0 21 0 0.10 1.90 0 21 0 -0.70 1.80 0 21 0 0.70 0.70 -1 -21 0 2.40 2.10 1 -21 0 1.60 2.10 1 -21 0 1.10 2.00 -1 -21 0 1.10 2.00 1 -21 0 2.80 1.30 -1 -21 0 2.00 1.50 -1 21 0 3.50 2.20 1 21 0 2.40 1.00 1 21 0 2.30 1.90 -1 21 0 2.10 2.00 1 21 0 6.00 2.10 -2 -21 0 79.09 5.00 2 -21 0 87.19 5.30 2 -21 0 79.99 4.20 -2 -21 0 70.99 4.40 -2 21 0 83.39 5.20 2 21 0 88.59 5.00 -2 21 0 79.79 5.00 2 21 0 76.79 4.00 -3 -21 0 207.58 9.60 3 -21 0 225.28 10.10 3 -21 0 193.68 9.20 -3 -21 0 209.48 10.10 3 21 0 207.78 9.20 -3 21 0 217.48 9.60 3 21 0 198.18 9.80 -3 21 0 193.78 10.10 -4 -21 0 1.80 2.10 -4 -21 0 1.60 2.50 4 -21 0 -0.50 2.40 4 -21 0 0.20 1.50 4 21 0 1.60 2.30 -4 21 0 0.60 2.40 4 21 0 1.80 1.60 -5 -21 0 29.90 3.70 5 -21 0 26.30 3.70 -5 -21 0 19.30 3.10 5 -21 0 20.80 2.30 5 21 0 20.30 2.50 -5 21 0 28.30 3.90 5 21 0 27.50 3.40 6 -21 0 6.70 2.20 6 -21 0 7.20 3.70 -6 -21 0 12.70 3.40 -6 21 0 13.50 3.60 6 21 0 8.80 3.00 6 21 0 9.30 2.40 7 -21 0 46.30 5.10 7 -21 0 35.90 3.60 -7 -21 0 44.30 5.10 7 21 0 45.00 4.80 7 21 0 49.70 4.50 -7 21 0 38.80 5.20 8 -21 0 7.90 4.40 -8 -21 0 5.40 4.30 8 -21 0 6.00 2.90 8 21 0 7.80 3.50 -8 21 0 6.70 4.50 0 -22 0 9.10 1.70 0 -22 0 8.10 2.50 0 -22 0 6.60 2.50 0 22 0 8.00 0.70 0 22 0 5.10 2.20 0 22 0 5.40 2.20 -1 -22 0 52.89 4.00 -1 -22 0 48.10 4.10 1 -22 0 43.50 3.10 1 -22 0 47.50 4.10 -1 -22 0 45.20 3.30 1 -22 0 44.70 3.80 1 22 0 44.00 2.50 -1 22 0 44.40 3.70 -1 22 0 47.70 4.10 1 22 0 44.50 3.80 1 22 0 46.60 3.90 2 -22 0 2.00 1.50 -2 -22 0 1.60 1.70 -2 -22 0 5.70 2.40 2 -22 0 -1.80 2.50 -2 22 0 5.10 2.40 2 22 0 4.10 1.30 2 22 0 -0.40 2.20 -2 22 0 2.30 2.30 -3 -22 0 80.09 5.20 3 -22 0 70.69 5.10 3 -22 0 74.19 4.20 -3 -22 0 72.89 4.60 -3 22 0 71.79 5.20 -3 22 0 78.69 4.80 3 22 0 78.99 4.10 3 22 0 72.69 5.00 4 -22 0 11.30 3.00 4 -22 0 10.20 1.80 -4 -22 0 10.20 2.50 -4 -22 0 8.00 2.90 4 22 0 11.50 1.90 4 22 0 12.70 2.80 -4 22 0 14.20 3.00 -5 -22 0 3.20 2.90 5 -22 0 3.80 2.90 -5 -22 0 2.50 2.60 5 -22 0 1.30 1.70 -5 22 0 3.60 3.10 5 22 0 3.90 2.70 5 22 0 4.40 1.90 6 -22 0 3.50 2.10 -6 -22 0 -0.20 3.20 6 -22 0 3.70 3.40 6 22 0 1.90 2.90 -6 22 0 2.20 3.40 6 22 0 1.00 2.30 7 -22 0 0.00 2.40 7 -22 0 0.60 4.30 -7 -22 0 -0.70 4.10 7 22 0 -0.10 3.30 -7 22 0 -1.50 3.80 7 22 0 -0.80 2.80 -8 -22 0 26.20 5.30 8 -22 0 37.50 6.40 8 -22 0 37.30 6.70 8 22 0 35.50 4.40 -8 22 0 39.40 5.90 0 -23 0 3.10 2.40 0 -23 0 0.30 1.50 0 -23 0 1.20 2.20 0 23 0 -0.80 2.20 0 23 0 1.30 2.30 -1 -23 0 1.70 3.90 -1 -23 0 2.10 1.70 1 -23 0 1.90 2.30 1 -23 0 -0.10 2.60 1 -23 0 1.10 1.40 -1 -23 0 0.80 2.40 -1 23 0 0.20 2.30 1 23 0 0.70 1.00 1 23 0 0.60 2.20 -1 23 0 -2.50 2.10 2 -23 0 -2.20 2.40 -2 -23 0 0.00 2.40 -2 -23 0 -0.40 1.80 2 -23 0 0.80 1.40 -2 23 0 -1.00 2.40 2 23 0 -0.40 2.20 2 23 0 -0.70 1.10 -2 23 0 -0.90 2.30 3 -23 0 71.29 4.20 -3 -23 0 70.79 4.70 -3 -23 0 70.99 5.20 3 -23 0 86.19 5.40 -3 23 0 78.49 4.90 3 23 0 72.39 4.00 3 23 0 72.89 5.10 -3 23 0 73.59 5.40 4 -23 0 0.50 2.80 -4 -23 0 6.80 2.40 -4 -23 0 1.50 2.80 4 -23 0 1.10 1.60 4 23 0 2.60 2.60 -4 23 0 -0.20 2.60 4 23 0 1.80 1.60 -5 -23 0 9.80 3.30 5 -23 0 9.80 2.20 5 -23 0 9.80 3.40 -5 -23 0 11.90 3.00 5 23 0 6.50 2.10 5 23 0 11.90 3.50 -5 23 0 10.90 3.40 6 -23 0 19.20 2.70 6 -23 0 23.10 4.30 -6 -23 0 21.60 4.30 6 23 0 20.60 3.00 6 23 0 24.50 3.90 -6 23 0 31.40 4.60 7 -23 0 17.80 4.60 7 -23 0 15.50 3.00 -7 -23 0 14.70 4.90 7 23 0 15.20 3.30 -7 23 0 9.60 4.50 7 23 0 17.40 4.50 0 -24 0 2.30 2.70 0 -24 0 1.20 1.60 0 -24 0 3.10 2.50 0 24 0 1.00 2.30 0 24 0 -0.60 2.40 -1 -24 0 0.00 1.70 1 -24 0 -0.10 1.50 -1 -24 0 -0.90 2.70 1 -24 0 -1.10 2.30 1 -24 0 1.30 2.80 1 24 0 -0.50 2.30 -1 24 0 0.10 2.30 1 24 0 -0.60 0.90 -1 24 0 -1.60 2.20 2 -24 0 60.19 4.80 2 -24 0 64.19 5.00 2 -24 0 65.89 4.00 -2 -24 0 67.09 5.00 -2 -24 0 63.89 4.40 -2 24 0 59.39 5.00 -2 24 0 66.79 5.10 2 24 0 66.19 3.50 2 24 0 60.69 4.70 -3 -24 0 28.10 3.70 3 -24 0 23.00 3.50 3 -24 0 24.30 2.40 -3 -24 0 24.20 2.90 -3 24 0 22.60 3.40 -3 24 0 23.50 3.60 3 24 0 16.60 3.20 3 24 0 26.20 2.50 -4 -24 0 31.20 3.40 -4 -24 0 31.00 4.10 4 -24 0 37.40 4.50 4 -24 0 33.00 3.20 4 24 0 26.80 2.70 -4 24 0 35.50 4.50 4 24 0 25.50 3.60 -5 -24 0 1.00 3.30 5 -24 0 1.20 3.30 5 -24 0 2.00 2.00 -5 -24 0 2.20 2.90 -5 24 0 0.10 3.20 5 24 0 2.70 3.10 5 24 0 -0.90 2.10 -6 -24 0 0.50 3.80 6 -24 0 -1.60 3.70 6 -24 0 0.00 2.00 6 24 0 -0.30 3.30 -6 24 0 -0.80 3.70 6 24 0 2.30 2.50 -7 -24 0 0.20 4.70 7 -24 0 3.00 4.40 7 -24 0 1.10 2.60 -7 24 0 5.70 4.40 7 24 0 4.10 3.10 7 24 0 1.10 4.50 0 -25 0 -2.10 2.50 0 -25 0 -0.20 2.60 0 -25 0 1.60 1.70 0 25 0 -0.50 2.50 0 25 0 -1.90 2.40 -1 -25 0 30.50 3.80 1 -25 0 26.50 2.60 -1 -25 0 27.20 2.90 1 -25 0 31.20 3.70 1 -25 0 32.60 3.90 -1 25 0 28.90 3.70 -1 25 0 25.10 3.40 1 25 0 23.50 3.40 1 25 0 27.00 1.80 2 -25 0 52.29 4.90 2 -25 0 58.29 4.80 2 -25 0 53.79 3.80 -2 -25 0 53.49 4.70 -2 -25 0 50.29 4.00 2 25 0 52.69 3.10 2 25 0 51.39 4.60 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5.60 3.80 4 -27 0 4.90 3.90 -4 -27 0 3.40 3.20 4 -27 0 2.30 2.30 -4 27 0 5.00 4.20 4 27 0 3.50 2.10 4 27 0 4.40 3.50 5 -27 0 49.50 4.60 -5 -27 0 54.09 5.10 5 -27 0 50.49 5.80 -5 -27 0 43.90 5.50 5 27 0 44.90 5.30 5 27 0 48.90 4.30 -5 27 0 36.70 5.40 0 -28 0 14.00 2.70 0 -28 0 10.90 3.80 0 28 0 14.50 3.50 0 28 0 15.50 3.80 1 -28 0 14.80 2.70 1 -28 0 12.10 3.80 -1 -28 0 15.20 2.90 -1 -28 0 15.90 3.90 1 28 0 14.50 3.60 -1 28 0 13.50 3.50 -1 28 0 15.60 3.70 -2 -28 0 4.60 3.50 -2 -28 0 3.70 2.70 2 -28 0 3.80 2.20 2 -28 0 3.10 3.50 2 -28 0 1.50 3.50 2 28 0 4.00 3.40 2 28 0 4.30 1.10 -2 28 0 4.50 3.30 -2 28 0 1.50 3.60 -3 -28 0 9.00 3.20 3 -28 0 11.70 3.90 3 -28 0 9.60 4.50 -3 -28 0 10.50 4.40 3 -28 0 11.20 2.60 -3 28 0 10.00 4.30 3 28 0 14.00 3.80 3 28 0 7.00 1.80 -4 -28 0 52.49 5.90 -4 -28 0 53.69 5.10 4 -28 0 56.39 4.60 4 -28 0 63.19 6.40 -4 28 0 39.40 5.50 4 28 0 62.79 6.10 -5 -28 0 37.40 5.60 5 -28 0 40.70 5.90 -5 -28 0 39.90 5.40 5 28 0 31.20 4.10 5 28 0 32.40 5.50 0 -29 0 1.90 2.40 0 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4.50 4.40 0 31 -1 3.20 3.90 -1 -31 -1 27.60 4.00 1 -31 1 23.10 5.60 -1 -31 -1 26.40 5.00 1 -31 1 23.40 3.70 -1 31 -1 29.50 5.20 -1 31 -1 24.90 5.80 1 31 1 20.40 4.60 -2 -31 -1 12.70 3.70 -2 -31 -1 10.50 4.70 -2 31 -1 12.00 4.40 -11 0 2 3.30 4.10 -11 0 2 0.10 3.10 -10 0 2 15.70 2.90 -10 0 2 11.50 3.60 -9 0 2 1.70 2.60 -9 0 2 -1.00 2.00 -8 0 2 7.70 2.60 -8 0 2 11.90 2.70 8 0 -2 10.60 2.60 8 0 -2 11.60 2.50 -8 0 2 9.50 2.20 -7 0 2 0.90 1.60 -7 0 2 0.60 1.60 7 0 -2 -1.50 1.50 7 0 -2 0.60 1.60 -7 0 2 -0.50 1.80 -6 0 2 176.88 8.30 -6 0 2 181.68 8.60 -6 0 2 177.58 8.40 6 0 -2 198.78 8.40 6 0 -2 175.88 8.30 6 0 -2 198.18 8.50 -5 0 2 -0.40 1.20 -5 0 2 0.50 1.10 5 0 -2 -0.60 1.10 5 0 -2 -1.20 1.00 -5 0 2 -1.10 1.00 -5 0 2 0.00 0.70 -5 0 2 -0.40 1.10 5 0 -2 0.00 1.00 4 0 -2 2009.20 81.49 -4 0 2 1985.80 81.69 -4 0 2 2006.80 81.39 -4 0 2 2035.00 81.59 -4 0 2 1953.80 81.59 4 0 -2 2052.29 81.39 -4 0 2 1965.80 81.59 4 0 -2 2015.60 81.59 4 0 -2 1891.21 81.59 -3 0 2 -0.30 0.50 3 0 -2 0.10 0.60 3 0 -2 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1.40 7 0 2 0.60 1.50 -7 0 -2 -0.50 1.90 -8 0 -2 0.70 1.60 -8 0 -2 0.60 2.30 -8 0 -2 5.10 2.40 8 0 2 1.80 2.00 -9 0 -2 0.90 2.70 9 0 2 0.00 2.50 -9 0 -2 0.30 1.90 -9 0 -2 1.30 2.80 -10 0 -2 140.79 7.90 10 0 2 119.79 7.70 -10 0 -2 124.49 8.30 -10 0 -2 124.39 6.80 -11 0 -2 -1.20 4.30 -11 0 -2 -1.60 4.10 -11 -1 2 8.10 3.40 -11 -1 2 16.60 4.90 -11 1 2 9.40 3.30 -11 1 2 4.50 4.10 -10 -1 2 1.90 2.60 -10 -1 2 4.00 3.40 -10 1 2 1.00 3.60 -10 1 2 2.80 2.50 -9 -1 2 1.20 2.30 9 -1 -2 3.20 2.90 -9 -1 2 1.90 2.70 9 -1 -2 1.90 2.50 -9 1 2 6.30 2.80 -9 1 2 1.60 3.40 -9 1 2 1.90 2.20 -8 -1 2 407.46 18.10 8 -1 -2 412.06 17.80 -8 -1 2 398.86 17.80 -8 -1 2 415.86 17.90 8 -1 -2 393.16 17.90 -8 1 2 386.16 17.70 8 1 -2 424.86 17.80 -8 1 2 419.36 18.00 -8 1 2 406.56 18.20 8 1 -2 428.86 17.90 -7 -1 2 54.39 3.60 7 -1 -2 50.69 3.60 -7 -1 2 60.69 3.90 -7 -1 2 51.69 3.60 7 -1 -2 53.69 3.70 -7 1 2 55.79 3.90 7 1 -2 55.19 3.70 7 1 -2 54.49 3.80 -7 1 2 55.19 3.80 -7 1 2 54.49 3.50 6 -1 -2 23.80 2.30 -6 -1 2 21.90 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26 2 5.10 3.00 1 -26 -2 38.60 4.40 -1 -26 2 39.50 3.70 -1 -26 2 46.80 4.70 1 -26 -2 37.10 3.70 1 -26 -2 48.70 4.70 -1 26 2 43.80 2.20 -1 26 2 40.80 4.40 -1 26 2 41.90 4.30 1 26 -2 42.60 4.20 0 -26 2 2.90 2.90 0 -26 -2 0.20 2.00 0 -26 2 -0.50 1.70 0 -26 -2 -1.00 3.10 0 -26 -2 0.60 2.80 0 26 2 0.50 2.60 0 26 2 1.10 2.80 0 26 -2 -0.60 2.70 0 26 2 0.00 1.20 0 26 -2 -1.10 2.50 -1 -26 -2 54.29 4.20 -1 -26 -2 53.39 4.90 1 -26 2 45.60 4.90 1 -26 2 48.30 3.60 -1 26 -2 46.70 4.50 -1 26 -2 44.50 4.70 1 26 2 43.20 4.60 1 26 2 49.50 3.20 2 -26 2 12.70 3.50 -2 -26 -2 13.90 2.90 -2 -26 -2 21.00 3.90 2 -26 2 18.10 2.20 2 -26 2 26.20 3.80 -2 26 -2 19.10 3.30 2 26 2 18.70 3.40 2 26 2 17.60 2.20 -2 26 -2 12.30 3.50 -3 -26 -2 79.59 6.30 3 -26 2 71.69 6.20 -3 -26 -2 90.99 5.90 3 -26 2 85.59 6.60 3 -26 2 83.09 4.70 -3 26 -2 81.39 6.40 3 26 2 78.99 4.80 3 26 2 83.49 6.10 -4 -26 -2 2.30 4.10 4 -26 2 1.30 3.50 -4 -26 -2 2.20 3.20 4 -26 2 4.40 2.00 4 26 2 4.70 3.50 -4 26 -2 1.80 3.60 4 26 2 5.10 2.30 5 -26 2 0.80 2.20 5 -26 2 1.20 4.10 -5 -26 -2 4.40 4.00 -5 26 -2 0.50 4.30 5 26 2 1.30 4.10 5 26 2 3.50 2.70 6 -26 2 26.30 5.90 -6 -26 -2 18.90 5.00 6 26 2 15.90 4.60 6 26 2 22.30 4.20 -6 26 -2 14.10 5.20 -6 -27 2 13.60 4.70 -5 -27 2 2.70 3.40 5 -27 -2 0.70 2.60 5 -27 -2 -0.20 4.10 -5 -27 2 1.60 4.00 5 27 -2 -2.70 3.70 -5 27 2 0.10 4.00 5 27 -2 1.50 1.90 4 -27 -2 0.50 3.70 -4 -27 2 1.10 2.90 4 -27 -2 2.00 2.40 -4 -27 2 5.40 3.70 4 27 -2 3.40 1.60 4 27 -2 0.90 3.40 -4 27 2 2.30 3.60 3 -27 -2 4.60 2.50 3 -27 -2 5.60 3.80 -3 -27 2 7.40 3.70 -3 -27 2 6.00 2.70 3 27 -2 5.40 3.30 -3 27 2 4.20 4.00 -3 27 2 8.50 3.60 -2 -27 2 119.29 7.80 2 -27 -2 126.19 8.00 2 -27 -2 136.99 7.80 -2 -27 2 124.79 6.80 2 -27 -2 129.89 7.00 -2 27 2 136.49 7.90 -2 27 2 139.29 8.10 2 27 -2 125.39 7.60 1 -27 -2 8.30 2.50 -1 -27 2 4.10 3.30 1 -27 -2 4.50 3.60 -1 -27 2 9.60 2.30 1 -27 -2 7.20 3.40 -1 27 2 8.90 3.70 -1 27 2 6.50 3.10 1 27 -2 9.00 3.20 0 -27 -2 0.20 2.20 0 -27 -2 -2.00 2.90 0 -27 2 0.80 1.90 0 -27 2 1.10 3.20 0 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34.60 1.80 1 4 3 34.20 1.80 -1 4 -3 35.60 1.80 2 -4 3 674.63 27.90 -2 -4 -3 664.73 27.90 -2 -4 -3 661.33 28.10 -2 -4 -3 685.03 28.00 -2 -4 -3 670.23 28.00 2 -4 3 650.33 27.80 2 -4 3 668.43 27.80 -2 4 -3 656.33 28.10 2 4 3 691.43 28.00 2 4 3 722.03 28.00 -2 4 -3 699.63 28.10 -2 4 -3 705.13 27.90 -3 -4 -3 1249.47 52.69 3 -4 