#------------------------------------------------------------------------------
#$Date: 2021-08-11 05:14:50 +0300 (Wed, 11 Aug 2021) $
#$Revision: 268022 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243890.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243890
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   8.3876
_cell_length_b                   8.3876
_cell_length_c                   30.0476
_exptl_crystal_F_000             1152.00
_reflns_d_resolution_high        0.7317
_cod_data_source_file            ru2076Na3_Li_2SO4_6H2O-90Ksup2.hkl
_cod_data_source_block           Na3_Li_2SO4_6H2O-90K
_shelx_title                     ' Na3Li_2SO4_6H2O-90k in R3c'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            209.12
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-y, -x, z+1/2'
'-x+y, y, z+1/2'
'x, x-y, z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'-y+2/3, -x+1/3, z+5/6'
'-x+y+2/3, y+1/3, z+5/6'
'x+2/3, x-y+1/3, z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-y+1/3, -x+2/3, z+7/6'
'-x+y+1/3, y+2/3, z+7/6'
'x+1/3, x-y+2/3, z+7/6'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 -40 4820.80 4968.76 75.48 o
-2 2 -40 6561.86 6410.67 71.65 o
-1 2 -39 748.77 737.07 10.71 o
-1 1 -38 857.74 851.80 14.17 o
0 2 -38 155.82 154.47 9.34 o
-2 3 -38 254.25 247.96 5.81 o
-1 4 -38 1308.88 1276.46 10.85 o
-1 3 -37 3604.55 3533.76 25.02 o
-3 4 -37 150.52 165.63 7.45 o
0 0 -36 2142.20 2169.12 10.35 o
-1 2 -36 4710.04 4673.20 28.55 o
-3 3 -36 7199.33 7618.88 48.32 o
0 3 -36 8771.12 8665.96 108.02 o
-2 4 -36 7860.14 7900.39 38.90 o
-4 5 -36 7126.93 6842.32 61.55 o
-1 5 -36 4201.82 3967.97 125.74 o
-2 3 -35 1685.08 1674.89 26.13 o
-1 4 -35 1004.03 1011.61 10.29 o
-3 5 -35 980.01 980.00 10.10 o
0 1 -34 91.43 100.24 2.95 o
-2 2 -34 1405.97 1383.42 20.09 o
-1 3 -34 1243.78 1288.20 22.38 o
-3 4 -34 364.64 374.05 4.99 o
0 4 -34 1610.32 1591.39 12.04 o
-5 5 -34 934.70 901.03 10.41 o
-2 5 -34 112.40 114.71 5.02 o
-4 6 -34 1429.08 1334.58 39.04 o
-1 6 -34 435.36 407.02 8.67 o
-1 2 -33 4182.66 4217.91 27.91 o
-2 4 -33 2406.32 2363.21 16.92 o
-4 5 -33 319.81 311.39 6.65 o
-1 5 -33 1155.26 1113.72 11.57 o
-3 6 -33 1785.46 1776.42 15.76 o
-1 1 -32 768.44 706.45 15.15 o
0 2 -32 3662.96 3899.06 63.99 o
-2 3 -32 9221.79 9688.81 44.57 o
-4 4 -32 2995.56 3092.75 33.56 o
-1 4 -32 4466.68 4481.65 36.53 o
-3 5 -32 2349.04 2376.00 22.82 o
0 5 -32 49.25 85.06 12.69 o
-5 6 -32 1421.87 1411.17 16.37 o
-2 6 -32 3380.51 3339.75 22.93 o
-4 7 -32 1241.57 1184.19 14.94 o
-1 3 -31 1118.57 1085.28 8.35 o
-3 4 -31 1980.74 1941.69 17.32 o
-2 5 -31 1134.12 1128.19 13.68 o
-4 6 -31 445.11 468.60 5.51 o
