#------------------------------------------------------------------------------ #$Date: 2021-06-26 08:54:34 +0300 (Sat, 26 Jun 2021) $ #$Revision: 266718 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243858.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243858 loop_ _publ_author_name 'Mehmood, Tahir' 'Bhosale, Rajesh S.' 'Reddy, J. Prakasha' _publ_section_title ; Bis(2-methylpyridinium) tetrachloridocuprate(II): synthesis, structure and Hirshfeld surface analysis ; _journal_coeditor_code DJ2020 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 726 _journal_page_last 729 _journal_paper_doi 10.1107/S2056989021006277 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac '(C6 H8 N)2 [Cu Cl4]' _chemical_formula_moiety '2(C6 H8 N +), Cl4 Cu 2-' _chemical_formula_sum 'C12 H16 Cl4 Cu N2' _chemical_formula_weight 393.62 _chemical_name_common 'bis(2-methylpyridinium) tetrachlorocuprate(II)' _chemical_name_systematic ; Bis(2-methylpyridinium) tetrachloridocuprate(II) ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2yc' _space_group_name_H-M_alt 'I 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 99.205(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.2354(8) _cell_length_b 8.3683(3) _cell_length_c 12.8372(6) _cell_measurement_reflns_used 5462 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 32.5119 _cell_measurement_theta_min 2.9112 _cell_volume 1615.59(13) _computing_cell_refinement ; CrysAlisPro (Agilent, 2014) ; _computing_data_collection ; CrysAlisPro (Agilent, 2014) ; _computing_data_reduction ; CrysAlisPro (Agilent, 2014) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; ShelXL (Sheldrick, 2015) ; _computing_structure_solution ; Superflip (Palatinus & Chapuis, 2007; Palatinus & van der Lee, 2008; Palatinus et al., 2012) ; _diffrn_ambient_temperature 120(2) _diffrn_detector_area_resol_mean 16.1511 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.955 _diffrn_measurement_device_type 'Agilent Xcalibur, Sapphire3' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0706 _diffrn_reflns_av_unetI/netI 0.0383 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 24556 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.586 _diffrn_reflns_theta_min 2.917 _exptl_absorpt_coefficient_mu 2.000 _exptl_absorpt_correction_T_max 0.965 _exptl_absorpt_correction_T_min 0.848 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; (CrysAlisPro; Agilent, 2014) ; _exptl_crystal_colour 'pale yellow' _exptl_crystal_density_diffrn 1.618 _exptl_crystal_description blocks _exptl_crystal_F_000 796 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.27 _exptl_crystal_size_min 0.25 _refine_diff_density_max 0.580 _refine_diff_density_min -0.582 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.078 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 88 _refine_ls_number_reflns 2821 