#------------------------------------------------------------------------------ #$Date: 2021-07-01 08:11:34 +0300 (Thu, 01 Jul 2021) $ #$Revision: 266841 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243860.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243860 _cell_angle_alpha 90.000 _cell_angle_beta 113.133 _cell_angle_gamma 90.000 _cell_length_a 24.2097 _cell_length_b 12.6311 _cell_length_c 10.4022 _exptl_crystal_F_000 1454.32 _reflns_d_resolution_high 0.7998 _cod_data_source_file yk2153Isup2.hkl _cod_data_source_block I _shelx_title ' R-269 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 592.83 530.92 7.25 o 8 0 0 10147.35 9162.52 137.37 o 10 0 0 2616.20 2522.51 17.87 o 12 0 0 1182.90 1523.58 12.16 o 14 0 0 2722.99 2683.56 19.33 o 16 0 0 126.36 142.64 3.88 o 18 0 0 4913.76 4913.71 144.80 o 20 0 0 526.11 478.88 6.48 o 22 0 0 826.57 834.98 8.84 o 24 0 0 1208.35 1248.78 11.62 o 26 0 0 673.80 743.88 9.08 o 5 1 0 172.22 114.31 1.78 o 7 1 0 3249.90 3020.75 37.17 o 9 1 0 9315.25 9633.98 116.80 o 11 1 0 775.97 825.00 4.94 o 13 1 0 931.47 832.04 5.17 o 15 1 0 3021.12 3096.68 15.71 o 17 1 0 69.91 71.90 2.14 o 19 1 0 839.58 890.75 10.82 o 21 1 0 2031.98 2070.00 11.62 o 23 1 0 19.87 19.00 2.08 o 25 1 0 7.90 4.11 2.12 o 27 1 0 135.24 173.67 4.28 o 0 2 0 1836.87 1952.75 12.17 o 2 2 0 0.22 3.61 0.72 o 4 2 0 477.42 436.45 3.10 o 6 2 0 36.66 25.40 0.87 o 8 2 0 242.57 251.31 2.46 o 10 2 0 145.66 155.38 2.23 o 12 2 0 426.72 404.44 3.06 o 14 2 0 30.22 29.46 1.27 o 16 2 0 181.85 184.15 2.86 o 18 2 0 10.50 9.87 2.23 o 20 2 0 1.71 0.26 1.85 o 22 2 0 41.45 42.46 2.11 o 24 2 0 7.53 11.85 2.06 o 26 2 0 7.77 1.19 2.35 o 1 3 0 1676.50 1623.50 9.03 o 5 3 0 79.18 119.91 1.97 o 7 3 0 1129.29 1030.23 5.68 o 9 3 0 5116.76 5529.18 24.20 o 11 3 0 338.13 373.64 2.87 o 13 3 0 1465.01 1304.17 7.77 o 15 3 0 1379.03 1370.51 7.48 o 17 3 0 1.67 1.77 1.61 o 19 3 0 625.25 661.47 6.08 o 21 3 0 271.91 272.79 3.88 o 23 3 0 2.09 0.97 1.96 o 25 3 0 204.60 205.65 4.12 o 27 3 0 171.96 225.18 4.88 o 2 4 0 380.39 319.63 3.51 o 4 4 0 1783.68 1921.69 9.34 o 6 4 0 86.76 79.12 2.12 o 8 4 0 4266.97 3737.09 20.66 o 10 4 0 1830.33 1919.76 9.98 o 12 4 0 674.75 686.39 4.00 o 14 4 0 671.40 665.53 4.36 o 16 4 0 4.23 12.81 1.38 o 18 4 0 4225.90 4057.18 30.24 o 20 4 0 534.94 514.26 4.46 o 22 4 0 397.05 392.40 4.04 o 24 4 0 733.37 736.08 6.01 o 26 4 0 410.72 437.43 5.37 o 1 5 0 13305.90 12856.62 110.68 o 3 5 0 644.47 606.70 4.53 o 5 5 0 894.20 