#------------------------------------------------------------------------------ #$Date: 2021-05-29 08:15:51 +0300 (Sat, 29 May 2021) $ #$Revision: 265612 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243843.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243843 _cell_angle_alpha 90.000 _cell_angle_beta 101.004 _cell_angle_gamma 90.000 _cell_length_a 10.3302 _cell_length_b 19.5926 _cell_length_c 13.1516 _exptl_crystal_F_000 1696.00 _reflns_d_resolution_high 0.5998 _cod_data_source_file zn2004Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 452.82 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5897.30 6744.78 131.16 o 4 0 0 11518.72 11838.24 199.51 o 6 0 0 34041.57 34610.96 421.77 o 8 0 0 383.54 440.08 40.39 o 10 0 0 3573.44 3895.59 73.39 o 12 0 0 107.20 154.62 31.60 o 14 0 0 3.67 54.54 33.51 o 16 0 0 148.73 266.01 86.82 o 2 1 0 12890.26 14872.55 112.82 o 5 1 0 15726.70 16548.79 137.08 o 6 1 0 1492.69 1663.20 26.67 o 7 1 0 12934.14 12698.86 112.38 o 8 1 0 2899.97 2991.63 42.67 o 9 1 0 51.98 81.26 12.66 o 10 1 0 371.97 353.16 25.16 o 11 1 0 1531.75 1613.00 39.52 o 12 1 0 811.13 678.11 35.42 o 13 1 0 110.61 104.60 28.33 o 14 1 0 1040.44 1073.07 57.81 o 15 1 0 142.29 145.67 143.17 o 16 1 0 55.16 87.54 54.10 o 1 2 0 12938.44 12166.37 150.87 o 2 2 0 40.30 70.91 10.18 o 3 2 0 8416.99 7791.38 71.87 o 4 2 0 2648.92 2453.67 28.19 o 6 2 0 143.07 60.22 8.57 o 7 2 0 10377.39 10749.59 101.77 o 8 2 0 5273.30 4897.14 63.55 o 9 2 0 190.93 217.78 17.62 o 10 2 0 4953.62 5077.04 66.94 o 11 2 0 5.21 33.59 15.98 o 12 2 0 3843.65 3928.02 62.65 o 13 2 0 3531.35 3579.07 70.60 o 14 2 0 11.39 37.02 31.25 o 15 2 0 58.08 12.25 40.58 o 16 2 0 114.36 65.87 56.81 o 1 3 0 15067.26 15374.70 129.26 o 2 3 0 4574.37 4586.49 52.61 o 3 3 0 1750.55 1689.86 28.20 o 4 3 0 18473.27 17687.35 159.42 o 5 3 0 9400.29 10063.16 109.85 o 6 3 0 7552.59 7670.73 80.25 o 7 3 0 4537.45 4846.43 59.67 o 8 3 0 392.45 383.67 20.00 o 9 3 0 20.86 19.47 12.65 o 10 3 0 92.40 61.16 15.97 o 11 3 0 12627.33 12841.62 128.62 o 12 3 0 2972.78 3126.91 74.07 o 13 3 0 2467.26 2541.09 67.03 o 14 3 0 388.42 398.35 41.19 o 15 3 0 123.80 146.92 108.62 o 16 3 0 328.40 281.84 62.04 o 0 4 0 2409.62 2783.97 41.01 o 1 4 0 6913.88 8132.86 72.37 o 2 4 0 95.58 36.19 5.98 o 3 4 0 8046.79 7801.45 92.36 o 4 4 0 162.04 