#------------------------------------------------------------------------------ #$Date: 2021-07-01 08:11:34 +0300 (Thu, 01 Jul 2021) $ #$Revision: 266841 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243860.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243860 loop_ _publ_author_name 'Atio\(glu, Zeliha' 'Akkurt, Mehmet' 'Mammadova, Gunay Z.' 'Huseynov, Fatali E.' 'Hajiyeva, Sevinj R.' 'Shamilov, Nazim T.' 'Bhattarai, Ajaya' _publ_section_title ; Crystal structure and Hirshfeld surface analysis of dimethyl 5-[2-(2,4,6-trioxo-1,3-diazinan-5-ylidene)hydrazin-1-yl]benzene-1,3-dicarboxylate 0.224-hydrate ; _journal_coeditor_code YK2153 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 759 _journal_page_last 764 _journal_paper_doi 10.1107/S2056989021006563 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac 'C14 H12 N4 O7, 0.224H2 O' _chemical_formula_moiety 'C14 H12 N4 O7, 0.224(H2O)' _chemical_formula_sum 'C14 H12.448 N4 O7.224' _chemical_formula_weight 351.86 _chemical_name_systematic ;Dimethyl 5-[2-(2,4,6-trioxo-1,3-diazinan-5-ylidene)hydrazin-1-yl]benzene-1,3-dicarboxylate 0.224-hydrate ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 113.133(2) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 24.2097(11) _cell_length_b 12.6311(6) _cell_length_c 10.4022(5) _cell_measurement_reflns_used 9840 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 26.37 _cell_measurement_theta_min 3.23 _cell_volume 2925.2(2) _computing_cell_refinement ; SAINT (Bruker, 2007) ; _computing_data_collection ; APEX2 (Bruker, 2007) ; _computing_data_reduction ; SAINT (Bruker, 2007) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.982 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0169 _diffrn_reflns_av_unetI/netI 0.0078 _diffrn_reflns_limit_h_max 30 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 34832 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.378 _diffrn_reflns_theta_min 3.226 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.132 _exptl_absorpt_correction_type none _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.598 _exptl_crystal_description block _exptl_crystal_F_000 1454 _exptl_crystal_size_max 0.340 _exptl_crystal_size_mid 0.320 _exptl_crystal_size_min 0.270 _refine_diff_density_max 0.286 _refine_diff_density_min -0.210 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 241 _refine_ls_number_reflns 2944 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0371 _refine_ls_R_factor_gt 0.0340 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0586P)^2^+2.1077P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0981 _refine_ls_wR_factor_ref 0.1022 _reflns_number_gt 2699 _reflns_number_total 2944 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yk2153sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 2243860 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.957 _shelx_estimated_absorpt_t_max 0.965 _shelx_hkl_file ; 6 0 0 141.49 2.60 6 0 0 130.09 2.60 -6 0 0 138.09 2.60 6 0 0 137.09 2.60 8 0 0 2361.16 35.40 10 0 0 651.93 10.30 -10 0 0 647.44 10.30 10 0 0 642.44 10.40 10 0 0 655.23 10.30 -10 0 0 652.83 10.20 -12 0 0 402.76 6.70 12 0 0 396.76 6.60 12 0 0 393.46 6.60 12 0 0 376.56 6.70 -12 0 0 392.46 6.60 14 0 0 693.93 11.10 -14 0 0 697.23 11.10 -14 0 0 686.33 11.10 14 0 0 690.73 11.10 14 0 0 689.33 11.30 16 0 0 34.10 2.40 -16 0 0 36.20 2.20 16 0 0 39.10 2.20 16 0 0 35.10 2.20 -16 0 0 38.40 2.20 -18 0 0 1397.76 21.60 -18 0 0 1197.68 19.80 18 0 0 1324.17 21.50 18 0 0 1199.08 20.00 18 0 0 1218.28 19.80 -20 0 0 121.29 3.70 -20 0 0 124.99 3.60 20 0 0 119.19 4.00 20 0 0 123.59 3.70 20 0 0 126.99 3.70 22 0 0 215.68 5.00 22 0 0 212.58 5.10 -22 0 0 217.38 5.00 22 0 0 212.98 5.30 -22 0 0 216.88 5.10 24 0 0 319.37 6.60 24 0 0 321.37 6.90 -24 0 0 320.77 6.70 -24 0 0 324.47 6.60 24 0 0 322.97 6.70 26 0 0 192.18 5.50 -26 0 0 197.88 5.10 26 0 0 183.78 5.10 26 0 0 194.08 5.30 -26 0 0 190.18 5.20 5 -1 0 29.70 1.00 -5 -1 0 27.50 1.50 5 -1 0 30.80 1.00 -5 -1 0 29.10 1.30 5 1 0 28.80 1.40 5 1 0 28.80 1.30 5 1 0 29.60 1.30 -7 -1 0 799.92 12.00 7 -1 0 788.72 11.80 -7 -1 0 793.02 12.00 -7 -1 0 762.82 12.10 7 1 0 806.22 12.30 7 1 0 800.82 12.00 7 1 0 777.22 12.10 -7 1 0 689.03 11.80 9 -1 0 2452.35 37.10 9 1 0 2512.55 37.30 11 -1 0 214.48 3.90 11 -1 0 206.48 4.10 -11 -1 0 209.58 4.10 11 -1 0 210.38 3.90 -11 -1 0 215.38 4.10 11 1 0 213.28 4.10 -11 1 0 215.48 3.90 11 1 0 213.08 4.10 11 1 0 206.98 4.20 -11 1 0 218.98 3.90 13 -1 0 211.38 4.10 13 -1 0 208.48 4.20 13 -1 0 219.68 4.10 -13 -1 0 210.68 4.30 -13 -1 0 210.88 4.30 -13 1 0 217.28 4.10 13 1 0 212.88 4.40 13 1 0 215.18 4.30 -13 1 0 217.08 4.10 13 1 0 219.38 4.30 15 -1 0 809.92 12.70 -15 -1 0 799.42 12.90 15 -1 0 783.32 12.80 15 -1 0 794.72 12.70 -15 -1 0 798.02 12.80 -15 1 0 807.92 12.70 15 1 0 794.72 12.90 -15 1 0 795.22 12.60 15 1 0 802.52 12.90 15 1 0 793.32 13.00 17 -1 0 15.90 1.70 17 -1 0 18.80 2.00 -17 -1 0 21.60 2.20 -17 -1 0 19.80 1.60 17 -1 0 20.00 2.10 17 1 0 15.40 1.80 -17 1 0 17.40 1.50 17 1 0 18.80 1.60 17 1 0 20.90 2.20 -17 1 0 17.90 1.40 19 -1 0 233.58 4.80 19 -1 0 204.38 6.70 -19 -1 0 228.38 5.00 19 -1 0 222.08 5.10 19 1 0 233.08 5.00 -19 1 0 240.38 5.10 19 1 0 220.68 5.30 19 1 0 239.28 5.20 -19 1 0 229.38 4.80 21 -1 0 540.45 9.30 -21 -1 0 536.35 9.50 21 -1 0 519.15 9.40 21 -1 0 545.65 9.60 -21 -1 0 528.25 9.50 -21 1 0 541.35 9.30 -21 1 0 535.15 9.30 21 1 0 524.35 9.50 21 1 0 531.05 9.50 21 1 0 531.15 9.80 -23 -1 0 4.80 1.70 23 -1 0 4.80 1.90 -23 -1 0 3.80 1.60 23 -1 0 3.20 1.50 23 -1 0 5.60 1.60 -23 1 0 4.80 1.60 23 1 0 5.20 1.60 23 1 0 7.00 1.80 23 1 0 6.70 2.10 -23 1 0 2.80 1.80 -25 -1 0 -0.30 1.70 25 -1 0 1.60 1.60 25 -1 0 1.50 2.00 -25 -1 0 -0.80 1.70 25 -1 0 2.60 1.60 25 1 0 2.00 2.20 25 1 0 0.20 1.70 -25 1 0 0.20 1.80 -25 1 0 1.60 1.60 25 1 0 2.00 1.60 -27 -1 0 47.70 3.60 -27 -1 0 41.40 3.40 27 -1 0 46.80 3.80 27 -1 0 40.90 3.30 27 -1 0 43.00 3.30 27 1 0 46.50 4.00 27 1 0 49.10 3.60 27 1 0 42.20 3.60 -27 1 0 44.50 3.30 -27 1 0 45.60 3.20 0 -2 0 507.05 7.60 0 -2 0 501.45 7.60 0 -2 0 504.15 7.70 0 -2 0 505.65 7.80 0 2 0 509.05 7.80 0 2 0 492.05 7.60 -2 -2 0 1.20 0.50 -2 -2 0 1.30 0.70 2 -2 0 0.80 0.50 -2 -2 0 0.40 0.50 2 2 0 0.60 0.50 2 2 0 1.80 0.60 2 2 0 0.70 0.50 -2 2 0 0.90 0.50 4 -2 0 110.49 2.00 -4 -2 0 111.39 2.20 -4 -2 0 114.39 2.30 -4 -2 0 109.59 2.50 4 2 0 110.19 2.50 4 2 0 113.59 2.30 -4 2 0 113.29 2.10 4 2 0 116.29 2.30 -6 -2 0 6.80 1.00 -6 -2 0 7.00 0.90 6 -2 0 6.20 0.50 6 -2 0 7.50 0.80 6 -2 0 7.30 0.80 -6 -2 0 5.70 0.80 -6 2 0 6.40 0.50 6 2 0 6.30 0.80 6 2 0 6.40 1.10 -6 2 0 6.40 0.60 8 -2 0 66.39 1.60 -8 -2 0 62.49 2.20 8 -2 0 66.39 1.60 -8 -2 0 65.99 2.00 -8 -2 0 64.49 2.10 8 2 0 64.59 2.10 -8 2 0 63.29 1.60 8 2 0 62.59 2.30 8 2 0 64.29 2.10 10 -2 0 39.10 1.50 -10 -2 0 40.50 1.50 -10 -2 0 41.10 2.00 -10 -2 0 40.00 2.20 -10 -2 0 38.70 2.20 10 -2 0 40.70 1.50 10 2 0 39.10 2.30 10 2 0 40.60 2.20 -10 2 0 39.10 1.60 10 2 0 41.30 2.00 -12 -2 0 105.59 3.10 12 -2 0 103.69 2.40 -12 -2 0 103.49 2.90 12 -2 0 103.49 2.40 -12 -2 0 104.79 2.80 -12 -2 0 105.09 2.20 12 2 0 102.49 3.10 -12 2 0 104.09 2.40 -12 2 0 105.79 2.40 12 2 0 102.39 2.80 12 2 0 104.69 2.80 -14 -2 0 8.40 0.90 -14 -2 0 7.60 1.20 14 -2 0 7.10 1.20 14 -2 0 7.10 1.00 14 -2 0 7.90 1.00 -14 -2 0 8.20 1.30 14 2 0 7.50 1.40 14 2 0 6.80 1.20 -14 2 0 8.10 1.00 14 2 0 7.20 1.20 -14 2 0 6.90 0.90 16 -2 0 46.30 2.10 16 -2 0 49.50 2.10 -16 -2 0 45.60 2.50 -16 -2 0 48.60 2.40 16 -2 0 44.70 2.40 16 2 0 47.30 2.50 -16 2 0 49.99 2.20 16 2 0 48.50 2.90 -16 2 0 48.10 2.00 16 2 0 43.70 2.60 18 -2 0 4.90 1.20 -18 -2 0 3.40 1.50 18 -2 0 4.20 1.20 -18 -2 0 2.70 1.30 18 -2 0 -1.90 1.40 -18 2 0 2.10 1.20 18 2 0 3.50 1.40 18 2 0 -2.60 1.70 -18 2 0 3.20 1.30 18 2 0 3.10 1.40 20 -2 0 1.70 1.20 -20 -2 0 1.20 1.50 -20 -2 0 -0.70 1.40 20 -2 0 0.60 1.30 20 -2 0 -3.10 1.60 20 2 0 -3.80 1.90 -20 2 0 1.20 1.20 20 2 0 -0.20 1.40 20 2 0 0.00 1.50 -20 2 0 1.80 1.30 -22 -2 0 9.50 1.80 22 -2 0 12.20 1.90 22 -2 0 12.00 1.50 -22 -2 0 8.20 1.70 22 -2 0 12.00 1.60 22 2 0 10.00 1.70 22 2 0 10.30 1.80 -22 2 0 10.50 1.60 22 2 0 11.10 2.30 -22 2 0 11.80 1.60 24 -2 0 1.80 1.50 -24 -2 0 2.70 1.70 -24 -2 0 2.50 1.70 24 -2 0 3.40 1.50 24 -2 0 3.20 1.90 -24 2 0 3.20 1.60 24 2 0 4.30 1.70 -24 2 0 3.30 1.50 24 2 0 4.00 2.20 24 2 0 2.40 1.80 26 -2 0 2.20 2.00 -26 -2 0 0.10 1.80 26 -2 0 0.00 1.60 26 -2 0 -0.40 1.50 -26 2 0 -1.00 1.50 26 2 0 -0.80 1.70 -26 2 0 1.80 1.70 26 2 0 1.40 2.30 -1 -3 0 430.86 6.50 -1 -3 0 423.66 6.80 -1 -3 0 414.76 6.70 -1 -3 0 411.96 6.50 1 3 0 407.76 6.50 1 3 0 418.76 6.80 1 3 0 419.66 6.40 1 3 0 418.96 6.50 -5 -3 0 31.80 1.50 -5 -3 0 30.10 1.70 -5 -3 0 29.10 1.80 5 -3 0 29.20 1.30 -5 -3 0 31.50 1.60 5 -3 0 32.80 1.20 5 3 0 31.10 1.60 5 3 0 30.20 1.60 5 3 0 30.50 1.80 7 -3 0 279.07 4.20 7 -3 0 256.37 4.60 -7 -3 0 262.57 4.60 -7 -3 0 263.37 4.70 7 -3 0 256.97 4.30 -7 -3 0 265.17 5.00 7 3 0 266.47 4.70 7 3 0 267.27 5.00 7 3 0 266.37 5.00 -7 3 0 268.27 4.40 -9 -3 0 1404.96 22.00 -9 -3 0 1438.96 21.80 -9 -3 0 1418.66 21.60 9 -3 0 1462.25 21.30 9 -3 0 1396.36 21.30 -9 -3 0 1421.16 21.80 9 -3 0 1415.96 21.30 -9 3 0 1436.86 21.30 -9 3 0 1429.16 21.30 9 3 0 1420.86 21.80 9 3 0 1406.66 22.00 9 3 0 1442.36 21.80 -11 -3 0 92.29 2.70 11 -3 0 96.69 2.10 -11 -3 0 99.49 2.80 -11 -3 0 97.19 3.00 -11 -3 0 97.49 2.40 11 -3 0 94.89 2.10 -11 3 0 96.99 2.10 11 3 0 94.19 2.80 11 3 0 100.09 3.00 11 3 0 95.09 2.80 -11 3 0 95.49 2.10 -13 -3 0 330.17 6.40 -13 -3 0 329.47 6.10 -13 -3 0 337.87 6.20 13 -3 0 338.67 5.60 13 -3 0 341.97 5.60 -13 3 0 342.47 5.60 13 3 0 324.37 6.40 13 3 0 334.77 6.20 13 3 0 339.77 6.20 -15 -3 0 358.16 6.60 15 -3 0 345.77 6.20 -15 -3 0 360.56 6.60 15 -3 0 356.26 6.00 -15 -3 0 346.67 6.20 15 -3 0 354.56 6.00 -15 -3 0 350.46 6.90 15 3 0 347.77 6.90 -15 3 0 352.96 6.00 15 3 0 357.76 6.60 15 3 0 353.56 6.60 17 -3 0 1.50 1.10 17 -3 0 -1.50 1.30 17 -3 0 1.40 1.00 -17 -3 0 0.20 1.30 -17 -3 0 1.50 1.40 17 3 0 -1.20 1.70 17 3 0 -0.10 1.40 17 3 0 0.50 1.30 -17 3 0 0.90 1.10 19 -3 0 164.28 4.10 -19 -3 0 182.68 4.30 19 -3 0 167.58 3.80 -19 -3 0 165.28 4.40 -19 -3 0 171.38 4.50 -19 3 0 173.68 4.10 19 3 0 159.88 4.80 19 3 0 170.28 4.50 19 3 0 175.18 4.50 -19 3 0 171.38 3.90 21 -3 0 72.29 2.80 -21 -3 0 73.59 3.50 21 -3 0 73.39 3.20 21 -3 0 