-1 6 -31 1066.95 1076.23 12.65 o
-3 7 -31 461.80 471.94 4.98 o
0 0 -30 2332.67 2287.77 20.40 o
-1 2 -30 656.53 678.19 6.57 o
-3 3 -30 548.11 562.27 4.52 o
0 3 -30 985.69 951.14 11.86 o
-2 4 -30 623.51 616.08 3.77 o
-4 5 -30 1459.71 1435.36 12.93 o
-1 5 -30 725.79 726.15 9.43 o
-6 6 -30 4525.22 4508.26 60.05 o
-3 6 -30 1002.39 1003.17 10.12 o
0 6 -30 1369.47 1360.82 20.54 o
-5 7 -30 55.97 54.70 3.81 o
-2 7 -30 630.73 616.77 7.91 o
-2 3 -29 2316.24 2363.88 19.94 o
-1 4 -29 2257.06 2232.37 12.94 o
-3 5 -29 123.61 137.52 4.82 o
-5 6 -29 1685.92 1689.44 13.99 o
-2 6 -29 2306.41 2300.54 15.60 o
-4 7 -29 71.06 92.63 12.27 o
-1 7 -29 140.01 149.10 3.59 o
-3 8 -29 2870.54 2787.00 34.48 o
0 1 -28 3092.51 3207.12 26.33 o
-2 2 -28 5760.15 5638.36 74.41 o
-1 3 -28 6712.02 6597.97 45.14 o
-3 4 -28 13559.94 13755.56 170.55 o
0 4 -28 17961.93 18371.72 262.60 o
-5 5 -28 3332.55 3331.96 28.29 o
-2 5 -28 3369.99 3348.76 27.27 o
-4 6 -28 2368.74 2381.62 23.82 o
-1 6 -28 2566.79 2631.59 20.40 o
-6 7 -28 1511.82 1468.55 10.03 o
-3 7 -28 2347.70 2277.62 21.98 o
0 7 -28 1299.84 1304.88 21.91 o
-5 8 -28 2742.07 2643.72 15.20 o
-2 8 -28 2589.92 2468.92 21.08 o
-1 2 -27 2264.93 2227.11 15.97 o
-2 4 -27 1427.34 1471.69 16.06 o
-4 5 -27 4.49 31.20 6.07 o
-1 5 -27 148.16 162.03 6.35 o
-3 6 -27 303.73 303.24 4.90 o
-5 7 -27 822.53 791.86 5.91 o
-2 7 -27 3577.62 3486.19 25.37 o
-4 8 -27 71.90 85.87 4.64 o
-1 1 -26 1091.79 1078.25 17.92 o
0 2 -26 573.67 550.25 9.70 o
-2 3 -26 3575.72 3592.69 35.29 o
-4 4 -26 2645.71 2677.96 31.44 o
-1 4 -26 3413.68 3499.52 20.14 o
-3 5 -26 63.61 90.32 7.11 o
0 5 -26 2265.51 2248.30 34.10 o
-5 6 -26 252.60 256.49 3.76 o
-2 6 -26 1712.79 1754.06 11.18 o
-7 7 -26 1049.43 1032.37 10.07 o
-4 7 -26 1774.91 1794.00 16.21 o
-1 7 -26 429.67 440.20 6.01 o
-6 8 -26 701.11 702.72 8.10 o
-3 8 -26 566.99 550.28 7.42 o
-1 3 -25 759.96 768.67 6.03 o
-3 4 -25 5009.15 5140.97 37.54 o
-2 5 -25 1450.68 1440.85 14.18 o
-4 6 -25 1481.21 1560.55 19.04 o
-1 6 -25 367.58 357.83 3.72 o
-6 7 -25 714.25 770.11 22.69 o
-3 7 -25 416.28 422.81 3.71 o
-5 8 -25 5621.94 5496.10 31.56 o
-2 8 -25 812.96 806.65 6.12 o
-4 9 -25 1351.16 1273.92 11.37 o
0 0 -24 15373.97 14970.53 581.02 o
-1 2 -24 15711.64 15693.43 138.79 o
-3 3 -24 9346.86 9641.38 92.15 o
0 3 -24 15812.77 16235.38 266.48 o
-2 4 -24 21299.75 21625.86 170.45 o
-4 5 -24 5925.80 5942.86 42.65 o
-1 5 -24 5505.37 5557.30 39.89 o
-6 6 -24 7417.37 7360.11 41.16 o
-3 6 -24 11133.12 11349.12 84.85 o
0 6 -24 8498.07 8716.99 57.03 o
-5 7 -24 8174.85 8155.84 59.54 o
-2 7 -24 4414.04 4427.45 24.85 o
-7 8 -24 2530.78 2498.17 10.29 o
-4 8 -24 2183.36 2242.25 18.54 o