3 1312.07 52.39 -3 -4 -3 1288.37 52.59 -3 -4 -3 1270.87 52.59 -3 -4 -3 1300.47 52.59 3 -4 3 1288.27 52.39 3 -4 3 1266.77 52.39 3 4 3 1264.97 52.49 -3 4 -3 1270.37 52.69 3 4 3 1250.67 52.59 3 4 3 1322.57 52.59 -4 -4 -3 66.39 3.40 4 -4 3 65.79 3.20 -4 -4 -3 62.79 3.40 -4 -4 -3 65.19 3.50 -4 -4 -3 66.89 3.40 4 -4 3 63.69 3.10 4 -4 3 66.69 2.90 4 4 3 61.39 3.20 -4 4 -3 55.69 3.50 -4 4 -3 66.49 2.90 4 4 3 67.69 3.50 -4 4 -3 63.19 2.90 -4 4 -3 67.99 3.50 4 4 3 65.69 3.40 5 -4 3 2.80 1.00 -5 -4 -3 3.20 1.50 -5 -4 -3 3.40 1.20 -5 -4 -3 3.90 1.30 5 4 3 2.70 1.00 -5 4 -3 2.10 0.80 -5 4 -3 2.40 1.50 -5 4 -3 3.60 1.40 -5 4 -3 2.20 0.70 5 4 3 3.70 1.30 6 -4 3 57.79 3.30 -6 -4 -3 46.70 3.50 -6 -4 -3 49.60 3.40 -6 -4 -3 59.89 3.50 6 4 3 54.39 3.50 -6 4 -3 58.09 3.80 -6 4 -3 47.70 3.40 -6 4 -3 54.79 2.80 -7 -4 -3 1.80 1.60 -7 -4 -3 0.80 2.00 7 -4 3 -0.50 1.40 -7 -4 -3 -0.40 2.10 -7 4 -3 -0.70 1.10 -7 4 -3 0.70 2.10 7 4 3 -0.50 1.70 -7 4 -3 -0.20 1.90 -8 -4 -3 1.40 2.00 -8 -4 -3 6.00 2.80 8 -4 3 2.90 1.90 -8 -4 -3 2.30 2.40 -8 4 -3 2.10 1.40 -8 4 -3 4.70 2.50 -8 4 -3 3.80 2.60 8 4 3 3.70 2.20 -9 -4 -3 38.50 4.50 9 -4 3 42.00 3.70 -9 -4 -3 51.69 4.70 -9 -4 -3 39.20 3.90 -9 4 -3 36.60 2.90 -9 4 -3 38.30 4.20 9 4 3 40.50 4.00 -9 4 -3 33.50 4.30 -10 -4 -3 3.00 2.80 -10 -4 -3 3.10 3.70 10 -4 3 4.90 3.20 -10 4 -3 -0.60 4.20 -10 4 -3 1.50 1.80 -10 4 -3 3.80 4.30 -11 -5 3 0.60 4.00 -11 -5 3 0.20 3.80 -11 5 3 2.10 4.10 -11 5 3 0.60 2.80 -10 -5 3 159.78 8.50 -10 -5 3 130.29 8.60 -10 5 3 157.18 7.80 -10 5 3 147.99 8.70 -9 -5 3 25.70 3.60 -9 -5 3 18.20 3.10 9 -5 -3 22.50 3.40 9 -5 -3 27.50 3.50 -9 5 3 27.30 3.70 -9 5 3 19.40 3.30 -9 5 3 20.50 2.70 -8 -5 3 2.80 2.40 -8 -5 3 2.60 2.50 8 -5 -3 2.30 2.30 8 -5 -3 1.70 2.50 -8 5 3 3.10 1.80 -8 5 3 3.40 2.30 -8 5 3 2.50 2.30 -7 -5 3 2.10 1.90 -7 -5 3 0.60 1.90 7 -5 -3 0.50 1.80 7 -5 -3 0.30 1.80 -7 5 3 0.40 1.50 -7 5 3 1.70 1.90 -7 5 3 1.30 1.90 7 5 -3 1.40 1.80 6 -5 -3 47.50 3.10 -6 -5 3 49.20 3.20 6 -5 -3 48.10 3.10 -6 -5 3 43.30 3.30 -6 -5 3 48.90 3.30 -6 5 3 41.30 2.80 6 5 -3 40.10 2.90 6 5 -3 53.29 3.50 -6 5 3 45.40 3.30 6 5 -3 43.30 2.90 -6 5 3 48.80 3.40 -5 -5 3 13.30 1.80 -5 -5 3 11.90 1.80 5 -5 -3 11.20 1.70 5 -5 -3 12.40 1.70 5 -5 -3 19.00 1.70 -5 -5 3 13.50 1.70 -5 -5 3 15.80 1.40 -5 5 3 13.90 1.80 5 5 -3 9.40 1.60 -5 5 3 13.30 1.20 5 5 -3 10.00 1.50 5 5 -3 13.70 1.50 -5 5 3 15.90 1.60 4 -5 -3 74.99 3.70 -4 -5 3 75.19 3.80 4 -5 -3 74.39 3.70 -4 -5 3 72.89 3.30 -4 -5 3 64.89 3.80 4 -5 -3 75.99 3.60 -4 5 3 76.79 3.70 4 5 -3 68.99 3.60 -4 5 3 73.29 3.40 4 5 -3 74.59 3.70 4 5 -3 68.09 3.50 -4 5 3 66.69 3.50 -4 5 3 70.69 3.80 -3 -5 3 2.90 0.50 3 -5 -3 5.10 1.10 -3 -5 3 4.30 0.80 -3 -5 3 4.10 1.10 -3 -5 3 3.00 1.00 3 -5 -3 3.00 1.00 3 -5 -3 2.40 0.80 -3 5 3 3.50 0.80 -3 5 3 2.90 1.00 3 5 -3 2.70 0.50 -3 5 3 2.80 0.70 -3 5 3 1.70 0.80 3 5 -3 1.70 0.80 3 5 -3 3.50 0.80 2 -5 -3 2013.20 86.29 2 -5 -3 2061.39 86.19 -2 -5 3 2078.29 86.19 -2 -5 3 2088.69 86.29 2 -5 -3 2191.18 86.29 -2 5 3 2186.88 86.19 -2 5 3 2172.68 86.29 -2 5 3 2079.19 86.19 2 5 -3 2067.09 86.09 2 5 -3 2087.39 86.29 -2 5 3 2163.58 86.19 -1 -5 3 273.07 11.40 1 -5 -3 266.37 11.40 -1 -5 3 269.87 11.20 -1 -5 3 261.87 11.20 1 -5 -3 281.47 11.40 1 -5 -3 266.67 11.50 -1 5 3 249.58 11.40 -1 5 3 268.47 11.40 1 5 -3 276.67 11.20 -1 5 3 272.67 11.40 -1 5 3 284.37 11.40 1 5 -3 280.27 11.20 1 5 -3 276.57 11.20 0 -5 -3 366.56 14.90 0 -5 -3 360.16 14.90 0 -5 3 364.26 14.90 0 5 -3 337.97 14.90 0 5 -3 352.66 14.90 0 5 3 349.47 14.90 0 5 3 353.56 14.80 0 5 3 363.66 14.90 0 5 3 368.46 14.90 0 5 -3 363.96 14.80 -1 -5 -3 174.68 7.60 -1 -5 -3 185.88 7.70 -1 -5 -3 178.98 7.40 1 5 3 180.38 7.50 -1 5 -3 177.38 7.50 1 5 3 176.68 7.50 -1 5 -3 170.58 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24 3 4.50 1.00 -3 24 3 6.30 2.70 -3 24 3 8.00 3.00 3 24 -3 6.40 2.80 2 -24 -3 9.90 2.30 -2 -24 3 6.70 1.90 -2 -24 3 6.30 2.70 2 -24 -3 4.90 2.70 2 24 -3 6.70 2.60 -2 24 3 7.00 2.60 -2 24 3 5.60 2.90 -2 24 3 6.70 1.30 -1 -24 3 3.80 1.70 1 -24 -3 9.80 2.90 1 -24 -3 5.00 2.60 1 -24 -3 5.40 2.00 -1 -24 3 5.60 2.70 -1 24 3 7.80 2.80 -1 24 3 1.00 2.40 -1 24 3 4.70 1.40 1 24 -3 2.10 2.40 0 -24 3 7.70 2.80 0 -24 3 7.70 1.60 0 -24 -3 5.50 2.20 0 -24 -3 4.70 3.00 0 -24 -3 5.60 2.70 0 24 -3 4.70 2.70 0 24 3 5.40 1.50 0 24 3 5.90 2.70 0 24 -3 5.40 2.50 0 24 3 5.00 2.50 1 -24 3 2.80 1.50 -1 -24 -3 2.10 2.00 1 -24 3 1.10 2.60 -1 -24 -3 4.60 2.80 -1 -24 -3 1.90 2.70 1 24 3 2.60 1.50 -1 24 -3 0.20 2.70 1 24 3 0.30 2.80 -1 24 -3 2.60 2.60 -2 -24 -3 51.29 4.40 -2 -24 -3 41.10 4.20 2 -24 3 38.20 2.90 -2 -24 -3 39.90 4.40 2 -24 3 45.60 4.50 2 -24 3 42.80 4.30 2 24 3 49.99 4.40 2 24 3 41.70 3.30 -2 24 -3 46.70 4.50 -2 24 -3 42.90 4.20 -3 -24 -3 38.40 3.80 3 -24 3 27.80 2.70 3 -24 3 35.40 4.30 -3 -24 -3 31.50 4.30 -3 24 -3 29.30 4.10 3 24 3 28.30 3.70 3 24 3 33.90 3.10 4 -24 3 0.60 1.60 4 -24 3 0.70 3.20 -4 -24 -3 2.60 3.10 4 24 3 2.00 2.20 -4 24 -3 2.40 3.20 4 24 3 -1.00 3.10 5 -24 3 17.70 4.10 -5 -24 -3 14.30 4.40 5 -24 3 15.40 2.30 5 24 3 19.70 3.80 -5 24 -3 16.80 4.00 5 24 3 16.70 2.80 -6 -24 -3 6.10 4.10 6 -24 3 4.60 2.20 6 -24 3 5.90 4.20 6 24 3 3.60 3.70 -6 24 -3 5.00 4.20 6 24 3 1.10 3.10 7 25 -3 1.70 4.40 6 -25 -3 4.20 2.80 -6 -25 3 11.80 3.90 -6 -25 3 8.90 4.10 6 -25 -3 11.20 4.50 -6 25 3 11.20 4.60 6 25 -3 13.20 4.00 6 25 -3 10.00 2.30 -5 -25 3 3.00 3.00 5 -25 -3 2.70 2.60 5 -25 -3 3.10 3.60 -5 -25 3 3.50 3.60 5 25 -3 5.90 3.90 -5 25 3 3.30 3.60 5 25 -3 5.30 1.80 4 -25 -3 55.99 5.30 -4 -25 3 47.70 5.00 -4 -25 3 43.40 4.00 4 -25 -3 42.20 4.10 4 25 -3 48.00 2.80 -4 25 3 40.20 4.80 4 25 -3 37.60 4.40 -3 -25 3 10.70 2.40 -3 -25 3 13.60 3.60 3 -25 -3 10.80 3.30 3 -25 -3 10.10 2.50 -3 25 3 12.60 3.30 -3 25 3 14.30 3.20 3 25 -3 12.70 3.10 -3 25 3 15.20 1.10 2 -25 -3 3.70 2.10 2 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0 -19 -4 11.00 2.20 0 -19 -4 12.10 1.90 0 -19 4 11.30 2.10 0 -19 4 9.20 1.20 0 19 -4 10.70 2.40 0 19 -4 9.90 2.20 0 19 4 13.80 2.30 0 19 4 12.90 2.30 0 19 4 10.90 1.70 -1 -19 -4 59.49 4.00 -1 -19 -4 70.49 4.30 -1 -19 -4 66.29 4.60 1 -19 4 61.29 4.40 1 -19 4 62.39 3.20 1 -19 4 60.79 4.20 1 19 4 64.59 4.30 -1 19 -4 64.29 4.40 -1 19 -4 62.09 4.10 1 19 4 71.39 4.30 1 19 4 65.59 3.80 -2 -19 -4 17.60 2.60 2 -19 4 20.10 2.80 2 -19 4 17.60 1.60 -2 -19 -4 21.40 2.60 -2 -19 -4 17.80 2.70 -2 19 -4 17.10 2.60 2 19 4 17.00 2.60 -2 19 -4 14.40 2.70 2 19 4 20.70 2.30 -3 -19 -4 1.50 2.20 3 -19 4 1.70 2.20 -3 -19 -4 1.20 2.20 -3 -19 -4 0.80 2.00 3 -19 4 2.00 1.00 -3 19 -4 0.20 2.10 -3 19 -4 2.30 1.90 3 19 4 2.50 1.90 3 19 4 0.20 2.00 4 -19 4 0.40 2.40 -4 -19 -4 1.40 2.60 4 -19 4 0.80 1.10 -4 -19 -4 0.90 2.30 -4 19 -4 0.90 2.40 4 19 4 -1.70 1.90 4 19 4 -0.10 2.20 -5 -19 -4 -0.60 2.90 5 -19 4 -1.00 2.60 5 -19 4 1.10 1.30 -5 19 -4 1.70 2.80 5 19 4 0.00 2.00 5 19 4 2.10 2.50 -5 19 -4 2.20 2.70 -6 -19 -4 107.19 6.50 6 -19 4 98.49 6.60 6 -19 4 90.79 5.10 6 19 4 103.69 6.30 -6 19 -4 97.99 6.70 6 19 4 98.29 6.20 -6 19 -4 113.59 7.20 7 -19 4 38.10 4.90 7 -19 4 44.00 3.60 -7 19 -4 29.50 4.80 -7 19 -4 25.30 4.60 8 -19 4 13.10 2.80 8 -19 4 18.20 4.80 -8 19 -4 8.80 5.10 -8 19 -4 6.90 4.90 8 -20 -4 13.10 3.50 -8 -20 4 11.40 4.30 8 -20 -4 13.90 4.40 8 20 -4 8.50 3.00 -8 20 4 11.90 4.50 -8 20 4 10.60 1.60 -7 -20 4 7.70 4.10 7 -20 -4 6.60 3.60 -7 -20 4 7.10 3.10 7 -20 -4 8.60 2.80 -7 20 4 7.80 1.60 -7 20 4 15.10 3.90 7 20 -4 9.80 3.30 7 20 -4 10.70 2.40 -6 -20 4 5.60 2.70 -6 -20 4 2.70 3.00 6 -20 -4 9.10 3.30 6 -20 -4 1.60 2.10 -6 20 4 3.90 1.40 6 20 -4 3.10 1.80 6 20 -4 4.70 2.80 -6 20 4 3.50 3.00 -5 -20 4 10.20 2.40 5 -20 -4 12.40 3.10 -5 -20 4 7.30 2.90 5 -20 -4 6.30 2.20 5 20 -4 7.90 1.70 5 20 -4 9.40 2.70 -5 20 4 11.10 1.50 -5 20 4 11.50 3.20 4 -20 -4 181.28 9.70 -4 -20 4 194.48 9.20 4 -20 -4 182.08 9.20 -4 -20 4 201.18 9.80 -4 20 4 193.88 8.60 4 20 -4 214.08 9.70 -4 20 4 184.08 9.30 -4 20 4 193.88 9.80 4 20 -4 205.58 8.60 -3 -20 4 301.57 13.40 3 -20 -4 280.47 13.30 -3 -20 4 286.77 12.60 3 -20 -4 276.17 12.80 3 20 -4 295.47 13.20 -3 20 4 293.87 13.50 -3 20 4 267.77 12.30 3 20 -4 289.37 12.00 -3 20 4 307.97 13.10 -2 -20 4 4.20 1.40 -2 -20 4 3.10 2.20 2 -20 -4 0.40 2.10 2 -20 -4 5.50 1.70 2 20 -4 3.90 2.10 -2 20 4 3.60 2.30 -2 20 4 3.60 1.40 -2 20 4 6.50 2.40 1 -20 -4 0.00 1.60 1 -20 -4 -0.20 2.00 1 -20 -4 -0.50 2.10 -1 -20 4 1.00 1.20 -1 -20 4 0.70 2.00 -1 20 4 0.80 2.00 1 20 -4 -0.50 2.20 -1 20 4 0.40 1.30 -1 20 4 0.70 2.00 0 -20 4 4.20 2.10 0 -20 -4 4.70 2.20 0 -20 -4 5.40 1.80 0 -20 -4 4.50 2.20 0 -20 4 4.90 1.20 0 20 -4 2.80 2.10 0 20 -4 4.00 2.10 0 20 4 3.20 1.50 0 20 4 2.10 2.10 0 20 4 2.70 2.00 1 -20 4 40.90 3.60 1 -20 4 36.90 2.40 -1 -20 -4 35.70 3.20 -1 -20 -4 38.00 3.50 1 -20 4 38.20 3.50 -1 -20 -4 38.60 3.60 -1 20 -4 39.10 3.60 1 20 4 39.30 3.00 1 20 4 42.60 3.50 1 20 4 40.60 3.50 -1 20 -4 39.70 3.50 2 -20 4 7.30 1.10 2 -20 4 9.90 2.60 2 -20 4 9.60 2.90 -2 -20 -4 9.40 2.80 -2 -20 -4 8.80 2.30 -2 -20 -4 9.50 2.30 2 20 4 5.70 2.30 -2 20 -4 8.60 2.80 2 20 4 9.60 2.00 -2 20 -4 6.50 2.10 3 -20 4 -0.20 2.60 -3 -20 -4 0.60 2.20 3 -20 4 0.30 0.90 -3 -20 -4 0.00 2.10 -3 -20 -4 0.50 2.30 -3 20 -4 -0.40 2.20 3 20 4 -0.80 2.20 -3 20 -4 0.30 2.50 3 20 4 0.80 1.80 -4 -20 -4 4.10 2.50 4 -20 4 3.20 1.20 4 -20 4 4.10 2.60 -4 -20 -4 1.50 2.90 -4 20 -4 2.50 2.50 4 20 4 2.10 2.40 4 20 4 1.90 2.00 5 -20 4 0.60 2.80 -5 -20 -4 -0.30 2.70 5 -20 4 0.90 1.40 -5 20 -4 0.90 3.10 5 20 4 1.50 2.90 5 20 4 -1.30 2.40 -6 -20 -4 26.30 4.90 6 -20 4 23.80 4.10 6 -20 4 24.90 2.40 6 20 4 23.90 3.70 -6 20 -4 30.10 4.30 6 20 4 27.40 3.70 7 -20 4 9.90 2.30 7 -20 4 10.10 4.10 7 20 4 6.70 3.40 -7 20 -4 4.80 4.00 -8 20 -4 33.60 6.10 8 -21 -4 5.80 3.30 8 -21 -4 2.80 4.30 -8 -21 4 1.40 4.80 8 21 -4 -1.00 2.90 -8 21 4 4.60 4.50 7 -21 -4 -1.80 3.60 -7 -21 4 -0.30 3.10 7 -21 -4 2.00 2.70 -7 -21 4 1.70 3.60 7 21 -4 0.30 3.60 -7 21 4 0.40 1.30 -7 21 4 -1.40 3.60 7 21 -4 1.70 2.20 -6 -21 4 28.50 3.50 6 -21 -4 23.80 3.30 -6 -21 4 32.60 4.30 6 -21 -4 32.60 4.30 6 21 -4 31.30 4.00 6 21 -4 32.90 3.20 -6 21 4 37.50 4.90 -6 21 4 32.40 2.40 -5 -21 4 -1.20 2.20 5 -21 -4 0.20 2.70 -5 -21 4 1.50 2.70 5 -21 -4 -0.70 2.00 -5 21 4 -2.10 2.70 -5 21 4 0.20 1.30 5 21 -4 -0.70 2.90 5 21 -4 -0.10 1.50 -4 -21 4 48.40 3.80 4 -21 -4 44.90 3.60 -4 -21 4 41.90 4.20 4 -21 -4 42.30 4.20 4 21 -4 41.50 2.60 -4 21 4 43.80 2.80 -4 21 4 42.60 3.80 -4 21 4 35.40 4.20 4 21 -4 36.70 3.80 3 -21 -4 9.90 2.20 3 -21 -4 11.40 2.90 -3 -21 4 12.00 2.00 -3 -21 4 13.40 2.90 -3 21 4 14.70 1.70 -3 21 4 14.70 2.60 3 21 -4 18.80 2.90 -3 21 4 20.30 3.10 2 -21 -4 14.50 