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.078 _refine_ls_R_factor_all 0.0492 _refine_ls_R_factor_gt 0.0355 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0308P)^2^+1.4147P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0742 _refine_ls_wR_factor_ref 0.0809 _reflns_number_gt 2324 _reflns_number_total 2821 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL CF solution in I2/c jpr12-t.res created by SHELXL-2018/3 at 19:04:29 on 16-Dec-2020 CELL 0.71073 15.235404 8.368287 12.837238 90 99.2051 90 ZERR 8 0.000772 0.000332 0.000639 0 0.0049 0 LATT 2 SYMM -X,+Y,0.5-Z SFAC C H Cl Cu N UNIT 48 64 16 4 8 L.S. 6 PLAN 10 SIZE 0.25 0.28 0.32 TEMP -153(2) LIST 4 BOND $H CONF HTAB fmap 2 acta REM REM REM WGHT 0.030800 1.414700 FVAR 2.35425 CU1 4 0.500000 0.222610 0.250000 10.50000 0.02142 0.01465 = 0.01929 0.00000 0.00510 0.00000 CL1 3 0.389531 0.105904 0.138631 11.00000 0.02533 0.01737 = 0.02265 -0.00185 0.00223 -0.00165 CL2 3 0.418977 0.320333 0.367393 11.00000 0.02761 0.01724 = 0.02464 -0.00340 0.00935 0.00035 N1 5 0.685012 0.012939 0.635209 11.00000 0.02683 0.01544 = 0.02350 0.00108 0.00543 -0.00234 AFIX 43 H1 2 0.642734 -0.054296 0.645210 11.00000 -1.20000 AFIX 0 C2 1 0.664344 0.169703 0.625425 11.00000 0.02637 0.01723 = 0.01548 0.00004 0.00333 -0.00038 C3 1 0.731756 0.274653 0.610762 11.00000 0.03109 0.01499 = 0.02034 0.00045 0.00398 -0.00300 AFIX 43 H3 2 0.720458 0.386273 0.605979 11.00000 -1.20000 AFIX 0 C4 1 0.833543 0.053264 0.612760 11.00000 0.02506 0.02655 = 0.02674 -0.00103 0.00397 0.00160 AFIX 43 H4 2 0.890816 0.012622 0.607122 11.00000 -1.20000 AFIX 0 C5 1 0.815483 0.216493 0.603112 11.00000 0.02807 0.02206 = 0.02439 -0.00082 0.00558 -0.00689 AFIX 43 H5 2 0.861102 0.288380 0.591178 11.00000 -1.20000 AFIX 0 C6 1 0.766319 -0.046756 0.630600 11.00000 0.03262 0.01720 = 0.02653 0.00156 0.00476 0.00310 AFIX 43 H6 2 0.777088 -0.158092 0.639704 11.00000 -1.20000 AFIX 0 C7 1 0.570386 0.217398 0.628514 11.00000 0.02635 0.02427 = 0.02765 0.00038 0.00609 0.00176 AFIX 137 H7A 2 0.536395 0.214343 0.556960 11.00000 -1.50000 H7B 2 0.569141 0.325976 0.656845 11.00000 -1.50000 H7C 2 0.543936 0.143189 0.673767 11.00000 -1.50000 AFIX 0 HKLF 4 REM CF solution in I2/c REM wR2 = 0.0809, GooF = S = 1.078, Restrained GooF = 1.078 for all data REM R1 = 0.0355 for 2324 Fo > 4sig(Fo) and 0.0492 for all 2821 data REM 88 parameters refined using 0 restraints END WGHT 0.0308 1.4147 REM Instructions for potential hydrogen bonds EQIV $2 -x+1, -y, -z+1 HTAB N1 Cl1_$2 HTAB N1 Cl2_$2 EQIV $3 x+1/2, y-1/2, z+1/2 HTAB C6 Cl1_$3 HTAB C7 Cl2 EQIV $4 -x+1, -y+1, -z+1 HTAB C7 Cl2_$4 REM Highest difference peak 0.580, deepest hole -0.582, 1-sigma level 0.097 Q1 1 0.4461 0.2270 0.2486 11.00000 0.05 0.58 Q2 1 0.4512 0.1727 0.1814 11.00000 0.05 0.49 Q3 1 0.7911 0.0186 0.6153 11.00000 0.05 0.48 Q4 1 0.3325 0.0971 0.1412 11.00000 0.05 0.44 Q5 1 