-1 8 -24 7007.11 6902.56 42.75 o
-6 9 -24 9200.33 8895.38 65.09 o
-3 9 -24 5252.31 5181.02 39.56 o
-2 3 -23 1302.76 1327.45 10.32 o
-1 4 -23 262.03 275.05 3.51 o
-3 5 -23 5689.68 5768.43 64.53 o
-5 6 -23 68.55 62.96 1.98 o
-2 6 -23 216.92 226.85 5.32 o
-4 7 -23 721.75 740.46 5.56 o
-1 7 -23 1874.12 1942.94 14.53 o
-6 8 -23 88.57 94.84 3.25 o
-3 8 -23 565.70 602.61 9.62 o
-5 9 -23 54.04 66.17 3.31 o
-2 9 -23 1732.11 1622.52 9.02 o
0 1 -22 2165.49 2153.79 31.56 o
-2 2 -22 2479.08 2469.06 11.60 o
-1 3 -22 4452.81 4445.91 37.89 o
-3 4 -22 2196.68 2180.81 17.92 o
0 4 -22 7364.29 7613.26 84.89 o
-5 5 -22 3422.01 3328.18 35.67 o
-2 5 -22 1992.85 2032.30 22.20 o
-4 6 -22 989.47 1033.15 10.45 o
-1 6 -22 265.53 264.86 4.81 o
-6 7 -22 2260.68 2297.84 20.20 o
-3 7 -22 309.54 310.46 4.70 o
0 7 -22 745.15 796.44 16.57 o
-8 8 -22 512.80 489.94 14.25 o
-5 8 -22 725.44 734.41 9.39 o
-2 8 -22 179.84 181.97 3.92 o
-7 9 -22 174.86 178.98 3.20 o
-4 9 -22 244.98 247.79 2.38 o
-1 2 -21 2843.80 2848.82 31.23 o
-2 4 -21 3134.67 3170.63 40.21 o
-4 5 -21 5286.76 5294.18 43.00 o
-1 5 -21 7276.94 7332.65 42.14 o
-3 6 -21 475.90 473.16 10.00 o
-5 7 -21 80.03 100.24 7.12 o
-2 7 -21 879.24 848.30 6.27 o
-7 8 -21 2329.88 2368.00 19.87 o
-4 8 -21 334.30 349.89 5.05 o
-1 8 -21 1676.92 1663.58 11.66 o
-6 9 -21 976.28 977.34 11.83 o
-3 9 -21 2251.49 2189.25 14.51 o
-1 1 -20 34407.46 35028.47 604.08 o
0 2 -20 7434.43 7538.83 105.13 o
-2 3 -20 19803.43 20050.07 145.57 o
-4 4 -20 42267.56 42228.88 283.10 o
-1 4 -20 29852.93 30198.05 234.33 o
-3 5 -20 7471.85 7604.89 47.20 o
0 5 -20 15594.55 16245.63 126.05 o
-5 6 -20 5813.32 5678.08 64.23 o
-2 6 -20 13320.06 13153.92 87.58 o
-7 7 -20 19887.66 20158.63 255.66 o
-4 7 -20 6889.04 7075.97 54.13 o
-1 7 -20 2222.86 2324.09 23.28 o
-6 8 -20 6173.85 6087.40 65.60 o
-3 8 -20 18052.13 18220.18 82.17 o
0 8 -20 9526.09 9517.38 42.08 o
-8 9 -20 8608.53 8091.67 65.33 o
-5 9 -20 9254.83 9475.86 104.50 o
-2 9 -20 9232.12 9127.29 61.32 o
-1 3 -19 13167.63 13600.19 87.52 o
-3 4 -19 1163.75 1187.53 11.18 o
-2 5 -19 1424.75 1475.37 12.44 o
-4 6 -19 947.49 971.07 6.38 o
-1 6 -19 180.28 182.50 4.03 o
-6 7 -19 745.38 789.33 7.91 o
-3 7 -19 2051.69 2075.79 15.93 o
-5 8 -19 1103.77 1131.28 9.09 o
-2 8 -19 485.77 482.18 3.07 o
-7 9 -19 1910.91 1853.38 18.23 o
-4 9 -19 387.37 392.19 5.52 o
-1 9 -19 61.22 80.65 4.58 o
-6 10 -19 29.15 41.17 4.43 o
0 0 -18 31786.52 30496.33 37.55 o
-1 2 -18 1801.37 1739.23 22.38 o
-3 3 -18 3076.14 3217.91 17.52 o
0 3 -18 4154.94 4288.44 58.31 o
-2 4 -18 438.71 444.55 5.29 o
-4 5 -18 832.12 859.77 14.14 o
-1 5 -18 3163.28 3203.90 24.17 o
-6 6 -18 739.74 727.54 6.21 o
