#------------------------------------------------------------------------------
#$Date: 2021-06-12 07:49:53 +0300 (Sat, 12 Jun 2021) $
#$Revision: 266412 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243852.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243852
loop_
_publ_author_name
'K\'eb\'e, Momath'
'Thiam, Ibrahima Elhadji'
'Sow, Mouhamadou Moustapha'
'Diouf, Ousmane'
'Barry, Aliou Hamady'
'Sall, Abdou Salam'
'Retailleau, Pascal'
'Gaye, Mohamed'
_publ_section_title
;
Hexanuclear copper(II) complex of
2-hydroxy-N,N'-bis[1-(2-hydroxyphenyl)ethylidene]propane-1,3-diamine
incorporating an open-cubane core
;
_journal_coeditor_code EX2045
_journal_issue 7
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first 708
_journal_page_last 713
_journal_paper_doi 10.1107/S2056989021005570
_journal_volume 77
_journal_year 2021
_chemical_formula_iupac
'[Cu6 (C19 H19 N2 O3)3 (N O3)2 (O H) (H2 O)2], 3C2 H6 O'
_chemical_formula_moiety 'C57 H62 Cu6 N8 O18, 3(C2 H6 O)'
_chemical_formula_sum 'C63 H80 Cu6 N8 O21'
_chemical_formula_weight 1666.59
_space_group_crystal_system triclinic
_space_group_IT_number 2
_space_group_name_Hall '-P 1'
_space_group_name_H-M_alt 'P -1'
_atom_sites_solution_hydrogens mixed
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_cell_angle_alpha 83.626(3)
_cell_angle_beta 86.186(3)
_cell_angle_gamma 72.288(3)
_cell_formula_units_Z 2
_cell_length_a 13.6406(5)
_cell_length_b 14.0568(5)
_cell_length_c 18.5907(7)
_cell_measurement_reflns_used 5100
_cell_measurement_temperature 293(2)
_cell_measurement_theta_max 28.6423
_cell_measurement_theta_min 2.4120
_cell_volume 3372.7(2)
_computing_cell_refinement 'SAINT (Bruker, 2016)'
_computing_data_collection 'APEX3 (Bruker, 2016)'
_computing_data_reduction 'SAINT (Bruker, 2016)'
_computing_molecular_graphics 'OLEX2 (Dolomanov et al., 2009)'
_computing_publication_material 'OLEX2 (Dolomanov et al., 2009)'
_computing_structure_refinement 'SHELXL (Sheldrick, 2015b)'
_computing_structure_solution 'SHELXT2018/2 (Sheldrick, 2015a)'
_diffrn_ambient_temperature 293(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type KappaCCD
_diffrn_measurement_method CCD
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0327
_diffrn_reflns_av_unetI/netI 0.0224
_diffrn_reflns_limit_h_max 17
_diffrn_reflns_limit_h_min -17
_diffrn_reflns_limit_k_max 17
_diffrn_reflns_limit_k_min -17
_diffrn_reflns_limit_l_max 23
_diffrn_reflns_limit_l_min -23
_diffrn_reflns_number 73743
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 26.732
_diffrn_reflns_theta_min 2.751
_exptl_absorpt_coefficient_mu 1.939
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.96705
_exptl_absorpt_correction_type multi-scan
_exptl_crystal_colour green
_exptl_crystal_density_diffrn 1.641
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description prismatic
_exptl_crystal_F_000 1712
_exptl_crystal_size_max 0.3
_exptl_crystal_size_mid 0.2
_exptl_crystal_size_min 0.1
_refine_diff_density_max 0.817
_refine_diff_density_min -0.556
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.037
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 929
_refine_ls_number_reflns 14284
_refine_ls_number_restraints 3
_refine_ls_restrained_S_all 1.038
_refine_ls_R_factor_all 0.0395
_refine_ls_R_factor_gt 0.0330
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0432P)^2^+3.2696P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0870
_refine_ls_wR_factor_ref 0.0911
_reflns_number_gt 12395
_reflns_number_total 14284
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file ex2045sup1.cif
_cod_data_source_block I
_cod_database_code 2243852
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
0 0 3 1010.32 34.49
0 0 -3 1073.46 34.50
0 0 4 99.39 3.43
0 0 -4 98.78 3.44
0 0 4 98.59 3.40
0 0 4 87.96 3.45
0 0 5 38.17 1.52
0 0 -5 34.97 1.52
0 0 5 35.70 1.47
0 0 5 36.06 1.57
0 0 6 122.07 4.25
0 0 -6 124.74 4.28
0 0 6 116.38 4.19
0 0 6 120.38 4.33
0 0 -6 103.70 4.31
0 0 7 476.91 16.06
0 0 7 477.14 16.12
0 0 -7 502.89 16.16
0 0 -7 438.43 16.37
0 0 7 494.42 16.22
0 0 -7 453.49 16.23
0 0 8 130.89 4.64
0 0 8 118.26 4.69
0 0 -8 136.44 4.76
0 0 -8 122.80 5.01
0 0 -8 126.34 4.88
0 0 8 128.09 4.81
0 0 9 514.20 17.23
0 0 -9 527.37 17.36
0 0 9 510.14 17.33
0 0 -9 485.57 17.70
0 0 -9 487.25 17.48
0 0 9 511.48 17.41
0 0 10 45.03 2.15
0 0 -10 52.19 2.34
0 0 10 51.64 2.39
0 0 10 52.15 2.30
0 0 -10 50.61 2.71
0 0 -10 48.46 2.47
0 0 11 8.95 1.09
0 0 -11 8.41 1.01
0 0 -11 8.62 1.11
0 0 11 10.12 1.01
0 0 -11 8.87 1.34
0 0 11 7.56 1.19
0 0 11 8.52 0.91
0 0 -12 294.81 10.22
0 0 -12 290.56 10.31
0 0 12 304.62 10.41
0 0 12 276.37 10.27
0 0 12 283.06 10.54
0 0 -12 279.23 10.80
0 0 12 282.37 10.12
0 0 -13 46.64 2.48
0 0 -13 45.58 2.59
0 0 13 48.26 2.62
0 0 13 51.00 2.53
0 0 13 51.72 2.90
0 0 -13 48.07 3.09
0 0 13 42.48 2.27
0 0 14 8.81 1.54
0 0 -14 8.90 1.37
0 0 -14 7.70 1.48
0 0 14 11.25 1.22
0 0 14 11.07 1.43
0 0 14 8.86 1.67
0 0 -14 8.86 1.91
0 0 -15 457.90 15.45
0 0 -15 445.35 15.61
0 0 15 457.22 15.68
0 0 15 429.16 15.58
0 0 15 447.92 15.85
0 0 -15 423.36 16.23
0 0 15 424.99 15.30
0 0 -16 329.36 11.44
0 0 -16 303.94 11.60
0 0 16 329.09 11.69
0 0 16 321.29 11.62
0 0 16 338.24 11.92
0 0 -16 311.16 12.34
0 0 16 297.27 11.29
0 0 -17 9.92 1.51
0 0 -17 8.40 1.78
0 0 17 9.60 1.77
0 0 17 10.73 1.36
0 0 17 9.41 1.72
0 0 17 10.22 1.84
0 0 -17 8.13 2.29
0 0 -18 10.15 1.56
0 0 -18 10.45 1.81
0 0 18 10.46 1.70
0 0 -18 11.28 2.46
0 0 18 9.75 2.02
0 0 18 9.71 1.77
0 0 18 10.83 1.45
0 0 19 308.33 11.12
0 0 19 282.75 10.67
0 0 -19 292.67 10.69
0 0 19 286.35 11.07
0 0 19 317.55 11.42
0 0 -19 285.61 12.03
0 0 20 0.75 1.60
0 0 20 1.34 1.23
0 0 -20 -0.70 1.30
0 0 20 1.15 1.61
0 0 20 0.59 1.74
0 0 -20 1.38 2.26
0 0 21 2.89 1.71
0 0 21 1.75 1.18
0 0 21 2.08 1.65
0 0 21 2.83 1.80
0 0 -21 3.95 2.45
0 0 -22 2.27 2.73
0 0 22 5.21 1.87
0 0 22 4.01 1.89
0 0 -23 63.28 5.11
0 0 23 70.23 4.02
0 0 23 73.63 4.05
0 1 -23 39.18 4.28
0 -1 23 38.08 3.08
0 -1 23 43.35 3.02
0 -1 22 65.53 3.84
0 -1 22 74.95 3.91
0 1 -22 65.11 4.90
0 -1 22 66.75 3.86
0 1 -21 0.17 2.39
0 -1 21 1.51 1.59
0 -1 21 1.60 1.24
0 -1 21 1.13 1.64
0 -1 21 0.58 1.74
0 -1 21 -2.60 1.82
0 -1 20 30.88 2.59
0 1 -20 34.08 1.75
0 1 -20 31.96 1.45
0 -1 20 31.68 2.55
0 -1 20 34.58 2.53
0 -1 20 28.51 2.13
0 -1 20 34.68 2.71
0 1 -20 31.60 3.40
0 1 -19 3.50 1.08
0 -1 19 4.04 1.74
0 -1 19 2.25 1.31
0 -1 19 6.08 1.68
0 -1 19 5.57 1.78
0 1 -19 2.75 2.06
0 1 -18 9.82 1.21
0 -1 18 9.67 1.66
0 -1 18 11.19 1.80
0 -1 18 7.98 1.37
0 -1 18 10.30 1.97
0 1 -18 10.81 2.41
0 1 -17 73.41 3.14
0 -1 17 72.53 3.65
0 -1 17 79.22 3.77
0 1 -17 73.06 4.47
0 -1 17 73.51 3.88
0 -1 17 69.27 3.38
0 1 -16 22.89 1.59
0 -1 16 19.31 1.91
0 -1 16 25.08 2.12
0 -1 16 21.08 2.10
0 -1 16 18.13 1.68
0 1 -16 25.06 2.60
0 1 -15 3.86 1.03
0 -1 15 2.45 1.32
0 -1 15 3.78 1.25
0 -1 15 4.98 1.43
0 -1 15 3.25 1.15
0 1 -15 0.75 1.74
0 1 -14 127.54 5.75
0 1 -14 140.43 5.14
0 1 -14 138.17 5.56
0 -1 14 135.81 5.51
0 -1 14 137.27 5.45
0 1 -14 137.54 6.12
0 -1 14 135.90 5.62
0 -1 14 127.30 5.26
0 1 -13 167.62 6.81
0 1 -13 168.17 6.23
0 1 -13 168.94 6.58
0 -1 13 178.77 6.59
0 -1 13 161.15 6.47
0 1 -13 173.77 7.10
0 -1 13 178.86 6.73
0 -1 13 165.64 6.34
0 1 -12 94.13 4.16
0 1 -12 96.29 3.66
0 1 -12 90.48 3.95
0 -1 12 101.77 3.99
0 -1 12 84.28 3.89
0 -1 12 94.33 4.09
0 1 -12 98.62 4.43
0 -1 12 87.94 3.78
0 1 -11 40.19 2.27
0 1 -11 38.40 1.85
0 1 -11 54.93 2.33
0 -1 11 40.04 2.16
0 -1 11 37.54 2.05
0 -1 11 38.78 2.23
0 1 -11 42.26 2.50
0 -1 11 37.73 1.98
0 1 -10 4.48 0.69
0 1 -10 4.21 0.99
0 -1 10 3.22 0.78
0 -1 10 4.93 0.91
0 1 -10 3.86 1.07
0 1 -10 4.38 0.93
0 -1 10 4.20 0.90
0 1 -9 17.98 1.38
0 -1 9 21.77 1.41
0 -1 9 20.31 1.33
0 -1 9 19.29 1.47
0 1 -9 18.52 1.58
0 1 -9 18.56 1.46
0 1 -8 2250.41 71.48
0 -1 8 2126.39 71.42
0 -1 8 2194.52 71.45
0 -1 8 2203.11 71.57
0 1 -8 2191.91 71.72
0 1 -8 1949.63 71.50
0 1 -7 7.36 0.85
0 -1 7 5.44 0.72
0 1 -7 4.81 0.93
0 -1 7 3.57 0.84
0 -1 7 2.36 0.71
0 -1 6 2678.55 92.61
0 1 -6 2798.91 92.79
0 -1 6 2845.32 92.70
0 -1 6 2786.66 92.63
0 1 -6 2903.53 92.66
0 1 -5 50.15 2.20
0 -1 5 47.42 2.09
0 -1 5 52.51 2.09
0 1 -5 57.94 2.15
0 1 -4 113.08 4.02
0 -1 4 107.95 3.94
0 1 -3 612.34 20.62
0 -1 3 623.00 20.61
0 1 -2 131.54 4.51
0 -1 -3 9.72 0.50
0 1 3 10.42 0.58
0 -1 -3 9.82 0.56
0 1 4 8.77 0.52
0 -1 -4 8.39 0.51
0 1 4 10.06 0.61
0 -1 -4 8.78 0.58
0 1 5 1.49 0.31
0 1 5 1.14 0.48
0 -1 -5 1.80 0.34
0 -1 -5 1.31 0.38
0 1 5 1.22 0.38
0 1 6 531.98 17.83
0 1 6 548.39 18.03
0 -1 -6 551.22 17.85
0 1 6 497.18 17.92
0 -1 -6 532.74 17.90
0 -1 -7 4.01 0.62
0 1 7 4.17 0.64
0 1 7 5.59 0.53
0 1 7 7.10 0.76
0 1 8 -0.03 0.64
0 -1 -8 -0.26 0.65
0 1 8 0.19 0.67
0 1 8 0.14 0.47
0 1 9 746.65 25.57
0 1 9 751.82 25.41
0 1 9 752.63 25.68
0 -1 -9 781.13 25.53
0 1 10 1.26 0.78
0 -1 -10 1.31 0.76
0 1 10 -0.32 0.82
0 1 10 0.41 0.54
0 1 11 107.54 4.30
0 1 11 106.80 4.06
0 1 11 104.50 4.37
0 -1 -11 108.19 4.24
0 -1 -12 399.45 13.55
0 1 12 388.02 13.36
0 1 12 376.48 13.60
0 -1 -12 381.08 13.68
0 1 12 390.62 13.69
0 -1 -13 1012.60 34.82
0 -1 -13 1087.01 34.75
0 1 13 1023.92 34.53
0 1 13 1058.59 34.80
0 1 13 1067.15 34.91
0 -1 -14 75.99 3.58
0 -1 -14 72.48 3.48
0 1 14 74.08 3.21
0 1 14 71.12 3.45
0 -1 -14 71.53 4.03
0 1 14 78.26 3.60
0 -1 -15 159.47 6.24
0 1 15 168.61 6.45
0 1 15 148.23 5.97
0 1 15 167.57 6.35
0 -1 -15 146.04 6.88
0 -1 -15 159.76 6.32
0 -1 -16 116.14 4.88
0 1 16 107.53 4.51
0 1 16 112.29 4.99
0 1 16 109.39 4.85
0 -1 -16 107.84 4.93
0 -1 -16 112.07 5.49
0 -1 -17 339.19 12.42
0 -1 -17 357.09 12.47
0 1 17 355.36 12.59
0 1 17 320.73 12.10
0 1 17 347.67 12.55
0 1 17 346.31 12.85
0 -1 -17 333.30 13.30
0 -1 -18 42.48 2.78
0 -1 -18 45.61 2.77
0 1 18 46.86 2.46
0 1 18 48.76 3.05
0 1 18 43.50 2.88
0 1 18 39.45 3.08
0 -1 -18 42.25 3.47
0 -1 -19 97.24 4.35
0 -1 -19 85.27 4.28
0 1 19 89.19 4.42
0 1 19 85.33 4.38
0 1 19 90.44 4.68
0 -1 -19 84.25 5.18
0 -1 -20 37.06 2.62
0 -1 -20 37.62 2.77
0 1 20 39.21 2.92
0 1 20 39.43 2.89
0 1 20 42.84 3.21
0 -1 -20 37.13 3.53
0 -1 -21 6.14 1.66
0 -1 -21 4.91 1.81
0 1 21 6.35 1.90
0 1 21 5.84 1.93
0 -1 -21 5.72 2.38
0 1 21 4.61 1.66
0 1 22 -1.40 1.76
0 -1 -22 -0.35 2.47
0 1 22 -0.73 1.71
0 1 23 -0.42 1.73
0 1 23 -1.61 1.91
0 -1 -23 0.92 2.66
0 -2 22 49.88 3.51
0 -2 22 56.83 3.55
0 -2 22 69.52 3.65
0 2 -22 65.56 4.90
0 -2 21 7.30 1.50
0 -2 21 10.43 1.91
0 -2 21 7.47 1.86
0 -2 21 7.05 1.80
0 -2 21 8.90 1.94
0 2 -21 8.15 2.67
0 -2 20 5.70 1.54
0 -2 20 5.00 1.46
0 -2 20 2.05 1.70
0 -2 20 2.73 1.67
0 -2 20 9.45 1.93
0 2 -20 5.60 2.42
0 -2 19 21.80 2.09
0 -2 19 13.34 2.00
0 -2 19 17.56 2.11
0 -2 19 26.51 2.38
0 -2 19 20.06 1.91
0 2 -19 25.22 3.03
0 2 -18 1.59 0.40
0 -2 18 2.45 1.54
0 -2 18 -0.30 1.66
0 -2 18 0.96 1.41
0 -2 18 2.34 1.68
0 2 -18 1.22 2.07
0 -2 18 1.42 1.21
0 2 -17 61.16 3.68
0 -2 17 63.08 3.27
0 2 -17 62.59 2.23
0 2 -17 54.22 2.29
0 -2 17 67.18 3.36
0 -2 17 62.60 3.30
0 2 -17 62.07 4.03
0 -2 17 74.56 3.50
0 -2 17 63.08 3.11
0 2 -16 74.56 3.94
0 -2 16 68.75 3.43
0 2 -16 72.09 2.60
0 2 -16 65.01 2.47
0 -2 16 70.19 3.40
0 -2 16 62.45 3.38
0 2 -16 64.41 4.08
0 -2 16 73.91 3.62
0 -2 16 69.73 3.29
0 2 -15 -0.19 1.58
0 -2 15 -0.68 1.30
0 2 -15 1.14 0.61
0 2 -15 0.61 0.45
0 -2 15 -0.12 1.23
0 -2 15 0.98 1.26
0 -2 15 1.37 1.26
0 2 -15 0.11 1.90
0 -2 15 1.02 1.12
0 2 -14 54.78 3.26
0 -2 14 55.10 2.84
0 2 -14 57.25 2.22
0 2 -14 53.58 2.04
0 -2 14 59.05 2.92
0 -2 14 53.73 2.85
0 -2 14 59.86 3.03
0 2 -14 56.67 3.51
0 -2 14 51.05 2.73
0 -2 13 -0.59 1.13
0 2 -13 -0.68 0.65
0 2 -13 0.38 0.39
0 -2 13 -0.53 1.24
0 -2 13 -0.63 1.05
0 2 -13 -1.62 1.54
0 -2 13 -0.30 1.15
0 2 -13 -0.70 1.29
0 -2 12 237.17 8.80
0 2 -12 233.42 8.33
0 2 -12 248.66 8.16
0 -2 12 250.43 8.85
0 -2 12 233.91 8.83
0 -2 12 240.53 8.90
0 2 -12 244.53 9.35
0 2 -12 236.14 9.16
0 -2 11 304.31 11.90
0 2 -11 347.04 11.29
0 2 -11 343.26 11.43
0 -2 11 333.06 11.89
0 2 -11 311.69 12.31
0 -2 11 341.60 11.99
0 2 -11 324.52 12.15
0 2 -10 102.61 3.46
0 -2 10 92.15 4.02
0 2 -10 102.50 3.59
0 -2 10 98.90 4.00
0 -2 10 101.92 4.10
0 2 -10 96.42 4.35
0 2 -10 95.28 4.24
0 -2 9 32.15 1.73
0 -2 9 26.46 1.69
0 2 -9 32.32 1.18
0 -2 9 29.59 1.72
0 2 -9 31.92 2.00
0 2 -9 32.70 1.30
0 2 -8 443.28 14.60
0 -2 8 425.95 14.36
0 -2 8 387.87 14.25
0 -2 8 422.34 14.38
0 -2 7 411.65 14.48
0 2 -7 427.07 14.64
0 -2 7 429.00 14.46
0 -2 6 390.41 13.38
0 2 -6 393.37 13.45
0 -2 6 388.01 13.31
0 -2 5 1114.02 38.56
0 2 -5 1182.59 38.60
0 -2 5 1173.06 38.48
0 -2 4 49.05 1.95
0 2 -4 51.16 2.04
0 2 -3 204.91 7.13
0 -2 3 210.97 7.10
0 -2 2 296.31 10.27
0 2 -2 308.63 10.27
0 -2 2 310.01 10.23
0 -2 1 1435.58 43.97
0 2 -1 1246.85 43.90
0 2 0 356.55 11.94
0 2 1 100.24 3.77
0 -2 -1 116.83 3.79
0 2 2 1645.87 52.66
0 -2 -2 1551.17 52.64
0 -2 -2 1571.65 52.67
0 2 3 179.60 6.28
0 -2 -3 182.53 6.24
0 2 3 172.75 6.23
0 2 4 253.31 8.48
0 -2 -4 239.52 8.34
0 2 4 235.34 8.37
0 2 5 99.45 3.88
0 2 5 101.37 3.76
0 -2 -5 99.65 3.68
0 -2 -5 98.98 3.59
0 2 6 348.26 12.32
0 -2 -6 364.01 11.98
0 -2 -6 357.60 12.09
0 2 6 337.27 12.15
0 -2 -7 6.79 0.64
0 2 7 4.87 1.04
0 2 7 5.69 0.83
0 2 7 4.98 0.74
0 -2 -7 5.94 0.73
0 -2 -8 90.38 3.27
0 2 8 79.59 3.66
0 -2 -8 87.22 3.38
0 2 8 85.25 3.48
0 2 8 87.86 3.52
0 2 9 159.37 6.08
0 -2 -9 163.02 5.97
0 -2 -9 166.18 5.87
0 2 9 168.52 6.17
0 2 10 196.10 7.13
0 -2 -10 183.28 6.93
0 2 10 195.49 7.05
0 2 11 1130.79 37.86
0 -2 -11 1131.72 37.64
0 2 11 1102.69 37.76
0 -2 -12 522.12 17.57
0 2 12 530.39 17.81
0 -2 -12 494.91 17.85
0 2 12 491.47 17.70
0 -2 -13 1201.85 39.22
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-10 -2 12 116.39 5.69
10 2 -12 106.72 4.76
-10 -2 11 54.81 3.71
-10 -2 11 61.67 3.68
-10 -2 11 60.36 3.05
-10 -2 11 60.45 3.97
10 2 -11 59.97 3.17
-10 -2 10 3.13 1.88
-10 -2 10 0.09 1.67
-10 -2 10 1.87 1.11
-10 -2 10 -0.11 1.93
-10 -2 10 0.51 1.99
10 2 -10 0.99 1.34
-10 -2 9 23.74 2.58
-10 -2 9 22.94 1.64
-10 -2 9 24.78 2.67
-10 -2 9 20.95 2.80
10 2 -9 20.38 1.97
-10 -2 8 252.74 9.78
-10 -2 8 236.90 8.83
-10 -2 8 253.44 10.03
-10 -2 8 253.51 10.23
10 2 -8 254.68 9.32
-10 -2 7 66.16 3.79
-10 -2 7 71.69 4.14
10 2 -7 66.23 3.42
-10 -2 7 63.62 2.79
-10 -2 7 71.46 4.06
-10 -2 6 321.18 11.95
-10 -2 6 326.10 12.18
10 2 -6 332.87 11.52
10 2 -6 300.72 10.64
-10 -2 6 318.53 10.79
-10 -2 6 322.15 12.11
-10 -2 5 6.84 1.80
10 2 -5 8.73 1.65
-10 -2 5 6.92 1.78
10 2 -5 7.01 1.18
10 2 -5 7.19 0.86
-10 -2 5 7.67 0.78
-10 -2 5 8.08 1.93
-10 -2 4 50.55 3.19
10 2 -4 55.36 2.97
10 2 -4 49.83 2.72
10 2 -4 52.47 2.41
-10 -2 4 54.81 2.03
-10 -2 4 54.25 3.37
-10 -2 3 263.02 9.75
10 2 -3 262.98 9.40
10 2 -3 252.51 9.18
10 2 -3 242.01 8.92
-10 -2 3 247.56 8.34
-10 -2 3 280.03 9.91
10 2 -2 72.29 3.51
10 2 -2 73.01 3.40
10 2 -2 64.55 3.10
-10 -2 2 75.32 3.89
-10 -2 2 70.00 3.69
10 2 -1 253.65 9.56
-10 -2 1 275.01 10.06
10 2 -1 268.96 9.80
10 2 0 0.48 1.11
10 2 0 -0.40 1.28
-10 -2 0 1.86 1.47
10 2 0 2.08 1.30
10 2 1 101.61 4.72
-10 -2 -1 113.13 4.76
10 2 1 112.99 4.86
10 2 1 117.28 4.70
-10 -2 -2 113.26 4.79
10 2 2 111.71 4.71
10 2 2 110.04 3.89
10 2 2 108.70 4.88
10 2 3 21.90 1.83
10 2 3 17.66 1.96
10 2 3 20.00 1.13
-10 -2 -3 22.86 1.99
-10 -2 -4 127.27 5.30
-10 -2 -4 132.73 5.34
-10 -2 -4 117.41 4.57
10 2 4 125.54 5.23
10 2 4 125.06 5.41
10 2 4 117.68 4.48
10 2 5 77.43 3.30
-10 -2 -5 89.27 4.03
-10 -2 -5 87.70 4.07
-10 -2 -5 77.41 3.29
10 2 5 81.58 4.03
-10 -2 -5 91.92 3.82
10 2 5 86.20 4.22
10 2 6 317.34 10.93
-10 -2 -6 324.93 11.63
-10 -2 -6 315.15 11.69
-10 -2 -6 311.64 10.91
10 2 6 306.44 11.71
-10 -2 -6 320.45 11.41
10 2 6 307.49 11.81
10 2 7 4.97 1.50
-10 -2 -7 4.08 1.52
-10 -2 -7 3.27 1.51
-10 -2 -7 2.71 0.99
10 2 7 3.15 1.54
-10 -2 -7 3.78 1.48
10 2 7 3.86 0.98
10 2 8 2.31 1.54
-10 -2 -8 1.86 1.64
-10 -2 -8 2.50 1.59
-10 -2 -8 4.31 1.02
10 2 8 3.43 1.63
-10 -2 -8 2.54 1.54
10 2 8 4.85 0.97
-10 -2 -9 4.06 1.62
-10 -2 -9 5.21 1.69
-10 -2 -9 6.80 1.10
10 2 9 7.98 1.82
-10 -2 -9 6.54 1.65
10 2 9 3.48 0.98