2.20 -2 -21 4 11.20 2.60 -2 -21 4 19.60 2.10 2 -21 -4 17.10 2.90 2 21 -4 23.90 3.00 -2 21 4 22.60 3.30 -2 21 4 19.50 2.70 -2 21 4 17.50 1.80 1 -21 -4 215.48 9.70 -1 -21 4 197.58 8.80 1 -21 -4 201.18 9.60 1 -21 -4 194.58 9.20 -1 -21 4 200.28 9.70 -1 21 4 194.58 9.70 -1 21 4 195.28 8.80 1 21 -4 201.98 9.50 -1 21 4 179.88 9.40 0 -21 -4 52.89 4.30 0 -21 -4 59.79 4.30 0 -21 -4 54.29 4.00 0 -21 4 58.49 3.20 0 -21 4 61.49 4.40 0 21 4 59.19 3.50 0 21 4 57.19 4.20 0 21 -4 49.10 4.10 0 21 -4 58.49 4.40 0 21 4 58.99 4.50 1 -21 4 20.40 1.90 -1 -21 -4 22.60 2.70 1 -21 4 22.00 3.00 -1 -21 -4 22.60 3.00 1 -21 4 18.30 3.00 -1 -21 -4 21.40 3.10 -1 21 -4 19.40 3.00 -1 21 -4 16.20 2.70 1 21 4 23.40 3.30 1 21 4 22.20 2.30 1 21 4 26.70 3.00 2 -21 4 1.10 1.00 -2 -21 -4 0.90 2.20 -2 -21 -4 2.40 2.00 -2 -21 -4 3.10 2.80 2 -21 4 0.30 2.40 2 -21 4 1.00 2.30 2 21 4 -1.00 2.20 -2 21 -4 -1.10 2.10 -2 21 -4 1.40 2.30 2 21 4 0.60 1.80 -3 -21 -4 4.50 2.90 3 -21 4 3.40 2.60 3 -21 4 1.50 1.10 -3 -21 -4 2.80 2.70 -3 -21 -4 2.10 2.40 3 21 4 5.40 2.50 -3 21 -4 2.90 2.90 3 21 4 2.40 2.00 -3 21 -4 1.80 2.50 -4 -21 -4 26.80 3.70 -4 -21 -4 25.50 3.50 4 -21 4 24.60 3.80 4 -21 4 26.80 2.30 4 21 4 27.40 3.00 4 21 4 26.00 3.40 -4 21 -4 20.40 3.70 5 -21 4 68.69 3.90 5 -21 4 62.39 5.40 -5 -21 -4 60.29 5.70 -5 21 -4 63.59 5.40 5 21 4 78.29 5.70 5 21 4 68.59 4.90 6 -21 4 4.70 3.70 6 -21 4 1.20 1.90 6 21 4 0.70 2.90 6 21 4 1.20 3.00 -6 21 -4 2.10 3.70 7 -21 4 10.60 2.50 7 -21 4 14.90 5.10 -7 21 -4 10.40 4.30 7 21 4 11.00 3.70 8 -22 -4 64.99 7.60 8 -22 -4 89.79 6.50 -8 -22 4 71.79 7.90 -8 22 4 85.49 8.60 -7 -22 4 1.60 3.50 7 -22 -4 -1.10 4.40 -7 -22 4 0.10 3.70 7 -22 -4 1.60 2.80 7 22 -4 3.60 2.40 -7 22 4 2.40 4.10 7 22 -4 2.10 3.50 6 -22 -4 85.89 6.30 -6 -22 4 79.39 5.60 -6 -22 4 83.19 6.30 6 -22 -4 63.89 5.20 6 22 -4 76.99 4.60 6 22 -4 69.59 5.80 -6 22 4 72.39 6.10 -6 22 4 69.09 3.60 -5 -22 4 41.80 3.70 5 -22 -4 39.60 3.80 -5 -22 4 35.30 4.30 5 -22 -4 29.90 4.20 -5 22 4 31.30 4.30 5 22 -4 34.70 4.30 5 22 -4 32.50 2.80 -5 22 4 37.60 2.50 4 -22 -4 0.30 2.00 -4 -22 4 1.40 2.70 -4 -22 4 -0.70 2.00 4 -22 -4 0.20 2.60 4 22 -4 0.50 2.50 -4 22 4 -1.00 2.60 -4 22 4 0.00 1.30 4 22 -4 1.20 1.20 -4 22 4 1.30 2.60 3 -22 -4 1.30 2.50 3 -22 -4 2.80 1.90 -3 -22 4 2.90 1.80 -3 -22 4 2.80 2.60 -3 22 4 4.00 2.60 -3 22 4 2.70 1.30 3 22 -4 3.10 2.50 -3 22 4 6.00 2.50 -2 -22 4 313.87 13.30 2 -22 -4 296.97 14.00 -2 -22 4 303.87 14.10 2 -22 -4 318.27 13.70 -2 22 4 297.27 14.10 -2 22 4 294.67 13.80 -2 22 4 304.17 13.10 2 22 -4 304.57 13.90 1 -22 -4 237.28 11.30 1 -22 -4 246.18 11.40 1 -22 -4 230.98 10.80 -1 -22 4 243.28 11.40 -1 -22 4 237.08 10.40 -1 22 4 230.88 11.30 -1 22 4 241.28 10.40 1 22 -4 224.78 11.10 -1 22 4 236.58 11.10 0 -22 -4 50.09 4.10 0 -22 4 52.69 3.00 0 -22 4 48.20 4.20 0 -22 -4 49.99 4.20 0 -22 -4 42.70 3.90 0 22 4 42.20 4.00 0 22 -4 50.99 4.30 0 22 4 52.09 3.20 0 22 -4 48.60 4.10 0 22 4 38.00 4.00 -1 -22 -4 38.80 3.70 -1 -22 -4 49.30 4.60 -1 -22 -4 44.20 4.00 1 -22 4 43.10 4.10 1 -22 4 44.80 2.80 1 22 4 47.00 4.00 -1 22 -4 37.00 3.80 -1 22 -4 38.50 4.00 1 22 4 47.00 3.20 -2 -22 -4 3.50 2.40 -2 -22 -4 7.90 3.10 2 -22 4 3.60 2.80 -2 -22 -4 4.20 2.20 2 -22 4 3.60 2.50 2 -22 4 5.80 1.20 2 22 4 3.60 1.90 -2 22 -4 4.50 2.60 -2 22 -4 5.30 2.40 2 22 4 5.40 2.50 3 -22 4 17.70 3.40 -3 -22 -4 10.60 2.70 3 -22 4 11.80 1.50 -3 -22 -4 8.80 2.90 -3 -22 -4 15.70 3.10 3 22 4 10.60 2.80 -3 22 -4 13.60 3.40 3 22 4 12.80 2.20 -4 -22 -4 6.20 3.00 4 -22 4 5.30 1.40 4 -22 4 7.20 3.10 4 22 4 6.40 2.20 -4 22 -4 6.30 3.00 4 22 4 8.20 2.90 5 -22 4 30.60 4.20 5 -22 4 30.80 2.90 -5 -22 -4 30.50 4.40 5 22 4 34.80 4.10 -5 22 -4 16.60 3.60 5 22 4 33.80 3.60 6 -22 4 0.90 3.70 6 -22 4 2.60 2.00 -6 22 -4 1.20 4.10 6 22 4 0.80 3.00 6 22 4 3.20 3.30 7 -22 4 6.50 4.50 7 -22 4 11.00 2.70 7 22 4 15.90 4.10 -7 22 -4 14.00 4.80 7 -23 -4 4.90 4.30 7 -23 -4 8.40 3.40 -7 -23 4 7.50 4.30 -7 -23 4 4.90 4.60 7 23 -4 6.00 2.60 7 23 -4 10.60 4.10 -7 23 4 1.90 4.30 6 -23 -4 8.10 2.90 6 -23 -4 10.00 3.80 -6 -23 4 7.80 3.90 -6 -23 4 8.50 3.20 -6 23 4 12.80 4.00 6 23 -4 8.40 2.20 6 23 -4 13.20 3.70 -5 -23 4 4.90 2.60 5 -23 -4 2.40 3.20 5 -23 -4 8.20 2.60 -5 -23 4 6.10 3.30 5 23 -4 5.40 1.70 -5 23 4 7.70 1.30 5 23 -4 4.70 3.00 -5 23 4 9.70 3.60 4 -23 -4 16.60 3.40 4 -23 -4 12.30 2.50 -4 -23 4 7.00 3.20 -4 -23 4 10.60 2.50 -4 23 4 12.90 3.30 4 23 -4 12.80 1.40 -4 23 4 11.40 1.50 4 23 -4 13.70 3.40 -3 -23 4 14.90 3.10 3 -23 -4 11.10 2.30 3 -23 -4 12.00 3.00 -3 -23 4 7.20 2.10 3 23 -4 8.20 2.80 -3 23 4 10.30 1.60 -3 23 4 10.20 3.00 -3 23 4 17.50 3.20 -2 -23 4 7.00 2.70 2 -23 -4 8.50 2.20 2 -23 -4 12.20 3.00 -2 -23 4 9.30 1.90 -2 23 4 11.70 2.70 -2 23 4 9.70 1.60 2 23 -4 9.10 2.70 -2 23 4 11.30 2.90 -1 -23 4 3.70 2.60 1 -23 -4 5.10 2.00 -1 -23 4 4.30 1.50 1 -23 -4 2.80 2.60 1 -23 -4 3.10 2.60 -1 23 4 5.30 2.70 1 23 -4 4.10 2.40 -1 23 4 5.80 2.80 -1 23 4 4.90 1.60 0 -23 4 6.80 1.50 0 -23 -4 5.60 2.60 0 -23 4 3.70 2.50 0 -23 -4 5.60 2.30 0 -23 -4 3.90 2.60 0 23 4 4.60 2.50 0 23 -4 3.50 2.60 0 23 4 7.70 2.60 0 23 4 5.90 1.70 0 23 -4 9.60 2.70 1 -23 4 -0.30 1.30 -1 -23 -4 -0.90 2.10 -1 -23 -4 0.50 2.80 -1 -23 -4 -0.20 2.60 1 -23 4 -1.70 2.50 1 23 4 -0.70 1.60 -1 23 -4 1.70 2.70 1 23 4 -0.40 2.40 -1 23 -4 -0.80 2.40 -2 -23 -4 52.99 4.80 -2 -23 -4 49.80 4.50 -2 -23 -4 44.30 4.30 2 -23 4 47.70 4.60 2 -23 4 45.80 3.00 2 -23 4 52.99 4.40 -2 23 -4 46.10 4.50 2 23 4 51.19 4.40 2 23 4 51.59 3.70 -2 23 -4 48.00 4.30 3 -23 4 75.59 5.30 -3 -23 -4 67.99 5.30 -3 -23 -4 60.49 5.20 -3 -23 -4 76.39 5.30 3 -23 4 68.89 3.80 3 23 4 73.89 5.60 -3 23 -4 66.49 5.40 3 23 4 74.79 4.60 4 -23 4 -0.70 1.40 4 -23 4 1.30 3.00 -4 -23 -4 -0.80 3.30 4 23 4 1.40 2.80 -4 23 -4 0.40 2.90 4 23 4 0.40 2.30 5 -23 4 0.70 3.40 5 -23 4 0.20 1.60 -5 -23 -4 -0.60 3.60 5 23 4 -0.20 2.60 -5 23 -4 -3.10 3.30 5 23 4 0.00 3.20 6 -23 4 0.30 2.00 6 -23 4 3.50 4.00 6 23 4 0.70 3.60 -6 23 -4 0.50 3.90 6 23 4 -0.60 3.10 7 -23 4 51.59 7.20 7 23 4 63.09 6.30 7 -24 -4 4.60 3.30 -7 -24 4 5.20 4.40 7 -24 -4 4.50 4.40 -7 24 4 9.10 4.80 7 24 -4 8.90 2.70 7 24 -4 14.80 4.50 -6 -24 4 9.30 3.40 6 -24 -4 7.70 2.90 6 -24 -4 5.80 4.10 -6 -24 4 8.10 4.00 -6 24 4 8.20 4.10 6 24 -4 6.00 2.10 6 24 -4 9.10 3.80 -5 -24 4 -2.10 3.40 5 -24 -4 -0.20 3.30 5 -24 -4 1.20 2.50 -5 -24 4 -0.20 2.70 5 24 -4 -0.40 3.10 -5 24 4 -0.40 1.00 5 24 -4 -0.20 1.50 -5 24 4 0.50 3.50 4 -24 -4 5.90 2.40 4 -24 -4 11.10 3.50 -4 -24 4 6.30 3.30 -4 -24 4 7.30 2.50 4 24 -4 8.40 1.10 -4 24 4 8.80 1.40 4 24 -4 6.80 3.10 -4 24 4 7.70 3.30 3 -24 -4 7.00 2.30 -3 -24 4 4.90 2.10 3 -24 -4 3.40 2.90 -3 -24 4 8.60 3.00 -3 24 4 6.30 3.00 -3 24 4 8.10 1.50 -3 24 4 6.70 2.70 3 24 -4 4.40 2.90 2 -24 -4 26.50 3.70 -2 -24 4 25.30 2.50 2 -24 -4 27.10 3.00 -2 -24 4 27.40 3.70 -2 24 4 24.50 3.60 -2 24 4 22.10 3.30 2 24 -4 23.90 3.50 -2 24 4 25.80 2.50 1 -24 -4 0.50 2.70 -1 -24 4 2.00 2.50 1 -24 -4 4.30 2.00 -1 -24 4 3.60 1.60 1 -24 -4 4.30 2.60 -1 24 4 4.00 2.60 -1 24 4 3.10 3.00 -1 24 4 3.70 1.50 1 24 -4 0.30 2.60 0 -24 -4 27.40 3.80 0 -24 4 22.50 2.20 0 -24 4 31.20 3.70 0 -24 -4 24.80 3.50 0 -24 -4 28.30 3.00 0 24 -4 24.00 3.50 0 24 4 27.20 3.40 0 24 4 28.00 3.60 0 24 4 27.80 2.80 0 24 -4 23.10 3.30 -1 -24 -4 148.09 7.70 1 -24 4 136.09 6.40 1 -24 4 133.59 7.70 -1 -24 -4 135.79 7.60 -1 -24 -4 138.19 7.20 1 24 4 131.19 7.50 1 24 4 132.39 6.70 -1 24 -4 135.29 7.40 -1 24 -4 138.39 7.70 2 -24 4 1.40 1.30 2 -24 4 2.50 3.40 -2 -24 -4 3.60 3.00 -2 -24 -4 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1.70 5 24 -5 8.40 3.50 5 24 -5 8.70 1.50 -4 -24 5 10.60 3.50 4 -24 -5 6.00 3.40 -4 -24 5 18.20 2.80 4 -24 -5 10.10 2.70 4 24 -5 14.00 3.70 -4 24 5 9.80 1.80 -4 24 5 9.50 3.40 -3 -24 5 57.29 5.10 3 -24 -5 55.89 4.40 3 -24 -5 48.80 5.00 -3 -24 5 61.09 4.20 -3 24 5 54.49 5.20 3 24 -5 52.09 4.90 -3 24 5 59.59 3.60 -3 24 5 50.89 5.40 2 -24 -5 69.29 4.80 2 -24 -5 65.69 5.10 -2 -24 5 65.49 5.30 -2 -24 5 62.69 4.10 2 -24 -5 62.19 5.20 2 24 -5 69.79 5.20 -2 24 5 62.39 5.20 -2 24 5 64.09 5.00 -2 24 5 64.99 3.90 1 -24 -5 26.90 3.50 1 -24 -5 21.90 2.90 1 -24 -5 21.50 3.60 -1 -24 5 23.50 3.60 -1 -24 5 22.10 2.20 1 24 -5 20.20 3.50 -1 24 5 22.10 3.30 -1 24 5 21.50 2.30 -1 24 5 24.80 3.40 0 -24 5 60.29 3.60 0 -24 -5 59.89 5.00 0 -24 5 64.59 5.00 0 -24 -5 62.89 4.70 0 -24 -5 55.29 4.80 0 24 -5 62.29 5.00 0 24 5 53.79 4.80 0 24 5 61.09 3.90 0 24 5 59.69 4.80 0 24 -5 48.40 4.60 -1 -24 -5 224.98 10.60 1 -24 5 219.98 11.10 1 -24 5 218.38 9.60 -1 -24 -5 230.78 11.10 -1 -24 -5 208.38 10.90 1 24 5 218.58 10.80 1 24 5 229.88 10.20 -1 24 -5 204.88 10.90 -1 24 -5 218.58 10.70 -2 -24 -5 15.00 3.30 -2 -24 -5 7.30 3.00 -2 -24 -5 5.70 3.10 2 -24 5 7.10 3.00 2 -24 5 8.30 1.50 -2 24 -5 6.90 3.10 2 24 5 7.20 2.30 2 24 5 7.10 3.00 -2 24 -5 7.80 2.90 3 -24 5 28.60 4.40 3 -24 5 30.90 4.50 -3 -24 -5 25.70 4.20 3 -24 5 26.60 2.40 -3 -24 -5 32.30 4.00 -3 24 -5 26.00 4.00 3 24 5 21.40 3.00 3 24 5 23.50 4.00 4 -24 5 3.90 3.40 4 -24 5 2.30 1.60 -4 24 -5 3.20 3.90 4 24 5 1.80 3.20 4 24 5 3.00 2.50 5 -24 5 5.40 1.80 5 -24 5 5.20 4.00 5 24 5 2.80 3.20 -5 24 -5 2.90 3.80 5 24 5 5.70 3.80 6 -24 5 192.48 11.00 6 -24 5 187.08 8.90 -6 24 -5 177.38 10.90 6 24 5 193.98 10.40 -6 -25 5 7.30 3.50 6 -25 -5 5.30 3.40 -6 -25 5 12.30 4.70 6 -25 -5 5.00 4.40 -6 25 5 7.60 4.40 6 25 -5 9.70 4.20 6 25 -5 7.20 2.00 5 -25 -5 1.50 2.80 5 -25 -5 1.40 3.90 -5 -25 5 2.10 2.90 -5 -25 5 1.20 3.70 -5 25 5 1.00 1.60 5 25 -5 2.30 4.00 -5 25 5 0.10 3.70 -4 -25 5 67.69 5.00 4 -25 -5 67.09 5.10 -4 -25 5 68.69 5.90 4 -25 -5 55.89 5.70 -4 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11 -6 60.09 2.80 -3 11 6 61.29 3.70 -3 11 6 59.39 3.40 3 11 -6 53.39 3.70 -3 11 6 60.19 3.40 3 11 -6 62.99 3.10 2 -11 -6 0.00 1.30 2 -11 -6 0.30 1.30 2 -11 -6 0.00 1.20 -2 -11 6 1.10 0.80 -2 -11 6 0.30 1.40 -2 11 6 0.30 1.20 2 11 -6 1.20 1.30 -2 11 6 0.80 1.40 -2 11 6 0.90 1.40 -1 -11 6 134.99 6.00 -1 -11 6 137.09 6.20 -1 -11 6 132.19 6.50 1 -11 -6 139.89 6.50 1 -11 -6 145.19 6.70 1 -11 -6 128.99 6.70 -1 11 6 131.59 6.50 1 11 -6 149.99 6.20 -1 11 6 140.39 6.60 1 11 -6 149.49 6.70 -1 11 6 151.28 6.50 -1 11 6 146.39 6.50 0 -11 -6 33.00 2.50 0 -11 6 32.50 1.60 0 -11 6 33.40 2.40 0 -11 -6 37.70 2.40 0 -11 -6 34.60 2.70 0 -11 -6 35.40 2.50 0 -11 6 32.50 1.60 0 11 -6 36.80 2.60 0 11 -6 33.60 2.20 0 11 6 36.70 2.60 0 11 6 29.40 2.30 0 11 -6 37.00 2.70 0 11 6 35.10 2.30 0 11 6 30.10 2.40 1 -11 6 8.00 1.50 -1 -11 -6 8.20 1.70 -1 -11 -6 9.80 1.60 -1 -11 -6 7.60 1.50 -1 -11 -6 13.80 1.50 -1 11 -6 6.70 1.50 1 11 6 6.60 1.60 -1 11 -6 9.30 1.60 -1 11 -6 9.20 1.60 1 11 6 7.50 1.50 1 11 6 8.90 1.60 2 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1.00 -3 5 9 4.00 1.40 -3 5 9 4.70 1.60 -3 5 9 5.00 1.50 -3 5 9 1.10 1.50 2 -5 -9 48.90 3.20 -2 -5 9 44.30 3.00 -2 -5 9 49.90 2.90 -2 -5 9 52.39 3.40 -2 5 9 45.20 3.20 2 5 -9 52.89 2.90 -2 5 9 58.79 3.30 -2 5 9 48.40 2.80 2 5 -9 53.09 2.60 -2 5 9 46.80 3.20 2 5 -9 50.79 2.60 -1 -5 9 14.80 1.40 -1 -5 9 14.40 2.00 -1 -5 9 15.90 1.60 1 -5 -9 14.00 1.90 1 -5 -9 15.10 1.80 1 5 -9 16.60 1.80 1 5 -9 15.80 0.90 -1 5 9 14.20 2.00 -1 5 9 13.60 1.70 1 5 -9 15.70 0.90 -1 5 9 15.10 2.20 0 -5 -9 59.89 3.60 0 -5 9 67.09 3.30 0 -5 -9 71.09 4.00 0 -5 9 62.99 3.90 0 5 9 67.89 3.90 0 5 9 74.79 3.80 0 5 -9 73.69 3.80 -1 -5 -9 178.28 8.30 1 -5 9 189.88 8.00 1 -5 9 182.98 8.60 -1 -5 -9 178.38 8.60 -1 5 -9 193.78 8.50 1 5 9 198.48 8.40 1 5 9 175.98 8.50 2 -5 9 19.70 1.70 -2 -5 -9 24.00 2.20 2 -5 9 20.50 2.30 -2 -5 -9 26.00 2.60 2 5 9 21.20 2.10 2 5 9 15.60 2.10 -2 5 -9 23.00 2.40 -3 -5 -9 151.88 7.70 -3 -5 -9 160.58 7.20 3 -5 9 150.08 7.30 3 -5 9 157.68 6.90 -3 5 -9 161.68 7.70 3 5 9 145.89 7.20 3 5 9 159.58 7.50 -4 -5 -9 11.20 1.80 -4 -5 -9 14.00 2.70 4 -5 9 17.40 1.60 4 5 9 13.10 2.30 -4 5 -9 16.30 2.70 4 5 9 12.70 2.10 -5 -5 -9 20.40 2.30 5 -5 9 20.90 2.10 -5 -5 -9 21.00 3.20 -5 5 -9 20.90 3.10 5 5 9 21.00 2.70 6 -5 9 98.69 4.90 -6 -5 -9 79.49 4.80 -6 -5 -9 83.89 5.80 -6 5 -9 92.99 6.00 6 5 9 90.89 5.50 -7 -5 -9 -0.30 1.90 7 -5 9 -1.40 2.00 -7 -5 -9 1.60 3.20 7 5 9 -0.70 2.60 -7 5 -9 -0.90 3.20 -8 -5 -9 -3.20 3.70 -8 -5 -9 -1.40 2.20 8 -5 9 0.60 2.50 -8 5 -9 -3.40 3.70 8 5 9 0.70 3.10 -10 -6 9 3.30 4.20 10 6 -9 6.80 3.80 -10 6 9 1.20 3.50 -10 6 9 1.70 4.60 -9 -6 9 5.20 3.60 -9 6 9 -0.30 2.90 -9 6 9 -0.10 3.20 9 6 -9 -1.40 2.80 -8 -6 9 285.17 13.70 -8 6 9 299.07 13.40 -8 6 9 269.37 13.60 8 6 -9 294.67 13.20 -7 -6 9 22.40 3.30 -7 -6 9 21.80 3.00 -7 -6 9 26.10 3.70 -7 6 9 20.20 3.20 7 6 -9 22.90 2.70 -7 6 9 17.50 2.90 -6 -6 9 86.69 5.70 6 -6 -9 96.19 5.30 -6 -6 9 93.69 5.50 -6 -6 9 97.19 5.50 6 -6 -9 94.29 5.70 -6 6 9 93.29 5.50 -6 6 9 92.19 5.50 6 6 -9 95.59 5.10 -6 6 9 92.69 5.30 -5 -6 9 294.97 12.90 5 -6 -9 285.77 13.00 5 -6 -9 308.87 13.10 -5 -6 9 294.77 13.10 -5 -6 9 313.67 13.20 -5 6 9 291.47 13.10 5 6 -9 287.47 13.10 -5 6 9 283.37 12.90 -5 6 9 293.67 13.00 5 6 -9 274.27 12.70 -4 -6 9 94.29 5.20 -4 -6 9 102.29 4.90 4 -6 -9 93.29 5.10 -4 -6 9 94.99 5.00 4 -6 -9 87.09 4.90 4 6 -9 99.49 4.70 -4 6 9 87.99 5.00 4 6 -9 108.39 5.50 -4 6 9 91.89 5.10 -4 6 9 91.39 5.00 -4 6 9 86.99 4.90 -3 -6 9 627.34 25.70 -3 -6 9 638.14 25.50 -3 -6 9 575.04 25.30 3 -6 -9 615.84 25.50 3 6 -9 603.74 25.70 -3 6 9 604.24 25.50 3 6 -9 599.54 25.10 -3 6 9 604.34 25.50 -3 6 9 611.44 25.30 -3 6 9 569.94 25.50 -2 -6 9 159.78 7.00 2 -6 -9 146.09 7.10 2 -6 -9 150.58 7.30 -2 -6 9 149.69 7.30 -2 -6 9 151.48 6.80 2 6 -9 137.79 7.30 2 6 -9 154.78 6.50 2 6 -9 148.89 6.50 -2 6 9 151.58 7.20 -2 6 9 163.08 7.30 -2 6 9 158.18 6.90 -2 6 9 153.38 7.10 -1 -6 9 65.39 4.20 -1 -6 9 72.19 3.60 1 -6 -9 71.29 3.90 -1 -6 9 74.99 3.80 1 -6 -9 75.49 4.20 -1 6 9 81.29 4.20 -1 6 9 78.49 4.00 -1 6 9 65.09 4.10 1 6 -9 83.79 3.90 0 -6 9 56.79 2.90 0 -6 -9 56.99 3.60 0 -6 9 57.39 3.60 0 -6 -9 53.49 3.30 0 6 9 61.49 3.50 0 6 -9 60.09 3.40 0 6 9 56.29 3.60 -1 -6 -9 -0.60 1.20 1 -6 9 -0.50 1.30 1 -6 9 -0.20 0.70 -1 -6 -9 -0.50 1.50 -1 6 -9 1.00 1.60 1 6 9 -0.40 1.20 1 6 9 -0.30 1.60 2 -6 9 14.70 1.30 -2 -6 -9 12.80 2.20 -2 -6 -9 14.50 1.80 2 -6 9 12.40 1.80 2 6 9 11.20 1.80 -2 6 -9 9.50 2.10 2 6 9 12.70 2.00 -3 -6 -9 2.50 1.40 -3 -6 -9 2.60 2.00 3 -6 9 2.50 1.80 3 -6 9 3.20 1.00 -3 6 -9 1.60 1.90 3 6 9 2.60 1.60 3 6 9 4.30 1.80 -4 -6 -9 52.69 3.50 -4 -6 -9 53.89 4.20 4 -6 9 55.39 3.10 -4 6 -9 50.69 4.10 4 6 9 52.89 3.80 4 6 9 63.99 4.10 5 -6 9 32.80 2.70 -5 -6 -9 35.60 3.10 -5 -6 -9 36.20 3.70 5 6 9 35.70 3.60 -5 6 -9 31.60 3.60 6 -6 9 13.30 2.00 -6 -6 -9 12.80 3.10 -6 -6 -9 12.30 2.20 6 6 9 10.50 2.50 -6 6 -9 9.90 3.30 -7 -6 -9 44.50 4.60 7 -6 9 37.00 3.60 -7 -6 -9 38.30 3.60 -7 6 -9 34.90 4.50 7 6 9 36.70 3.80 -8 -6 -9 2.40 4.30 -8 -6 -9 2.30 2.40 8 -6 9 1.60 2.50 -8 6 -9 2.20 3.80 8 6 9 2.20 3.40 -10 -7 9 40.70 5.60 -10 7 9 41.30 4.90 -10 7 9 36.10 5.50 10 7 -9 40.70 5.00 -9 -7 9 75.99 6.10 -9 7 9 73.29 5.70 -9 7 9 61.09 6.00 9 7 -9 69.19 5.60 -8 -7 9 291.77 13.80 -8 7 9 299.27 13.50 -8 7 9 268.97 13.60 8 7 -9 293.77 13.30 -7 -7 9 50.99 4.20 -7 -7 9 40.20 4.00 -7 -7 9 42.50 4.20 7 -7 -9 39.10 3.90 -7 7 9 45.70 4.20 -7 7 9 51.29 4.00 7 7 -9 41.30 3.60 -6 -7 9 -1.60 2.00 -6 -7 9 0.40 2.50 6 -7 -9 0.70 2.00 -6 -7 9 -0.20 2.10 6 7 -9 -1.10 2.10 -6 7 9 0.40 2.20 6 7 -9 -1.20 1.50 -6 7 9 0.50 2.40 -6 7 9 -0.50 2.10 -5 -7 9 47.90 3.60 -5 -7 9 42.40 3.60 5 -7 -9 32.20 3.30 5 -7 -9 41.80 3.30 -5 -7 9 43.00 3.30 -5 7 9 40.80 3.60 5 7 -9 44.50 3.60 -5 7 9 43.10 3.60 -5 7 9 40.50 3.60 5 7 -9 42.20 2.90 -4 -7 9 20.60 2.50 -4 -7 9 15.60 2.00 4 -7 -9 18.30 2.30 4 -7 -9 13.10 2.20 -4 -7 9 18.20 2.50 -4 7 9 23.10 2.40 4 7 -9 19.50 1.80 -4 7 9 14.40 2.20 4 7 -9 22.00 2.70 -4 7 9 16.60 2.20 3 -7 -9 -0.40 1.40 3 -7 -9 0.30 1.50 -3 -7 9 0.80 1.20 -3 -7 9 -0.70 1.60 -3 -7 9 0.20 1.60 -3 7 9 1.50 1.50 -3 7 9 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8 -9 1.50 1.60 -6 8 9 1.20 2.20 6 8 -9 5.10 2.30 -5 -8 9 36.30 3.40 5 -8 -9 28.50 3.20 -5 -8 9 38.00 3.20 5 -8 -9 35.90 3.20 -5 -8 9 40.90 3.50 5 8 -9 38.00 3.50 5 8 -9 33.80 2.60 -5 8 9 37.70 3.60 -5 8 9 37.80 3.40 -5 8 9 39.50 3.20 -4 -8 9 1.10 1.80 -4 -8 9 0.10 1.80 -4 -8 9 1.10 1.40 4 -8 -9 0.90 1.70 4 -8 -9 2.30 2.00 -4 8 9 0.70 1.70 -4 8 9 0.80 1.60 -4 8 9 0.70 1.60 4 8 -9 2.40 1.90 4 8 -9 -0.10 1.10 3 -8 -9 25.00 2.60 3 -8 -9 29.30 2.70 -3 -8 9 30.20 2.40 -3 -8 9 26.90 2.80 -3 -8 9 25.90 2.80 -3 8 9 23.30 2.50 -3 8 9 30.30 3.10 3 8 -9 31.90 1.90 -3 8 9 26.60 2.60 -3 8 9 34.60 2.80 3 8 -9 27.80 2.80 -2 -8 9 3.70 1.60 2 -8 -9 4.50 1.60 -2 -8 9 5.50 1.10 -2 -8 9 4.80 1.80 2 -8 -9 7.40 1.90 -2 8 9 7.40 1.90 -2 8 9 6.10 1.70 -2 8 9 5.50 1.70 -2 8 9 5.20 1.70 2 8 -9 3.80 1.70 -1 -8 9 51.39 3.40 1 -8 -9 42.40 3.30 1 -8 -9 42.70 3.10 -1 -8 9 40.90 2.90 -1 -8 9 46.90 2.50 -1 8 9 45.00 3.20 1 8 -9 51.49 2.80 -1 8 9 45.10 3.30 -1 8 9 43.20 3.20 1 8 -9 48.70 3.40 0 -8 9 125.49 6.00 0 -8 -9 130.69 6.20 0 -8 -9 132.39 6.50 0 -8 9 123.69 6.30 0 -8 9 123.49 5.60 0 8 9 142.59 6.50 0 8 -9 122.99 6.40 0 8 9 129.79 6.60 0 8 9 121.69 6.20 0 8 -9 137.59 6.20 1 -8 9 19.70 1.40 -1 -8 -9 13.60 1.90 1 -8 9 17.60 2.20 -1 -8 -9 16.20 2.10 1 8 9 17.90 2.30 -1 8 -9 20.50 2.10 1 8 9 24.00 2.30 -2 -8 -9 5.10 2.10 2 -8 9 5.40 0.90 2 -8 9 3.10 1.60 -2 -8 -9 4.10 1.60 -2 8 -9 5.20 1.80 2 8 9 7.20 1.80 2 8 9 5.00 1.80 -3 -8 -9 151.18 7.80 -3 -8 -9 153.48 7.40 3 -8 9 153.98 7.40 3 -8 9 156.78 6.80 -3 8 -9 150.88 7.70 3 8 9 162.78 7.60 3 8 9 153.08 7.50 -4 -8 -9 22.60 3.10 4 -8 9 23.10 2.00 -4 -8 -9 25.00 2.60 4 8 9 23.10 2.70 -4 8 -9 19.90 2.90 4 8 9 26.30 3.00 5 -8 9 54.19 3.30 -5 -8 -9 60.79 4.70 5 8 9 55.49 4.30 -5 8 -9 41.60 4.40 -6 -8 -9 4.10 3.00 -6 -8 -9 4.30 2.10 6 -8 9 5.40 1.70 6 8 9 1.70 2.60 -6 8 -9 5.50 3.00 -7 -8 -9 1.00 2.30 -7 -8 -9 1.20 3.40 7 -8 9 2.70 2.00 7 8 9 0.00 2.80 -7 8 -9 3.70 3.90 -8 -8 -9 0.90 3.90 8 -8 9 4.20 2.50 -8 -8 -9 0.50 2.70 -8 8 -9 1.50 3.90 -10 -9 9 5.40 4.40 -10 9 9 2.90 5.10 -10 9 9 5.00 3.70 10 9 -9 3.00 3.70 -9 -9 9 5.50 3.70 9 9 -9 3.90 3.00 -9 9 9 5.20 3.80 -9 9 9 3.50 3.10 -8 -9 9 82.29 6.10 -8 9 9 70.49 5.70 8 9 -9 60.29 4.80 -8 9 9 69.59 5.20 -7 -9 9 18.50 3.10 -7 -9 9 20.00 3.20 -7 -9 9 22.30 3.50 7 -9 -9 24.30 3.40 -7 9 9 26.70 3.60 -7 9 9 20.30 3.10 7 9 -9 26.20 2.80 7 9 -9 18.10 3.40 6 -9 -9 38.20 3.60 -6 -9 9 31.40 3.20 -6 -9 9 44.40 4.30 -6 -9 9 40.90 3.80 -6 9 9 34.50 3.50 6 9 -9 36.40 3.60 -6 9 9 41.10 3.90 -6 9 9 43.80 3.90 6 9 -9 33.10 2.90 5 -9 -9 12.50 2.60 -5 -9 9 12.40 2.10 -5 -9 9 11.10 2.50 5 -9 -9 18.10 2.90 -5 -9 9 16.10 2.60 -5 9 9 14.80 2.30 5 9 -9 13.30 2.60 -5 9 9 17.20 2.40 -5 9 9 13.70 2.40 5 9 -9 13.80 1.70 4 -9 -9 132.69 6.60 -4 -9 9 127.29 6.60 -4 -9 9 129.79 6.50 -4 -9 9 122.59 6.10 4 -9 -9 125.89 6.60 -4 9 9 129.29 6.40 4 9 -9 115.69 6.50 -4 9 9 115.59 6.30 -4 9 9 135.29 6.50 4 9 -9 126.59 5.80 3 -9 -9 74.39 4.50 -3 -9 9 89.79 4.90 3 -9 -9 87.39 4.70 -3 -9 9 82.29 4.60 -3 -9 9 76.49 4.20 -3 9 9 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10 -1.10 1.70 4 -2 -10 -0.90 1.40 -4 -2 10 -0.40 1.40 4 -2 -10 0.40 1.60 -4 2 10 0.60 1.60 -4 2 10 0.20 1.60 4 2 -10 0.00 1.30 -4 2 10 -0.60 1.70 3 -2 -10 83.29 4.60 -3 -2 10 92.79 4.60 3 -2 -10 85.19 4.60 -3 -2 10 88.39 4.60 -3 -2 10 94.19 5.00 -3 2 10 82.19 4.70 -3 2 10 86.69 4.70 -3 2 10 86.69 4.90 3 2 -10 92.09 4.60 3 2 -10 92.29 4.50 -2 -2 10 139.09 6.80 2 -2 -10 129.39 6.40 -2 -2 10 144.59 6.50 2 -2 -10 131.69 6.50 2 2 -10 136.89 6.30 -2 2 10 145.79 6.60 2 2 -10 146.99 6.50 -2 2 10 138.69 6.80 -1 -2 10 0.80 1.00 1 -2 -10 -0.60 1.10 1 -2 -10 0.40 1.40 -1 -2 10 -0.20 1.40 1 2 -10 -1.20 1.40 -1 2 10 -1.00 1.10 -1 2 10 0.70 1.60 1 2 -10 -0.10 0.80 0 -2 -10 185.88 8.10 0 -2 10 187.48 8.50 0 -2 10 187.08 8.10 0 -2 -10 166.68 8.40 0 2 10 170.58 8.40 0 2 -10 181.28 7.70 0 2 -10 188.08 7.70 0 2 10 173.18 8.20 0 2 -10 187.38 8.40 -1 -2 -10 59.59 4.00 -1 -2 -10 67.19 3.50 1 -2 10 61.69 3.90 1 -2 10 67.39 3.50 -1 2 -10 69.39 2.90 -1 2 -10 58.79 3.90 1 2 10 68.59 4.00 1 2 10 67.19 3.70 2 -2 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3 -10 9.30 2.30 -7 3 10 10.80 2.90 -6 -3 10 58.59 4.20 -6 -3 10 59.89 4.30 6 -3 -10 55.69 4.30 -6 -3 10 62.79 4.40 -6 3 10 53.49 4.40 6 3 -10 55.29 3.90 -6 3 10 55.49 4.20 5 -3 -10 0.80 1.70 5 -3 -10 1.20 1.80 -5 -3 10 0.80 1.90 -5 -3 10 -1.10 1.80 -5 -3 10 0.30 2.20 -5 3 10 1.20 1.80 5 3 -10 -0.10 1.50 -5 3 10 0.40 1.80 -5 3 10 -0.20 1.80 -4 -3 10 109.79 5.80 -4 -3 10 110.19 5.70 4 -3 -10 108.39 5.70 4 -3 -10 115.89 5.70 -4 -3 10 115.09 6.20 -4 3 10 110.59 5.90 -4 3 10 107.59 5.60 -4 3 10 114.89 5.90 4 3 -10 117.99 5.50 -3 -3 10 154.78 7.00 -3 -3 10 155.38 7.00 -3 -3 10 142.49 7.30 3 -3 -10 147.69 7.20 3 -3 -10 148.29 7.10 3 3 -10 154.58 6.80 -3 3 10 146.09 7.20 -3 3 10 150.08 7.30 -2 -3 10 9.60 2.00 2 -3 -10 10.10 2.00 -2 -3 10 12.10 1.60 2 -3 -10 9.70 1.60 -2 3 10 11.40 2.10 2 3 -10 13.10 1.30 -2 3 10 9.70 1.60 2 3 -10 14.80 1.80 -1 -3 10 78.29 4.00 1 -3 -10 79.09 4.30 -1 -3 10 79.69 4.50 1 -3 -10 69.49 4.10 -1 3 10 83.09 4.20 1 3 -10 79.89 4.20 -1 3 10 78.99 4.50 1 3 -10 80.89 3.70 0 -3 10 191.28 9.40 0 -3 -10 199.88 9.50 0 -3 10 198.48 9.00 0 -3 -10 205.78 9.10 0 3 -10 201.58 9.40 0 3 -10 209.58 8.60 0 3 10 215.98 9.20 0 3 -10 212.28 