#------------------------------------------------------------------------------ #$Date: 2021-08-11 05:14:50 +0300 (Wed, 11 Aug 2021) $ #$Revision: 268022 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243891.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243891 loop_ _publ_author_name 'Schmidt, Horst' 'Paschke, Iris' 'Voigt, Wolfgang' _publ_section_title ; LiNa~3~(SO~4~)~2~·6H~2~O: a lithium double salt causing trouble in the industrial conversion of Li~2~SO~4~ into LiOH ; _journal_coeditor_code RU2076 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989021008057 _journal_volume 77 _journal_year 2021 _chemical_formula_moiety '3(Na) Li 2(SO4) 6(H2O)' _chemical_formula_sum 'H12 Li Na3 O14 S2' _chemical_formula_weight 376.13 _chemical_name_systematic Sodium-Lithium-Sulfate-Hexahydrate _space_group_crystal_system trigonal _space_group_IT_number 161 _space_group_name_Hall 'R 3 -2"c' _space_group_name_H-M_alt 'R 3 c :H' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 8.4006(19) _cell_length_b 8.4006(19) _cell_length_c 30.111(9) _cell_measurement_reflns_used 7724 _cell_measurement_temperature 180 _cell_measurement_theta_max 30.01 _cell_measurement_theta_min 2.83 _cell_volume 1840.2(8) _computing_cell_refinement ; X-AREA (Stoe & Cie, 2015) ; _computing_data_collection ; X-AREA (Stoe & Cie, 2015) ; _computing_data_reduction ; X-RED (Stoe & Cie, 2015) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 2017) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 180(2) _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.937 _diffrn_measured_fraction_theta_max 0.959 _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'Stoe IPDS 2' _diffrn_measurement_method 'rotation method' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0350 _diffrn_reflns_av_unetI/netI 0.0197 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 40 _diffrn_reflns_limit_l_min -40 _diffrn_reflns_number 4345 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.465 _diffrn_reflns_theta_min 3.110 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 40 _diffrn_source_power 2.000 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.612 _exptl_absorpt_correction_T_max 0.9408 _exptl_absorpt_correction_T_min 0.6823 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; Coppens (1970) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 2.036 _exptl_crystal_description needle _exptl_crystal_F_000 1152 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.227 _refine_diff_density_min -0.327 _refine_ls_abs_structure_details ; Classical Flack method preferred over Parsons because s.u. lower ; _refine_ls_abs_structure_Flack -0.08(10) _refine_ls_extinction_coef 0.055(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2018/3 (Sheldrick 2015) ; _refine_ls_goodness_of_fit_ref 1.176 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 78 _refine_ls_number_reflns 1088 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.175 _refine_ls_R_factor_all 0.0214 _refine_ls_R_factor_gt 0.0214 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0413P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0534 _refine_ls_wR_factor_ref 0.0534 _reflns_number_gt 1087 _reflns_number_total 1088 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ru2076sup1.cif _cod_data_source_block Na3_Li_2SO4_6H2O-180K _cod_original_cell_volume 1840.3(10) _cod_database_code 2243891 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 2 -4 0 793.10 2.52 0 4 -2 0 740.74 2.40 0 4 -2 0 758.08 4.98 0 -2 4 0 715.18 2.39 0 -4 2 0 731.11 2.32 0 6 -3 0 3079.65 4.05 0 -6 3 0 3252.01 3.99 0 -3 6 0 3074.29 4.14 0 6 -6 0 4289.61 4.76 0 6 0 0 3900.81 3.96 0 -6 6 0 4162.35 4.76 0 -2 7 0 4511.98 4.69 0 7 -5 0 4691.28 4.93 0 5 -7 0 4882.56 5.08 0 -7 5 0 4387.16 4.49 0 5 2 0 4479.66 4.19 0 -5 7 0 4436.92 4.92 0 7 -2 0 4264.56 4.29 0 8 -4 0 7001.51 5.58 0 -8 4 0 7123.79 5.31 0 8 -7 0 4697.75 4.98 0 7 -8 0 4749.33 4.96 0 -1 8 0 4527.46 4.53 0 -8 1 0 4053.55 7.03 0 -7 -1 0 4118.97 5.47 0 7 1 0 3997.66 3.88 0 -7 8 0 4050.17 4.53 0 -8 7 0 3989.59 4.28 0 8 -1 0 3909.97 3.88 0 -3 9 0 3647.05 4.25 0 9 -6 0 3610.09 4.03 0 -6 9 0 3560.78 4.23 0 9 -3 0 3547.98 3.78 0 6 3 0 3736.16 3.74 0 -9 6 0 3761.69 4.05 0 -9 0 0 1725.66 4.33 0 9 -9 0 2117.51 3.49 0 0 9 0 1896.63 2.91 0 9 0 0 1824.44 2.82 0 -9 9 0 1773.87 3.11 0 5 5 0 1014.50 2.05 0 10 -5 0 987.33 2.15 0 -5 10 0 995.09 2.47 0 10 -8 0 2710.44 3.70 0 8 -10 0 3015.68 4.12 0 -8 -2 0 2427.46 4.07 0 -2 10 0 2638.82 3.66 0 -10 8 0 2498.91 3.35 0 10 -2 0 2431.02 3.11 0 -8 10 0 2493.78 3.67 0 8 2 0 2581.32 3.20 0 11 -7 0 1455.00 2.68 0 -4 11 0 1414.91 2.88 0 -7 -4 0 1427.14 3.05 0 11 -4 0 1415.10 2.65 0 -7 11 0 1379.48 2.95 0 7 4 0 1437.11 2.50 0 11 -10 0 1228.80 2.79 0 10 -11 0 1333.49 3.25 0 1 10 0 1178.93 2.60 0 -1 11 0 1088.47 2.58 0 -10 11 0 1015.28 2.61 0 10 1 0 980.37 2.14 0 11 -1 0 986.20 2.14 0 -11 10 0 1024.54 2.56 0 -6 12 0 1981.86 3.53 0 12 -6 0 1920.47 3.13 0 6 6 0 1954.14 2.78 0 -6 -6 0 1912.87 3.13 0 -9 -3 0 2566.83 4.42 0 12 -9 0 2810.75 3.95 0 -3 12 0 2568.44 3.69 0 12 -3 0 2344.76 3.17 0 -9 12 0 2500.90 3.91 0 9 3 0 2424.62 3.12 0 -3 2 1 2937.45 5.11 0 3 -1 1 2788.31 4.71 0 3 -2 -1 2966.48 5.37 0 2 -3 -1 2941.26 5.42 0 -3 1 -1 2934.11 4.78 0 -1 3 -1 2951.12 4.87 0 3 -4 1 3375.32 4.80 0 4 -3 1 3345.52 4.86 0 -3 4 -1 3086.71 4.55 0 4 -1 -1 3012.83 4.24 0 -4 3 -1 3293.78 4.72 0 -6 5 1 298.24 1.68 0 5 1 1 275.41 1.28 0 6 -1 1 289.58 1.56 0 -5 6 1 287.35 1.69 0 6 -5 -1 312.69 1.58 0 -6 1 -1 298.09 2.32 0 5 -6 -1 317.05 1.58 0 -1 6 -1 308.49 1.74 0 4 -6 1 2665.08 3.84 0 6 -4 1 2528.29 3.68 0 -2 6 1 2523.96 3.71 0 -4 6 -1 2482.07 3.71 0 6 -2 -1 2375.62 3.39 0 -6 4 -1 2406.91 3.44 0 7 -3 1 451.23 1.87 0 -4 7 1 419.30 1.87 0 -7 4 1 441.28 1.64 0 -7 3 -1 454.12 1.63 0 -3 7 -1 438.16 1.67 0 7 -4 -1 441.93 1.69 0 -6 -1 1 1150.68 3.01 0 7 -6 1 1373.75 2.93 0 6 -7 1 1280.01 2.63 0 -7 1 1 1208.62 3.78 0 -1 7 1 1298.67 2.57 0 7 -1 -1 1112.35 2.23 0 6 1 -1 1131.08 2.20 0 -6 7 -1 1151.04 2.49 0 -7 6 -1 1155.16 2.43 0 6 2 1 217.23 1.17 0 8 -2 1 225.93 1.26 0 -6 8 1 229.13 1.58 0 -8 6 1 221.69 1.49 0 -2 8 -1 239.70 1.57 0 8 -6 -1 232.67 1.63 0 6 -8 -1 248.54 1.45 0 8 -6 -1 229.67 2.60 0 -3 8 1 1068.19 2.51 0 8 -5 1 1079.32 2.32 0 -5 8 -1 995.01 2.29 0 -8 5 -1 1075.00 2.18 0 8 -3 -1 1044.27 2.23 0 9 -1 1 718.32 2.03 0 -9 8 1 733.10 2.22 0 8 1 1 706.23 1.79 0 -8 9 1 740.28 2.10 0 1 8 -1 815.01 1.99 0 8 -9 -1 851.62 2.31 0 9 -8 -1 835.06 2.33 0 -8 -1 -1 721.03 2.64 0 -1 9 -1 765.36 2.00 0 5 4 1 221.85 1.44 0 9 -4 1 244.86 1.52 0 -5 9 1 222.03 1.54 0 9 -5 -1 228.80 1.58 0 -4 9 -1 216.80 1.27 0 7 -9 1 908.65 2.48 0 -2 9 1 780.04 2.21 0 -7 -2 1 757.43 2.49 0 9 -7 1 849.48 2.33 0 -7 9 -1 763.52 2.26 0 9 -2 -1 766.95 2.05 0 7 2 -1 747.64 1.78 0 -9 7 -1 745.23 1.90 0 -10 7 1 87.89 1.09 0 7 3 1 87.79 1.33 0 10 -3 1 85.00 1.09 0 -7 10 1 88.45 1.10 0 -3 10 -1 87.67 1.11 0 10 -7 -1 94.63 1.49 0 -7 -3 -1 82.06 1.15 0 -6 -4 1 484.42 2.06 0 -4 10 1 481.40 1.97 0 10 -6 1 501.69 1.74 0 -6 10 -1 565.63 2.04 0 10 -4 -1 481.79 1.82 0 6 4 -1 505.38 1.59 0 -10 6 -1 493.40 1.63 0 -9 -1 1 175.68 1.81 0 -1 10 1 193.65 1.64 0 9 -10 1 228.46 1.88 0 10 -9 1 208.65 1.85 0 1 9 1 206.50 1.36 0 9 1 -1 173.32 1.19 0 10 -1 -1 166.48 1.26 0 -9 10 -1 174.72 1.59 0 -10 9 -1 168.64 1.46 0 11 -2 1 114.58 1.45 0 -9 11 1 122.79 1.59 0 9 2 1 111.51 1.19 0 -11 9 1 120.78 1.53 0 -9 -2 -1 119.91 1.37 0 11 -9 -1 143.20 1.60 0 -2 11 -1 123.98 1.26 0 2 9 -1 141.30 1.30 0 -6 11 1 323.64 1.62 0 11 -5 1 342.05 1.73 0 6 5 1 328.18 1.40 0 11 -6 -1 328.02 1.48 0 -5 11 -1 323.18 1.55 0 -8 -3 1 29.06 1.43 0 -3 11 1 18.62 1.03 0 11 -8 1 21.29 1.08 0 -8 11 -1 23.14 1.41 0 -11 8 -1 20.79 1.01 0 8 3 -1 13.23 1.35 0 11 -3 -1 22.43 1.00 0 8 4 1 175.77 1.57 0 -8 12 1 157.35 1.46 0 12 -4 1 182.38 1.61 0 -8 -4 -1 173.66 1.43 0 12 -8 -1 185.81 1.62 0 -4 12 -1 176.58 1.37 0 5 7 1 256.04 1.69 0 -7 -5 1 250.50 1.52 0 12 -7 1 273.29 1.64 0 -5 12 1 240.82 1.51 0 -7 12 -1 248.52 1.52 0 12 -5 -1 248.13 1.45 0 7 5 -1 266.63 1.35 0 1 -1 2 298.51 2.49 0 -1 0 2 308.88 3.34 0 -1 1 -2 276.97 2.66 0 1 0 -2 309.02 3.49 0 -2 2 2 1285.51 4.45 0 2 0 2 1243.89 3.43 0 -2 0 -2 1322.20 3.55 0 2 -2 -2 1245.56 4.37 0 3 -2 2 3667.41 5.49 0 3 -1 -2 3358.33 5.17 0 -3 2 -2 3630.01 5.37 0 -4 3 2 3550.06 5.13 0 3 1 2 3484.75 4.37 0 4 -1 2 3392.51 4.48 0 -4 1 -2 3494.18 4.54 0 4 -3 -2 3578.65 5.42 0 -1 4 -2 3534.38 4.65 0 -4 0 2 580.52 2.46 0 4 -4 2 578.92 2.00 0 -4 4 -2 550.11 1.93 0 4 0 -2 541.27 1.80 0 -5 5 2 1906.05 3.51 0 5 0 2 1805.38 2.85 0 -5 0 -2 2023.31 4.53 0 5 -5 -2 1943.11 3.64 0 5 -3 2 1493.02 2.97 0 -2 5 2 1504.98 3.25 0 3 -5 2 1592.58 3.18 0 5 -2 -2 1500.10 3.05 0 -5 3 -2 1436.12 2.78 0 -3 5 -2 1424.62 2.98 0 -6 4 2 2264.29 3.47 0 -4 6 2 2156.94 3.71 0 6 -2 2 2207.93 3.23 0 4 2 2 2436.11 3.30 0 6 -4 -2 2258.59 6.02 0 -2 6 -2 2357.65 3.56 0 -6 2 -2 2354.88 3.27 0 6 -4 -2 2341.53 3.68 0 4 -6 -2 2478.68 3.99 0 -5 -1 2 375.98 1.95 0 -1 6 2 386.43 1.81 0 -6 1 2 371.66 2.28 0 5 -6 2 394.80 1.63 0 6 -5 2 395.82 1.86 0 6 -1 -2 349.89 1.60 0 -5 6 -2 369.38 1.73 0 -6 5 -2 352.72 1.55 0 5 1 -2 353.63 1.57 0 7 -1 2 1190.53 2.31 0 6 1 2 1184.00 2.24 0 -7 6 2 1260.13 2.73 0 -6 7 2 1219.01 2.70 0 -7 1 -2 1254.54 4.33 0 -1 7 -2 1273.73 2.46 0 -6 -1 -2 1212.30 3.21 0 7 -6 -2 1352.79 2.97 0 6 -7 -2 1326.62 3.00 0 7 -4 2 331.76 1.72 0 -3 7 2 327.19 1.77 0 -4 7 -2 310.96 1.67 0 -7 4 -2 320.52 1.62 0 7 -3 -2 327.48 1.72 0 7 -7 2 135.82 1.18 0 -7 0 2 124.35 1.59 0 0 7 2 135.93 1.18 0 -7 7 -2 115.02 1.06 0 7 0 -2 115.12 1.03 0 -8 8 2 1007.75 2.39 0 8 0 2 1007.60 2.06 0 8 -8 -2 1160.32 2.64 0 0 8 -2 1100.81 2.27 0 -8 0 -2 1035.57 3.41 0 5 3 2 210.03 1.17 0 -8 5 2 219.67 1.48 0 8 -3 2 225.51 1.50 0 -5 8 2 214.84 1.52 0 8 -5 -2 232.20 1.36 0 -3 8 -2 218.49 1.26 0 6 -8 2 186.89 1.32 0 -6 -2 2 166.29 1.55 0 8 -6 2 182.57 1.25 0 -2 8 2 186.35 1.49 0 -8 6 -2 170.89 1.42 0 8 -2 -2 167.32 1.48 0 6 2 -2 160.97 1.08 0 -6 8 -2 168.54 1.21 0 -9 7 2 354.59 1.72 0 7 2 2 334.31 1.35 0 -7 9 2 344.88 1.82 0 9 -2 2 333.42 1.41 0 9 -7 -2 337.72 3.04 0 -2 9 -2 355.39 1.70 0 9 -7 -2 361.01 1.63 0 7 -9 -2 409.47 1.74 0 -7 -2 -2 335.28 1.66 0 9 -5 2 325.20 1.66 0 -4 9 2 288.25 1.65 0 9 -4 -2 300.08 1.38 0 -9 5 -2 307.72 1.33 0 -5 9 -2 293.81 1.58 0 8 -9 2 54.06 1.46 0 -8 -1 2 39.16 1.39 0 9 -8 2 58.40 1.12 0 -1 9 2 47.87 1.32 0 8 1 -2 44.48 1.27 0 9 -1 -2 52.13 0.98 0 -9 8 -2 42.35 1.29 0 -8 9 -2 44.01 1.31 0 10 -1 2 237.51 1.31 0 -9 10 2 258.14 1.73 0 -10 9 2 242.05 1.57 0 9 1 2 239.57 1.33 0 9 -10 -2 302.52 1.76 0 -1 10 -2 249.71 1.64 0 10 -9 -2 235.93 2.42 0 1 9 -2 290.56 1.75 0 10 -9 -2 301.39 1.96 0 -9 -1 -2 240.16 1.95 0 -6 10 2 603.05 1.99 0 6 4 2 648.68 1.92 0 10 -4 2 619.66 1.78 0 -4 10 -2 616.98 2.00 0 10 -6 -2 630.98 2.12 0 -3 10 2 253.18 1.64 0 10 -7 2 263.82 1.40 0 -7 -3 2 245.49 1.76 0 7 3 -2 241.22 1.21 0 -7 10 -2 240.28 1.65 0 10 -3 -2 252.05 1.59 0 -10 7 -2 247.05 1.30 0 10 -10 2 924.21 4.15 0 10 -10 2 1083.19 2.61 0 0 10 2 940.71 2.25 0 -10 10 -2 861.79 2.35 0 10 0 -2 831.34 1.96 0 -8 11 2 159.00 1.63 0 11 -3 2 151.72 1.17 0 8 3 2 151.83 1.22 0 -8 -3 -2 156.32 1.69 0 -3 11 -2 153.28 1.48 0 11 -8 -2 158.20 1.73 0 5 6 2 8.12 1.29 0 11 -6 2 13.51 0.99 0 -6 -5 2 9.79 1.02 0 -5 11 2 9.68 0.97 0 -6 11 -2 11.66 1.18 0 11 -5 -2 7.03 1.34 0 6 5 -2 13.79 1.24 0 2 9 2 28.62 1.13 0 -2 11 2 24.80 1.09 0 9 -11 2 24.11 1.46 0 11 -9 2 23.79 1.14 0 -9 -2 2 27.22 1.37 0 -11 9 -2 29.72 1.33 0 -9 11 -2 23.41 1.32 0 11 -2 -2 31.84 1.42 0 9 2 -2 16.22 1.24 0 -5 -7 2 34.96 1.07 0 7 5 2 30.51 1.05 0 -7 12 2 35.94 1.42 0 12 -5 2 32.34 1.05 0 12 -7 -2 36.77 1.08 0 -5 12 -2 31.97 1.02 0 -7 -5 -2 30.93 1.10 0 5 7 -2 29.97 1.03 0 12 -8 2 62.61 1.20 0 -8 -4 2 57.06 1.40 0 4 8 2 59.94 1.42 0 -4 12 2 57.15 1.33 0 12 -4 -2 62.18 1.44 0 -8 12 -2 61.53 1.46 0 8 4 -2 59.90 1.09 0 -1 2 3 1036.57 4.74 0 2 -1 3 1027.71 3.57 0 1 -2 3 1062.43 3.33 0 2 -1 -3 1001.01 3.84 0 2 -1 -3 1072.84 4.84 0 -1 2 -3 1032.50 3.40 0 -2 1 -3 981.27 3.29 0 -2 4 3 560.08 2.47 0 4 -2 3 595.20 2.11 0 -4 2 3 631.47 2.31 0 2 -4 3 668.69 2.28 0 4 -2 -3 624.35 2.37 0 -2 4 -3 576.84 2.04 0 4 -2 -3 591.79 3.13 0 -4 2 -3 573.31 2.01 0 4 1 3 1667.02 2.84 0 5 -1 3 1663.35 2.92 0 -5 4 3 1770.46 3.44 0 -4 5 3 1733.54 3.64 0 4 -5 -3 1741.12 3.66 0 5 -4 -3 1801.43 3.60 0 -5 1 -3 1749.77 5.78 0 -1 5 -3 1793.91 3.05 0 4 -5 3 3762.97 4.51 0 5 -4 3 3359.25 4.34 0 -4 -1 3 3413.94 4.90 0 5 -1 -3 2980.31 3.86 0 -5 4 -3 3055.69 4.04 0 -4 5 -3 3011.19 4.02 0 -3 6 