0.7273 -0.0125 0.6324 11.00000 0.05 0.43 Q6 1 0.4253 0.2420 0.3687 11.00000 0.05 0.43 Q7 1 0.7741 0.2340 0.6129 11.00000 0.05 0.42 Q8 1 0.6916 -0.1945 0.7411 11.00000 0.05 0.42 Q9 1 0.4728 0.3020 0.3537 11.00000 0.05 0.42 Q10 1 0.4009 0.2673 0.2508 11.00000 0.05 0.41 REM The information below was added by Olex2. REM REM R1 = 0.0355 for 2324 Fo > 4sig(Fo) and 0.0492 for all 25468 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.58, deepest hole -0.58 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0492 REM R1_gt = 0.0355 REM wR_ref = 0.0809 REM GOOF = 1.078 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 25468 REM Reflections_gt = 2324 REM Parameters = n/a REM Hole = -0.58 REM Peak = 0.58 REM Flack = n/a ; _cod_data_source_file dj2020sup1.cif _cod_data_source_block I _cod_original_cell_volume 1615.60(13) _cod_original_sg_symbol_H-M 'I 2/c' _cod_database_code 2243858 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.567 _shelx_estimated_absorpt_t_max 0.635 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, -y+1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu1 0.500000 0.22261(4) 0.250000 0.01825(9) Uani d 1 . . Cl Cl1 0.38953(3) 0.10590(5) 0.13863(3) 0.02196(11) Uani d 1 . . Cl Cl2 0.41898(3) 0.32033(5) 0.36739(4) 0.02260(11) Uani d 1 . . N N1 0.68501(11) 0.01294(19) 0.63521(12) 0.0218(3) Uani d 1 . . H H1 0.642734 -0.054296 0.645210 0.026 Uiso calc 1 . . C C2 0.66434(12) 0.1697(2) 0.62543(13) 0.0197(3) Uani d 1 . . C C3 0.73176(13) 0.2747(2) 0.61076(14) 0.0222(4) Uani d 1 . . H H3 0.720458 0.386273 0.605979 0.027 Uiso calc 1 . . C C4 0.83354(14) 0.0533(2) 0.61276(16) 0.0261(4) Uani d 1 . . H H4 0.890816 0.012622 0.607122 0.031 Uiso calc 1 . . C C5 0.81548(14) 0.2165(2) 0.60311(15) 0.0247(4) Uani d 1 . . H H5 0.861102 0.288380 0.591178 0.030 Uiso calc 1 . . C C6 0.76632(14) -0.0468(2) 0.63060(15) 0.0254(4) Uani d 1 . . H H6 0.777088 -0.158092 0.639704 0.031 Uiso calc 1 . . C C7 0.57039(13) 0.2174(2) 0.62851(16) 0.0259(4) Uani d 1 . . H H7A 0.536395 0.214343 0.556960 0.039 Uiso calc 1 . . H H7B 0.569141 0.325976 0.656845 0.039 Uiso calc 1 . . H H7C 0.543936 0.143189 0.673767 0.039 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu1 0.02142(16) 0.01465(15) 0.01929(16) 0.000 0.00510(12) 0.000 Cl1 0.0253(2) 0.0174(2) 0.0226(2) -0.00165(16) 0.00223(17) -0.00185(15) Cl2 0.0276(2) 0.0172(2) 0.0246(2) 0.00035(16) 0.00935(17) -0.00340(16) N1 0.0268(8) 0.0154(7) 0.0235(7) -0.0023(6) 0.0054(6) 0.0011(6) C2 0.0264(9) 0.0172(8) 0.0155(8) -0.0004(7) 0.0033(7) 0.0000(6) C3 0.0311(10) 0.0150(8) 0.0203(8) -0.0030(7) 0.0040(7) 0.0004(6) C4 0.0251(10) 0.0266(10) 0.0267(9) 0.0016(8) 0.0040(8) -0.0010(8) C5 0.0281(10) 0.0221(9) 0.0244(9) -0.0069(7) 0.0056(8) -0.0008(7) C6 0.0326(10) 0.0172(9) 0.0265(10) 0.0031(7) 0.0048(8) 0.0016(7) C7 0.0263(10) 0.0243(10) 0.0276(10) 0.0018(7) 0.0061(8) 0.0004(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Cl1 Cu1 Cl1 . 