8.60 0 3 10 214.98 9.50 -1 -3 -10 4.60 1.90 1 -3 10 3.20 1.10 -1 -3 -10 2.70 1.20 1 -3 10 2.70 1.80 1 3 10 4.70 1.80 -1 3 -10 3.40 1.70 1 3 10 2.50 1.30 -2 -3 -10 1.80 1.80 2 -3 10 0.80 1.60 -2 -3 -10 0.50 1.10 2 -3 10 0.30 1.10 2 3 10 -0.70 1.90 2 3 10 1.10 1.40 -2 3 -10 1.50 1.90 -3 -3 -10 -0.50 1.20 -3 -3 -10 0.90 2.10 3 -3 10 -1.60 1.10 3 -3 10 0.10 1.90 -3 3 -10 -0.30 1.90 3 3 10 0.00 1.80 3 3 10 1.20 1.50 -4 -3 -10 1.40 1.30 -4 -3 -10 3.30 2.40 4 -3 10 1.20 1.40 -4 3 -10 5.20 2.40 4 3 10 2.60 1.60 4 3 10 2.80 2.20 -5 -3 -10 3.40 1.50 -5 -3 -10 0.00 2.30 5 -3 10 3.00 1.60 -5 3 -10 0.30 2.50 5 3 10 0.30 1.90 6 -3 10 37.50 3.40 -6 -3 -10 41.30 2.90 -6 -3 -10 37.40 4.20 6 3 10 37.70 3.70 -6 3 -10 32.80 4.10 -7 -3 -10 0.90 1.70 -7 -3 -10 0.20 3.30 7 -3 10 0.00 2.10 7 3 10 1.10 2.60 -7 3 -10 -2.10 3.30 -8 -3 -10 5.50 4.40 -8 -3 -10 6.00 2.00 8 -3 10 4.70 2.90 8 3 10 3.50 3.30 -8 3 -10 6.30 4.20 -10 -4 10 47.60 5.90 -10 4 10 49.10 6.30 10 4 -10 49.80 5.40 -9 -4 10 31.00 4.50 9 4 -10 40.60 4.30 -9 4 10 39.60 5.10 -8 -4 10 23.50 4.10 -8 4 10 24.10 3.70 8 4 -10 19.60 3.20 -7 -4 10 12.00 3.00 -7 -4 10 10.20 3.20 7 -4 -10 8.60 2.70 -7 4 10 8.90 2.80 7 4 -10 9.80 2.20 -6 -4 10 142.29 7.40 -6 -4 10 150.98 7.60 -6 -4 10 148.29 7.40 6 -4 -10 139.89 7.40 -6 4 10 130.49 7.40 6 4 -10 139.19 7.00 -6 4 10 147.09 7.40 -5 -4 10 140.59 7.30 -5 -4 10 153.68 7.50 5 -4 -10 149.88 7.30 5 -4 -10 150.98 7.40 -5 -4 10 155.68 7.60 -5 4 10 161.58 9.20 -5 4 10 146.09 7.40 -5 4 10 147.39 7.40 5 4 -10 147.89 7.10 -4 -4 10 1487.85 61.59 -4 -4 10 1471.45 61.29 4 -4 -10 1488.05 61.39 4 -4 -10 1483.55 61.39 -4 4 10 1480.05 61.49 4 4 -10 1467.55 61.19 -4 4 10 1489.65 61.29 -4 4 10 1514.55 61.49 -3 -4 10 123.69 5.90 -3 -4 10 108.39 5.40 3 -4 -10 107.59 5.60 -3 -4 10 105.89 5.50 3 -4 -10 108.19 5.70 3 4 -10 120.19 5.30 -3 4 10 102.59 5.60 -3 4 10 109.09 5.90 -2 -4 10 94.79 5.20 2 -4 -10 97.29 5.20 -2 -4 10 97.29 4.80 2 4 -10 98.19 4.50 -2 4 10 95.69 5.00 -2 4 10 90.89 5.20 2 4 -10 104.99 4.80 1 -4 -10 21.50 2.10 -1 -4 10 19.30 1.90 -1 -4 10 21.80 2.40 1 -4 -10 24.40 2.40 -1 4 10 21.30 2.40 -1 4 10 22.00 2.10 1 4 -10 22.10 2.20 1 4 -10 22.90 1.40 1 4 -10 20.40 1.40 0 -4 10 133.59 6.40 0 -4 -10 120.39 6.00 0 -4 10 132.89 5.80 0 -4 -10 121.29 6.40 0 4 10 131.59 6.40 0 4 -10 121.19 6.20 0 4 10 125.19 6.10 1 -4 10 40.50 3.30 -1 -4 -10 42.00 2.70 -1 -4 -10 43.50 3.30 1 -4 10 41.10 2.50 -1 4 -10 43.60 3.10 1 4 10 39.50 2.90 1 4 10 34.50 3.10 -2 -4 -10 70.29 3.70 2 -4 10 62.39 3.50 2 -4 10 68.09 4.10 -2 -4 -10 66.69 4.30 -2 4 -10 67.49 4.20 2 4 10 64.99 4.10 2 4 10 70.59 3.90 3 -4 10 -0.40 1.80 -3 -4 -10 1.80 2.20 3 -4 10 0.30 1.10 -3 -4 -10 1.40 1.30 3 4 10 -0.20 1.70 -3 4 -10 1.70 2.00 3 4 10 1.30 1.50 -4 -4 -10 180.18 9.30 4 -4 10 174.98 8.40 -4 -4 -10 200.38 8.60 4 4 10 188.28 8.80 -4 4 -10 195.08 9.30 4 4 10 193.48 9.10 5 -4 10 16.70 2.00 -5 -4 -10 12.00 3.10 -5 -4 -10 16.80 2.00 5 4 10 13.60 2.50 -5 4 -10 22.00 3.40 -6 -4 -10 2.80 3.00 6 -4 10 1.00 1.80 -6 -4 -10 -0.10 1.60 -6 4 -10 3.60 2.80 6 4 10 2.50 2.30 -7 -4 -10 -1.10 3.40 7 -4 10 0.10 2.30 -7 -4 -10 2.80 1.90 -7 4 -10 4.00 3.50 7 4 10 0.20 2.60 8 -4 10 43.10 3.90 -8 -4 -10 30.80 3.10 -8 -4 -10 31.90 5.20 -8 4 -10 33.10 5.10 8 4 10 34.00 4.40 -10 -5 10 20.00 4.90 10 5 -10 20.70 4.20 -10 5 10 15.90 4.80 -10 5 10 18.90 4.40 -9 -5 10 101.59 7.00 -9 5 10 94.19 6.90 -9 5 10 87.09 6.30 9 5 -10 86.79 6.20 -8 -5 10 150.58 8.70 8 5 -10 159.08 8.20 -8 5 10 170.28 8.80 -7 -5 10 10.90 2.80 -7 -5 10 13.30 3.10 7 -5 -10 10.60 3.00 -7 -5 10 12.00 3.20 7 5 -10 8.20 2.10 -7 5 10 14.60 3.20 -6 -5 10 10.10 2.60 -6 -5 10 8.00 2.60 -6 -5 10 6.00 2.40 6 -5 -10 3.30 2.30 -6 5 10 5.50 2.30 6 5 -10 2.70 1.80 -6 5 10 4.50 2.40 -5 -5 10 130.59 6.90 5 -5 -10 120.19 6.50 -5 -5 10 120.89 6.40 5 -5 -10 142.39 6.80 -5 -5 10 145.89 6.90 -5 5 10 124.39 6.70 5 5 -10 123.09 6.20 -5 5 10 118.19 6.60 -4 -5 10 -2.30 2.10 -4 -5 10 1.00 1.60 4 -5 -10 2.70 1.70 4 -5 -10 3.30 1.90 -4 -5 10 1.70 2.00 -4 5 10 0.90 1.70 -4 5 10 0.90 1.80 -4 5 10 0.10 2.00 4 5 -10 3.20 1.30 -3 -5 10 402.06 17.20 -3 -5 10 398.66 17.10 -3 -5 10 408.36 17.50 3 -5 -10 396.96 17.40 3 -5 -10 397.86 17.30 -3 5 10 391.36 17.40 3 5 -10 407.66 16.90 -3 5 10 410.66 17.30 -2 -5 10 0.50 1.50 -2 -5 10 -0.70 1.70 2 -5 -10 -1.10 1.70 -2 -5 10 0.00 1.10 2 -5 -10 1.10 1.30 -2 5 10 -1.40 1.50 -2 5 10 -0.40 1.50 2 5 -10 -0.20 0.80 1 -5 -10 179.28 8.70 -1 -5 10 192.98 8.30 -1 -5 10 186.28 8.80 1 -5 -10 174.88 8.50 1 5 -10 184.88 8.50 -1 5 10 201.68 8.60 -1 5 10 198.38 8.80 0 -5 10 99.69 5.10 0 -5 10 92.19 4.40 0 -5 -10 91.99 4.70 0 -5 -10 84.99 5.00 0 5 10 89.59 4.80 0 5 10 97.39 5.20 0 5 -10 98.19 4.80 -1 -5 -10 56.79 3.30 1 -5 10 54.69 3.00 -1 -5 -10 58.09 3.80 1 -5 10 52.89 3.80 -1 5 -10 61.49 3.80 1 5 10 55.19 3.40 1 5 10 52.69 3.70 -2 -5 -10 158.68 7.30 -2 -5 -10 147.39 6.70 2 -5 10 123.09 6.90 2 -5 10 138.79 6.40 2 5 10 143.39 6.80 -2 5 -10 138.29 7.10 2 5 10 153.28 7.10 3 -5 10 14.50 2.40 3 -5 10 13.10 1.60 -3 -5 -10 15.00 2.70 -3 -5 -10 15.40 1.90 -3 5 -10 19.20 2.70 3 5 10 16.50 2.20 3 5 10 13.60 2.50 -4 -5 -10 123.69 7.20 4 -5 10 129.59 6.20 -4 -5 -10 137.89 6.40 4 5 10 137.49 6.80 -4 5 -10 129.29 7.10 4 5 10 134.19 6.70 5 -5 10 4.90 1.60 -5 -5 -10 4.70 2.60 -5 -5 -10 4.60 1.70 5 5 10 3.60 2.20 -5 5 -10 5.50 2.60 -6 -5 -10 35.70 4.20 6 -5 10 31.80 2.90 -6 -5 -10 31.50 3.00 -6 5 -10 28.60 4.00 6 5 10 30.60 3.30 -7 -5 -10 18.10 2.50 7 -5 10 16.40 2.80 -7 -5 -10 17.80 4.00 -7 5 -10 13.20 3.90 7 5 10 19.30 3.30 8 -5 10 27.30 3.40 -8 -5 -10 22.10 2.90 -8 -5 -10 31.40 5.10 8 5 10 28.20 4.40 -8 5 -10 21.30 4.80 -10 -6 10 5.10 4.50 10 6 -10 6.90 4.00 -10 6 10 5.70 4.60 -10 6 10 11.20 4.30 -9 -6 10 104.69 7.30 9 6 -10 88.59 6.50 -9 6 10 106.39 7.20 -9 6 10 96.49 6.90 -8 -6 10 1.80 3.00 8 6 -10 4.20 2.50 -8 6 10 2.00 2.90 -8 6 10 6.30 3.50 -7 -6 10 18.80 3.00 -7 -6 10 22.30 3.20 -7 -6 10 21.30 3.40 -7 6 10 20.40 3.40 7 6 -10 15.40 2.40 -7 6 10 15.70 3.10 -6 -6 10 238.88 11.30 6 -6 -10 231.48 11.00 -6 -6 10 237.88 11.20 6 -6 -10 243.48 11.40 -6 -6 10 245.68 11.50 6 6 -10 232.68 10.80 -6 6 10 252.27 11.40 -6 6 10 243.48 11.40 -6 6 10 244.58 11.20 5 -6 -10 118.19 6.30 -5 -6 10 120.79 6.50 -5 -6 10 113.89 6.60 5 -6 -10 117.59 6.40 -5 -6 10 121.89 6.10 5 6 -10 118.49 5.80 -5 6 10 115.39 6.30 -5 6 10 108.29 6.00 -5 6 10 116.09 6.40 -4 -6 10 39.50 3.40 4 -6 -10 38.10 3.40 -4 -6 10 33.70 2.90 4 -6 -10 31.60 3.10 -4 -6 10 32.60 3.20 -4 6 10 36.20 3.10 -4 6 10 33.10 4.50 -4 6 10 29.50 3.00 4 6 -10 32.30 2.50 -4 6 10 36.20 3.20 -3 -6 10 366.16 15.60 3 -6 -10 355.96 15.80 -3 -6 10 360.46 15.90 -3 -6 10 368.16 15.50 3 -6 -10 350.66 15.70 -3 6 10 374.46 15.80 -3 6 10 359.96 15.80 3 6 -10 359.26 15.20 -2 -6 10 15.80 1.70 2 -6 -10 17.20 2.10 2 -6 -10 15.00 2.20 -2 -6 10 19.30 2.10 -2 -6 10 18.20 2.40 -2 6 10 16.60 2.30 -2 6 10 18.50 2.20 2 6 -10 19.60 1.40 2 6 -10 16.60 1.40 -1 -6 10 11.60 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28.60 3.10 -7 -6 -10 33.70 3.10 -7 -6 -10 27.60 4.40 7 6 10 33.60 4.00 -7 6 -10 22.00 4.70 -8 -6 -10 25.70 3.00 -8 -6 -10 25.80 4.90 8 -6 10 24.80 3.40 8 6 10 27.30 4.50 -8 6 -10 19.30 4.70 -10 -7 10 19.10 5.60 -10 7 10 19.30 4.50 -10 7 10 20.70 5.10 10 7 -10 12.20 4.10 -9 -7 10 49.80 5.60 9 7 -10 33.40 4.10 -9 7 10 43.70 5.40 -9 7 10 33.40 4.40 -8 -7 10 17.80 3.60 -8 7 10 15.00 3.80 8 7 -10 11.60 2.70 -8 7 10 14.90 3.20 -7 -7 10 0.20 2.60 -7 -7 10 -1.10 2.90 -7 -7 10 -2.50 2.60 -7 7 10 0.30 2.60 7 7 -10 2.10 1.90 -7 7 10 0.60 2.80 -6 -7 10 39.30 3.80 -6 -7 10 40.60 4.30 6 -7 -10 41.80 3.90 -6 -7 10 45.10 4.00 6 -7 -10 43.90 4.00 -6 7 10 37.30 3.70 -6 7 10 37.60 3.60 6 7 -10 38.80 3.10 -6 7 10 45.00 4.20 -5 -7 10 679.23 29.50 -5 -7 10 670.83 29.70 5 -7 -10 710.53 29.70 -5 -7 10 715.03 29.80 5 -7 -10 726.93 29.70 -5 7 10 704.53 29.70 -5 7 10 696.93 29.60 -5 7 10 743.63 29.80 5 7 -10 661.13 29.30 -4 -7 10 1.10 2.00 4 -7 -10 2.30 2.00 -4 -7 10 2.00 1.50 -4 -7 10 0.20 2.00 4 -7 -10 1.00 1.80 4 7 -10 1.70 1.20 -4 7 10 -0.20 1.90 -4 7 10 2.00 1.90 -4 7 10 1.40 1.80 4 7 -10 0.60 2.00 -3 -7 10 61.99 3.60 3 -7 -10 61.69 3.90 3 -7 -10 58.39 3.90 -3 -7 10 58.59 3.90 -3 -7 10 55.79 4.10 3 7 -10 67.69 3.20 -3 7 10 53.69 3.90 -3 7 10 65.79 4.30 -3 7 10 57.09 3.90 3 7 -10 66.19 4.20 2 -7 -10 2.60 1.50 -2 -7 10 2.80 1.90 -2 -7 10 4.60 1.20 2 -7 -10 3.30 2.00 -2 -7 10 4.70 1.70 2 7 -10 5.80 0.60 -2 7 10 5.60 1.60 2 7 -10 6.60 0.70 -2 7 10 4.60 1.80 1 -7 -10 92.49 5.40 1 -7 -10 109.89 5.70 -1 -7 10 113.19 5.80 -1 -7 10 117.59 5.10 -1 7 10 105.99 5.50 -1 7 10 107.69 5.80 1 7 -10 110.79 5.40 0 -7 10 46.90 3.70 0 -7 10 43.50 2.50 0 -7 -10 39.90 2.90 0 -7 -10 46.90 3.40 0 7 10 42.80 3.10 0 7 -10 43.60 3.10 0 7 10 39.70 3.30 1 -7 10 193.58 8.30 1 -7 10 190.48 9.10 -1 -7 -10 195.88 8.80 -1 -7 -10 189.08 9.10 1 7 10 198.08 9.10 1 7 10 191.18 8.80 -1 7 -10 185.68 8.80 -2 -7 -10 107.09 6.10 2 -7 10 113.79 5.90 -2 -7 -10 113.99 5.60 2 -7 10 109.59 5.00 2 7 10 110.69 5.90 2 7 10 102.69 5.70 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14 185.58 9.40 -2 -2 14 22.70 3.30 2 -2 -14 20.60 3.20 2 -2 -14 23.40 2.40 -2 -2 14 16.50 2.40 -2 2 14 21.80 2.70 -2 2 14 19.00 3.10 2 2 -14 23.50 2.20 -1 -2 14 8.20 2.00 1 -2 -14 7.20 2.60 -1 -2 14 5.90 2.60 1 -2 -14 6.70 1.70 1 2 -14 5.80 1.20 -1 2 14 3.30 2.10 -1 2 14 4.20 2.60 0 -2 -14 58.79 3.60 0 -2 14 60.29 4.70 0 -2 -14 62.79 4.70 0 -2 14 63.79 4.10 0 2 14 58.19 5.10 0 2 14 53.89 4.20 0 2 -14 66.09 5.00 -1 -2 -14 1.50 2.60 1 -2 14 1.20 2.60 -1 -2 -14 -0.40 1.30 1 -2 14 -2.00 1.80 -1 2 -14 0.10 2.60 1 2 14 0.00 1.90 1 2 14 -2.40 2.70 2 -2 14 47.10 3.70 2 -2 14 59.89 4.70 -2 -2 -14 46.20 4.80 -2 -2 -14 55.29 3.10 2 2 14 46.40 4.20 2 2 14 46.80 4.70 -2 2 -14 50.79 4.70 -3 -2 -14 0.30 1.10 3 -2 14 -1.80 2.00 3 -2 14 1.40 3.20 -3 -2 -14 1.30 3.00 3 2 14 -1.60 2.20 3 2 14 -1.20 2.80 -3 2 -14 -1.10 2.90 4 -2 14 8.60 2.40 -4 -2 -14 5.10 3.50 -4 2 -14 4.60 3.60 4 2 14 6.50 2.60 -5 -2 -14 1.30 3.90 5 -2 14 7.50 2.70 5 2 14 8.70 3.10 -5 2 -14 7.00 4.00 6 2 14 1.90 3.40 8 -3 -14 5.30 3.60 8 3 -14 5.40 3.20 -7 -3 14 26.20 4.70 7 -3 -14 23.10 3.90 7 3 -14 16.40 3.20 -7 3 14 20.40 4.40 -6 -3 14 20.60 3.90 -6 -3 14 19.50 3.70 6 -3 -14 22.10 3.30 6 3 -14 20.80 2.80 -6 3 14 22.10 3.80 -5 -3 14 -1.50 2.80 5 -3 -14 0.90 2.20 -5 -3 14 0.90 2.60 -5 3 14 0.50 2.70 5 3 -14 0.60 1.90 -4 -3 14 70.29 5.50 -4 -3 14 81.49 5.00 -4 3 14 69.99 5.40 4 3 -14 78.09 4.30 -4 3 14 64.39 5.30 -3 -3 14 -0.90 2.50 3 -3 -14 0.50 1.80 -3 -3 14 -1.40 1.90 3 3 -14 0.90 1.50 -3 