3 85.52 1.32 0 6 -3 3 74.47 1.28 0 -3 6 -3 79.84 1.03 0 -6 3 -3 74.92 0.96 0 6 -3 -3 85.37 1.37 0 6 -3 -3 77.86 1.65 0 5 2 3 914.65 2.19 0 -7 5 3 888.90 2.21 0 7 -2 3 894.63 2.11 0 -5 7 3 860.59 2.53 0 -2 7 -3 970.82 2.38 0 7 -5 -3 979.14 2.58 0 7 -5 -3 899.13 3.60 0 5 -7 -3 1008.24 2.77 0 5 -7 3 1130.54 2.61 0 -5 -2 3 981.35 2.47 0 7 -5 3 1023.12 2.33 0 -2 7 3 997.65 2.44 0 -7 5 -3 950.98 2.16 0 7 -2 -3 975.13 2.20 0 -5 7 -3 956.38 2.21 0 -7 8 3 887.52 2.48 0 7 1 3 869.55 2.08 0 8 -1 3 883.14 2.14 0 -8 7 3 874.96 2.34 0 8 -7 -3 1012.13 2.70 0 7 -8 -3 980.03 2.46 0 -8 1 -3 850.19 3.85 0 -1 8 -3 945.24 2.12 0 -7 -1 -3 828.49 2.72 0 -4 8 3 589.41 1.99 0 8 -4 3 634.22 1.83 0 8 -4 -3 618.42 1.88 0 -8 4 -3 621.94 1.77 0 -4 8 -3 579.58 1.78 0 8 -7 3 1397.29 2.69 0 -8 1 3 1199.75 3.59 0 -7 -1 3 1225.45 3.04 0 7 -8 3 1406.76 2.65 0 -1 8 3 1291.16 2.58 0 -7 8 -3 1244.17 2.61 0 7 1 -3 1153.64 2.16 0 -8 7 -3 1194.84 2.38 0 8 -1 -3 1152.86 2.20 0 6 3 3 887.99 2.13 0 -6 9 3 807.76 2.29 0 9 -3 3 828.73 1.98 0 -9 6 3 849.21 2.09 0 9 -6 -3 883.41 2.22 0 -3 9 -3 871.33 2.28 0 -3 9 3 595.92 1.93 0 -6 -3 3 610.92 2.16 0 9 -6 3 622.83 1.81 0 -9 6 -3 615.50 1.94 0 6 3 -3 600.08 1.67 0 9 -3 -3 637.36 2.00 0 -6 9 -3 589.38 1.85 0 10 -2 3 249.67 1.63 0 8 2 3 235.29 1.31 0 -8 10 3 242.26 1.51 0 -10 8 3 243.18 1.68 0 10 -8 -3 269.15 1.56 0 -8 -2 -3 229.03 1.75 0 8 -10 -3 284.82 1.86 0 -2 10 -3 257.52 1.67 0 10 -8 -3 231.76 3.20 0 10 -5 3 464.96 1.85 0 5 5 3 468.70 1.58 0 -5 10 3 442.95 1.90 0 -5 10 -3 441.31 1.86 0 10 -5 -3 440.86 1.64 0 -8 -2 3 209.89 1.74 0 10 -8 3 228.38 1.71 0 8 -10 3 241.07 1.48 0 -2 10 3 213.51 1.68 0 8 2 -3 192.83 1.21 0 -8 10 -3 209.90 1.61 0 -10 8 -3 210.74 1.56 0 10 -2 -3 197.05 1.28 0 10 1 3 119.85 1.47 0 -10 11 3 100.42 1.43 0 -11 10 3 116.30 1.49 0 11 -1 3 103.44 1.19 0 11 -10 -3 130.27 1.80 0 11 -10 -3 99.96 2.65 0 1 10 -3 116.51 1.24 0 -1 11 -3 121.43 1.55 0 10 -11 -3 149.54 1.87 0 -7 11 3 678.58 2.39 0 7 4 3 671.99 1.80 0 11 -4 3 672.05 2.04 0 -4 11 -3 648.14 1.93 0 11 -7 -3 687.22 2.24 0 -7 -4 -3 669.03 2.29 0 11 -7 3 135.45 1.51 0 -7 -4 3 119.54 1.53 0 -4 11 3 117.65 1.49 0 4 7 3 122.99 1.16 0 11 -4 -3 133.06 1.44 0 -11 7 -3 125.93 1.32 0 -7 11 -3 119.18 1.45 0 7 4 -3 119.18 1.12 0 -10 -1 3 4.67 1.40 0 10 -11 3 6.73 1.65 0 11 -10 3 16.78 1.16 0 -1 11 3 48.79 1.44 0 10 -11 3 13.23 1.20 0 1 10 3 9.73 1.07 0 -11 10 -3 10.42 1.30 0 11 -1 -3 -2.35 1.22 0 10 1 -3 12.46 0.95 0 -10 11 -3 12.02 1.00 0 -9 12 3 241.46 1.83 0 12 -3 3 232.37 1.39 0 9 3 3 238.87 1.70 0 -9 -3 -3 232.87 1.94 0 -3 12 -3 244.50 1.47 0 6 6 3 81.28 1.42 0 -6 -6 3 66.30 1.16 0 12 -6 3 69.06 1.10 0 -6 12 3 62.61 1.16 0 12 -6 -3 65.21 1.43 0 6 6 -3 68.42 1.09 0 -6 12 -3 65.45 1.41 0 12 -9 3 346.10 1.71 0 -3 12 3 330.88 1.85 0 -9 -3 3 317.27 1.83 0 -12 9 -3 326.98 1.51 0 12 -3 -3 307.88 1.50 0 -9 12 -3 335.30 1.93 0 9 3 -3 323.91 1.48 0 -3 -1 4 1228.84 3.20 0 -4 1 4 1205.95 3.72 0 3 -4 4 1165.92 2.71 0 -1 4 4 1239.96 3.27 0 4 -3 4 1202.74 2.88 0 -3 4 -4 973.02 2.47 0 4 -1 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1 4 1031.73 2.09 0 -9 8 4 1010.20 2.38 0 -8 -1 -4 952.04 3.02 0 8 -9 -4 1154.18 2.88 0 1 8 -4 1098.01 2.20 0 -1 9 -4 1058.78 2.41 0 9 -8 -4 1149.33 2.76 0 -5 9 4 502.74 1.85 0 9 -4 4 557.14 1.71 0 5 4 4 571.15 1.84 0 -4 9 -4 521.53 1.87 0 9 -5 -4 531.13 1.98 0 -7 -2 4 360.37 1.67 0 -2 9 4 380.33 1.82 0 7 -9 4 421.10 1.64 0 9 -7 4 532.17 1.71 0 9 -2 -4 362.85 1.68 0 -9 7 -4 361.49 1.61 0 7 2 -4 352.07 1.54 0 -7 9 -4 338.95 1.48 0 -10 10 4 1189.12 2.67 0 10 0 4 1213.56 2.29 0 0 10 -4 1357.73 2.50 0 10 -10 -4 1575.90 3.50 0 10 -3 4 1491.18 2.45 0 -7 10 4 1567.46 3.32 0 7 3 4 1494.58 2.41 0 10 -7 -4 1545.24 2.86 0 -3 10 -4 1473.50 2.60 0 4 6 4 2949.14 3.44 0 -4 10 4 2852.65 4.14 0 10 -6 4 2908.74 3.51 0 -6 -4 4 2911.93 3.93 0 -10 6 -4 2905.03 3.47 0 10 -4 -4 2733.09 3.55 0 6 4 -4 2809.19 3.18 0 -6 10 -4 2793.80 3.72 0 10 -9 4 1893.68 3.29 0 1 9 4 1929.86 3.19 0 9 -10 4 2022.62 3.27 0 -1 10 4 1833.17 3.25 0 -9 -1 4 1633.35 3.51 0 9 1 -4 1610.02 2.68 0 -10 9 -4 1552.95 2.71 0 -9 10 -4 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577.29 2.06 0 -2 5 5 541.19 2.31 0 3 -5 5 582.47 1.89 0 -5 3 -5 527.41 1.79 0 5 -2 -5 573.89 2.78 0 -3 5 -5 512.88 1.77 0 5 -2 -5 549.06 1.91 0 -6 4 5 206.36 1.58 0 -4 6 5 187.59 1.62 0 6 -2 5 205.62 1.49 0 4 2 5 201.54 1.42 0 6 -4 -5 190.49 1.90 0 -6 2 -5 202.29 1.18 0 -2 6 -5 195.49 1.25 0 4 -6 -5 216.33 1.54 0 6 -4 -5 216.31 1.66 0 6 -5 5 41.34 1.22 0 -5 -1 5 35.22 0.92 0 -1 6 5 39.13 0.93 0 6 -5 5 39.50 1.62 0 -6 1 5 41.76 1.29 0 5 -6 5 38.63 0.93 0 -5 6 -5 34.97 0.84 0 -6 5 -5 44.09 0.87 0 6 -1 -5 33.39 0.78 0 -6 7 5 355.37 1.75 0 6 1 5 363.80 1.63 0 -7 6 5 360.62 1.80 0 7 -1 5 363.23 1.46 0 -7 1 -5 360.96 2.93 0 6 -7 -5 384.63 1.79 0 -1 7 -5 386.66 1.76 0 7 -6 -5 392.38 2.04 0 -3 7 5 332.51 1.84 0 7 -4 5 347.77 1.49 0 7 -3 -5 331.61 1.51 0 -7 4 -5 335.10 1.61 0 -4 7 -5 313.63 1.42 0 5 3 5 1782.10 2.66 0 -5 8 5 1780.07 3.54 0 8 -3 5 1784.96 2.87 0 8 -5 -5 1839.27 3.12 0 -3 8 -5 1805.22 2.91 0 8 -5 -5 1784.74 5.06 0 8 -6 5 1691.47 2.82 0 -2 8 5 1647.21 3.23 0 6 -8 5 1742.97 2.87 0 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1105.25 3.14 0 2 -1 -6 1118.76 3.83 0 -2 1 -6 1004.85 3.02 0 -2 1 -6 1110.38 5.30 0 -1 2 -6 1055.28 2.93 0 3 0 6 1896.97 3.57 0 -3 3 6 1985.01 5.11 0 3 -3 -6 1831.33 4.95 0 -3 0 -6 1897.21 3.50 0 2 2 6 491.64 2.01 0 -2 4 6 474.64 2.59 0 4 -2 6 496.60 1.90 0 2 -4 6 517.26 2.03 0 4 -2 -6 514.71 2.62 0 4 -2 -6 453.46 1.97 0 -2 4 -6 494.00 1.94 0 -4 2 -6 510.06 2.00 0 -4 5 6 703.15 2.81 0 -5 4 6 749.32 2.39 0 5 -1 6 718.46 2.00 0 4 1 6 681.12 1.91 0 4 -5 -6 731.97 2.79 0 -5 1 -6 756.36 2.15 0 -1 5 -6 735.79 1.98 0 5 -4 -6 778.09 2.74 0 4 -5 6 1170.07 2.48 0 5 -4 6 1257.02 5.49 0 -4 -1 6 1134.93 2.94 0 -5 1 6 1101.21 3.15 0 5 -4 6 1151.21 2.50 0 -1 5 6 1227.77 3.15 0 5 -1 -6 1058.79 2.37 0 -5 4 -6 1103.71 2.39 0 -4 5 -6 1066.39 2.36 0 -6 6 6 639.75 2.30 0 6 0 6 627.54 1.92 0 6 -6 -6 668.31 2.43 0 0 6 -6 706.49 2.08 0 -3 6 6 685.22 2.52 0 6 -3 6 713.79 1.96 0 3 3 6 723.30 1.96 0 6 -3 -6 706.89 2.30 0 -3 6 -6 671.90 1.88 0 6 -3 -6 717.70 2.94 0 -6 3 -6 673.73 1.83 0 6 -6 6 4056.34 4.27 0 -6 0 6 3926.98 5.28 0 6 0 -6 3655.56 3.84 