66.89 2.70 -21 -3 0 70.29 3.40 -21 3 0 69.59 2.70 21 3 0 62.79 4.60 -21 3 0 70.29 2.90 21 3 0 67.59 3.50 21 3 0 72.69 3.40 23 -3 0 2.10 1.70 -23 -3 0 -1.20 1.60 23 -3 0 1.40 1.40 -23 -3 0 -1.30 1.60 23 -3 0 0.10 1.30 23 3 0 3.00 2.10 -23 3 0 -1.60 1.30 23 3 0 0.40 1.70 -23 3 0 0.40 1.40 -25 -3 0 50.09 3.70 25 -3 0 57.79 3.00 25 -3 0 53.49 3.30 25 -3 0 49.30 3.00 -25 -3 0 54.79 3.70 25 3 0 53.99 4.20 -25 3 0 51.79 3.10 -25 3 0 50.59 2.90 25 3 0 53.49 3.60 25 3 0 54.69 3.80 -27 -3 0 59.89 3.90 27 -3 0 59.19 3.60 -27 -3 0 59.19 3.90 27 -3 0 58.59 3.20 27 -3 0 53.29 3.20 27 3 0 56.69 4.10 27 3 0 53.89 3.90 -27 3 0 61.69 3.10 -2 -4 0 80.49 2.00 2 -4 0 79.79 1.60 2 -4 0 82.59 2.20 -2 -4 0 85.59 2.00 2 -4 0 87.49 2.20 2 -4 0 80.29 1.80 2 -4 0 81.39 1.60 -2 -4 0 80.19 2.60 -2 -4 0 79.59 2.40 2 4 0 86.59 2.80 -2 4 0 86.59 2.20 -2 4 0 78.79 1.60 2 4 0 83.49 2.30 2 4 0 71.39 1.90 -2 4 0 86.29 1.60 2 4 0 89.29 2.00 -4 -4 0 492.45 8.00 4 -4 0 487.05 7.90 4 -4 0 478.45 7.80 -4 -4 0 498.85 8.20 4 -4 0 506.45 7.90 -4 -4 0 486.55 8.30 -4 -4 0 492.55 7.90 4 4 0 503.45 8.20 4 4 0 501.65 7.90 4 4 0 495.25 7.90 4 4 0 503.55 7.90 6 -4 0 20.00 1.40 -6 -4 0 19.00 1.60 -6 -4 0 19.80 1.60 -6 -4 0 17.50 2.00 6 -4 0 20.90 1.40 -6 -4 0 20.70 1.70 6 4 0 21.00 1.70 6 4 0 23.10 2.00 6 4 0 20.90 1.70 -8 -4 0 966.20 15.30 -8 -4 0 968.50 15.00 8 -4 0 942.11 14.70 -8 -4 0 962.60 15.10 -8 -4 0 970.60 15.00 8 4 0 967.70 15.10 8 4 0 955.00 15.30 8 4 0 971.60 15.00 -10 -4 0 499.95 8.40 10 -4 0 477.15 7.80 -10 -4 0 499.75 8.10 -10 -4 0 489.25 8.30 10 -4 0 509.05 7.60 -10 -4 0 489.45 8.60 10 -4 0 497.95 7.60 10 4 0 501.15 8.30 10 4 0 495.05 8.30 10 4 0 484.45 8.60 -12 -4 0 179.98 4.00 -12 -4 0 177.98 3.90 12 -4 0 179.88 3.20 -12 -4 0 177.28 4.30 12 -4 0 178.18 3.20 -12 -4 0 179.38 3.60 12 -4 0 171.28 3.10 -12 4 0 174.48 3.20 12 4 0 173.18 3.90 12 4 0 176.08 4.30 -12 4 0 175.68 3.10 12 4 0 181.38 4.00 14 -4 0 173.48 3.30 -14 -4 0 172.08 4.00 14 -4 0 172.18 3.30 -14 -4 0 168.68 3.60 -14 -4 0 170.18 4.40 -14 -4 0 172.18 4.20 -14 4 0 167.68 3.20 -14 4 0 173.28 3.30 14 4 0 170.28 4.10 14 4 0 176.08 4.40 14 4 0 171.38 4.10 -16 -4 0 2.20 1.30 -16 -4 0 3.90 1.40 -16 -4 0 3.10 1.10 -16 -4 0 0.30 1.60 16 -4 0 3.20 1.00 16 -4 0 3.10 0.90 -16 4 0 5.50 1.00 16 4 0 4.20 1.40 16 4 0 3.30 1.40 -16 4 0 1.70 1.00 16 4 0 2.90 1.70 18 -4 0 1068.89 16.20 -18 -4 0 1017.60 16.20 -18 -4 0 1057.39 17.70 18 -4 0 1069.19 16.30 -18 -4 0 1063.59 17.00 18 -4 0 1035.50 16.50 -18 4 0 1053.29 16.20 18 4 0 1029.40 17.30 -18 4 0 1069.79 16.20 18 4 0 974.80 17.50 -20 -4 0 132.09 4.20 20 -4 0 130.79 3.70 20 -4 0 137.09 3.40 -20 -4 0 130.19 4.30 20 -4 0 135.79 3.30 -20 -4 0 125.79 3.20 -20 4 0 137.19 3.30 20 4 0 123.19 6.60 20 4 0 132.69 4.30 -20 4 0 134.19 3.70 20 4 0 128.99 4.20 22 -4 0 108.49 3.10 22 -4 0 103.69 3.20 22 -4 0 101.79 3.50 -22 -4 0 93.59 4.00 -22 -4 0 99.49 4.00 -22 -4 0 98.99 2.70 -22 4 0 98.79 3.00 22 4 0 102.99 4.20 -22 4 0 103.49 3.20 22 4 0 98.19 4.00 22 4 0 96.29 4.50 24 -4 0 195.28 4.70 -24 -4 0 185.08 5.30 -24 -4 0 191.48 5.40 24 -4 0 191.48 4.60 24 -4 0 193.28 4.40 -24 4 0 190.28 4.50 24 4 0 192.98 5.50 24 4 0 187.78 5.30 -24 4 0 179.98 4.20 24 4 0 190.08 5.90 -26 -4 0 108.89 4.50 -26 -4 0 110.49 5.60 26 -4 0 113.79 3.60 26 -4 0 114.89 3.70 -26 4 0 112.39 3.40 26 4 0 109.29 4.50 26 4 0 113.49 4.70 -26 4 0 113.09 3.70 26 4 0 116.39 5.20 1 5 0 3289.37 49.30 1 5 0 3316.57 49.30 1 5 0 3333.37 49.60 3 -5 0 164.08 3.30 3 -5 0 160.28 3.30 -3 -5 0 154.68 3.10 3 -5 0 164.58 2.60 -3 -5 0 150.18 3.30 -3 -5 0 155.28 3.20 -3 -5 0 155.78 3.60 3 -5 0 153.88 2.90 -3 5 0 147.29 4.50 3 5 0 154.18 3.60 3 5 0 152.38 2.90 3 5 0 152.58 3.10 3 5 0 158.18 3.20 5 -5 0 163.58 3.20 -5 -5 0 161.58 3.50 5 -5 0 166.48 3.30 -5 -5 0 163.58 3.40 5 -5 0 166.88 3.30 -5 -5 0 162.68 3.30 -5 -5 0 158.38 3.80 5 5 0 163.78 3.40 5 5 0 161.88 3.40 5 5 0 160.88 3.30 5 5 0 164.08 3.80 7 -5 0 167.18 3.30 7 -5 0 165.78 3.30 -7 -5 0 163.98 3.90 -7 -5 0 161.08 3.50 -7 -5 0 166.58 3.60 -7 -5 0 165.68 3.50 7 5 0 158.88 3.90 7 5 0 168.68 3.60 7 5 0 168.68 3.60 9 -5 0 854.11 14.30 -9 -5 0 884.91 13.80 -9 -5 0 875.01 14.20 9 -5 0 861.21 13.50 -9 -5 0 867.91 13.70 -9 -5 0 871.51 13.80 9 5 0 863.71 14.10 9 5 0 868.51 13.80 9 5 0 868.81 13.80 -11 -5 0 160.28 3.50 11 -5 0 154.98 3.10 -11 -5 0 154.98 3.70 -11 -5 0 154.88 3.80 -11 -5 0 154.88 4.00 11 5 0 153.98 3.70 11 5 0 151.28 3.70 11 5 0 154.08 4.00 13 -5 0 29.30 1.30 -13 -5 0 27.30 2.00 13 -5 0 29.20 1.30 -13 -5 0 26.00 2.40 -13 -5 0 21.00 2.30 -13 -5 0 25.80 2.70 13 -5 0 24.00 1.40 13 5 0 23.90 2.70 13 5 0 22.40 2.30 13 5 0 25.00 2.40 -15 -5 0 649.24 11.50 15 -5 0 658.03 10.10 -15 -5 0 651.83 11.10 -15 -5 0 645.64 10.60 15 -5 0 655.53 10.20 -15 -5 0 649.24 11.10 15 5 0 645.14 11.10 15 5 0 657.03 11.10 15 5 0 638.44 11.40 -17 -5 0 -2.40 1.30 17 -5 0 1.50 0.90 -17 -5 0 -2.90 1.80 -17 -5 0 2.30 1.50 17 -5 0 1.80 0.90 -17 -5 0 -0.70 1.50 17 5 0 -0.90 1.50 -17 5 0 1.30 0.90 17 5 0 0.50 1.80 -17 5 0 1.30 0.90 17 5 0 2.80 1.60 -19 -5 0 175.78 4.90 -19 -5 0 176.48 4.70 19 -5 0 169.48 4.10 19 -5 0 181.88 3.70 19 -5 0 181.28 4.10 -19 -5 0 170.88 4.00 19 5 0 172.58 4.70 -19 5 0 185.78 3.60 19 5 0 159.98 5.20 -19 5 0 176.18 3.50 19 5 0 174.48 4.80 21 -5 0 718.83 11.90 21 -5 0 725.73 11.60 -21 -5 0 708.73 11.70 -21 -5 0 715.43 12.70 21 -5 0 737.33 11.70 -21 -5 0 735.73 12.70 -21 5 0 722.63 11.50 21 5 0 712.83 13.10 21 5 0 727.63 12.80 -21 5 0 723.43 11.50 21 5 0 721.63 12.60 23 -5 0 21.00 2.20 -23 -5 0 18.70 2.20 -23 -5 0 19.40 2.20 23 -5 0 25.30 2.30 23 -5 0 24.20 2.70 -23 -5 0 22.20 2.40 23 5 0 20.70 2.70 23 5 0 28.60 3.20 -23 5 0 20.80 2.20 23 5 0 19.70 2.40 -23 5 0 21.80 2.30 -25 -5 0 34.10 3.80 25 -5 0 34.80 2.50 25 -5 0 30.90 2.60 -25 5 0 32.40 2.50 -25 5 0 35.10 2.40 25 5 0 36.10 3.70 25 5 0 28.70 3.10 25 5 0 31.60 3.00 0 -6 0 1005.90 15.10 0 -6 0 974.40 15.10 0 -6 0 989.80 15.50 0 -6 0 983.80 15.50 0 6 0 997.90 15.60 0 6 0 969.30 15.00 -2 -6 0 22.10 2.10 2 -6 0 29.10 1.20 -2 -6 0 28.00 1.70 2 -6 0 29.20 1.90 -2 -6 0 22.90 1.50 2 -6 0 26.70 2.00 -2 -6 0 21.80 1.90 2 6 0 20.40 2.20 2 6 0 22.20 1.60 2 6 0 21.40 1.60 4 -6 0 308.57 5.60 -4 -6 0 312.27 5.90 -4 -6 0 306.97 5.50 -4 -6 0 304.07 5.40 -4 -6 0 313.57 5.70 4 -6 0 326.47 5.60 4 6 0 302.47 5.30 4 6 0 311.07 6.00 4 6 0 310.17 5.50 4 6 0 305.97 5.50 -4 6 0 320.57 5.60 -6 -6 0 43.30 2.50 -6 -6 0 44.30 2.20 -6 -6 0 44.00 2.00 6 -6 0 44.10 2.00 6 -6 0 46.70 1.90 -6 -6 0 43.20 2.20 6 -6 0 45.20 1.90 6 6 0 42.10 2.10 6 6 0 40.80 2.50 6 6 0 42.90 2.60 6 6 0 39.70 2.00 -8 -6 0 224.78 4.60 8 -6 0 224.58 4.20 -8 -6 0 226.98 4.60 8 -6 0 226.18 4.30 8 -6 0 228.58 4.40 -8 -6 0 225.38 5.00 -8 -6 0 220.48 4.50 8 6 0 227.28 4.50 8 6 0 216.48 5.00 8 6 0 222.48 4.50 10 -6 0 57.09 2.10 -10 -6 0 55.39 2.90 10 -6 0 55.79 2.00 -10 -6 0 53.79 2.60 -10 -6 0 54.59 2.40 -10 -6 0 53.79 2.40 10 -6 0 57.19 2.40 10 6 0 52.89 2.50 10 6 0 56.99 2.50 10 6 0 53.69 2.90 -12 -6 0 280.07 6.00 -12 -6 0 273.47 5.60 -12 -6 0 273.77 5.30 12 -6 0 269.77 4.90 -12 -6 0 267.77 5.50 12 -6 0 275.87 5.00 12 6 0 280.97 5.60 12 6 0 269.57 5.90 12 6 0 267.57 5.50 -14 -6 0 10.90 1.50 -14 -6 0 9.50 1.60 14 -6 0 9.20 1.30 -14 -6 0 8.10 1.80 14 -6 0 9.00 1.10 -14 -6 0 9.70 1.50 14 6 0 9.20 1.60 14 6 0 6.50 1.90 14 6 0 7.60 1.50 -16 -6 0 311.17 6.60 -16 -6 0 328.17 7.00 -16 -6 0 313.67 6.50 -16 -6 0 306.67 6.10 16 6 0 327.87 6.60 16 6 0 322.07 7.00 16 6 0 314.27 6.50 -18 -6 0 0.70 1.60 -18 -6 0 -3.40 2.00 -18 -6 0 0.00 1.60 18 -6 0 2.00 0.90 -18 -6 0 -4.40 1.50 18 -6 0 2.70 0.90 18 6 0 -0.90 1.70 18 6 0 -2.20 2.20 18 6 0 1.50 1.70 -20 -6 0 2.40 1.60 20 -6 0 4.90 1.00 -20 -6 0 4.10 1.90 -20 -6 0 3.10 2.40 20 -6 0 5.30 1.10 20 -6 0 3.00 1.50 -20 -6 0 7.00 1.90 20 6 0 2.50 2.30 20 6 0 2.50 1.90 -22 -6 0 74.59 4.00 -22 -6 0 75.49 3.00 22 -6 0 74.29 2.50 -22 -6 0 72.59 4.00 22 -6 0 72.89 2.50 22 6 0 66.39 6.20 22 6 0 74.69 4.70 22 6 0 81.09 4.00 -24 -6 0 3.50 2.00 -24 -6 0 3.80 1.40 24 -6 0 3.90 1.20 -24 -6 0 2.60 2.10 24 6 0 -0.20 2.00 24 6 0 -0.30 2.70 24 6 0 4.10 2.20 -1 -7 0 506.05 8.70 -1 -7 0 499.75 8.10 1 -7 0 501.05 8.60 1 -7 0 507.25 8.60 1 -7 0 502.95 7.90 1 -7 0 491.35 8.00 -1 -7 0 499.85 8.10 -1 7 0 500.65 8.60 1 7 0 517.35 8.70 -1 7 0 497.05 7.90 1 7 0 498.25 8.10 1 7 0 498.85 8.10 3 7 0 6641.74 99.09 -5 -7 0 60.19 2.40 -5 -7 0 57.69 2.50 5 -7 0 59.49 2.30 5 -7 0 61.69 1.90 -5 -7 0 54.09 2.80 -5 -7 0 56.29 2.20 5 -7 0 65.99 2.40 5 7 0 51.69 2.50 5 7 0 57.99 2.20 -5 7 0 54.19 2.50 5 7 0 54.89 2.90 5 7 0 56.99 2.30 7 -7 0 1.90 1.10 -7 -7 0 -0.40 1.00 -7 -7 0 -0.70 1.10 -7 -7 0 0.70 1.40 -7 -7 0 1.50 1.10 7 -7 0 1.30 1.10 7 -7 0 0.70 1.00 7 7 0 1.50 1.10 7 7 0 -1.50 1.50 7 7 0 -0.60 1.10 7 7 0 0.60 1.10 -9 -7 0 202.08 4.40 -9 -7 0 208.88 4.50 -9 -7 0 208.68 5.00 -9 -7 0 202.88 4.50 9 -7 0 209.68 4.30 9 -7 0 209.48 4.10 9 -7 0 207.88 4.20 9 7 0 206.38 5.00 9 7 0 204.48 4.40 9 7 0 203.68 4.40 9 7 0 201.38 4.40 11 -7 0 22.60 1.90 11 -7 0 23.90 1.90 -11 -7 0 19.60 1.60 -11 -7 0 22.60 2.90 -11 -7 0 19.90 2.30 -11 -7 0 24.20 1.80 11 -7 0 21.80 2.30 11 7 0 21.80 2.40 11 7 0 24.00 3.00 11 7 0 18.30 1.60 13 -7 0 60.49 2.30 -13 -7 0 55.29 2.70 -13 -7 0 62.79 3.10 13 -7 0 60.39 2.80 -13 -7 0 61.59 3.50 13 -7 0 54.79 2.40 -13 -7 0 61.29 2.90 13 7 0 56.39 3.00 13 7 0 57.69 3.60 13 7 0 61.59 3.00 -15 -7 0 6.00 1.70 -15 -7 0 8.10 1.60 -15 -7 0 4.90 1.50 15 -7 0 8.90 1.20 15 7 0 7.10 2.50 15 7 0 3.10 1.60 15 7 0 6.80 1.70 17 -7 0 28.90 1.90 -17 -7 0 26.90 2.60 -17 -7 0 26.00 2.70 -17 -7 0 19.70 2.00 17 -7 0 22.20 2.20 -17 -7 0 23.10 2.30 17 7 0 21.90 2.20 17 7 0 18.60 2.60 17 7 0 25.20 3.40 -19 -7 0 31.50 2.80 -19 -7 0 23.70 2.70 -19 -7 0 35.40 3.30 19 -7 0 30.60 2.40 -19 -7 0 32.80 3.40 19 7 0 34.80 3.40 19 7 0 30.90 2.50 19 7 0 25.60 3.00 -21 -7 0 16.70 2.20 -21 -7 0 13.50 2.70 -21 -7 0 17.70 2.30 -21 -7 0 17.80 1.90 21 7 0 13.70 3.60 21 7 0 16.50 2.40 21 7 0 12.30 2.20 -23 -7 0 4.70 1.70 -23 -7 0 0.90 2.00 -23 -7 0 -2.50 2.00 23 7 0 0.60 2.00 23 7 0 0.40 2.80 23 7 0 -2.00 2.10 -2 -8 0 16.60 1.30 -2 -8 0 17.30 1.80 2 -8 0 21.70 2.40 -2 -8 0 19.40 1.80 2 -8 0 21.70 1.50 -2 -8 0 20.60 2.30 2 -8 0 23.50 1.50 2 -8 0 17.20 1.70 -2 8 0 20.00 1.50 2 8 0 15.30 1.30 2 8 0 13.30 1.90 2 8 0 16.60 1.30 -2 8 0 23.20 1.60 -2 8 0 21.20 2.60 4 -8 0 2.70 1.30 4 -8 0 0.50 1.20 -4 -8 0 3.20 1.40 -4 -8 0 0.60 1.00 4 -8 0 2.80 0.70 -4 -8 0 0.80 1.10 -4 -8 0 -0.20 1.40 4 -8 0 2.10 0.70 -4 8 0 2.80 1.40 4 8 0 1.60 1.70 4 8 0 0.10 1.10 4 8 0 5.50 1.20 4 8 0 1.10 1.00 6 -8 0 98.09 2.90 -6 -8 0 90.69 2.80 6 -8 0 90.09 2.90 -6 -8 0 93.69 3.50 -6 -8 0 91.79 3.10 6 8 0 99.79 4.40 6 8 0 90.59 2.60 6 8 0 90.99 3.60 6 8 0 91.29 2.80 8 -8 0 120.69 3.20 -8 -8 0 120.79 3.90 8 -8 0 120.79 3.30 -8 -8 0 116.29 3.20 -8 -8 0 117.29 3.50 8 -8 0 116.59 3.00 -8 -8 0 125.49 3.50 8 8 0 121.19 3.40 8 8 0 116.09 3.20 8 8 0 120.59 4.00 8 8 0 120.39 3.40 -10 -8 0 183.78 4.30 -10 -8 0 178.98 4.90 -10 -8 0 183.48 4.50 10 -8 0 168.98 4.00 10 -8 0 162.68 3.90 -10 -8 0 177.18 4.30 10 -8 0 167.98 3.90 10 8 0 195.98 4.40 10 8 0 187.48 4.30 10 8 0 185.18 5.00 10 8 0 184.68 4.40 -12 -8 0 7.80 1.70 -12 -8 0 6.90 1.70 -12 -8 0 7.00 1.50 12 -8 0 5.50 1.30 12 -8 0 6.30 1.50 -12 -8 0 6.20 1.90 12 -8 0 8.50 1.30 12 8 0 7.60 2.30 12 8 0 8.90 1.60 12 8 0 6.30 1.70 12 8 0 8.20 1.60 -14 -8 0 3.60 1.70 -14 -8 0 2.40 1.90 14 -8 0 0.60 1.30 14 -8 0 3.10 1.20 14 -8 0 3.40 1.60 -14 -8 0 5.00 1.80 -14 -8 0 1.60 1.60 14 8 0 3.00 1.80 14 8 0 2.20 1.70 14 8 0 2.00 2.20 14 8 0 0.50 2.50 -16 -8 0 59.69 3.60 16 -8 0 66.19 2.40 16 -8 0 57.59 2.70 -16 -8 0 57.29 3.20 -16 -8 0 60.99 3.40 -16 -8 0 61.69 4.00 16 -8 0 62.29 3.30 16 8 0 59.19 3.60 16 8 0 64.49 3.50 16 8 0 62.99 4.30 -18 -8 0 680.83 12.20 -18 -8 0 687.13 12.30 18 -8 0 693.03 11.00 -18 -8 0 672.13 11.80 -18 -8 0 677.93 12.80 18 8 0 684.43 12.90 18 8 0 674.93 12.10 18 8 0 685.73 12.30 -20 -8 0 155.08 5.10 -20 -8 0 149.99 5.70 -20 -8 0 150.78 5.10 20 -8 0 161.28 5.00 -20 -8 0 152.78 4.40 20 8 0 147.39 5.30 20 8 0 153.38 5.00 20 8 0 152.18 6.00 -22 -8 0 7.30 1.90 -22 -8 0 4.20 2.50 -22 -8 0 3.50 2.20 -22 -8 0 9.30 2.30 22 -8 0 4.70 2.20 22 8 0 3.60 3.10 22 8 0 3.10 2.10 22 8 0 4.50 2.40 -1 -9 0 1621.94 25.00 1 -9 0 1637.24 24.80 1 -9 0 1618.74 25.50 -1 -9 0 1642.64 24.90 -1 -9 0 1629.94 25.50 1 -9 0 1650.73 25.60 -1 -9 0 1617.34 25.60 1 -9 0 1651.83 24.80 -1 9 0 1668.23 25.60 1 9 0 1660.43 25.70 1 9 0 1635.44 24.90 -1 9 0 1642.04 24.80 1 9 0 1612.14 24.90 3 -9 0 46.20 2.60 3 -9 0 50.19 1.80 3 -9 0 51.39 1.70 -3 -9 0 49.40 2.20 3 -9 0 48.70 2.80 -3 -9 0 50.79 2.30 -3 -9 0 50.49 2.80 -3 -9 0 48.60 3.00 -3 9 0 51.39 1.70 3 9 0 43.50 2.30 3 9 0 45.30 2.30 3 9 0 46.50 3.20 -3 9 0 50.39 3.00 -3 9 0 50.79 1.70 -5 -9 0 15.10 1.40 -5 -9 0 21.20 2.10 -5 -9 0 16.80 1.50 -5 -9 0 16.50 1.80 5 9 0 12.10 1.40 5 9 0 15.50 1.50 5 9 0 13.00 1.90 -7 -9 0 2.40 1.30 -7 -9 0 0.90 1.60 -7 -9 0 1.60 1.20 7 -9 0 4.10 1.40 -7 -9 0 4.30 1.60 7 -9 0 3.80 1.40 7 -9 0 2.30 1.10 7 9 0 2.20 1.20 7 9 0 0.60 1.80 7 9 0 2.00 1.30 7 9 0 3.80 1.30 9 -9 0 52.29 2.70 9 -9 0 48.80 2.40 -9 -9 0 49.10 2.90 -9 -9 0 52.69 2.70 -9 -9 0 48.90 3.40 9 -9 0 57.09 2.60 -9 -9 0 52.19 2.90 9 9 0 48.90 2.90 9 9 0 49.10 3.60 9 9 0 45.80 2.60 9 9 0 48.60 2.80 11 -9 0 90.19 3.00 -11 -9 0 93.29 4.40 11 -9 0 94.49 3.20 -11 -9 0 88.69 3.50 11 -9 0 93.79 3.10 -11 -9 0 99.39 4.10 -11 -9 0 92.99 3.70 11 9 0 90.59 3.60 11 9 0 92.89 4.30 11 9 0 88.19 3.40 -13 -9 0 145.19 4.30 -13 -9 0 148.09 4.30 -13 -9 0 144.39 4.90 13 -9 0 144.39 3.70 -13 -9 0 146.09 4.50 13 -9 0 147.29 3.80 13 -9 0 141.99 4.10 13 9 0 145.59 5.10 13 9 0 144.19 4.30 13 9 0 149.09 4.50 13 9 0 146.79 4.30 -15 -9 0 445.76 8.50 15 -9 0 435.86 7.70 -15 -9 0 432.96 8.60 15 -9 0 438.96 7.70 15 -9 0 441.26 8.30 -15 -9 0 424.56 8.50 -15 -9 0 426.76 9.20 15 9 0 429.06 8.40 15 9 0 441.06 9.30 15 9 0 440.16 8.60 15 9 0 441.86 8.60 -17 -9 0 17.80 2.60 -17 -9 0 19.80 2.20 -17 -9 0 15.90 2.50 17 -9 0 26.50 2.30 -17 -9 0 17.00 2.20 17 -9 0 17.90 2.20 17 9 0 11.70 2.90 17 9 0 17.70 2.60 17 9 0 18.30 2.40 17 9 0 15.40 2.20 19 -9 0 63.89 3.80 -19 -9 0 64.19 4.00 -19 -9 0 56.49 4.70 -19 -9 0 56.99 3.50 -19 -9 0 66.89 4.10 19 -9 0 68.69 2.70 19 9 0 57.09 4.60 19 9 0 70.59 4.40 19 9 0 59.59 4.10 19 9 0 58.79 5.20 21 -9 0 397.46 8.50 -21 -9 0 394.76 9.30 -21 -9 0 394.26 8.70 -21 -9 0 396.86 8.60 -21 -9 0 398.26 8.00 21 9 0 411.06 9.70 21 9 0 388.06 8.60 21 9 0 402.56 10.70 0 -10 0 466.95 8.70 0 -10 0 465.85 8.70 0 -10 0 468.75 7.90 0 -10 0 468.75 7.80 0 10 0 469.05 7.80 0 10 0 476.15 8.90 -2 -10 0 1.60 1.10 2 -10 0 1.90 1.00 -2 -10 0 1.10 1.60 2 -10 0 0.30 1.50 2 -10 0 2.00 1.60 2 -10 0 0.70 0.90 -2 -10 0 4.60 1.80 -2 -10 0 2.90 1.20 2 10 0 2.30 1.20 -2 10 0 0.90 1.00 -2 10 0 2.00 1.00 -2 10 0 2.60 1.70 2 10 0 0.10 1.90 2 10 0 0.90 1.20 -4 -10 0 37.90 2.30 -4 -10 0 40.50 2.90 -4 -10 0 40.60 3.30 4 -10 0 48.20 1.70 4 -10 0 46.20 2.90 4 -10 0 48.10 3.00 4 -10 0 48.90 1.80 -4 -10 0 41.70 2.50 -4 10 0 50.59 3.20 4 10 0 37.70 2.50 4 10 0 42.80 3.50 4 10 0 41.50 2.60 -6 -10 0 137.99 4.10 6 -10 0 135.89 4.00 -6 -10 0 134.79 4.50 6 -10 0 135.29 3.90 -6 -10 0 139.89 3.80 -6 -10 0 132.99 4.10 6 10 0 130.59 4.70 6 10 0 130.09 4.20 6 10 0 137.09 3.70 8 -10 0 83.69 3.30 8 -10 0 84.19 3.30 -8 -10 0 79.89 3.90 -8 -10 0 77.49 3.30 -8 -10 0 76.99 3.10 8 -10 0 77.49 2.70 -8 -10 0 75.49 4.60 8 10 0 79.39 3.20 8 10 0 80.69 4.10 8 10 0 80.39 2.90 8 10 0 74.79 3.30 -10 -10 0 5.50 1.90 -10 -10 0 2.80 1.60 10 -10 0 4.30 1.40 -10 -10 0 3.70 2.00 10 -10 0 3.60 1.50 -10 -10 0 3.60 1.60 10 -10 0 6.00 1.50 10 10 0 3.30 2.20 10 10 0 2.60 1.60 10 10 0 1.90 1.70 10 10 0 5.70 1.60 12 -10 0 49.10 2.80 -12 -10 0 50.89 3.30 -12 -10 0 44.10 3.90 -12 -10 0 43.90 3.10 -12 -10 0 45.70 3.30 12 -10 0 39.10 2.80 12 -10 0 50.49 2.80 12 10 0 44.30 3.40 12 10 0 45.10 3.30 12 10 0 43.50 3.20 12 10 0 43.60 4.30 14 -10 0 -1.00 1.60 -14 -10 0 1.50 1.80 14 -10 0 2.00 1.50 -14 -10 0 1.30 2.00 14 -10 0 -1.10 1.50 -14 -10 0 -1.60 1.60 -14 -10 0 -0.70 1.80 14 10 0 0.90 1.90 14 10 0 -1.00 2.00 14 10 0 -0.80 1.80 14 10 0 2.30 2.50 -16 -10 0 364.26 7.80 16 -10 0 374.16 7.80 16 -10 0 384.06 7.10 -16 -10 0 382.36 8.70 -16 -10 0 385.66 8.00 16 -10 0 379.96 7.10 -16 -10 0 382.26 10.40 16 10 0 382.26 8.10 16 10 0 390.76 9.10 16 10 0 377.46 8.50 16 10 0 387.76 8.00 -18 -10 0 14.80 2.20 18 -10 0 11.40 2.20 -18 -10 0 15.60 3.00 -18 -10 0 15.60 2.30 18 -10 0 24.40 2.50 -18 -10 0 15.10 2.40 18 10 0 16.80 3.50 18 10 0 12.10 2.70 18 10 0 12.90 2.50 18 10 0 11.10 2.30 20 -10 0 -1.10 2.00 -20 -10 0 2.60 2.00 -20 -10 0 3.10 2.10 -20 -10 0 2.80 2.20 -20 -10 0 -0.60 4.20 20 10 0 3.90 2.20 20 10 0 2.60 2.80 20 10 0 2.30 2.50 1 -11 0 213.78 5.40 -1 -11 0 206.48 4.50 1 -11 0 197.28 6.80 -1 -11 0 210.98 5.50 1 -11 0 200.28 4.10 -1 -11 0 215.78 4.50 1 -11 0 201.38 4.20 -1 -11 0 206.78 5.30 1 11 0 198.58 4.60 -1 11 0 203.58 4.20 -1 11 0 198.08 4.20 -1 11 0 205.98 5.60 1 11 0 210.28 5.80 1 11 0 207.58 4.40 -3 -11 0 2846.12 42.30 3 -11 0 2756.02 41.80 -3 -11 0 2767.42 42.30 -3 -11 0 2727.63 42.90 3 -11 0 2768.62 42.80 3 -11 0 2791.92 41.80 -3 -11 0 2749.02 43.10 3 -11 0 2837.52 44.00 -3 11 0 2802.52 41.70 3 11 0 2828.72 43.20 -3 11 0 2807.52 41.70 -3 11 0 2822.22 42.90 3 11 0 2776.52 42.20 -5 -11 0 18.30 2.10 -5 -11 0 22.80 2.40 -5 -11 0 19.10 1.80 -5 -11 0 14.90 2.20 5 -11 0 24.30 3.00 5 -11 0 19.10 2.00 5 11 0 17.00 2.40 5 11 0 17.10 1.70 5 11 0 18.30 1.70 -5 11 0 19.50 2.30 -7 -11 0 21.70 2.50 7 -11 0 14.60 1.90 -7 -11 0 19.00 2.10 7 -11 0 12.70 1.90 -7 -11 0 20.30 1.80 7 11 0 17.00 1.80 7 11 0 14.90 2.40 7 11 0 15.40 1.80 -9 -11 0 11.50 2.00 -9 -11 0 11.00 1.70 -9 -11 0 11.90 1.80 9 -11 0 10.70 1.90 -9 -11 0 11.90 2.20 9 -11 0 8.50 1.80 9 11 0 8.50 1.70 9 11 0 11.70 2.60 9 11 0 8.90 1.90 9 11 0 9.50 1.60 11 -11 0 3.10 1.70 11 -11 0 4.40 1.70 -11 -11 0 1.40 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4.00 1.90 -13 -11 3 3.60 1.70 13 -11 -3 6.30 1.90 -13 -11 3 5.30 1.80 -13 -11 3 4.70 2.10 13 -11 -3 4.30 1.30 13 11 -3 4.60 1.80 13 11 -3 6.40 2.80 -13 11 3 7.20 2.30 13 11 -3 4.30 2.20 13 11 -3 4.50 2.00 -11 -11 3 178.48 4.70 -11 -11 3 173.98 5.10 11 -11 -3 189.48 3.80 -11 -11 3 183.98 4.80 -11 -11 3 176.58 5.60 11 -11 -3 181.18 3.80 11 -11 -3 177.18 5.00 11 11 -3 180.28 4.90 11 11 -3 182.98 5.10 11 11 -3 174.78 4.70 -11 11 3 179.48 5.20 11 11 -3 181.38 5.90 9 -11 -3 221.38 4.50 -9 -11 3 222.48 5.70 9 -11 -3 236.28 4.50 -9 -11 3 223.88 6.10 9 -11 -3 231.28 5.10 -9 -11 3 227.98 5.20 9 -11 -3 228.08 5.60 -9 -11 3 226.08 5.20 9 11 -3 230.48 5.50 9 11 -3 229.18 6.40 -9 11 3 226.98 4.40 -9 11 3 233.68 5.90 -9 11 3 232.88 4.40 9 11 -3 223.68 5.10 9 11 -3 229.08 5.50 -9 11 3 233.18 5.20 -7 -11 3 0.10 1.30 -7 -11 3 -1.80 1.40 7 -11 -3 0.40 1.10 -7 -11 3 -0.90 1.70 -7 -11 3 -0.30 1.80 7 -11 -3 0.00 1.70 7 -11 -3 1.10 1.10 7 -11 -3 2.00 1.60 -7 11 3 0.50 1.20 7 11 -3 -2.20 1.50 7 11 -3 0.00 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1.80 0 -10 4 26.90 2.80 0 -10 4 16.20 3.70 0 -10 -4 20.80 1.80 0 -10 -4 19.80 2.20 0 10 4 17.10 1.80 0 10 4 17.60 1.80 0 10 -4 18.70 1.70 0 10 -4 19.10 2.10 0 10 -4 20.80 1.80 0 10 4 21.20 2.40 0 10 4 19.90 2.20 2 -10 4 11.60 1.80 -2 -10 -4 16.10 2.00 -2 -10 -4 15.20 2.20 -2 -10 -4 13.60 1.70 -2 -10 -4 12.20 1.80 2 -10 4 15.50 3.90 2 10 4 12.20 1.80 2 10 4 10.00 1.80 2 10 4 9.90 2.10 2 10 4 13.10 2.70 -2 10 -4 13.30 2.10 -4 -10 -4 114.59 3.90 -4 -10 -4 117.79 4.50 4 -10 4 117.59 3.80 4 -10 4 126.09 4.10 4 -10 4 117.99 4.60 -4 -10 -4 115.69 4.10 -4 -10 -4 118.29 4.00 4 10 4 118.89 4.10 4 10 4 109.09 4.40 4 10 4 112.99 4.00 4 10 4 111.49 4.60 -6 -10 -4 121.29 4.00 -6 -10 -4 116.39 4.30 -6 -10 -4 119.89 4.20 6 -10 4 113.99 3.70 6 -10 4 119.49 4.30 6 -10 4 123.79 4.20 -6 -10 -4 118.99 4.80 6 10 4 114.79 4.90 6 10 4 112.99 4.10 6 10 4 119.39 4.40 8 -10 4 0.80 1.90 8 -10 4 0.10 1.40 -8 -10 -4 -0.60 1.70 -8 -10 -4 0.10 1.80 8 -10 4 3.20 2.40 -8 -10 -4 -2.50 1.80 8 10 4 0.40 2.40 8 10 4 -2.40 1.80 -10 -10 -4 59.19 3.60 10 -10 4 55.99 3.80 -10 -10 -4 64.99 5.10 10 -10 4 58.69 3.80 -10 -10 -4 57.49 3.70 10 -10 4 58.99 2.80 10 10 4 63.99 3.40 10 10 4 58.99 4.80 10 10 4 55.59 3.80 -12 -10 -4 27.70 2.60 12 -10 4 30.50 3.50 12 -10 4 31.60 3.80 -12 -10 -4 33.50 3.30 -12 -10 -4 27.50 2.70 12 -10 4 27.60 2.50 12 10 4 24.20 2.50 12 10 4 34.00 2.90 12 10 4 38.00 4.80 12 10 4 34.20 3.40 14 -10 4 20.20 1.70 -14 -10 -4 18.80 2.60 -14 -10 -4 20.00 2.50 -14 -10 -4 21.90 2.50 14 -10 4 22.10 2.70 14 -10 4 20.00 2.40 14 10 4 20.70 5.10 14 10 4 16.60 2.50 14 10 4 17.70 2.80 14 10 4 20.80 2.40 -16 -10 -4 2.50 2.30 -16 -10 -4 4.90 2.30 -16 -10 -4 3.20 2.00 16 -10 4 0.40 2.10 16 -10 4 5.20 2.40 16 10 4 6.40 2.40 16 10 4 1.50 2.60 16 10 4 3.10 3.20 -21 -11 4 2.20 2.30 -21 -11 4 7.80 2.60 -21 -11 4 3.10 2.20 21 -11 -4 5.60 2.20 21 -11 -4 7.90 1.90 -21 -11 4 4.80 2.30 21 11 -4 2.70 2.30 21 11 -4 7.30 3.30 21 11 -4 9.60 3.10 21 11 -4 1.60 2.70 -19 -11 4 2.00 2.10 -19 -11 4 3.00 2.40 -19 -11 4 0.20 2.30 -19 -11 4 2.50 2.10 19 -11 -4 1.10 2.00 19 11 -4 -0.10 2.70 -19 11 4 0.40 2.30 19 11 -4 -1.30 2.30 19 11 -4 -1.30 2.80 17 -11 -4 12.10 2.20 -17 -11 4 10.80 2.60 -17 -11 4 13.30 2.20 17 -11 -4 10.30 1.30 -17 -11 4 12.50 2.10 -17 11 4 14.50 2.30 17 11 -4 11.40 2.40 17 11 -4 14.00 2.70 17 11 -4 10.20 3.10 17 11 -4 10.70 2.20 15 -11 -4 278.57 5.20 15 -11 -4 274.37 6.40 -15 -11 4 279.17 6.40 15 -11 -4 274.37 5.20 -15 -11 4 267.47 7.10 -15 -11 4 275.77 6.40 15 11 -4 281.07 7.50 15 11 -4 277.17 6.90 15 11 -4 276.27 6.30 15 11 -4 280.17 6.60 -15 11 4 287.17 6.70 13 -11 -4 73.79 3.90 -13 -11 4 74.69 4.40 13 -11 -4 79.19 2.70 -13 -11 4 69.99 3.60 13 -11 -4 76.39 2.70 -13 -11 4 73.49 4.20 -13 11 4 74.49 2.60 -13 11 4 76.99 4.10 13 11 -4 76.59 4.90 13 11 -4 74.49 4.00 13 11 -4 75.59 3.60 13 11 -4 74.49 4.40 -13 11 4 73.39 2.60 11 -11 -4 275.87 6.40 11 -11 -4 282.27 5.40 -11 -11 4 272.87 7.00 11 -11 -4 281.67 5.60 11 -11 -4 282.77 5.40 -11 -11 4 280.07 6.10 11 11 -4 276.87 7.30 11 11 -4 275.67 6.00 11 11 -4 290.87 6.30 11 11 -4 284.07 6.60 -11 11 4 281.67 5.30 -11 11 4 285.77 5.30 -11 11 4 288.47 6.70 -9 -11 4 62.59 3.10 9 -11 -4 64.59 2.70 9 -11 -4 66.69 3.10 9 -11 -4 65.49 3.70 9 -11 -4 69.39 2.70 -9 -11 4 64.29 4.00 9 11 -4 59.59 3.10 -9 11 4 65.79 3.40 9 11 -4 62.89 4.50 -9 11 4 68.69 3.90 -9 11 4 66.79 2.70 9 11 -4 66.99 3.90 9 11 -4 58.09 3.60 7 -11 -4 1.40 1.30 7 -11 -4 3.00 1.30 7 -11 -4 1.90 1.60 -7 -11 4 0.10 1.70 -7 -11 4 1.70 1.40 7 -11 -4 3.40 1.90 -7 -11 4 1.20 1.90 7 11 -4 2.50 1.60 7 11 -4 -0.50 1.40 -7 11 4 2.10 1.80 7 11 -4 0.10 2.40 -7 11 4 2.90 1.40 7 11 -4 -0.60 2.00 -7 11 4 2.40 1.30 -7 11 4 0.60 1.90 -5 -11 4 46.20 3.90 5 -11 -4 49.80 2.70 5 -11 -4 52.09 3.20 5 -11 -4 46.60 3.40 -5 -11 4 48.60 2.60 -5 -11 4 48.80 3.20 5 -11 -4 47.30 2.70 5 11 -4 52.09 4.30 -5 11 4 48.90 3.70 5 11 -4 45.90 2.60 5 11 -4 43.80 2.70 -5 11 4 46.50 2.80 -5 11 4 49.00 2.70 5 11 -4 44.30 3.50 -5 11 4 49.80 3.50 -3 -11 4 23.90 2.50 3 -11 -4 26.90 3.20 3 -11 -4 26.60 3.20 3 -11 -4 24.90 2.60 3 -11 -4 27.20 2.50 -3 -11 4 24.90 2.20 -3 -11 4 24.90 3.00 3 11 -4 17.80 1.70 -3 11 4 22.30 2.40 -3 11 4 26.70 2.60 3 11 -4 24.70 2.30 -3 11 4 19.50 2.30 3 11 -4 21.50 2.30 -3 11 4 25.00 2.80 1 -11 -4 536.85 10.20 1 -11 -4 546.15 9.60 -1 -11 4 547.25 9.30 1 -11 -4 536.55 9.60 -1 -11 4 555.54 9.90 -1 -11 4 537.35 10.40 1 -11 -4 545.85 10.20 1 11 -4 552.44 10.00 -1 11 4 542.55 10.30 -1 11 4 544.65 9.60 -1 11 4 553.74 10.30 -1 11 4 543.65 9.70 1 11 -4 525.35 8.80 1 11 -4 553.34 8.90 -1 -11 -4 105.89 4.10 -1 -11 -4 111.39 3.90 1 -11 4 107.99 2.70 1 -11 4 113.39 3.90 1 -11 4 112.49 2.70 1 -11 4 114.29 4.10 -1 -11 -4 115.29 3.80 -1 -11 -4 112.99 4.50 1 -11 4 102.79 4.40 1 11 4 110.09 3.90 1 11 4 113.79 4.50 -1 11 -4 107.09 4.20 1 11 4 110.99 4.00 1 11 4 113.49 4.80 3 -11 4 5.10 1.70 -3 -11 -4 3.20 2.10 -3 -11 -4 5.60 1.70 -3 -11 -4 3.30 1.90 3 -11 4 4.50 1.90 -3 -11 -4 2.30 1.70 3 -11 4 4.20 1.80 3 11 4 4.30 1.90 3 11 4 1.60 2.40 3 11 4 5.30 1.70 -5 -11 -4 47.10 3.30 5 -11 4 53.59 3.50 5 -11 4 54.49 3.20 -5 -11 -4 50.39 4.00 -5 -11 -4 48.60 3.60 5 -11 4 48.00 3.60 -5 -11 -4 46.60 3.60 5 11 4 51.79 3.70 5 11 4 49.99 3.50 5 11 4 50.69 4.40 7 -11 4 -0.30 1.70 -7 -11 -4 4.00 2.00 7 -11 4 1.30 2.00 7 -11 4 4.90 2.30 -7 -11 -4 -0.10 1.90 7 11 4 4.10 2.80 7 11 4 2.00 1.90 -9 -11 -4 13.90 2.20 9 -11 4 13.40 2.30 -9 -11 -4 12.60 2.10 9 -11 4 16.00 2.20 -9 -11 -4 12.10 2.60 9 11 4 14.60 2.50 9 11 4 14.60 2.30 9 11 4 13.70 2.80 11 -11 4 -0.10 2.10 -11 -11 -4 2.50 2.00 11 -11 4 1.00 2.00 -11 -11 -4 -2.30 1.90 -11 -11 -4 -3.70 2.10 11 -11 4 1.30 1.50 11 11 4 2.00 2.40 11 11 4 2.00 1.80 11 11 4 -0.60 2.20 11 11 4 -0.10 3.00 -13 -11 -4 35.40 3.60 13 -11 4 35.40 2.80 13 -11 4 34.90 3.70 -13 -11 -4 38.70 4.00 -13 -11 -4 30.10 2.80 13 -11 4 37.40 4.00 13 11 4 33.70 3.20 13 11 4 26.00 4.70 13 11 4 44.60 5.50 13 11 4 37.60 3.60 -18 -12 4 65.49 4.80 -18 -12 4 65.59 4.20 -18 -12 4 66.59 4.20 18 -12 -4 71.99 4.20 18 12 -4 72.09 5.10 18 12 -4 64.79 4.90 18 12 -4 62.39 4.20 18 12 -4 61.59 5.80 -16 -12 4 26.80 2.40 -16 -12 4 23.70 3.10 16 -12 -4 30.90 2.00 16 -12 -4 26.40 2.60 16 -12 -4 29.00 2.10 -16 -12 4 31.70 3.70 -16 -12 4 36.70 3.80 16 12 -4 29.30 3.00 16 12 -4 27.80 2.80 16 12 -4 23.00 2.60 16 12 -4 24.20 3.60 -16 12 4 26.40 2.80 14 -12 -4 4.50 2.10 -14 -12 4 7.20 2.40 14 -12 -4 5.20 1.30 -14 -12 4 7.50 2.00 14 -12 -4 6.00 1.20 -14 -12 4 11.70 2.50 -14 -12 4 7.50 2.00 14 12 -4 9.20 2.80 14 12 -4 8.90 2.30 14 12 -4 7.10 2.00 14 12 -4 8.20 2.50 -14 12 4 6.10 2.40 12 -12 -4 237.38 6.10 -12 -12 4 232.98 5.70 12 -12 -4 246.08 4.90 12 -12 -4 241.18 4.80 -12 -12 4 240.78 6.70 -12 -12 4 240.28 5.80 12 12 -4 233.98 5.70 -12 12 4 244.58 4.80 12 12 -4 240.78 7.20 12 12 -4 233.28 7.20 12 12 -4 248.68 6.00 -12 12 4 251.67 6.50 -12 12 4 243.28 4.70 -10 -12 4 1.20 2.20 10 -12 -4 1.80 1.30 10 -12 -4 0.20 2.00 10 -12 -4 -0.50 1.30 -10 -12 4 0.60 1.60 10 -12 -4 1.10 1.60 10 12 -4 1.70 2.20 10 12 -4 -0.90 1.80 10 12 -4 -1.80 2.80 -10 12 4 1.00 2.20 10 12 -4 -0.30 1.60 -10 12 4 0.70 1.30 -10 12 4 -0.50 1.30 -10 12 4 1.20 1.90 -8 -12 4 0.30 2.20 8 -12 -4 0.70 1.30 8 -12 -4 1.90 1.70 8 -12 -4 -0.80 1.30 -8 -12 4 0.10 1.50 8 -12 -4 -1.00 2.00 -8 -12 4 0.80 1.50 -8 12 4 1.80 1.40 8 12 -4 0.40 2.10 8 12 -4 -1.90 1.60 -8 12 4 2.10 2.20 8 12 -4 1.90 2.70 -8 12 4 0.50 0.90 8 12 -4 -0.50 1.70 -8 12 4 -0.40 2.00 -6 -12 4 2.20 2.00 6 -12 -4 1.60 1.90 6 -12 -4 2.50 1.40 -6 -12 4 3.40 1.40 -6 -12 4 2.50 1.50 -6 -12 4 3.90 1.80 -6 -12 4 3.20 2.00 6 -12 -4 3.50 1.40 6 -12 -4 4.40 1.80 6 12 -4 2.80 1.50 6 12 -4 0.90 2.10 6 12 -4 2.90 1.60 -6 12 4 3.70 2.20 -6 12 4 3.40 2.10 -6 12 4 3.70 1.50 -6 12 4 3.50 1.40 6 12 -4 3.60 2.70 4 -12 -4 158.68 5.00 -4 -12 4 159.88 5.40 -4 -12 4 160.18 5.00 4 -12 -4 159.38 4.80 -4 -12 4 157.48 4.00 4 -12 -4 163.68 4.30 4 -12 -4 158.68 4.20 -4 -12 4 158.18 3.90 -4 -12 4 164.38 4.60 -4 12 4 157.48 5.30 4 12 -4 159.58 3.80 -4 12 4 169.38 4.30 -4 12 4 164.98 5.20 4 12 -4 165.18 5.80 -4 12 4 155.58 4.10 4 12 -4 158.48 4.80 -2 -12 4 3.90 1.70 -2 -12 4 4.30 1.30 -2 -12 4 5.60 1.80 -2 -12 4 5.50 1.30 -2 -12 4 4.80 2.10 2 12 -4 5.30 1.30 2 12 -4 4.50 2.00 2 12 -4 3.50 1.20 0 -12 -4 36.20 3.50 0 -12 4 34.40 2.10 0 -12 -4 39.10 3.80 0 -12 4 37.10 3.80 0 -12 4 34.70 3.20 0 -12 4 36.30 2.10 0 -12 -4 29.80 3.10 0 -12 4 34.00 3.20 0 -12 -4 37.40 3.20 0 12 4 35.60 3.00 0 12 -4 39.90 3.60 0 12 4 40.20 3.30 0 12 4 33.90 4.20 2 -12 4 11.70 1.90 -2 -12 -4 10.00 1.90 2 -12 4 9.00 2.30 -2 -12 -4 9.90 2.10 -2 -12 -4 13.40 2.50 2 -12 4 9.10 1.90 2 12 4 10.70 2.60 2 12 4 13.10 2.10 2 12 4 10.30 1.90 -4 -12 -4 16.50 2.20 -4 -12 -4 21.20 2.70 4 -12 4 18.10 2.20 -4 -12 -4 18.90 2.10 4 -12 4 25.70 3.20 4 -12 4 19.80 2.60 -4 -12 -4 20.00 2.40 4 12 4 16.00 2.10 4 12 4 17.50 2.80 6 -12 4 91.29 3.90 6 -12 4 89.09 4.40 6 -12 4 94.79 5.10 -6 -12 -4 96.99 4.40 -6 -12 -4 98.09 4.10 -6 -12 -4 90.19 4.30 -6 -12 -4 91.19 4.90 6 12 4 103.09 4.60 6 12 4 101.49 4.30 6 12 4 102.59 5.50 -8 -12 -4 -0.30 2.00 -8 -12 -4 2.70 1.90 8 -12 4 0.60 2.00 8 -12 4 -1.90 2.00 -8 -12 -4 1.70 2.00 8 -12 4 -1.60 1.70 8 12 4 1.40 2.80 8 12 4 1.50 2.00 8 12 4 0.80 2.40 -10 -12 -4 11.10 2.30 10 -12 4 10.20 2.30 10 -12 4 10.70 1.80 -10 -12 -4 6.10 2.30 10 -12 4 10.70 2.20 -10 -12 -4 12.50 3.50 10 12 4 1.10 3.90 10 12 4 13.20 2.70 12 -12 4 12.40 2.40 12 -12 4 11.80 1.80 -12 -12 -4 9.10 2.60 -12 -12 -4 8.70 2.40 12 -12 4 11.80 2.40 -12 -12 -4 12.00 2.50 12 12 4 14.10 2.30 12 12 4 11.00 3.50 12 12 4 7.90 2.50 12 12 4 15.80 2.10 12 12 4 9.90 2.80 -15 -13 4 2.20 2.50 -15 -13 4 4.70 2.40 -15 -13 4 2.10 2.10 15 -13 -4 4.60 2.30 -15 -13 4 4.90 2.10 15 13 -4 1.70 3.00 15 13 -4 3.30 2.40 15 13 -4 5.40 2.10 -13 -13 4 7.60 3.20 -13 -13 4 7.70 2.10 -13 -13 4 6.10 2.50 13 -13 -4 5.70 1.30 13 -13 -4 4.00 2.20 13 13 -4 5.50 2.60 13 13 -4 7.70 4.10 13 13 -4 6.80 2.30 13 13 -4 4.20 3.10 11 -13 -4 4.20 1.80 -11 -13 4 2.60 2.00 11 -13 -4 2.10 2.10 -11 -13 4 3.00 2.30 -11 -13 4 3.30 1.80 -11 -13 4 1.00 1.90 11 -13 -4 6.20 1.40 11 13 -4 1.90 2.00 11 13 -4 0.00 2.80 11 13 -4 -2.10 3.90 11 13 -4 2.20 1.90 -11 13 4 1.70 2.10 -11 13 4 0.30 1.30 9 -13 -4 169.88 4.10 9 -13 -4 171.78 4.80 -9 -13 4 167.98 5.90 -9 -13 4 162.48 5.30 -9 -13 4 170.98 4.70 9 -13 -4 167.98 5.40 -9 13 4 171.38 4.10 9 13 -4 168.48 5.30 9 13 -4 170.48 4.80 9 13 -4 169.78 4.60 9 13 -4 174.78 6.50 -9 13 4 175.98 4.10 -9 13 4 175.68 5.20 7 -13 -4 58.09 3.00 -7 -13 4 59.39 3.30 -7 -13 4 60.69 3.90 7 -13 -4 55.29 4.00 7 -13 -4 62.09 3.60 -7 -13 4 59.99 4.50 -7 -13 4 60.79 3.20 -7 13 4 57.39 3.00 -7 13 4 59.29 4.10 7 13 -4 55.89 3.10 7 13 -4 53.09 4.00 7 13 -4 61.79 5.30 7 13 -4 58.59 3.30 5 -13 -4 150.78 7.70 -5 -13 4 150.68 4.10 -5 -13 4 143.79 4.50 5 -13 -4 145.29 4.10 5 -13 -4 146.69 5.00 5 -13 -4 158.38 4.30 -5 -13 4 143.19 5.50 -5 -13 4 144.09 5.00 5 13 -4 144.09 4.90 -5 13 4 163.48 8.60 5 13 -4 143.79 3.90 -5 13 4 144.89 4.10 5 13 -4 149.79 6.10 -5 13 4 139.99 4.20 -3 -13 4 32.00 3.30 3 -13 -4 32.00 3.70 -3 -13 4 26.20 2.60 3 -13 -4 30.70 3.60 -3 -13 4 32.40 2.60 3 -13 -4 29.90 3.00 -3 -13 4 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-3 9 -0.20 1.90 9 -3 9 -0.10 1.50 -9 -3 -9 -0.70 2.00 9 3 9 0.70 2.20 9 3 9 -0.70 4.40 9 3 9 -1.90 1.80 -9 3 -9 0.40 1.70 9 3 9 -1.20 2.20 -9 3 -9 1.00 1.70 -11 -3 -9 55.99 4.70 11 -3 9 58.89 2.60 11 -3 9 52.19 3.50 11 -3 9 56.99 3.20 -11 -3 -9 51.99 4.00 11 -3 9 59.19 4.70 -11 3 -9 55.19 3.50 11 3 9 57.39 3.10 -11 3 -9 60.89 3.10 11 3 9 53.09 3.70 11 3 9 56.19 5.60 11 3 9 53.09 4.10 -26 -4 9 2.70 2.30 -26 -4 9 4.40 2.30 -26 -4 9 3.20 2.00 26 -4 -9 2.00 2.40 26 -4 -9 5.20 1.90 26 -4 -9 4.00 2.00 -26 -4 9 3.90 2.10 -26 4 9 3.20 2.30 -26 4 9 3.30 2.00 -26 4 9 1.50 1.80 26 4 -9 3.30 2.00 26 4 -9 4.80 2.50 26 4 -9 1.60 3.00 24 -4 -9 56.39 3.70 -24 -4 9 58.69 4.20 -24 -4 9 60.09 4.50 24 -4 -9 49.99 4.30 24 -4 -9 52.09 3.60 -24 -4 9 52.19 