633.34 3.99 o 7 5 0 795.25 641.75 4.61 o 9 5 0 3227.08 3370.39 17.96 o 11 5 0 659.04 601.67 5.01 o 13 5 0 66.82 103.39 3.14 o 15 5 0 2435.67 2523.81 14.07 o 17 5 0 0.24 2.42 1.87 o 19 5 0 685.03 683.91 6.11 o 21 5 0 2782.49 2805.17 14.18 o 23 5 0 94.26 85.11 2.80 o 25 5 0 134.80 128.43 3.88 o 0 6 0 4057.73 3829.52 24.23 o 2 6 0 80.87 98.27 4.25 o 4 6 0 1267.39 1207.10 6.54 o 6 6 0 196.87 169.01 2.50 o 8 6 0 1004.29 871.28 5.57 o 10 6 0 273.02 214.64 2.97 o 12 6 0 1069.12 1059.97 7.04 o 14 6 0 33.70 35.39 1.91 o 16 6 0 1135.75 1231.50 11.24 o 18 6 0 4.83 0.23 2.72 o 20 6 0 13.84 16.57 1.98 o 22 6 0 278.60 289.01 4.67 o 24 6 0 13.92 10.77 2.57 o 1 7 0 1843.51 1945.95 9.26 o 3 7 0 25749.08 25773.39 384.52 o 5 7 0 213.84 225.94 3.55 o 7 7 0 0.00 1.91 1.31 o 9 7 0 781.90 799.45 5.21 o 11 7 0 81.28 84.29 2.49 o 13 7 0 244.51 229.46 3.50 o 15 7 0 15.73 27.35 2.34 o 17 7 0 103.06 93.41 3.90 o 19 7 0 121.35 119.13 4.42 o 21 7 0 56.24 62.47 3.45 o 23 7 0 4.41 1.93 3.22 o 2 8 0 96.81 74.69 2.81 o 4 8 0 15.16 7.74 1.43 o 6 8 0 384.95 359.30 3.97 o 8 8 0 516.23 463.76 3.96 o 10 8 0 618.53 695.58 9.54 o 12 8 0 36.87 28.53 1.86 o 14 8 0 8.58 9.76 1.94 o 16 8 0 247.77 238.92 4.00 o 18 8 0 2649.35 2647.66 16.65 o 20 8 0 637.93 594.28 7.05 o 22 8 0 26.99 20.80 3.12 o 1 9 0 6230.13 6354.99 27.11 o 3 9 0 180.62 191.86 2.30 o 5 9 0 77.18 61.00 3.29 o 7 9 0 5.20 9.94 1.57 o 9 9 0 185.02 196.37 3.29 o 11 9 0 368.21 358.09 4.35 o 13 9 0 528.04 565.50 5.02 o 15 9 0 1685.73 1693.44 9.89 o 17 9 0 84.30 72.69 3.49 o 19 9 0 247.84 246.71 5.86 o 21 9 0 1495.29 1542.43 12.23 o 0 10 0 1886.53 1820.67 13.09 o 2 10 0 5.53 6.43 1.27 o 4 10 0 151.63 173.66 4.76 o 6 10 0 523.04 525.11 5.28 o 8 10 0 318.91 307.59 3.89 o 10 10 0 22.69 15.64 1.93 o 12 10 0 165.42 178.02 3.76 o 14 10 0 2.99 0.33 2.06 o 16 10 0 1373.34 1477.77 9.48 o 18 10 0 68.18 60.78 3.44 o 20 10 0 15.01 8.01 3.19 o 1 11 0 808.75 796.47 5.22 o 3 11 0 10654.54 10831.20 45.74 o 5 11 0 62.59 73.30 2.54 o 7 11 0 55.42 66.85 3.82 o 9 11 0 36.71 40.38 2.30 o 11 11 0 16.84 10.01 2.24 o 13 11 0 13.50 10.01 2.25 o 15 11 0 289.52 313.21 4.96 o 17 11 0 268.35 277.56 6.24 o 19 11 0 26.31 20.68 3.55 o 0 12 0 11747.36 11577.28 79.45 o 2 12 0 31.82 21.38 2.44 o 4 12 0 287.41 270.67 3.83 o 6 12 0 168.54 160.34 4.37 o 8 12 0 9.25 11.03 2.41 o 10 12 0 60.88 54.29 2.85 o 12 12 0 78.47 78.37 3.00 o 14 12 0 116.31 139.33 5.45 o 16 12 0 118.89 108.83 4.11 o 18 12 0 1087.51 1095.24 11.27 o 1 13 0 