0 -6 6 -6 3818.93 4.11 0 7 -2 6 402.79 1.54 0 5 2 6 373.19 1.42 0 -7 5 6 427.43 1.89 0 -5 7 6 397.25 2.04 0 5 -7 -6 450.16 1.97 0 7 -5 -6 388.19 2.35 0 -2 7 -6 398.74 1.51 0 7 -5 -6 429.75 1.99 0 -2 7 6 821.25 2.52 0 5 -7 6 916.91 2.33 0 -5 -2 6 821.57 2.42 0 7 -5 6 835.38 2.09 0 -5 7 -6 777.36 2.12 0 -7 5 -6 748.73 1.93 0 7 -2 -6 745.46 1.96 0 7 1 6 162.87 1.41 0 -7 8 6 164.86 1.49 0 -8 7 6 167.25 1.45 0 8 -1 6 168.86 1.39 0 1 7 -6 188.62 1.18 0 -1 8 -6 167.42 1.18 0 8 -7 -6 194.31 1.70 0 7 -8 -6 189.65 1.62 0 -8 1 -6 167.47 2.57 0 -4 -4 6 846.08 2.10 0 8 -4 6 894.11 2.18 0 -4 8 6 822.31 2.56 0 4 4 6 836.15 1.96 0 8 -4 -6 843.33 2.28 0 -4 8 -6 795.59 1.97 0 -8 4 -6 870.27 2.07 0 8 -7 6 164.38 1.23 0 8 -7 6 159.46 2.92 0 -1 8 6 158.40 1.24 0 7 -8 6 169.70 1.24 0 -7 -1 6 139.52 1.26 0 -8 7 -6 148.92 1.40 0 8 -1 -6 138.95 1.07 0 7 1 -6 142.22 1.31 0 -7 8 -6 138.47 1.11 0 9 0 6 637.41 1.99 0 -9 9 6 603.59 2.18 0 0 9 -6 677.09 2.05 0 -9 0 -6 593.97 3.16 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84.74 1.30 0 -10 6 -7 89.02 1.03 0 10 -9 7 294.38 1.55 0 9 -10 7 309.59 1.59 0 1 9 7 282.30 1.51 0 -1 10 7 275.71 1.81 0 -9 -1 7 252.20 1.81 0 9 -10 7 251.61 2.10 0 10 -1 -7 247.84 1.49 0 -9 10 -7 258.51 1.67 0 9 1 -7 237.66 1.56 0 -10 9 -7 251.44 1.53 0 -9 11 7 13.43 1.31 0 11 -2 7 10.79 0.99 0 9 2 7 12.23 0.98 0 2 9 -7 6.70 1.41 0 11 -9 -7 8.63 1.82 0 -2 11 -7 0.69 1.02 0 11 -9 -7 12.77 1.13 0 -9 -2 -7 12.64 1.35 0 -5 -6 7 42.52 1.31 0 -6 11 7 37.85 1.35 0 6 5 7 36.38 1.32 0 11 -5 7 37.24 1.01 0 11 -6 -7 41.68 1.04 0 -5 11 -7 29.34 1.01 0 -3 11 7 232.70 1.66 0 3 8 7 234.88 1.62 0 -8 -3 7 223.85 1.79 0 11 -8 7 250.03 1.44 0 -11 8 -7 226.49 1.28 0 -8 11 -7 217.48 1.36 0 8 3 -7 227.46 1.25 0 11 -3 -7 220.53 1.36 0 -4 -8 7 196.85 1.40 0 12 -4 7 207.49 1.50 0 -8 12 7 208.25 1.88 0 8 4 7 211.61 1.59 0 12 -8 -7 214.30 1.79 0 -4 12 -7 215.05 1.61 0 -8 -4 -7 169.93 1.60 0 -5 12 7 125.43 1.65 0 12 -7 7 124.12 1.21 0 5 7 7 130.77 1.21 0 -7 -5 7 131.30 1.29 0 -7 12 -7 116.37 1.17 0 7 5 -7 120.51 1.15 0 12 -5 -7 113.19 1.19 0 0 -2 8 3323.85 5.31 0 2 0 8 3127.56 5.13 0 0 2 -8 3391.85 4.68 0 -2 0 -8 3214.95 5.20 0 2 -3 8 4214.05 4.89 0 -2 -1 8 4235.18 5.65 0 3 -2 8 3874.27 4.86 0 -3 2 -8 3734.29 4.69 0 3 -1 -8 4029.28 6.16 0 -2 3 -8 3770.68 4.65 0 4 -1 8 3374.10 4.33 0 3 1 8 3607.90 4.55 0 -1 4 -8 3246.89 4.02 0 -4 1 -8 3131.62 4.01 0 -4 0 8 5847.92 6.46 0 2 3 8 3648.85 4.59 0 -3 -2 8 3460.79 4.56 0 5 -3 8 3440.44 4.20 0 3 -5 8 3657.41 4.13 0 -3 5 -8 3124.61 3.80 0 5 -2 -8 3085.16 4.29 0 -5 3 -8 3212.90 3.89 0 5 -2 -8 3257.94 5.41 0 4 2 8 610.31 1.80 0 -4 6 8 641.91 2.65 0 6 -2 8 635.97 1.80 0 -2 6 -8 559.00 1.70 0 -6 2 -8 555.18 1.64 0 6 -4 -8 576.72 2.10 0 6 -4 -8 541.72 2.30 0 6 -5 8 2840.20 3.55 0 5 -6 8 2916.53 3.62 0 -5 -1 8 2949.21 4.18 0 -6 1 8 2813.35 4.56 0 -1 6 8 3013.24 4.56 0 6 -1 -8 2489.75 3.43 0 -6 5 -8 2669.60 3.50 0 -5 6 -8 2630.80 3.29 0 6 1 8 2567.24 3.19 0 7 -1 8 2578.79 3.18 0 -7 6 8 2745.44 4.20 0 -6 7 8 2708.50 4.57 0 7 -6 -8 2937.18 4.55 0 6 -7 -8 3047.75 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11 -8 -8 1157.64 2.95 0 -6 -5 8 72.55 1.45 0 5 6 8 79.80 1.38 0 -5 11 8 71.05 1.17 0 11 -6 8 68.28 1.10 0 -11 6 -8 60.89 1.30 0 11 -5 -8 73.92 1.11 0 -6 11 -8 62.92 1.30 0 -9 -2 8 1633.10 3.29 0 2 9 8 1849.84 3.10 0 9 -11 8 1737.67 4.21 0 11 -9 8 1925.87 3.15 0 -2 11 8 1797.43 3.56 0 9 -11 8 2122.27 3.28 0 9 2 -8 1603.83 2.72 0 11 -2 -8 1619.31 2.80 0 -9 11 -8 1718.75 2.86 0 -11 9 -8 1647.85 2.82 0 7 5 8 1309.09 2.45 0 -5 -7 8 1264.98 2.66 0 12 -5 8 1299.24 2.39 0 12 -7 -8 1307.59 2.93 0 -5 12 -8 1338.08 2.70 0 8 -12 8 798.58 2.72 0 4 8 8 810.18 2.28 0 -8 -4 8 808.53 2.55 0 -4 12 8 772.81 2.75 0 12 -8 8 845.54 2.30 0 12 -4 -8 736.16 2.02 0 -8 12 -8 783.32 2.11 0 8 4 -8 789.65 2.03 0 -12 8 -8 789.09 2.15 0 2 -4 9 972.96 2.42 0 -2 -2 9 953.25 2.59 0 4 -2 9 929.55 2.37 0 2 2 9 885.24 2.59 0 -2 4 9 875.99 4.26 0 4 -2 -9 836.14 2.70 0 -4 2 -9 906.75 5.01 0 -4 2 -9 928.52 2.40 0 -2 4 -9 866.04 2.16 0 4 -2 -9 910.29 2.87 0 4 1 9 2346.73 3.38 0 5 -1 9 2384.69 3.41 0 4 -5 -9 2558.71 5.51 0 5 -4 -9 2553.39 4.87 0 -1 5 -9 2538.30 3.40 0 -5 1 -9 2348.03 3.39 0 4 -5 9 227.75 1.47 0 4 -5 9 216.70 1.80 0 5 -4 9 232.90 2.57 0 -4 -1 9 262.09 1.65 0 -5 1 9 212.76 1.47 0 -1 5 9 240.20 1.79 0 5 -4 9 213.77 1.46 0 5 -1 -9 233.13 1.77 0 -5 4 -9 223.88 1.21 0 -4 5 -9 205.04 1.37 0 5 -1 -9 202.26 1.41 0 -3 -3 9 2972.04 3.93 0 3 3 9 2976.21 3.89 0 6 -3 9 2897.41 3.58 0 -3 6 -9 2677.03 3.35 0 -6 3 -9 2699.57 3.34 0 6 -3 -9 2733.34 4.75 0 6 -3 -9 2787.63 4.15 0 7 -2 9 1246.11 2.38 0 -5 7 9 1291.58 3.66 0 5 2 9 1251.42 2.39 0 7 -5 -9 1338.92 3.19 0 -7 2 -9 1261.11 2.31 0 7 -5 -9 1210.46 3.21 0 -2 7 -9 1282.60 2.37 0 5 -7 9 4016.93 4.13 0 -5 -2 9 3824.96 4.53 0 2 5 9 3592.20 4.21 0 -2 7 9 3669.20 5.21 0 7 -5 9 3685.18 4.08 0 -7 5 -9 3302.44 3.67 0 7 -2 -9 3148.68 3.84 0 -5 7 -9 3281.58 3.67 0 -7 8 9 139.31 1.48 0 8 -1 9 152.52 1.41 0 7 1 9 147.79 1.15 0 1 7 -9 158.40 1.50 0 7 -8 -9 158.27 1.75 0 -1 8 -9 148.14 1.36 0 8 -7 -9 167.34 1.77 0 8 -4 9 466.29 1.61 0 -4 -4 9 448.92 1.67 0 -4 8 9 426.31 2.17 0 4 4 9 432.05 1.58 0 8 -4 -9 436.41 2.41 0 -4 8 -9 419.68 1.50 0 -8 4 -9 417.62 1.43 0 8 -4 -9 451.24 1.94 0 -7 -1 9 838.06 2.50 0 7 -8 9 895.55 2.29 0 7 -8 9 785.46 2.74 0 8 -7 9 892.83 2.25 0 -1 8 9 822.48 2.35 0 -8 7 -9 806.22 2.11 0 7 1 -9 728.41 1.76 0 -7 8 -9 732.76 1.87 0 8 -1 -9 744.76 2.01 0 -3 -6 9 62.22 1.31 0 9 -3 9 64.57 1.25 0 6 3 9 65.24 0.94 0 -6 9 9 61.77 1.39 0 9 -6 -9 61.47 1.55 0 -3 9 -9 60.78 1.01 0 9 -6 -9 59.88 1.06 0 -3 9 9 54.64 1.29 0 3 6 9 54.73 0.96 0 9 -6 9 57.32 1.00 0 -6 -3 9 56.38 1.34 0 6 -9 9 66.71 1.06 0 -9 6 -9 55.31 1.13 0 9 -3 -9 54.15 1.01 0 -6 9 -9 51.70 1.16 0 -2 -8 9 124.24 1.22 0 8 2 9 139.07 1.18 0 10 -2 9 132.73 1.47 0 -8 10 9 117.49 1.30 0 2 8 -9 132.89 1.21 0 -8 -2 -9 115.20 1.33 0 10 -8 -9 110.26 1.89 0 10 -8 -9 134.05 1.38 0 -2 10 -9 117.84 1.47 0 5 5 9 425.76 1.54 0 -5 10 9 428.51 2.19 0 -5 -5 9 423.29 1.64 0 10 -5 9 435.97 1.54 0 10 -5 -9 422.71 1.87 0 -10 5 -9 437.09 1.68 0 -5 10 -9 395.96 1.48 0 8 -10 9 67.63 1.58 0 2 8 9 69.22 1.30 0 -2 10 9 64.97 1.13 0 10 -8 9 70.80 1.19 0 8 -10 9 73.66 1.39 0 -8 -2 9 64.25 1.14 0 8 2 -9 59.25 1.00 