-10 -2 -10 10.59 1.73
-10 -2 -10 14.03 1.99
-10 -2 -10 15.61 1.42
10 2 10 18.37 2.18
-10 -2 -10 17.15 2.01
10 2 10 12.38 1.26
-10 -2 -11 137.14 5.70
-10 -2 -11 135.70 6.06
-10 -2 -11 133.75 5.38
10 2 11 135.94 6.17
-10 -2 -11 145.02 6.12
10 2 11 128.17 5.12
-10 -2 -12 10.30 1.52
-10 -2 -12 8.10 2.24
-10 -2 -12 14.39 1.80
10 2 12 10.06 2.33
10 2 12 15.13 1.43
-10 -2 -12 12.75 2.27
10 2 12 10.59 2.21
10 2 13 245.66 9.02
-10 -2 -13 260.22 9.51
-10 -2 -13 252.83 9.39
10 2 13 230.49 10.14
-10 -2 -13 248.99 10.24
10 2 13 263.28 10.27
10 2 14 22.09 1.82
-10 -2 -14 21.07 2.16
10 2 14 28.53 2.78
-10 -2 -14 22.26 2.99
-10 -2 -14 26.30 2.17
-10 -2 -15 2.30 1.50
-10 -2 -15 2.05 1.50
10 2 15 4.16 1.98
-10 -2 -15 -0.14 2.48
10 2 15 1.71 1.21
-10 -2 -16 30.99 2.65
10 2 16 34.08 2.25
-10 -2 -16 37.33 2.58
-10 -2 -16 41.55 3.31
10 2 16 31.17 3.33
-10 -2 -16 29.12 3.68
10 2 16 37.85 3.29
-10 -2 -17 1.34 1.84
-10 -2 -17 2.44 2.22
-10 -2 -17 1.51 1.65
10 2 17 1.02 1.67
10 2 17 5.29 2.36
10 2 17 2.15 2.22
-10 -2 -17 -0.69 3.08
10 2 17 2.82 1.46
-10 -2 -18 15.48 2.28
-10 -2 -18 15.14 2.02
10 2 18 15.65 1.98
10 2 18 19.28 2.83
10 2 18 15.13 2.81
-10 -2 -18 15.13 3.30
10 2 18 18.83 1.96
-10 -2 -19 15.21 2.22
-10 -2 -19 15.29 1.87
10 2 19 14.74 2.89
-10 -2 -19 10.61 2.99
10 2 19 14.01 1.95
10 2 19 18.49 2.78
10 2 19 14.42 1.80
10 2 20 0.45 1.72
10 2 20 1.36 2.23
10 2 20 1.41 1.50
10 2 21 2.22 1.69
10 3 -19 34.48 3.50
10 3 -18 36.93 3.48
-10 -3 18 36.84 3.63
-10 -3 18 35.79 3.11
-10 -3 18 36.75 3.28
-10 -3 18 31.93 2.40
10 3 -17 64.72 4.35
-10 -3 17 60.74 3.19
-10 -3 17 65.82 4.36
-10 -3 17 52.91 3.58
-10 -3 17 68.03 4.15
-10 -3 16 5.57 2.15
-10 -3 16 4.28 1.84
10 3 -16 3.45 1.40
-10 -3 16 3.26 1.97
-10 -3 16 4.43 1.25
-10 -3 16 5.38 2.33
10 3 -16 5.14 2.32
-10 -3 15 1.90 1.94
-10 -3 15 0.34 1.56
10 3 -15 0.99 1.39
-10 -3 15 2.18 2.01
-10 -3 15 -0.11 1.28
-10 -3 15 1.05 2.20
10 3 -15 1.42 2.08
-10 -3 14 123.85 5.49
-10 -3 14 127.50 5.94
10 3 -14 127.25 5.23
-10 -3 14 111.57 5.71
-10 -3 14 122.15 4.98
-10 -3 14 135.92 6.44
10 3 -14 128.65 6.03
10 3 -13 -0.57 1.36
-10 -3 13 -0.21 1.78
-10 -3 13 0.78 1.37
10 3 -13 0.64 1.91
-10 -3 13 0.12 2.11
-10 -3 13 0.10 1.80
10 3 -12 19.32 1.92
-10 -3 12 19.39 2.33
-10 -3 12 18.84 1.83
-10 -3 12 16.26 2.57
-10 -3 12 17.38 2.31
10 3 -11 250.07 9.53
-10 -3 11 269.32 10.10
-10 -3 11 251.86 9.42
-10 -3 11 271.31 10.41
-10 -3 11 242.95 9.95
-10 -3 10 39.08 3.35
10 3 -10 38.92 2.61
-10 -3 10 43.13 3.02
-10 -3 10 45.17 2.36
-10 -3 10 44.22 3.21
-10 -3 10 41.40 3.02
10 3 -9 11.13 1.59
-10 -3 9 7.03 2.16
-10 -3 9 10.47 1.27
-10 -3 9 10.73 1.89
-10 -3 9 8.90 2.12
-10 -3 9 10.58 1.89
-10 -3 8 146.27 6.67
10 3 -8 146.08 5.83
-10 -3 8 134.54 5.35
-10 -3 8 145.86 6.08
-10 -3 8 147.84 6.48
-10 -3 8 146.59 6.23
10 3 -7 0.57 1.40
-10 -3 7 1.32 2.01
-10 -3 7 2.81 1.70
-10 -3 7 1.15 0.84
-10 -3 7 1.42 1.86
-10 -3 6 157.65 5.39
-10 -3 6 162.86 6.94
10 3 -6 166.89 6.31
-10 -3 6 160.36 6.60
10 3 -6 144.45 5.33
-10 -3 6 155.20 5.50
-10 -3 6 166.01 6.77
-10 -3 5 417.59 13.89
-10 -3 5 415.97 15.10
10 3 -5 400.40 14.12
-10 -3 5 420.46 15.43
10 3 -5 411.72 14.79
-10 -3 5 419.31 13.96
-10 -3 5 438.26 15.24
10 3 -4 3.55 1.26
10 3 -4 2.34 0.86
-10 -3 4 2.16 1.52
-10 -3 4 1.62 1.63
10 3 -3 2.16 1.34
10 3 -3 1.61 1.17
10 3 -3 2.46 0.95
-10 -3 3 1.01 1.41
-10 -3 3 0.99 1.58
10 3 -2 229.46 8.41
10 3 -2 215.14 8.24
10 3 -2 211.03 7.98
-10 -3 2 218.48 8.53
-10 -3 2 230.65 8.65
10 3 -1 642.92 21.79
-10 -3 1 645.15 21.55
10 3 -1 602.03 21.73
10 3 -1 603.28 21.50
-10 -3 1 621.56 21.95
-10 -3 1 665.76 22.10
10 3 0 312.39 11.94
10 3 0 331.07 12.18
-10 -3 0 353.60 12.00
-10 -3 0 349.64 12.34
10 3 1 26.17 1.97
10 3 1 26.45 2.12
-10 -3 -1 31.16 2.01
-10 -3 -1 29.72 2.21
10 3 2 392.81 14.44
10 3 2 405.11 14.65
-10 -3 -2 421.77 14.44
-10 -3 -3 40.08 2.41
10 3 3 40.25 2.47
10 3 3 37.65 2.56
10 3 3 36.66 1.41
-10 -3 -4 6.91 1.50
-10 -3 -4 4.70 1.41
-10 -3 -4 5.35 0.84
10 3 4 5.09 1.44
10 3 4 4.25 1.38
-10 -3 -4 8.59 1.28
10 3 4 5.68 0.66
10 3 5 202.44 6.74
-10 -3 -5 190.59 7.50
-10 -3 -5 189.37 7.47
-10 -3 -5 183.32 6.77
10 3 5 182.64 7.59
-10 -3 -5 205.11 7.31
10 3 5 180.15 7.71
10 3 6 61.96 2.46
-10 -3 -6 65.90 3.28
-10 -3 -6 57.15 3.21
-10 -3 -6 54.33 2.53
10 3 6 60.63 3.40
-10 -3 -6 67.94 3.10
10 3 6 55.32 3.35
-10 -3 -7 16.32 1.89
-10 -3 -7 15.38 1.71
-10 -3 -7 12.18 1.18
10 3 7 16.59 1.94
10 3 7 13.49 1.91
-10 -3 -7 17.12 1.77
10 3 7 18.03 1.13
10 3 8 103.27 4.16
-10 -3 -8 121.84 4.93
-10 -3 -8 117.78 5.07
-10 -3 -8 115.30 4.28
10 3 8 106.74 5.13
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10 3 8 103.91 5.12
-10 -3 -9 198.87 7.42
-10 -3 -9 190.67 7.57
-10 -3 -9 186.84 6.83
10 3 9 190.12 7.79
-10 -3 -9 178.67 7.41
10 3 9 180.87 6.68
-10 -3 -10 191.77 7.74
-10 -3 -10 205.69 7.56
-10 -3 -10 192.46 7.04
10 3 10 196.79 8.01
-10 -3 -10 185.16 7.78
10 3 10 180.18 6.85
-10 -3 -11 12.15 1.49
-10 -3 -11 13.48 2.06
-10 -3 -11 17.36 1.94
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10 3 11 13.84 1.33
-10 -3 -12 15.83 1.50
-10 -3 -12 12.54 2.08
-10 -3 -12 14.35 1.84
10 3 12 8.67 2.13
10 3 12 9.34 2.19
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10 3 12 10.63 1.33
-10 -3 -13 0.29 1.16
-10 -3 -13 0.42 1.53
10 3 13 -0.24 1.78
10 3 13 -2.29 2.37
-10 -3 -13 -0.97 2.18
10 3 13 0.31 1.17
10 3 14 36.46 2.19
-10 -3 -14 40.21 2.60
10 3 14 35.23 3.08
-10 -3 -14 27.81 3.33
-10 -3 -14 34.64 2.33
10 3 15 -0.13 1.84
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-10 -3 -16 1.60 1.46
-10 -3 -16 2.25 1.54
-10 -3 -16 -0.68 1.90
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10 3 16 1.45 1.27
-10 -3 -17 50.93 3.30
-10 -3 -17 59.31 3.84
-10 -3 -17 54.89 3.21
10 3 17 55.39 2.94
10 3 17 58.69 4.09
10 3 17 55.39 4.16
-10 -3 -17 51.38 4.47
10 3 17 57.98 3.06
10 3 18 167.41 6.58
-10 -3 -18 173.80 6.81
-10 -3 -18 166.69 7.59
10 3 18 171.91 6.48
10 3 18 161.17 7.73
10 3 18 157.88 7.90
-10 -3 -18 143.36 8.16
-10 -3 -18 155.41 6.88
-10 -3 -19 17.67 2.30
-10 -3 -19 24.36 2.26
10 3 19 22.27 2.05
10 3 19 20.91 3.02
10 3 19 22.76 3.21
-10 -3 -19 19.90 3.46
10 3 19 24.97 2.31
-10 -3 -20 3.40 1.62
10 3 20 4.76 2.33
10 3 20 5.36 1.58
10 3 21 -0.15 1.61
10 4 -20 1.50 2.61
-10 -4 19 20.37 2.06
10 4 -19 23.09 3.06
10 4 -18 68.37 4.52
-10 -4 18 78.08 4.30
-10 -4 18 70.03 4.43
-10 -4 18 63.53 3.88
-10 -4 18 57.88 3.26
10 4 -17 31.97 3.35
-10 -4 17 32.91 2.24
-10 -4 17 35.02 3.24
-10 -4 17 33.21 2.74
-10 -4 17 37.83 3.01
10 4 -16 1.15 1.38
10 4 -16 4.50 2.17
-10 -4 16 3.12 1.31
-10 -4 16 2.91 2.31
-10 -4 16 2.34 1.69
-10 -4 16 5.56 2.06
-10 -4 15 21.08 2.52
-10 -4 15 20.55 2.06
10 4 -15 19.03 1.77
-10 -4 15 22.42 2.33
-10 -4 15 17.87 1.75
-10 -4 15 22.16 2.81
10 4 -15 21.98 2.62
-10 -4 14 93.07 4.30
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10 4 -14 85.56 3.89
-10 -4 14 88.61 4.48
-10 -4 14 83.25 3.77
-10 -4 14 89.27 4.85
10 4 -14 84.28 4.68
-10 -4 13 6.53 1.86
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10 4 -13 9.05 1.39
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10 4 -13 9.77 2.21
-10 -4 12 15.08 1.43
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-10 -4 12 21.15 2.34
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10 4 -12 19.03 1.79
10 4 -11 82.73 3.83
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-10 -4 11 80.38 3.39
-10 -4 11 86.64 4.62
-10 -4 11 79.40 3.75
-10 -4 11 87.71 4.35
10 4 -10 57.15 3.09
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-10 -4 10 59.45 3.44
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-10 -4 10 62.79 3.51
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-10 -4 9 14.01 1.97
-10 -4 9 11.90 1.91
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-10 -4 9 9.38 1.97
10 4 -9 8.72 1.63
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-10 -4 8 120.91 5.19
-10 -4 8 113.21 4.45
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10 4 -8 115.61 4.88
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-10 -4 7 1.05 0.77
-10 -4 7 0.51 1.45
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10 4 -7 0.91 1.37
-10 -4 7 0.32 2.05
-10 -4 6 668.30 22.05
-10 -4 6 665.54 23.53
10 4 -6 677.56 22.90
-10 -4 6 675.53 23.21
-10 -4 6 640.04 22.18
-10 -4 6 668.90 22.99
-10 -4 6 673.05 23.29
-10 -4 5 1.67 0.41
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10 4 -5 2.45 0.78
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-10 -4 5 -0.08 1.96
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10 4 -4 420.53 14.74
-10 -4 3 40.63 2.08
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10 4 -3 38.02 2.05
-10 -4 2 143.82 5.66
10 4 -2 147.60 5.69
-10 -4 2 153.86 6.30
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-10 -4 1 5.59 1.16
10 4 -1 6.21 1.53
10 4 -1 6.63 1.33
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-10 -4 1 4.91 1.52
10 4 0 321.72 11.70
10 4 0 306.03 11.93
-10 -4 0 337.61 11.63
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10 4 1 6.82 1.42
-10 -4 -1 8.89 1.28
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10 4 2 4.22 1.46
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10 4 3 6.55 1.55
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-10 -4 -4 26.81 2.02
-10 -4 -4 28.34 1.37
10 4 4 26.99 2.27
10 4 4 26.24 2.17
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-10 -4 -5 118.98 5.13
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10 4 5 110.98 5.26
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10 4 6 6.64 1.67
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10 4 7 3.66 1.48
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10 4 8 9.93 1.84
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-10 -4 -11 183.82 6.95
-10 -4 -11 202.30 7.84
-10 -4 -11 204.80 7.55
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10 4 11 189.10 6.90
-10 -4 -12 173.34 6.66
-10 -4 -12 188.83 7.48
-10 -4 -12 196.65 7.19
10 4 12 178.01 7.75
10 4 12 181.06 7.92
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10 4 12 171.61 6.59
-10 -4 -13 1.73 1.17
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10 4 13 -1.12 2.39
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10 4 15 6.79 1.95
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-10 -4 -15 4.24 2.55
10 4 15 6.87 1.39
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10 4 16 -0.92 1.32
-10 -4 -16 -0.63 2.12
10 4 16 -0.74 1.36
-10 -4 -17 72.01 3.70
-10 -4 -17 73.53 4.51
-10 -4 -17 81.01 3.91
10 4 17 79.59 3.45
10 4 17 66.30 4.60
10 4 17 70.84 4.84
-10 -4 -17 65.72 5.06
10 4 17 73.18 3.60
-10 -4 -18 1.44 2.29
-10 -4 -18 0.53 1.79
10 4 18 1.03 2.35
10 4 18 2.59 1.49
10 4 18 1.42 2.53
-10 -4 -18 2.75 2.86
10 4 18 -0.71 1.57
-10 -4 -19 47.19 3.01
10 4 19 44.05 3.92
10 4 19 46.58 4.02
-10 -4 -19 43.51 4.33
10 4 19 48.56 2.98
10 4 20 -1.10 2.41
-10 -4 -20 -3.16 3.16
-10 -4 -20 -0.86 1.55
10 4 20 -0.65 1.62
10 4 21 0.93 1.59
10 5 -20 4.38 2.53
10 5 -19 56.63 4.28
-10 -5 19 59.18 4.31
10 5 -18 5.43 2.52
-10 -5 18 5.46 2.24
-10 -5 18 2.36 1.44
-10 -5 17 65.34 4.14
-10 -5 17 66.51 4.21
-10 -5 17 61.14 3.16
10 5 -17 71.19 4.30
-10 -5 16 20.33 1.79
10 5 -16 18.71 2.57
-10 -5 16 19.89 2.59
-10 -5 16 24.61 2.60
-10 -5 15 3.33 1.86
-10 -5 15 1.98 1.24
-10 -5 15 0.64 1.48
-10 -5 15 3.28 1.86
10 5 -15 1.77 1.91
-10 -5 14 26.89 2.42
-10 -5 14 26.34 1.84
-10 -5 14 23.89 2.33
-10 -5 14 25.51 2.70
10 5 -14 27.08 2.74
-10 -5 13 3.91 1.72
-10 -5 13 5.51 1.21
-10 -5 13 3.36 1.69
-10 -5 13 5.43 2.04
10 5 -13 4.75 1.92
-10 -5 12 147.88 6.29
-10 -5 12 141.74 5.37
-10 -5 12 134.37 6.08
-10 -5 12 140.17 6.42
10 5 -12 143.23 6.32
-10 -5 11 5.89 1.75
-10 -5 11 6.52 1.11
-10 -5 11 2.16 1.98
-10 -5 11 5.78 1.73
-10 -5 10 35.99 1.78
-10 -5 10 33.78 2.55
-10 -5 10 33.45 2.58
-10 -5 10 31.03 2.76
-10 -5 10 31.10 3.00
-10 -5 9 12.85 1.06
-10 -5 9 13.11 1.86
-10 -5 9 11.56 1.80
-10 -5 9 13.28 1.99
-10 -5 9 12.25 2.28
-10 -5 8 96.26 3.59
-10 -5 8 97.95 4.48
-10 -5 8 99.97 3.87
-10 -5 8 96.38 4.45
-10 -5 8 91.04 3.83
-10 -5 8 97.51 4.70
-10 -5 8 95.62 4.96
-10 -5 7 6.53 0.72
-10 -5 7 4.21 1.59
-10 -5 7 5.24 1.48
-10 -5 7 6.28 0.94
-10 -5 7 2.25 1.76
-10 -5 7 5.50 1.08
-10 -5 7 5.00 2.05
-10 -5 6 130.81 4.59
-10 -5 6 141.94 6.09
-10 -5 6 140.60 5.71
-10 -5 6 131.88 5.47
-10 -5 6 126.47 4.73
-10 -5 6 129.08 5.63
-10 -5 6 135.29 5.11
-10 -5 5 372.63 12.42
-10 -5 5 373.88 13.48
10 5 -5 365.57 12.75
-10 -5 5 378.47 12.71
-10 -5 5 391.24 13.92
-10 -5 5 386.54 13.30
-10 -5 5 360.30 12.47
-10 -5 5 384.69 13.53
-10 -5 5 378.23 13.06
-10 -5 4 65.76 3.43
10 5 -4 64.70 2.90
-10 -5 4 67.79 2.83
-10 -5 4 69.74 3.27
-10 -5 4 68.73 3.53
-10 -5 4 69.40 3.12
-10 -5 3 133.14 5.54
10 5 -3 120.50 5.11
-10 -5 3 138.87 4.96
-10 -5 3 113.41 5.22
-10 -5 3 146.77 5.70
-10 -5 3 129.31 5.16
-10 -5 2 52.78 2.98
10 5 -2 51.45 2.70
-10 -5 2 53.98 2.56
-10 -5 2 54.37 2.69
-10 -5 2 56.59 2.78
-10 -5 2 61.76 3.08
-10 -5 1 302.15 10.62
-10 -5 1 306.53 11.04
-10 -5 1 293.95 10.79
-10 -5 1 315.37 11.00
10 5 -1 280.78 10.75
-10 -5 0 121.29 4.88
-10 -5 0 123.92 5.20
-10 -5 0 124.02 5.05
10 5 0 122.69 5.05
-10 -5 -1 82.52 3.51
10 5 1 77.93 3.67
-10 -5 -1 82.61 3.80
-10 -5 -1 75.62 3.64
-10 -5 -2 10.25 1.45
10 5 2 10.20 1.62
10 5 2 8.41 1.64
-10 -5 -2 11.74 1.67
-10 -5 -2 8.80 1.39
-10 -5 -3 452.85 15.15
-10 -5 -3 392.99 15.16
10 5 3 422.23 15.34
-10 -5 -3 441.99 15.29
-10 -5 -3 472.49 14.93
-10 -5 -3 414.84 14.42
10 5 3 431.63 15.51
10 5 4 10.43 0.60
10 5 4 9.63 1.77
-10 -5 -4 10.73 0.76
-10 -5 -4 9.46 1.57
-10 -5 -4 10.64 1.42
10 5 4 6.71 1.68
-10 -5 -4 12.25 1.38
10 5 4 9.44 0.64
10 5 5 4.47 0.55
-10 -5 -5 1.29 1.54
10 5 5 1.53 1.48
-10 -5 -5 3.18 0.58
-10 -5 -5 2.99 1.30
10 5 5 2.30 1.78
-10 -5 -5 6.82 1.64
10 5 5 2.37 0.74
10 5 6 18.71 1.03
-10 -5 -6 17.63 1.86
-10 -5 -6 17.52 1.71
10 5 6 19.49 2.04
-10 -5 -6 19.24 0.96
10 5 6 18.23 2.01
-10 -5 -6 18.96 1.77
-10 -5 -6 18.04 1.69
10 5 6 19.41 1.26
10 5 7 4.61 1.02
-10 -5 -7 5.40 1.30
-10 -5 -7 2.48 1.41
10 5 7 5.27 1.45
-10 -5 -7 5.77 0.61
10 5 7 4.69 1.56
-10 -5 -7 6.05 1.30
10 5 7 4.78 0.72
10 5 8 2.25 1.05
-10 -5 -8 2.64 0.57
-10 -5 -8 2.19 1.27
-10 -5 -8 1.19 1.37
10 5 8 -0.10 1.50
10 5 8 2.45 1.53
-10 -5 -8 2.70 1.33
10 5 8 3.15 0.74
-10 -5 -9 0.65 0.64
10 5 9 -0.39 1.21
10 5 9 1.66 1.53
-10 -5 -9 1.07 1.24
-10 -5 -9 -0.08 1.52
-10 -5 -9 -0.16 1.38
10 5 9 0.89 0.89
-10 -5 -10 32.90 2.58
-10 -5 -10 37.89 2.48
-10 -5 -10 27.08 2.52
10 5 10 30.06 2.20
-10 -5 -10 32.21 1.63
10 5 10 29.95 2.71
-10 -5 -11 324.13 11.72
-10 -5 -11 338.64 11.52
10 5 11 314.62 12.18
-10 -5 -11 283.14 11.83
-10 -5 -11 301.10 10.81
-10 -5 -12 104.25 4.87
-10 -5 -12 120.22 4.79
10 5 12 98.76 5.27
10 5 12 111.56 5.44
-10 -5 -12 82.85 5.16
-10 -5 -12 90.44 3.99
-10 -5 -13 198.88 7.06
10 5 13 163.99 7.63
10 5 13 174.67 7.71
-10 -5 -13 161.09 7.64
-10 -5 -13 159.33 6.35
-10 -5 -14 -3.18 2.45
-10 -5 -14 0.96 1.65
10 5 14 -0.39 1.93
-10 -5 -15 -0.29 2.17
-10 -5 -15 -0.22 1.56
10 5 15 0.81 1.93
-10 -5 -16 16.87 2.06
-10 -5 -16 11.22 2.28
10 5 16 14.00 2.59
10 5 16 12.91 1.42
-10 -5 -16 11.23 2.62
10 5 16 13.27 1.67
-10 -5 -17 8.10 1.95
-10 -5 -17 3.60 2.08
10 5 17 0.29 2.34
10 5 17 4.44 1.29
10 5 17 0.15 2.29
-10 -5 -17 4.71 2.69
10 5 17 4.39 1.52
-10 -5 -18 27.58 2.94
-10 -5 -18 28.83 2.54
10 5 18 29.62 3.37
10 5 18 28.19 1.96
10 5 18 23.34 3.22
-10 -5 -18 23.14 3.44
10 5 18 28.67 2.30
-10 -5 -19 7.14 1.92
10 5 19 7.59 2.57
10 5 19 5.57 2.59
-10 -5 -19 6.23 2.95
10 5 19 9.00 1.85
10 5 20 -1.43 2.32
-10 -5 -20 1.67 2.96
10 5 20 -1.11 1.54
-10 -5 -20 -2.17 1.77
10 5 21 -0.23 1.74
-10 -5 -21 0.41 1.64
10 6 -19 11.39 2.65
-10 -6 18 2.28 2.31
-10 -6 18 3.73 1.52
10 6 -18 -0.13 2.22
-10 -6 17 0.65 1.32
-10 -6 17 -2.77 2.43
-10 -6 17 -0.44 1.96
10 6 -17 -0.85 2.05
-10 -6 16 1.17 1.18
-10 -6 16 3.35 1.86
-10 -6 16 -0.52 1.91
10 6 -16 1.81 1.97
-10 -6 15 1.80 1.14
10 6 -15 2.44 1.81
-10 -6 15 1.15 1.62
-10 -6 15 0.20 1.90
-10 -6 14 26.04 1.84