2_655 128.54(3) ? Cl2 Cu1 Cl1 2_655 . 99.614(17) ? Cl2 Cu1 Cl1 2_655 2_655 98.550(17) ? Cl2 Cu1 Cl1 . . 98.549(17) ? Cl2 Cu1 Cl1 . 2_655 99.616(17) ? Cl2 Cu1 Cl2 2_655 . 137.36(3) ? C2 N1 H1 . . 118.0 ? C6 N1 H1 . . 118.0 ? C6 N1 C2 . . 124.00(17) ? N1 C2 C3 . . 117.46(17) ? N1 C2 C7 . . 117.88(17) ? C3 C2 C7 . . 124.64(17) ? C2 C3 H3 . . 120.1 ? C5 C3 C2 . . 119.88(17) ? C5 C3 H3 . . 120.1 ? C5 C4 H4 . . 121.0 ? C6 C4 H4 . . 121.0 ? C6 C4 C5 . . 118.10(19) ? C3 C5 C4 . . 120.61(18) ? C3 C5 H5 . . 119.7 ? C4 C5 H5 . . 119.7 ? N1 C6 C4 . . 119.91(18) ? N1 C6 H6 . . 120.0 ? C4 C6 H6 . . 120.0 ? C2 C7 H7A . . 109.5 ? C2 C7 H7B . . 109.5 ? C2 C7 H7C . . 109.5 ? H7A C7 H7B . . 109.5 ? H7A C7 H7C . . 109.5 ? H7B C7 H7C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cu1 Cl1 2_655 2.2496(5) ? Cu1 Cl1 . 2.2496(5) ? Cu1 Cl2 . 2.2492(4) ? Cu1 Cl2 2_655 2.2492(4) ? N1 H1 . 0.8800 ? N1 C2 . 1.350(2) ? N1 C6 . 1.346(2) ? C2 C3 . 1.387(3) ? C2 C7 . 1.493(3) ? C3 H3 . 0.9500 ? C3 C5 . 1.383(3) ? C4 H4 . 0.9500 ? C4 C5 . 1.395(3) ? C4 C6 . 1.370(3) ? C5 H5 . 0.9500 ? C6 H6 . 0.9500 ? C7 H7A . 0.9800 ? C7 H7B . 0.9800 ? C7 H7C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 Cl1 5_656 0.88 2.93 3.4297(16) 118.1 yes N1 H1 Cl2 5_656 0.88 2.41 3.2050(16) 150.1 yes C6 H6 Cl1 3_545 0.95 2.62 3.453(2) 147.2 yes C7 H7A Cl2 . 0.98 2.92 3.850(2) 159.3 yes C7 H7B Cl2 5_666 0.98 2.98 3.872(2) 151.1 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N1 C2 C3 C5 . . . . 2.2(3) ? C2 N1 C6 C4 . . . . -1.5(3) ? C2 C3 C5 C4 . . . . -1.7(3) ? C5 C4 C6 N1 . . . . 2.0(3) ? C6 N1 C2 C3 . . . . -0.6(3) ? C6 N1 C2 C7 . . . . 177.92(17) ? C6 C4 C5 C3 . . . . -0.4(3) ? C7 C2 C3 C5 . . . . -176.27(18) ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 -2 96469.3 1740.57 0 0 2 80714.1 2050.65 0 0 2 93959.3 2061.86 0 0 -2 82172 1999.99 0 0 -2 85544.1 2042.06 0 0 -2 82499.4 1870.64 0 0 4 610673 11360.1 0 0 -4 674417 11635.5 0 0 4 698542 11585.1 0 0 4 640716 11590.4 0 0 4 737053 11012.9 0 0 -4 665628 10870.6 0 0 4 699884 11738.1 0 0 -4 690336 11785.2 0 0 6 9914.94 675.612 0 0 6 9411.58 840.753 0 0 -6 7479.76 831.376 0 0 6 8900.47 758.155 0 0 -6 8629.18 848.353 0 0 6 8997.28 871.779 0 0 8 439257 9548.97 0 0 8 452586 8881.08 0 0 8 444009 9287.52 0 0 8 448974 8457.48 0 0 -8 446209 9491.98 0 0 -8 444097 9820.77 0 0 -10 60450.3 3106.71 0 0 10 62583.3 2555.26 0 0 10 53338.4 2179 0 0 10 60828.4 3170.39 0 0 10 58162.2 2915.71 0 0 10 60797.5 2803.37 0 0 -10 63554.5 2996.2 0 0 12 17941.9 1616.49 0 0 -12 17643.1 1830.18 0 0 12 17818.2 1678.79 0 0 -12 18628.1 1800.66 0 0 12 18420.2 1919.66 0 0 12 17652.1 1291.36 0 0 12 18335.7 1434.18 0 0 14 305.927 324.303 0 0 -14 181.513 325.094 0 0 14 884.143 548.469 0 0 14 464.529 283.96 0 0 -14 104.025 247.937 0 0 14 272.211 352.976 0 0 16 21960.7 2223.99 0 0 16 