0 -10 8 -9 61.40 1.23 0 -8 10 -9 61.57 1.36 0 10 -2 -9 58.36 1.00 0 10 1 9 24.44 1.37 0 -1 -10 9 24.73 1.12 0 11 -1 9 23.10 1.02 0 -1 11 -9 29.69 1.10 0 11 -10 -9 28.28 1.30 0 11 -10 -9 19.57 1.53 0 1 10 -9 25.21 1.05 0 -7 11 9 61.13 1.50 0 7 4 9 58.05 1.09 0 -4 -7 9 59.94 1.46 0 11 -4 9 68.37 1.05 0 -4 11 -9 60.78 1.05 0 11 -7 -9 66.98 1.37 0 -7 -4 9 190.07 1.69 0 4 7 9 209.56 1.58 0 11 -7 9 213.79 1.65 0 -4 11 9 201.36 1.74 0 -11 7 -9 199.54 1.26 0 7 4 -9 190.15 1.21 0 11 -4 -9 187.91 1.33 0 -7 11 -9 188.28 1.29 0 -10 -1 9 66.18 1.47 0 10 -11 9 80.50 1.32 0 11 -10 9 78.13 1.63 0 -1 11 9 70.19 1.49 0 1 10 9 78.39 1.21 0 1 10 9 68.13 1.36 0 10 -11 9 68.06 2.04 0 -11 10 -9 65.41 1.09 0 -10 11 -9 66.68 1.44 0 11 -1 -9 61.07 1.09 0 10 1 -9 64.84 1.06 0 6 6 9 86.87 1.15 0 12 -6 9 99.35 1.15 0 -6 -6 9 86.58 1.18 0 -6 12 -9 89.71 1.43 0 12 -6 -9 91.58 1.45 0 0 -1 10 434.05 2.37 0 1 0 10 377.52 2.16 0 0 1 -10 394.31 1.92 0 -1 0 -10 391.25 2.26 0 0 1 -10 397.63 2.09 0 1 -1 -10 425.88 3.02 0 -2 0 10 2791.69 4.67 0 2 -2 10 2644.72 4.05 0 2 -2 10 2996.85 6.00 0 -2 2 -10 2763.31 5.54 0 2 0 -10 3021.23 5.14 0 -2 2 -10 2509.22 3.94 0 3 -1 10 791.18 2.37 0 1 -3 10 806.67 2.72 0 2 1 10 800.56 2.61 0 -1 -2 10 799.49 2.46 0 -3 1 -10 813.63 2.53 0 -2 -1 -10 853.20 2.70 0 -1 3 -10 780.34 2.19 0 3 -2 -10 771.56 3.16 0 -3 1 -10 761.33 3.37 0 0 -4 10 4451.20 4.95 0 4 0 10 4168.02 4.69 0 0 4 -10 4810.03 4.56 0 -4 0 -10 4326.76 4.74 0 1 3 10 307.86 1.68 0 3 -4 10 325.85 1.43 0 -3 -1 10 330.28 1.61 0 3 -4 10 331.91 2.00 0 4 -3 10 309.68 1.43 0 4 -1 -10 330.10 1.75 0 -4 3 -10 312.13 1.55 0 -3 4 -10 295.79 1.36 0 5 -2 10 1014.79 2.28 0 3 2 10 1020.32 2.51 0 -3 5 10 1013.59 4.39 0 -2 -3 10 1008.13 2.38 0 -5 2 -10 928.61 2.13 0 5 -3 -10 959.15 2.81 0 5 -3 -10 992.68 2.84 0 -2 5 -10 1005.01 2.27 0 5 -5 10 1083.94 3.57 0 5 -5 10 1047.28 2.20 0 -5 0 10 1038.80 2.78 0 -5 5 -10 958.48 2.11 0 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10 172.49 1.23 0 -3 -7 10 196.72 1.59 0 -7 10 10 171.82 1.69 0 10 -7 -10 161.95 1.91 0 -3 10 -10 167.45 1.49 0 10 -7 -10 190.38 1.62 0 -4 10 10 524.61 2.33 0 10 -6 10 555.28 1.70 0 4 6 10 530.91 1.70 0 -6 -4 10 536.24 1.79 0 10 -4 -10 502.74 1.74 0 -10 6 -10 519.66 1.69 0 -6 10 -10 507.86 1.83 0 1 9 10 1134.14 2.57 0 -1 10 10 1058.80 2.82 0 10 -9 10 1148.88 2.62 0 1 9 10 1081.05 2.72 0 9 -10 10 1007.94 3.86 0 9 -10 10 1193.62 2.50 0 -9 -1 10 1014.33 2.86 0 -10 9 -10 952.26 2.23 0 -9 10 -10 952.50 2.31 0 9 1 -10 894.31 2.21 0 10 -1 -10 908.74 2.08 0 11 -2 10 236.71 1.55 0 -2 -9 10 262.99 1.73 0 -9 11 10 239.86 1.97 0 9 2 10 239.27 1.37 0 -9 -2 -10 235.02 1.98 0 2 9 -10 274.73 1.71 0 -2 11 -10 239.51 1.65 0 11 -9 -10 259.26 1.95 0 11 -9 -10 222.46 2.19 0 11 -5 10 356.39 1.50 0 -5 -6 10 365.79 1.60 0 6 5 10 365.19 1.53 0 -6 11 10 380.54 2.32 0 11 -6 -10 366.55 1.89 0 -5 11 -10 347.43 1.48 0 8 -11 10 43.55 1.22 0 11 -8 10 37.63 1.15 0 -3 11 10 39.69 1.41 0 -8 -3 10 49.78 1.55 0 3 8 10 47.12 1.07 0 -8 11 -10 42.55 1.05 0 -11 8 -10 39.75 1.21 0 11 -3 -10 38.77 1.05 0 8 3 -10 37.96 1.01 0 -4 -8 10 17.70 1.07 0 12 -4 10 23.22 1.02 0 4 8 -10 23.55 1.07 0 -4 12 -10 18.85 1.31 0 12 -8 -10 23.75 1.49 0 7 -12 10 36.75 1.16 0 12 -7 10 42.30 1.05 0 5 7 10 41.22 1.37 0 -7 -5 10 36.71 1.12 0 -7 12 -10 39.21 1.33 0 7 5 -10 37.11 1.01 0 -12 7 -10 32.86 0.97 0 12 -5 -10 41.31 1.37 0 4 -1 11 642.92 2.15 0 1 -4 11 647.85 2.15 0 -1 -3 11 645.32 2.08 0 3 1 11 643.14 2.12 0 -1 4 -11 672.88 2.03 0 -4 1 -11 652.43 2.09 0 4 -3 -11 663.78 2.96 0 3 -5 11 20.21 0.82 0 2 3 11 15.52 1.12 0 -3 -2 11 16.82 1.16 0 3 -5 11 22.51 1.27 0 -2 5 11 18.13 1.33 0 5 -3 11 32.22 0.86 0 5 -2 -11 14.55 0.82 0 -5 3 -11 44.62 1.12 0 -3 5 -11 21.63 1.03 0 5 -2 -11 46.18 1.34 0 -4 6 11 895.75 3.85 0 6 -2 11 868.04 2.20 0 4 2 11 824.36 2.05 0 -2 -4 11 868.32 2.14 0 -6 2 -11 861.62 2.08 0 6 -4 -11 829.89 2.67 0 -2 6 -11 841.93 2.06 0 6 -4 -11 873.76 2.73 0 6 -5 11 2577.60 3.33 0 1 5 11 2651.92 4.00 0 -1 6 11 2716.75 4.72 0 5 -6 11 2617.64 3.29 0 5 -6 11 2581.53 4.69 0 -5 -1 11 2478.71 3.76 0 6 -5 11 2482.03 6.92 0 -6 5 -11 2323.27 3.27 0 6 -1 -11 2214.69 3.28 0 -5 6 -11 2350.10 3.13 0 -6 7 11 116.58 1.55 0 -1 -6 11 118.18 1.12 0 7 -1 11 121.47 1.32 0 6 1 11 117.67 1.32 0 6 -7 -11 134.12 1.67 0 -1 7 -11 120.08 1.29 0 -7 1 -11 104.63 2.08 0 7 -6 -11 130.67 1.67 0 1 6 -11 125.27 1.07 0 4 -7 11 281.39 1.38 0 7 -4 11 260.84 1.56 0 3 4 11 248.57 1.56 0 -3 7 11 243.12 1.95 0 -4 -3 11 243.76 1.38 0 -4 7 -11 235.80 1.27 0 -7 4 -11 262.59 1.45 0 7 -3 -11 246.01 1.88 0 7 -3 -11 234.23 1.40 0 -3 -5 11 1246.70 2.61 0 8 -3 11 1217.30 2.29 0 5 3 11 1188.09 2.49 0 -5 8 11 1246.10 3.92 0 8 -5 -11 1174.70 3.32 0 8 -5 -11 1271.69 2.98 0 -3 8 -11 1181.11 2.21 0 -8 3 -11 1245.50 2.37 0 6 -8 11 72.18 1.36 0 2 6 11 70.41 1.02 0 -2 8 11 73.31 1.35 0 6 -8 11 86.32 1.06 0 -6 -2 11 68.43 1.31 0 8 -6 11 78.63 1.37 0 -8 6 -11 70.80 0.94 0 -6 8 -11 67.11 1.23 0 8 -2 -11 65.88 0.95 0 9 -2 11 234.18 1.26 0 -7 9 11 242.13 2.05 0 7 2 11 244.43 1.33 0 -2 -7 11 245.40 1.36 0 2 7 -11 269.63 1.60 0 -2 9 -11 236.67 1.28 0 9 -7 -11 272.79 1.84 0 9 -7 -11 229.88 1.90 0 4 5 11 421.15 1.56 0 -4 9 11 419.00 2.28 0 9 -5 11 456.52 1.76 0 -5 -4 11 430.69 1.61 0 -9 5 -11 418.54 1.58 0 -5 9 -11 430.42 1.65 0 9 -4 -11 422.29 1.64 0 1 8 11 181.85 1.53 0 8 -9 11 191.95 1.32 0 -1 9 11 182.54 1.61 0 9 -8 11 183.16 1.33 0 8 -9 11 171.85 1.85 0 -8 -1 11 165.74 1.61 0 -8 9 -11 161.06 1.17 0 -9 8 -11 154.71 1.42 0 8 1 -11 147.35 1.09 0 9 -1 -11 154.42 1.35 0 9 1 11 14.92 0.97 0 10 -1 11 8.16 0.98 0 -1 -9 11 5.57 1.07 0 -1 10 -11 24.80 1.36 0 -9 -1 -11 13.82 1.38 0 1 9 -11 18.38 1.02 0 10 -9 -11 27.86 1.69 0 10 -9 -11 14.97 1.10 0 10 -4 11 366.40 1.52 0 -4 -6 11 361.11 1.56 0 6 4 11 381.86 1.53 0 -6 10 11 376.45 2.38 0 10 -6 -11 385.02 1.97 0 -4 10 -11 365.93 1.72 0 10 -6 -11 353.47 2.34 0 -3 10 11 65.85 1.38 0 3 7 11 65.10 1.05 0 10 -7 11 74.57 1.12 0 7 -10 11 67.84 1.18 0 -7 -3 11 64.54 1.15 0 -7 10 -11 67.12 1.03 0 10 -3 -11 68.17 1.25 0 7 3 -11 65.30 0.98 0 -10 7 -11 58.23 1.01 0 -8 11 11 220.03 2.00 0 11 -3 11 223.95 1.31 0 8 3 11 232.57 1.64 0 -3 -8 11 234.07 1.40 0 11 -8 -11 217.00 2.15 0 11 -8 -11 258.25 1.90 0 3 8 -11 261.49 1.38 0 -3 11 -11 222.65 1.34 0 -5 11 11 