-10 -6 14 31.33 2.35
-10 -6 14 30.09 2.62
-10 -6 14 32.14 2.64
10 6 -14 30.14 2.74
-10 -6 13 80.48 3.40
-10 -6 13 69.06 3.86
-10 -6 13 82.38 4.24
-10 -6 13 80.73 4.25
10 6 -13 74.62 4.20
-10 -6 12 239.58 8.37
-10 -6 12 219.49 8.91
-10 -6 12 230.80 9.13
-10 -6 12 232.72 9.32
10 6 -12 234.99 9.13
-10 -6 11 143.06 5.88
-10 -6 11 138.61 5.04
-10 -6 11 130.95 5.66
-10 -6 11 138.40 6.05
-10 -6 11 124.26 4.86
-10 -6 10 220.26 8.48
-10 -6 10 208.83 8.34
-10 -6 10 222.00 7.69
-10 -6 10 229.29 8.70
-10 -6 10 207.56 7.70
-10 -6 9 77.38 3.85
-10 -6 9 80.39 4.40
-10 -6 9 73.50 3.81
-10 -6 9 77.20 3.10
-10 -6 9 78.47 4.04
-10 -6 9 76.06 3.23
-10 -6 8 14.67 1.89
-10 -6 8 13.03 1.02
-10 -6 8 10.14 2.14
-10 -6 8 10.28 1.62
-10 -6 8 13.37 1.85
-10 -6 8 12.77 1.24
-10 -6 7 26.18 2.08
-10 -6 7 24.22 1.24
-10 -6 7 23.02 1.06
-10 -6 7 24.14 2.50
-10 -6 7 24.10 1.97
-10 -6 7 24.04 1.61
-10 -6 7 21.08 1.99
-10 -6 6 128.82 5.68
-10 -6 6 134.54 4.83
-10 -6 6 138.79 4.89
-10 -6 6 147.43 6.23
-10 -6 6 136.12 5.55
-10 -6 6 139.37 5.33
-10 -6 6 132.35 5.69
-10 -6 5 2.69 1.48
-10 -6 5 5.27 1.74
-10 -6 5 3.61 0.79
-10 -6 5 3.10 0.59
-10 -6 5 5.49 1.23
-10 -6 5 5.50 1.48
-10 -6 5 3.32 1.18
-10 -6 4 117.21 4.40
-10 -6 4 107.20 4.99
10 6 -4 116.39 4.58
-10 -6 4 115.90 4.72
-10 -6 4 119.14 4.97
-10 -6 4 117.58 4.75
-10 -6 3 34.07 1.94
-10 -6 3 34.15 2.42
10 6 -3 35.19 2.14
-10 -6 3 36.13 2.10
-10 -6 3 44.07 2.40
-10 -6 3 36.17 2.21
-10 -6 2 291.83 10.02
-10 -6 2 273.83 10.41
10 6 -2 270.67 10.22
-10 -6 2 289.36 10.04
-10 -6 2 277.19 10.29
-10 -6 2 289.19 10.34
-10 -6 1 51.23 2.45
-10 -6 1 50.39 2.77
10 6 -1 45.12 2.65
-10 -6 1 50.59 2.68
-10 -6 1 50.34 2.68
-10 -6 1 47.16 2.28
10 6 0 18.49 1.69
-10 -6 0 18.21 1.47
-10 -6 0 17.03 1.73
-10 -6 0 16.98 1.56
-10 -6 0 16.17 1.59
-10 -6 0 15.70 1.17
10 6 1 58.42 3.07
-10 -6 -1 62.18 2.86
-10 -6 -1 62.94 3.05
-10 -6 -1 61.44 3.07
-10 -6 -1 54.60 2.40
-10 -6 -2 242.68 9.03
-10 -6 -2 238.01 8.93
-10 -6 -2 257.49 8.87
10 6 2 233.35 9.09
-10 -6 -2 241.75 8.55
-10 -6 -2 232.95 8.24
-10 -6 -3 661.03 22.58
-10 -6 -3 693.37 22.52
-10 -6 -3 705.61 22.44
10 6 3 641.59 22.71
-10 -6 -3 627.87 21.65
-10 -6 -3 656.16 22.11
-10 -6 -3 647.60 21.58
-10 -6 -4 6.34 1.60
10 6 4 7.81 1.93
-10 -6 -4 9.87 1.55
-10 -6 -4 6.48 1.38
10 6 4 5.43 0.55
10 6 4 5.48 0.71
-10 -6 -5 284.22 10.47
-10 -6 -5 297.52 10.36
10 6 5 277.29 10.67
-10 -6 -5 258.43 10.02
10 6 5 283.97 9.67
-10 -6 -6 0.68 1.36
10 6 6 1.52 1.68
10 6 6 0.90 1.46
-10 -6 -6 1.62 1.39
-10 -6 -6 2.73 1.23
10 6 6 0.14 0.92
-10 -6 -7 148.16 5.95
-10 -6 -7 147.86 5.90
-10 -6 -7 145.40 5.75
10 6 7 133.51 6.19
10 6 7 138.13 6.21
-10 -6 -7 130.99 5.64
10 6 7 139.37 5.37
-10 -6 -8 128.72 5.07
-10 -6 -8 117.41 5.18
10 6 8 113.26 5.56
-10 -6 -8 110.30 5.03
10 6 8 118.43 4.77
10 6 8 114.43 5.48
-10 -6 -9 2.50 1.28
-10 -6 -9 0.89 1.50
10 6 9 0.67 1.17
-10 -6 -9 0.55 1.46
10 6 9 0.42 1.66
-10 -6 -10 40.88 2.52
-10 -6 -10 31.29 2.55
-10 -6 -10 31.71 2.69
10 6 10 36.84 2.38
10 6 10 34.35 2.89
-10 -6 -11 202.45 7.28
-10 -6 -11 180.70 7.41
10 6 11 176.24 7.88
-10 -6 -11 165.53 7.50
10 6 11 169.18 7.10
-10 -6 -12 76.87 3.77
-10 -6 -12 71.51 3.98
10 6 12 76.42 4.44
10 6 12 73.56 4.38
-10 -6 -12 62.07 4.23
10 6 12 73.06 3.83
-10 -6 -13 21.11 2.14
10 6 13 16.05 2.49
10 6 13 20.46 2.64
-10 -6 -13 13.67 2.43
10 6 13 19.15 2.21
-10 -6 -14 -1.97 1.55
-10 -6 -14 -1.17 2.17
10 6 14 -0.92 1.76
10 6 14 -0.39 2.04
-10 -6 -15 28.23 2.40
-10 -6 -15 23.63 3.03
10 6 15 22.83 2.54
10 6 15 20.80 2.77
-10 -6 -16 7.39 1.81
-10 -6 -16 4.80 2.00
10 6 16 3.80 2.07
10 6 16 4.41 1.16
-10 -6 -16 5.33 2.32
10 6 16 5.49 1.99
-10 -6 -17 1.44 1.72
-10 -6 -17 -0.89 2.10
10 6 17 -1.60 2.48
10 6 17 0.18 1.22
10 6 17 -0.32 2.47
-10 -6 -17 1.48 2.63
10 6 17 2.54 2.15
-10 -6 -18 22.36 2.79
-10 -6 -18 27.80 2.40
10 6 18 18.44 2.99
10 6 18 22.24 3.17
-10 -6 -18 23.87 3.43
10 6 18 23.78 2.98
10 6 19 7.76 2.69
-10 -6 -19 11.59 2.01
10 6 19 9.44 2.46
-10 -6 -19 10.47 3.01
-10 -6 -20 4.07 1.91
-10 -6 -20 5.91 3.15
10 6 20 6.12 2.55
-10 -6 -21 0.67 1.73
10 6 21 -0.88 1.68
-10 -7 17 46.99 3.36
10 7 -17 41.59 3.51
-10 -7 17 49.01 2.74
-10 -7 16 -0.40 1.77
10 7 -16 1.73 1.80
-10 -7 16 0.39 1.87
-10 -7 16 -0.46 1.25
-10 -7 15 -1.74 1.87
10 7 -15 2.42 1.69
-10 -7 15 -0.75 1.83
-10 -7 15 0.05 1.17
-10 -7 14 3.68 1.31
-10 -7 14 4.00 1.39
-10 -7 14 1.57 1.76
-10 -7 14 2.72 1.73
10 7 -14 3.85 1.82
-10 -7 13 51.06 2.48
-10 -7 13 43.29 2.79
-10 -7 13 46.16 3.10
-10 -7 13 49.95 3.22
10 7 -13 50.47 3.13
-10 -7 13 46.64 2.04
-10 -7 12 53.02 2.52
-10 -7 12 42.61 2.84
-10 -7 12 56.10 3.27
-10 -7 12 53.48 3.25
-10 -7 12 45.32 2.24
10 7 -12 60.36 3.24
-10 -7 11 100.66 4.02
-10 -7 11 94.42 4.44
-10 -7 11 105.59 4.77
-10 -7 11 102.39 4.72
-10 -7 11 96.74 3.93
-10 -7 10 28.71 2.40
-10 -7 10 31.25 2.33
-10 -7 10 31.05 1.79
-10 -7 10 35.71 2.46
-10 -7 10 33.12 1.83
-10 -7 9 1.90 1.58
-10 -7 9 3.46 0.98
-10 -7 9 5.50 1.99
-10 -7 9 3.69 1.42
-10 -7 9 4.56 1.55
-10 -7 9 3.88 1.02
-10 -7 8 95.96 3.59
-10 -7 8 88.31 4.16
-10 -7 8 88.99 3.23
-10 -7 8 93.16 4.74
-10 -7 8 93.43 4.23
-10 -7 8 95.33 4.21
-10 -7 8 94.61 3.87
-10 -7 7 3.01 0.78
-10 -7 7 2.82 1.41
-10 -7 7 2.46 1.62
-10 -7 7 4.06 1.07
-10 -7 7 1.86 0.62
-10 -7 7 1.35 1.44
-10 -7 7 4.18 1.27
-10 -7 6 1.80 0.68
-10 -7 6 0.27 1.33
-10 -7 6 1.18 1.62
-10 -7 6 1.64 1.05
-10 -7 6 -0.49 0.79
-10 -7 6 -0.28 1.29
-10 -7 6 0.48 1.28
-10 -7 5 270.87 10.55
-10 -7 5 298.58 10.99
-10 -7 5 287.29 10.01
-10 -7 5 296.70 10.46
-10 -7 5 287.30 10.45
-10 -7 5 289.19 9.84
-10 -7 5 283.99 10.37
-10 -7 4 8.51 0.72
-10 -7 4 10.13 1.58
-10 -7 4 11.80 1.16
-10 -7 4 10.93 1.40
-10 -7 4 10.13 1.30
-10 -7 4 9.10 1.41
-10 -7 3 49.82 2.78
10 7 -3 51.96 2.67
-10 -7 3 55.51 2.42
-10 -7 3 50.92 2.48
-10 -7 3 47.06 1.82
-10 -7 3 50.34 2.59
-10 -7 3 55.30 2.75
-10 -7 2 68.03 3.02
10 7 -2 62.22 3.40
-10 -7 2 75.36 3.13
-10 -7 2 67.79 3.39
-10 -7 2 75.37 3.46
-10 -7 2 72.09 3.21
10 7 -1 29.55 2.09
-10 -7 1 28.23 1.81
-10 -7 1 21.83 1.49
-10 -7 1 27.21 1.98
-10 -7 1 23.83 1.73
-10 -7 1 29.26 2.04
-10 -7 0 10.08 1.48
-10 -7 0 10.38 1.32
10 7 0 9.41 1.54
-10 -7 0 10.73 1.29
-10 -7 0 12.05 1.55
-10 -7 0 7.21 0.88
-10 -7 -1 225.98 8.73
-10 -7 -1 224.91 8.06
10 7 1 235.14 8.99
-10 -7 -1 248.44 8.73
-10 -7 -1 244.84 8.29
-10 -7 -1 251.54 8.95
-10 -7 -2 0.24 1.07
-10 -7 -2 1.35 0.40
-10 -7 -2 1.09 1.10
10 7 2 -1.56 1.62
-10 -7 -2 0.23 0.87
-10 -7 -2 0.28 1.22
-10 -7 -3 2.91 1.36
-10 -7 -3 2.43 1.37
-10 -7 -3 3.69 1.30
10 7 3 0.41 1.63
-10 -7 -3 2.41 1.07
10 7 3 1.73 0.53
-10 -7 -4 413.32 14.45
10 7 4 400.98 14.85
-10 -7 -4 434.78 14.56
-10 -7 -4 432.75 14.74
-10 -7 -4 364.43 14.05
10 7 4 413.19 13.75
-10 -7 -5 734.82 24.47
-10 -7 -5 653.20 23.90
10 7 5 700.34 23.62
-10 -7 -5 754.11 24.34
10 7 5 700.30 24.67
-10 -7 -6 158.19 6.18
-10 -7 -6 129.52 5.66
10 7 6 149.48 5.48
-10 -7 -6 146.48 6.01
10 7 6 149.56 6.45
-10 -7 -7 4.50 1.45
10 7 7 4.03 1.79
-10 -7 -7 3.52 1.41
-10 -7 -7 2.62 1.42
10 7 7 1.99 1.10
-10 -7 -8 186.20 7.04
10 7 8 167.87 7.41
-10 -7 -8 177.61 6.82
-10 -7 -8 155.72 6.84
10 7 8 174.49 6.61
10 7 9 20.76 2.44
-10 -7 -9 21.67 2.17
-10 -7 -9 27.69 2.02
-10 -7 -9 19.53 2.09
10 7 9 21.45 1.83
10 7 10 50.16 3.58
-10 -7 -10 54.40 3.25
-10 -7 -10 55.41 3.34
10 7 10 53.66 3.01
-10 -7 -11 69.96 3.91
10 7 11 67.01 4.32
-10 -7 -11 73.38 3.88
-10 -7 -11 70.27 3.99
10 7 11 68.60 3.58
-10 -7 -12 -0.38 1.78
10 7 12 -0.39 2.14
-10 -7 -12 -0.09 1.73
10 7 12 -1.19 1.66
-10 -7 -12 2.12 1.94
10 7 13 0.81 1.95
-10 -7 -13 -0.69 2.11
10 7 13 -0.87 1.59
-10 -7 -14 132.89 6.56
10 7 14 136.18 6.06
-10 -7 -15 1.92 2.58
10 7 15 4.97 2.12
-10 -7 -16 74.03 3.57
-10 -7 -16 69.79 3.90
-10 -7 -16 58.82 4.40
10 7 16 64.25 3.86
10 7 17 0.98 2.39
-10 -7 -17 5.36 1.90
-10 -7 -17 1.00 2.03
-10 -7 -17 -0.32 2.90
10 7 17 1.98 2.06
10 7 18 0.51 2.44
-10 -7 -18 4.02 1.91
-10 -7 -18 -0.86 2.86
10 7 18 -2.11 2.42
10 7 19 12.34 2.79
-10 -7 -19 16.40 2.13
10 7 19 10.19 2.52
-10 -7 -19 13.30 3.32
-10 -7 -20 14.49 2.15
10 7 20 10.38 2.52
-10 -7 -20 10.46 3.27
-10 -8 17 14.08 1.67
-10 -8 16 -1.07 1.95
10 8 -16 -0.62 1.72
-10 -8 16 -0.06 1.38
-10 -8 15 8.29 2.07
10 8 -15 10.53 1.98
-10 -8 15 8.20 1.78
-10 -8 15 6.20 1.40
-10 -8 14 5.62 1.95
10 8 -14 5.84 1.79
-10 -8 14 5.32 1.75
-10 -8 14 6.65 1.40
-10 -8 13 5.96 1.29
-10 -8 13 3.04 1.91
-10 -8 13 3.23 1.30
-10 -8 13 3.63 1.72
10 8 -13 5.73 1.76
-10 -8 12 50.23 2.52
-10 -8 12 45.22 3.06
-10 -8 12 46.08 2.69
-10 -8 12 48.55 2.94
10 8 -12 50.25 2.98
-10 -8 12 45.65 2.30
-10 -8 11 46.82 2.35
-10 -8 11 43.47 2.91
-10 -8 11 41.98 2.65
-10 -8 11 46.41 2.80
-10 -8 11 46.63 2.34
-10 -8 10 6.49 1.45
-10 -8 10 4.37 1.64
-10 -8 10 5.58 1.17
-10 -8 10 6.12 1.54
-10 -8 10 4.16 1.09
-10 -8 9 0.51 1.35
-10 -8 9 -0.10 1.81
-10 -8 9 -1.74 1.73
-10 -8 9 0.94 1.16
-10 -8 9 -0.03 0.52
-10 -8 9 -0.48 1.28
-10 -8 9 -0.71 1.10
-10 -8 8 121.41 5.05
-10 -8 8 116.49 5.46
-10 -8 8 121.71 5.12
-10 -8 8 124.14 4.92
-10 -8 8 114.40 4.28
-10 -8 8 125.35 4.91
-10 -8 8 114.80 4.55
-10 -8 7 39.44 2.54
-10 -8 7 44.38 3.00
-10 -8 7 43.62 2.52
-10 -8 7 38.52 2.53
-10 -8 7 43.76 1.96
-10 -8 7 46.32 2.46
-10 -8 7 46.01 2.09
-10 -8 6 9.34 1.55
-10 -8 6 10.81 1.83
-10 -8 6 8.32 1.48
-10 -8 6 10.58 1.47
-10 -8 6 11.51 1.04
-10 -8 6 9.10 1.32
-10 -8 6 11.92 1.03
-10 -8 5 7.81 1.45
-10 -8 5 13.82 1.90
-10 -8 5 9.15 1.33
-10 -8 5 10.61 1.54
-10 -8 5 12.18 1.18
-10 -8 5 10.99 1.27
-10 -8 5 11.51 0.97
-10 -8 4 14.06 1.80
-10 -8 4 13.11 1.57
-10 -8 4 11.45 1.27
-10 -8 4 14.02 1.64
-10 -8 4 13.10 1.25
-10 -8 4 12.54 1.25
-10 -8 4 11.80 0.95
-10 -8 3 5.18 1.00
-10 -8 3 3.83 1.30
-10 -8 3 4.95 1.03
-10 -8 3 4.56 1.36
-10 -8 3 5.53 1.08
10 8 -3 3.59 1.21
-10 -8 3 5.26 0.68
-10 -8 2 42.85 2.59
-10 -8 2 45.42 2.15
-10 -8 2 51.78 2.53
10 8 -2 40.35 2.68
-10 -8 2 50.33 2.81
-10 -8 2 47.95 2.26
-10 -8 2 46.34 1.86
-10 -8 1 215.94 7.75
-10 -8 1 247.22 8.45
-10 -8 1 214.41 8.08
-10 -8 1 217.72 7.58
10 8 -1 213.19 8.32
-10 -8 1 240.09 8.12
-10 -8 1 219.39 7.51
-10 -8 1 203.36 7.36
-10 -8 0 189.60 7.72
-10 -8 0 204.17 7.14
-10 -8 0 228.19 7.86
10 8 0 210.20 8.12
-10 -8 0 203.18 7.19
-10 -8 0 215.95 8.06
-10 -8 0 207.25 7.45
-10 -8 -1 4.07 1.02
-10 -8 -1 4.86 1.30
-10 -8 -1 5.85 0.56
-10 -8 -1 6.63 1.54
-10 -8 -1 6.31 1.37
10 8 1 6.17 1.56
-10 -8 -1 3.18 0.80
10 8 1 4.83 0.54
-10 -8 -2 95.21 4.38
-10 -8 -2 86.94 3.99
-10 -8 -2 103.95 4.21
10 8 2 95.83 4.50
-10 -8 -2 85.89 3.55
10 8 2 94.17 3.32
-10 -8 -3 16.70 1.68
-10 -8 -3 16.49 1.82
-10 -8 -3 18.19 1.84
10 8 3 16.17 2.01
-10 -8 -3 14.70 1.29
10 8 3 15.25 1.02
-10 -8 -4 187.07 6.98
-10 -8 -4 199.47 7.36
10 8 4 192.01 7.61
-10 -8 -4 201.50 7.23
-10 -8 -4 163.93 6.59
10 8 4 170.40 6.37
-10 -8 -5 80.71 3.71
10 8 5 82.75 4.31
-10 -8 -5 81.68 3.99
-10 -8 -5 89.18 4.12
-10 -8 -5 69.28 3.45
10 8 5 83.24 3.31
-10 -8 -6 10.33 1.65
10 8 6 12.05 1.90
-10 -8 -6 10.32 1.67
-10 -8 -6 7.43 1.35
10 8 6 7.41 1.14
-10 -8 -7 0.58 1.41
-10 -8 -7 -0.55 1.39
10 8 7 1.00 1.11
-10 -8 -7 3.66 1.50
10 8 7 0.96 1.73
-10 -8 -8 153.84 6.48
10 8 8 163.13 6.28
10 8 8 162.58 7.15
-10 -8 -8 167.65 6.68
-10 -8 -9 2.51 1.66
10 8 9 0.85 1.45
-10 -8 -9 3.22 1.49
10 8 9 0.59 2.03
-10 -8 -10 2.13 1.68
10 8 10 1.15 1.55
10 8 10 -0.86 2.08
-10 -8 -10 4.80 1.70
-10 -8 -11 12.02 2.04
-10 -8 -11 11.97 2.06
10 8 11 9.04 1.79
10 8 11 11.85 2.48
-10 -8 -11 6.77 1.85
-10 -8 -12 58.44 3.53
10 8 12 58.15 4.08
-10 -8 -12 62.65 3.56
-10 -8 -12 56.75 3.69
10 8 12 58.67 3.37
-10 -8 -13 93.45 4.72
10 8 13 92.90 5.25
-10 -8 -13 90.11 4.98
10 8 13 89.37 4.64
-10 -8 -13 93.85 4.74
-10 -8 -14 44.29 3.17
10 8 14 40.79 3.11
-10 -8 -14 37.67 3.36
10 8 15 36.75 3.01
-10 -8 -15 28.95 3.27
-10 -8 -16 58.91 3.85
-10 -8 -16 59.84 4.44
10 8 16 55.05 3.85
-10 -8 -17 8.56 3.18
10 8 17 13.19 2.34
10 8 17 16.19 2.63
10 8 17 14.35 2.98
-10 -8 -17 18.51 2.55
-10 -8 -18 108.79 6.75
10 8 18 138.64 5.64
10 8 18 119.24 6.18
10 8 18 117.27 6.72
10 8 19 5.69 2.12
-10 -8 -19 2.86 2.84
10 8 19 1.11 2.62
10 8 19 2.00 2.30
-10 -8 -20 1.52 2.83
10 8 20 3.12 2.45
-10 -9 16 37.27 2.87
-10 -9 16 29.92 2.33
-10 -9 15 2.48 1.87
-10 -9 15 1.97 1.48
-10 -9 14 67.48 3.77
10 9 -14 62.47 3.64
-10 -9 14 66.46 3.25
-10 -9 13 10.24 2.01
10 9 -13 13.47 1.90
-10 -9 13 11.56 1.78
-10 -9 13 13.36 1.67
-10 -9 12 21.48 1.79
-10 -9 12 22.60 1.69
-10 -9 12 23.62 2.30
-10 -9 12 21.45 1.96
-10 -9 12 24.73 1.87
-10 -9 11 27.15 2.02
-10 -9 11 23.49 1.13
-10 -9 11 25.53 1.06
-10 -9 11 32.32 2.29
-10 -9 11 29.86 1.96
-10 -9 11 29.72 2.06
-10 -9 11 31.65 1.99
-10 -9 10 69.84 3.32
-10 -9 10 62.19 2.58
-10 -9 10 74.71 3.51
-10 -9 10 69.66 3.28
-10 -9 10 68.92 3.20
-10 -9 10 71.28 3.15
-10 -9 9 -0.18 1.31
-10 -9 9 -0.43 1.22
-10 -9 9 -0.70 1.53
-10 -9 9 0.55 0.71
-10 -9 9 -1.18 1.22
-10 -9 9 -1.01 1.22
-10 -9 8 72.42 3.54
-10 -9 8 69.15 3.91
-10 -9 8 79.07 3.60
-10 -9 8 74.49 3.57
-10 -9 8 73.88 3.05
-10 -9 8 69.91 3.24
-10 -9 8 78.31 3.28
-10 -9 7 10.22 1.55
-10 -9 7 9.27 1.81
-10 -9 7 7.76 1.56
-10 -9 7 9.34 1.46
-10 -9 7 9.25 1.16
-10 -9 7 5.22 1.15
-10 -9 7 7.40 1.25
-10 -9 6 191.44 8.20
-10 -9 6 221.67 8.67
-10 -9 6 223.98 8.11
-10 -9 6 240.65 8.51
-10 -9 6 226.00 7.99
-10 -9 6 215.13 7.80
-10 -9 6 222.81 7.91
-10 -9 5 3.60 1.61
-10 -9 5 1.15 1.34
-10 -9 5 4.28 1.50
-10 -9 5 4.42 1.12
-10 -9 5 3.95 1.07
-10 -9 5 4.54 0.81
-10 -9 5 3.51 0.94
-10 -9 4 21.08 1.83
-10 -9 4 26.12 2.14
-10 -9 4 22.85 1.99
-10 -9 4 23.92 1.56
-10 -9 4 24.14 1.72
-10 -9 4 21.49 1.25
-10 -9 4 22.22 1.39
-10 -9 3 0.69 1.18
-10 -9 3 1.78 0.86
-10 -9 3 2.31 1.27
-10 -9 3 1.29 1.04
-10 -9 3 1.49 0.65
-10 -9 3 2.09 0.77
-10 -9 2 111.73 4.77
-10 -9 2 119.20 4.32
-10 -9 2 120.67 5.13
-10 -9 2 123.83 4.88
-10 -9 2 112.55 4.01
-10 -9 2 114.40 4.14
10 9 -2 115.53 5.06
-10 -9 2 113.90 4.28
10 9 -1 1.41 0.58
-10 -9 1 1.59 0.60
-10 -9 1 2.46 1.13
-10 -9 1 4.64 0.75
-10 -9 1 0.85 1.47
-10 -9 1 0.96 1.25
-10 -9 1 2.16 0.47
10 9 -1 0.39 1.48
-10 -9 1 1.32 0.66
10 9 0 24.00 1.12
-10 -9 0 19.99 1.07
-10 -9 0 17.33 1.60
-10 -9 0 18.34 1.03
-10 -9 0 16.98 1.96
-10 -9 0 19.15 1.79
-10 -9 0 17.39 0.94
10 9 0 17.61 1.99
-10 -9 0 15.54 1.08
-10 -9 -1 9.19 0.90
-10 -9 -1 11.16 1.45
-10 -9 -1 10.72 0.66
-10 -9 -1 11.21 1.66
10 9 1 10.15 1.79
-10 -9 -1 11.42 1.57
-10 -9 -1 9.19 0.80
10 9 1 11.38 0.86
-10 -9 -2 29.17 2.31
-10 -9 -2 27.52 1.47
-10 -9 -2 28.87 2.19
10 9 2 29.23 2.49
-10 -9 -2 27.17 1.92
-10 -9 -2 23.87 1.36
10 9 2 25.60 1.37
-10 -9 -3 35.21 2.56
10 9 3 32.39 2.71
-10 -9 -3 33.87 2.48
-10 -9 -3 33.63 2.17
-10 -9 -3 34.33 1.74
10 9 3 33.46 1.74
10 9 4 306.67 10.87
-10 -9 -4 311.80 10.94
-10 -9 -4 327.35 11.77
-10 -9 -4 320.62 11.64
10 9 4 310.50 12.01
10 9 5 28.47 1.78
-10 -9 -5 32.62 2.35
10 9 5 28.03 2.76
-10 -9 -5 31.85 1.84
-10 -9 -5 32.15 2.46
10 9 6 2.05 1.82
-10 -9 -6 2.40 1.44
10 9 6 1.67 1.10
-10 -9 -6 3.39 1.09
-10 -9 -6 2.06 1.41
-10 -9 -7 76.78 3.92
-10 -9 -7 77.24 3.51
10 9 7 74.55 3.43
-10 -9 -7 78.78 3.83
10 9 7 68.90 4.18
-10 -9 -8 141.44 5.87
10 9 8 137.28 5.77
10 9 8 148.73 6.77
-10 -9 -8 154.37 6.28
-10 -9 -9 199.44 8.17
10 9 9 211.44 8.10
10 9 9 223.40 9.13
-10 -9 -9 216.02 8.43
-10 -9 -10 121.43 5.68
10 9 10 130.01 5.58
10 9 10 133.63 6.44
-10 -9 -10 139.26 5.94
-10 -9 -11 0.67 1.72
-10 -9 -11 0.18 1.67
10 9 11 0.47 1.65
-10 -9 -11 0.09 1.43
10 9 11 -2.01 2.23
-10 -9 -12 -1.28 1.81
-10 -9 -12 -0.40 1.72
10 9 12 -0.42 1.68
-10 -9 -12 -0.10 1.66
10 9 12 -0.42 2.10
-10 -9 -13 -0.51 1.78
-10 -9 -13 -0.87 2.07
10 9 13 -1.65 1.79
10 9 13 -1.77 2.34
-10 -9 -13 -0.20 1.82
-10 -9 -14 1.46 1.76
-10 -9 -14 -1.43 2.08
10 9 14 0.79 1.76
10 9 14 -1.39 2.71
-10 -9 -15 1.51 1.90
10 9 15 0.11 1.97
-10 -9 -15 -1.68 2.27
-10 -9 -16 24.40 2.62
10 9 16 16.75 2.13
-10 -9 -16 14.84 2.76
10 9 16 21.90 2.71
-10 -9 -17 97.76 6.17
10 9 17 117.35 5.18
10 9 17 116.49 5.78
10 9 17 110.41 6.45
-10 -9 -18 9.49 3.15
10 9 18 18.65 2.40
10 9 18 14.46 2.66
10 9 18 13.47 3.18
10 9 19 38.33 2.82
10 9 19 29.08 3.21