102.04 10.99 o 5 4 0 3294.16 3088.19 38.37 o 6 4 0 24404.11 24962.43 220.39 o 7 4 0 269.23 258.95 20.89 o 8 4 0 56.10 113.83 13.18 o 9 4 0 3486.01 3715.56 87.01 o 10 4 0 5783.34 6206.12 80.94 o 11 4 0 10.14 36.89 17.85 o 12 4 0 13706.55 13703.85 243.80 o 13 4 0 486.44 516.90 36.98 o 14 4 0 27.14 46.97 27.88 o 15 4 0 16.40 85.96 41.98 o 16 4 0 25.25 87.36 55.99 o 1 5 0 334.96 369.10 9.64 o 2 5 0 25424.64 25291.42 248.86 o 3 5 0 9.57 26.12 7.82 o 4 5 0 517.43 634.99 58.23 o 5 5 0 12550.62 12348.61 138.62 o 6 5 0 1.76 11.14 19.17 o 7 5 0 1782.20 1807.84 43.97 o 8 5 0 2285.65 2417.07 40.10 o 9 5 0 8.23 28.25 13.33 o 10 5 0 277.19 263.42 28.67 o 11 5 0 13696.78 14002.02 265.57 o 12 5 0 71.38 108.26 30.34 o 13 5 0 837.07 906.18 71.73 o 14 5 0 97.23 109.96 30.46 o 15 5 0 258.59 288.09 49.53 o 16 5 0 373.64 258.04 67.63 o 0 6 0 3193.75 3196.40 57.27 o 1 6 0 33569.02 31256.34 283.44 o 3 6 0 3408.99 3512.25 53.84 o 4 6 0 17.37 83.93 13.69 o 5 6 0 14696.87 14760.13 162.80 o 7 6 0 5815.16 5774.73 91.41 o 8 6 0 1738.09 1702.64 47.97 o 9 6 0 3742.40 3986.71 76.28 o 10 6 0 6339.50 6828.98 109.97 o 11 6 0 89.54 94.29 36.99 o 12 6 0 2195.41 2236.24 71.42 o 13 6 0 601.66 539.09 40.28 o 14 6 0 27.59 33.28 42.13 o 15 6 0 66.19 80.55 33.56 o 16 6 0 67.42 0.83 40.46 o 1 7 0 72161.29 72860.73 598.51 o 2 7 0 5858.78 5946.12 60.80 o 3 7 0 8205.96 8450.53 98.11 o 4 7 0 169.62 157.29 13.48 o 5 7 0 96.56 104.27 13.87 o 6 7 0 184.21 160.92 16.69 o 7 7 0 3017.76 3432.53 62.85 o 8 7 0 10189.86 10298.91 135.04 o 9 7 0 2145.43 2283.49 59.49 o 10 7 0 3.36 -1.09 22.90 o 11 7 0 871.19 877.39 56.17 o 12 7 0 68.60 29.21 28.50 o 13 7 0 182.79 242.54 35.86 o 14 7 0 50.04 55.77 33.23 o 15 7 0 51.09 29.99 32.43 o 16 7 0 5.43 -14.84 48.71 o 0 8 0 109085.91 111699.74 1289.91 o 1 8 0 20308.97 19560.55 240.79 o 2 8 0 5488.95 6638.11 92.20 o 3 8 0 11360.48 10224.77 116.61 o 4 8 0 7354.08 7360.80 92.42 o 5 8 0 3869.91 3685.26 59.35 o 6 8 0 5601.94 6073.37 86.72 o 7 8 0 35.21 45.10 23.26 o 8 8 0 13.30 17.79 17.75 o 9 8 0 849.48 976.33 60.75 o 10 8 0 399.22 374.61 33.87 o 11 8 0 341.05 302.54 34.78 o 12 8 0 64.92 76.82 39.12 o 13 8 0 73.70 93.66 33.24 o 14 8 0 188.23 216.65 34.20 o 15 8 0 67.71 68.14 32.19 o 16 8 0 179.86 80.78 64.32 o 1 9 0 13671.13 14178.97 129.42 o 2 9 0 4494.63 3799.40 44.53 o 3 9 0 594.97 