382.11 2.41 0 11 -6 11 408.77 1.55 0 6 -11 11 414.07 2.09 0 5 6 11 413.01 1.61 0 -6 -5 11 408.84 1.92 0 11 -5 -11 395.97 1.89 0 -11 6 -11 394.07 1.70 0 -6 11 -11 372.81 1.51 0 9 -11 11 59.18 1.65 0 2 9 11 67.49 1.48 0 11 -9 11 67.63 1.52 0 -2 11 11 63.05 1.46 0 9 -11 11 76.95 1.29 0 -9 -2 11 59.27 1.22 0 9 2 -11 54.04 1.36 0 -9 11 -11 64.61 1.40 0 11 -2 -11 52.83 1.10 0 -11 9 -11 57.63 1.29 0 5 -12 11 314.63 1.89 0 7 5 11 302.11 1.45 0 -5 -7 11 291.33 1.71 0 12 -5 11 304.17 1.73 0 12 -7 -11 286.72 1.59 0 -5 12 -11 306.21 1.71 0 -1 -1 12 3762.38 5.24 0 1 -2 12 3770.71 4.73 0 1 -2 12 4150.93 5.88 0 2 -1 12 3400.11 4.63 0 -1 2 -12 3841.28 5.39 0 -2 1 -12 3420.88 4.71 0 -1 2 -12 3648.39 4.59 0 1 1 -12 3773.10 5.17 0 2 -1 -12 3850.33 5.43 0 0 -3 12 4998.72 5.62 0 3 0 12 4851.95 5.45 0 -3 0 -12 4484.61 5.19 0 -3 0 12 3599.12 4.79 0 3 -3 12 3842.30 4.31 0 3 0 -12 3729.19 5.06 0 -3 3 -12 3446.48 4.10 0 2 2 12 1720.97 3.50 0 2 -4 12 1742.53 2.91 0 2 -4 12 1704.03 3.56 0 -2 -2 12 1690.38 3.07 0 4 -2 12 1654.83 2.97 0 4 -2 -12 1608.73 3.51 0 4 -2 -12 1475.67 3.51 0 -4 2 -12 1501.82 2.83 0 -2 4 -12 1517.33 2.70 0 -4 2 -12 1577.57 4.90 0 -1 -4 12 3371.41 4.05 0 5 -1 12 3247.37 3.96 0 1 -5 12 3337.86 4.18 0 4 1 12 3353.26 4.17 0 -1 5 -12 3416.44 3.70 0 -5 1 -12 3142.05 3.72 0 4 -5 12 57.68 1.09 0 -1 5 12 69.81 1.43 0 4 -5 12 58.01 1.23 0 1 4 12 73.54 1.30 0 -4 -1 12 58.85 1.32 0 5 -4 12 78.05 1.23 0 5 -1 -12 79.49 1.13 0 -4 5 -12 71.27 0.89 0 -5 4 -12 73.09 0.92 0 0 -6 12 460.83 1.69 0 6 0 12 434.32 1.59 0 0 6 -12 538.74 1.63 0 6 -6 -12 511.18 2.55 0 3 3 12 2083.07 3.36 0 3 -6 12 2025.30 3.42 0 -3 -3 12 2024.73 3.15 0 6 -3 12 2023.78 2.97 0 6 -3 -12 1963.64 3.73 0 -3 6 -12 1968.88 2.81 0 6 -3 -12 1916.49 3.49 0 -6 3 -12 1894.79 2.81 0 5 2 12 4900.99 4.58 0 7 -2 12 4777.91 4.30 0 -2 -5 12 5129.09 4.74 0 -2 7 -12 4989.01 4.35 0 -7 2 -12 4818.04 4.27 0 7 -5 -12 4705.78 5.71 0 7 -5 -12 4977.35 5.98 0 7 -5 12 320.89 1.40 0 5 -7 12 327.96 1.39 0 5 -7 12 318.96 1.89 0 -2 7 12 302.57 2.15 0 2 5 12 301.19 1.48 0 -5 -2 12 302.05 1.44 0 7 -2 -12 278.63 1.57 0 -5 7 -12 284.27 1.44 0 -7 5 -12 292.61 1.31 0 -1 -7 12 1312.34 2.47 0 8 -1 12 1292.86 2.49 0 7 1 12 1285.71 2.37 0 7 -8 -12 1472.61 3.99 0 1 7 -12 1423.26 2.48 0 -1 8 -12 1310.63 2.49 0 8 -7 -12 1504.60 3.77 0 -4 8 12 1993.55 5.15 0 4 4 12 1942.87 2.99 0 -4 -4 12 2074.88 3.22 0 8 -4 12 2031.17 2.99 0 4 -8 12 1955.10 3.26 0 -4 8 -12 1830.69 2.69 0 -8 4 -12 1790.21 2.65 0 8 -4 -12 1860.57 3.78 0 8 -4 -12 1935.45 3.42 0 -7 -1 12 2128.75 3.58 0 1 7 12 2191.53 3.63 0 -1 8 12 2262.14 4.03 0 7 -8 12 2331.91 3.08 0 8 -7 12 2342.80 3.30 0 7 -8 12 2107.75 4.46 0 7 1 -12 1850.10 2.69 0 -7 8 -12 1993.94 2.97 0 8 -1 -12 1835.12 2.89 0 -8 7 -12 2054.15 3.01 0 9 0 12 542.74 1.65 0 0 -9 12 564.61 2.02 0 9 -9 -12 624.56 2.78 0 0 9 -12 569.75 1.68 0 -9 0 -12 519.11 3.72 0 9 -3 12 597.01 1.70 0 6 3 12 624.94 1.93 0 -6 9 12 598.12 3.02 0 -3 -6 12 593.24 1.78 0 9 -6 -12 647.57 2.32 0 9 -6 -12 585.71 2.48 0 -9 3 -12 611.63 1.65 0 -3 9 -12 579.03 1.64 0 6 -9 12 823.37 1.95 0 -6 -3 12 677.98 1.97 0 3 6 12 672.97 1.92 0 -3 9 12 669.60 2.64 0 9 -6 12 737.52 1.90 0 6 -9 12 698.29 2.23 0 -6 9 -12 679.54 1.77 0 -9 6 -12 659.92 1.88 0 9 -3 -12 656.32 1.89 0 0 9 12 1285.00 3.06 0 9 -9 12 1395.57 2.58 0 0 9 12 1270.22 3.00 0 9 -9 12 1126.27 5.73 0 -9 9 -12 1124.03 2.44 0 9 0 -12 1016.05 2.09 0 10 -2 12 1938.27 2.79 0 2 -10 12 2014.18 3.10 0 8 2 12 1940.69 2.87 0 -2 -8 12 1921.07 2.92 0 2 8 -12 2240.09 3.08 0 -2 10 -12 1980.46 2.83 0 10 -8 -12 2206.93 4.23 0 10 -8 -12 1858.59 4.23 0 5 5 12 816.03 2.17 0 5 -10 12 840.29 2.47 0 -5 10 12 836.27 3.42 0 -5 -5 12 833.54 2.31 0 10 -5 12 871.09 2.00 0 10 -5 -12 787.73 2.19 0 -5 10 -12 753.32 1.90 0 -10 5 -12 827.21 2.06 0 8 -10 12 11.62 1.10 0 8 -10 12 5.30 1.45 0 10 -8 12 8.42 1.40 0 -2 10 12 11.14 1.30 0 2 8 12 9.36 0.97 0 -8 -2 12 11.17 1.01 0 10 -2 -12 12.15 0.95 0 -8 10 -12 6.50 1.20 0 -10 8 -12 7.00 0.93 0 8 2 -12 15.32 0.90 0 11 -4 12 469.85 1.82 0 7 4 12 463.35 1.68 0 4 -11 12 463.47 2.06 0 -4 -7 12 456.15 1.85 0 -4 11 -12 417.88 1.54 0 11 -7 -12 434.38 2.00 0 -4 11 12 1772.62 4.56 0 -7 -4 12 1759.73 3.20 0 7 -11 12 1780.43 3.43 0 11 -7 12 1863.00 3.04 0 4 7 12 1823.39 3.02 0 -7 11 -12 1757.73 2.93 0 11 -4 -12 1652.03 2.90 0 -11 7 -12 1711.19 2.64 0 7 4 -12 1662.85 2.54 0 6 -12 12 856.88 2.40 0 12 -6 12 907.73 2.06 0 -6 -6 12 857.89 2.23 0 6 6 12 889.26 2.35 0 -6 12 -12 820.31 2.05 0 12 -6 -12 843.74 2.45 0 1 3 13 320.81 1.81 0 3 -4 13 320.39 1.39 0 -1 4 13 333.44 2.97 0 -3 -1 13 354.74 1.80 0 4 -3 13 310.52 1.39 0 3 -4 13 336.12 1.77 0 4 -1 -13 335.89 1.72 0 -4 3 -13 306.71 1.55 0 -3 4 -13 300.54 1.51 0 3 2 13 363.02 1.64 0 5 -2 13 345.00 1.47 0 -2 -3 13 358.87 1.75 0 2 -5 13 353.01 1.65 0 5 -3 -13 329.10 1.95 0 -5 2 -13 334.93 1.58 0 -2 5 -13 347.20 1.57 0 -5 2 -13 324.26 2.68 0 5 -3 -13 338.08 1.97 0 1 -6 13 1652.40 2.89 0 5 1 13 1666.69 2.85 0 -1 -5 13 1765.84 3.06 0 6 -1 13 1673.97 2.89 0 1 5 -13 1837.07 2.72 0 -1 6 -13 1659.42 2.60 0 -6 1 -13 1621.86 2.67 0 6 -5 -13 1807.01 4.38 0 4 -6 13 2064.51 2.92 0 4 -6 13 1968.90 3.66 0 2 4 13 1905.71 3.40 0 6 -4 13 1981.83 3.00 0 -4 -2 13 1914.83 3.17 0 6 -2 -13 1770.66 3.21 0 -4 6 -13 1786.35 2.72 0 -6 4 -13 1882.49 2.97 0 6 -2 -13 1863.77 3.71 0 7 -3 13 289.05 1.32 0 4 3 13 290.67 1.58 0 -4 7 13 286.31 2.91 0 -3 -4 13 276.16 1.40 0 3 -7 13 280.04 1.49 0 7 -4 -13 279.12 1.82 0 -7 3 -13 265.84 1.44 0 -3 7 -13 262.05 1.23 0 7 -4 -13 275.82 1.76 0 1 6 13 255.68 1.52 0 -1 7 13 286.74 1.72 0 6 -7 13 277.76 2.00 0 6 -7 13 303.50 1.64 0 7 -6 13 294.59 1.72 0 -6 -1 13 259.32 1.49 0 -6 7 -13 256.46 1.31 0 7 -1 -13 242.14 1.32 0 -7 6 -13 254.66 1.31 0 -2 -6 13 316.77 1.48 0 -6 8 13 336.31 2.71 0 2 -8 13 343.87 1.53 0 8 -2 13 332.42 1.65 0 6 2 13 335.19 1.69 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13 142.82 1.55 0 3 7 -13 162.85 1.24 0 -3 10 -13 135.02 1.17 0 10 -7 -13 123.83 1.78 0 10 -7 -13 145.60 1.41 0 -6 -4 13 268.15 1.72 0 -4 10 13 266.76 2.13 0 4 6 13 255.65 1.41 0 10 -6 13 291.97 1.64 0 6 -10 13 279.28 1.84 0 -6 10 -13 261.10 1.54 0 -10 6 -13 259.84 1.27 0 10 -4 -13 249.55 1.41 0 -9 -1 13 338.40 1.73 0 1 9 13 396.86 2.03 0 -1 10 13 369.68 2.11 0 9 -10 13 432.08 