-10 -9 -19 25.07 3.54
10 9 20 4.60 2.41
-10 -9 -20 2.76 2.67
-10 -10 16 33.85 2.73
-10 -10 15 7.57 1.70
-10 -10 15 13.31 2.09
-10 -10 14 71.79 3.72
-10 -10 14 83.80 4.06
-10 -10 13 19.38 1.96
-10 -10 13 22.87 2.33
-10 -10 12 14.56 1.84
-10 -10 12 12.42 1.65
-10 -10 12 15.71 2.05
-10 -10 11 22.80 1.78
-10 -10 11 23.54 2.05
-10 -10 11 21.11 1.83
-10 -10 11 24.33 1.64
-10 -10 11 21.96 1.88
-10 -10 10 7.25 1.34
-10 -10 10 5.93 0.97
-10 -10 10 7.22 1.49
-10 -10 10 9.45 1.60
-10 -10 10 8.53 1.09
-10 -10 10 5.24 1.38
-10 -10 9 -0.06 1.25
-10 -10 9 -0.58 0.99
-10 -10 9 -1.48 1.49
-10 -10 9 -0.84 1.30
-10 -10 9 -0.29 0.88
-10 -10 9 0.45 1.17
-10 -10 8 34.79 2.25
-10 -10 8 36.13 2.29
-10 -10 8 33.89 1.99
-10 -10 8 33.95 1.71
-10 -10 8 33.38 2.13
-10 -10 7 43.01 2.61
-10 -10 7 42.45 2.89
-10 -10 7 48.05 2.51
-10 -10 7 50.54 2.92
-10 -10 7 42.95 2.39
-10 -10 7 44.02 1.92
-10 -10 7 44.78 2.42
-10 -10 6 190.69 8.12
-10 -10 6 221.72 8.52
-10 -10 6 228.90 8.02
-10 -10 6 231.81 8.64
-10 -10 6 226.39 8.11
-10 -10 6 212.95 7.42
-10 -10 6 229.50 8.01
-10 -10 5 58.94 3.21
-10 -10 5 59.37 2.64
-10 -10 5 54.46 3.24
-10 -10 5 57.03 2.83
-10 -10 5 45.15 2.77
-10 -10 5 50.55 2.63
-10 -10 4 1.20 1.21
-10 -10 4 1.31 1.45
-10 -10 4 0.68 1.01
-10 -10 4 0.78 0.97
-10 -10 4 0.07 1.49
-10 -10 4 0.68 1.22
-10 -10 3 45.06 2.58
-10 -10 3 44.29 2.13
-10 -10 3 44.88 2.80
-10 -10 3 47.34 2.20
-10 -10 3 35.96 2.35
-10 -10 2 30.19 2.08
-10 -10 2 36.93 1.78
-10 -10 2 34.84 2.56
-10 -10 2 36.53 2.33
-10 -10 2 34.92 1.87
10 10 -2 36.52 1.75
-10 -10 1 4.55 1.13
-10 -10 1 3.78 1.50
-10 -10 1 4.82 0.76
-10 -10 1 3.06 1.44
-10 -10 1 3.81 0.88
10 10 -1 6.28 0.88
-10 -10 0 55.84 2.94
-10 -10 0 66.75 2.45
-10 -10 0 66.12 3.53
10 10 0 59.43 3.52
-10 -10 0 68.18 3.40
-10 -10 0 60.13 2.68
10 10 0 62.32 2.60
-10 -10 -1 60.03 3.12
-10 -10 -1 71.51 3.60
10 10 1 69.42 3.87
10 10 1 72.97 2.85
-10 -10 -1 72.33 3.73
-10 -10 -1 69.47 2.91
10 10 2 71.12 3.95
-10 -10 -2 72.48 3.63
10 10 2 63.94 2.79
-10 -10 -2 66.67 3.71
-10 -10 -2 65.72 2.83
-10 -10 -3 38.92 2.81
10 10 3 36.09 2.00
-10 -10 -3 37.66 1.67
-10 -10 -3 38.33 1.68
-10 -10 -3 36.93 2.66
10 10 3 40.57 2.99
10 10 4 41.24 2.17
-10 -10 -4 45.74 2.84
10 10 4 37.66 3.12
-10 -10 -4 39.14 1.95
-10 -10 -4 47.73 2.95
10 10 5 1.32 1.90
-10 -10 -5 3.46 1.57
10 10 5 3.98 1.15
-10 -10 -5 3.70 1.02
-10 -10 -5 3.68 1.58
-10 -10 -6 -0.75 1.46
10 10 6 -1.04 2.07
10 10 6 -0.95 1.18
-10 -10 -6 -0.23 0.96
-10 -10 -6 -1.09 1.59
-10 -10 -7 4.45 1.56
10 10 7 2.98 1.90
10 10 7 2.08 1.22
-10 -10 -7 4.33 1.22
-10 -10 -7 4.77 1.61
-10 -10 -8 33.24 2.24
10 10 8 36.18 2.38
-10 -10 -8 35.68 2.64
10 10 8 35.67 3.17
-10 -10 -9 82.65 4.02
10 10 9 82.72 3.99
-10 -10 -9 84.53 4.35
10 10 9 92.73 4.96
-10 -10 -10 39.86 3.04
-10 -10 -10 35.56 2.73
10 10 10 38.82 2.75
10 10 10 44.50 3.54
-10 -10 -10 44.62 3.03
-10 -10 -11 87.64 4.60
-10 -10 -11 78.40 4.30
10 10 11 89.43 4.27
10 10 11 79.30 4.96
-10 -10 -11 93.33 4.54
-10 -10 -12 13.70 2.12
-10 -10 -12 12.17 2.11
10 10 12 14.33 2.08
-10 -10 -12 13.98 2.17
10 10 12 13.76 2.50
-10 -10 -13 22.34 2.49
-10 -10 -13 21.55 2.36
10 10 13 19.27 2.20
-10 -10 -13 20.06 2.49
10 10 13 17.89 2.82
-10 -10 -14 27.74 2.73
-10 -10 -14 26.82 2.71
10 10 14 23.83 2.50
10 10 14 24.26 3.19
-10 -10 -15 10.05 2.15
-10 -10 -15 7.45 2.20
10 10 15 10.20 2.16
10 10 15 7.83 1.74
-10 -10 -16 4.09 1.95
-10 -10 -16 1.21 2.19
10 10 16 2.56 1.59
10 10 16 3.24 1.93
-10 -10 -17 0.14 2.35
-10 -10 -17 1.05 2.00
10 10 17 4.44 1.89
10 10 17 1.35 2.20
10 10 17 -1.44 2.98
-10 -10 -18 14.13 2.93
10 10 18 13.58 2.65
10 10 18 16.61 2.22
-10 -10 -19 0.33 2.66
10 10 19 1.80 2.45
10 10 19 1.13 1.86
-10 -10 -20 1.77 2.86
-10 -11 15 11.18 2.02
-10 -11 14 94.95 4.54
-10 -11 14 103.02 4.73
-10 -11 13 18.68 2.10
-10 -11 13 28.26 2.39
-10 -11 12 195.88 7.68
-10 -11 12 199.16 7.77
-10 -11 11 9.72 1.73
-10 -11 11 9.21 1.68
-10 -11 11 9.87 1.70
-10 -11 10 -0.49 1.08
-10 -11 10 -0.76 1.42
-10 -11 10 1.40 1.44
-10 -11 10 0.82 1.11
-10 -11 10 -0.06 1.38
-10 -11 9 1.89 1.23
-10 -11 9 1.85 1.03
-10 -11 9 0.40 1.48
-10 -11 9 1.55 1.33
-10 -11 9 2.70 0.72
-10 -11 9 1.12 1.27
-10 -11 8 19.06 1.73
-10 -11 8 17.15 2.08
-10 -11 8 18.68 1.76
-10 -11 8 20.51 1.70
-10 -11 8 19.62 0.98
-10 -11 8 22.00 1.81
-10 -11 7 5.99 1.33
-10 -11 7 4.99 1.61
-10 -11 7 4.45 1.37
-10 -11 7 2.78 1.31
-10 -11 6 4.44 1.38
-10 -11 6 3.13 1.67
-10 -11 6 0.05 1.46
-10 -11 6 2.00 1.28
-10 -11 6 2.46 1.54
-10 -11 5 2.56 1.37
-10 -11 5 0.62 1.68
-10 -11 5 -0.26 1.30
-10 -11 5 -0.46 1.29
-10 -11 5 0.49 1.46
-10 -11 5 -0.28 1.21
-10 -11 4 31.91 2.30
-10 -11 4 33.90 1.93
-10 -11 4 32.79 2.64
-10 -11 4 34.40 2.05
-10 -11 4 29.40 2.27
-10 -11 4 25.78 2.04
-10 -11 3 127.69 5.85
-10 -11 3 167.17 6.36
-10 -11 3 160.91 5.74
-10 -11 3 155.40 6.60
-10 -11 3 163.44 6.38
-10 -11 3 149.39 5.90
10 11 -3 162.27 5.78
-10 -11 2 28.09 1.99
-10 -11 2 37.86 1.85
-10 -11 2 35.65 2.70
-10 -11 2 39.34 2.65
-10 -11 2 38.70 2.12
10 11 -2 38.23 1.94
-10 -11 1 5.38 1.05
-10 -11 1 2.31 1.57
-10 -11 1 4.84 0.86
-10 -11 1 3.87 1.53
-10 -11 1 1.85 1.14
10 11 -1 5.35 1.03
-10 -11 0 2.37 1.01
-10 -11 0 1.80 1.56
10 11 0 3.59 0.95
-10 -11 0 2.13 1.52
-10 -11 0 0.49 1.13
-10 -11 -1 187.19 7.46
10 11 1 181.60 6.45
-10 -11 -1 185.95 7.27
10 11 1 174.85 7.49
-10 -11 -1 163.77 6.59
-10 -11 -2 1.31 1.63
10 11 2 1.06 1.11
-10 -11 -2 0.49 1.55
10 11 2 2.62 1.82
-10 -11 -2 0.40 1.10
-10 -11 -3 346.81 12.33
10 11 3 319.13 12.64
10 11 3 318.73 11.49
-10 -11 -3 348.05 12.46
-10 -11 -3 322.53 11.57
-10 -11 -4 5.92 1.97
10 11 4 -0.22 1.23
10 11 4 2.26 1.99
-10 -11 -4 0.47 1.79
-10 -11 -5 90.89 4.35
10 11 5 84.04 4.71
10 11 5 88.97 3.73
-10 -11 -5 86.06 4.41
-10 -11 -5 79.25 3.27
10 11 6 0.73 2.08
-10 -11 -6 0.44 1.57
10 11 6 1.71 1.29
-10 -11 -6 1.83 1.62
-10 -11 -6 1.07 0.90
-10 -11 -7 57.56 3.41
10 11 7 57.17 3.77
10 11 7 52.09 2.89
-10 -11 -7 53.46 2.66
-10 -11 -7 54.48 3.37
-10 -11 -8 27.91 2.02
-10 -11 -8 26.27 2.53
10 11 8 27.84 2.93
10 11 8 26.04 2.22
-10 -11 -9 17.98 1.73
10 11 9 16.17 2.56
-10 -11 -9 13.74 2.15
10 11 9 13.05 1.89
-10 -11 -10 16.49 2.25
-10 -11 -10 14.44 2.03
10 11 10 16.11 2.03
-10 -11 -10 16.68 2.20
10 11 10 18.53 2.73
-10 -11 -11 209.30 8.40
-10 -11 -11 192.41 8.00
10 11 11 194.74 8.07
-10 -11 -11 210.15 8.30
10 11 11 197.54 8.98
-10 -11 -12 13.46 2.19
-10 -11 -12 11.54 2.02
10 11 12 11.51 2.00
-10 -11 -12 13.65 2.03
10 11 12 11.30 2.71
-10 -11 -13 2.83 1.74
-10 -11 -13 3.35 1.69
10 11 13 2.44 1.63
-10 -11 -13 2.43 1.73
10 11 13 -0.16 2.32
-10 -11 -14 0.22 1.85
-10 -11 -14 0.89 1.70
10 11 14 2.24 1.43
10 11 14 1.57 1.82
10 11 14 -0.17 2.13
-10 -11 -15 15.40 2.25
-10 -11 -15 14.16 2.33
10 11 15 11.74 2.21
10 11 15 14.68 1.79
-10 -11 -16 -0.35 1.84
-10 -11 -16 0.39 2.07
10 11 16 -0.83 2.04
10 11 16 2.96 1.56
-10 -11 -17 3.63 2.19
10 11 17 4.64 2.20
10 11 17 9.71 1.90
-10 -11 -18 2.40 2.35
10 11 18 1.86 2.31
10 11 18 2.92 1.87
-10 -11 -19 4.97 2.54
10 11 19 2.67 2.29
10 11 19 5.90 1.91
-10 -11 -20 2.39 2.60
-10 -12 14 5.44 1.88
-10 -12 13 81.63 4.14
-10 -12 12 1.56 1.59
-10 -12 12 0.80 1.67
-10 -12 11 25.72 2.20
-10 -12 11 27.26 2.26
-10 -12 10 -1.32 1.59
-10 -12 10 0.26 1.48
-10 -12 9 78.17 3.63
-10 -12 9 73.18 3.69
-10 -12 9 69.29 3.35
-10 -12 9 74.38 3.49
-10 -12 8 7.26 1.51
-10 -12 8 5.36 1.57
-10 -12 8 4.60 1.26
-10 -12 8 6.55 1.43
-10 -12 7 28.01 2.03
-10 -12 7 27.73 2.18
-10 -12 7 27.50 2.11
-10 -12 7 23.39 1.98
-10 -12 6 9.64 1.66
-10 -12 6 7.81 1.50
-10 -12 6 6.92 1.55
-10 -12 6 6.24 1.60
-10 -12 6 4.53 1.35
-10 -12 5 311.74 11.02
-10 -12 5 322.52 11.42
-10 -12 5 304.72 10.49
-10 -12 5 308.06 10.74
-10 -12 5 285.98 10.71
-10 -12 5 250.90 10.46
-10 -12 4 15.15 1.60
-10 -12 4 16.74 1.87
-10 -12 4 18.58 2.43
-10 -12 4 20.19 1.62
-10 -12 4 15.87 2.08
-10 -12 4 17.07 1.86
10 12 -4 17.35 1.72
-10 -12 3 17.14 1.86
-10 -12 3 11.95 1.42
-10 -12 3 16.86 2.23
-10 -12 3 18.15 1.56
-10 -12 3 14.62 2.03
-10 -12 3 13.32 1.63
10 12 -3 14.88 1.57
-10 -12 2 34.35 2.23
-10 -12 2 44.64 2.18
-10 -12 2 42.74 3.03
-10 -12 2 42.01 2.90
-10 -12 2 44.18 2.48
10 12 -2 47.47 2.35
-10 -12 1 36.33 2.15
-10 -12 1 40.29 2.86
-10 -12 1 37.90 2.38
-10 -12 1 41.55 1.98
-10 -12 1 46.18 3.04
10 12 -1 45.14 2.26
-10 -12 0 5.70 1.81
-10 -12 0 4.20 1.27
-10 -12 0 3.50 1.72
10 12 0 5.02 1.15
-10 -12 -1 1.32 1.57
-10 -12 -1 1.28 1.24
10 12 1 0.53 1.08
-10 -12 -1 0.60 1.78
-10 -12 -2 3.93 1.83
-10 -12 -2 7.59 1.33
-10 -12 -2 4.10 1.79
10 12 2 5.97 2.07
10 12 2 5.97 1.25
-10 -12 -3 209.85 8.18
10 12 3 190.15 8.48
-10 -12 -3 200.58 7.52
10 12 3 194.66 7.40
-10 -12 -3 207.41 8.36
-10 -12 -4 25.79 2.63
-10 -12 -4 27.68 1.99
-10 -12 -4 23.76 2.39
10 12 4 24.30 3.03
10 12 4 25.13 1.96
-10 -12 -5 291.83 11.18
10 12 5 288.26 11.63
10 12 5 285.82 10.52
-10 -12 -5 300.63 11.33
-10 -12 -6 97.72 4.97
10 12 6 101.87 5.51
-10 -12 -6 98.04 3.78
10 12 6 108.91 4.46
-10 -12 -6 110.95 5.11
-10 -12 -7 5.54 1.92
10 12 7 5.49 2.10
-10 -12 -7 5.91 1.12
10 12 7 7.28 1.66
-10 -12 -7 6.94 1.98
10 12 8 68.09 4.40
-10 -12 -8 69.15 3.94
-10 -12 -8 65.48 3.12
10 12 8 64.92 3.46
10 12 9 11.21 2.63
-10 -12 -9 14.88 2.21
-10 -12 -9 12.31 1.56
10 12 9 13.84 1.98
-10 -12 -10 28.89 2.70
10 12 10 28.15 3.19
10 12 10 25.50 2.45
-10 -12 -10 30.83 2.70
-10 -12 -10 27.65 2.18
-10 -12 -11 4.10 1.90
10 12 11 5.40 2.83
-10 -12 -11 4.23 1.84
10 12 11 5.33 1.90
-10 -12 -11 3.93 1.95
-10 -12 -12 11.19 1.94
-10 -12 -12 7.09 2.11
10 12 12 10.19 1.98
-10 -12 -12 10.91 1.94
10 12 12 11.94 2.81
-10 -12 -13 0.10 1.56
-10 -12 -13 0.79 1.67
10 12 13 -0.91 1.69
-10 -12 -13 0.55 1.70
10 12 13 -1.65 2.34
-10 -12 -14 58.31 3.70
-10 -12 -14 51.96 3.61
10 12 14 58.58 2.99
10 12 14 50.24 3.52
10 12 14 56.11 4.35
-10 -12 -15 2.55 1.95
10 12 15 1.83 2.18
10 12 15 5.22 1.54
-10 -12 -16 0.38 2.01
10 12 16 3.40 2.02
10 12 16 1.88 1.55
-10 -12 -17 5.10 2.23
10 12 17 5.15 2.34
-10 -12 -18 4.48 2.30
10 12 18 6.92 2.50
-10 -13 14 0.75 1.79
-10 -13 13 0.63 1.66
-10 -13 12 25.02 2.32
-10 -13 11 6.29 1.70
-10 -13 11 7.63 1.74
-10 -13 10 0.86 1.59
-10 -13 10 0.13 1.50
-10 -13 9 18.86 2.21
-10 -13 9 20.34 1.91
-10 -13 8 19.76 2.02
-10 -13 8 18.08 1.82
-10 -13 8 17.26 2.05
-10 -13 8 13.88 1.67
-10 -13 7 1.87 1.59
-10 -13 7 3.26 1.39
-10 -13 7 3.79 1.55
-10 -13 7 1.12 1.22
-10 -13 6 131.64 5.50
-10 -13 6 128.30 4.98
-10 -13 6 133.68 5.31
-10 -13 6 98.96 4.80
-10 -13 5 63.94 3.54
-10 -13 5 63.61 2.97
-10 -13 5 59.85 3.20
-10 -13 5 56.26 2.84
-10 -13 5 48.63 2.77
-10 -13 4 29.61 2.12
-10 -13 4 25.08 1.90
-10 -13 4 36.12 2.13
-10 -13 4 33.08 2.72
-10 -13 4 37.47 2.50
10 13 -4 33.57 2.26
-10 -13 3 117.28 5.46
-10 -13 3 143.99 5.76
-10 -13 3 156.10 5.58
-10 -13 3 153.60 6.39
-10 -13 3 157.68 6.02
10 13 -3 151.19 5.77
-10 -13 2 44.57 2.63
-10 -13 2 58.19 3.03
-10 -13 2 61.89 3.53
-10 -13 2 57.09 3.10
-10 -13 2 62.73 3.80
-10 -13 2 58.60 2.70
10 13 -2 59.22 2.89
-10 -13 1 104.39 4.86
-10 -13 1 90.39 4.36
-10 -13 1 99.40 5.09
10 13 -1 97.53 4.12
-10 -13 0 223.88 9.00
-10 -13 0 215.34 8.47
-10 -13 0 233.59 9.25
10 13 0 225.38 8.20
-10 -13 -1 10.55 2.02
-10 -13 -1 9.42 1.64
-10 -13 -1 13.34 2.26
10 13 1 11.20 1.44
-10 -13 -2 6.74 1.71
-10 -13 -2 5.72 1.46
-10 -13 -2 4.34 1.92
10 13 2 5.36 1.30
-10 -13 -3 75.62 3.94
-10 -13 -3 66.28 3.36
10 13 3 65.31 3.26
-10 -13 -3 69.56 4.05
-10 -13 -4 63.57 3.89
-10 -13 -4 64.45 3.26
-10 -13 -4 67.62 3.86
10 13 4 64.64 4.14
10 13 4 61.68 3.19
-10 -13 -5 5.66 1.96
-10 -13 -5 5.02 1.42
-10 -13 -5 3.36 1.81
10 13 5 4.52 2.23
10 13 5 3.99 1.48
-10 -13 -6 -2.06 1.89
10 13 6 2.60 1.35
10 13 6 -0.14 2.02
-10 -13 -6 0.54 1.70
-10 -13 -7 31.40 3.02
-10 -13 -7 26.39 1.39
10 13 7 27.84 3.15
10 13 7 25.33 2.26
-10 -13 -7 30.30 2.70
-10 -13 -8 42.53 2.24
10 13 8 48.96 3.08
-10 -13 -8 46.58 3.22
10 13 8 51.29 3.84
-10 -13 -9 3.50 1.26
-10 -13 -9 0.65 1.85
10 13 9 0.61 2.40
10 13 9 3.57 1.76
-10 -13 -10 2.72 1.87
-10 -13 -10 3.44 1.64
-10 -13 -10 -0.55 1.97
10 13 10 0.94 2.33
10 13 10 0.09 1.91
10 13 11 7.11 2.54
-10 -13 -11 10.19 2.15
-10 -13 -11 8.93 2.18
10 13 11 7.63 2.03
-10 -13 -11 9.88 1.72
10 13 12 13.20 2.82
-10 -13 -12 8.19 2.08
-10 -13 -12 10.56 2.11
10 13 12 8.67 2.03
-10 -13 -12 13.30 1.86
10 13 13 20.92 2.40
10 13 13 10.22 2.86
-10 -13 -13 16.78 2.10
-10 -13 -13 17.35 2.44
10 13 14 28.74 3.37
-10 -13 -14 24.97 2.76
10 13 14 28.32 2.94
10 13 15 7.10 2.31
10 13 16 48.97 3.67
10 13 17 2.23 2.35
-10 -14 13 10.64 1.93
-10 -14 12 8.95 1.88
-10 -14 11 18.80 2.18
-10 -14 10 10.79 1.83
-10 -14 9 5.75 1.82
-10 -14 9 8.68 1.74
-10 -14 8 85.81 4.36
-10 -14 8 89.95 4.15
-10 -14 7 51.70 3.38
-10 -14 7 47.89 3.17
-10 -14 7 54.25 2.95
-10 -14 6 32.02 2.76
-10 -14 6 33.35 2.34
-10 -14 6 32.44 2.57
-10 -14 6 27.87 1.92
-10 -14 5 13.83 1.47
-10 -14 5 18.69 1.80
-10 -14 5 20.15 2.25
-10 -14 5 16.68 2.02
10 14 -5 18.15 1.87
-10 -14 4 30.29 1.98
-10 -14 4 38.86 2.28
-10 -14 4 38.99 2.62
10 14 -4 36.79 2.42
-10 -14 4 35.21 2.86
-10 -14 3 30.75 1.96
-10 -14 3 38.97 2.61
10 14 -3 39.46 2.40
-10 -14 3 42.95 2.99
-10 -14 2 42.26 2.37
-10 -14 2 46.30 3.16
-10 -14 2 43.67 2.81
10 14 -2 43.77 2.55
-10 -14 1 2.46 1.81
-10 -14 1 -0.12 2.18
-10 -14 1 0.66 1.64
10 14 -1 -0.69 1.37
-10 -14 0 83.61 4.45
-10 -14 0 81.62 4.61
-10 -14 0 76.93 3.96
10 14 0 80.07 3.64
-10 -14 -1 27.60 2.60
-10 -14 -1 25.78 2.72
-10 -14 -1 25.23 2.14
10 14 1 24.42 1.89
-10 -14 -2 -0.42 1.69
-10 -14 -2 -0.70 1.82
-10 -14 -2 -0.14 1.35
10 14 2 0.98 1.20
-10 -14 -3 0.21 1.65
-10 -14 -3 1.63 2.02
-10 -14 -3 -0.94 1.48
10 14 3 -0.17 1.27
-10 -14 -4 9.74 2.07
-10 -14 -4 9.47 2.12
-10 -14 -4 10.42 1.59
10 14 4 8.57 1.58
-10 -14 -5 -1.31 1.98
-10 -14 -5 -1.05 1.85
-10 -14 -5 -1.33 1.39
10 14 5 -1.17 1.53
-10 -14 -6 67.33 4.13
-10 -14 -6 71.43 4.13
10 14 6 70.43 4.59
10 14 6 66.23 3.47
-10 -14 -7 110.10 5.52
-10 -14 -7 101.07 5.45
10 14 7 117.07 4.97
10 14 7 103.51 5.92
10 14 8 108.60 5.13
10 14 8 117.57 6.20
-10 -14 -8 115.48 5.69
-10 -14 -9 5.49 2.30
10 14 9 7.00 2.70
10 14 9 7.78 2.13
-10 -14 -10 1.40 2.00
-10 -14 -10 3.00 2.08
10 14 10 6.41 2.47
10 14 10 2.56 1.98
10 14 11 17.64 3.02
10 14 11 17.54 2.58
-10 -14 -11 11.87 2.40
10 14 12 -1.44 2.15
10 14 12 0.17 2.43
10 14 13 -0.98 2.34
10 14 13 3.25 2.55
10 14 14 -1.38 2.06
10 14 15 13.72 2.59
10 14 16 33.52 3.36
-10 -15 7 22.08 2.38
-10 -15 7 20.75 2.35
-10 -15 6 113.39 5.56
-10 -15 6 114.91 5.25
-10 -15 6 109.88 4.84
-10 -15 5 -1.54 1.92
-10 -15 5 -1.78 1.65
-10 -15 5 1.39 1.54
-10 -15 5 1.56 1.06
-10 -15 4 5.74 1.06
-10 -15 4 3.40 1.65
10 15 -4 4.69 1.50
-10 -15 4 5.22 1.88
-10 -15 3 2.62 0.97
-10 -15 3 1.34 1.87
10 15 -3 1.53 1.47
-10 -15 3 1.26 1.65
-10 -15 2 36.70 3.05
10 15 -2 33.46 2.33
-10 -15 2 29.92 2.54
-10 -15 1 10.75 2.23
-10 -15 1 5.69 1.81
10 15 -1 6.02 1.46
-10 -15 0 38.83 3.19
-10 -15 0 39.16 3.34
-10 -15 0 35.39 2.73
10 15 0 40.44 2.46
-10 -15 -1 0.80 1.91
-10 -15 -1 -0.25 1.93
-10 -15 -1 -0.33 1.62
10 15 1 -0.17 1.34
-10 -15 -2 35.44 3.14
-10 -15 -2 35.94 3.22
-10 -15 -2 32.62 2.60
10 15 2 36.14 2.33
-10 -15 -3 6.35 2.10
-10 -15 -3 6.30 2.08
-10 -15 -3 5.31 1.77
10 15 3 6.78 1.56
-10 -15 -4 8.27 2.05
-10 -15 -4 6.01 2.16
-10 -15 -4 6.17 1.72
10 15 4 6.18 1.55
-10 -15 -5 14.48 2.34
-10 -15 -5 10.92 2.35
-10 -15 -5 10.32 1.90
10 15 5 10.23 1.84
-10 -15 -6 8.63 2.26
-10 -15 -6 6.99 2.20
10 15 6 9.82 1.92
-10 -15 -6 12.09 1.90
10 15 7 82.58 4.14
-10 -15 -7 81.08 4.75
10 15 8 5.86 2.85
10 15 8 6.51 2.04
-10 -15 -8 5.20 2.37
10 15 9 66.12 4.79
10 15 9 66.62 3.85
10 15 10 84.73 5.41
10 15 10 75.67 4.35
10 15 11 1.24 2.61
10 15 11 0.71 2.01
10 15 12 1.49 2.22
10 15 13 24.75 2.95
10 15 14 28.92 3.12
-10 -16 5 0.24 1.89
-10 -16 4 5.89 1.93
-10 -16 4 8.29 2.27
-10 -16 3 16.97 2.23
-10 -16 3 22.37 2.69
-10 -16 2 10.30 1.90
-10 -16 2 10.84 2.30
10 16 -1 31.33 2.31
-10 -16 1 28.24 2.58
-10 -16 1 32.99 3.11
10 16 0 2.37 1.42
-10 -16 0 1.74 1.70
-10 -16 0 2.61 2.29
10 16 1 75.57 3.89
-10 -16 -1 84.80 4.31
-10 -16 -1 91.22 4.85