350.94 19.47 o 4 9 0 993.43 665.62 25.23 o 5 9 0 8879.75 8672.83 109.49 o 6 9 0 2810.68 2916.41 58.72 o 7 9 0 1445.20 1466.43 49.00 o 8 9 0 1179.37 1034.09 42.47 o 9 9 0 2006.28 2047.63 58.93 o 10 9 0 1539.72 1481.44 57.02 o 11 9 0 84.99 60.54 27.60 o 12 9 0 470.04 422.51 39.91 o 13 9 0 446.56 412.21 47.52 o 14 9 0 2315.31 2369.94 74.97 o 15 9 0 2.80 15.69 45.06 o 16 9 0 19.93 24.84 43.46 o 0 10 0 85.78 111.40 36.95 o 1 10 0 646.97 623.18 17.75 o 2 10 0 1043.41 1408.64 31.73 o 3 10 0 59.12 86.94 13.47 o 4 10 0 71.64 136.97 15.26 o 5 10 0 177.60 169.84 17.75 o 6 10 0 360.22 248.51 21.98 o 7 10 0 2414.11 2290.37 54.70 o 8 10 0 352.86 419.28 34.38 o 9 10 0 309.30 333.78 30.13 o 10 10 0 5358.82 5321.24 100.91 o 11 10 0 148.62 145.94 35.45 o 12 10 0 664.77 618.82 45.80 o 13 10 0 5300.01 5326.88 122.97 o 14 10 0 527.65 544.96 96.06 o 15 10 0 4.25 0.93 37.48 o 16 10 0 24.27 9.63 41.60 o 2 11 0 1639.13 1982.27 31.36 o 3 11 0 93.40 152.54 12.53 o 4 11 0 11380.19 11144.14 133.66 o 5 11 0 5164.64 5257.54 87.37 o 6 11 0 2206.28 2356.46 53.65 o 7 11 0 1180.54 1177.02 43.23 o 8 11 0 1022.74 1049.46 45.04 o 9 11 0 5133.54 5129.22 94.87 o 10 11 0 2704.58 2899.27 79.84 o 11 11 0 4537.82 4685.80 106.51 o 12 11 0 1213.54 1237.85 109.33 o 13 11 0 658.38 607.47 57.98 o 14 11 0 1768.68 1712.75 83.70 o 15 11 0 262.14 207.25 38.22 o 0 12 0 3686.04 3822.61 68.90 o 1 12 0 59.83 114.50 10.92 o 2 12 0 202.41 301.77 14.79 o 3 12 0 2701.57 2685.64 39.49 o 4 12 0 155.53 236.09 20.21 o 5 12 0 636.24 498.95 32.18 o 6 12 0 6336.97 6242.74 103.82 o 7 12 0 1709.09 1575.93 49.31 o 8 12 0 1778.86 1969.00 63.08 o 9 12 0 4490.03 4629.69 91.63 o 10 12 0 4336.56 4650.01 100.50 o 11 12 0 318.68 312.63 37.23 o 12 12 0 2018.04 2037.29 124.60 o 13 12 0 2026.20 2196.65 114.56 o 14 12 0 22.54 -18.68 34.79 o 15 12 0 51.04 9.57 41.96 o 1 13 0 1372.58 1684.64 31.44 o 2 13 0 12595.04 12650.50 124.97 o 3 13 0 8687.69 8729.62 92.58 o 4 13 0 1987.99 1622.09 70.50 o 6 13 0 276.78 267.72 25.55 o 7 13 0 3078.62 3218.57 68.96 o 8 13 0 1843.07 2011.98 60.46 o 9 13 0 0.36 -16.22 24.48 o 10 13 0 2536.43 2592.85 75.29 o 11 13 0 5359.75 5558.35 113.24 o 12 13 0 171.10 139.96 36.00 o 13 13 0 227.89 228.41 40.62 o 14 13 0 4.58 48.03 66.50 o 15 13 0 26.85 -43.99 43.99 o 0 14 0 186.72 160.05 36.02 o 1 14 0 24397.40 25220.89 