1862.95 1940.28 9.84 o 3 13 0 85.13 81.25 2.41 o 5 13 0 0.02 1.50 2.41 o 7 13 0 70.44 71.56 3.04 o 9 13 0 11.26 4.28 2.57 o 11 13 0 278.65 276.41 5.36 o 13 13 0 225.77 244.73 5.84 o 15 13 0 770.69 778.30 7.09 o 0 14 0 661.46 675.10 7.56 o 2 14 0 21.53 28.16 1.93 o 4 14 0 12.55 8.80 2.27 o 6 14 0 527.66 523.92 6.45 o 8 14 0 64.64 59.67 3.04 o 10 14 0 18.95 6.31 3.08 o 12 14 0 1.26 0.88 2.87 o 1 15 0 382.69 289.54 4.05 o 3 15 0 3409.85 3325.18 29.30 o 5 15 0 2.37 1.09 3.24 o 7 15 0 22.50 9.80 2.91 o -27 1 1 7.93 15.30 2.57 o -25 1 1 76.58 65.91 2.44 o -23 1 1 340.44 356.84 4.65 o -21 1 1 11353.62 11126.82 53.58 o -19 1 1 16085.77 16054.70 76.28 o -17 1 1 199.63 153.75 2.81 o -15 1 1 164.34 154.96 2.81 o -13 1 1 910.40 901.01 5.21 o -11 1 1 21.06 17.44 1.01 o -9 1 1 2240.45 2389.71 10.80 o -7 1 1 96.73 109.73 1.44 o 5 1 1 8190.22 7304.34 109.82 o 7 1 1 179.61 214.60 2.23 o 9 1 1 198.40 195.61 2.43 o 11 1 1 1752.52 1779.38 9.87 o 13 1 1 3.35 7.00 2.10 o 15 1 1 862.43 869.74 5.65 o 17 1 1 173.90 153.94 3.59 o 19 1 1 265.81 224.29 3.60 o 21 1 1 734.85 744.53 5.86 o 23 1 1 4.40 2.93 2.03 o 25 1 1 283.04 335.72 5.23 o -28 2 1 25.86 24.98 2.35 o -26 2 1 99.69 115.10 3.93 o -24 2 1 903.14 962.81 7.30 o -22 2 1 464.20 518.07 4.90 o -20 2 1 1253.60 1291.73 8.39 o -18 2 1 23291.15 23164.34 154.61 o -16 2 1 1597.79 1671.07 9.18 o -14 2 1 2234.38 2236.90 11.59 o -12 2 1 6044.38 5858.71 25.70 o -10 2 1 3907.56 4057.71 30.83 o -6 2 1 2387.73 2647.83 12.30 o 0 2 1 2217.20 1681.97 6.75 o 6 2 1 8258.43 8141.31 70.64 o 8 2 1 133.78 212.52 2.46 o 12 2 1 16.83 6.50 1.09 o 14 2 1 4972.39 5074.34 26.21 o 16 2 1 1480.39 1613.63 9.10 o 18 2 1 253.80 263.53 3.81 o 20 2 1 159.25 150.47 3.47 o 22 2 1 143.49 158.71 3.90 o 24 2 1 65.02 63.56 2.49 o 26 2 1 480.75 676.74 6.61 o -27 3 1 41.11 56.86 2.69 o -25 3 1 43.74 43.45 2.26 o -23 3 1 696.36 698.68 6.22 o -21 3 1 6164.41 6160.28 28.92 o -19 3 1 22879.19 23061.34 103.85 o -17 3 1 266.03 230.36 3.15 o -15 3 1 491.60 496.06 4.53 o -13 3 1 1122.15 1024.06 5.91 o -11 3 1 2381.50 2246.54 10.88 o -9 3 1 247.62 205.65 2.10 o -7 3 1 1398.93 1502.80 7.35 o 1 3 1 326.56 506.49 7.28 o 3 3 1 8857.74 8537.84 132.33 o 5 3 1 4167.14 4299.25 20.92 o 7 3 1 1648.77 1644.30 8.07 o 9 3 1 4204.95 4205.93 19.53 o 11 3 1 605.63 569.44 3.88 o 13 3 1 5.12 0.87 1.11 o 15 3 1 2633.10 2468.96 13.60 o 17 3 1 78.68 68.32 2.09 o 19 3 1 194.63 184.57 3.71 o 21 3 1 111.68 117.97 3.49 o 23 3 1 108.19 108.72 3.29 o 25 3 