3 14 -1.40 2.50 -3 3 14 1.00 2.30 2 -3 -14 2.30 2.50 -2 -3 14 1.90 1.90 2 -3 -14 0.70 1.80 -2 -3 14 0.80 2.50 2 3 -14 2.70 1.20 -2 3 14 2.90 2.60 -2 3 14 3.10 2.20 -1 -3 14 31.80 2.80 -1 -3 14 27.20 3.60 1 -3 -14 33.20 3.80 1 -3 -14 31.00 2.90 -1 3 14 28.20 3.50 1 3 -14 28.90 1.60 -1 3 14 28.60 3.00 0 -3 -14 88.49 4.80 0 -3 -14 95.99 5.80 0 -3 14 96.39 5.10 0 -3 14 93.29 5.80 0 3 -14 89.29 5.60 0 3 14 88.99 5.40 0 3 14 89.69 5.80 -1 -3 -14 40.60 4.10 1 -3 14 42.90 3.50 1 -3 14 45.90 4.30 -1 -3 -14 39.90 3.00 1 3 14 40.60 3.70 1 3 14 42.50 4.30 -1 3 -14 45.30 4.30 -2 -3 -14 58.19 5.00 2 -3 14 56.39 5.20 -2 -3 -14 57.89 3.40 2 -3 14 55.89 3.90 -2 3 -14 58.79 4.90 2 3 14 55.19 4.50 2 3 14 59.59 5.00 -3 -3 -14 -0.30 1.40 -3 -3 -14 2.40 3.20 3 -3 14 2.00 3.20 3 -3 14 1.90 2.00 -3 3 -14 1.80 3.10 3 3 14 0.10 3.20 3 3 14 1.70 2.40 -4 -3 -14 1.30 1.40 4 -3 14 2.50 2.20 -4 -3 -14 1.20 3.60 -4 3 -14 2.10 3.40 4 3 14 2.10 2.60 -5 -3 -14 -0.10 4.30 5 -3 14 2.60 2.60 5 3 14 1.00 3.00 -5 3 -14 -2.50 3.80 6 3 14 56.39 5.20 8 -4 -14 19.10 4.10 8 4 -14 14.10 3.50 -7 -4 14 2.90 3.70 7 -4 -14 1.70 3.30 -7 4 14 5.30 5.30 7 4 -14 2.40 2.70 -6 -4 14 76.19 5.70 6 -4 -14 59.19 5.30 -6 -4 14 74.59 6.50 6 4 -14 71.39 4.70 -6 4 14 76.39 5.70 5 -4 -14 0.50 2.30 -5 -4 14 4.70 2.60 -5 -4 14 2.50 3.00 5 4 -14 0.40 1.80 -5 4 14 3.50 2.90 -4 -4 14 32.10 3.20 4 -4 -14 37.00 3.50 -4 -4 14 27.80 3.80 -4 4 14 27.50 3.50 -4 4 14 28.50 3.70 4 4 -14 32.50 2.80 -3 -4 14 13.30 2.30 3 -4 -14 16.80 2.50 3 -4 -14 13.30 3.50 -3 -4 14 13.80 3.20 3 4 -14 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3.60 8 -5 -14 45.40 5.20 8 5 -14 41.60 4.30 7 -5 -14 40.10 4.60 -7 -5 14 39.30 4.90 7 5 -14 29.20 3.50 6 -5 -14 2.20 2.70 -6 -5 14 0.30 2.80 -6 -5 14 -0.50 3.50 6 5 -14 3.10 2.10 -6 5 14 0.00 3.10 -5 -5 14 0.60 2.90 -5 -5 14 0.70 2.60 5 -5 -14 -0.60 2.40 -5 5 14 0.40 2.80 5 5 -14 -0.60 1.70 4 -5 -14 28.70 3.20 -4 -5 14 32.20 3.20 -4 -5 14 28.30 3.80 4 5 -14 35.00 2.70 -4 5 14 38.20 4.10 -3 -5 14 -0.10 2.60 3 -5 -14 -0.40 2.80 3 -5 -14 0.50 2.00 -3 -5 14 3.60 2.00 3 5 -14 1.70 1.20 -3 5 14 -1.30 2.50 -3 5 14 -0.70 2.60 -2 -5 14 -1.30 1.80 2 -5 -14 0.10 2.80 -2 -5 14 0.20 2.60 2 -5 -14 0.80 2.00 -2 5 14 1.30 2.20 -2 5 14 2.10 2.60 -1 -5 14 5.00 1.80 -1 -5 14 6.40 3.10 1 -5 -14 6.30 3.00 1 -5 -14 7.30 2.00 -1 5 14 8.30 2.80 -1 5 14 4.20 2.50 0 -5 -14 17.90 2.30 0 -5 14 16.00 3.10 0 -5 -14 13.00 3.10 0 -5 14 13.90 2.10 0 5 14 20.10 3.20 0 5 14 13.80 2.70 -1 -5 -14 4.60 1.80 1 -5 14 3.00 2.70 1 -5 14 5.40 1.80 -1 -5 -14 4.70 2.80 1 5 14 3.50 2.40 1 5 14 2.10 2.70 -1 5 -14 3.10 3.00 2 -5 14 88.59 4.80 -2 -5 -14 87.49 6.00 2 -5 14 95.49 5.90 -2 -5 -14 80.49 4.80 2 5 14 93.99 5.60 -2 5 -14 77.49 5.80 2 5 14 84.19 5.80 -3 -5 -14 3.90 1.90 -3 -5 -14 5.30 3.40 3 -5 14 3.40 2.00 3 5 14 4.00 2.60 -3 5 -14 4.30 3.20 3 5 14 2.00 2.90 -4 -5 -14 3.10 1.80 4 -5 14 3.30 2.20 -4 -5 -14 2.70 3.70 -4 5 -14 6.20 3.70 4 5 14 1.70 2.70 5 -5 14 10.40 2.70 -5 -5 -14 12.00 4.40 -5 -5 -14 10.90 2.10 -5 5 -14 8.70 4.70 5 5 14 12.20 3.50 8 -6 -14 17.20 4.70 8 6 -14 10.30 3.20 -7 -6 14 34.20 4.70 -7 -6 14 35.30 4.50 7 -6 -14 31.90 4.40 7 6 -14 29.90 3.40 -6 -6 14 -0.20 3.70 -6 -6 14 -0.60 2.90 6 -6 -14 -1.90 2.70 -6 6 14 0.40 3.20 6 6 -14 0.40 2.00 -5 -6 14 19.90 3.70 5 -6 -14 19.30 3.30 -5 -6 14 23.40 3.10 5 6 -14 17.30 2.20 -5 6 14 17.00 3.40 -4 -6 14 -2.00 2.10 4 -6 -14 0.20 2.10 -4 -6 14 0.60 2.80 4 6 -14 0.40 1.40 -4 6 14 1.50 2.80 3 -6 -14 66.89 5.30 -3 -6 14 64.99 4.50 3 -6 -14 66.29 4.70 -3 -6 14 77.99 5.40 3 6 -14 70.39 3.40 -3 6 14 76.59 5.30 -3 6 14 69.89 5.20 2 -6 -14 18.60 2.70 -2 -6 14 19.60 3.20 2 -6 -14 18.50 3.20 -2 -6 14 18.20 2.30 -2 6 14 16.50 3.10 -2 6 14 11.20 2.80 1 -6 -14 3.60 2.70 1 -6 -14 2.90 1.90 -1 -6 14 2.10 1.70 -1 -6 14 2.50 2.90 -1 6 14 0.30 2.60 -1 6 14 1.10 2.40 0 -6 -14 16.90 3.50 0 -6 14 22.00 2.30 0 -6 -14 14.30 2.30 0 -6 14 16.80 3.20 0 6 14 23.10 3.40 0 6 14 15.70 2.80 1 -6 14 33.70 3.80 -1 -6 -14 18.80 3.40 -1 -6 -14 27.40 2.70 1 -6 14 24.20 2.40 1 6 14 27.20 3.10 1 6 14 23.60 3.50 -1 6 -14 20.80 3.30 2 -6 14 11.20 3.10 -2 -6 -14 8.50 2.00 -2 -6 -14 8.30 3.20 2 -6 14 10.40 1.90 2 6 14 12.10 2.90 -2 6 -14 8.10 3.50 2 6 14 7.70 3.40 -3 -6 -14 68.39 6.40 -3 -6 -14 67.99 4.50 3 -6 14 69.29 4.40 3 6 14 88.89 6.10 -3 6 -14 62.99 5.60 3 6 14 68.59 5.20 -4 -6 -14 3.40 2.10 4 -6 14 3.30 2.20 -4 -6 -14 5.20 3.80 4 6 14 4.10 3.00 -4 6 -14 2.00 4.10 5 -6 14 29.80 3.30 -5 -6 -14 29.70 5.20 -5 -6 -14 29.40 2.90 5 6 14 30.40 4.20 -5 6 -14 23.40 5.20 8 7 -14 -0.40 2.90 -7 -7 14 0.70 3.40 7 -7 -14 1.10 3.60 -7 -7 14 -0.40 4.20 7 7 -14 0.60 2.40 -6 -7 14 28.00 3.90 -6 -7 14 32.60 4.40 6 -7 -14 31.00 4.00 6 7 -14 30.30 3.00 -6 7 14 35.30 4.30 -5 -7 14 19.20 4.00 5 -7 -14 14.10 3.20 -5 -7 14 16.90 2.90 -5 7 14 16.00 3.80 5 7 -14 14.40 2.00 4 -7 -14 -1.10 2.30 4 -7 -14 0.90 3.10 -4 -7 14 0.20 2.20 -4 -7 14 3.50 2.90 -4 7 14 -0.20 2.80 4 7 -14 -0.20 1.30 -3 -7 14 41.60 3.60 -3 -7 14 33.80 4.10 3 -7 -14 44.60 4.40 3 -7 -14 44.60 4.00 -3 7 14 39.10 4.20 2 -7 -14 -0.70 2.10 -2 -7 14 -0.40 2.50 -2 -7 14 -0.20 1.70 2 -7 -14 -1.80 2.60 -2 7 14 -0.40 2.60 -2 7 14 1.70 2.60 1 -7 -14 9.70 3.30 -1 -7 14 7.80 2.80 1 -7 -14 12.50 2.30 -1 -7 14 10.70 2.00 -1 7 14 7.80 2.90 -1 7 14 13.40 2.80 0 -7 14 2.30 2.70 0 -7 14 0.50 1.50 0 -7 -14 -0.10 2.60 0 -7 -14 1.90 2.00 0 7 14 3.20 2.70 0 7 14 3.30 2.40 -1 -7 -14 4.60 2.00 1 -7 14 3.50 1.60 -1 -7 -14 4.00 2.80 1 -7 14 3.10 2.80 1 7 14 2.90 3.10 1 7 14 2.70 2.60 -2 -7 -14 2.60 2.00 2 -7 14 2.60 1.60 -2 -7 -14 4.30 3.10 2 -7 14 2.50 2.90 -2 7 -14 9.40 3.10 2 7 14 1.30 2.90 2 7 14 4.40 2.80 -3 -7 -14 3.00 3.40 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301.87 13.50 0 -8 14 322.97 14.60 0 -8 -14 296.87 14.60 0 -8 -14 304.07 13.90 0 8 14 335.97 14.20 0 8 14 305.97 14.40 1 -8 14 211.68 9.40 -1 -8 -14 199.38 9.70 1 -8 14 218.78 10.70 -1 -8 -14 192.28 10.40 1 8 14 197.68 10.30 1 8 14 216.08 10.20 -2 -8 -14 40.10 3.60 2 -8 14 47.40 4.70 -2 -8 -14 37.80 4.40 2 -8 14 43.50 3.30 -2 8 -14 27.40 4.30 2 8 14 46.20 4.70 2 8 14 36.60 3.90 3 -8 14 31.40 2.80 -3 -8 -14 31.30 3.10 -3 -8 -14 30.40 4.50 3 8 14 30.90 4.10 3 8 14 25.00 3.60 -3 8 -14 27.90 4.20 -4 -8 -14 11.60 2.70 4 -8 14 15.00 2.40 -4 -8 -14 12.10 4.60 4 8 14 11.90 3.60 4 8 14 11.60 4.90 -4 8 -14 12.50 4.50 -5 -8 -14 3.20 4.30 -5 -8 -14 4.80 2.60 5 -8 14 4.00 2.50 5 8 14 8.70 4.00 -5 8 -14 2.90 4.80 -8 -9 14 1.10 5.20 -7 -9 14 7.70 3.70 -7 -9 14 7.10 4.60 7 9 -14 3.90 2.40 -6 -9 14 2.40 3.60 6 -9 -14 3.60 3.40 -6 -9 14 1.10 3.10 -6 9 14 2.40 3.40 6 9 -14 1.40 1.90 5 -9 -14 69.19 5.60 -5 -9 14 78.69 6.50 -5 -9 14 69.29 5.30 5 9 -14 67.99 3.80 -5 9 14 67.79 6.10 4 -9 -14 -0.50 2.40 -4 -9 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16.10 4.60 0 -9 -17 2.80 2.90 0 -9 17 1.80 2.50 0 -9 -17 1.30 4.60 0 -9 17 -0.10 4.30 0 9 17 5.60 4.20 -1 -9 -17 12.40 4.70 -1 -9 -17 12.00 5.30 1 -9 17 17.50 5.40 1 -9 17 9.10 3.10 1 9 17 22.30 5.40 4 -10 -17 101.19 7.50 -4 -10 17 104.29 7.00 -4 10 17 112.29 8.10 3 -10 -17 29.90 4.30 -3 -10 17 17.50 4.80 -3 -10 17 19.60 3.40 -3 10 17 22.00 5.30 2 -10 -17 2.20 3.30 -2 -10 17 1.30 4.80 2 -10 -17 1.20 4.70 -2 -10 17 0.10 2.70 -2 10 17 3.40 4.00 1 -10 -17 37.60 5.40 -1 -10 17 36.00 3.70 -1 -10 17 48.10 5.70 1 -10 -17 37.70 4.30 -1 10 17 49.10 5.60 0 -10 17 6.10 4.60 0 -10 -17 6.20 3.20 0 -10 17 4.10 2.60 0 -10 -17 5.40 4.50 0 10 17 5.50 4.30 1 -10 17 -1.80 5.10 -1 -10 -17 1.10 4.30 1 10 17 2.10 4.40 4 -11 -17 121.79 8.10 -4 11 17 107.79 9.30 -3 -11 17 5.50 3.10 3 -11 -17 9.40 4.60 3 -11 -17 11.50 4.00 -3 -11 17 8.00 5.20 -3 11 17 10.90 4.50 2 -11 -17 15.50 3.80 2 -11 -17 11.80 5.20 -2 -11 17 17.30 3.20 -2 -11 17 16.40 4.70 -2 11 17 17.50 4.50 -1 -11 17 8.00 4.60 1 -11 -17 7.90 4.50 -1 -11 17 10.10 2.80 1 -11 -17 10.50 3.60 -1 11 17 11.60 4.50 0 -11 -17 5.20 4.30 0 -11 -17 7.20 4.80 0 -11 17 9.30 4.80 0 11 17 7.10 5.00 3 -12 -17 2.30 5.10 3 -12 -17 -0.30 3.80 2 -12 -17 9.10 5.30 2 -12 -17 16.80 4.00 -2 -12 17 14.30 5.60 1 -12 -17 3.30 3.90 -1 -12 17 3.70 4.40 1 -12 -17 2.00 4.60 -4 0 18 99.69 7.80 4 0 -18 90.39 5.70 -4 0 18 118.29 7.80 -3 0 18 -1.40 4.60 -3 0 18 -0.90 3.50 3 0 -18 1.30 2.20 -2 0 18 7.20 4.30 2 0 -18 3.50 1.80 -2 0 18 1.40 3.30 -1 0 18 0.70 3.30 -1 0 18 2.20 4.20 0 0 18 -0.10 4.40 0 0 18 -1.70 3.00 1 0 18 -1.50 5.00 1 0 18 1.40 3.50 -4 -1 18 0.30 4.80 4 -1 -18 0.60 3.80 -4 -1 18 -1.90 3.80 4 1 -18 -0.60 2.20 -4 1 18 2.40 4.00 -4 1 18 3.00 4.40 -3 -1 18 -0.80 3.50 3 -1 -18 -0.40 2.30 -3 -1 18 1.00 4.10 3 1 -18 0.50 2.00 -3 1 18 -3.10 4.10 -3 1 18 1.10 3.60 -2 -1 18 1.50 3.30 2 -1 -18 3.00 2.00 -2 -1 18 2.90 4.20 -2 1 18 1.00 3.30 -2 1 18 4.00 4.30 -1 -1 18 3.30 3.40 -1 -1 18 1.00 4.20 1 -1 -18 2.90 1.70 -1 1 18 4.10 4.80 -1 1 18 1.50 3.40 0 -1 18 56.09 5.30 0 -1 18 49.60 6.30 0 1 18 60.29 6.50 0 1 18 45.10 4.80 1 -1 18 3.70 4.60 1 -1 18 13.30 5.10 1 1 18 9.30 3.60 1 1 18 11.10 4.90 -4 -2 18 16.20 5.60 -4 -2 18 17.10 4.20 -4 2 18 10.00 5.10 4 2 -18 14.60 2.40 -3 -2 18 1.70 3.50 -3 -2 18 2.80 4.20 3 -2 -18 2.50 2.40 3 2 -18 0.70 1.60 -3 2 18 2.10 4.20 -3 2 18 2.80 3.70 -2 -2 18 7.80 4.90 -2 -2 18 15.10 3.60 2 -2 -18 7.30 2.40 -2 2 18 8.30 3.90 -2 2 18 9.70 4.60 1 -2 -18 1.60 1.90 -1 -2 18 7.70 4.40 -1 -2 18 2.80 3.00 -1 2 18 4.10 3.70 -1 2 18 0.40 4.30 0 -2 18 9.30 4.60 0 -2 18 10.10 3.40 0 2 18 7.80 4.50 0 2 18 12.70 3.70 1 -2 18 1.40 5.10 1 2 18 0.80 3.50 1 2 18 -1.00 5.10 -4 -3 18 8.50 3.80 4 3 -18 11.70 2.20 -3 -3 18 9.90 3.70 -3 -3 18 10.70 4.50 3 -3 -18 11.00 2.80 -3 3 18 5.00 4.70 -3 3 18 11.10 4.10 -2 -3 18 1.40 3.20 -2 -3 18 0.80 4.30 2 -3 -18 1.10 2.40 -2 3 18 -1.00 3.60 -2 3 18 -1.00 4.10 1 -3 -18 5.90 2.30 -1 -3 18 4.40 4.30 -1 -3 18 3.20 3.00 -1 3 18 6.00 3.80 -1 3 18 4.10 4.30 0 -3 -18 11.80 2.20 0 -3 18 10.40 4.50 0 -3 18 11.30 3.40 0 3 18 16.70 4.90 0 3 18 14.80 3.90 -4 -4 18 3.20 3.60 -3 -4 18 10.60 5.10 3 -4 -18 10.40 3.10 -3 -4 18 15.40 3.70 -3 4 18 14.10 5.10 2 -4 -18 1.30 2.50 -2 -4 18 -0.50 4.20 -2 -4 18 -0.60 3.20 -2 4 18 -0.30 4.80 -2 4 18 1.50 3.90 -1 -4 18 15.60 3.30 1 -4 -18 11.60 2.50 -1 -4 18 14.10 4.90 -1 4 18 11.70 3.90 -1 4 18 30.30 5.60 0 -4 -18 83.59 5.00 0 -4 18 87.19 8.40 0 -4 18 75.79 6.20 0 -4 -18 87.59 10.80 0 4 18 81.79 6.80 0 4 18 89.29 8.30 -4 -5 18 4.30 3.60 -3 -5 18 3.60 5.10 -3 -5 18 1.00 3.20 -3 5 18 0.30 4.90 -2 -5 18 13.20 3.40 2 -5 -18 17.90 3.10 -2 -5 18 17.70 5.30 -2 5 18 16.10 4.70 -1 -5 18 27.70 5.20 -1 -5 18 27.90 3.70 1 -5 -18 20.00 3.00 -1 5 18 29.30 5.20 -1 5 18 25.70 4.50 0 -5 18 2.80 4.70 0 -5 -18 1.50 2.30 0 -5 -18 2.70 5.00 0 5 18 1.30 4.40 0 5 18 2.00 3.70 -3 -6 18 2.20 3.20 -2 -6 18 -2.80 5.30 -2 -6 18 -0.90 2.90 -2 6 18 -0.90 4.90 -1 -6 18 1.90 3.20 -1 -6 18 2.80 4.40 -1 6 18 5.00 5.20 0 -6 18 7.40 4.80 0 -6 -18 6.10 5.20 0 6 18 6.80 4.10 1 -7 -18 8.70 5.20 -1 -7 18 7.90 5.