-3 6 -18 263.32 277.66 4.40 o
0 6 -18 5511.22 5787.26 56.42 o
-5 7 -18 439.66 426.62 4.97 o
-2 7 -18 1027.28 1024.84 9.03 o
-7 8 -18 628.67 627.22 9.42 o
-4 8 -18 2794.14 2835.68 22.12 o
-1 8 -18 436.18 424.15 3.78 o
-6 9 -18 767.09 763.95 7.62 o
-3 9 -18 72.72 74.98 2.17 o
-5 10 -18 393.76 366.41 5.77 o
-2 3 -17 2303.32 2357.01 27.76 o
-1 4 -17 440.25 442.19 3.12 o
-3 5 -17 12573.62 13002.70 88.96 o
-5 6 -17 1232.29 1277.36 10.13 o
-2 6 -17 1945.24 2037.70 15.86 o
-4 7 -17 2658.94 2679.78 22.06 o
-1 7 -17 882.93 890.87 10.90 o
-6 8 -17 4488.87 4503.73 38.63 o
-3 8 -17 1214.39 1228.88 7.79 o
-8 9 -17 2286.59 2298.12 15.00 o
-5 9 -17 950.64 938.39 8.10 o
-2 9 -17 171.44 174.03 3.08 o
-7 10 -17 717.84 693.10 13.86 o
-4 10 -17 820.21 797.03 5.81 o
0 1 -16 32138.25 32221.95 181.05 o
-2 2 -16 6629.10 6321.22 72.61 o
-1 3 -16 32515.21 31954.55 387.21 o
-3 4 -16 4896.30 4779.45 34.95 o
0 4 -16 5613.08 5626.16 66.32 o
-5 5 -16 5337.97 5273.92 69.18 o
-2 5 -16 9892.77 9880.33 83.48 o
-4 6 -16 31888.93 32871.55 237.42 o
-1 6 -16 12369.03 12476.73 90.11 o
-6 7 -16 6322.77 6417.52 47.69 o
-3 7 -16 3860.10 3740.63 23.83 o
0 7 -16 20077.81 20568.80 135.43 o
-8 8 -16 3245.26 3214.54 25.18 o
-5 8 -16 9251.60 9321.95 88.62 o
-2 8 -16 4307.24 4418.84 32.06 o
-7 9 -16 8675.40 8707.35 65.26 o
-4 9 -16 6775.07 6978.21 61.87 o
-1 9 -16 1932.12 1935.13 13.29 o
-6 10 -16 2417.74 2378.44 26.20 o
-3 10 -16 11051.32 10707.57 84.83 o
-1 2 -15 7971.72 7819.89 66.19 o
-2 4 -15 3203.72 3234.77 13.36 o
-4 5 -15 1729.48 1784.06 16.79 o
-1 5 -15 1650.58 1676.75 10.46 o
-3 6 -15 3483.02 3575.92 29.63 o
-5 7 -15 1979.00 1983.02 21.40 o
-2 7 -15 7025.73 7257.76 62.08 o
-7 8 -15 412.39 398.42 4.39 o
-4 8 -15 727.73 758.34 10.28 o
-1 8 -15 2864.93 2865.73 20.97 o
-6 9 -15 763.38 774.04 10.83 o
-3 9 -15 38.61 48.00 3.13 o
-8 10 -15 449.07 419.93 6.71 o
-5 10 -15 281.75 295.92 8.40 o
-2 10 -15 932.96 902.73 10.75 o
-1 1 -14 4725.98 4412.70 48.05 o
0 2 -14 11365.55 10637.15 122.00 o
-2 3 -14 1119.86 1077.55 8.93 o
-4 4 -14 15224.09 15298.20 196.34 o
-1 4 -14 3163.56 3284.21 33.79 o
-3 5 -14 2087.65 2118.71 7.57 o
0 5 -14 226.53 245.31 7.17 o
-5 6 -14 2057.70 2029.05 15.28 o
-2 6 -14 442.47 474.74 4.28 o
-7 7 -14 541.58 508.27 7.60 o
-4 7 -14 2004.03 2046.44 12.64 o
-1 7 -14 454.83 439.93 5.92 o
-6 8 -14 360.08 354.63 5.26 o
-3 8 -14 1482.51 1527.41 9.33 o
0 8 -14 881.75 934.76 8.30 o
-8 9 -14 816.98 829.34 6.24 o
-5 9 -14 1647.59 1697.45 18.23 o
-2 9 -14 595.61 610.32 6.00 o
-7 10 -14 236.84 226.15 5.30 o
-4 10 -14 2105.27 2077.53 23.33 o
-1 3 -13 43689.66 47896.88 47.94 o
-3 4 -13 787.24 786.26 10.87 o
-2 5 -13 948.14 940.24 13.54 o