227.35 o 2 14 0 13801.93 13603.12 133.78 o 3 14 0 233.41 389.00 18.99 o 4 14 0 8451.49 8240.67 113.37 o 5 14 0 2395.69 2388.56 61.94 o 6 14 0 2682.02 2943.46 64.70 o 7 14 0 2540.40 2526.84 63.60 o 8 14 0 53.59 98.81 25.68 o 9 14 0 2665.01 2700.73 76.73 o 10 14 0 501.19 484.46 41.47 o 11 14 0 191.05 245.96 37.77 o 12 14 0 1317.04 1361.42 75.75 o 13 14 0 7.58 -39.47 39.47 o 14 14 0 63.18 91.38 40.49 o 15 14 0 26.83 -38.14 57.32 o 1 15 0 11807.02 11767.78 120.09 o 2 15 0 20373.16 20603.67 192.58 o 3 15 0 6946.55 7058.98 92.61 o 4 15 0 1059.71 1112.80 40.76 o 5 15 0 3120.91 3204.16 66.11 o 6 15 0 112.10 144.22 22.64 o 7 15 0 517.60 578.88 37.13 o 8 15 0 3568.53 3718.65 90.13 o 9 15 0 24.98 24.64 28.18 o 10 15 0 79.70 48.77 39.36 o 11 15 0 4.01 28.68 31.19 o 12 15 0 59.09 76.82 35.98 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28.16 o 2 18 0 1256.18 1218.53 33.92 o 3 18 0 325.77 385.88 22.49 o 4 18 0 175.96 208.76 33.97 o 5 18 0 165.09 219.82 27.69 o 6 18 0 89.29 114.10 26.29 o 7 18 0 2404.66 2423.51 79.64 o 8 18 0 3759.23 3687.87 87.76 o 9 18 0 234.00 212.14 35.91 o 10 18 0 364.83 311.53 40.11 o 11 18 0 47.56 86.93 34.68 o 12 18 0 49.45 92.84 45.87 o 13 18 0 2276.03 2522.35 130.45 o 14 18 0 1705.94 1711.74 90.34 o 1 19 0 886.08 824.48 31.66 o 2 19 0 557.71 548.12 27.17 o 3 19 0 12.15 4.54 13.29 o 4 19 0 2587.71 2624.51 63.60 o 5 19 0 248.88 277.09 29.83 o 6 19 0 1023.97 1027.99 52.57 o 7 19 0 4187.56 4311.87 121.42 o 8 19 0 1.20 8.42 28.78 o 9 19 0 1358.60 1261.67 65.53 o 10 19 0 517.51 455.45 44.57 o 11 19 0 204.49 180.02 38.68 o 12 19 0 326.49 391.68 67.48 o 13 19 0 1094.82 957.17 64.74 o 0 20 0 916.41 911.00 47.86 o 1 20 0 25.58 21.62 15.30 o 2 20 0 141.51 142.26 18.44 o 3 20 0 1369.57 1402.38 39.46 o 4 20 0 368.61 328.76 30.81 o 5 20 0 167.15 162.33 27.90 o 6 20 0 3269.86 3267.43 80.67 o 7 20 0 507.59 520.26 40.71 o 8 20 0 3034.04 2841.77 84.82 o 9 20 0 1533.70 1641.99 77.00 o 10 20 0 126.60 132.98 37.21 o 11 20 0 129.89 116.57 47.66 o 12 20 0 780.53 771.64 65.56 o 13 20 0 487.64 497.31 72.37 o 1 21 0 85.99 71.92 18.96 o 2 21 0 7.67 33.09 17.51 o 3 21 0 2061.47 1930.35 46.26 o 4 21 0 771.26 712.78 34.13 o 5 21 0 5.06 36.02 67.43 o 6 21 0 93.90 98.94 29.08 o 7 21 0 3409.29 3395.61 88.69 o 8 21 0 871.29 953.08 56.17 o 9 21 0 20.59 15.72 30.24 o 10 