1 371.07 482.79 5.97 o -26 4 1 120.18 116.46 3.76 o -24 4 1 313.97 316.85 4.49 o -22 4 1 11.45 14.51 2.03 o -20 4 1 905.44 936.55 6.66 o -18 4 1 29.51 49.01 1.86 o -16 4 1 255.88 252.21 2.80 o -14 4 1 339.76 339.75 2.95 o -12 4 1 170.51 159.54 2.07 o -10 4 1 259.48 256.94 2.29 o -8 4 1 4.91 3.98 0.89 o -6 4 1 1194.54 1231.78 6.23 o -4 4 1 10.27 47.76 8.34 o 4 4 1 4050.69 4002.12 18.62 o 6 4 1 406.91 363.00 3.28 o 8 4 1 856.97 811.31 5.40 o 10 4 1 31.14 58.71 2.21 o 12 4 1 189.97 184.04 2.29 o 14 4 1 109.20 112.06 2.36 o 16 4 1 417.36 375.22 3.59 o 18 4 1 290.49 283.99 3.79 o 20 4 1 575.11 583.70 6.86 o 22 4 1 276.57 247.20 3.96 o 24 4 1 6.64 3.28 2.09 o -27 5 1 0.02 -2.22 2.22 o -25 5 1 82.54 72.70 2.70 o -23 5 1 20.00 25.72 2.01 o -21 5 1 8951.57 8980.58 41.61 o -19 5 1 3280.44 3473.16 27.96 o -17 5 1 82.67 85.05 2.25 o -15 5 1 120.79 140.37 2.19 o -13 5 1 631.03 638.16 4.15 o -11 5 1 1477.01 1495.31 7.32 o -9 5 1 2751.08 2612.41 13.22 o -7 5 1 71.53 66.85 1.69 o -5 5 1 661.04 630.54 4.82 o -3 5 1 2051.72 2191.96 9.00 o -1 5 1 7413.81 7513.18 30.24 o 1 5 1 4578.71 4273.20 17.50 o 3 5 1 6614.50 6682.03 30.59 o 5 5 1 598.64 574.45 6.82 o 7 5 1 121.48 86.31 2.57 o 9 5 1 643.27 697.75 5.12 o 11 5 1 2883.77 2789.34 15.30 o 13 5 1 63.79 73.96 2.27 o 15 5 1 34.62 37.75 1.73 o 17 5 1 73.35 71.42 3.17 o 19 5 1 46.55 38.61 1.79 o 21 5 1 822.17 846.58 5.80 o 23 5 1 270.19 273.94 4.49 o 25 5 1 82.66 88.53 3.11 o -26 6 1 0.13 1.12 2.03 o -24 6 1 573.36 618.94 6.44 o -22 6 1 17.44 26.62 1.95 o -20 6 1 790.73 831.96 6.86 o -18 6 1 14637.30 14968.93 71.85 o -16 6 1 133.74 126.55 2.98 o -14 6 1 208.60 215.14 3.20 o -12 6 1 1886.87 1799.79 10.59 o -10 6 1 914.55 910.37 6.17 o -8 6 1 4947.57 4789.99 23.53 o -6 6 1 775.75 838.02 4.50 o -4 6 1 8340.03 7866.64 31.70 o -2 6 1 1414.63 1501.86 6.53 o 0 6 1 38.27 21.40 0.96 o 2 6 1 6151.50 6442.34 26.16 o 4 6 1 1623.79 1629.60 9.49 o 6 6 1 3394.87 3386.07 17.92 o 8 6 1 374.82 349.17 3.46 o 10 6 1 9252.59 10118.33 48.63 o 12 6 1 89.05 105.98 2.85 o 14 6 1 1699.97 1805.07 10.97 o 16 6 1 851.26 919.61 7.68 o 18 6 1 369.56 363.37 4.33 o 20 6 1 137.28 136.51 3.96 o 22 6 1 178.72 200.09 3.94 o 24 6 1 56.04 52.77 3.06 o -25 7 1 21.55 23.30 2.49 o -23 7 1 282.46 279.51 4.71 o -21 7 1 1164.22 1204.24 11.72 o -19 7 1 14743.02 14888.41 71.41 o -17 7 1 16.85 29.25 2.32 o -15 7 1 282.96 284.13 4.23 o -13 7 1 739.00 696.81 5.74 o -11 7 1 1366.07 1212.89 7.91 o -9 7 1 1417.37 1456.89 9.31 o -7 7 1 1567.13 1706.74 8.31 o -5 7 1 2117.25 2001.99 8.26 o -3 7 1 12195.94 12398.76 47.99 o -1 7 1 6166.08 6602.84 25.93 o 1 7 1 784.25 728.27 4.01 o 3 7 1 1065.84 1102.69 10.46 o 5 7 1 133.60 188.34 2.69 o 7 7 1 1053.06 946.20 6.11 o 9 7 1 3849.20 3664.80 18.68 o 11 7 1 312.75 291.26 3.69 o 13 7 1 32.07 25.89 1.91 o 15 7 1 2097.39 2009.90 11.54 o 17 7 1 0.26 -2.33 2.33 o 19 7 1 36.92 35.84 2.75 o 21 7 1 36.58 27.96 2.82 o 23 7 1 43.70 45.59 3.10 o -24 8 1 642.18 622.02 7.87 o -22 8 1 17.11 25.55 3.48 o -20 8 1 1083.27 1187.67 9.10 o -18 8 1 80.53 112.53 7.24 o -16 8 1 416.09 425.36 5.18 o -14 8 1 122.19 135.23 3.62 o -12 8 1 78.45 66.58 2.38 o -10 8 1 84.33 86.24 2.49 o -8 8 1 2.35 3.34 1.53 o -6 8 1 742.02 812.93 4.41 o -4 8 1 372.16 382.35 3.44 o -2 8 1 7792.29 8054.79 32.69 o 0 8 1 11749.70 11748.47 55.01 o 2 8 1 5999.28 5976.88 22.92 o 4 8 1 2711.87 2812.66 14.62 o 6 8 1 90.80 75.41 2.19 o 8 8 1 1087.64 1079.98 6.61 o 10 8 1 281.59 324.80 3.91 o 12 8 1 208.08 196.85 3.64 o 14 8 1 254.39 272.40 4.10 o 16 8 1 256.21 235.49 4.20 o 18 8 1 367.63 365.51 5.59 o 20 8 1 464.71 481.89 6.41 o 22 8 1 442.69 411.54 12.63 o -23 9 1 3.49 3.35 3.21 o -21 9 1 3907.41 4049.76 21.97 o -19 9 1 17.29 27.14 2.70 o -17 9 1 141.34 153.01 4.26 o -15 9 1 492.48 544.16 5.51 o -13 9 1 195.85 215.46 3.96 o -11 9 1 1179.60 1104.77 8.25 o -9 9 1 893.86 887.78 6.26 o -7 9 1 46.76 47.83 2.36 o -5 9 1 284.10 299.07 2.61 o -3 9 1 10.97 32.32 3.17 o -1 9 1 2506.66 2517.00 11.10 o 1 9 1 591.98 523.39 3.67 o 3 9 1 2126.00 2272.00 11.10 o 5 9 1 1.07 1.92 1.65 o 7 9 1 18.68 37.60 1.82 o 9 9 1 713.34 712.20 5.55 o 11 9 1 1041.81 1063.97 6.99 o 13 9 1 423.92 447.23 4.68 o 15 9 1 4.31 1.55 2.18 o 17 9 1 47.72 40.51 2.51 o 19 9 1 0.37 -2.70 2.70 o 21 9 1 403.69 408.43 6.42 o -22 10 1 634.68 699.24 7.47 o -20 10 1 323.23 323.67 5.49 o -18 10 1 5827.60 6138.74 48.12 o -16 10 1 166.67 184.34 4.48 o -14 10 1 2.73 -2.12 2.12 o -12 10 1 322.04 302.32 4.06 o -10 10 1 7.06 4.57 1.96 o -8 10 1 135.51 127.77 4.12 o -6 10 1 282.82 265.58 3.03 o -4 10 1 846.27 815.70 4.53 o -2 10 1 26.53 22.89 1.44 o 0 10 1 43.91 40.19 1.43 o 2 10 1 1231.35 1286.63 6.46 o 4 10 1 230.92 223.58 3.99 o 6 10 1 460.06 498.18 5.16 o 8 10 1 781.82 810.74 6.16 o 10 10 1 2679.26 2759.30 14.37 o 12 10 1 206.42 212.99 3.99 o 14 10 1 472.30 473.49 5.09 o 16 10 1 371.08 361.75 5.58 o 18 10 1 252.15 241.07 4.64 o 20 10 1 95.17 79.68 3.67 o -19 11 1 5948.63 6174.90 43.74 o -17 11 1 