2.02 0 10 -9 13 419.02 1.68 0 -1 10 13 377.94 2.07 0 1 9 13 367.34 1.76 0 9 -10 13 354.01 2.72 0 9 1 -13 321.82 1.61 0 -10 9 -13 336.02 1.45 0 10 -1 -13 310.49 1.44 0 -9 10 -13 348.69 1.50 0 11 -2 13 356.21 1.49 0 -2 -9 13 401.55 1.89 0 9 2 13 373.87 1.74 0 2 -11 13 453.47 2.05 0 11 -9 -13 328.61 2.31 0 2 9 -13 430.01 1.85 0 11 -9 -13 414.24 2.37 0 -2 11 -13 375.20 1.52 0 -9 -2 -13 344.54 2.25 0 6 5 13 67.84 1.11 0 -5 -6 13 68.62 1.15 0 5 -11 13 76.46 1.52 0 11 -5 13 73.23 1.12 0 -5 11 -13 62.43 1.06 0 11 -6 -13 72.28 1.15 0 -11 5 -13 83.17 1.06 0 3 8 13 760.35 2.28 0 11 -8 13 766.02 2.17 0 8 -11 13 721.67 2.72 0 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120.19 1.04 0 -5 0 -14 100.42 1.04 0 5 -5 -14 100.33 1.65 0 3 -5 14 851.15 1.96 0 2 3 14 839.24 2.60 0 3 -5 14 870.76 2.59 0 -3 -2 14 834.04 2.32 0 5 -3 14 824.73 2.01 0 -3 5 -14 757.79 1.85 0 5 -2 -14 785.41 2.35 0 -5 3 -14 764.28 2.05 0 5 -2 -14 735.47 2.25 0 6 -2 14 193.36 1.26 0 4 2 14 189.83 1.48 0 2 -6 14 194.58 1.58 0 -2 -4 14 193.18 1.51 0 -6 2 -14 174.83 1.42 0 -2 6 -14 177.82 1.39 0 6 -4 -14 194.37 1.76 0 -6 2 -14 173.67 2.70 0 6 -4 -14 182.30 1.37 0 1 5 14 779.42 2.41 0 -1 6 14 851.74 3.09 0 5 -6 14 806.65 1.93 0 -1 6 14 815.22 3.12 0 6 -5 14 810.52 2.15 0 5 -6 14 787.86 2.60 0 -5 -1 14 770.58 2.35 0 -5 6 -14 726.89 1.97 0 -6 5 -14 731.81 1.86 0 6 -1 -14 676.47 2.08 0 7 -1 14 162.82 1.20 0 1 -7 14 202.41 1.64 0 -1 -6 14 166.87 1.26 0 6 1 14 169.80 1.22 0 1 6 -14 182.76 1.59 0 -7 1 -14 158.72 2.12 0 -1 7 -14 173.33 1.20 0 7 -6 -14 191.09 1.90 0 4 -7 14 820.92 2.44 0 3 4 14 761.04 2.09 0 7 -4 14 803.33 1.91 0 -3 7 14 789.34 4.39 0 -4 -3 14 775.58 2.21 0 4 -7 14 899.38 2.00 0 7 -3 -14 742.77 2.30 0 -7 4 -14 765.04 1.98 0 7 -3 -14 738.55 2.31 0 -4 7 -14 787.21 1.98 0 -7 0 14 131.30 1.23 0 7 -7 14 154.55 1.44 0 0 7 14 149.38 1.54 0 7 -7 14 145.92 1.83 0 7 0 -14 135.39 1.29 0 -7 7 -14 139.08 1.07 0 0 -8 14 293.53 1.47 0 8 0 14 294.26 1.37 0 0 8 -14 314.14 1.37 0 8 -8 -14 361.30 2.34 0 8 -3 14 535.08 1.65 0 -3 -5 14 515.30 1.71 0 3 -8 14 613.55 2.12 0 5 3 14 516.40 1.69 0 -8 3 -14 526.78 1.74 0 8 -5 -14 526.15 2.14 0 -3 8 -14 515.28 1.73 0 8 -5 -14 526.69 2.24 0 2 6 14 124.52 1.18 0 6 -8 14 162.44 1.50 0 -2 8 14 133.55 1.64 0 8 -6 14 132.60 1.48 0 -6 -2 14 131.14 1.22 0 6 -8 14 135.66 1.35 0 -8 6 -14 133.24 1.34 0 -6 8 -14 116.41 1.37 0 8 -2 -14 111.96 1.08 0 9 -2 14 186.50 1.23 0 2 -9 14 205.39 1.36 0 -2 -7 14 213.64 1.62 0 7 2 14 203.44 1.30 0 2 7 -14 221.21 1.25 0 9 -7 -14 230.93 1.96 0 -2 9 -14 200.07 1.42 0 9 -7 -14 193.06 1.75 0 -5 -4 14 556.09 2.00 0 5 -9 14 562.08 2.12 0 9 -5 14 585.55 1.74 0 4 5 14 543.95 1.81 0 -4 9 14 554.37 3.39 0 -9 5 -14 508.43 1.57 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1212.81 3.82 0 4 -2 -15 1198.51 3.23 0 -2 4 -15 1218.10 2.35 0 -4 2 -15 1226.41 2.49 0 1 -5 15 645.22 1.96 0 5 -1 15 649.41 2.00 0 4 1 15 654.58 1.97 0 -1 -4 15 644.37 1.90 0 -5 1 -15 595.19 1.75 0 1 4 -15 749.34 2.00 0 5 -4 -15 680.66 3.11 0 -1 5 -15 647.30 1.90 0 -1 5 15 710.65 3.44 0 4 -5 15 676.67 1.77 0 1 4 15 661.75 2.49 0 -1 5 15 695.33 3.59 0 5 -4 15 649.17 1.77 0 4 -5 15 665.96 2.34 0 -4 -1 15 652.01 1.98 0 -5 4 -15 639.02 1.89 0 5 -1 -15 649.15 2.23 0 -4 5 -15 602.15 1.65 0 3 3 15 1287.40 2.89 0 -3 -3 15 1223.15 2.49 0 3 -6 15 1259.22 2.74 0 6 -3 15 1266.19 2.42 0 6 -3 -15 1212.17 2.93 0 -6 3 -15 1155.60 2.26 0 6 -3 -15 1173.10 2.95 0 -3 6 -15 1184.08 2.35 0 7 -2 15 2468.58 3.30 0 2 -7 15 2432.29 3.55 0 -2 -5 15 2403.12 3.26 0 5 2 15 2370.45 3.30 0 -7 2 -15 2316.84 3.06 0 7 -5 -15 2497.27 4.68 0 -2 7 -15 2386.43 3.07 0 7 -5 -15 2206.85 3.68 0 -2 7 15 708.44 3.43 0 5 -7 15 721.79 1.80 0 5 -7 15 663.28 2.22 0 -2 7 15 682.44 3.33 0 2 5 15 690.72 2.27 0 7 -5 15 725.73 2.03 0 -5 -2 15 664.92 2.15 0 7 -2 -15 588.15 1.79 0 -5 7 -15 617.48 1.66 0 7 -2 -15 643.35 2.33 0 -7 5 -15 641.37 1.71 0 8 -1 15 959.47 2.26 0 7 1 15 977.57 2.32 0 1 -8 15 940.60 2.20 0 -1 -7 15 980.89 2.38 0 8 -7 -15 852.19 2.60 0 -1 8 -15 967.32 2.16 0 8 -7 -15 1070.18 3.53 0 1 7 -15 1027.93 2.08 0 4 4 15 264.02 1.37 0 4 -8 15 274.85 1.77 0 -4 -4 15 271.07 1.38 0 8 -4 15 277.70 1.56 0 8 -4 -15 254.57 1.73 0 8 -4 -15 256.31 1.49 0 -4 8 -15 287.22 1.47 0 -8 4 -15 251.95 1.23 0 7 -8 15 171.76 1.58 0 -1 8 15 156.58 1.60 0 1 7 15 148.02 1.56 0 -7 -1 15 154.57 1.58 0 8 -7 15 175.23 1.56 0 7 -8 15 148.97 1.70 0 -1 8 15 151.15 1.67 0 7 1 -15 133.52 1.10 0 8 -1 -15 135.12 1.36 0 -7 8 -15 141.40 1.12 0 -8 7 -15 159.90 1.16 0 9 -3 15 14.16 0.97 0 6 3 15 4.81 0.99 0 3 -9 15 12.80 1.03 0 -3 -6 15 14.96 1.34 0 9 -6 -15 12.73 1.36 0 -3 9 -15 8.81 0.95 0 9 -6 -15 8.33 1.37 0 -9 3 -15 9.37 1.19 0 -3 9 15 243.12 2.37 0 6 -9 15 289.37 1.43 0 -6 -3 15 234.02 1.44 0 6 -9 15 247.29 1.76 0 -3 9 15 261.50 2.47 0 3 6 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17.69 1.32 0 -11 7 -15 21.94 0.93 0 11 -4 -15 19.56 1.05 0 2 -2 16 2164.18 3.33 0 -2 2 -16 2223.58 4.00 0 -2 2 -16 2125.67 3.40 0 2 0 -16 2678.69 4.21 0 2 0 -16 2456.05 3.97 0 4 0 16 2166.93 3.45 0 0 -4 16 2249.68 3.55 0 0 4 -16 2280.49 3.02 0 -4 0 -16 2172.56 3.32 0 1 3 16 1880.65 4.24 0 3 -4 16 1955.89 3.88 0 3 -4 16 1865.78 2.82 0 4 -3 16 1801.53 2.82 0 -3 -1 16 1846.87 3.14 0 4 -1 -16 1848.36 3.31 0 -4 3 -16 1721.01 2.75 0 -3 4 -16 1735.50 2.71 0 3 1 -16 2049.05 3.51 0 2 -5 16 3497.36 4.35 0 3 2 16 3537.64 4.55 0 -2 -3 16 3550.20 4.23 0 5 -2 16 3534.00 4.02 0 -5 2 -16 3155.79 3.69 0 5 -3 -16 3176.38 5.15 0 -2 5 -16 3357.67 3.69 0 5 -3 -16 3316.96 4.37 0 -5 0 16 1841.15 3.15 0 0 5 16 2076.23 4.71 0 5 -5 16 1945.67 2.82 0 5 -5 16 1973.68 4.35 0 -5 5 -16 1818.45 2.74 0 6 -1 16 4089.38 4.13 0 -1 -5 16 4234.71 4.41 0 5 1 16 4081.43 4.31 0 1 -6 16 4346.66 4.56 0 -6 1 -16 3984.81 3.98 0 1 5 -16 4630.23 4.05 0 -1 6 -16 4420.66 4.05 0 4 -6 16 9999.99 6.13 0 -4 -2 16 8969.73 6.53 0 7 0 16 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705.55 1.79 0 -6 7 -22 723.40 1.97 0 7 -1 -22 665.42 2.08 0 6 2 22 64.30 1.06 0 2 -8 22 58.44 1.13 0 -2 -6 22 62.82 1.44 0 8 -2 22 57.46 1.35 0 2 6 -22 65.36 1.05 0 -2 8 -22 57.39 0.99 0 -8 2 -22 55.30 0.98 0 8 -6 -22 67.23 2.13 0 8 -6 -22 57.92 1.45 0 3 5 22 301.24 1.90 0 8 -5 22 299.05 1.74 0 5 -8 22 283.82 1.62 0 -5 -3 22 274.29 1.43 0 -5 8 -22 