21 0 1407.13 1532.05 74.16 o 11 21 0 643.57 688.42 55.40 o 12 21 0 22.44 29.84 38.11 o 0 22 0 141.33 137.94 27.88 o 1 22 0 646.57 734.75 34.36 o 2 22 0 2598.92 2408.05 52.42 o 3 22 0 1102.48 1120.54 59.46 o 4 22 0 3020.06 2995.41 77.80 o 5 22 0 0.86 -3.64 27.66 o 6 22 0 411.72 380.07 38.13 o 7 22 0 604.42 538.79 44.08 o 8 22 0 45.50 29.67 44.00 o 9 22 0 557.27 593.82 53.32 o 10 22 0 10.95 19.87 38.25 o 11 22 0 17.89 -10.42 54.27 o 12 22 0 70.33 63.15 42.30 o 1 23 0 1235.24 1287.61 42.91 o 2 23 0 2825.64 2743.99 61.02 o 3 23 0 5094.68 4941.63 77.58 o 4 23 0 6.24 38.08 30.48 o 5 23 0 329.07 321.91 36.03 o 6 23 0 10.10 4.24 26.83 o 7 23 0 243.52 268.55 53.72 o 8 23 0 431.62 446.13 44.02 o 9 23 0 66.15 97.23 38.16 o 10 23 0 10.65 -24.29 71.47 o 11 23 0 33.74 33.97 36.89 o 12 23 0 6.26 -25.86 66.50 o 0 24 0 3007.94 2981.75 87.59 o 1 24 0 298.62 304.18 26.41 o 2 24 0 1622.22 1681.39 62.66 o 3 24 0 82.81 136.10 23.73 o 4 24 0 2537.95 2550.85 75.63 o 5 24 0 91.89 28.27 28.43 o 6 24 0 539.81 529.22 42.58 o 7 24 0 456.45 425.23 44.06 o 8 24 0 248.32 259.31 38.40 o 9 24 0 97.43 68.56 89.59 o 10 24 0 32.33 -43.94 59.12 o 11 24 0 469.53 492.06 50.70 o 1 25 0 521.15 546.33 36.31 o 2 25 0 954.21 1090.09 54.59 o 3 25 0 609.78 625.56 72.99 o 4 25 0 70.23 77.32 44.91 o 5 25 0 571.70 485.29 41.40 o 6 25 0 67.31 30.25 31.44 o 7 25 0 462.14 478.87 44.75 o 8 25 0 311.97 333.67 44.90 o 9 25 0 945.74 740.13 63.86 o 10 25 0 301.20 153.80 41.51 o 0 26 0 1.09 -26.48 31.02 o 1 26 0 256.74 252.44 29.69 o 2 26 0 79.05 58.46 23.40 o 3 26 0 14.26 25.79 42.65 o 4 26 0 9.39 -0.26 33.90 o 5 26 0 68.95 33.30 30.36 o 6 26 0 48.00 82.01 32.93 o 7 26 0 27.16 -2.25 42.44 o 8 26 0 2035.42 1966.99 79.44 o 9 26 0 0.75 -28.68 122.85 o 10 26 0 65.53 -20.24 82.27 o 1 27 0 620.77 739.28 40.15 o 2 27 0 14.15 25.14 28.32 o 3 27 0 32.64 23.93 30.49 o 4 27 0 357.28 320.00 37.85 o 5 27 0 0.46 25.29 52.82 o 6 27 0 18.14 44.45 32.62 o 7 27 0 1384.81 1329.11 87.40 o 8 27 0 1.15 -13.81 52.46 o 9 27 0 1177.76 1127.83 103.42 o 0 28 0 355.63 306.37 46.18 o 1 28 0 115.92 79.55 32.80 o 2 28 0 146.85 133.41 32.70 o 3 28 0 100.13 105.91 33.06 o 4 28 0 51.71 80.10 33.34 o 5 28 0 889.29 676.69 48.85 o 6 28 0 392.77 260.95 86.82 o 7 28 0 2.32 42.92 35.07 o 8 28 0 1239.92 1286.70 77.30 o 1 29 0 6.25 -0.96 36.35 o 2 29 0 371.02 