11.53 16.24 2.75 o -15 11 1 49.93 42.28 2.70 o -13 11 1 352.85 338.13 4.83 o -11 11 1 259.79 265.25 4.62 o -9 11 1 614.55 644.89 5.73 o -7 11 1 523.17 574.24 5.02 o -5 11 1 12.22 9.72 2.17 o -3 11 1 3396.73 3415.39 15.58 o -1 11 1 4237.41 4350.09 20.97 o 1 11 1 1301.35 1312.67 10.93 o 3 11 1 13.18 13.23 2.11 o 5 11 1 9.33 8.55 1.98 o 7 11 1 29.46 24.99 2.11 o 9 11 1 1148.17 1203.49 8.23 o 11 11 1 180.71 184.51 4.02 o 13 11 1 24.43 33.59 2.51 o 15 11 1 759.29 799.58 7.28 o 17 11 1 14.30 11.59 2.56 o -18 12 1 180.06 161.02 4.86 o -16 12 1 273.90 287.47 6.22 o -14 12 1 1.79 -1.27 2.40 o -12 12 1 16.73 10.76 2.37 o -10 12 1 0.34 -2.21 2.21 o -8 12 1 4.92 -2.22 2.22 o -6 12 1 101.19 79.32 2.53 o -4 12 1 444.76 450.83 4.69 o -2 12 1 2254.79 2317.49 14.34 o 0 12 1 4684.62 4688.66 20.90 o 2 12 1 1161.19 1149.72 7.28 o 4 12 1 921.02 896.10 7.37 o 6 12 1 50.82 49.80 2.63 o 8 12 1 381.33 427.67 5.55 o 10 12 1 355.14 354.46 4.71 o 12 12 1 80.68 70.76 2.69 o 14 12 1 133.12 162.41 4.43 o 16 12 1 20.65 13.88 2.75 o -15 13 1 550.92 562.51 7.69 o -13 13 1 2.80 6.24 2.70 o -11 13 1 296.15 294.62 5.04 o -9 13 1 127.83 124.55 4.10 o -7 13 1 245.17 274.70 5.16 o -5 13 1 269.05 298.62 3.93 o -3 13 1 102.41 85.36 3.54 o -1 13 1 722.82 639.48 6.13 o 1 13 1 36.25 30.76 1.73 o 3 13 1 742.00 755.96 5.74 o 5 13 1 24.69 23.10 2.63 o 7 13 1 323.77 342.56 5.50 o 9 13 1 260.44 233.66 5.20 o 11 13 1 91.24 95.48 3.52 o 13 13 1 630.55 630.99 6.68 o -12 14 1 59.32 48.73 3.20 o -10 14 1 4.55 1.06 3.55 o -8 14 1 0.01 2.12 2.67 o -6 14 1 336.20 260.25 4.37 o -4 14 1 0.65 3.75 1.83 o -2 14 1 0.49 0.26 1.85 o 0 14 1 187.46 178.53 3.50 o 2 14 1 521.60 464.86 4.76 o 4 14 1 0.94 2.49 2.63 o 6 14 1 12.72 11.40 2.73 o 8 14 1 310.59 309.50 6.75 o 10 14 1 499.99 488.56 6.67 o -9 15 1 116.46 115.86 5.39 o -7 15 1 247.93 230.59 5.48 o -5 15 1 56.15 44.43 3.56 o -3 15 1 726.06 698.31 5.94 o -1 15 1 2091.89 2056.50 13.87 o 1 15 1 767.51 758.19 8.77 o 3 15 1 101.77 75.19 3.52 o 5 15 1 16.41 16.48 3.06 o 7 15 1 25.69 21.98 3.05 o -28 0 2 475.91 496.72 8.23 o -26 0 2 0.01 2.97 3.02 o -24 0 2 1.23 3.42 2.76 o -22 0 2 4742.54 4755.42 33.84 o -20 0 2 3636.28 3702.60 34.83 o -18 0 2 6698.83 6675.49 45.92 o -16 0 2 1921.21 1919.69 28.20 o -14 0 2 51.64 54.96 1.77 o -12 0 2 700.64 996.51 6.74 o -6 0 2 181.78 273.47 2.40 o -2 0 2 100.82 143.69 1.76 o 2 0 2 4805.57 4550.87 90.40 o 4 0 2 205.95 210.57 3.34 o 6 0 2 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