3.70 -24 -4 9 48.40 3.80 -24 4 9 57.99 3.80 -24 4 9 52.29 5.60 24 4 -9 49.80 4.90 24 4 -9 54.49 3.90 -24 4 9 54.19 3.70 -22 -4 9 51.79 4.00 22 -4 -9 60.29 4.10 -22 -4 9 54.69 3.70 22 -4 -9 61.59 3.70 22 -4 -9 59.69 3.70 -22 -4 9 53.89 3.50 22 4 -9 57.19 4.20 -22 4 9 58.79 4.00 -22 4 9 60.39 3.70 22 4 -9 58.09 4.80 22 4 -9 54.99 3.80 -22 4 9 57.69 3.50 -20 -4 9 17.80 2.50 -20 -4 9 18.50 3.60 20 -4 -9 15.00 3.40 -20 -4 9 15.50 2.20 -20 -4 9 16.00 2.10 20 -4 -9 14.80 2.00 20 -4 -9 16.60 2.30 -20 4 9 13.40 1.80 -20 4 9 15.40 2.40 20 4 -9 14.50 3.00 20 4 -9 16.90 2.20 -20 4 9 15.50 2.10 20 4 -9 15.90 2.40 18 -4 -9 38.00 3.30 -18 -4 9 35.10 3.90 -18 -4 9 39.20 4.30 -18 -4 9 42.70 3.60 18 -4 -9 32.70 3.50 18 -4 -9 37.00 4.70 -18 -4 9 41.90 3.50 18 -4 -9 46.30 3.40 -18 4 9 40.80 3.30 18 4 -9 38.80 4.20 -18 4 9 37.00 3.70 -18 4 9 44.20 3.10 18 4 -9 35.60 3.40 18 4 -9 45.70 5.00 16 -4 -9 159.38 4.70 -16 -4 9 167.08 4.60 16 -4 -9 156.68 5.00 16 -4 -9 159.68 4.60 -16 -4 9 167.68 4.80 -16 -4 9 171.88 5.10 16 -4 -9 173.18 5.00 -16 -4 9 156.28 5.60 -16 -4 9 156.68 5.30 16 4 -9 168.38 4.80 16 4 -9 165.68 5.60 -16 4 9 158.58 4.70 -16 4 9 162.68 4.50 16 4 -9 166.88 5.00 -16 4 9 155.98 5.10 -14 -4 9 615.24 12.50 14 -4 -9 627.44 11.00 14 -4 -9 599.34 11.10 -14 -4 9 608.54 11.50 -14 -4 9 600.84 11.20 -14 -4 9 597.74 10.80 14 -4 -9 616.14 10.90 14 -4 -9 615.64 10.90 -14 -4 9 609.64 10.90 14 4 -9 600.84 10.90 -14 4 9 611.14 11.20 -14 4 9 619.64 10.90 14 4 -9 606.24 11.70 14 4 -9 613.84 11.00 -14 4 9 604.44 10.90 -14 4 9 614.04 10.90 12 -4 -9 16.30 1.90 -12 -4 9 24.00 2.50 -12 -4 9 22.10 2.20 12 -4 -9 18.70 2.00 -12 -4 9 17.20 2.00 -12 -4 9 15.40 1.80 12 -4 -9 24.80 2.20 12 -4 -9 22.70 2.20 -12 4 9 20.00 1.90 12 4 -9 17.50 2.00 12 4 -9 15.40 2.10 -12 4 9 22.60 2.30 -12 4 9 17.70 2.00 -12 4 9 22.00 2.00 12 4 -9 19.90 2.60 -10 -4 9 106.79 4.30 -10 -4 9 102.29 3.80 10 -4 -9 102.79 3.80 -10 -4 9 107.39 4.00 -10 -4 9 104.59 3.60 -10 -4 9 111.59 4.30 10 -4 -9 110.29 4.10 10 -4 -9 112.69 3.90 10 -4 -9 102.39 3.90 10 4 -9 99.79 3.90 10 4 -9 107.79 4.60 -10 4 9 107.59 4.10 10 4 -9 99.89 3.70 -10 4 9 106.09 3.90 -10 4 9 105.79 3.80 -10 4 9 107.39 3.70 8 -4 -9 9.40 1.80 -8 -4 9 8.70 2.00 8 -4 -9 8.70 1.80 8 -4 -9 9.70 2.00 -8 -4 9 9.40 1.50 -8 -4 9 10.10 1.70 -8 -4 9 13.70 2.10 8 -4 -9 10.00 2.00 -8 -4 9 9.40 1.80 8 4 -9 8.20 2.10 -8 4 9 9.60 1.80 8 4 -9 8.10 1.70 -8 4 9 8.90 1.70 -8 4 9 12.30 2.00 8 4 -9 9.10 1.80 -8 4 9 8.90 1.80 -6 -4 9 1.10 1.80 6 -4 -9 2.80 1.70 -6 -4 9 1.70 1.40 -6 -4 9 1.30 1.50 6 -4 -9 0.50 1.70 -6 -4 9 3.50 1.80 -6 -4 9 2.40 1.70 6 -4 -9 3.00 1.70 6 4 -9 1.10 1.50 6 4 -9 1.10 2.10 6 4 -9 2.30 1.60 -6 4 9 1.30 1.70 -6 4 9 4.60 1.70 -6 4 9 2.50 1.90 4 -4 -9 75.39 3.70 -4 -4 9 77.19 4.00 4 -4 -9 75.59 3.60 -4 -4 9 80.29 3.30 4 -4 -9 79.99 3.60 -4 -4 9 74.79 3.10 -4 -4 9 74.19 3.50 4 -4 -9 77.49 3.60 4 4 -9 77.09 3.30 4 4 -9 78.19 3.30 -4 4 9 77.49 3.50 4 4 -9 73.59 4.30 -4 4 9 76.59 3.60 -4 4 9 75.99 3.60 2 -4 -9 5.20 1.90 2 -4 -9 3.90 1.70 2 -4 -9 4.00 1.70 2 -4 -9 4.10 1.80 -2 -4 9 5.80 1.80 -2 -4 9 5.10 2.10 -2 -4 9 4.70 1.40 -2 -4 9 3.40 1.60 -2 4 9 4.90 1.80 2 4 -9 3.00 1.60 2 4 -9 3.90 1.60 -2 4 9 5.00 1.90 2 4 -9 2.50 2.20 -2 4 9 5.70 1.80 -2 4 9 6.70 2.10 0 -4 9 8.90 1.60 0 -4 -9 0.90 1.80 0 -4 9 5.40 1.40 0 -4 9 6.70 2.00 0 -4 -9 1.10 1.70 0 -4 -9 0.60 1.70 0 -4 9 10.30 3.20 0 4 -9 6.30 2.40 0 4 9 1.40 2.30 0 4 9 -0.50 1.90 0 4 9 1.70 1.70 0 4 -9 8.50 1.60 0 4 9 0.30 1.80 0 4 -9 11.40 1.70 2 -4 9 4.50 2.30 -2 -4 -9 -1.10 2.70 -2 -4 -9 -1.20 1.80 2 -4 9 2.90 1.40 2 -4 9 3.60 1.90 2 -4 9 2.00 1.60 -2 -4 -9 0.70 1.70 -2 4 -9 0.70 1.60 2 4 9 -0.60 1.90 2 4 9 -5.00 2.40 2 4 9 -1.30 1.90 -2 4 -9 4.50 2.40 2 4 9 -2.50 1.80 2 4 9 -0.70 1.70 -2 4 -9 1.20 1.90 4 -4 9 22.80 2.80 -4 -4 -9 14.80 3.40 -4 -4 -9 14.80 2.10 -4 -4 -9 12.60 2.00 4 4 9 10.50 2.00 4 4 9 14.20 2.20 4 4 9 10.90 2.30 4 4 9 10.40 1.90 -6 -4 -9 167.18 4.70 6 -4 9 181.38 4.50 -6 -4 -9 171.78 5.10 6 -4 9 179.48 4.70 -6 -4 -9 171.68 5.30 6 -4 9 176.98 5.90 6 -4 9 165.28 4.40 6 4 9 166.58 6.20 -6 4 -9 181.88 4.70 6 4 9 163.48 5.20 6 4 9 163.68 4.90 6 4 9 168.18 4.80 -6 4 -9 175.08 4.40 6 4 9 164.18 5.40 8 -4 9 5.70 1.60 -8 -4 -9 2.90 2.10 8 -4 9 4.30 1.60 -8 -4 -9 2.80 2.00 -8 -4 -9 4.20 1.80 8 -4 9 6.20 1.70 8 4 9 4.50 3.60 8 4 9 5.00 1.90 -8 4 -9 4.30 1.80 8 4 9 6.60 2.00 8 4 9 6.90 2.50 -8 4 -9 3.70 1.40 8 4 9 3.60 2.10 10 -4 9 13.10 1.60 -10 -4 -9 12.40 2.30 10 -4 9 15.50 1.90 10 -4 9 12.10 2.70 -10 -4 -9 11.10 2.20 10 -4 9 11.90 1.70 10 4 9 8.30 2.50 10 4 9 15.20 3.50 10 4 9 17.60 2.10 -10 4 -9 12.50 1.60 10 4 9 13.30 2.20 10 4 9 15.20 2.40 -10 4 -9 13.30 2.20 -25 -5 9 14.10 2.60 25 -5 -9 18.50 2.20 25 -5 -9 13.80 2.10 -25 -5 9 19.60 2.50 -25 -5 9 15.80 2.60 -25 -5 9 16.90 2.40 25 5 -9 15.90 2.40 -25 5 9 14.00 2.00 25 5 -9 18.60 2.80 -25 5 9 16.70 2.60 -25 5 9 17.50 2.20 25 5 -9 15.50 3.00 23 -5 -9 6.50 2.30 -23 -5 9 7.90 2.20 -23 -5 9 9.90 2.50 23 -5 -9 7.60 1.90 -23 -5 9 8.20 2.10 -23 -5 9 10.70 2.40 23 5 -9 6.00 2.10 -23 5 9 4.40 1.80 -23 5 9 6.30 2.00 23 5 -9 7.50 3.00 23 5 -9 10.70 2.50 -21 -5 9 71.39 3.90 -21 -5 9 71.99 4.30 -21 -5 9 75.09 4.00 21 -5 -9 74.79 4.00 21 -5 -9 73.09 3.80 21 -5 -9 75.59 4.10 21 -5 -9 70.19 3.70 -21 -5 9 73.89 4.40 21 5 -9 78.29 4.10 -21 5 9 72.59 3.80 -21 5 9 75.79 3.60 21 5 -9 70.59 4.40 21 5 -9 74.99 5.00 -21 5 9 71.19 4.20 -19 -5 9 75.59 3.80 19 -5 -9 77.09 3.90 19 -5 -9 77.49 3.70 -19 -5 9 75.19 3.90 -19 -5 9 78.39 5.50 -19 -5 9 82.99 4.10 19 -5 -9 65.69 4.00 19 -5 -9 78.39 4.80 19 5 -9 81.39 4.40 -19 5 9 72.59 4.20 19 5 -9 77.29 4.00 -19 5 9 77.79 3.80 -19 5 9 75.99 3.50 19 5 -9 68.79 4.70 17 -5 -9 326.57 7.00 -17 -5 9 326.47 7.00 -17 -5 9 337.77 7.10 -17 -5 9 332.47 7.40 -17 -5 9 319.47 7.20 17 -5 -9 325.37 7.30 17 -5 -9 337.47 7.00 17 -5 -9 330.07 6.90 -17 -5 9 317.17 7.80 -17 5 9 332.27 7.00 -17 5 9 327.47 6.90 17 5 -9 325.37 7.10 17 5 -9 327.97 7.20 -17 5 9 326.87 7.40 -15 -5 9 207.08 5.30 15 -5 -9 206.38 5.30 15 -5 -9 206.38 5.70 15 -5 -9 208.88 5.30 -15 -5 9 218.18 5.70 -15 -5 9 206.48 5.60 -15 -5 9 203.88 6.00 15 -5 -9 218.98 5.40 -15 -5 9 214.78 5.40 15 5 -9 211.58 5.60 -15 5 9 195.58 5.80 15 5 -9 201.78 6.20 15 5 -9 214.58 5.40 -15 5 9 213.38 5.30 -15 5 9 208.58 5.30 13 -5 -9 438.46 8.80 -13 -5 9 443.96 9.20 13 -5 -9 452.95 8.50 -13 -5 9 440.26 8.50 -13 -5 9 446.16 8.90 -13 -5 9 449.16 8.90 13 -5 -9 449.86 8.60 -13 -5 9 439.06 8.50 13 -5 -9 446.46 8.50 -13 5 9 442.46 8.90 -13 5 9 452.05 8.10 -13 5 9 439.96 8.60 -13 5 9 440.36 8.50 13 5 -9 445.36 9.40 13 5 -9 450.85 8.60 13 5 -9 437.36 8.60 -13 5 9 454.65 8.50 -11 -5 9 116.59 4.00 11 -5 -9 123.09 4.10 -11 -5 9 118.59 4.30 -11 -5 9 124.19 4.40 11 -5 -9 122.39 4.30 -11 -5 9 113.79 3.80 11 -5 -9 122.79 4.10 -11 -5 9 121.99 4.70 11 -5 -9 124.19 4.00 11 5 -9 120.99 4.90 11 5 -9 109.89 4.00 -11 5 9 118.79 3.90 -11 5 9 118.19 3.90 -11 5 9 122.89 4.20 11 5 -9 112.69 4.20 -11 5 9 119.69 4.00 -11 5 9 122.59 4.40 -9 -5 9 70.09 3.10 9 -5 -9 70.09 3.50 9 -5 -9 75.69 3.40 9 -5 -9 73.89 3.60 9 -5 -9 71.99 3.50 -9 -5 9 72.09 4.10 -9 -5 9 66.39 3.40 -9 -5 9 77.09 3.60 -9 -5 9 72.09 3.80 9 5 -9 64.59 3.30 -9 5 9 74.19 3.80 9 5 -9 73.99 3.50 -9 5 9 69.99 3.50 -9 5 9 71.89 3.40 -9 5 9 70.79 3.30 -9 5 9 70.59 3.60 9 5 -9 64.69 4.30 -7 -5 9 50.29 3.00 -7 -5 9 48.50 3.30 -7 -5 9 49.20 3.70 7 -5 -9 48.30 3.20 7 -5 -9 43.70 3.20 -7 -5 9 46.50 2.70 7 -5 -9 44.00 3.00 -7 -5 9 46.30 3.40 7 -5 -9 45.10 3.30 -7 5 9 47.60 3.10 7 5 -9 47.00 3.20 -7 5 9 47.20 3.40 7 5 -9 47.70 3.00 -7 5 9 45.00 3.00 7 5 -9 46.90 4.10 -7 5 9 49.70 3.50 -7 5 9 45.70 3.30 -5 -5 9 46.20 3.30 -5 -5 9 42.40 3.50 5 -5 -9 49.00 3.30 -5 -5 9 40.50 3.40 5 -5 -9 40.60 3.10 -5 -5 9 46.70 2.70 -5 -5 9 44.00 2.90 5 -5 -9 44.20 3.20 5 -5 -9 46.00 3.30 -5 5 9 50.59 3.50 -5 5 9 43.00 3.00 -5 5 9 46.60 3.60 5 5 -9 41.20 4.00 -5 5 9 38.70 3.00 5 5 -9 47.30 3.10 -5 5 9 44.00 3.40 5 5 -9 42.10 2.90 3 -5 -9 412.96 8.10 3 -5 -9 421.16 10.40 -3 -5 9 414.46 7.70 -3 -5 9 408.86 8.10 3 -5 -9 420.56 8.20 -3 -5 9 418.06 7.90 3 -5 -9 420.16 8.30 -3 -5 9 414.36 8.70 -3 -5 9 416.86 8.80 3 5 -9 413.46 7.80 -3 5 9 406.76 8.10 3 5 -9 420.56 7.80 -3 5 9 414.76 8.40 -3 5 9 418.96 8.10 -3 5 9 416.36 8.60 3 5 -9 424.96 9.00 -1 -5 9 42.20 2.70 -1 -5 9 40.60 3.70 1 -5 -9 40.90 3.40 1 -5 -9 40.80 3.40 -1 -5 9 40.50 3.00 1 -5 -9 44.90 3.30 -1 -5 9 38.10 3.10 1 5 -9 40.70 4.20 -1 5 9 39.30 3.20 1 5 -9 39.80 3.00 -1 5 9 43.90 4.00 -1 5 9 39.00 3.20 -1 5 9 44.40 3.50 1 5 -9 39.60 2.90 -1 5 9 37.80 3.40 -1 -5 -9 141.29 4.60 1 -5 9 144.29 3.90 1 -5 9 139.69 5.20 -1 -5 -9 144.39 4.60 1 -5 9 145.19 4.20 -1 -5 -9 142.49 4.60 1 -5 9 151.58 4.40 -1 5 -9 143.79 4.10 1 5 9 140.79 4.70 1 5 9 141.09 4.50 -1 5 -9 143.29 4.00 1 5 9 145.29 4.60 1 5 9 138.79 4.80 1 5 9 147.19 5.40 -1 5 -9 140.59 5.50 3 -5 9 43.30 4.00 -3 -5 -9 38.40 3.30 3 -5 9 41.20 3.50 -3 -5 -9 39.50 3.60 -3 -5 -9 39.80 3.40 3 -5 9 41.20 2.70 3 5 9 39.10 3.70 3 5 9 38.30 3.30 -3 5 -9 41.20 3.00 3 5 9 36.90 3.50 3 5 9 36.10 3.60 -3 5 -9 41.70 2.80 -5 -5 -9 283.77 6.80 5 -5 9 290.07 6.80 5 -5 9 282.77 6.10 5 -5 9 293.37 7.40 5 -5 9 272.57 5.80 -5 -5 -9 289.07 6.40 -5 -5 -9 285.17 6.60 5 5 9 285.07 6.50 5 5 9 281.07 6.90 5 5 9 278.37 7.70 -5 5 -9 279.87 5.90 5 5 9 273.87 6.50 5 5 9 282.07 7.70 -5 5 -9 274.37 5.80 7 -5 9 7.60 1.70 -7 -5 -9 4.90 2.10 7 -5 9 5.20 1.50 -7 -5 -9 6.00 1.90 7 -5 9 5.50 1.70 7 -5 9 7.70 3.20 -7 -5 -9 6.90 2.10 -7 5 -9 6.70 1.70 7 5 9 8.20 2.30 7 5 9 5.20 2.80 7 5 9 3.40 1.90 -7 5 -9 3.40 1.50 7 5 9 4.00 2.10 7 5 9 7.50 2.00 -9 -5 -9 2.70 1.80 -9 -5 -9 0.70 2.00 9 -5 9 -0.10 1.50 9 -5 9 -0.40 1.40 9 -5 9 -0.30 2.50 9 -5 9 -1.50 2.30 -9 -5 -9 -0.60 2.00 -9 5 -9 -1.40 1.80 -9 5 -9 0.00 1.60 9 5 9 1.90 1.90 9 5 9 -2.90 3.00 9 5 9 -2.00 1.90 9 5 9 -1.90 2.20 9 5 9 -0.20 2.40 -24 -6 9 84.19 4.70 -24 -6 9 75.69 4.40 24 -6 -9 76.59 3.90 -24 -6 9 78.09 4.30 24 -6 -9 76.79 4.00 -24 -6 9 75.99 4.50 24 -6 -9 77.99 4.30 -24 6 9 78.79 3.80 24 6 -9 77.79 5.60 -24 6 9 79.09 3.90 -24 6 9 93.89 4.80 24 6 -9 79.59 4.40 22 -6 -9 81.09 4.20 -22 -6 9 81.09 4.20 -22 -6 9 85.69 4.60 -22 -6 9 81.69 4.30 22 -6 -9 85.89 4.30 22 -6 -9 88.59 4.00 -22 -6 9 88.59 4.50 22 -6 -9 83.79 3.90 -22 6 9 89.09 4.60 -22 6 9 88.19 4.10 -22 6 9 80.89 3.90 22 6 -9 86.99 4.30 