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 13237 _shelx_res_file ; TITL SKM282_0m_a.res in P2(1)/n SKM282_0m_a.res created by SHELXL-2018/3 at 15:50:54 on 17-Mar-2020 REM Old TITL SKM282_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.129, Rweak 0.004, Alpha 0.017, Orientation as input REM Formula found by SHELXT: C29 N4 O3 S CELL 0.71073 8.4506 23.1123 13.6006 90.000 99.021 90.000 ZERR 4.000 0.0016 0.0045 0.0026 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O S UNIT 116 116 12 16 4 TEMP -123 SIZE 0.138 0.251 0.386 L.S. 5 BOND $H LIST 4 FMAP 2 PLAN 5 MPLA C10 > C15 MPLA N1 C5 > C9 MPLA C24 > C29 CONF HTAB O2 O1 EQIV $1 x-1, y, z HTAB N3 O2_$1 EQIV $2 x+1/2, -y+1/2, z+1/2 HTAB C2 S1_$2 HTAB C18 N2_$2 EQIV $3 -x+2, -y+1, -z+1 HTAB C21 O1_$3 ACTA 58 WGHT 0.079800 0.154600 FVAR 0.46408 S1 5 0.497435 0.219509 0.342014 11.00000 0.02272 0.03016 = 0.03103 -0.01154 0.00246 0.00082 O1 4 1.208333 0.465488 0.594622 11.00000 0.03742 0.03815 = 0.05327 0.00176 0.01186 -0.01430 O2 4 1.156925 0.364115 0.476670 11.00000 0.02513 0.03416 = 0.02113 0.00072 0.00845 -0.00262 AFIX 3 H2A 2 1.193331 0.399275 0.484612 11.00000 -1.50000 AFIX 0 O3 4 0.608068 0.500375 0.892809 11.00000 0.03624 0.04241 = 0.03034 -0.01284 0.01303 -0.00063 O4 4 0.224119 0.253556 0.175217 11.00000 0.06122 0.05519 = 0.02361 -0.01004 0.00143 0.02609 N1 3 0.551287 0.326677 0.414552 11.00000 0.02032 0.02480 = 0.02156 -0.00056 0.00425 0.00168 N2 3 0.898895 0.163510 0.415036 11.00000 0.03872 0.03077 = 0.04229 -0.00530 0.00352 0.00866 N3 3 0.110787 0.315120 0.275231 11.00000 0.03176 0.03220 = 0.02089 -0.00298 0.00389 0.00555 AFIX 3 H3A 2 0.123005 0.327808 0.339295 11.00000 -1.20000 AFIX 0 C1 1 0.892051 0.405782 0.576156 11.00000 0.01914 0.02008 = 0.01940 0.00109 0.00509 -0.00007 AFIX 13 H1 2 0.912963 0.436858 0.528669 11.00000 -1.20000 AFIX 0 C2 1 1.057043 0.384738 0.632293 11.00000 0.02033 0.02306 = 0.01860 0.00033 0.00442 -0.00009 AFIX 13 H2 2 1.037934 0.365533 0.695266 11.00000 -1.20000 AFIX 0 C3 1 1.141031 0.340726 0.572882 11.00000 0.01928 0.02747 = 0.01862 0.00052 0.00479 0.00128 C4 1 1.032462 0.288585 0.553175 11.00000 0.01932 0.02377 = 0.02437 -0.00045 0.00340 0.00384 AFIX 23 H4A 2 1.079572 0.261207 0.509824 11.00000 -1.20000 H4B 2 1.026798 0.268725 0.617023 11.00000 -1.20000 AFIX 0 C5 1 0.865879 0.303930 0.504510 11.00000 0.01857 0.02222 = 0.01811 0.00185 0.00606 0.00132 C6 1 0.773539 0.262201 0.446637 11.00000 0.02085 0.02147 = 0.01960 -0.00018 0.00545 0.00242 C7 1 0.615101 0.274907 0.406266 11.00000 0.01990 0.02439 = 0.01880 -0.00149 0.00523 -0.00016 C8 1 0.640769 0.368038 0.466514 11.00000 0.02024 0.02224 = 0.02060 0.00155 0.00583 0.00160 C9 1 0.797590 0.358001 0.516116 11.00000 0.01831 0.02060 = 0.01800 0.00140 0.00537 0.00055 C10 1 0.805533 0.433240 0.654447 11.00000 0.01938 0.02087 = 0.02100 -0.00043 0.00343 0.00149 C11 1 0.718538 0.399361 0.712052 11.00000 0.02225 0.02165 = 0.02384 0.00051 0.00460 0.00017 AFIX 43 H11 2 0.704102 0.359333 0.697472 11.00000 -1.20000 AFIX 0 C12 1 0.652888 0.423027 0.790064 11.00000 0.02241 0.02906 = 0.02471 0.00056 0.00650 -0.00123 AFIX 43 H12 2 0.592213 0.399454 0.827603 11.00000 -1.20000 AFIX 0 C13 1 0.675801 0.481328 0.813456 11.00000 0.02219 0.03344 = 0.02371 -0.00583 0.00455 0.00369 C14 1 0.761320 0.515976 0.756976 11.00000 0.02971 0.02345 = 0.03194 -0.00582 0.00491 0.00060 AFIX 43 H14 2 0.776837 0.555878 0.772287 11.00000 -1.20000 AFIX 0 C15 1 0.824273 0.491653 0.677511 11.00000 0.02501 0.02194 = 0.02874 0.00095 0.00739 -0.00069 AFIX 43 H15 2 0.881237 0.515577 0.638293 11.00000 -1.20000 AFIX 0 C16 1 0.667580 0.553115 0.938422 11.00000 0.04576 0.05244 = 0.04260 -0.02527 0.01068 -0.00033 AFIX 137 H16A 2 0.784465 0.550913 0.955575 11.00000 -1.50000 H16B 2 0.620648 0.559492 0.999005 11.00000 -1.50000 H16C 2 0.638604 0.585256 0.892094 11.00000 -1.50000 AFIX 0 C17 1 1.164739 0.436732 0.660456 11.00000 0.02167 0.02722 = 0.03594 -0.00373 0.00163 0.00095 C18 1 1.216261 0.449329 0.768227 11.00000 0.04015 0.04196 = 0.04202 -0.01559 -0.01012 0.00374 AFIX 137 H18A 2 1.267619 0.414967 0.801321 11.00000 -1.50000 H18B 2 1.122528 0.459723 0.798737 11.00000 -1.50000 H18C 2 1.292503 0.481576 0.775466 11.00000 -1.50000 AFIX 0 C19 1 1.304681 0.323018 0.628692 11.00000 0.02022 0.03748 = 0.02855 -0.00278 0.00115 0.00377 AFIX 137 H19A 2 1.293501 0.310103 0.695891 11.00000 -1.50000 H19B 2 1.377685 0.356189 0.633079 11.00000 -1.50000 H19C 2 1.347991 0.291385 0.592961 11.00000 -1.50000 AFIX 0 C20 1 0.841622 0.206896 0.430263 11.00000 0.02429 0.02598 = 0.02355 -0.00230 0.00304 0.00170 C21 1 0.560210 0.425953 0.465288 11.00000 0.02305 0.02203 = 0.03348 0.00259 0.00166 0.00437 AFIX 137 H21A 2 0.519924 0.431841 0.528302 11.00000 -1.50000 H21B 2 0.470632 0.427392 0.410039 11.00000 -1.50000 H21C 2 0.637465 0.456448 0.456723 11.00000 -1.50000 AFIX 0 C22 1 0.299092 0.245067 0.351840 11.00000 0.02173 0.03047 = 0.02476 -0.00371 0.00349 -0.00040 AFIX 23 H22A 2 0.234973 0.212181 0.370639 11.00000 -1.20000 H22B 2 0.307145 0.274003 0.406068 11.00000 -1.20000 AFIX 0 C23 1 0.211352 0.272076 0.257462 11.00000 0.02755 0.03010 = 0.02364 -0.00536 0.00256 0.00001 C24 1 -0.008306 0.342537 0.205895 11.00000 0.03318 0.02600 = 0.02612 -0.00026 0.00373 0.00220 C25 1 -0.136204 0.367823 0.242977 11.00000 0.04484 0.04337 = 0.03230 0.00659 0.01178 0.01373 AFIX 43 H25 2 -0.141122 0.365874 0.312204 11.00000 -1.20000 AFIX 0 C26 1 -0.255596 0.395630 0.180090 11.00000 0.04882 0.05876 = 0.04820 0.00857 0.01264 0.02553 AFIX 43 H26 2 -0.343050 0.412373 0.206057 11.00000 -1.20000 AFIX 0 C27 1 -0.249148 0.399384 0.079055 11.00000 0.05095 0.05240 = 0.04129 0.00723 -0.00226 0.01679 AFIX 43 H27 2 -0.331596 0.418599 0.035625 11.00000 -1.20000 AFIX 0 C28 1 -0.121613 0.374885 0.042464 11.00000 0.05317 0.04800 = 0.02766 0.00155 -0.00056 0.00804 AFIX 43 H28 2 -0.115917 0.377920 -0.026552 11.00000 -1.20000 AFIX 0 C29 1 -0.001344 0.345870 0.104446 11.00000 0.03937 0.03937 = 0.02643 -0.00200 0.00516 0.00518 AFIX 43 H29 2 0.084748 0.328480 0.077982 11.00000 -1.20000 AFIX 0 HKLF 4 REM SKM282_0m_a.res in P2(1)/n REM wR2 = 0.126215, GooF = S = 1.10156, Restrained GooF = 1.10156 for all data REM R1 = 0.043276 for 5632 Fo > 4sig(Fo) and 0.053045 for all 7039 data REM 338 parameters refined using 0 restraints END WGHT 0.0798 0.1546 REM Highest difference peak 0.489, deepest hole -0.196, 1-sigma level 0.061 Q1 1 0.8172 0.2807 0.4762 11.00000 0.05 0.45 Q2 1 0.8420 0.3818 0.5444 11.00000 0.05 0.45 Q3 1 0.5566 0.2481 0.3775 11.00000 0.05 0.43 Q4 1 0.6966 0.2702 0.4217 11.00000 0.05 0.39 Q5 1 0.8394 0.4583 0.6809 11.00000 0.05 0.38 ; _shelx_res_checksum 24690 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S S1 0.49743(4) 0.21951(2) 0.34201(2) 0.02816(10) Uani d 1 . . O O1 1.20833(12) 0.46549(4) 0.59462(8) 0.0424(3) Uani d 1 . . O O2 1.15692(10) 0.36411(4) 0.47667(6) 0.02629(19) Uani d 1 . . H H2A 1.193331 0.399275 0.484612 0.039 Uiso d 1 . . O O3 0.60807(11) 0.50037(4) 0.89281(7) 0.0355(2) Uani d 1 . . O O4 0.22412(14) 0.25356(5) 0.17522(7) 0.0472(3) Uani d 1 . . N N1 0.55129(11) 0.32668(4) 0.41455(7) 0.0221(2) Uani d 1 . . N N2 0.89889(15) 0.16351(5) 0.41504(9) 0.0376(3) Uani d 1 . . N N3 0.11079(13) 0.31512(5) 0.27523(7) 0.0283(2) Uani d 1 . . H H3A 0.123005 0.327808 0.339295 0.034 Uiso d 1 . . C C1 0.89205(13) 0.40578(4) 0.57616(8) 0.0193(2) Uani d 1 . . H H1 0.912963 0.436858 0.528669 0.023 Uiso calc 1 . . C C2 1.05704(13) 0.38474(5) 0.63229(8) 0.0205(2) Uani d 1 . . H H2 1.037934 0.365533 0.695266 0.025 Uiso calc 1 . . C C3 1.14103(13) 0.34073(5) 0.57288(8) 0.0216(2) Uani d 1 . . C C4 1.03246(13) 0.28858(5) 0.55317(9) 0.0225(2) Uani d 1 . . H H4A 1.079572 0.261207 0.509824 0.027 Uiso calc 1 . . H H4B 1.026798 0.268725 0.617023 0.027 Uiso calc 1 . . C C5 0.86588(13) 0.30393(5) 0.50451(8) 0.0193(2) Uani d 1 . . C C6 0.77354(13) 0.26220(5) 0.44664(8) 0.0204(2) Uani d 1 . . C C7 0.61510(13) 0.27491(5) 0.40627(8) 0.0208(2) Uani d 1 . . C C8 0.64077(13) 0.36804(5) 0.46651(8) 0.0207(2) Uani d 1 . . C C9 0.79759(13) 0.35800(4) 0.51612(8) 0.0187(2) Uani d 1 . . C C10 0.80553(13) 0.43324(5) 0.65445(8) 0.0204(2) Uani d 1 . . C C11 0.71854(14) 0.39936(5) 0.71205(9) 0.0225(2) Uani d 1 . . H H11 0.704102 0.359333 0.697472 0.027 Uiso calc 1 . . C C12 0.65289(14) 0.42303(5) 0.79006(9) 0.0251(2) Uani d 1 . . H H12 0.592213 0.399454 0.827603 0.030 Uiso calc 1 . . C C13 0.67580(14) 0.48133(5) 0.81346(9) 0.0263(2) Uani d 1 . . C C14 0.76132(15) 0.51598(5) 0.75698(9) 0.0284(3) Uani d 1 . . H H14 0.776837 0.555878 0.772287 0.034 Uiso calc 1 . . C C15 0.82427(14) 0.49165(5) 0.67751(9) 0.0249(2) Uani d 1 . . H H15 0.881237 0.515577 0.638293 0.030 Uiso calc 1 . . C C16 0.6676(2) 0.55312(7) 0.93842(12) 0.0465(4) Uani d 1 . . H H16A 0.784465 0.550913 0.955575 0.070 Uiso calc 1 . . H H16B 0.620648 0.559492 0.999005 0.070 Uiso calc 1 . . H H16C 0.638604 0.585256 0.892094 0.070 Uiso calc 1 . . C C17 1.16474(14) 0.43673(5) 0.66046(10) 0.0286(3) Uani d 1 . . C C18 1.21626(19) 0.44933(7) 0.76823(11) 0.0431(4) Uani d 1 . . H H18A 1.267619 0.414967 0.801321 0.065 Uiso calc 1 . . H H18B 1.122528 0.459723 0.798737 0.065 Uiso calc 1 . . H H18C 1.292503 0.481576 0.775466 0.065 Uiso calc 1 . . C C19 1.30468(14) 0.32302(6) 0.62869(9) 0.0290(3) Uani d 1 . . H H19A 1.293501 0.310103 0.695891 0.044 Uiso calc 1 . . H H19B 1.377685 0.356189 0.633079 0.044 Uiso calc 1 . . H H19C 1.347991 0.291385 0.592961 0.044 Uiso calc 1 . . C C20 0.84162(14) 0.20690(5) 0.43026(9) 0.0247(2) Uani d 1 . . C C21 0.56021(15) 0.42595(5) 0.46529(10) 0.0265(2) Uani d 1 . . H H21A 0.519924 0.431841 0.528302 0.040 Uiso calc 1 . . H H21B 0.470632 0.427392 0.410039 0.040 Uiso calc 1 . . H H21C 0.637465 0.456448 0.456723 0.040 Uiso calc 1 . . C C22 0.29909(14) 0.24507(5) 0.35184(9) 0.0257(2) Uani d 1 . . H H22A 0.234973 0.212181 0.370639 0.031 Uiso calc 1 . . H H22B 0.307145 0.274003 0.406068 0.031 Uiso calc 1 . . C C23 0.21135(15) 0.27208(5) 0.25746(9) 0.0273(3) Uani d 1 . . C C24 -0.00831(16) 0.34254(5) 0.20589(9) 0.0285(3) Uani d 1 . . C C25 -0.13620(19) 0.36782(6) 0.24298(11) 0.0396(3) Uani d 1 . . H H25 -0.141122 0.365874 0.312204 0.047 Uiso calc 