10 16 2 2.22 1.57
-10 -16 -2 1.18 1.68
-10 -16 -2 1.50 1.96
10 16 3 10.19 1.82
-10 -16 -3 10.11 1.88
-10 -16 -3 10.59 2.49
10 16 4 15.39 1.99
-10 -16 -4 16.68 2.17
-10 -16 -4 18.74 2.63
10 16 5 12.95 2.01
-10 -16 -5 16.31 2.08
-10 -16 -5 18.54 2.57
10 16 6 4.37 1.81
-10 -16 -6 5.13 1.77
10 16 7 -0.08 1.75
10 16 8 5.51 2.00
10 16 9 69.31 3.96
10 16 10 7.16 2.14
10 16 11 31.96 2.86
-10 -17 4 2.44 2.09
-10 -17 3 6.55 2.29
-10 -17 2 3.81 2.25
-10 -17 1 2.04 1.74
-10 -17 1 3.54 2.17
-10 -17 0 7.79 1.94
-10 -17 0 14.54 2.48
-10 -17 -1 3.84 1.86
-10 -17 -1 6.70 2.25
-10 -17 -2 -0.20 1.76
-10 -17 -3 32.51 2.81
-10 -17 -4 1.32 1.67
-10 -17 -5 21.32 2.40
-10 -17 -6 37.05 2.93
-10 -17 -7 0.93 2.01
11 -11 -1 7.40 3.19
11 -10 -9 4.22 2.48
11 -10 -8 3.23 2.56
11 -10 -7 3.57 2.64
11 -10 -6 43.33 4.01
11 -10 -6 42.61 4.02
11 -10 -5 -0.82 2.68
-11 10 5 1.09 1.70
11 -10 -4 12.35 3.09
-11 10 4 11.61 1.93
-11 10 3 31.18 3.75
11 -10 -3 27.47 3.82
-11 10 3 28.10 2.38
-11 10 2 -1.54 2.98
11 -10 -2 -0.67 2.82
-11 10 2 -0.85 1.59
11 -10 -1 -1.24 2.19
-11 10 1 -0.84 2.90
11 -10 -1 0.34 2.87
-11 10 1 -0.35 1.50
11 -10 0 3.41 2.41
-11 10 0 3.96 2.80
11 -10 0 7.55 2.98
-11 10 0 6.17 1.76
11 -10 1 85.82 5.11
-11 10 -1 85.51 5.56
11 -10 1 88.09 5.79
-11 10 -1 87.59 4.13
-11 10 -2 13.50 1.89
11 -10 2 8.14 2.52
11 -10 2 18.17 3.39
-11 10 -2 19.20 3.29
11 -10 3 24.60 3.51
11 -10 3 16.94 2.61
11 -10 4 4.20 2.80
11 -10 4 -0.84 2.02
11 -10 5 2.10 2.81
11 -10 5 -0.82 1.95
11 -10 6 1.22 2.76
11 -10 6 -0.50 1.86
11 -10 7 0.98 1.88
11 -10 8 1.81 1.76
11 -9 -9 0.45 2.50
-11 9 9 4.24 1.75
11 -9 -8 0.74 2.53
-11 9 8 -1.32 2.04
-11 9 7 40.67 2.96
11 -9 -7 46.03 4.05
11 -9 -7 51.42 3.87
11 -9 -6 62.23 4.67
-11 9 6 66.01 3.68
-11 9 5 68.20 5.08
11 -9 -5 65.32 4.71
-11 9 5 65.15 3.57
-11 9 4 0.84 1.68
11 -9 -4 0.46 1.91
-11 9 4 1.56 2.61
11 -9 -4 -2.69 2.78
-11 9 3 21.16 2.11
11 -9 -3 20.94 2.54
-11 9 3 21.01 3.22
11 -9 -3 18.02 3.16
-11 9 2 15.14 1.96
11 -9 -2 14.96 2.34
11 -9 -2 17.34 2.51
-11 9 2 16.47 3.13
11 -9 -2 14.50 2.90
-11 9 1 -1.50 1.53
11 -9 -1 0.11 1.63
11 -9 -1 0.46 2.19
-11 9 1 0.49 2.62
11 -9 -1 -0.77 2.65
-11 9 0 3.83 1.55
11 -9 0 7.57 2.02
11 -9 0 5.90 2.24
-11 9 0 9.08 2.83
11 -9 0 2.81 2.57
-11 9 -1 21.19 2.10
11 -9 1 25.46 2.59
11 -9 1 23.13 2.83
-11 9 -1 26.95 3.45
11 -9 1 23.19 3.31
-11 9 -2 3.40 1.61
11 -9 2 4.02 2.04
-11 9 -2 9.57 2.95
11 -9 2 -0.99 2.32
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16 7 11 42.14 4.16
-16 -7 -11 42.04 3.51
-16 -7 -12 11.74 2.62
-16 -7 -13 8.06 2.56
-16 -7 -14 -3.26 2.83
-16 -8 9 37.49 3.56
-16 -8 8 8.70 2.55
-16 -8 7 4.77 2.22
-16 -8 7 5.69 2.94
-16 -8 6 5.38 2.43
-16 -8 6 17.19 3.24
-16 -8 5 -1.99 2.35
-16 -8 5 2.04 2.75
-16 -8 4 8.45 2.39
-16 -8 4 8.97 2.95
-16 -8 3 3.69 2.15
-16 -8 2 2.90 1.86
-16 -8 1 6.18 1.43
-16 -8 1 6.52 2.07
-16 -8 0 3.60 1.79
16 8 0 3.84 1.91
-16 -8 0 1.12 1.48
-16 -8 0 2.88 1.35
-16 -8 0 3.70 1.81
-16 -8 -1 4.94 2.04
16 8 1 3.70 2.02
-16 -8 -1 5.05 1.64
-16 -8 -1 4.65 1.36
-16 -8 -1 3.65 1.80
-16 -8 -2 13.88 2.24
16 8 2 9.86 2.34
-16 -8 -2 8.16 1.77
-16 -8 -2 10.52 1.69
-16 -8 -2 8.88 1.92
16 8 3 95.47 5.22
-16 -8 -3 104.78 4.75
-16 -8 -3 101.16 4.33
-16 -8 -3 80.16 4.55
-16 -8 -4 21.14 2.14
16 8 4 17.82 2.88
-16 -8 -4 23.38 2.51
-16 -8 -5 117.58 4.84
16 8 5 97.62 5.69
-16 -8 -5 105.70 5.34
-16 -8 -6 8.16 1.68
16 8 6 4.36 2.35
-16 -8 -6 7.53 2.09
-16 -8 -7 7.75 1.75
16 8 7 8.53 2.67
-16 -8 -7 9.13 2.12
-16 -8 -8 3.78 1.76
16 8 8 1.68 2.40
-16 -8 -8 4.69 2.09
-16 -8 -9 11.04 2.19
16 8 9 13.59 2.88
-16 -8 -9 13.17 2.45
-16 -8 -10 22.32 2.68
16 8 10 21.48 3.21
-16 -8 -11 0.46 2.09
16 8 11 -2.07 2.75
-16 -8 -12 32.66 3.33
-16 -8 -13 -1.73 2.56
-16 -9 8 -0.87 2.63
-16 -9 8 0.91 2.18
-16 -9 7 10.19 2.94
-16 -9 7 12.08 2.43
-16 -9 6 10.15 3.01
-16 -9 6 8.58 2.25
-16 -9 5 -1.67 2.72
-16 -9 5 -1.16 2.13
-16 -9 4 37.57 3.77
-16 -9 4 27.33 2.93
-16 -9 3 48.64 4.18
-16 -9 3 46.09 3.46
-16 -9 2 13.30 2.35
-16 -9 1 5.87 1.91
16 9 0 11.19 2.25
-16 -9 0 9.74 1.73
-16 -9 0 13.65 2.06
16 9 1 3.38 1.97
-16 -9 -1 4.71 1.69
-16 -9 -1 4.07 1.84
16 9 2 3.59 2.11
-16 -9 -2 4.94 1.68
16 9 3 14.72 2.52
-16 -9 -3 15.52 2.22
-16 -9 -4 150.86 6.00
16 9 4 148.86 7.20
-16 -9 -4 145.28 6.54
16 9 5 8.83 2.70
-16 -9 -5 9.25 2.21
16 9 6 18.20 2.96
-16 -9 -6 20.24 2.41
16 9 7 -0.61 2.41
-16 -9 -7 2.05 1.85
16 9 8 10.54 2.80
-16 -9 -8 11.11 2.21
16 9 9 1.49 2.51
16 9 10 2.41 2.60
-16 -10 7 0.50 2.49
-16 -10 7 -2.38 2.15
-16 -10 6 -2.29 2.55
-16 -10 6 -0.34 1.96
-16 -10 5 8.43 2.74
-16 -10 5 6.13 2.09
-16 -10 4 61.19 4.45
-16 -10 4 47.47 3.49
-16 -10 3 18.58 3.32
-16 -10 3 13.41 2.30
-16 -10 3 17.12 2.25
-16 -10 2 131.37 6.15
-16 -10 2 144.59 6.30
-16 -10 1 10.09 2.15
-16 -10 1 9.62 2.23
-16 -10 0 2.75 1.96
-16 -10 -1 47.12 3.33
16 10 1 37.29 3.21
-16 -10 -1 40.04 2.68
-16 -10 -2 19.96 2.50
16 10 2 15.33 2.56
-16 -10 -2 13.98 2.01
-16 -10 -3 2.76 2.05
16 10 3 2.49 2.10
-16 -10 -3 -0.54 1.86
16 10 4 3.71 2.31
-16 -10 -4 2.75 1.94
16 10 5 3.04 2.34
-16 -10 -5 3.78 1.94
16 10 6 3.94 2.45
-16 -10 -6 2.40 1.97
16 10 7 9.81 2.68
-16 -10 -7 11.20 2.09
16 10 8 0.66 2.47
-16 -10 -8 0.79 1.96
16 10 9 4.12 2.51
16 10 10 2.14 2.90
-16 -11 6 4.11 1.96
-16 -11 5 4.66 1.85
-16 -11 4 14.81 2.19
-16 -11 4 13.50 2.79
-16 -11 3 26.00 2.59
-16 -11 3 28.41 2.78
-16 -11 3 34.02 3.53
-16 -11 2 86.89 4.65
-16 -11 1 8.38 2.21
-16 -11 0 4.27 2.01
16 11 1 9.54 2.33
-16 -11 -1 8.11 2.18
-16 -11 -2 5.02 1.76
-16 -11 -2 4.39 2.04
16 11 2 5.52 2.17
-16 -11 -3 8.70 1.99
-16 -11 -3 6.98 2.16
16 11 3 14.35 2.59
-16 -11 -4 1.45 1.76
16 11 4 2.42 2.34
-16 -11 -5 4.17 1.93
16 11 5 1.94 2.30
-16 -11 -6 1.70 1.81
16 11 6 1.56 2.33
-16 -11 -7 2.21 2.01
16 11 7 1.47 2.37
16 11 8 2.38 2.44
16 11 9 13.62 3.15
-16 -12 2 6.53 2.02
-16 -12 1 1.22 1.89
-16 -12 0 25.66 2.75
16 12 2 -0.53 2.22
-16 -12 -3 0.66 1.73
16 12 3 0.70 2.22
16 12 4 18.77 3.05
-16 -12 -4 17.81 2.36
16 12 5 3.09 2.61
-16 -12 -5 5.73 2.01
16 12 6 2.26 2.44
-16 -12 -6 4.78 1.94
16 12 7 1.51 2.35
16 12 8 6.49 2.74
16 13 3 75.70 4.89
-16 -13 -4 2.67 1.94
16 13 4 1.07 2.39
-16 -13 -5 12.14 2.37
16 13 5 8.34 2.63
16 13 6 0.84 2.45
16 13 7 7.14 2.81
16 14 4 66.04 4.75
16 14 5 2.82 2.68
16 14 6 -1.73 2.63
17 -2 1 5.43 2.28
17 -2 4 1.89 2.15
17 -1 0 9.21 2.34
-17 1 -1 -2.03 1.87
17 -1 1 2.17 2.03
17 -1 2 4.47 2.21
17 -1 3 3.58 2.04
17 -1 3 3.09 2.31
17 -1 4 4.52 2.18
17 -1 5 57.61 3.94
17 0 -1 101.73 5.43
17 0 0 14.32 2.55
17 0 1 16.78 2.70
17 0 2 1.58 2.22
17 0 3 9.61 2.25
17 0 3 13.69 2.66
17 0 4 17.59 2.62
17 0 4 20.27 2.88
17 0 5 9.07 2.43
17 0 6 30.20 3.10
17 1 -1 10.21 2.46
17 1 0 13.92 2.54
17 1 1 11.54 2.61
17 1 2 21.02 2.53
17 1 2 23.96 2.95
17 1 3 7.21 2.20
17 1 3 8.48 2.51
-17 -1 -4 5.74 2.32
17 1 4 3.21 2.28
17 1 4 3.03 2.29
17 1 5 19.81 2.73
17 1 5 15.26 2.80
17 1 6 2.97 2.28
17 1 7 10.16 2.62
17 2 -2 4.32 2.17
17 2 -1 35.60 3.16
-17 -2 1 30.65 3.53
17 2 0 -2.39 2.32
-17 -2 0 1.36 2.40
17 2 1 -0.51 2.29
-17 -2 -1 1.72 2.21
17 2 2 5.46 2.16
17 2 2 9.38 2.47
17 2 3 14.84 2.47
17 2 3 13.79 2.68
-17 -2 -4 11.44 2.30
17 2 4 7.11 2.27
-17 -2 -5 14.79 2.39
17 2 5 7.30 2.34
17 2 5 10.97 2.63
-17 -2 -6 -0.09 1.82
17 2 6 -0.88 2.36
17 2 6 2.49 2.54
-17 -2 -7 2.44 1.92
17 2 7 1.56 2.29
17 2 8 -1.08 2.35
-17 -3 9 2.36 2.00
-17 -3 8 2.15 1.89
-17 -3 5 -0.86 2.61
-17 -3 4 16.84 3.05
-17 -3 3 4.59 2.53
17 3 -2 -1.85 2.15
-17 -3 2 0.47 2.27
17 3 -1 2.43 2.29
-17 -3 1 7.72 2.49
17 3 0 5.08 2.29
-17 -3 0 9.53 2.39
17 3 1 1.44 2.32
-17 -3 -1 4.83 2.21
17 3 2 0.65 2.07
17 3 2 2.97 2.24
-17 -3 -2 3.58 2.15
-17 -3 -3 16.01 2.37
17 3 3 8.46 2.35
17 3 3 10.37 2.54
-17 -3 -4 72.77 3.93
17 3 4 61.18 4.18
-17 -3 -5 3.62 2.17
17 3 5 2.62 2.47
17 3 5 1.44 2.44
-17 -3 -6 76.18 4.17
17 3 6 71.89 4.60
17 3 6 70.38 4.92
-17 -3 -7 1.53 2.00
17 3 7 1.34 2.33
-17 -3 -8 16.54 2.39
17 3 8 12.14 2.79
-17 -4 9 14.88 2.35
-17 -4 8 10.20 2.24
-17 -4 7 26.95 2.74
-17 -4 7 29.47 3.66
-17 -4 6 -1.77 2.11
-17 -4 6 -0.50 2.67
-17 -4 5 1.94 2.42
-17 -4 4 3.35 2.49
-17 -4 3 6.37 2.54
-17 -4 2 20.71 2.94
-17 -4 1 6.68 2.45
17 4 0 -2.27 2.27
-17 -4 0 -1.67 2.18
17 4 1 18.98 2.85
-17 -4 -1 15.78 2.51
17 4 2 -1.37 2.40
-17 -4 -2 -0.51 1.85
17 4 2 0.44 1.73
-17 -4 -3 8.66 2.06
17 4 3 8.02 2.45
17 4 3 7.96 2.11
-17 -4 -4 4.78 2.08
17 4 4 2.78 2.23
-17 -4 -5 111.77 4.95
17 4 5 87.95 5.73
17 4 5 96.95 5.40
-17 -4 -6 18.19 2.42
17 4 6 10.45 2.93
17 4 6 11.84 2.87
-17 -4 -7 7.69 2.15
17 4 7 5.30 2.81
17 4 7 2.88 2.63
-17 -4 -8 0.09 2.03
17 4 8 -0.85 2.54
-17 -4 -9 20.49 2.43
17 4 9 12.05 2.89
-17 -4 -10 5.44 2.07
-17 -5 5 1.06 2.27
-17 -5 4 2.83 2.39
-17 -5 3 33.29 3.47
-17 -5 2 19.15 2.90
-17 -5 1 43.95 3.77
-17 -5 0 0.80 2.17
-17 -5 -1 12.86 2.39
-17 -5 -2 6.00 1.71
-17 -5 -2 2.69 1.95
17 5 2 4.24 2.02
-17 -5 -3 2.50 1.76
17 5 3 1.69 2.32
17 5 3 1.77 1.98
-17 -5 -4 39.50 2.83
17 5 4 29.48 3.11
-17 -5 -5 11.18 2.10
17 5 5 7.80 2.80
17 5 5 11.21 2.58
-17 -5 -6 36.27 2.80
17 5 6 32.05 3.88
17 5 6 34.60 3.45
-17 -5 -7 1.79 1.87
17 5 7 1.74 2.52
17 5 7 3.80 2.37
-17 -5 -8 39.26 2.89
17 5 8 31.89 3.42
-17 -5 -9 5.98 2.02
17 5 9 4.69 2.42
-17 -5 -10 2.09 2.00
-17 -5 -11 2.46 2.13
-17 -6 2 6.97 2.39
-17 -6 1 37.22 3.46
-17 -6 0 18.01 2.69
-17 -6 -1 4.08 1.63
-17 -6 -1 0.49 1.98
-17 -6 -2 -0.12 1.88
17 6 2 -1.50 1.99
-17 -6 -3 3.47 1.63
-17 -6 -3 1.81 1.85
17 6 3 -1.10 1.94
17 6 4 1.14 2.12
-17 -6 -4 5.18 1.68
17 6 5 11.92 2.55
-17 -6 -5 18.29 2.10
17 6 6 0.55 2.18
-17 -6 -6 0.79 1.69
-17 -6 -6 0.67 1.99
17 6 7 1.14 2.18
17 6 7 -0.64 2.60
-17 -6 -7 4.74 1.81
-17 -6 -7 0.58 1.95
-17 -6 -8 3.10 1.85
17 6 8 3.73 2.26
-17 -6 -9 0.58 1.85
17 6 9 1.55 2.43
-17 -6 -10 27.36 2.87
-17 -6 -11 12.17 2.42
-17 -6 -12 1.71 2.16
-17 -7 0 1.35 1.41
-17 -7 -1 5.78 1.58
-17 -7 -2 15.20 2.18
-17 -7 -2 16.49 2.24
17 7 2 18.59 2.62
-17 -7 -3 -0.48 1.80
-17 -7 -3 2.74 1.62
-17 -7 -3 -0.21 1.76
17 7 3 1.74 2.10
17 7 4 -2.63 2.32
-17 -7 -4 -1.71 2.10
-17 -7 -4 0.97 1.54
17 7 5 -3.17 2.46
-17 -7 -5 -2.10 1.99
-17 -7 -5 -1.18 1.59
17 7 6 6.99 2.50
-17 -7 -6 8.24 2.21
-17 -7 -6 11.76 1.81
17 7 7 7.65 2.54
-17 -7 -7 7.56 2.17
-17 -7 -7 8.35 1.79
17 7 8 -0.78 2.34
-17 -7 -8 2.38 1.74
17 7 9 2.08 2.45
-17 -7 -9 2.74 1.91
-17 -7 -10 65.04 4.09
-17 -7 -11 -0.57 2.01
17 8 2 26.85 2.98
17 8 3 0.65 2.21
-17 -8 -3 0.85 1.90
17 8 4 44.77 3.79
-17 -8 -4 47.24 3.35
17 8 5 -1.00 2.48
-17 -8 -5 2.39 1.96
17 8 6 0.45 2.34
-17 -8 -6 5.35 2.10
17 8 7 5.88 2.46
-17 -8 -7 4.89 2.06
17 8 8 1.77 2.46
17 8 9 10.17 2.94
17 9 3 14.88 2.69
-17 -9 -3 16.06 2.26
17 9 4 95.41 5.46
-17 -9 -4 95.43 4.88
17 9 5 47.22 3.99
-17 -9 -5 47.43 3.41
17 9 6 13.04 2.98
-17 -9 -6 16.28 2.42
17 9 7 -0.16 2.42
-17 -9 -7 2.16 2.03
17 9 8 0.67 2.52
17 9 9 -0.17 2.71
17 10 4 1.73 2.36
-17 -10 -4 0.30 1.87
17 10 5 10.42 2.67
-17 -10 -5 9.47 2.20
17 10 6 6.33 2.56
-17 -10 -6 7.11 2.08
17 10 7 5.45 2.64
17 10 8 3.43 2.60
17 11 4 -1.18 2.61
17 11 5 1.24 2.41
-17 -11 -5 -0.42 1.84
17 11 6 6.03 2.55
17 11 7 3.40 2.58
17 12 5 -0.48 2.40
17 12 6 1.51 2.60
17 12 7 1.39 2.50
18 1 1 -1.23 2.28
18 1 2 2.39 2.42
18 2 1 4.15 2.43
18 2 2 5.68 2.47
18 2 3 7.82 2.52
18 2 5 4.78 2.43
18 2 6 1.06 2.26
18 3 1 3.50 2.43
18 3 2 3.44 2.38
-18 -3 -3 7.16 2.20
18 3 3 4.27 2.47
-18 -3 -4 7.96 2.24
18 3 5 15.95 2.75
18 3 6 1.36 2.38
-18 -4 1 -0.46 2.27
-18 -4 0 3.54 2.27
-18 -4 -1 -0.28 2.06
18 4 1 2.24 2.33
-18 -4 -2 0.35 1.98
18 4 2 -0.73 2.39
-18 -4 -3 2.51 2.11
18 4 3 -0.45 2.44
-18 -4 -4 12.69 2.25
18 4 4 9.20 2.74
-18 -4 -5 53.42 3.41
18 4 5 46.42 3.77
-18 -4 -6 9.99 2.27
18 4 6 10.84 2.65
18 4 7 12.35 2.78
-18 -5 -1 2.30 2.17
-18 -5 -1 4.08 1.79
-18 -5 -2 11.77 2.40
-18 -5 -2 24.80 2.44
-18 -5 -3 4.84 2.07
-18 -5 -3 9.08 1.92
18 5 4 16.97 3.10
-18 -5 -4 27.19 2.53
-18 -5 -5 8.87 2.10
18 5 5 9.49 2.45
-18 -5 -6 19.28 2.52
18 5 6 18.32 2.91
-18 -5 -7 0.64 2.06
18 5 7 1.03 2.21
-18 -5 -8 23.12 2.47
-18 -6 -3 5.63 1.74
-18 -6 -4 2.59 1.68
-18 -6 -5 20.50 2.23
18 6 5 15.51 2.66
-18 -6 -6 4.50 1.84
18 6 6 3.91 2.39
-18 -6 -7 0.89 1.60
18 6 7 0.61 2.36
18 7 5 -2.74 2.57
18 7 6 0.90 2.42
18 7 7 -2.18 2.45
18 8 6 -2.17 2.58
18 8 7 -1.29 2.50
18 9 6 5.63 2.68
18 9 7 1.33 2.51
0 0 0 0.00 0.00
TITL exp_50 in P-1
REM P-1 (#2 in standard setting)
CELL 0.71073 13.640637 14.056777 18.590651 83.6258 86.1864 72.2885
ZERR 15.00 0.000484 0.000541 0.000652 0.0030 0.0029 0.0033
LATT 1
SFAC C H N O
UNIT 165.00 150.00 15.00 15.00
TREF
HKLF 4
END
_computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'
;
_shelx_hkl_checksum 55611
_shelx_res_file
;
TITL exp_50_a.res in P-1
z4_tmp.res
created by SHELXL-2018/3 at 11:28:45 on 27-May-2021
REM Old TITL exp_50 in P-1
REM SHELXT solution in P-1: R1 0.096, Rweak 0.005, Alpha 0.053
REM 0.000 for 0 systematic absences, Orientation as input
REM Formula found by SHELXT: C67 Cu6 N6 O18
REM ETHANOL
REM #####
CELL 0.71073 13.6406 14.0568 18.5907 83.626 86.186 72.288
ZERR 2 0.0005 0.0005 0.0007 0.003 0.003 0.003
LATT 1
SFAC C H Cu N O
UNIT 126 160 12 16 42
EQIV $1 1-X,1-Y,1-Z
EQIV $2 1-X,1-Y,-Z
DFIX 2.2 0.01 H1E H1Wa
DFIX 2.2 0.01 H10 H2Wb
DANG 1.44 0.004 C9E C8E
L.S. 10 0 0
PLAN 8
HTAB O1W O13
HTAB O1W O1E
HTAB O10 O11
HTAB O10 O2W
HTAB O10 O1W
HTAB C11 O4E_$1
HTAB C18 O13_$2
HTAB O4E N202
HTAB O4E O16B
HTAB O4E O15B
FREE O16A O14A
BIND Cu5 O1
BIND Cu6 O14B
FREE Cu6 O11
CONF
list 4
MORE -1
HTAB
fmap 2 53
acta
SHEL 999 0.79
OMIT -4 0 14
OMIT 4 -9 2
OMIT 5 -2 5
OMIT 2 10 2
OMIT -4 0 13
OMIT 3 -11 3
OMIT 6 -1 3
OMIT 5 -8 1
OMIT 1 -13 7
REM
REM
REM
WGHT 0.043200 3.269600
FVAR 0.27286 0.56568
CU3 3 0.269146 0.401247 0.158877 11.00000 0.03783 0.02639 =
0.02544 0.00037 -0.00082 -0.00612
CU1 3 0.277755 0.426239 0.327899 11.00000 0.03459 0.02884 =
0.02828 -0.00249 0.00320 -0.00970
CU5 3 0.342762 0.208957 0.272332 11.00000 0.03869 0.02569 =
0.03087 0.00283 -0.00316 -0.01019
CU4 3 0.453149 0.201823 0.108094 11.00000 0.03985 0.02640 =
0.03622 -0.00257 -0.00088 -0.01025
CU2 3 0.345368 0.582939 0.204078 11.00000 0.03940 0.02984 =
0.03844 -0.00033 0.00403 -0.01114
O11 5 0.471626 0.471746 0.184589 11.00000 0.04833 0.03896 =
0.07024 0.01124 0.02106 -0.01027
N102 4 0.549115 0.492916 0.155067 11.00000 0.04959 0.03498 =
0.04552 -0.00624 0.00812 -0.01528
O12 5 0.556563 0.576308 0.154530 11.00000 0.08378 0.04154 =
0.11513 -0.00039 -0.01586 -0.03216
O13 5 0.614055 0.424076 0.128000 11.00000 0.08524 0.06601 =
0.12410 -0.02536 0.06219 -0.01269
CU6 3 0.469021 0.252211 0.409154 11.00000 0.03732 0.04047 =
0.03351 0.00147 -0.00105 -0.01265
PART 2
O14B 5 0.647470 0.152053 0.430657 -21.00000 0.03571 0.09640 =
0.08187 -0.02479 -0.00739 -0.00018
PART 0
N202 4 0.696123 0.160542 0.484949 11.00000 0.06224 0.07870 =
0.08301 -0.00220 -0.00933 -0.02308
PART 2
O16B 5 0.763749 0.202884 0.468231 -21.00000 0.06404 0.14286 =
0.07255 -0.00351 -0.00780 -0.06037
O15B 5 0.707716 0.101615 0.541849 -21.00000 0.15342 0.14856 =
0.14782 0.05313 -0.04254 -0.09251
PART 0
O10 5 0.352310 0.346397 0.247266 11.00000 0.02965 0.02749 =
0.02828 0.00124 0.00149 -0.00772
H10 2 0.383759 0.349935 0.231768 11.00000 0.07266
O2 5 0.348843 0.527830 0.304529 11.00000 0.03589 0.03291 =
0.03657 -0.00305 0.00121 -0.01242
O5 5 0.376952 0.340712 0.090288 11.00000 0.04325 0.02775 =
0.03130 -0.00339 0.00335 -0.00883
O8 5 0.458283 0.167929 0.336365 11.00000 0.03811 0.03269 =
0.03602 0.00370 -0.00316 -0.00934
O4 5 0.173007 0.478757 0.224243 11.00000 0.03760 0.03723 =
0.03038 -0.00361 -0.00266 -0.00043
O1 5 0.229116 0.316416 0.358266 11.00000 0.05381 0.03685 =
0.03577 -0.00452 0.01271 -0.01916
O7 5 0.244636 0.244276 0.199289 11.00000 0.05061 0.03279 =
0.03925 0.00620 -0.01183 -0.01890
O9 5 0.460669 0.346748 0.473845 11.00000 0.06162 0.05461 =
0.03768 -0.00532 0.00336 -0.02622
O3 5 0.331695 0.622545 0.105793 11.00000 0.05303 0.04560 =
0.04010 0.00024 0.00646 -0.00925
O2W 5 0.524618 0.340178 0.333826 11.00000 0.05447 0.04885 =
0.04286 -0.00011 0.00294 -0.02187
AFIX 7
H2WA 2 0.483126 0.400782 0.330414 11.00000 -1.50000