-4 6 -13 5690.88 5707.68 62.18 o
-1 6 -13 4765.22 4822.88 51.80 o
-6 7 -13 689.09 664.04 6.25 o
-3 7 -13 768.48 705.86 5.77 o
-5 8 -13 163.76 175.19 4.81 o
-2 8 -13 899.58 942.77 7.34 o
-7 9 -13 1709.84 1680.97 7.00 o
-4 9 -13 196.00 195.78 2.54 o
-1 9 -13 389.79 389.79 4.68 o
-6 10 -13 833.23 825.28 9.11 o
-3 10 -13 525.81 518.33 8.01 o
-1 2 -12 11405.79 10474.41 64.70 o
-3 3 -12 10801.99 10508.17 128.39 o
0 3 -12 12809.44 13163.16 158.53 o
-2 4 -12 4035.95 3979.30 19.29 o
-4 5 -12 216.29 205.85 8.53 o
-1 5 -12 9410.00 9336.78 52.26 o
-6 6 -12 32976.83 33253.58 225.32 o
-3 6 -12 5584.65 5538.89 36.20 o
0 6 -12 1613.75 1577.05 22.52 o
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-1 8 -12 3019.95 3248.14 27.66 o
-9 9 -12 3037.73 3007.42 33.29 o
-6 9 -12 1714.08 1739.73 9.36 o
-3 9 -12 1619.77 1597.96 13.67 o
0 9 -12 1324.64 1361.77 19.70 o
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-5 10 -12 2074.33 2104.75 12.09 o
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-2 3 -11 25237.03 24784.03 248.14 o
-1 4 -11 1668.42 1614.56 11.85 o
-3 5 -11 61.55 92.06 7.65 o
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-2 6 -11 2576.85 2582.22 18.58 o
-4 7 -11 626.61 666.80 7.33 o
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-6 8 -11 172.06 172.55 4.18 o
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-5 9 -11 1216.12 1240.99 9.02 o
-2 9 -11 797.65 800.46 9.41 o
-7 10 -11 290.70 275.23 4.97 o
-4 10 -11 1120.97 1123.48 17.38 o
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-1 2 -9 29916.83 28714.42 729.45 o
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-4 5 -9 488.69 643.40 65.72 o
-1 5 -9 6624.12 6765.54 47.59 o
-3 6 -9 8647.83 8539.93 46.20 o
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-2 7 -9 3494.77 3523.74 27.85 o
-7 8 -9 2247.41 2292.19 19.89 o
-4 8 -9 1247.00 1222.26 9.09 o
-1 8 -9 368.78 396.96 5.09 o
-6 9 -9 170.88 182.60 5.84 o
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-8 10 -9 172.26 182.42 4.31 o
-5 10 -9 1313.08 1346.76 10.91 o
-2 10 -9 344.46 367.09 6.74 o
-7 11 -9 589.24 577.53 9.32 o
-4 11 -9 266.43 261.37 11.75 o
0 2 -8 9873.38 8871.48 109.99 o
-2 3 -8 11962.89 12873.59 91.65 o
-4 4 -8 19479.01 18679.63 272.27 o
-1 4 -8 9870.22 9261.21 71.28 o
-3 5 -8 9302.65 9658.98 96.81 o
0 5 -8 28098.56 28381.01 299.21 o
-5 6 -8 7600.25 7687.54 49.51 o
-2 6 -8 1401.22 1494.76 10.20 o
-7 7 -8 738.74 724.59 24.20 o
-4 7 -8 13537.56 13598.52 108.30 o
-1 7 -8 7155.28 7294.62 47.59 o
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0 1 26 1089.29 1127.23 12.45 o
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