1 . . C C26 -0.2556(2) 0.39563(8) 0.18009(13) 0.0514(4) Uani d 1 . . H H26 -0.343050 0.412373 0.206057 0.062 Uiso calc 1 . . C C27 -0.2491(2) 0.39938(7) 0.07906(12) 0.0492(4) Uani d 1 . . H H27 -0.331596 0.418599 0.035625 0.059 Uiso calc 1 . . C C28 -0.1216(2) 0.37489(7) 0.04246(11) 0.0437(4) Uani d 1 . . H H28 -0.115917 0.377920 -0.026552 0.052 Uiso calc 1 . . C C29 -0.00134(18) 0.34587(6) 0.10445(10) 0.0351(3) Uani d 1 . . H H29 0.084748 0.328480 0.077982 0.042 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.02272(16) 0.03016(17) 0.03103(18) 0.00082(11) 0.00246(12) -0.01154(12) O1 0.0374(5) 0.0381(5) 0.0533(6) -0.0143(4) 0.0119(5) 0.0018(5) O2 0.0251(4) 0.0342(4) 0.0211(4) -0.0026(3) 0.0085(3) 0.0007(3) O3 0.0362(5) 0.0424(5) 0.0303(5) -0.0006(4) 0.0130(4) -0.0128(4) O4 0.0612(7) 0.0552(6) 0.0236(5) 0.0261(5) 0.0014(5) -0.0100(4) N1 0.0203(5) 0.0248(4) 0.0216(5) 0.0017(4) 0.0043(4) -0.0006(4) N2 0.0387(6) 0.0308(5) 0.0423(7) 0.0087(5) 0.0035(5) -0.0053(5) N3 0.0318(6) 0.0322(5) 0.0209(5) 0.0055(4) 0.0039(4) -0.0030(4) C1 0.0191(5) 0.0201(5) 0.0194(5) -0.0001(4) 0.0051(4) 0.0011(4) C2 0.0203(5) 0.0231(5) 0.0186(5) -0.0001(4) 0.0044(4) 0.0003(4) C3 0.0193(5) 0.0275(5) 0.0186(5) 0.0013(4) 0.0048(4) 0.0005(4) C4 0.0193(5) 0.0238(5) 0.0244(6) 0.0038(4) 0.0034(4) -0.0004(4) C5 0.0186(5) 0.0222(5) 0.0181(5) 0.0013(4) 0.0061(4) 0.0019(4) C6 0.0209(5) 0.0215(5) 0.0196(5) 0.0024(4) 0.0054(4) -0.0002(4) C7 0.0199(5) 0.0244(5) 0.0188(5) -0.0002(4) 0.0052(4) -0.0015(4) C8 0.0202(5) 0.0222(5) 0.0206(5) 0.0016(4) 0.0058(4) 0.0015(4) C9 0.0183(5) 0.0206(5) 0.0180(5) 0.0006(4) 0.0054(4) 0.0014(4) C10 0.0194(5) 0.0209(5) 0.0210(5) 0.0015(4) 0.0034(4) -0.0004(4) C11 0.0222(5) 0.0216(5) 0.0238(5) 0.0002(4) 0.0046(4) 0.0005(4) C12 0.0224(6) 0.0291(6) 0.0247(6) -0.0012(4) 0.0065(5) 0.0006(4) C13 0.0222(6) 0.0334(6) 0.0237(6) 0.0037(5) 0.0045(4) -0.0058(5) C14 0.0297(6) 0.0234(5) 0.0319(6) 0.0006(5) 0.0049(5) -0.0058(5) C15 0.0250(6) 0.0219(5) 0.0287(6) -0.0007(4) 0.0074(5) 0.0010(4) C16 0.0458(9) 0.0524(9) 0.0426(8) -0.0003(7) 0.0107(7) -0.0253(7) C17 0.0217(6) 0.0272(6) 0.0359(7) 0.0009(4) 0.0016(5) -0.0037(5) C18 0.0401(8) 0.0420(8) 0.0420(8) 0.0037(6) -0.0101(6) -0.0156(6) C19 0.0202(6) 0.0375(7) 0.0285(6) 0.0038(5) 0.0011(5) -0.0028(5) C20 0.0243(6) 0.0260(5) 0.0236(6) 0.0017(4) 0.0030(5) -0.0023(4) C21 0.0230(6) 0.0220(5) 0.0335(6) 0.0044(4) 0.0017(5) 0.0026(5) C22 0.0217(5) 0.0305(6) 0.0248(6) -0.0004(5) 0.0035(4) -0.0037(5) C23 0.0275(6) 0.0301(6) 0.0236(6) 0.0000(5) 0.0026(5) -0.0054(5) C24 0.0332(7) 0.0260(6) 0.0261(6) 0.0022(5) 0.0037(5) -0.0003(5) C25 0.0448(8) 0.0434(7) 0.0323(7) 0.0137(6) 0.0118(6) 0.0066(6) C26 0.0488(9) 0.0588(10) 0.0482(9) 0.0255(8) 0.0126(8) 0.0086(7) C27 0.0509(10) 0.0524(9) 0.0413(8) 0.0168(7) -0.0023(7) 0.0072(7) C28 0.0532(9) 0.0480(8) 0.0277(7) 0.0080(7) -0.0006(6) 0.0016(6) C29 0.0394(7) 0.0394(7) 0.0264(6) 0.0052(6) 0.0052(6) -0.0020(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C7 S1 C22 . . 100.59(6) ? C3 O2 H2A . . 108.6 ? C13 O3 C16 . . 117.10(11) ? C7 N1 C8 . . 118.87(10) ? C23 N3 C24 . . 127.59(10) ? C23 N3 H3A . . 115.3 ? C24 N3 H3A . . 117.1 ? C10 C1 C9 . . 114.12(9) ? C10 C1 C2 . . 106.17(9) ? C9 C1 C2 . . 112.94(8) ? C10 C1 H1 . . 107.8 ? C9 C1 H1 . . 107.8 ? C2 C1 H1 . . 107.8 ? C17 C2 C3 . . 110.33(9) ? C17 C2 C1 . . 109.33(9) ? C3 C2 C1 . . 113.55(9) ? C17 C2 H2 . . 107.8 ? C3 C2 H2 . . 107.8 ? C1 C2 H2 . . 107.8 ? O2 C3 C4 . . 106.15(9) ? O2 C3 C19 . . 110.25(9) ? C4 C3 C19 . . 110.59(10) ? O2 C3 C2 . . 110.17(9) ? C4 C3 C2 . . 107.61(9) ? C19 C3 C2 . . 111.88(9) ? C5 C4 C3 . . 112.99(9) ? C5 C4 H4A . . 109.0 ? C3 C4 H4A . . 109.0 ? C5 C4 H4B . . 109.0 ? C3 C4 H4B . . 109.0 ? H4A C4 H4B . . 107.8 ? C9 C5 C6 . . 118.41(10) ? C9 C5 C4 . . 122.51(10) ? C6 C5 C4 . . 119.07(9) ? C7 C6 C5 . . 119.41(10) ? C7 C6 C20 . . 120.66(10) ? C5 C6 C20 . . 119.93(10) ? N1 C7 C6 . . 122.32(10) ? N1 C7 S1 . . 119.46(9) ? C6 C7 S1 . . 118.22(8) ? N1 C8 C9 . . 122.85(10) ? N1 C8 C21 . . 114.24(10) ? C9 C8 C21 . . 122.90(10) ? C5 C9 C8 . . 117.89(10) ? C5 C9 C1 . . 121.24(10) ? C8 C9 C1 . . 120.80(9) ? C15 C10 C11 . . 118.02(10) ? C15 C10 C1 . . 120.86(10) ? C11 C10 C1 . . 120.80(10) ? C12 C11 C10 . . 121.20(11) ? C12 C11 H11 . . 119.4 ? C10 C11 H11 . . 119.4 ? C11 C12 C13 . . 119.99(11) ? C11 C12 H12 . . 120.0 ? C13 C12 H12 . . 120.0 ? O3 C13 C14 . . 124.61(11) ? O3 C13 C12 . . 115.51(11) ? C14 C13 C12 . . 119.87(11) ? C13 C14 C15 . . 119.40(11) ? C13 C14 H14 . . 120.3 ? C15 C14 H14 . . 120.3 ? C10 C15 C14 . . 121.50(11) ? C10 C15 H15 . . 119.3 ? C14 C15 H15 . . 119.3 ? O3 C16 H16A . . 109.5 ? O3 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? O3 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? O1 C17 C18 . . 122.75(13) ? O1 C17 C2 . . 118.98(12) ? C18 C17 C2 . . 118.24(12) ? C17 C18 H18A . . 109.5 ? C17 C18 H18B . . 109.5 ? H18A C18 H18B . . 109.5 ? C17 C18 H18C . . 109.5 ? H18A C18 H18C . . 109.5 ? H18B C18 H18C . . 109.5 ? C3 C19 H19A . . 109.5 ? C3 C19 H19B . . 109.5 ? H19A C19 H19B . . 109.5 ? C3 C19 H19C . . 109.5 ? H19A C19 H19C . . 109.5 ? H19B C19 H19C . . 109.5 ? N2 C20 C6 . . 177.76(14) ? C8 C21 H21A . . 109.5 ? C8 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C8 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C23 C22 S1 . . 114.22(9) ? C23 C22 H22A . . 108.7 ? S1 C22 H22A . . 108.7 ? C23 C22 H22B . . 108.7 ? S1 C22 H22B . . 108.7 ? H22A C22 H22B . . 107.6 ? O4 C23 N3 . . 124.77(12) ? O4 C23 C22 . . 122.14(11) ? N3 C23 C22 . . 112.92(10) ? C25 C24 C29 . . 119.47(12) ? C25 C24 N3 . . 117.25(11) ? C29 C24 N3 . . 123.27(12) ? C26 C25 C24 . . 120.45(14) ? C26 C25 H25 . . 119.8 ? C24 C25 H25 . . 119.8 ? C25 C26 C27 . . 120.43(14) ? C25 C26 H26 . . 119.8 ? C27 C26 H26 . . 119.8 ? C28 C27 C26 . . 119.13(14) ? C28 C27 H27 . . 120.4 ? C26 C27 H27 . . 120.4 ? C27 C28 C29 . . 121.28(14) ? C27 C28 H28 . . 119.4 ? C29 C28 H28 . . 119.4 ? C28 C29 C24 . . 119.22(13) ? C28 C29 H29 . . 120.4 ? C24 C29 H29 . . 120.4 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S1 C7 . 1.7661(12) ? S1 C22 . 1.8018(12) ? O1 C17 . 1.2176(16) ? O2 C3 . 1.4414(13) ? O2 H2A . 0.8696 ? O3 C13 . 1.3711(14) ? O3 C16 . 1.4233(17) ? O4 C23 . 1.2182(15) ? N1 C7 . 1.3245(14) ? N1 C8 . 1.3482(15) ? N2 C20 . 1.1463(15) ? N3 C23 . 1.3545(16) ? N3 C24 . 1.4164(16) ? N3 H3A . 0.9097 ? C1 C10 . 1.5216(15) ? C1 C9 . 1.5229(15) ? C1 C2 . 1.5587(15) ? C1 H1 . 1.0000 ? C2 C17 . 1.5198(16) ? C2 C3 . 1.5399(15) ? C2 H2 . 1.0000 ? C3 C4 . 1.5129(16) ? C3 C19 . 1.5255(16) ? C4 C5 . 1.5011(15) ? C4 H4A . 0.9900 ? C4 H4B . 0.9900 ? C5 C9 . 1.3958(15) ? C5 C6 . 1.4021(16) ? C6 C7 . 1.3964(16) ? C6 C20 . 1.4334(15) ? C8 C9 . 1.4088(15) ? C8 C21 . 1.5006(15) ? C10 C15 . 1.3894(16) ? C10 C11 . 1.3957(15) ? C11 C12 . 1.3847(16) ? C11 H11 . 0.9500 ? C12 C13 . 1.3911(17) ? C12 H12 . 0.9500 ? C13 C14 . 1.3884(18) ? C14 C15 . 1.3955(16) ? C14 H14 . 0.9500 ? C15 H15 . 0.9500 ? C16 H16A . 0.9800 ? C16 H16B . 0.9800 ? C16 H16C . 0.9800 ? C17 C18 . 1.4908(19) ? C18 H18A . 0.9800 ? C18 H18B . 0.9800 ? C18 H18C . 0.9800 ? C19 H19A . 0.9800 ? C19 H19B . 0.9800 ? C19 H19C . 0.9800 ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 C23 . 1.5128(17) ? C22 H22A . 0.9900 ? C22 H22B . 0.9900 ? C24 C25 . 1.3911(19) ? C24 C29 . 1.3923(18) ? C25 C26 . 1.375(2) ? C25 H25 . 0.9500 ? C26 C27 . 1.386(2) ? C26 H26 . 0.9500 ? C27 C28 . 1.378(2) ? C27 H27 . 0.9500 ? C28 C29 . 1.387(2) ? C28 H28 . 0.9500 ? C29 H29 . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O2 H2A O1 . 0.87 2.13 2.8343(14) 138 yes N3 H3A O2 1_455 0.91 2.03 2.9335(14) 174 yes C2 H2 S1 4_666 1.00 2.86 3.8269(12) 163 yes C18 H18A N2 4_666 0.98 2.52 3.493(2) 170 yes C21 H21C O1 3_766 0.98 2.39 3.3593(16) 169 yes C25 H25 Cg1 1_455 0.95 2.79 3.6141(18) 146 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C10 C1 C2 C17 . . . . -73.07(11) ? C9 C1 C2 C17 . . . . 161.14(9) ? C10 C1 C2 C3 . . . . 163.24(9) ? C9 C1 C2 C3 . . . . 37.45(12) ? C17 C2 C3 O2 . . . . -68.34(12) ? C1 C2 C3 O2 . . . . 54.80(12) ? C17 C2 C3 C4 . . . . 176.35(9) ? C1 C2 C3 C4 . . . . -60.51(11) ? C17 C2 C3 C19 . . . . 54.68(13) ? C1 C2 C3 C19 . . . . 177.82(9) ? O2 C3 C4 C5 . . . . -64.32(11) ? C19 C3 C4 C5 . . . . 176.09(9) ? C2 C3 C4 C5 . . . . 53.62(12) ? C3 C4 C5 C9 . . . . -26.75(15) ? C3 C4 C5 C6 . . . . 154.50(10) ? C9 C5 C6 C7 . . . . -2.77(16) ? C4 C5 C6 C7 . . . . 176.02(10) ? C9 C5 C6 C20 . . . . 177.84(10) ? C4 C5 C6 C20 . . . . -3.36(16) ? C8 N1 C7 C6 . . . . -2.18(16) ? C8 N1 C7 S1 . . . . 177.89(8) ? C5 C6 C7 N1 . . . . 4.95(17) ? C20 C6 C7 N1 . . . . -175.67(11) ? C5 C6 C7 S1 . . . . -175.12(8) ? C20 C6 C7 S1 . . . . 4.25(15) ? C22 S1 C7 N1 . . . . -22.84(10) ? C22 S1 C7 C6 . . . . 157.23(9) ? C7 N1 C8 C9 . . . . -2.71(16) ? C7 N1 C8 C21 . . . . 176.15(10) ? C6 C5 C9 C8 . . . . -1.73(15) ? C4 C5 C9 C8 . . . . 179.52(10) ? C6 C5 C9 C1 . . . . -178.72(9) ? C4 C5 C9 C1 . . . . 2.53(16) ? N1 C8 C9 C5 . . . . 4.65(16) ? C21 C8 C9 C5 . . . . -174.11(10) ? N1 C8 C9 C1 . . . . -178.34(10) ? C21 C8 C9 C1 . . . . 2.90(16) ? C10 C1 C9 C5 . . . . -129.19(11) ? C2 C1 C9 C5 . . . . -7.81(14) ? C10 C1 C9 C8 . . . . 53.90(13) ? C2 C1 C9 C8 . . . . 175.28(9) ? C9 C1 C10 C15 . . . . -145.75(11) ? C2 C1 C10 C15 . . . . 89.18(12) ? C9 C1 C10 C11 . . . . 40.85(14) ? C2 C1 C10 C11 . . . . -84.22(12) ? C15 C10 C11 C12 . . . . -0.12(17) ? C1 C10 C11 C12 . . . . 173.46(10) ? C10 C11 C12 C13 . . . . -1.27(18) ? C16 O3 C13 C14 . . . . -19.52(18) ? C16 O3 C13 C12 . . . . 161.09(12) ? C11 C12 C13 O3 . . . . -179.06(10) ? C11 C12 C13 C14 . . . . 1.52(18) ? O3 C13 C14 C15 . . . . -179.75(11) ? C12 C13 C14 C15 . . . . -0.39(18) ? C11 C10 C15 C14 . . . . 1.28(17) ? C1 C10 C15 C14 . . . . -172.30(11) ? C13 C14 C15 C10 . . . . -1.03(18) ? C3 C2 C17 O1 . . . . 59.92(14) ? C1 C2 C17 O1 . . . . -65.65(14) ? C3 C2 C17 C18 . . . . -118.40(12) ? C1 C2 C17 C18 . . . . 116.04(12) ? C7 S1 C22 C23 . . . . 103.44(9) ? C24 N3 C23 O4 . . . . 7.0(2) ? C24 N3 C23 C22 . . . . -168.25(11) ? S1 C22 C23 O4 . . . . 36.74(17) ? S1 C22 C23 N3 . . . . -147.86(9) ? C23 N3 C24 C25 . . . . 155.07(13) ? C23 N3 C24 C29 . . . . -25.9(2) ? C29 C24 C25 C26 . . . . 0.4(2) ? N3 C24 C25 C26 . . . . 179.45(14) ? C24 C25 C26 C27 . . . . -0.7(3) ? C25 C26 C27 C28 . . . . 0.0(3) ? C26 C27 C28 C29 . . . . 1.0(3) ? C27 C28 C29 C24 . . . . -1.3(2) ? C25 C24 C29 C28 . . . . 0.6(2) ? N3 C24 C29 C28 . . . . -178.39(13) ? _cod_database_fobs_code 2243840