22 6 -9 85.59 5.40 22 6 -9 87.39 4.80 -20 -6 9 221.48 6.00 -20 -6 9 219.38 6.10 20 -6 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-1 -3 -10 7.70 2.00 1 -3 10 9.60 1.90 -1 3 -10 7.20 1.80 1 3 10 6.00 1.80 -1 3 -10 5.50 1.80 1 3 10 5.90 2.10 -1 3 -10 9.40 2.60 1 3 10 6.00 2.10 3 -3 10 30.30 2.40 -3 -3 -10 36.90 3.50 3 -3 10 31.10 2.90 -3 -3 -10 36.60 3.60 3 -3 10 35.30 3.30 3 -3 10 33.60 4.00 -3 3 -10 35.90 3.20 3 3 10 37.00 3.90 -3 3 -10 36.90 3.30 3 3 10 34.50 3.40 3 3 10 33.90 3.30 3 3 10 34.60 3.30 3 3 10 40.50 3.80 -5 -3 -10 90.49 4.30 5 -3 10 75.89 8.20 5 -3 10 85.79 3.60 5 -3 10 91.59 4.80 5 -3 10 85.69 3.70 -5 -3 -10 83.49 4.10 -5 3 -10 82.29 3.60 5 3 10 89.29 4.40 5 3 10 85.09 4.10 -5 3 -10 88.19 4.00 5 3 10 96.29 5.80 5 3 10 87.29 4.00 5 3 10 86.09 4.60 7 -3 10 50.29 3.60 7 -3 10 50.09 3.10 7 -3 10 51.89 3.20 -7 -3 -10 52.29 4.00 -7 -3 -10 47.00 3.80 7 -3 10 47.20 4.50 7 3 10 48.90 5.40 7 3 10 48.90 4.50 -7 3 -10 45.10 3.50 7 3 10 46.30 4.00 7 3 10 44.70 3.60 7 3 10 55.69 3.60 -7 3 -10 45.80 3.20 -24 -4 10 7.40 2.10 24 -4 -10 7.30 2.10 24 -4 -10 6.20 2.40 24 -4 -10 7.10 2.10 -24 -4 10 9.50 2.30 -24 -4 10 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252.37 7.20 16 -4 -10 248.08 6.30 -16 -4 10 249.97 6.10 16 -4 -10 252.27 6.40 -16 -4 10 251.57 6.80 -16 -4 10 254.37 6.20 16 -4 -10 249.68 6.10 16 -4 -10 259.17 6.00 -16 4 10 247.58 5.90 16 4 -10 249.68 9.90 -16 4 10 253.07 5.20 16 4 -10 250.97 6.10 -16 4 10 249.88 6.10 -16 4 10 231.98 8.70 16 4 -10 256.47 6.30 14 -4 -10 22.50 2.40 14 -4 -10 22.20 2.30 -14 -4 10 22.60 2.20 -14 -4 10 23.90 2.30 -14 -4 10 27.30 2.60 -14 -4 10 22.30 2.30 14 -4 -10 26.00 2.30 -14 -4 10 23.50 2.70 14 -4 -10 23.10 4.30 14 4 -10 22.80 2.30 14 4 -10 24.20 2.40 -14 4 10 24.50 2.60 -14 4 10 21.40 2.70 -14 4 10 25.90 2.40 -14 4 10 21.50 2.10 14 4 -10 23.30 2.90 -12 -4 10 81.39 3.90 -12 -4 10 86.89 4.00 12 -4 -10 84.99 3.90 -12 -4 10 82.49 3.50 -12 -4 10 82.49 3.80 12 -4 -10 86.69 3.90 12 -4 -10 80.29 3.90 12 -4 -10 80.59 3.90 -12 -4 10 78.09 4.30 12 4 -10 80.49 4.70 -12 4 10 84.89 3.70 12 4 -10 76.89 3.70 -12 4 10 86.39 4.00 -12 4 10 84.39 3.80 12 4 -10 79.89 3.90 -12 4 10 85.19 4.20 -10 -4 10 11.60 2.10 -10 -4 10 8.10 1.80 10 -4 -10 7.80 2.00 -10 -4 10 8.30 2.40 10 -4 -10 7.50 2.00 10 -4 -10 8.10 1.80 -10 -4 10 8.00 2.10 -10 -4 10 8.10 1.70 10 4 -10 6.30 2.50 -10 4 10 7.10 1.80 10 4 -10 8.00 2.00 10 4 -10 4.70 1.80 -10 4 10 9.80 2.00 -10 4 10 8.40 2.00 -10 4 10 9.70 2.20 -8 -4 10 55.99 4.00 8 -4 -10 56.19 3.50 -8 -4 10 53.19 3.00 8 -4 -10 48.10 3.50 8 -4 -10 54.59 3.50 -8 -4 10 53.09 3.60 -8 -4 10 53.59 3.30 -8 -4 10 52.29 3.60 8 -4 -10 54.79 3.60 8 4 -10 56.09 3.60 -8 4 10 55.79 3.80 8 4 -10 46.50 4.30 -8 4 10 51.89 3.50 8 4 -10 52.39 3.40 -8 4 10 55.89 3.30 -8 4 10 57.19 3.70 -6 -4 10 337.97 7.80 -6 -4 10 337.77 7.70 -6 -4 10 339.67 7.30 6 -4 -10 334.67 7.40 -6 -4 10 342.27 7.10 6 -4 -10 335.97 7.20 -6 -4 10 342.37 7.00 6 -4 -10 344.37 8.10 6 -4 -10 336.47 7.20 6 4 -10 340.87 7.00 6 4 -10 348.97 8.20 6 4 -10 339.47 7.10 -6 4 10 343.77 7.30 -6 4 10 342.67 7.50 -6 4 10 341.87 7.20 -6 4 10 341.37 7.30 -4 -4 10 903.91 16.50 4 -4 -10 935.51 15.90 4 -4 -10 942.11 16.00 -4 -4 10 931.61 15.90 -4 -4 10 959.60 16.00 -4 -4 10 931.71 15.60 4 -4 -10 957.70 16.00 4 -4 -10 943.31 15.90 4 4 -10 941.21 15.60 -4 4 10 955.10 16.90 -4 4 10 931.11 15.90 -4 4 10 948.81 16.10 4 4 -10 954.40 17.00 -4 4 10 942.91 16.00 4 4 -10 924.01 15.60 2 -4 -10 181.08 5.10 -2 -4 10 173.28 4.60 -2 -4 10 177.98 5.00 2 -4 -10 172.88 5.10 2 -4 -10 179.58 5.10 -2 -4 10 173.38 5.50 -2 -4 10 174.68 5.70 2 4 -10 191.48 7.00 -2 4 10 178.28 5.90 -2 4 10 182.88 5.20 2 4 -10 169.68 4.80 -2 4 10 184.48 5.30 -2 4 10 180.98 5.30 -2 4 10 178.58 5.00 2 4 -10 177.78 4.80 0 -4 -10 18.80 2.20 0 -4 10 19.60 2.20 0 -4 10 17.70 1.90 0 -4 10 17.80 2.70 0 -4 10 19.60 2.10 0 -4 -10 21.80 2.30 0 -4 -10 19.00 2.30 0 4 -10 17.00 2.90 0 4 10 15.50 2.00 0 4 10 19.20 2.30 0 4 10 15.50 4.70 0 4 10 17.30 2.30 0 4 -10 15.20 1.90 0 4 10 15.90 2.30 0 4 -10 19.70 2.00 2 -4 10 58.59 3.50 2 -4 10 62.29 3.50 -2 -4 -10 56.59 3.60 -2 -4 -10 59.79 3.80 2 -4 10 56.49 4.40 -2 -4 -10 65.79 3.80 2 -4 10 59.79 3.20 2 4 10 63.09 3.70 2 4 10 64.19 3.80 2 4 10 60.99 5.00 -2 4 -10 62.59 4.80 -2 4 -10 60.69 3.30 2 4 10 65.69 4.10 -2 4 -10 59.89 3.50 2 4 10 60.09 4.10 4 -4 10 563.64 10.30 -4 -4 -10 568.84 10.50 -4 -4 -10 579.64 10.80 4 -4 10 579.44 10.40 -4 -4 -10 563.04 10.80 4 -4 10 564.84 10.20 4 -4 10 545.55 14.30 4 4 10 581.54 10.70 4 4 10 570.34 11.10 -4 4 -10 549.54 10.20 -4 4 -10 561.44 10.30 4 4 10 553.94 10.70 4 4 10 565.74 10.90 4 4 10 596.84 11.90 6 -4 10 -1.30 1.50 6 -4 10 2.60 1.80 6 -4 10 1.10 2.30 -6 -4 -10 -1.60 1.90 6 -4 10 0.10 1.70 -6 -4 -10 0.80 2.00 -6 -4 -10 0.90 1.90 -6 4 -10 0.70 1.70 6 4 10 -2.20 2.80 6 4 10 1.40 3.50 -6 4 -10 1.20 1.90 6 4 10 2.20 2.10 6 4 10 -0.70 2.30 6 4 10 2.60 1.90 23 -5 -10 182.08 5.50 -23 -5 10 179.08 5.60 -23 -5 10 175.58 5.50 23 -5 -10 184.38 5.80 23 -5 -10 183.58 5.40 -23 -5 10 182.58 5.90 -23 -5 10 180.88 6.50 23 5 -10 179.08 5.70 -23 5 10 198.28 6.10 -23 5 10 175.38 5.20 23 5 -10 190.88 6.80 -23 5 10 184.88 5.50 21 -5 -10 120.79 4.80 -21 -5 10 122.89 4.70 21 -5 -10 122.69 4.60 -21 -5 10 130.69 5.20 -21 -5 10 122.59 4.90 21 -5 -10 117.39 4.60 -21 -5 10 120.19 4.70 21 5 -10 128.59 6.10 21 5 -10 124.59 4.90 -21 5 10 125.09 5.20 -21 5 10 129.09 5.00 21 5 -10 119.29 5.30 -21 5 10 125.89 4.70 -19 -5 10 48.20 4.00 19 -5 -10 44.50 3.60 19 -5 -10 43.60 3.60 -19 -5 10 48.60 4.30 -19 -5 10 41.80 3.70 -19 -5 10 47.80 3.90 19 -5 -10 42.20 3.90 -19 -5 10 44.50 3.60 19 -5 -10 44.60 3.80 -19 5 10 41.00 3.60 19 5 -10 45.80 3.90 -19 5 10 49.80 3.40 19 5 -10 46.70 4.80 19 5 -10 47.00 4.10 -19 5 10 42.60 4.30 17 -5 -10 55.49 3.80 17 -5 -10 48.50 3.90 -17 -5 10 67.09 4.10 -17 -5 10 52.59 3.70 17 -5 -10 53.09 3.60 -17 -5 10 56.39 4.00 -17 -5 10 55.39 4.30 17 -5 -10 55.99 3.60 -17 -5 10 58.49 4.00 -17 5 10 54.49 4.30 -17 5 10 57.59 3.40 17 5 -10 60.79 5.00 -17 5 10 56.79 3.70 17 5 -10 58.79 4.80 17 5 -10 59.39 3.80 -15 -5 10 3.70 1.70 15 -5 -10 1.80 1.80 15 -5 -10 4.50 2.30 -15 -5 10 4.90 2.30 15 -5 -10 0.40 2.10 -15 -5 10 6.10 2.20 -15 -5 10 3.00 1.90 15 5 -10 5.10 2.50 -15 5 10 1.90 2.30 -15 5 10 2.60 1.70 -15 5 10 1.70 1.70 15 5 -10 2.90 1.90 -15 5 10 1.80 1.90 15 5 -10 5.70 2.10 13 -5 -10 309.47 6.80 13 -5 -10 307.57 6.70 13 -5 -10 302.37 6.80 13 -5 -10 298.97 7.00 -13 -5 10 298.77 6.60 -13 -5 10 295.27 7.70 -13 -5 10 301.97 7.10 -13 -5 10 303.27 7.40 -13 5 10 305.77 6.60 -13 5 10 300.37 6.70 13 5 -10 298.17 6.70 13 5 -10 303.77 6.90 -13 5 10 305.87 6.40 -13 5 10 308.17 6.90 11 -5 -10 36.40 3.30 -11 -5 10 36.20 2.90 -11 -5 10 46.50 3.60 11 -5 -10 39.90 3.30 -11 -5 10 35.80 3.50 -11 -5 10 38.20 3.50 -11 -5 10 37.30 3.90 11 -5 -10 42.90 3.60 11 -5 -10 36.80 3.40 11 5 -10 39.30 3.40 -11 5 10 44.50 4.80 11 5 -10 40.30 3.80 11 5 -10 37.00 3.60 -11 5 10 34.40 3.20 -11 5 10 41.80 3.40 -11 5 10 39.90 3.40 -11 5 10 36.90 3.20 -9 -5 10 38.20 3.90 9 -5 -10 38.80 3.30 9 -5 -10 35.40 3.30 -9 -5 10 37.60 3.40 -9 -5 10 38.10 3.00 9 -5 -10 39.10 4.20 -9 -5 10 34.40 3.50 -9 -5 10 44.10 3.50 9 -5 -10 42.30 3.60 -9 5 10 37.60 3.00 -9 5 10 42.90 3.60 -9 5 10 44.50 3.70 -9 5 10 36.70 3.10 9 5 -10 39.30 3.20 9 5 -10 42.60 4.50 9 5 -10 40.90 3.50 -9 5 10 41.30 3.30 -7 -5 10 2.80 1.90 -7 -5 10 3.40 2.20 7 -5 -10 2.80 1.80 -7 -5 10 1.40 1.50 -7 -5 10 2.80 2.00 7 -5 -10 6.30 1.90 7 -5 -10 4.00 1.80 7 -5 -10 4.20 2.00 7 5 -10 3.40 1.80 -7 5 10 5.00 2.20 -7 5 10 4.00 1.90 7 5 -10 2.00 1.70 7 5 -10 1.10 3.20 -7 5 10 2.50 1.80 -7 5 10 1.40 1.70 -7 5 10 4.70 2.20 -5 -5 10 561.14 11.20 5 -5 -10 569.54 10.70 -5 -5 10 565.74 11.20 -5 -5 10 567.84 10.70 5 -5 -10 579.94 10.70 5 -5 -10 576.34 10.60 -5 -5 10 568.64 10.20 5 -5 -10 571.34 10.80 5 5 -10 574.84 10.30 -5 5 10 577.84 10.60 -5 5 10 570.34 10.50 -5 5 10 574.74 11.00 -5 5 10 581.74 10.70 5 5 -10 569.44 14.80 -5 5 10 591.64 11.00 5 5 -10 582.74 10.30 -3 -5 10 6.60 2.40 3 -5 -10 11.50 2.10 3 -5 -10 10.60 2.10 3 -5 -10 10.80 2.10 -3 -5 10 8.40 2.10 -3 -5 10 10.50 2.50 -3 -5 10 10.60 1.70 -3 -5 10 13.30 1.90 3 5 -10 13.00 2.60 -3 5 10 10.40 2.00 3 5 -10 10.30 1.90 -3 5 10 11.10 2.10 -3 5 10 13.40 2.70 3 5 -10 10.80 1.90 -3 5 10 11.00 2.30 1 -5 -10 -1.00 1.80 1 -5 -10 1.30 1.90 -1 -5 10 2.30 1.90 -1 -5 10 -1.40 1.70 -1 -5 10 0.40 1.50 -1 -5 10 0.60 2.20 1 -5 -10 -0.10 2.00 -1 5 10 -1.20 1.70 1 5 -10 -1.30 2.40 1 5 -10 1.40 1.60 -1 5 10 0.00 2.00 -1 5 10 -1.00 1.90 -1 5 10 1.00 1.90 -1 5 10 0.00 2.60 1 5 -10 -0.70 1.60 1 -5 10 3.10 1.90 -1 -5 -10 0.80 1.90 -1 -5 -10 1.40 2.00 1 -5 10 3.20 1.80 1 -5 10 0.00 2.30 -1 -5 -10 2.80 1.90 1 -5 10 3.00 1.50 1 5 10 2.80 2.10 -1 5 -10 1.10 2.60 -1 5 -10 2.60 1.70 1 5 10 -0.80 1.80 1 5 10 -0.30 2.00 1 5 10 0.90 2.60 3 -5 10 229.68 5.50 3 -5 10 208.38 9.20 3 -5 10 227.28 5.60 -3 -5 -10 233.28 6.20 -3 -5 -10 229.48 6.10 3 -5 10 238.98 5.60 -3 -5 -10 237.08 6.00 3 5 10 231.48 6.30 -3 5 -10 233.68 5.50 3 5 10 243.78 7.40 3 5 10 229.08 6.30 -3 5 -10 229.68 5.50 3 5 10 222.78 6.00 3 5 10 242.98 6.10 5 -5 10 158.98 4.80 5 -5 10 163.38 4.70 5 -5 10 167.78 4.80 -5 -5 -10 167.38 5.30 5 -5 10 163.08 6.10 -5 -5 -10 164.28 5.00 5 5 10 167.18 5.80 5 5 10 164.88 6.60 5 5 10 162.28 5.50 5 5 10 155.88 5.20 5 5 10 165.58 5.40 -5 5 -10 157.38 4.30 -22 -6 10 28.80 2.80 22 -6 -10 34.50 3.60 -22 -6 10 30.60 3.40 -22 -6 10 30.30 3.80 22 -6 -10 31.00 3.80 22 -6 -10 36.80 3.90 22 -6 -10 28.90 2.50 -22 -6 10 27.70 2.60 22 6 -10 29.50 2.90 -22 6 10 29.50 3.10 -22 6 10 31.50 2.60 22 6 -10 23.80 4.60 22 6 -10 27.90 3.40 -22 6 10 31.60 3.10 20 -6 -10 19.00 2.40 -20 -6 10 18.10 2.30 -20 -6 10 19.10 2.50 -20 -6 10 22.20 2.80 -20 -6 10 19.10 2.50 20 -6 -10 20.00 2.70 20 -6 -10 22.40 2.30 -20 6 10 26.20 3.00 -20 6 10 16.30 2.30 20 6 -10 20.80 2.50 20 6 -10 16.30 4.70 20 6 -10 20.80 2.70 18 -6 -10 12.60 2.20 -18 -6 10 9.40 2.60 -18 -6 10 15.80 2.60 18 -6 -10 12.10 2.10 -18 -6 10 10.40 2.20 -18 -6 10 13.70 2.40 18 -6 -10 11.50 2.40 -18 -6 10 10.70 2.00 18 -6 -10 11.60 2.00 18 6 -10 16.80 2.80 -18 6 10 11.30 2.20 18 6 -10 13.40 2.30 -18 6 10 13.50 2.00 18 6 -10 11.50 3.10 -18 6 10 10.10 2.60 -16 -6 10 53.29 3.60 16 -6 -10 55.09 3.70 -16 -6 10 54.39 3.80 -16 -6 10 