H2WB 2 0.524712 0.321109 0.291044 11.00000 -1.50000
AFIX 0
O6 5 0.520420 0.068429 0.135534 11.00000 0.05728 0.02917 =
0.05922 -0.00062 -0.02161 -0.01135
O1W 5 0.553786 0.244092 0.157006 11.00000 0.05564 0.03439 =
0.08285 -0.00197 -0.01963 -0.01755
AFIX 7
H1WA 2 0.552628 0.224827 0.202374 11.00000 -1.50000
H1WB 2 0.535206 0.308242 0.155417 11.00000 -1.50000
AFIX 0
N5 4 0.344653 0.069086 0.283118 11.00000 0.04420 0.02741 =
0.03695 0.00142 -0.00141 -0.01063
N1 4 0.231706 0.489266 0.417868 11.00000 0.03788 0.03636 =
0.03045 -0.00468 -0.00075 -0.00853
N3 4 0.192972 0.474960 0.073865 11.00000 0.04763 0.02838 =
0.02763 0.00189 -0.00219 -0.00963
N4 4 0.356425 0.175106 0.047606 11.00000 0.04447 0.02962 =
0.03185 -0.00186 -0.00181 -0.01020
N2 4 0.222629 0.686555 0.232301 11.00000 0.04267 0.02991 =
0.04016 -0.00330 -0.00063 -0.01082
N6 4 0.403436 0.171465 0.475571 11.00000 0.03859 0.03889 =
0.03525 0.00471 -0.00345 -0.00907
C7 1 0.186073 0.456028 0.473986 11.00000 0.03417 0.03948 =
0.03040 -0.00135 -0.00180 -0.00068
C20 1 0.076348 0.527702 0.210004 11.00000 0.03480 0.03222 =
0.03755 -0.00116 -0.00354 -0.00867
C1 1 0.160667 0.313447 0.411291 11.00000 0.03749 0.03419 =
0.03791 0.00600 0.00224 -0.00813
C26 1 0.106128 0.544510 0.073212 11.00000 0.04670 0.02960 =
0.03392 0.00144 -0.00940 -0.01305
C10 1 0.299109 0.610666 0.346266 11.00000 0.04741 0.03692 =
0.03889 -0.00935 0.00029 -0.01804
AFIX 13
H10A 2 0.344598 0.652585 0.347556 11.00000 -1.20000
AFIX 0
C25 1 0.039822 0.563172 0.139059 11.00000 0.03881 0.03595 =
0.04083 0.00232 -0.00552 -0.01008
C48 1 0.460545 0.073394 0.374279 11.00000 0.03904 0.03153 =
0.04366 0.00576 -0.00598 -0.00297
AFIX 13
H48 2 0.530044 0.040509 0.391873 11.00000 -1.20000
AFIX 0
C11 1 0.200297 0.672250 0.310418 11.00000 0.05047 0.03399 =
0.03856 -0.00763 0.00492 -0.01125
AFIX 23
H11A 2 0.148399 0.637664 0.319344 11.00000 -1.20000
H11B 2 0.174402 0.736740 0.330030 11.00000 -1.20000
AFIX 0
C45 1 0.288056 0.028592 0.251892 11.00000 0.05354 0.03256 =
0.03581 -0.00034 0.00755 -0.01790
C39 1 0.178799 0.195314 0.191475 11.00000 0.05025 0.04364 =
0.02804 0.00046 -0.00124 -0.02391
C12 1 0.153874 0.746588 0.190128 11.00000 0.04662 0.02851 =
0.04816 -0.00532 -0.00179 -0.01279
C33 1 0.411380 -0.004131 0.074857 11.00000 0.04393 0.03039 =
0.03767 -0.00427 0.00373 -0.01375
C38 1 0.495478 -0.008992 0.117580 11.00000 0.04812 0.02882 =
0.04023 -0.00150 0.00093 -0.01175
C14 1 0.175537 0.762849 0.112492 11.00000 0.05513 0.03232 =
0.04390 -0.00022 -0.00763 -0.01550
C31 1 0.341168 0.089691 0.042567 11.00000 0.04589 0.03479 =
0.03740 -0.00531 0.00071 -0.01429
C6 1 0.139510 0.375963 0.469342 11.00000 0.03399 0.04014 =
0.03477 0.00472 0.00240 -0.00314
C29 1 0.336333 0.352473 0.020493 11.00000 0.05333 0.03166 =
0.02807 -0.00080 0.00598 -0.01118
AFIX 13
H29 2 0.392788 0.346029 -0.015882 11.00000 -1.20000
AFIX 0
C52 1 0.386103 0.268305 0.577057 11.00000 0.03578 0.05008 =
0.03495 0.00060 -0.00353 -0.00419
C57 1 0.433300 0.339346 0.542794 11.00000 0.03435 0.05570 =
0.03663 -0.00416 -0.00430 -0.00949
C50 1 0.363011 0.191945 0.539112 11.00000 0.03405 0.04109 =
0.03833 0.00915 -0.00271 -0.00278
C30 1 0.287264 0.269726 0.015036 11.00000 0.05216 0.03301 =
0.03224 -0.00188 -0.00614 -0.00687
AFIX 23
H30A 2 0.220724 0.285068 0.040503 11.00000 -1.20000
H30B 2 0.277218 0.264110 -0.035304 11.00000 -1.20000
AFIX 0
C28 1 0.260264 0.456340 0.008310 11.00000 0.06440 0.03170 =
0.02793 0.00377 0.00267 -0.01025
AFIX 23
H28A 2 0.296647 0.506237 -0.000681 11.00000 -1.20000
H28B 2 0.219496 0.460380 -0.033360 11.00000 -1.20000
AFIX 0
C49 1 0.385425 0.090971 0.438969 11.00000 0.04668 0.03743 =
0.03979 0.00655 -0.00300 -0.01255
AFIX 23
H49A 2 0.315113 0.110708 0.423144 11.00000 -1.20000
H49B 2 0.396950 0.030161 0.471690 11.00000 -1.20000
AFIX 0
C47 1 0.435670 0.007651 0.323428 11.00000 0.04903 0.02988 =
0.04768 0.00146 -0.00131 -0.00255
AFIX 23
H47A 2 0.493601 -0.016513 0.290148 11.00000 -1.20000
H47B 2 0.421140 -0.049776 0.350687 11.00000 -1.20000
AFIX 0
C34 1 0.396127 -0.095947 0.062302 11.00000 0.05030 0.03351 =
0.05564 -0.00818 0.00203 -0.01577
AFIX 43
H34 2 0.341428 -0.094117 0.034323 11.00000 -1.20000
AFIX 0
C9 1 0.278271 0.569593 0.422813 11.00000 0.05165 0.04306 =
0.03824 -0.00964 -0.00467 -0.01615
AFIX 23
H9A 2 0.342047 0.543434 0.448457 11.00000 -1.20000
H9B 2 0.231806 0.622368 0.448939 11.00000 -1.20000
AFIX 0
C44 1 0.196749 0.091201 0.213628 11.00000 0.05642 0.04393 =
0.03650 0.00083 -0.00185 -0.02670
C19 1 0.263390 0.701373 0.076121 11.00000 0.05521 0.03928 =
0.03997 -0.00126 -0.00198 -0.02311
C37 1 0.558112 -0.104309 0.144356 11.00000 0.05168 0.03362 =
0.05065 -0.00049 -0.00533 -0.00786
AFIX 43
H37 2 0.613835 -0.108570 0.172097 11.00000 -1.20000
AFIX 0
C40 1 0.086246 0.248513 0.157706 11.00000 0.05723 0.05390 =
0.04379 0.00933 -0.01258 -0.02358
AFIX 43
H40 2 0.074005 0.316381 0.142863 11.00000 -1.20000
AFIX 0
C21 1 0.005539 0.548342 0.269065 11.00000 0.04175 0.06057 =
0.04173 0.00312 0.00168 -0.00984
AFIX 43
H21 2 0.027877 0.524611 0.315701 11.00000 -1.20000
AFIX 0
C27 1 0.069703 0.609601 0.004288 11.00000 0.06167 0.03843 =
0.04290 0.00860 -0.01284 -0.00737
AFIX 137
H27A 2 0.027849 0.674821 0.015851 11.00000 -1.50000
H27B 2 0.029929 0.579511 -0.021464 11.00000 -1.50000
H27C 2 0.128140 0.615913 -0.025405 11.00000 -1.50000
AFIX 0
C35 1 0.458294 -0.187559 0.089492 11.00000 0.05566 0.02769 =
0.06912 -0.00984 0.00739 -0.01478
AFIX 43
H35 2 0.445766 -0.246387 0.080161 11.00000 -1.20000
AFIX 0
C56 1 0.450078 0.410487 0.584862 11.00000 0.05051 0.07430 =
0.04947 -0.01211 -0.00188 -0.02656
AFIX 43
H56 2 0.478737 0.458896 0.562606 11.00000 -1.20000
AFIX 0
C5 1 0.069825 0.358733 0.525160 11.00000 0.04428 0.05264 =
0.04446 0.00310 0.01227 -0.00362
AFIX 43
H5 2 0.056342 0.397695 0.564032 11.00000 -1.20000
AFIX 0
C8 1 0.179181 0.499661 0.545388 11.00000 0.05818 0.05957 =
0.03019 -0.00717 0.00142 -0.00994
AFIX 137
H8A 2 0.197019 0.446278 0.583647 11.00000 -1.50000
H8B 2 0.110182 0.541525 0.553991 11.00000 -1.50000
H8C 2 0.225958 0.538942 0.543959 11.00000 -1.50000
AFIX 0
C36 1 0.539400 -0.190921 0.130754 11.00000 0.06101 0.02917 =
0.05841 -0.00042 0.00401 -0.00764
AFIX 43
H36 2 0.582000 -0.252565 0.149631 11.00000 -1.20000
AFIX 0
C53 1 0.361210 0.271810 0.652027 11.00000 0.05674 0.06930 =
0.04048 0.00314 0.00210 -0.01493
AFIX 43
H53 2 0.330892 0.225414 0.675595 11.00000 -1.20000
AFIX 0
C2 1 0.108199 0.241807 0.411367 11.00000 0.05815 0.04482 =
0.06041 -0.00012 0.00789 -0.02169
AFIX 43
H2 2 0.119918 0.201860 0.373136 11.00000 -1.20000
AFIX 0
C18 1 0.277992 0.725269 0.000779 11.00000 0.07264 0.05378 =
0.04129 -0.00090 0.00096 -0.03066
AFIX 43
H18 2 0.334628 0.685543 -0.023813 11.00000 -1.20000
AFIX 0
C4 1 0.021431 0.286847 0.524157 11.00000 0.04773 0.05821 =
0.06948 0.01048 0.02209 -0.01174
AFIX 43
H4 2 -0.023576 0.276928 0.562031 11.00000 -1.20000
AFIX 0
C51 1 0.290189 0.138146 0.574904 11.00000 0.05220 0.05554 =
0.05086 0.00660 0.00968 -0.01463
AFIX 137
H51A 2 0.230334 0.185992 0.593733 11.00000 -1.50000
H51B 2 0.323795 0.091260 0.613790 11.00000 -1.50000
H51C 2 0.269921 0.102823 0.540051 11.00000 -1.50000
AFIX 0
C13 1 0.049398 0.800071 0.220896 11.00000 0.04975 0.04378 =
0.06108 -0.00241 0.00004 -0.00304
AFIX 137
H13A 2 0.000138 0.817472 0.183404 11.00000 -1.50000
H13B 2 0.051906 0.859959 0.240006 11.00000 -1.50000
H13C 2 0.029410 0.756948 0.258935 11.00000 -1.50000
AFIX 0
C17 1 0.210999 0.805079 -0.036471 11.00000 0.09663 0.05883 =
0.04228 0.00604 -0.01267 -0.03678
AFIX 43
H17 2 0.222439 0.819080 -0.085837 11.00000 -1.20000
AFIX 0
C46 1 0.313099 -0.084032 0.255077 11.00000 0.07430 0.03532 =
0.05972 -0.00525 0.00429 -0.02423
AFIX 137
H46A 2 0.288793 -0.101614 0.212633 11.00000 -1.50000
H46B 2 0.280145 -0.107984 0.297433 11.00000 -1.50000
H46C 2 0.386285 -0.114111 0.257190 11.00000 -1.50000
AFIX 0
C55 1 0.425296 0.410015 0.657393 11.00000 0.06392 0.09613 =
0.04688 -0.02200 -0.00355 -0.03256
AFIX 43
H55 2 0.439053 0.456522 0.683947 11.00000 -1.20000
AFIX 0
C24 1 -0.064341 0.618419 0.132611 11.00000 0.03986 0.07744 =
0.05362 0.00899 -0.01017 -0.00747
AFIX 43
H24 2 -0.089030 0.642032 0.086524 11.00000 -1.20000
AFIX 0
C3 1 0.039878 0.229229 0.466591 11.00000 0.05519 0.05446 =
0.08172 0.00504 0.01376 -0.02740
AFIX 43
H3 2 0.005786 0.181409 0.465104 11.00000 -1.20000
AFIX 0
C43 1 0.119923 0.048453 0.199376 11.00000 0.08312 0.06116 =
0.07061 0.01354 -0.01974 -0.04754
AFIX 43
H43 2 0.130776 -0.019621 0.212685 11.00000 -1.20000
AFIX 0
C15 1 0.109284 0.843783 0.071329 11.00000 0.07490 0.04268 =
0.05791 -0.00164 -0.01362 -0.00690
AFIX 43
H15 2 0.051529 0.884516 0.094237 11.00000 -1.20000
AFIX 0
C22 1 -0.096110 0.602901 0.259359 11.00000 0.03897 0.09431 =
0.05895 0.00616 0.01037 -0.00807
AFIX 43
H22 2 -0.141280 0.615301 0.299338 11.00000 -1.20000
AFIX 0
C16 1 0.126344 0.865125 -0.001237 11.00000 0.09777 0.04875 =
0.05799 0.00954 -0.02559 -0.01364
AFIX 43
H16 2 0.081091 0.919827 -0.026654 11.00000 -1.20000
AFIX 0
C32 1 0.249566 0.084854 0.004067 11.00000 0.06347 0.05017 =
0.07160 -0.00247 -0.02432 -0.02162
AFIX 137
H32A 2 0.214545 0.044365 0.034003 11.00000 -1.50000
H32B 2 0.272193 0.055764 -0.040759 11.00000 -1.50000
H32C 2 0.203461 0.151345 -0.005629 11.00000 -1.50000
AFIX 0
C41 1 0.013173 0.203204 0.145938 11.00000 0.06377 0.08015 =
0.06272 0.01868 -0.02373 -0.03850
AFIX 43
H41 2 -0.047657 0.240543 0.123863 11.00000 -1.20000
AFIX 0
C54 1 0.380112 0.341036 0.691213 11.00000 0.07457 0.09810 =
0.03567 -0.00974 0.00025 -0.02958
AFIX 43
H54 2 0.362483 0.341361 0.740396 11.00000 -1.20000
AFIX 0
C42 1 0.030145 0.102320 0.166897 11.00000 0.08557 0.09015 =
0.08303 0.02311 -0.03540 -0.06265
AFIX 43
H42 2 -0.018959 0.071318 0.159012 11.00000 -1.20000
AFIX 0
C23 1 -0.131396 0.639234 0.190951 11.00000 0.03500 0.10405 =
0.07540 0.01160 -0.00537 -0.00099
AFIX 43
H23 2 -0.199653 0.677280 0.184504 11.00000 -1.20000
AFIX 0
O1E 5 0.718446 0.147345 0.230390 11.00000 0.11552 0.07845 =
0.13524 -0.00379 -0.05638 -0.01825
AFIX 147
H1E 2 0.696426 0.187818 0.260536 11.00000 -1.50000
AFIX 0
C2E 1 0.719527 0.049764 0.261757 11.00000 0.10355 0.09581 =
0.08477 0.01692 -0.01025 -0.02993
AFIX 23
H2EA 2 0.649987 0.044852 0.267654 11.00000 -1.20000
H2EB 2 0.750187 0.035764 0.308862 11.00000 -1.20000
AFIX 0
C3E 1 0.780446 -0.020816 0.212254 11.00000 0.08870 0.10864 =
0.20698 -0.05449 0.01308 -0.02539
AFIX 137
H3EA 2 0.780131 -0.087531 0.229966 11.00000 -1.50000
H3EB 2 0.849951 -0.017689 0.208977 11.00000 -1.50000
H3EC 2 0.751412 -0.003753 0.165191 11.00000 -1.50000
AFIX 0
O4E 5 0.882651 0.118727 0.610967 11.00000 0.10349 0.08828 =
0.12917 -0.05205 -0.02366 -0.01573
AFIX 147
H4E 2 0.829086 0.136427 0.588792 11.00000 -1.50000
AFIX 0
C5E 1 0.936197 0.024103 0.598013 11.00000 0.13597 0.07748 =
0.09451 -0.02558 0.01072 -0.02582
AFIX 23
H5EA 2 0.937397 0.017419 0.546563 11.00000 -1.20000
H5EB 2 0.902534 -0.022216 0.623292 11.00000 -1.20000
AFIX 0
C6E 1 1.041631 -0.001125 0.622166 11.00000 0.13730 0.12654 =
0.11764 -0.01975 -0.02565 0.01162
AFIX 137
H6EA 2 1.080592 -0.065847 0.607859 11.00000 -1.50000
H6EB 2 1.040758 -0.002482 0.673943 11.00000 -1.50000
H6EC 2 1.072798 0.048381 0.600560 11.00000 -1.50000
AFIX 0
O7E 5 0.731861 0.283408 0.327904 11.00000 0.08715 0.17159 =
0.10334 0.01599 -0.00091 -0.06065
AFIX 147
H7E 2 0.695981 0.316198 0.359088 11.00000 -1.50000
AFIX 0
C8E 1 0.823239 0.317656 0.310236 11.00000 0.26386 0.17729 =
0.11427 -0.03269 0.02576 -0.12254
AFIX 23
H8EA 2 0.836358 0.352431 0.349068 11.00000 -1.20000
H8EB 2 0.883662 0.261511 0.301851 11.00000 -1.20000
AFIX 0
C9E 1 0.797673 0.383694 0.246151 11.00000 0.17413 0.17173 =
0.34039 -0.04453 0.03236 -0.05340
AFIX 137
H9EA 2 0.778579 0.349547 0.209975 11.00000 -1.50000
H9EB 2 0.856115 0.405052 0.228575 11.00000 -1.50000
H9EC 2 0.741038 0.441138 0.256569 11.00000 -1.50000
AFIX 0
PART 1
O16A 5 0.750344 0.216281 0.477910 21.00000 0.13409 0.10335 =
0.12563 -0.02549 -0.00774 -0.07024
O15A 5 0.674545 0.138392 0.546611 21.00000 0.13123 0.14576 =
0.06118 0.02592 0.00004 -0.04269
O14A 5 0.649866 0.144114 0.437593 21.00000 0.07904 0.07127 =
0.11138 -0.01544 -0.02769 -0.02654
HKLF 4
REM exp_50_a.res in P-1
REM wR2 = 0.0911, GooF = S = 1.037, Restrained GooF = 1.038 for all data
REM R1 = 0.0330 for 12395 Fo > 4sig(Fo) and 0.0395 for all 14284 data
REM 929 parameters refined using 3 restraints
END
WGHT 0.0432 3.2694
REM Instructions for potential hydrogen bonds
HTAB O2W O2
HTAB O2W O10
HTAB O1W O11
HTAB O1W N102
HTAB O1W O13
HTAB C11 O4E_$1
EQIV $3 -x+1, -y, -z+1
HTAB C47 O15A_$3
HTAB C18 O13_$2
HTAB O1E O7E
HTAB O4E N202
HTAB O4E O16B
HTAB O4E O15B
HTAB O4E O16A
HTAB O4E O15A
REM Highest difference peak 0.817, deepest hole -0.556, 1-sigma level 0.064
Q1 1 0.6489 0.1426 0.2656 11.00000 0.05 0.82
Q2 1 0.5000 0.5000 0.0000 10.50000 0.05 0.72
Q3 1 0.7138 0.3401 0.3705 11.00000 0.05 0.67
Q4 1 0.7851 0.3616 0.2999 11.00000 0.05 0.61
Q5 1 0.8998 0.3169 0.3122 11.00000 0.05 0.59
Q6 1 0.6113 0.1172 0.2150 11.00000 0.05 0.54
Q7 1 0.5965 0.3233 0.3350 11.00000 0.05 0.51
Q8 1 0.6113 0.2039 0.1754 11.00000 0.05 0.46
;
_shelx_res_checksum 18701
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cu Cu3 0.26915(2) 0.40125(2) 0.15888(2) 0.03091(7) Uani d 1 . .
Cu Cu1 0.27776(2) 0.42624(2) 0.32790(2) 0.03074(7) Uani d 1 . .
Cu Cu5 0.34276(2) 0.20896(2) 0.27233(2) 0.03197(7) Uani d 1 . .
Cu Cu4 0.45315(2) 0.20182(2) 0.10809(2) 0.03414(8) Uani d 1 . .
Cu Cu2 0.34537(2) 0.58294(2) 0.20408(2) 0.03620(8) Uani d 1 . .
O O11 0.47163(16) 0.47175(15) 0.18459(13) 0.0555(6) Uani d 1 . .
N N102 0.54911(19) 0.49292(17) 0.15507(13) 0.0430(5) Uani d 1 . .
O O12 0.5566(2) 0.57631(18) 0.15453(17) 0.0771(8) Uani d 1 . .
O O13 0.6141(2) 0.4241(2) 0.12800(19) 0.0958(11) Uani d 1 . .
Cu Cu6 0.46902(2) 0.25221(2) 0.40915(2) 0.03727(8) Uani d 1 . .
O O14B 0.6475(14) 0.152(2) 0.4307(18) 0.074(6) Uani d 0.43(8) A 2
N N202 0.6961(3) 0.1605(3) 0.4849(2) 0.0743(9) Uani d 1 . .
O O16B 0.7637(19) 0.203(3) 0.4682(15) 0.087(7) Uani d 0.43(8) A 2
O O15B 0.708(5) 0.102(5) 0.5418(17) 0.143(11) Uani d 0.43(8) A 2
O O10 0.35231(15) 0.34640(13) 0.24727(10) 0.0291(4) Uani d 1 . .
H H10 0.384(2) 0.350(4) 0.232(2) 0.073(17) Uiso d 1 . .
O O2 0.34884(13) 0.52783(13) 0.30453(9) 0.0348(4) Uani d 1 . .
O O5 0.37695(14) 0.34071(12) 0.09029(9) 0.0347(4) Uani d 1 . .
O O8 0.45828(14) 0.16793(13) 0.33636(9) 0.0364(4) Uani d 1 . .
O O4 0.17301(13) 0.47876(13) 0.22424(9) 0.0374(4) Uani d 1 . .
O O1 0.22912(15) 0.31642(14) 0.35827(10) 0.0415(4) Uani d 1 . .
O O7 0.24464(15) 0.24428(13) 0.19929(10) 0.0397(4) Uani d 1 . .
O O9 0.46067(17) 0.34675(16) 0.47384(10) 0.0495(5) Uani d 1 . .
O O3 0.33169(16) 0.62254(15) 0.10579(11) 0.0482(5) Uani d 1 . .
O O2W 0.52462(16) 0.34018(16) 0.33383(11) 0.0478(5) Uani d 1 . .
H H2WA 0.483126 0.400782 0.330414 0.072 Uiso d 1 . .
H H2WB 0.524712 0.321109 0.291044 0.072 Uiso d 1 . .
O O6 0.52042(16) 0.06843(14) 0.13553(12) 0.0483(5) Uani d 1 . .
O O1W 0.55379(17) 0.24409(15) 0.15701(14) 0.0562(6) Uani d 1 . .
H H1WA 0.552628 0.224827 0.202374 0.084 Uiso d 1 . .
H H1WB 0.535206 0.308242 0.155417 0.084 Uiso d 1 . .
N N5 0.34465(17) 0.06909(15) 0.28312(12) 0.0366(5) Uani d 1 . .
N N1 0.23171(16) 0.48927(16) 0.41787(11) 0.0354(4) Uani d 1 . .
N N3 0.19297(17) 0.47496(15) 0.07387(11) 0.0353(4) Uani d 1 . .
N N4 0.35642(17) 0.17511(15) 0.04761(11) 0.0356(4) Uani d 1 . .
N N2 0.22263(17) 0.68655(16) 0.23230(12) 0.0376(5) Uani d 1 . .
N N6 0.40344(17) 0.17147(17) 0.47557(12) 0.0387(5) Uani d 1 . .
C C7 0.18607(19) 0.4560(2) 0.47399(13) 0.0371(5) Uani d 1 . .
C C20 0.07635(19) 0.52770(19) 0.21000(14) 0.0352(5) Uani d 1 . .
C C1 0.1607(2) 0.31345(19) 0.41129(14) 0.0380(5) Uani d 1 . .
C C26 0.1061(2) 0.54451(18) 0.07321(13) 0.0363(5) Uani d 1 . .
C C10 0.2991(2) 0.6107(2) 0.34627(14) 0.0395(6) Uani d 1 . .