308.36 38.74 o 3 29 0 913.09 1023.33 62.38 o 4 29 0 889.55 867.55 95.52 o 5 29 0 61.80 6.26 65.58 o 6 29 0 347.58 315.90 43.65 o 7 29 0 754.90 645.79 51.54 o 0 30 0 692.37 655.19 162.56 o 1 30 0 23.89 62.36 49.53 o 2 30 0 1018.73 922.73 55.06 o 3 30 0 33.72 56.69 35.48 o 4 30 0 2563.02 2418.97 110.79 o 5 30 0 698.40 776.65 66.58 o 6 30 0 242.68 228.80 41.94 o 1 31 0 30.13 -40.34 63.73 o 2 31 0 307.29 275.91 46.43 o 3 31 0 4475.51 4732.10 135.83 o 4 31 0 21.14 12.61 41.72 o 5 31 0 292.15 229.68 41.57 o 0 32 0 104.10 7.39 59.11 o 1 32 0 200.02 63.53 53.29 o 2 32 0 764.47 759.17 53.31 o 3 32 0 46.06 94.23 38.57 o -17 0 1 1242.04 1488.94 160.72 o -15 0 1 1655.77 1657.04 144.09 o -13 0 1 143.40 139.44 32.73 o -11 0 1 815.31 919.68 49.19 o -9 0 1 4996.89 4934.05 78.65 o -7 0 1 1274.62 1313.88 88.67 o -5 0 1 393.65 419.88 16.02 o -3 0 1 11167.23 10116.79 127.31 o 1 0 1 205043.00 184731.42 3587.48 o 3 0 1 16416.69 15126.68 187.36 o 5 0 1 9642.22 10348.13 157.95 o 7 0 1 55289.37 56092.99 552.69 o 9 0 1 3362.54 3449.66 65.79 o 11 0 1 710.21 768.18 62.66 o 13 0 1 351.24 308.16 39.16 o 15 0 1 95.04 31.40 92.37 o -17 1 1 31.47 102.73 79.43 o -16 1 1 2235.85 2450.30 127.99 o -15 1 1 0.46 5.54 53.57 o -14 1 1 197.67 172.85 26.47 o -13 1 1 1842.17 1908.00 115.00 o -12 1 1 344.14 345.93 27.05 o -11 1 1 37.79 39.06 15.97 o -10 1 1 11.90 22.69 12.86 o -9 1 1 537.23 527.88 22.88 o -8 1 1 130.36 110.50 14.72 o -7 1 1 5164.99 5306.88 63.10 o -6 1 1 66.54 86.31 9.53 o -5 1 1 1754.74 1905.82 45.87 o -4 1 1 1716.23 1685.19 25.18 o -3 1 1 3739.75 3765.91 38.95 o -2 1 1 798.10 590.43 10.52 o -1 1 1 22464.56 21391.90 633.63 o 1 1 1 14469.86 14233.02 426.49 o 2 1 1 9554.26 10114.14 88.84 o 5 1 1 4534.52 4952.84 59.65 o 6 1 1 47228.79 48936.41 417.90 o 7 1 1 6651.34 6668.70 69.23 o 8 1 1 7760.78 8155.15 76.70 o 9 1 1 7.15 6.32 11.85 o 10 1 1 1671.81 1546.75 36.55 o 11 1 1 14.18 5.02 24.91 o 12 1 1 182.66 182.28 24.09 o 13 1 1 2266.12 2286.48 57.30 o 14 1 1 38.92 41.34 31.46 o 15 1 1 369.38 355.63 73.15 o 16 1 1 192.28 278.43 86.82 o -17 2 1 71.56 13.95 55.50 o -16 2 1 29.31 43.41 53.56 o -15 2 1 1101.08 879.92 57.07 o -14 2 1 602.88 621.36 56.33 o -13 2 1 210.57 209.84 22.94 o -12 2 1 2294.35 2374.94 52.58 o -11 2 1 1828.04 1816.81 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