52.29 3.90 16 -6 -10 57.19 3.70 16 -6 -10 44.40 4.00 16 -6 -10 53.69 3.60 -16 -6 10 51.19 4.30 -16 -6 10 53.09 4.00 -16 6 10 57.79 3.90 16 6 -10 50.59 4.90 -16 6 10 42.30 4.40 -16 6 10 53.29 3.60 16 6 -10 54.09 4.20 16 6 -10 57.79 3.90 -14 -6 10 3.80 1.70 14 -6 -10 6.20 2.00 -14 -6 10 8.70 2.30 -14 -6 10 6.10 2.00 -14 -6 10 6.00 2.30 14 -6 -10 6.40 2.10 -14 -6 10 4.80 2.30 14 -6 -10 4.20 1.90 14 -6 -10 6.50 1.90 -14 6 10 5.80 2.00 14 6 -10 1.80 2.10 -14 6 10 6.50 1.90 14 6 -10 5.40 2.50 14 6 -10 4.10 2.00 -14 6 10 3.90 2.40 -14 6 10 8.80 1.90 12 -6 -10 1.20 1.80 -12 -6 10 0.10 1.80 12 -6 -10 -2.50 1.90 -12 -6 10 -1.40 1.60 -12 -6 10 -0.40 2.10 -12 -6 10 0.40 2.00 -12 -6 10 -1.40 2.20 12 -6 -10 0.40 1.70 12 6 -10 -0.80 2.50 -12 6 10 -0.50 1.90 -12 6 10 0.40 1.70 -12 6 10 -1.40 1.80 12 6 -10 -0.80 2.00 -12 6 10 -1.10 1.70 -12 6 10 -3.80 2.10 12 6 -10 -3.50 1.80 10 -6 -10 5.80 2.10 -10 -6 10 0.80 1.60 -10 -6 10 3.70 2.30 10 -6 -10 3.60 1.80 -10 -6 10 5.30 2.40 -10 -6 10 1.50 2.00 -10 -6 10 2.20 1.80 10 -6 -10 3.00 1.90 10 -6 -10 3.50 2.10 -10 6 10 2.90 1.70 10 6 -10 2.30 2.40 -10 6 10 4.40 2.30 10 6 -10 1.50 1.90 -10 6 10 5.20 2.10 10 6 -10 5.50 1.90 -10 6 10 2.80 1.80 -10 6 10 2.10 1.90 -8 -6 10 177.38 4.90 8 -6 -10 184.38 5.40 -8 -6 10 177.98 5.70 -8 -6 10 178.28 4.80 8 -6 -10 184.68 5.20 -8 -6 10 184.28 7.80 8 -6 -10 187.08 5.20 -8 -6 10 177.88 5.80 8 -6 -10 182.78 4.90 -8 6 10 186.58 8.70 8 6 -10 191.28 5.10 -8 6 10 188.18 5.20 8 6 -10 176.58 4.90 8 6 -10 182.28 6.10 -8 6 10 179.28 4.90 -8 6 10 199.08 5.80 6 -6 -10 12.00 2.30 -6 -6 10 13.40 1.80 6 -6 -10 18.00 2.20 -6 -6 10 10.60 2.40 -6 -6 10 12.50 1.90 6 -6 -10 11.90 2.00 6 -6 -10 12.20 2.10 -6 -6 10 10.60 2.30 -6 -6 10 11.90 2.30 6 6 -10 11.60 2.80 -6 6 10 16.10 2.60 -6 6 10 10.90 1.90 6 6 -10 12.20 2.00 -6 6 10 12.60 2.50 6 6 -10 10.20 1.80 -6 6 10 10.80 2.00 -6 6 10 13.00 2.20 -4 -6 10 47.80 3.40 -4 -6 10 42.10 3.90 -4 -6 10 42.40 2.90 4 -6 -10 47.10 3.70 4 -6 -10 51.79 3.70 4 -6 -10 42.00 3.70 -4 -6 10 50.79 3.60 -4 -6 10 46.80 3.90 -4 6 10 48.20 4.40 4 6 -10 45.40 4.60 4 6 -10 49.10 3.30 -4 6 10 48.90 3.40 -4 6 10 42.70 3.90 4 6 -10 41.20 3.30 -4 6 10 45.10 4.20 -4 6 10 46.00 3.40 2 -6 -10 102.39 4.40 2 -6 -10 102.79 4.40 -2 -6 10 105.69 4.20 -2 -6 10 101.19 4.80 -2 -6 10 100.49 4.00 -2 -6 10 97.39 3.60 2 -6 -10 99.79 4.30 -2 -6 10 97.99 4.70 -2 6 10 106.59 5.20 2 6 -10 108.29 5.40 -2 6 10 98.79 4.60 -2 6 10 95.29 6.50 2 6 -10 101.99 3.80 -2 6 10 92.59 4.10 -2 6 10 109.09 4.70 0 -6 -10 2.10 2.10 0 -6 -10 0.20 1.90 0 -6 10 3.10 1.90 0 -6 10 0.10 1.70 0 -6 10 -0.60 2.10 0 -6 10 2.70 2.20 0 -6 -10 0.90 1.90 0 6 -10 2.20 1.60 0 6 10 0.40 2.20 0 6 10 0.20 2.60 0 6 10 3.30 1.90 0 6 10 1.10 1.90 0 6 -10 2.70 2.80 0 6 10 0.60 2.10 0 6 -10 0.90 1.70 -2 -6 -10 3.80 2.10 -2 -6 -10 5.60 2.10 -2 -6 -10 7.60 3.30 2 -6 10 4.90 2.00 2 -6 10 3.20 1.60 2 -6 10 7.10 1.90 2 -6 10 5.40 4.30 2 6 10 6.60 2.90 -2 6 -10 4.90 4.70 -2 6 -10 4.50 1.80 2 6 10 3.50 2.00 2 6 10 3.90 2.40 2 6 10 4.30 2.10 -2 6 -10 3.60 1.60 2 6 10 4.80 2.20 -4 -6 -10 46.40 4.00 -4 -6 -10 42.00 3.70 4 -6 10 42.60 3.70 -4 -6 -10 35.50 3.90 4 -6 10 43.90 3.00 4 -6 10 43.70 3.40 4 -6 10 39.40 4.40 4 6 10 50.89 4.20 4 6 10 39.30 4.10 4 6 10 45.80 3.80 4 6 10 42.20 3.90 4 6 10 48.60 5.50 -4 6 -10 42.20 2.80 21 -7 -10 14.50 2.30 -21 -7 10 14.90 2.50 21 -7 -10 16.90 2.20 -21 -7 10 13.70 2.30 21 -7 -10 18.20 4.60 -21 -7 10 14.20 2.50 21 -7 -10 15.60 2.20 -21 -7 10 20.60 2.90 -21 7 10 14.40 2.30 21 7 -10 11.50 2.70 -21 7 10 18.10 4.60 21 7 -10 16.00 2.50 21 7 -10 10.70 3.30 -21 7 10 12.90 2.00 -19 -7 10 44.10 4.20 19 -7 -10 42.30 3.60 -19 -7 10 47.30 3.80 19 -7 -10 42.50 3.60 -19 -7 10 44.10 4.00 -19 -7 10 44.90 5.20 -19 -7 10 47.50 4.70 19 -7 -10 48.20 3.70 19 -7 -10 44.70 4.10 -19 7 10 43.00 3.40 -19 7 10 43.10 4.60 -19 7 10 43.40 3.80 19 7 -10 42.50 4.40 19 7 -10 47.60 6.00 17 -7 -10 1.70 1.90 17 -7 -10 0.70 1.90 -17 -7 10 -0.80 2.00 -17 -7 10 -0.10 2.40 -17 -7 10 -2.50 2.10 17 -7 -10 0.50 2.20 -17 -7 10 1.70 2.30 17 -7 -10 -1.20 1.90 -17 7 10 0.20 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84.79 4.90 -8 -4 12 91.39 5.40 -8 4 12 67.99 6.30 8 4 -12 77.09 4.10 -8 4 12 82.59 4.50 8 4 -12 83.59 5.40 -8 4 12 83.39 4.30 8 4 -12 76.49 4.20 -8 4 12 82.79 4.40 6 -4 -12 37.20 3.90 6 -4 -12 33.10 2.80 -6 -4 12 35.90 3.00 -6 -4 12 33.80 2.70 -6 -4 12 36.40 4.30 -6 -4 12 34.10 4.20 -6 -4 12 36.10 3.40 6 4 -12 35.10 3.60 6 4 -12 30.40 3.60 6 4 -12 25.90 2.50 -6 4 12 35.60 3.90 -6 4 12 31.60 2.70 -6 4 12 29.80 2.80 -4 -4 12 -0.80 2.30 4 -4 -12 1.40 3.70 -4 -4 12 1.40 1.80 4 -4 -12 2.40 2.10 -4 -4 12 1.90 2.30 -4 -4 12 1.10 2.20 -4 -4 12 -1.10 1.90 -4 4 12 -1.00 2.10 -4 4 12 0.20 1.90 -4 4 12 -0.10 2.70 4 4 -12 -1.80 1.90 4 4 -12 -1.10 1.80 -4 4 12 -2.30 4.10 -4 4 12 0.30 2.10 4 4 -12 -0.60 2.90 -17 -5 12 194.28 5.70 -17 -5 12 199.28 6.00 17 -5 -12 199.88 6.10 17 -5 -12 192.38 5.90 -17 -5 12 187.08 6.00 -17 -5 12 194.78 6.60 -17 -5 12 194.28 6.40 17 -5 -12 190.48 5.80 -17 5 12 194.58 6.00 -17 5 12 205.78 6.70 17 5 -12 191.78 5.90 17 5 -12 187.38 7.00 -17 5 12 201.48 5.30 -17 5 12 183.48 4.90 17 5 -12 194.38 6.20 -15 -5 12 6.20 2.20 -15 -5 12 3.40 2.50 -15 -5 12 6.40 2.10 15 -5 -12 8.30 2.50 15 -5 -12 5.50 2.20 -15 -5 12 6.70 2.50 15 -5 -12 7.20 2.80 -15 -5 12 5.70 2.30 15 -5 -12 6.70 2.30 -15 5 12 5.60 2.70 -15 5 12 7.20 4.40 -15 5 12 4.30 2.00 -15 5 12 6.90 2.30 15 5 -12 5.50 2.30 -15 5 12 4.60 2.10 15 5 -12 4.80 3.00 15 5 -12 3.60 2.20 13 -5 -12 20.00 2.50 13 -5 -12 23.70 2.90 -13 -5 12 16.80 2.60 13 -5 -12 17.00 2.50 13 -5 -12 20.00 2.70 -13 -5 12 24.30 2.90 -13 -5 12 24.10 2.90 -13 -5 12 22.50 2.50 -13 -5 12 22.20 2.30 -13 5 12 23.30 3.00 13 5 -12 19.30 2.50 -13 5 12 19.50 2.60 13 5 -12 20.10 3.40 -13 5 12 23.20 2.50 -13 5 12 23.70 2.70 13 5 -12 21.20 2.80 -13 5 12 17.80 3.60 -11 -5 12 185.48 8.80 11 -5 -12 180.28 5.90 11 -5 -12 180.78 5.60 11 -5 -12 179.88 5.60 -11 -5 12 169.08 5.20 -11 -5 12 181.68 5.60 -11 -5 12 178.38 5.80 -11 -5 12 174.28 6.30 11 -5 -12 179.38 5.70 -11 5 12 180.68 6.70 11 5 -12 175.58 5.50 -11 5 12 186.68 6.20 -11 5 12 177.48 5.40 -11 5 12 182.58 5.80 -11 5 12 187.48 6.20 11 5 -12 177.88 6.70 11 5 -12 167.88 5.40 9 -5 -12 -1.20 2.10 -9 -5 12 0.60 2.40 -9 -5 12 1.20 1.80 -9 -5 12 3.00 2.00 -9 -5 12 1.70 2.40 9 -5 -12 -1.00 2.20 9 -5 -12 1.60 2.10 -9 -5 12 2.90 2.50 9 -5 -12 0.70 2.10 -9 5 12 1.40 2.00 9 5 -12 -1.90 2.00 -9 5 12 -0.30 2.10 9 5 -12 1.50 3.00 -9 5 12 0.20 2.60 9 5 -12 5.10 2.10 -9 5 12 1.10 2.00 -9 5 12 0.70 2.50 7 -5 -12 3.00 2.20 -7 -5 12 3.80 2.10 7 -5 -12 1.80 2.30 -7 -5 12 0.10 2.20 7 -5 -12 5.40 2.20 -7 -5 12 2.40 2.50 7 -5 -12 5.30 2.20 -7 -5 12 1.90 1.70 7 5 -12 0.80 2.00 -7 5 12 1.30 2.70 7 5 -12 1.80 2.00 -7 5 12 5.10 2.10 -7 5 12 4.20 2.60 -7 5 12 0.50 2.10 7 5 -12 1.60 2.80 -7 5 12 0.90 1.90 -5 -5 12 27.70 2.60 -5 -5 12 23.80 2.80 5 -5 -12 31.90 2.80 5 -5 -12 30.70 3.00 -5 -5 12 31.40 3.40 -5 -5 12 26.00 2.90 -5 -5 12 26.50 2.30 5 -5 -12 25.40 2.80 5 5 -12 26.40 3.40 5 5 -12 22.90 2.30 -5 5 12 24.20 2.50 -5 5 12 25.50 2.70 -5 5 12 32.60 3.50 -5 5 12 28.20 3.10 -5 5 12 24.70 2.70 5 5 -12 29.40 2.40 12 -6 -12 12.50 2.40 -12 -6 12 16.40 2.40 -12 -6 12 19.00 2.30 -12 -6 12 17.10 2.80 -12 -6 12 16.00 2.70 12 -6 -12 13.40 2.40 12 -6 -12 14.50 2.50 12 -6 -12 17.20 2.40 -12 -6 12 13.50 2.60 12 6 -12 12.30 2.30 -12 6 12 15.80 2.30 -12 6 12 22.20 2.80 -12 6 12 16.40 2.30 12 6 -12 16.40 2.50 12 6 -12 10.50 3.10 -12 6 12 21.40 3.00 -12 6 12 18.00 2.60 10 -6 -12 5.90 2.50 10 -6 -12 2.30 2.10 -10 -6 12 3.30 2.50 -10 -6 12 5.40 2.10 -10 -6 12 0.80 1.80 10 -6 -12 -0.40 2.10 10 -6 -12 2.40 2.50 -10 -6 12 4.00 2.30 -10 -6 12 2.40 2.40 -10 6 12 2.60 2.60 10 6 -12 2.40 2.80 10 6 -12 1.70 2.00 -10 6 12 3.20 2.00 -10 6 12 4.80 2.70 10 6 -12 1.00 2.00 -10 6 12 1.30 2.00 12 0 -13 -3.90 2.40 -12 0 13 -1.00 2.20 -12 0 13 0.10 2.50 -12 0 13 -2.00 2.30 -12 0 13 -1.00 2.00 12 0 -13 -1.90 2.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 62507 _shelx_res_file ; TITL R-269 in C2/c shelx.res created by SHELXL-2018/3 at 14:52:52 on 03-Jun-2021 CELL 0.71073 24.2097 12.6311 10.4022 90.000 113.133 90.000 ZERR 8.00 0.0011 0.0006 0.0005 0.000 0.002 0.000 LATT 7 SYMM - X, Y, 1/2 - Z SFAC C H N O UNIT 112 96 32 57.79 MERG 2 ISOR 0.01 OW1 FMAP 2 PLAN 3 SIZE 0.270 0.320 0.340 ACTA BOND $H CONF LIST 4 L.S. 13 TEMP -123.00 WGHT 0.058600 2.107700 FVAR 0.50764 0.22417 C1 1 0.370569 0.394232 0.829091 11.00000 0.01576 0.02118 = 0.01866 -0.00006 0.00538 -0.00076 C2 1 0.378334 0.399023 0.976483 11.00000 0.01836 0.02326 = 0.02034 -0.00260 0.00745 -0.00223 C3 1 0.486935 0.377423 1.042696 11.00000 0.01922 0.02367 = 0.01791 -0.00027 0.00542 0.00088 C4 1 0.422789 0.383654 0.793606 11.00000 0.01657 0.01982 = 0.01746 0.00101 0.00465 -0.00016 C5 1 0.241655 0.383444 0.508326 11.00000 0.01566 0.01952 = 0.01929 0.00163 0.00338 -0.00031 C6 1 0.231296 0.377940 0.367164 11.00000 0.01881 0.02198 = 0.02087 0.00183 0.00814 0.00061 AFIX 43 H6 2 0.263906 0.380695 0.338172 11.00000 -1.20000 AFIX 0 C7 1 0.172539 0.368336 0.268736 11.00000 0.02031 0.01976 = 0.01769 0.00103 0.00614 0.00055 C8 1 0.124589 0.365389 0.310788 11.00000 0.01706 0.02108 = 0.01890 0.00031 0.00344 -0.00017 AFIX 43 H8 2 0.084612 0.358679 0.243355 11.00000 -1.20000 AFIX 0 C9 1 0.135693 0.372367 0.452775 11.00000 0.01730 0.02232 = 0.01933 0.00062 0.00609 -0.00074 C10 1 0.194226 0.381110 0.552816 11.00000 0.01975 0.02290 = 0.01723 0.00057 0.00612 -0.00063 AFIX 43 H10 2 0.201704 0.385399 0.649417 11.00000 -1.20000 AFIX 0 C11 1 0.158589 0.359366 0.115625 11.00000 0.02103 0.02220 = 0.01918 0.00106 0.00697 0.00077 C12 1 0.196999 0.351820 -0.059775 11.00000 0.02530 0.03647 = 0.01803 0.00081 0.00922 0.00027 AFIX 137 H12A 2 0.177183 0.284238 -0.096410 11.00000 -1.50000 H12B 2 0.235389 0.355077 -0.070599 11.00000 -1.50000 H12C 2 0.171209 0.410245 -0.111573 11.00000 -1.50000 AFIX 0 C13 1 0.082359 0.370781 0.492199 11.00000 0.01852 0.02947 = 0.01924 0.00018 0.00530 -0.00064 C14 1 0.046710 0.398309 0.669918 11.00000 0.02208 0.04620 = 0.02625 -0.00355 0.01207 -0.00231 AFIX 137 H14A 2 0.022390 0.461429 0.630597 11.00000 -1.50000 H14B 2 0.062181 0.401216 0.772194 11.00000 -1.50000 H14C 2 0.021864 0.334851 0.636695 11.00000 -1.50000 