H H10A 0.344598 0.652585 0.347556 0.047 Uiso calc 1 . .
C C25 0.0398(2) 0.5632(2) 0.13906(15) 0.0391(6) Uani d 1 . .
C C48 0.4605(2) 0.07339(19) 0.37428(15) 0.0403(6) Uani d 1 . .
H H48 0.530044 0.040509 0.391873 0.048 Uiso calc 1 . .
C C11 0.2003(2) 0.6723(2) 0.31042(14) 0.0413(6) Uani d 1 . .
H H11A 0.148399 0.637664 0.319344 0.050 Uiso calc 1 . .
H H11B 0.174402 0.736740 0.330030 0.050 Uiso calc 1 . .
C C45 0.2881(2) 0.0286(2) 0.25189(14) 0.0402(6) Uani d 1 . .
C C39 0.1788(2) 0.1953(2) 0.19148(13) 0.0387(6) Uani d 1 . .
C C12 0.1539(2) 0.74659(19) 0.19013(15) 0.0406(6) Uani d 1 . .
C C33 0.4114(2) -0.00413(19) 0.07486(14) 0.0369(5) Uani d 1 . .
C C38 0.4955(2) -0.00899(19) 0.11758(14) 0.0393(6) Uani d 1 . .
C C14 0.1755(2) 0.7628(2) 0.11249(15) 0.0432(6) Uani d 1 . .
C C31 0.3412(2) 0.0897(2) 0.04257(14) 0.0388(6) Uani d 1 . .
C C6 0.1395(2) 0.3760(2) 0.46934(14) 0.0389(6) Uani d 1 . .
C C29 0.3363(2) 0.35247(19) 0.02049(13) 0.0385(6) Uani d 1 . .
H H29 0.392788 0.346029 -0.015882 0.046 Uiso calc 1 . .
C C52 0.3861(2) 0.2683(2) 0.57706(14) 0.0425(6) Uani d 1 . .
C C57 0.4333(2) 0.3393(2) 0.54279(15) 0.0430(6) Uani d 1 . .
C C50 0.3630(2) 0.1919(2) 0.53911(14) 0.0407(6) Uani d 1 . .
C C30 0.2873(2) 0.26973(19) 0.01504(14) 0.0403(6) Uani d 1 . .
H H30A 0.220724 0.285068 0.040503 0.048 Uiso calc 1 . .
H H30B 0.277218 0.264110 -0.035304 0.048 Uiso calc 1 . .
C C28 0.2603(2) 0.45634(19) 0.00831(14) 0.0430(6) Uani d 1 . .
H H28A 0.296647 0.506237 -0.000681 0.052 Uiso calc 1 . .
H H28B 0.219496 0.460380 -0.033360 0.052 Uiso calc 1 . .
C C49 0.3854(2) 0.0910(2) 0.43897(15) 0.0420(6) Uani d 1 . .
H H49A 0.315113 0.110708 0.423144 0.050 Uiso calc 1 . .
H H49B 0.396950 0.030161 0.471690 0.050 Uiso calc 1 . .
C C47 0.4357(2) 0.0077(2) 0.32343(16) 0.0447(6) Uani d 1 . .
H H47A 0.493601 -0.016513 0.290148 0.054 Uiso calc 1 . .
H H47B 0.421140 -0.049776 0.350687 0.054 Uiso calc 1 . .
C C34 0.3961(2) -0.0959(2) 0.06230(17) 0.0456(6) Uani d 1 . .
H H34 0.341428 -0.094117 0.034323 0.055 Uiso calc 1 . .
C C9 0.2783(2) 0.5696(2) 0.42281(15) 0.0433(6) Uani d 1 . .
H H9A 0.342047 0.543434 0.448457 0.052 Uiso calc 1 . .
H H9B 0.231806 0.622368 0.448939 0.052 Uiso calc 1 . .
C C44 0.1967(2) 0.0912(2) 0.21363(15) 0.0433(6) Uani d 1 . .
C C19 0.2634(2) 0.7014(2) 0.07612(15) 0.0430(6) Uani d 1 . .
C C37 0.5581(2) -0.1043(2) 0.14436(16) 0.0465(6) Uani d 1 . .
H H37 0.613835 -0.108570 0.172097 0.056 Uiso calc 1 . .
C C40 0.0862(2) 0.2485(2) 0.15771(16) 0.0507(7) Uani d 1 . .
H H40 0.074005 0.316381 0.142863 0.061 Uiso calc 1 . .
C C21 0.0055(2) 0.5483(2) 0.26906(16) 0.0500(7) Uani d 1 . .
H H21 0.027877 0.524611 0.315701 0.060 Uiso calc 1 . .
C C27 0.0697(3) 0.6096(2) 0.00429(16) 0.0498(7) Uani d 1 . .
H H27A 0.027849 0.674821 0.015851 0.075 Uiso calc 1 . .
H H27B 0.029929 0.579511 -0.021464 0.075 Uiso calc 1 . .
H H27C 0.128140 0.615913 -0.025405 0.075 Uiso calc 1 . .
C C35 0.4583(2) -0.1876(2) 0.08949(18) 0.0503(7) Uani d 1 . .
H H35 0.445766 -0.246387 0.080161 0.060 Uiso calc 1 . .
C C56 0.4501(3) 0.4105(3) 0.58486(17) 0.0558(8) Uani d 1 . .
H H56 0.478737 0.458896 0.562606 0.067 Uiso calc 1 . .
C C5 0.0698(2) 0.3587(2) 0.52516(16) 0.0508(7) Uani d 1 . .
H H5 0.056342 0.397695 0.564032 0.061 Uiso calc 1 . .
C C8 0.1792(3) 0.4997(2) 0.54539(15) 0.0510(7) Uani d 1 . .
H H8A 0.197019 0.446278 0.583647 0.076 Uiso calc 1 . .
H H8B 0.110182 0.541525 0.553991 0.076 Uiso calc 1 . .
H H8C 0.225958 0.538942 0.543959 0.076 Uiso calc 1 . .
C C36 0.5394(3) -0.1909(2) 0.13075(17) 0.0514(7) Uani d 1 . .
H H36 0.582000 -0.252565 0.149631 0.062 Uiso calc 1 . .
C C53 0.3612(3) 0.2718(3) 0.65203(17) 0.0572(8) Uani d 1 . .
H H53 0.330892 0.225414 0.675595 0.069 Uiso calc 1 . .
C C2 0.1082(3) 0.2418(2) 0.41137(19) 0.0539(7) Uani d 1 . .
H H2 0.119918 0.201860 0.373136 0.065 Uiso calc 1 . .
C C18 0.2780(3) 0.7253(3) 0.00078(16) 0.0537(7) Uani d 1 . .
H H18 0.334628 0.685543 -0.023813 0.064 Uiso calc 1 . .
C C4 0.0214(3) 0.2868(3) 0.5242(2) 0.0618(9) Uani d 1 . .
H H4 -0.023576 0.276928 0.562031 0.074 Uiso calc 1 . .
C C51 0.2902(2) 0.1381(3) 0.57490(18) 0.0547(8) Uani d 1 . .
H H51A 0.230334 0.185992 0.593733 0.082 Uiso calc 1 . .
H H51B 0.323795 0.091260 0.613790 0.082 Uiso calc 1 . .
H H51C 0.269921 0.102823 0.540051 0.082 Uiso calc 1 . .
C C13 0.0494(2) 0.8001(2) 0.22090(19) 0.0543(7) Uani d 1 . .
H H13A 0.000138 0.817472 0.183404 0.081 Uiso calc 1 . .
H H13B 0.051906 0.859959 0.240006 0.081 Uiso calc 1 . .
H H13C 0.029410 0.756948 0.258935 0.081 Uiso calc 1 . .
C C17 0.2110(3) 0.8051(3) -0.03647(18) 0.0633(9) Uani d 1 . .
H H17 0.222439 0.819080 -0.085837 0.076 Uiso calc 1 . .
C C46 0.3131(3) -0.0840(2) 0.25508(18) 0.0549(8) Uani d 1 . .
H H46A 0.288793 -0.101614 0.212633 0.082 Uiso calc 1 . .
H H46B 0.280145 -0.107984 0.297433 0.082 Uiso calc 1 . .
H H46C 0.386285 -0.114111 0.257190 0.082 Uiso calc 1 . .
C C55 0.4253(3) 0.4100(3) 0.65739(18) 0.0658(10) Uani d 1 . .
H H55 0.439053 0.456522 0.683947 0.079 Uiso calc 1 . .
C C24 -0.0643(2) 0.6184(3) 0.13261(19) 0.0600(9) Uani d 1 . .
H H24 -0.089030 0.642032 0.086524 0.072 Uiso calc 1 . .
C C3 0.0399(3) 0.2292(3) 0.4666(2) 0.0630(9) Uani d 1 . .
H H3 0.005786 0.181409 0.465104 0.076 Uiso calc 1 . .
C C43 0.1199(3) 0.0485(3) 0.1994(2) 0.0666(10) Uani d 1 . .
H H43 0.130776 -0.019621 0.212685 0.080 Uiso calc 1 . .
C C15 0.1093(3) 0.8438(2) 0.07133(19) 0.0606(8) Uani d 1 . .
H H15 0.051529 0.884516 0.094237 0.073 Uiso calc 1 . .
C C22 -0.0961(3) 0.6029(3) 0.2594(2) 0.0684(10) Uani d 1 . .
H H22 -0.141280 0.615301 0.299338 0.082 Uiso calc 1 . .
C C16 0.1263(3) 0.8651(3) -0.0012(2) 0.0701(10) Uani d 1 . .
H H16 0.081091 0.919827 -0.026654 0.084 Uiso calc 1 . .
C C32 0.2496(3) 0.0849(3) 0.0041(2) 0.0599(8) Uani d 1 . .
H H32A 0.214545 0.044365 0.034003 0.090 Uiso calc 1 . .
H H32B 0.272193 0.055764 -0.040759 0.090 Uiso calc 1 . .
H H32C 0.203461 0.151345 -0.005629 0.090 Uiso calc 1 . .
C C41 0.0132(3) 0.2032(3) 0.1459(2) 0.0661(10) Uani d 1 . .
H H41 -0.047657 0.240543 0.123863 0.079 Uiso calc 1 . .
C C54 0.3801(3) 0.3410(3) 0.69121(18) 0.0684(10) Uani d 1 . .
H H54 0.362483 0.341361 0.740396 0.082 Uiso calc 1 . .
C C42 0.0301(3) 0.1023(3) 0.1669(2) 0.0790(13) Uani d 1 . .
H H42 -0.018959 0.071318 0.159012 0.095 Uiso calc 1 . .
C C23 -0.1314(3) 0.6392(4) 0.1910(2) 0.0774(12) Uani d 1 . .
H H23 -0.199653 0.677280 0.184504 0.093 Uiso calc 1 . .
O O1E 0.7184(3) 0.1473(3) 0.2304(2) 0.1102(12) Uani d 1 . .
H H1E 0.696426 0.187818 0.260536 0.165 Uiso calc 1 . .
C C2E 0.7195(4) 0.0498(4) 0.2618(3) 0.0964(15) Uani d 1 . .
H H2EA 0.649987 0.044852 0.267654 0.116 Uiso calc 1 . .
H H2EB 0.750187 0.035764 0.308862 0.116 Uiso calc 1 . .
C C3E 0.7804(5) -0.0208(5) 0.2123(4) 0.133(2) Uani d 1 . .
H H3EA 0.780131 -0.087531 0.229966 0.200 Uiso calc 1 . .
H H3EB 0.849951 -0.017689 0.208977 0.200 Uiso calc 1 . .
H H3EC 0.751412 -0.003753 0.165191 0.200 Uiso calc 1 . .
O O4E 0.8827(3) 0.1187(3) 0.6110(2) 0.1057(12) Uani d 1 . .
H H4E 0.829086 0.136427 0.588792 0.159 Uiso calc 1 . .
C C5E 0.9362(5) 0.0241(4) 0.5980(3) 0.1034(17) Uani d 1 . .
H H5EA 0.937397 0.017419 0.546563 0.124 Uiso calc 1 . .
H H5EB 0.902534 -0.022216 0.623292 0.124 Uiso calc 1 . .
C C6E 1.0416(6) -0.0011(5) 0.6222(4) 0.137(3) Uani d 1 . .
H H6EA 1.080592 -0.065847 0.607859 0.206 Uiso calc 1 . .
H H6EB 1.040758 -0.002482 0.673943 0.206 Uiso calc 1 . .
H H6EC 1.072798 0.048381 0.600560 0.206 Uiso calc 1 . .
O O7E 0.7319(3) 0.2834(4) 0.3279(2) 0.1182(13) Uani d 1 . .
H H7E 0.695981 0.316198 0.359088 0.177 Uiso calc 1 . .
C C8E 0.8232(9) 0.3177(8) 0.3102(4) 0.172(4) Uani d 1 . .
H H8EA 0.836358 0.352431 0.349068 0.207 Uiso calc 1 . .
H H8EB 0.883662 0.261511 0.301851 0.207 Uiso calc 1 . .
C C9E 0.7977(8) 0.3837(7) 0.2462(6) 0.229(6) Uani d 1 . .
H H9EA 0.778579 0.349547 0.209975 0.343 Uiso calc 1 . .
H H9EB 0.856115 0.405052 0.228575 0.343 Uiso calc 1 . .
H H9EC 0.741038 0.441138 0.256569 0.343 Uiso calc 1 . .
O O16A 0.750(2) 0.216(2) 0.4779(17) 0.112(7) Uani d 0.57(8) A 1
O O15A 0.675(2) 0.138(2) 0.5466(7) 0.115(5) Uani d 0.57(8) A 1
O O14A 0.6499(14) 0.1441(17) 0.4376(16) 0.085(6) Uani d 0.57(8) A 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Cu3 0.03783(16) 0.02639(14) 0.02544(14) -0.00612(12) -0.00082(11) 0.00037(11)
Cu1 0.03459(15) 0.02884(15) 0.02828(14) -0.00970(12) 0.00320(11) -0.00249(11)
Cu5 0.03869(16) 0.02569(14) 0.03087(15) -0.01019(12) -0.00316(12) 0.00283(11)
Cu4 0.03985(16) 0.02640(14) 0.03622(16) -0.01025(12) -0.00088(12) -0.00257(12)
Cu2 0.03940(17) 0.02984(15) 0.03844(16) -0.01114(13) 0.00403(13) -0.00033(12)
O11 0.0483(12) 0.0390(11) 0.0702(14) -0.0103(9) 0.0211(10) 0.0112(10)
N102 0.0496(13) 0.0350(12) 0.0455(13) -0.0153(10) 0.0081(10) -0.0062(10)
O12 0.0838(18) 0.0415(13) 0.115(2) -0.0322(13) -0.0159(16) -0.0004(13)
O13 0.085(2) 0.0660(17) 0.124(3) -0.0127(15) 0.0622(19) -0.0254(17)
Cu6 0.03732(16) 0.04047(17) 0.03351(16) -0.01265(13) -0.00105(12) 0.00147(13)
O14B 0.036(8) 0.096(13) 0.082(9) 0.000(7) -0.007(6) -0.025(8)
N202 0.062(2) 0.079(2) 0.083(3) -0.0231(18) -0.0093(18) -0.002(2)
O16B 0.064(8) 0.143(18) 0.073(8) -0.060(8) -0.008(5) -0.004(9)
O15B 0.15(2) 0.15(2) 0.148(16) -0.09(2) -0.043(12) 0.053(12)
O10 0.0297(8) 0.0275(8) 0.0283(8) -0.0077(7) 0.0015(7) 0.0012(6)
O2 0.0359(9) 0.0329(9) 0.0366(9) -0.0124(7) 0.0012(7) -0.0030(7)
O5 0.0433(10) 0.0277(8) 0.0313(8) -0.0088(7) 0.0034(7) -0.0034(7)
O8 0.0381(9) 0.0327(9) 0.0360(9) -0.0093(7) -0.0032(7) 0.0037(7)
O4 0.0376(9) 0.0372(9) 0.0304(8) -0.0004(7) -0.0027(7) -0.0036(7)
O1 0.0538(11) 0.0369(10) 0.0358(9) -0.0192(8) 0.0127(8) -0.0045(7)
O7 0.0506(11) 0.0328(9) 0.0392(9) -0.0189(8) -0.0118(8) 0.0062(7)
O9 0.0616(13) 0.0546(12) 0.0377(10) -0.0262(10) 0.0034(9) -0.0053(9)
O3 0.0530(12) 0.0456(11) 0.0401(10) -0.0093(9) 0.0065(9) 0.0002(8)
O2W 0.0545(12) 0.0488(11) 0.0429(10) -0.0219(10) 0.0029(9) -0.0001(9)
O6 0.0573(12) 0.0292(9) 0.0592(12) -0.0113(9) -0.0216(10) -0.0006(8)
O1W 0.0556(12) 0.0344(10) 0.0829(16) -0.0175(9) -0.0196(11) -0.0020(10)
N5 0.0442(12) 0.0274(10) 0.0369(11) -0.0106(9) -0.0014(9) 0.0014(8)
N1 0.0379(11) 0.0364(11) 0.0304(10) -0.0085(9) -0.0008(8) -0.0047(8)
N3 0.0476(12) 0.0284(10) 0.0276(10) -0.0096(9) -0.0022(9) 0.0019(8)
N4 0.0445(12) 0.0296(10) 0.0318(10) -0.0102(9) -0.0018(9) -0.0019(8)
N2 0.0427(12) 0.0299(10) 0.0402(11) -0.0108(9) -0.0006(9) -0.0033(9)
N6 0.0386(11) 0.0389(12) 0.0352(11) -0.0091(9) -0.0035(9) 0.0047(9)
C7 0.0342(12) 0.0395(13) 0.0304(12) -0.0007(10) -0.0018(10) -0.0013(10)
C20 0.0348(12) 0.0322(12) 0.0376(13) -0.0087(10) -0.0035(10) -0.0012(10)
C1 0.0375(13) 0.0342(13) 0.0379(13) -0.0081(10) 0.0022(10) 0.0060(10)
C26 0.0467(14) 0.0296(12) 0.0339(12) -0.0131(11) -0.0094(11) 0.0014(10)
C10 0.0474(15) 0.0369(13) 0.0389(13) -0.0180(12) 0.0003(11) -0.0094(11)
C25 0.0388(13) 0.0359(13) 0.0408(14) -0.0101(11) -0.0055(11) 0.0023(11)
C48 0.0390(13) 0.0315(13) 0.0437(14) -0.0030(10) -0.0060(11) 0.0058(11)
C11 0.0505(15) 0.0340(13) 0.0386(13) -0.0113(11) 0.0049(11) -0.0076(11)
C45 0.0535(16) 0.0326(13) 0.0358(13) -0.0179(12) 0.0075(11) -0.0003(10)
C39 0.0503(15) 0.0436(14) 0.0280(12) -0.0239(12) -0.0012(10) 0.0005(10)
C12 0.0466(15) 0.0285(12) 0.0482(15) -0.0128(11) -0.0018(12) -0.0053(11)
C33 0.0439(14) 0.0304(12) 0.0377(13) -0.0138(11) 0.0037(11) -0.0043(10)
C38 0.0481(15) 0.0288(12) 0.0402(13) -0.0118(11) 0.0009(11) -0.0015(10)
C14 0.0551(16) 0.0323(13) 0.0439(14) -0.0155(12) -0.0076(12) -0.0002(11)
C31 0.0459(14) 0.0348(13) 0.0374(13) -0.0143(11) 0.0007(11) -0.0053(10)
C6 0.0340(13) 0.0401(14) 0.0348(13) -0.0031(11) 0.0024(10) 0.0047(10)
C29 0.0533(15) 0.0317(12) 0.0281(12) -0.0112(11) 0.0060(11) -0.0008(10)
C52 0.0358(13) 0.0501(16) 0.0349(13) -0.0042(12) -0.0035(10) 0.0006(11)
C57 0.0344(13) 0.0557(17) 0.0366(13) -0.0095(12) -0.0043(11) -0.0042(12)
C50 0.0340(13) 0.0411(14) 0.0383(13) -0.0028(11) -0.0027(10) 0.0092(11)
C30 0.0522(15) 0.0330(13) 0.0322(12) -0.0069(11) -0.0061(11) -0.0019(10)
C28 0.0644(18) 0.0317(13) 0.0279(12) -0.0103(12) 0.0027(12) 0.0038(10)
C49 0.0467(15) 0.0374(14) 0.0398(14) -0.0125(12) -0.0030(11) 0.0065(11)
C47 0.0490(16) 0.0299(13) 0.0477(15) -0.0025(11) -0.0013(12) 0.0015(11)
C34 0.0503(16) 0.0335(14) 0.0556(17) -0.0158(12) 0.0020(13) -0.0082(12)
C9 0.0516(16) 0.0431(15) 0.0382(14) -0.0161(12) -0.0047(12) -0.0096(11)
C44 0.0564(17) 0.0439(15) 0.0365(13) -0.0267(13) -0.0019(12) 0.0008(11)
C19 0.0552(16) 0.0393(14) 0.0400(14) -0.0231(13) -0.0020(12) -0.0013(11)
C37 0.0517(16) 0.0336(14) 0.0506(16) -0.0079(12) -0.0053(13) -0.0005(12)
C40 0.0572(18) 0.0539(17) 0.0438(15) -0.0236(15) -0.0126(13) 0.0093(13)
C21 0.0418(15) 0.0606(19) 0.0417(15) -0.0098(13) 0.0017(12) 0.0031(13)
C27 0.0617(18) 0.0384(15) 0.0429(15) -0.0074(13) -0.0128(13) 0.0086(12)
C35 0.0557(17) 0.0277(13) 0.069(2) -0.0148(12) 0.0074(15) -0.0098(13)
C56 0.0505(17) 0.074(2) 0.0495(17) -0.0266(16) -0.0019(14) -0.0121(15)
C5 0.0443(16) 0.0526(17) 0.0445(15) -0.0036(13) 0.0123(12) 0.0031(13)
C8 0.0582(18) 0.0596(18) 0.0302(13) -0.0099(15) 0.0014(12) -0.0072(12)
C36 0.0610(19) 0.0292(13) 0.0584(18) -0.0076(13) 0.0040(15) -0.0004(12)
C53 0.0567(19) 0.069(2) 0.0405(16) -0.0149(16) 0.0021(13) 0.0031(15)
C2 0.0582(18) 0.0448(16) 0.0604(19) -0.0217(14) 0.0079(15) -0.0001(14)
C18 0.073(2) 0.0538(18) 0.0413(15) -0.0307(16) 0.0010(14) -0.0009(13)
C4 0.0477(17) 0.0582(19) 0.069(2) -0.0117(15) 0.0221(16) 0.0105(17)
C51 0.0522(17) 0.0555(18) 0.0509(17) -0.0146(14) 0.0097(14) 0.0066(14)
C13 0.0498(17) 0.0438(16) 0.0611(19) -0.0030(13) 0.0000(14) -0.0024(14)
C17 0.097(3) 0.059(2) 0.0423(16) -0.037(2) -0.0127(17) 0.0060(15)
C46 0.074(2) 0.0353(15) 0.0597(19) -0.0242(15) 0.0043(16) -0.0052(13)
C55 0.064(2) 0.096(3) 0.0469(18) -0.033(2) -0.0036(15) -0.0220(18)
C24 0.0399(16) 0.077(2) 0.0536(18) -0.0075(15) -0.0102(14) 0.0090(16)
C3 0.0552(19) 0.0545(19) 0.082(2) -0.0274(16) 0.0138(17) 0.0050(17)
C43 0.083(2) 0.061(2) 0.071(2) -0.048(2) -0.0197(19) 0.0135(17)
C15 0.075(2) 0.0427(17) 0.0579(19) -0.0069(15) -0.0136(17) -0.0016(14)
C22 0.0390(16) 0.094(3) 0.059(2) -0.0081(17) 0.0104(14) 0.0062(19)
C16 0.098(3) 0.0488(19) 0.058(2) -0.0136(19) -0.026(2) 0.0095(16)
C32 0.063(2) 0.0502(18) 0.072(2) -0.0216(16) -0.0243(17) -0.0025(16)
C41 0.064(2) 0.080(2) 0.063(2) -0.0385(19) -0.0237(17) 0.0187(18)
C54 0.075(2) 0.098(3) 0.0357(16) -0.030(2) 0.0003(15) -0.0097(17)
C42 0.086(3) 0.090(3) 0.083(3) -0.063(2) -0.035(2) 0.023(2)
C23 0.0350(16) 0.104(3) 0.075(2) -0.0010(18) -0.0054(16) 0.012(2)
O1E 0.116(3) 0.078(2) 0.135(3) -0.0183(19) -0.056(2) -0.004(2)
C2E 0.104(4) 0.096(4) 0.085(3) -0.030(3) -0.010(3) 0.017(3)
C3E 0.089(4) 0.109(5) 0.207(8) -0.025(3) 0.013(4) -0.054(5)
O4E 0.103(3) 0.088(2) 0.129(3) -0.0157(19) -0.024(2) -0.052(2)
C5E 0.136(5) 0.077(3) 0.095(4) -0.026(3) 0.011(3) -0.026(3)
C6E 0.137(6) 0.127(5) 0.118(5) 0.012(4) -0.026(4) -0.020(4)
O7E 0.087(2) 0.172(4) 0.103(3) -0.061(3) -0.001(2) 0.016(3)
C8E 0.264(12) 0.177(9) 0.114(6) -0.123(9) 0.026(7) -0.033(5)
C9E 0.174(10) 0.172(10) 0.340(18) -0.053(8) 0.032(11) -0.045(11)
O16A 0.134(14) 0.103(8) 0.126(13) -0.070(8) -0.008(9) -0.025(8)
O15A 0.131(10) 0.146(12) 0.061(8) -0.043(10) 0.000(5) 0.026(5)
O14A 0.079(10) 0.071(7) 0.111(12) -0.027(6) -0.028(7) -0.015(6)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O10 Cu3 O7 . . 72.48(7) ?
O5 Cu3 O10 . . 95.79(8) ?
O5 Cu3 O7 . . 91.62(7) ?
O5 Cu3 N3 . . 85.86(8) ?
O4 Cu3 O10 . . 84.02(8) ?
O4 Cu3 O5 . . 170.39(8) y
O4 Cu3 O7 . . 97.46(7) ?
O4 Cu3 N3 . . 92.84(8) ?
N3 Cu3 O10 . . 170.79(8) y
N3 Cu3 O7 . . 116.59(8) ?
O10 Cu1 O4 . . 72.34(6) ?
O2 Cu1 O10 . . 92.40(8) ?
O2 Cu1 O4 . . 93.94(7) ?
O2 Cu1 N1 . . 86.00(8) ?
O1 Cu1 O10 . . 86.17(8) ?
O1 Cu1 O2 . . 170.60(8) y
O1 Cu1 O4 . . 94.47(8) ?
O1 Cu1 N1 . . 93.42(8) ?
N1 Cu1 O10 . . 167.74(8) y
N1 Cu1 O4 . . 119.88(8) ?
O10 Cu5 O1 . . 72.65(7) ?
O8 Cu5 O10 . . 94.68(7) ?
O8 Cu5 O1 . . 93.29(7) ?
O8 Cu5 N5 . . 86.72(8) ?
O7 Cu5 O10 . . 84.42(7) ?
O7 Cu5 O8 . . 171.86(8) y
O7 Cu5 O1 . . 94.15(8) ?
O7 Cu5 N5 . . 92.98(8) ?
N5 Cu5 O10 . . 171.32(9) y
N5 Cu5 O1 . . 115.87(8) ?
O5 Cu4 O1W . . 87.84(8) ?