23361.2 2588.93 0 0 -16 28157.6 2549.31 0 0 -16 31515 2582.08 0 0 -16 20926.5 2315.03 0 0 18 13278.5 2170.47 0 0 -18 12268.9 1839.85 0 0 18 12262.1 1821.91 0 -1 1 121537 2208.31 0 -1 -3 102843 2105.4 0 1 3 97931.8 2497.95 0 -1 3 90358.2 2323.99 0 1 3 83680.7 2151.75 0 1 -3 76540.2 1966.6 0 -1 -3 88704 2197.55 0 1 -3 89471.8 2119.45 0 -1 -3 88694.4 2106.03 0 1 3 97593.9 2414.3 0 1 3 88798.5 2259.14 0 1 3 82587 2023.67 0 -1 -3 82120.3 1917.81 0 -1 -3 88624.5 2472.6 0 -1 -3 93569 2204.38 0 -1 3 89392.8 2572.79 0 1 -3 87453.4 2491.08 0 1 3 90758.9 2090.81 0 1 3 96566.4 2009.29 0 1 3 94499.1 2140.14 0 1 3 96640.5 1980.85 0 1 5 1048.52 207.693 0 1 5 883.878 263.234 0 1 -5 503.792 122.532 0 1 5 502.361 180.896 0 -1 5 913.579 192.407 0 1 5 779.849 208.279 0 1 5 1176.48 349.726 0 -1 5 674.686 313.778 0 1 -5 778.455 295.509 0 -1 5 925.189 298.38 0 1 5 958.251 258.334 0 -1 -5 445.166 273.195 0 -1 -5 461.749 92.3836 0 -1 -5 799.772 272.693 0 1 -5 965.288 272.353 0 1 5 741.432 286.285 0 -1 5 1000.72 360.678 0 1 5 941.142 160.869 0 1 -7 9246.2 875.483 0 1 7 10466.7 1041.51 0 1 7 10055.2 919.788 0 1 7 10451.3 1064.63 0 1 7 10143.2 836.404 0 -1 -7 10602.3 1023.1 0 1 7 9296.24 851.974 0 -1 7 10905.3 737.766 0 1 -7 9915.07 1070.95 0 1 7 11210.8 787.342 0 -1 7 11033.2 1089.59 0 1 7 9423.96 786.493 0 -1 7 9921.41 921.097 0 1 7 10904 472.426 0 -1 7 10242.6 1037.34 0 -1 -7 11253.4 1094.65 0 -1 7 8854.99 963.852 0 -1 -9 97913.4 3781.13 0 1 9 99615.9 3314.7 0 1 -9 100765 4050.42 0 1 9 95203.9 3359.94 0 1 9 102416 3974.79 0 1 9 97830.5 2985.98 0 -1 9 96316.4 3673.22 0 1 -9 102117 3560.92 0 -1 9 94759.7 2835.99 0 -1 -9 101233 3895.58 0 -1 9 100374 3917.83 0 1 9 101346 3614.82 0 1 9 96166.6 3833.97 0 -1 9 103822 3577.01 0 1 -11 32072.5 2390.48 0 1 11 26908.1 1912.94 0 1 -11 32965.6 2131.1 0 1 11 29194.6 2275.79 0 -1 11 29155.4 2226.52 0 -1 11 29984.7 2121.07 0 -1 -11 35328.7 2396.19 0 1 11 32421.8 1956.96 0 1 11 27331.6 1603.88 0 -1 11 30026.2 1593.19 0 -1 -11 32651.8 2341.16 0 -1 11 30468.1 1969.13 0 1 11 29265.1 1715.75 0 -1 -13 1331.16 555.893 0 -1 13 1511.91 589.071 0 -1 13 853.577 423.727 0 -1 13 1330.17 450.384 0 1 13 1612.87 579.679 0 1 13 1182.45 659.471 0 1 13 839.255 333.258 0 -1 -13 1894.53 649 0 1 -13 981.609 504.418 0 1 -13 1472.62 579.6 0 -1 13 1942.46 751.234 0 1 15 431.805 401.05 0 -1 -15 168.436 415.077 0 -1 15 385.454 347.048 0 1 15 103.172 398.618 0 -1 -15 468.173 426.904 0 -1 15 -1.01339 497.897 0 1 -15 749.136 428.321 0 -1 15 101.101 259.247 0 1 -15 291.58 376.029 0 -1 -15 1192.67 423.443 0 1 -17 23679.1 2224.37 0 1 -17 19570.2 2324.76 0 -1 17 13545 1894.41 0 1 17 14155.9 1768.77 0 -1 -17 17178.3 2041.26 0 -1 -17 15229.3 2074.53 0 1 -17 12775 1782.63 0 -1 -17 21360.8 2244.53 0 -1 17 14124.7 2117.9 0 1 17 12874.1 2008.14 0 1 -19 6835.18 1425.32 0 2 0 177501 3297.79 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