AFIX 0 N1 3 0.437157 0.388980 1.072293 11.00000 0.01838 0.03103 = 0.01407 -0.00229 0.00539 -0.00014 AFIX 3 H1N 2 0.445330 0.388946 1.160377 11.00000 0.02563 AFIX 0 N2 3 0.477520 0.374825 0.903404 11.00000 0.01492 0.03041 = 0.01671 0.00053 0.00563 0.00253 AFIX 3 H2N 2 0.510968 0.367522 0.886519 11.00000 0.03249 AFIX 0 N3 3 0.314160 0.394564 0.737710 11.00000 0.01743 0.02188 = 0.01814 -0.00009 0.00526 -0.00072 N4 3 0.301735 0.389516 0.604886 11.00000 0.01530 0.02701 = 0.01756 0.00169 0.00553 -0.00049 AFIX 3 H4N 2 0.329280 0.391432 0.572748 11.00000 0.04086 AFIX 0 O1 4 0.338090 0.411064 1.017066 11.00000 0.01920 0.04394 = 0.02438 -0.00656 0.01079 -0.00263 O2 4 0.537680 0.371909 1.133923 11.00000 0.01896 0.04414 = 0.01691 -0.00043 0.00317 0.00425 O3 4 0.419465 0.381633 0.671721 11.00000 0.01778 0.03438 = 0.01606 0.00143 0.00618 -0.00011 O4 4 0.108267 0.350769 0.027761 11.00000 0.02113 0.05102 = 0.01874 -0.00279 0.00561 -0.00238 O5 4 0.207732 0.360600 0.087909 11.00000 0.02045 0.03702 = 0.01719 0.00147 0.00708 0.00080 O6 4 0.032576 0.350682 0.411526 11.00000 0.01748 0.08528 = 0.02521 -0.01300 0.00692 -0.00853 O7 4 0.096679 0.394500 0.625829 11.00000 0.01896 0.04977 = 0.01928 -0.00375 0.00802 -0.00375 OW1 4 0.346255 0.348399 0.315062 21.00000 0.03100 0.05622 = 0.05811 0.00407 0.02352 0.00112 HKLF 4 REM R-269 in C2/c REM wR2 = 0.1022, GooF = S = 1.041, Restrained GooF = 1.040 for all data REM R1 = 0.0340 for 2699 Fo > 4sig(Fo) and 0.0371 for all 2944 data REM 241 parameters refined using 6 restraints END WGHT 0.0586 2.1077 REM Highest difference peak 0.286, deepest hole -0.210, 1-sigma level 0.037 Q1 1 0.1687 0.3646 0.2005 11.00000 0.05 0.29 Q2 1 0.1101 0.3683 0.4752 11.00000 0.05 0.28 Q3 1 0.3952 0.3900 0.8195 11.00000 0.05 0.27 ; _shelx_res_checksum 30265 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.37057(5) 0.39423(9) 0.82909(12) 0.0190(2) Uani d 1 . . C C2 0.37833(5) 0.39902(9) 0.97648(12) 0.0207(2) Uani d 1 . . C C3 0.48693(5) 0.37742(9) 1.04270(12) 0.0208(2) Uani d 1 . . C C4 0.42279(5) 0.38365(8) 0.79361(12) 0.0186(2) Uani d 1 . . C C5 0.24165(5) 0.38344(8) 0.50833(12) 0.0192(2) Uani d 1 . . C C6 0.23130(5) 0.37794(9) 0.36716(12) 0.0204(2) Uani d 1 . . H H6 0.263906 0.380695 0.338172 0.025 Uiso calc 1 . . C C7 0.17254(5) 0.36834(9) 0.26874(11) 0.0197(2) Uani d 1 . . C C8 0.12459(5) 0.36539(9) 0.31079(12) 0.0201(2) Uani d 1 . . H H8 0.084612 0.358679 0.243355 0.024 Uiso calc 1 . . C C9 0.13569(5) 0.37237(9) 0.45277(12) 0.0200(2) Uani d 1 . . C C10 0.19423(5) 0.38111(9) 0.55282(12) 0.0203(2) Uani d 1 . . H H10 0.201704 0.385399 0.649417 0.024 Uiso calc 1 . . C C11 0.15859(5) 0.35937(9) 0.11562(12) 0.0211(2) Uani d 1 . . C C12 0.19700(5) 0.35182(11) -0.05977(12) 0.0264(3) Uani d 1 . . H H12A 0.177183 0.284238 -0.096410 0.040 Uiso calc 1 . . H H12B 0.235389 0.355077 -0.070599 0.040 Uiso calc 1 . . H H12C 0.171209 0.410245 -0.111573 0.040 Uiso calc 1 . . C C13 0.08236(5) 0.37078(10) 0.49220(12) 0.0231(3) Uani d 1 . . C C14 0.04671(6) 0.39831(12) 0.66992(14) 0.0307(3) Uani d 1 . . H H14A 0.022390 0.461429 0.630597 0.046 Uiso calc 1 . . H H14B 0.062181 0.401216 0.772194 0.046 Uiso calc 1 . . H H14C 0.021864 0.334851 0.636695 0.046 Uiso calc 1 . . N N1 0.43716(4) 0.38898(8) 1.07229(10) 0.0215(2) Uani d 1 . . H H1N 0.445330 0.388946 1.160377 0.026(4) Uiso d 1 . . N N2 0.47752(4) 0.37483(8) 0.90340(10) 0.0209(2) Uani d 1 . . H H2N 0.510968 0.367522 0.886519 0.032(4) Uiso d 1 . . N N3 0.31416(4) 0.39456(7) 0.73771(10) 0.0197(2) Uani d 1 . . N N4 0.30173(4) 0.38952(8) 0.60489(10) 0.0202(2) Uani d 1 . . H H4N 0.329280 0.391432 0.572748 0.041(5) Uiso d 1 . . O O1 0.33809(4) 0.41106(8) 1.01707(9) 0.0285(2) Uani d 1 . . O O2 0.53768(4) 0.37191(8) 1.13392(9) 0.0279(2) Uani d 1 . . O O3 0.41946(4) 0.38163(7) 0.67172(8) 0.0229(2) Uani d 1 . . O O4 0.10827(4) 0.35077(8) 0.02776(9) 0.0310(2) Uani d 1 . . O O5 0.20773(4) 0.36060(7) 0.08791(8) 0.0250(2) Uani d 1 . . O O6 0.03258(4) 0.35068(10) 0.41153(10) 0.0431(3) Uani d 1 . . O O7 0.09668(4) 0.39450(8) 0.62583(9) 0.0292(2) Uani d 1 . . O OW1 0.3463(2) 0.3484(4) 0.3151(6) 0.0466(19) Uani d 0.224(5) . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0158(5) 0.0212(5) 0.0187(5) -0.0008(4) 0.0054(4) -0.0001(4) C2 0.0184(5) 0.0233(6) 0.0203(6) -0.0022(4) 0.0074(5) -0.0026(4) C3 0.0192(5) 0.0237(6) 0.0179(5) 0.0009(4) 0.0054(4) -0.0003(4) C4 0.0166(5) 0.0198(5) 0.0175(5) -0.0002(4) 0.0047(4) 0.0010(4) C5 0.0157(5) 0.0195(5) 0.0193(5) -0.0003(4) 0.0034(4) 0.0016(4) C6 0.0188(5) 0.0220(5) 0.0209(6) 0.0006(4) 0.0081(4) 0.0018(4) C7 0.0203(5) 0.0198(5) 0.0177(6) 0.0005(4) 0.0061(4) 0.0010(4) C8 0.0171(5) 0.0211(5) 0.0189(5) -0.0002(4) 0.0034(4) 0.0003(4) C9 0.0173(5) 0.0223(5) 0.0193(5) -0.0007(4) 0.0061(4) 0.0006(4) C10 0.0197(5) 0.0229(5) 0.0172(5) -0.0006(4) 0.0061(4) 0.0006(4) C11 0.0210(5) 0.0222(5) 0.0192(5) 0.0008(4) 0.0070(4) 0.0011(4) C12 0.0253(6) 0.0365(7) 0.0180(6) 0.0003(5) 0.0092(5) 0.0008(5) C13 0.0185(6) 0.0295(6) 0.0192(5) -0.0006(4) 0.0053(4) 0.0002(4) C14 0.0221(6) 0.0462(8) 0.0262(6) -0.0023(5) 0.0121(5) -0.0036(5) N1 0.0184(5) 0.0310(5) 0.0141(5) -0.0001(4) 0.0054(4) -0.0023(4) N2 0.0149(5) 0.0304(5) 0.0167(5) 0.0025(4) 0.0056(4) 0.0005(4) N3 0.0174(5) 0.0219(5) 0.0181(5) -0.0007(3) 0.0053(4) -0.0001(3) N4 0.0153(5) 0.0270(5) 0.0176(5) -0.0005(3) 0.0055(4) 0.0017(4) O1 0.0192(4) 0.0439(5) 0.0244(4) -0.0026(4) 0.0108(3) -0.0066(4) O2 0.0190(4) 0.0441(5) 0.0169(4) 0.0043(4) 0.0032(3) -0.0004(3) O3 0.0178(4) 0.0344(5) 0.0161(4) -0.0001(3) 0.0062(3) 0.0014(3) O4 0.0211(4) 0.0510(6) 0.0187(4) -0.0024(4) 0.0056(3) -0.0028(4) O5 0.0204(4) 0.0370(5) 0.0172(4) 0.0008(3) 0.0071(3) 0.0015(3) O6 0.0175(4) 0.0853(8) 0.0252(5) -0.0085(5) 0.0069(4) -0.0130(5) O7 0.0190(4) 0.0498(6) 0.0193(4) -0.0038(4) 0.0080(3) -0.0038(4) OW1 0.031(3) 0.056(3) 0.058(3) 0.001(2) 0.024(2) 0.004(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N3 C1 C4 . . 124.93(10) ? N3 C1 C2 . . 114.97(10) ? C4 C1 C2 . . 120.00(10) ? O1 C2 N1 . . 119.97(10) ? O1 C2 C1 . . 125.19(10) ? N1 C2 C1 . . 114.84(9) ? O2 C3 N1 . . 122.53(10) ? O2 C3 N2 . . 121.04(10) ? N1 C3 N2 . . 116.41(10) ? O3 C4 N2 . . 120.22(10) ? O3 C4 C1 . . 123.21(10) ? N2 C4 C1 . . 116.56(10) ? C6 C5 C10 . . 121.20(10) ? C6 C5 N4 . . 117.59(10) ? C10 C5 N4 . . 121.20(10) ? C5 C6 C7 . . 119.25(10) ? C5 C6 H6 . . 120.4 ? C7 C6 H6 . . 120.4 ? C8 C7 C6 . . 120.52(10) ? C8 C7 C11 . . 117.69(10) ? C6 C7 C11 . . 121.79(10) ? C7 C8 C9 . . 119.52(10) ? C7 C8 H8 . . 120.2 ? C9 C8 H8 . . 120.2 ? C10 C9 C8 . . 120.75(11) ? C10 C9 C13 . . 121.89(10) ? C8 C9 C13 . . 117.35(10) ? C9 C10 C5 . . 118.75(10) ? C9 C10 H10 . . 120.6 ? C5 C10 H10 . . 120.6 ? O4 C11 O5 . . 124.04(10) ? O4 C11 C7 . . 123.45(10) ? O5 C11 C7 . . 112.50(9) ? O5 C12 H12A . . 109.5 ? O5 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? O5 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? O6 C13 O7 . . 124.04(11) ? O6 C13 C9 . . 123.36(11) ? O7 C13 C9 . . 112.60(9) ? O7 C14 H14A . . 109.5 ? O7 C14 H14B . . 109.5 ? H14A C14 H14B . . 109.5 ? O7 C14 H14C . . 109.5 ? H14A C14 H14C . . 109.5 ? H14B C14 H14C . . 109.5 ? C3 N1 C2 . . 126.63(9) ? C3 N1 H1N . . 112.8 ? C2 N1 H1N . . 120.6 ? C4 N2 C3 . . 125.51(10) ? C4 N2 H2N . . 119.7 ? C3 N2 H2N . . 114.8 ? N4 N3 C1 . . 120.55(10) ? N3 N4 C5 . . 120.38(9) ? N3 N4 H4N . . 121.7 ? C5 N4 H4N . . 117.9 ? C11 O5 C12 . . 115.04(9) ? C13 O7 C14 . . 115.50(9) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 N3 . 1.3223(15) ? C1 C4 . 1.4557(16) ? C1 C2 . 1.4708(15) ? C2 O1 . 1.2140(14) ? C2 N1 . 1.3864(14) ? C3 O2 . 1.2242(14) ? C3 N1 . 1.3638(15) ? C3 N2 . 1.3759(15) ? C4 O3 . 1.2387(14) ? C4 N2 . 1.3724(14) ? C5 C6 . 1.3909(16) ? C5 C10 . 1.3968(16) ? C5 N4 . 1.4080(14) ? C6 C7 . 1.3936(16) ? C6 H6 . 0.9500 ? C7 C8 . 1.3926(16) ? C7 C11 . 1.4970(15) ? C8 C9 . 1.3963(16) ? C8 H8 . 0.9500 ? C9 C10 . 1.3945(16) ? C9 C13 . 1.5006(16) ? C10 H10 . 0.9500 ? C11 O4 . 1.2068(14) ? C11 O5 . 1.3298(14) ? C12 O5 . 1.4581(14) ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 O6 . 1.1944(15) ? C13 O7 . 1.3280(15) ? C14 O7 . 1.4533(14) ? C14 H14A . 0.9800 ? C14 H14B . 0.9800 ? C14 H14C . 0.9800 ? N1 H1N . 0.8580 ? N2 H2N . 0.8982 ? N3 N4 . 1.2950(14) ? N4 H4N . 0.8557 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N O2 2_657 0.86 2.03 2.8800(13) 174 yes N2 H2N O3 2_656 0.90 2.01 2.8931(15) 168 yes N4 H4N O3 . 0.86 2.02 2.6571(15) 131 yes N4 H4N O1 6_565 0.86 2.59 2.9302(14) 105 no C6 H6 Ow1 . 0.95 2.14 3.061(6) 163 yes C12 H12B O1 1_554 0.98 2.39 3.2743(17) 149 yes C14 H14B O4 1_556 0.98 2.53 3.4754(16) 163 yes C12 H12C Cg2 6_565 0.98 2.73 3.4717(15) 133 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N3 C1 C2 O1 . . . . -5.85(17) ? C4 C1 C2 O1 . . . . 177.58(11) ? N3 C1 C2 N1 . . . . 174.41(9) ? C4 C1 C2 N1 . . . . -2.17(15) ? N3 C1 C4 O3 . . . . 5.51(18) ? C2 C1 C4 O3 . . . . -178.27(10) ? N3 C1 C4 N2 . . . . -173.94(10) ? C2 C1 C4 N2 . . . . 2.27(15) ? C10 C5 C6 C7 . . . . -0.97(16) ? N4 C5 C6 C7 . . . . 177.91(10) ? C5 C6 C7 C8 . . . . 0.67(16) ? C5 C6 C7 C11 . . . . -178.47(10) ? C6 C7 C8 C9 . . . . 0.14(16) ? C11 C7 C8 C9 . . . . 179.32(10) ? C7 C8 C9 C10 . . . . -0.68(16) ? C7 C8 C9 C13 . . . . 178.92(10) ? C8 C9 C10 C5 . . . . 0.40(16) ? C13 C9 C10 C5 . . . . -179.18(10) ? C6 C5 C10 C9 . . . . 0.43(16) ? N4 C5 C10 C9 . . . . -178.40(10) ? C8 C7 C11 O4 . . . . 0.70(17) ? C6 C7 C11 O4 . . . . 179.87(11) ? C8 C7 C11 O5 . . . . -178.51(10) ? C6 C7 C11 O5 . . . . 0.66(15) ? C10 C9 C13 O6 . . . . -170.65(13) ? C8 C9 C13 O6 . . . . 9.75(18) ? C10 C9 C13 O7 . . . . 9.60(16) ? C8 C9 C13 O7 . . . . -170.00(10) ? O2 C3 N1 C2 . . . . 177.97(11) ? N2 C3 N1 C2 . . . . -0.46(17) ? O1 C2 N1 C3 . . . . -178.47(11) ? C1 C2 N1 C3 . . . . 1.29(17) ? O3 C4 N2 C3 . . . . 179.07(11) ? C1 C4 N2 C3 . . . . -1.46(16) ? O2 C3 N2 C4 . . . . -177.92(11) ? N1 C3 N2 C4 . . . . 0.53(17) ? C4 C1 N3 N4 . . . . -2.91(17) ? C2 C1 N3 N4 . . . . -179.30(9) ? C1 N3 N4 C5 . . . . 176.15(10) ? C6 C5 N4 N3 . . . . -179.84(10) ? C10 C5 N4 N3 . . . . -0.97(16) ? O4 C11 O5 C12 . . . . 0.65(16) ? C7 C11 O5 C12 . . . . 179.85(9) ? O6 C13 O7 C14 . . . . -1.96(19) ? C9 C13 O7 C14 . . . . 177.79(10) ? _cod_database_fobs_code 2243860