O5 Cu4 N4 . . 86.56(8) ?
O6 Cu4 O5 . . 173.69(9) y
O6 Cu4 O1W . . 90.97(9) ?
O6 Cu4 N4 . . 95.34(9) ?
N4 Cu4 O1W . . 171.10(9) y
O2 Cu2 O11 . . 88.40(8) ?
O2 Cu2 N2 . . 86.37(8) ?
O3 Cu2 O11 . . 90.92(9) ?
O3 Cu2 O2 . . 171.60(8) y
O3 Cu2 N2 . . 94.27(9) ?
N2 Cu2 O11 . . 174.77(9) y
N102 O11 Cu2 . . 118.74(17) ?
O12 N102 O11 . . 120.6(3) ?
O12 N102 O13 . . 123.8(3) ?
O13 N102 O11 . . 115.7(2) ?
O8 Cu6 O14B . . 91.3(6) ?
O8 Cu6 O2W . . 90.96(8) ?
O8 Cu6 N6 . . 86.12(9) ?
O9 Cu6 O14B . . 97.2(6) ?
O9 Cu6 O8 . . 171.27(9) ?
O9 Cu6 O2W . . 87.48(9) ?
O9 Cu6 N6 . . 94.66(9) ?
O2W Cu6 O14B . . 87.7(8) ?
N6 Cu6 O14B . . 97.4(8) ?
N6 Cu6 O2W . . 174.23(9) ?
N202 O14B Cu6 . . 122.5(12) ?
O16B N202 O14B . . 113.4(19) ?
O16B N202 O15B . . 117.3(19) ?
O15B N202 O14B . . 123.7(19) ?
O15A N202 O16A . . 114(2) ?
O15A N202 O14A . . 119.3(16) ?
O14A N202 O16A . . 125(2) ?
Cu3 O10 Cu1 . . 106.62(9) y
Cu5 O10 Cu3 . . 106.11(8) y
Cu5 O10 Cu1 . . 105.99(9) y
Cu2 O2 Cu1 . . 115.44(9) ?
C10 O2 Cu1 . . 107.68(14) ?
C10 O2 Cu2 . . 106.34(14) ?
Cu4 O5 Cu3 . . 119.32(8) ?
C29 O5 Cu3 . . 109.95(15) ?
C29 O5 Cu4 . . 106.28(14) ?
Cu6 O8 Cu5 . . 120.77(9) ?
C48 O8 Cu5 . . 108.23(15) ?
C48 O8 Cu6 . . 106.02(15) ?
Cu3 O4 Cu1 . . 96.50(7) y
C20 O4 Cu3 . . 124.71(16) ?
C20 O4 Cu1 . . 137.80(16) ?
Cu1 O1 Cu5 . . 93.56(7) y
C1 O1 Cu1 . . 125.52(17) ?
C1 O1 Cu5 . . 140.83(16) ?
Cu5 O7 Cu3 . . 96.20(7) y
C39 O7 Cu3 . . 138.45(17) ?
C39 O7 Cu5 . . 124.21(16) ?
C57 O9 Cu6 . . 125.90(19) ?
C19 O3 Cu2 . . 126.46(18) ?
C38 O6 Cu4 . . 125.81(18) ?
C45 N5 Cu5 . . 128.00(19) ?
C45 N5 C47 . . 121.5(2) ?
C47 N5 Cu5 . . 109.65(17) ?
C7 N1 Cu1 . . 127.63(19) ?
C7 N1 C9 . . 120.5(2) ?
C9 N1 Cu1 . . 110.30(16) ?
C26 N3 Cu3 . . 127.41(18) ?
C26 N3 C28 . . 121.8(2) ?
C28 N3 Cu3 . . 109.53(16) ?
C31 N4 Cu4 . . 127.25(19) ?
C31 N4 C30 . . 121.8(2) ?
C30 N4 Cu4 . . 110.24(16) ?
C11 N2 Cu2 . . 110.48(17) ?
C12 N2 Cu2 . . 127.20(19) ?
C12 N2 C11 . . 120.5(2) ?
C50 N6 Cu6 . . 127.0(2) ?
C50 N6 C49 . . 121.3(2) ?
C49 N6 Cu6 . . 110.64(16) ?
N1 C7 C6 . . 120.7(2) ?
N1 C7 C8 . . 120.6(3) ?
C6 C7 C8 . . 118.7(2) ?
O4 C20 C25 . . 124.2(2) ?
O4 C20 C21 . . 117.6(2) ?
C21 C20 C25 . . 118.2(2) ?
O1 C1 C6 . . 124.2(2) ?
O1 C1 C2 . . 117.4(3) ?
C2 C1 C6 . . 118.4(2) ?
N3 C26 C25 . . 121.4(2) ?
N3 C26 C27 . . 120.4(2) ?
C25 C26 C27 . . 118.2(2) ?
O2 C10 C11 . . 108.7(2) ?
O2 C10 C9 . . 108.7(2) ?
C11 C10 C9 . . 111.4(2) ?
C20 C25 C26 . . 123.0(2) ?
C24 C25 C20 . . 117.7(3) ?
C24 C25 C26 . . 119.3(3) ?
O8 C48 C49 . . 108.9(2) ?
O8 C48 C47 . . 109.7(2) ?
C47 C48 C49 . . 112.2(2) ?
N2 C11 C10 . . 108.1(2) ?
N5 C45 C44 . . 120.5(2) ?
N5 C45 C46 . . 120.9(3) ?
C44 C45 C46 . . 118.6(3) ?
O7 C39 C44 . . 123.9(3) ?
O7 C39 C40 . . 117.7(2) ?
C40 C39 C44 . . 118.4(2) ?
N2 C12 C14 . . 121.1(3) ?
N2 C12 C13 . . 119.9(3) ?
C14 C12 C13 . . 119.0(3) ?
C38 C33 C31 . . 123.9(2) ?
C34 C33 C38 . . 117.4(2) ?
C34 C33 C31 . . 118.7(2) ?
O6 C38 C33 . . 125.7(2) ?
O6 C38 C37 . . 116.1(3) ?
C37 C38 C33 . . 118.1(2) ?
C19 C14 C12 . . 122.9(3) ?
C15 C14 C12 . . 119.4(3) ?
C15 C14 C19 . . 117.7(3) ?
N4 C31 C33 . . 121.2(2) ?
N4 C31 C32 . . 120.4(3) ?
C33 C31 C32 . . 118.5(2) ?
C1 C6 C7 . . 123.7(2) ?
C5 C6 C7 . . 118.7(3) ?
C5 C6 C1 . . 117.6(3) ?
O5 C29 C30 . . 108.9(2) ?
O5 C29 C28 . . 108.9(2) ?
C28 C29 C30 . . 112.4(2) ?
C57 C52 C50 . . 123.6(2) ?
C53 C52 C57 . . 117.5(3) ?
C53 C52 C50 . . 119.0(3) ?
O9 C57 C52 . . 125.2(3) ?
O9 C57 C56 . . 116.4(3) ?
C56 C57 C52 . . 118.4(3) ?
N6 C50 C52 . . 121.0(2) ?
N6 C50 C51 . . 120.1(3) ?
C52 C50 C51 . . 118.9(3) ?
N4 C30 C29 . . 108.1(2) ?
N3 C28 C29 . . 107.97(19) ?
N6 C49 C48 . . 107.0(2) ?
N5 C47 C48 . . 107.5(2) ?
C35 C34 C33 . . 123.0(3) ?
N1 C9 C10 . . 107.8(2) ?
C39 C44 C45 . . 123.6(2) ?
C43 C44 C45 . . 119.2(3) ?
C43 C44 C39 . . 117.2(3) ?
O3 C19 C14 . . 125.6(2) ?
O3 C19 C18 . . 116.2(3) ?
C18 C19 C14 . . 118.1(3) ?
C36 C37 C38 . . 122.0(3) ?
C41 C40 C39 . . 122.0(3) ?
C22 C21 C20 . . 121.5(3) ?
C34 C35 C36 . . 118.9(3) ?
C55 C56 C57 . . 121.8(3) ?
C4 C5 C6 . . 122.4(3) ?
C37 C36 C35 . . 120.6(3) ?
C54 C53 C52 . . 122.5(3) ?
C3 C2 C1 . . 121.5(3) ?
C17 C18 C19 . . 121.6(3) ?
C5 C4 C3 . . 119.5(3) ?
C18 C17 C16 . . 120.3(3) ?
C56 C55 C54 . . 120.3(3) ?
C23 C24 C25 . . 123.1(3) ?
C2 C3 C4 . . 120.6(3) ?
C42 C43 C44 . . 123.1(3) ?
C16 C15 C14 . . 122.6(3) ?
C23 C22 C21 . . 120.6(3) ?
C15 C16 C17 . . 119.7(3) ?
C40 C41 C42 . . 120.0(3) ?
C53 C54 C55 . . 119.6(3) ?
C43 C42 C41 . . 119.3(3) ?
C24 C23 C22 . . 118.9(3) ?
O1E C2E C3E . . 106.6(5) ?
O4E C5E C6E . . 110.7(5) ?
C9E C8E O7E . . 104.3(9) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Cu3 O10 . 2.0040(17) y
Cu3 O5 . 1.9346(17) ?
Cu3 O4 . 1.8963(17) y
Cu3 O7 . 2.3648(17) y
Cu3 N3 . 1.962(2) ?
Cu1 O10 . 2.0043(19) y
Cu1 O2 . 1.9538(17) ?
Cu1 O4 . 2.3893(17) y
Cu1 O1 . 1.8767(18) y
Cu1 N1 . 1.956(2) ?
Cu5 O10 . 1.9778(19) y
Cu5 O8 . 1.9434(18) ?
Cu5 O1 . 2.4533(18) y
Cu5 O7 . 1.8894(18) ?
Cu5 N5 . 1.946(2) ?
Cu4 O5 . 1.9155(17) y
Cu4 O6 . 1.8496(19) y
Cu4 O1W . 1.961(2) y
Cu4 N4 . 1.934(2) y
Cu2 O11 . 1.986(2) y
Cu2 O2 . 1.9385(17) y
Cu2 O3 . 1.855(2) y
Cu2 N2 . 1.941(2) y
O11 N102 . 1.259(3) ?
N102 O12 . 1.206(3) ?
N102 O13 . 1.225(3) ?
Cu6 O14B . 2.45(2) y
Cu6 O8 . 1.9350(18) y
Cu6 O9 . 1.863(2) y
Cu6 O2W . 2.0273(19) y
Cu6 N6 . 1.942(2) y
O14B N202 . 1.28(3) ?
N202 O16B . 1.25(2) ?
N202 O15B . 1.26(3) ?
N202 O16A . 1.22(2) ?
N202 O15A . 1.196(14) ?
N202 O14A . 1.20(2) ?
O2 C10 . 1.438(3) ?
O5 C29 . 1.418(3) ?
O8 C48 . 1.426(3) ?
O4 C20 . 1.318(3) ?
O1 C1 . 1.318(3) ?
O7 C39 . 1.310(3) ?
O9 C57 . 1.313(3) ?
O3 C19 . 1.306(4) ?
O6 C38 . 1.316(3) ?
N5 C45 . 1.287(4) ?
N5 C47 . 1.475(3) ?
N1 C7 . 1.295(3) y
N1 C9 . 1.468(3) ?
N3 C26 . 1.286(3) y
N3 C28 . 1.474(3) ?
N4 C31 . 1.294(3) y
N4 C30 . 1.469(3) ?
N2 C11 . 1.468(3) ?
N2 C12 . 1.295(4) y
N6 C50 . 1.294(3) y
N6 C49 . 1.472(4) ?
C7 C6 . 1.463(4) ?
C7 C8 . 1.509(4) ?
C20 C25 . 1.424(4) ?
C20 C21 . 1.408(4) ?
C1 C6 . 1.427(4) ?
C1 C2 . 1.402(4) ?
C26 C25 . 1.471(4) ?
C26 C27 . 1.508(3) ?
C10 C11 . 1.514(4) ?
C10 C9 . 1.518(4) ?
C25 C24 . 1.402(4) ?
C48 C49 . 1.518(4) ?
C48 C47 . 1.513(4) ?
C45 C44 . 1.464(4) ?
C45 C46 . 1.510(4) ?
C39 C44 . 1.426(4) ?
C39 C40 . 1.405(4) ?
C12 C14 . 1.461(4) ?
C12 C13 . 1.503(4) ?
C33 C38 . 1.419(4) ?
C33 C31 . 1.466(4) ?
C33 C34 . 1.414(4) ?
C38 C37 . 1.409(4) ?
C14 C19 . 1.425(4) ?
C14 C15 . 1.403(4) ?
C31 C32 . 1.503(4) ?
C6 C5 . 1.411(4) ?
C29 C30 . 1.523(4) ?
C29 C28 . 1.515(4) ?
C52 C57 . 1.419(4) ?
C52 C50 . 1.467(4) ?
C52 C53 . 1.415(4) ?
C57 C56 . 1.414(4) ?
C50 C51 . 1.503(4) ?
C34 C35 . 1.371(4) ?
C44 C43 . 1.409(4) ?
C19 C18 . 1.419(4) ?
C37 C36 . 1.370(4) ?
C40 C41 . 1.376(4) ?
C21 C22 . 1.378(4) ?
C35 C36 . 1.374(5) ?
C56 C55 . 1.368(5) ?
C5 C4 . 1.367(5) ?
C53 C54 . 1.371(5) ?
C2 C3 . 1.373(4) ?
C18 C17 . 1.364(5) ?
C4 C3 . 1.377(5) ?
C17 C16 . 1.380(6) ?
C55 C54 . 1.376(5) ?
C24 C23 . 1.369(5) ?
C43 C42 . 1.368(6) ?
C15 C16 . 1.369(5) ?
C22 C23 . 1.378(5) ?
C41 C42 . 1.381(6) ?
O1E C2E . 1.426(6) ?
C2E C3E . 1.456(8) ?
O4E C5E . 1.348(6) ?
C5E C6E . 1.461(8) ?
O7E C8E . 1.473(9) ?
C8E C9E . 1.420(4) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O10 H10 O11 . 0.51(4) 2.43(4) 2.854(3) 142(6) yes
O10 H10 O2W . 0.51(4) 2.75(3) 2.910(3) 103(4) yes
O10 H10 O1W . 0.51(4) 2.73(4) 3.155(3) 143(6) yes
O1W H1WA O1E . 0.86 2.26 2.625(4) 105.8 yes
O1W H1WB O13 . 0.86 2.21 2.876(4) 134.7 yes
C11 H11B O4E 2_666 0.97 2.31 3.280(4) 173.8 yes
C18 H18 O13 2_665 0.93 2.54 3.328(4) 142.9 yes
O4E H4E N202 . 0.82 2.66 3.447(5) 161.4 yes
O4E H4E O16B . 0.82 2.45 3.13(2) 141.1 yes
O4E H4E O15B . 0.82 2.12 2.87(3) 150.5 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Cu3 O5 C29 C30 . . . . -83.1(2) ?
Cu3 O5 C29 C28 . . . . 39.9(2) ?
Cu3 O4 C20 C25 . . . . -25.9(3) ?
Cu3 O4 C20 C21 . . . . 155.9(2) ?
Cu3 O7 C39 C44 . . . . 167.82(19) ?
Cu3 O7 C39 C40 . . . . -10.6(4) ?
Cu3 N3 C26 C25 . . . . -13.9(4) ?
Cu3 N3 C26 C27 . . . . 165.9(2) ?
Cu3 N3 C28 C29 . . . . 30.0(3) ?
Cu1 O2 C10 C11 . . . . -78.1(2) ?
Cu1 O2 C10 C9 . . . . 43.3(2) ?
Cu1 O4 C20 C25 . . . . 168.43(19) ?
Cu1 O4 C20 C21 . . . . -9.8(4) ?
Cu1 O1 C1 C6 . . . . -23.0(4) ?
Cu1 O1 C1 C2 . . . . 159.2(2) ?
Cu1 N1 C7 C6 . . . . -15.7(3) ?
Cu1 N1 C7 C8 . . . . 164.7(2) ?
Cu1 N1 C9 C10 . . . . 28.2(3) ?
Cu5 O8 C48 C49 . . . . -82.9(2) ?
Cu5 O8 C48 C47 . . . . 40.2(2) ?
Cu5 O1 C1 C6 . . . . 152.5(2) ?
Cu5 O1 C1 C2 . . . . -25.3(4) ?
Cu5 O7 C39 C44 . . . . -27.5(4) ?
Cu5 O7 C39 C40 . . . . 154.0(2) ?
Cu5 N5 C45 C44 . . . . -13.1(4) ?
Cu5 N5 C45 C46 . . . . 168.1(2) ?
Cu5 N5 C47 C48 . . . . 29.9(3) ?
Cu4 O5 C29 C30 . . . . 47.4(2) ?
Cu4 O5 C29 C28 . . . . 170.32(17) ?
Cu4 O6 C38 C33 . . . . -1.1(4) ?
Cu4 O6 C38 C37 . . . . 179.6(2) ?
Cu4 N4 C31 C33 . . . . -10.9(4) ?
Cu4 N4 C31 C32 . . . . 168.2(2) ?
Cu4 N4 C30 C29 . . . . 17.8(2) ?
Cu2 O11 N102 O12 . . . . 17.8(4) ?
Cu2 O11 N102 O13 . . . . -162.3(3) ?
Cu2 O2 C10 C11 . . . . 46.2(2) ?
Cu2 O2 C10 C9 . . . . 167.61(17) ?
Cu2 O3 C19 C14 . . . . -11.2(4) ?
Cu2 O3 C19 C18 . . . . 170.3(2) ?
Cu2 N2 C11 C10 . . . . 22.4(2) ?
Cu2 N2 C12 C14 . . . . -17.9(4) ?
Cu2 N2 C12 C13 . . . . 161.5(2) ?
O11 Cu2 O3 C19 . . . . -175.2(2) ?
Cu6 O14B N202 O16B . . . . -108(3) ?
Cu6 O14B N202 O15B . . . . 99(4) ?
Cu6 O8 C48 C49 . . . . 48.0(2) ?
Cu6 O8 C48 C47 . . . . 171.09(17) ?
Cu6 O9 C57 C52 . . . . -13.1(4) ?
Cu6 O9 C57 C56 . . . . 168.9(2) ?
Cu6 N6 C50 C52 . . . . -16.4(4) ?
Cu6 N6 C50 C51 . . . . 162.9(2) ?
Cu6 N6 C49 C48 . . . . 22.4(2) ?
O14B Cu6 O9 C57 . . . . -88.6(8) ?
O10 Cu3 O4 Cu1 . . . . 5.17(7) ?
O10 Cu3 O4 C20 . . . . -165.2(2) ?
O10 Cu1 O1 Cu5 . . . . 8.93(7) ?
O10 Cu1 O1 C1 . . . . -173.9(2) ?
O10 Cu5 O7 Cu3 . . . . 6.37(8) ?
O10 Cu5 O7 C39 . . . . -163.5(2) ?
O2 C10 C11 N2 . . . . -45.5(3) ?
O2 C10 C9 N1 . . . . -47.3(3) ?
O5 C29 C30 N4 . . . . -43.1(3) ?
O5 C29 C28 N3 . . . . -45.9(3) ?
O8 C48 C49 N6 . . . . -46.7(3) ?
O8 C48 C47 N5 . . . . -46.5(3) ?
O4 Cu1 O1 Cu5 . . . . 80.85(7) ?
O4 Cu1 O1 C1 . . . . -102.0(2) ?
O4 C20 C25 C26 . . . . 3.0(4) ?
O4 C20 C25 C24 . . . . -176.9(3) ?
O4 C20 C21 C22 . . . . 177.1(3) ?
O1 Cu5 O7 Cu3 . . . . 78.46(7) ?
O1 Cu5 O7 C39 . . . . -91.4(2) ?
O1 C1 C6 C7 . . . . 4.7(4) ?
O1 C1 C6 C5 . . . . -175.2(2) ?
O1 C1 C2 C3 . . . . 176.2(3) ?
O7 Cu3 O4 Cu1 . . . . 76.57(7) ?
O7 Cu3 O4 C20 . . . . -93.8(2) ?
O7 C39 C44 C45 . . . . 4.1(4) ?
O7 C39 C44 C43 . . . . -177.9(3) ?
O7 C39 C40 C41 . . . . 178.9(3) ?
O9 C57 C56 C55 . . . . -179.6(3) ?
O3 C19 C18 C17 . . . . 179.1(3) ?
O2W Cu6 O9 C57 . . . . -175.9(2) ?
O6 C38 C37 C36 . . . . 178.8(3) ?
O1W Cu4 O6 C38 . . . . -177.0(2) ?
N5 Cu5 O7 Cu3 . . . . -165.33(8) ?
N5 Cu5 O7 C39 . . . . 24.8(2) ?
N5 C45 C44 C39 . . . . 17.2(4) ?
N5 C45 C44 C43 . . . . -160.8(3) ?
N1 Cu1 O1 Cu5 . . . . -158.80(8) ?
N1 Cu1 O1 C1 . . . . 18.4(2) ?
N1 C7 C6 C1 . . . . 15.4(4) ?
N1 C7 C6 C5 . . . . -164.7(2) ?
N3 Cu3 O4 Cu1 . . . . -166.14(8) ?
N3 Cu3 O4 C20 . . . . 23.5(2) ?
N3 C26 C25 C20 . . . . 17.9(4) ?
N3 C26 C25 C24 . . . . -162.2(3) ?
N4 Cu4 O6 C38 . . . . -3.3(2) ?
N2 Cu2 O3 C19 . . . . 5.5(2) ?
N2 C12 C14 C19 . . . . 12.4(4) ?
N2 C12 C14 C15 . . . . -165.9(3) ?
N6 Cu6 O9 C57 . . . . 9.4(2) ?
C7 N1 C9 C10 . . . . -165.0(2) ?
C7 C6 C5 C4 . . . . 178.6(3) ?
C20 C25 C24 C23 . . . . -0.1(5) ?
C20 C21 C22 C23 . . . . -0.2(6) ?
C1 C6 C5 C4 . . . . -1.5(4) ?
C1 C2 C3 C4 . . . . -0.4(5) ?
C26 N3 C28 C29 . . . . -162.2(2) ?
C26 C25 C24 C23 . . . . 180.0(4) ?
C25 C20 C21 C22 . . . . -1.2(5) ?
C25 C24 C23 C22 . . . . -1.3(7) ?
C11 N2 C12 C14 . . . . 179.0(2) ?
C11 N2 C12 C13 . . . . -1.6(4) ?
C11 C10 C9 N1 . . . . 72.4(3) ?
C45 N5 C47 C48 . . . . -159.8(2) ?
C45 C44 C43 C42 . . . . 177.0(4) ?
C39 C44 C43 C42 . . . . -1.1(6) ?
C39 C40 C41 C42 . . . . -0.6(6) ?
C12 N2 C11 C10 . . . . -171.9(2) ?
C12 C14 C19 O3 . . . . 2.8(4) ?
C12 C14 C19 C18 . . . . -178.7(3) ?
C12 C14 C15 C16 . . . . 178.2(3) ?
C33 C38 C37 C36 . . . . -0.5(4) ?
C33 C34 C35 C36 . . . . -0.1(5) ?
C38 C33 C31 N4 . . . . 4.6(4) ?
C38 C33 C31 C32 . . . . -174.6(3) ?
C38 C33 C34 C35 . . . . 0.1(4) ?
C38 C37 C36 C35 . . . . 0.5(5) ?
C14 C19 C18 C17 . . . . 0.5(4) ?
C14 C15 C16 C17 . . . . 0.6(6) ?
C31 N4 C30 C29 . . . . -171.1(2) ?
C31 C33 C38 O6 . . . . 1.8(4) ?
C31 C33 C38 C37 . . . . -178.9(3) ?
C31 C33 C34 C35 . . . . 179.3(3) ?
C6 C1 C2 C3 . . . . -1.8(5) ?
C6 C5 C4 C3 . . . . -0.6(5) ?
C52 C57 C56 C55 . . . . 2.2(5) ?
C52 C53 C54 C55 . . . . -0.3(6) ?
C57 C52 C50 N6 . . . . 14.5(4) ?
C57 C52 C50 C51 . . . . -164.8(3) ?
C57 C52 C53 C54 . . . . 0.7(5) ?
C57 C56 C55 C54 . . . . -1.9(6) ?
C50 N6 C49 C48 . . . . -168.5(2) ?
C50 C52 C57 O9 . . . . 0.9(4) ?
C50 C52 C57 C56 . . . . 178.9(3) ?
C50 C52 C53 C54 . . . . -179.8(3) ?
C30 N4 C31 C33 . . . . 179.5(2) ?
C30 N4 C31 C32 . . . . -1.4(4) ?
C30 C29 C28 N3 . . . . 74.9(3) ?
C28 N3 C26 C25 . . . . -179.5(2) ?
C28 N3 C26 C27 . . . . 0.4(4) ?
C28 C29 C30 N4 . . . . -163.9(2) ?
C49 N6 C50 C52 . . . . 176.4(2) ?
C49 N6 C50 C51 . . . . -4.3(4) ?
C49 C48 C47 N5 . . . . 74.7(3) ?
C47 N5 C45 C44 . . . . 178.6(2) ?
C47 N5 C45 C46 . . . . -0.3(4) ?
C47 C48 C49 N6 . . . . -168.3(2) ?
C34 C33 C38 O6 . . . . -179.1(3) ?
C34 C33 C38 C37 . . . . 0.2(4) ?
C34 C33 C31 N4 . . . . -174.5(3) ?
C34 C33 C31 C32 . . . . 6.3(4) ?
C34 C35 C36 C37 . . . . -0.2(5) ?
C9 N1 C7 C6 . . . . 180.0(2) ?
C9 N1 C7 C8 . . . . 0.4(4) ?
C9 C10 C11 N2 . . . . -165.2(2) ?
C44 C39 C40 C41 . . . . 0.3(5) ?
C44 C43 C42 C41 . . . . 0.8(7) ?
C19 C14 C15 C16 . . . . -0.1(5) ?
C19 C18 C17 C16 . . . . 0.0(5) ?
C40 C39 C44 C45 . . . . -177.4(3) ?
C40 C39 C44 C43 . . . . 0.5(4) ?
C40 C41 C42 C43 . . . . 0.1(7) ?
C21 C20 C25 C26 . . . . -178.8(3) ?
C21 C20 C25 C24 . . . . 1.3(4) ?
C21 C22 C23 C24 . . . . 1.4(7) ?
C27 C26 C25 C20 . . . . -162.0(3) ?
C27 C26 C25 C24 . . . . 18.0(4) ?
C56 C55 C54 C53 . . . . 0.8(6) ?
C5 C4 C3 C2 . . . . 1.6(5) ?
C8 C7 C6 C1 . . . . -165.0(3) ?
C8 C7 C6 C5 . . . . 14.9(4) ?
C53 C52 C57 O9 . . . . -179.6(3) ?
C53 C52 C57 C56 . . . . -1.6(4) ?
C53 C52 C50 N6 . . . . -165.0(3) ?
C53 C52 C50 C51 . . . . 15.7(4) ?
C2 C1 C6 C7 . . . . -177.5(3) ?
C2 C1 C6 C5 . . . . 2.6(4) ?
C18 C17 C16 C15 . . . . -0.5(6) ?
C13 C12 C14 C19 . . . . -167.0(3) ?
C13 C12 C14 C15 . . . . 14.7(4) ?
C46 C45 C44 C39 . . . . -164.0(3) ?
C46 C45 C44 C43 . . . . 18.1(4) ?
C15 C14 C19 O3 . . . . -178.9(3) ?
C15 C14 C19 C18 . . . . -0.4(4) ?
_cod_database_fobs_code 2243852