264.65 1.56 0 -8 5 -22 265.44 1.32 0 8 -3 -22 248.64 1.49 0 8 -3 -22 265.69 1.55 0 0 8 22 134.25 1.89 0 8 -8 22 143.37 1.33 0 0 8 22 123.20 2.13 0 8 0 -22 105.84 1.37 0 -8 8 -22 123.50 1.15 0 9 -1 22 291.77 1.70 0 8 1 22 293.21 1.45 0 1 -9 22 282.55 1.54 0 -1 -8 22 291.43 1.55 0 1 8 -22 312.38 1.73 0 -1 9 -22 268.77 1.35 0 9 -8 -22 251.48 1.56 0 5 4 22 72.91 1.19 0 9 -4 22 70.07 1.46 0 4 -9 22 66.54 1.45 0 -4 -5 22 68.53 1.54 0 4 5 -22 81.67 1.12 0 9 -5 -22 65.05 1.26 0 -9 4 -22 64.33 1.02 0 9 -5 -22 71.80 1.52 0 -4 9 -22 68.68 1.32 0 -7 -2 22 37.80 1.45 0 7 -9 22 62.65 1.50 0 9 -7 22 42.20 1.51 0 2 7 22 45.24 1.52 0 7 -9 22 41.57 1.51 0 -9 7 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1902.70 5.38 0 -6 -3 24 2871.06 3.63 0 3 6 24 3172.34 4.90 0 9 -6 24 3254.14 3.69 0 6 -9 24 2901.05 4.47 0 -6 9 -24 2672.59 3.19 0 9 -3 -24 2645.70 4.09 0 -9 6 -24 2603.80 3.15 0 9 -9 24 2858.56 3.47 0 9 0 -24 1811.72 3.04 0 -9 9 -24 2213.35 3.14 0 8 2 24 1559.11 2.77 0 2 -10 24 1587.21 2.90 0 -2 -8 24 1593.47 2.81 0 10 -8 -24 1333.69 3.04 0 5 5 24 2251.98 3.81 0 10 -5 24 2213.30 3.03 0 5 -10 24 2147.80 3.53 0 -5 -5 24 2102.85 3.15 0 5 5 -24 2388.21 3.08 0 10 -5 -24 2038.16 4.16 0 10 -5 -24 1845.98 3.54 0 -10 5 -24 2037.36 2.94 0 -5 10 -24 2006.80 2.89 0 8 -10 24 1711.60 2.75 0 10 -8 24 1693.11 2.86 0 -8 10 -24 1388.96 2.60 0 8 2 -24 1111.99 2.42 0 1 -3 25 284.61 1.54 0 -1 -2 25 242.21 1.41 0 3 -1 25 276.32 1.41 0 2 1 25 266.32 1.55 0 1 2 -25 286.61 1.42 0 3 -2 -25 289.91 2.10 0 -1 3 -25 264.13 1.46 0 1 2 -25 295.42 1.73 0 -1 3 -25 267.17 1.33 0 -2 -1 -25 305.97 1.89 0 -3 1 -25 283.41 1.45 0 -3 1 -25 269.37 1.52 0 3 -2 -25 289.52 1.51 0 3 -4 25 2004.30 2.81 0 4 -3 25 1921.31 2.82 0 1 3 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1048.35 2.28 0 -1 6 -28 998.17 2.22 0 -6 1 -28 999.43 2.36 0 -6 1 -28 979.91 3.00 0 6 -5 -28 1031.24 2.53 0 4 -6 28 979.56 2.46 0 4 -6 28 1094.88 2.12 0 6 -4 28 1018.76 2.12 0 2 4 28 997.60 3.03 0 -4 6 -28 863.87 1.92 0 6 -2 -28 1068.62 2.91 0 4 2 -28 1064.49 2.39 0 6 -2 -28 926.06 2.23 0 -6 4 -28 888.27 2.02 0 6 -2 -28 834.99 2.60 0 7 0 28 597.47 1.85 0 0 -7 28 572.79 1.90 0 7 -7 -28 521.43 1.83 0 0 7 -28 536.95 1.81 0 -7 0 -28 484.15 2.24 0 -3 -4 28 986.91 2.40 0 7 -3 28 1033.64 2.45 0 4 3 28 1013.89 2.75 0 3 -7 28 995.47 2.61 0 7 -4 -28 1078.15 3.70 0 3 4 -28 1035.58 2.16 0 7 -4 -28 954.24 3.70 0 -7 3 -28 903.82 2.21 0 7 -4 -28 884.24 2.25 0 -3 7 -28 921.40 2.09 0 6 -7 28 729.08 1.84 0 7 -6 28 719.40 1.88 0 1 6 28 646.75 3.49 0 6 1 -28 723.57 2.01 0 -6 7 -28 600.75 1.88 0 -7 6 -28 596.24 1.94 0 7 -1 -28 497.05 1.81 0 8 -2 28 1006.68 2.24 0 2 -8 28 971.56 2.39 0 -2 -6 28 995.73 2.31 0 6 2 28 1011.55 2.63 0 2 6 -28 1030.32 2.33 0 -8 2 -28 908.36 2.07 0 -2 8 -28 953.73 2.20 0 8 -6 -28 887.76 2.32 0 5 -8 28 997.91 2.59 0 -5 -3 28 972.36 2.24 0 8 -5 28 1111.31 2.41 0 3 5 28 1017.60 2.98 0 -5 8 -28 928.21 2.00 0 5 3 -28 1102.02 2.27 0 -8 5 -28 936.10 2.04 0 8 -3 -28 877.66 2.80 0 8 -3 -28 947.92 2.38 0 8 -8 28 2856.35 3.57 0 8 0 -28 1772.83 2.97 0 -8 8 -28 2244.17 2.97 0 5 4 28 2449.55 3.88 0 9 -4 28 2519.57 3.26 0 4 -9 28 2412.76 3.59 0 -4 -5 28 2391.26 3.32 0 9 -5 -28 2378.02 5.51 0 4 5 -28 2611.77 3.22 0 -9 4 -28 2158.58 2.92 0 9 -5 -28 2116.73 3.45 0 -4 9 -28 2340.02 3.10 0 7 -9 28 1694.18 2.71 0 9 -7 28 1675.19 2.71 0 -9 7 -28 1365.50 2.43 0 -7 9 -28 1380.42 2.40 0 9 -2 -28 1225.72 2.89 0 2 -3 29 866.31 2.04 0 3 -2 29 881.41 2.29 0 1 2 29 860.92 2.81 0 -2 3 -29 789.30 2.12 0 -3 2 -29 776.85 2.04 0 2 1 -29 816.64 2.15 0 3 -1 -29 843.79 2.67 0 -2 3 -29 741.84 2.06 0 2 1 -29 793.00 2.36 0 -3 2 -29 782.09 2.37 0 3 -1 -29 884.82 2.40 0 -1 -2 -29 884.21 3.01 0 1 -4 29 835.61 2.15 0 -1 -3 29 838.75 2.13 0 4 -1 29 811.68 2.07 0 3 1 29 805.19 2.24 0 4 -3 -29 856.96 4.60 0 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30.62 1.69 0 7 -3 -35 23.84 1.34 0 0 0 -36 964.18 2.77 0 0 0 -36 915.81 2.14 0 -1 2 -36 1688.86 2.96 0 2 -1 -36 1781.14 4.08 0 -1 -1 -36 1981.60 4.24 0 -2 1 -36 1778.76 3.20 0 1 -2 -36 1984.22 5.60 0 -1 2 -36 1693.51 2.84 0 1 1 -36 1716.48 2.79 0 -2 1 -36 1698.39 3.11 0 2 -1 -36 1813.92 2.89 0 1 1 -36 1783.90 3.29 0 1 -2 -36 1772.98 2.88 0 -1 -1 -36 1788.35 3.09 0 3 0 36 3296.67 4.38 0 -3 0 -36 3182.59 4.45 0 0 3 -36 2954.55 3.74 0 -3 0 -36 2911.33 3.89 0 3 -3 -36 3240.87 4.01 0 3 -3 36 2945.89 3.56 0 0 -3 -36 2640.16 3.46 0 -3 3 -36 2605.00 3.56 0 -3 3 -36 2542.25 3.79 0 3 0 -36 2636.19 4.08 0 3 0 -36 2756.50 3.57 0 4 -2 36 2900.63 3.63 0 2 2 36 2847.99 4.74 0 2 -4 -36 2750.27 3.54 0 -2 -2 -36 2740.02 3.69 0 -4 2 -36 2704.18 3.74 0 -2 4 -36 2641.18 3.49 0 2 2 -36 2692.38 3.61 0 2 2 -36 2702.04 3.45 0 -4 2 -36 2592.16 3.95 0 4 -2 -36 2924.14 3.80 0 4 -2 -36 2813.35 5.90 0 5 -1 36 1537.93 2.81 0 4 1 36 1561.07 3.23 0 -5 1 -36 1465.99 2.91 0 -4 -1 -36 1607.33 3.34 0 1 4 -36 1401.42 2.55 0 -1 5 -36 1440.09 2.66 0 -5 1 -36 1380.67 3.13 0 5 -4 -36 1463.99 2.72 0 -4 -1 -36 1429.05 2.89 0 4 -5 -36 1500.99 2.91 0 5 -4 36 2565.03 3.31 0 -4 5 -36 2199.22 3.03 0 4 1 -36 2405.13 3.61 0 5 -1 -36 2389.45 4.27 0 4 1 -36 2381.24 3.35 0 5 -1 -36 2280.58 3.27 0 -5 4 -36 2287.54 3.34 0 0 -6 36 1668.93 2.81 0 6 0 36 1790.01 3.28 0 0 6 -36 1639.81 2.65 0 -6 0 -36 1582.24 3.43 0 6 -6 -36 1683.16 3.08 0 6 -3 36 1289.94 2.52 0 3 3 36 1237.80 3.39 0 -3 6 -36 1135.95 2.29 0 -3 -3 -36 1145.07 2.53 0 6 -3 -36 1156.89 4.81 0 -6 3 -36 1152.67 2.55 0 3 3 -36 1214.66 2.47 0 -6 3 -36 1109.05 3.13 0 6 -3 -36 1138.23 2.49 0 6 -3 -36 1249.42 5.05 0 6 -6 36 645.50 1.87 0 6 0 -36 570.10 2.20 0 -6 6 -36 500.81 1.67 0 7 -2 36 753.65 2.07 0 5 2 36 751.60 2.53 0 -5 -2 -36 647.48 2.45 0 5 -7 -36 680.41 2.23 0 2 5 -36 734.26 2.13 0 -7 2 -36 646.49 2.76 0 -7 2 -36 653.55 1.94 0 7 -5 -36 660.91 2.28 0 -2 7 -36 680.66 2.03 0 7 -5 36 1083.02 2.29 0 -7 5 -36 974.51 2.38 0 7 -2 -36 859.99 2.92 0 -5 7 -36 962.21 2.31 0 5 2 -36 1054.29 2.42 0 7 -2 -36 1063.74 3.25 0 7 -2 -36 910.28 2.31 0 2 1 37 1236.02 3.13 0 3 -1 37 1215.52 2.60 0 -1 3 -37 1058.60 2.44 0 -3 1 -37 1100.55 2.57 0 -2 -1 -37 1248.38 3.39 0 3 -2 -37 1254.51 4.76 0 -1 3 -37 1071.97 2.47 0 1 2 -37 1255.47 2.60 0 -3 1 -37 1038.85 2.43 0 1 2 -37 1096.42 2.59 0 3 -2 -37 1113.56 2.40 0 -2 -1 -37 1063.86 2.41 0 2 -3 -37 1093.61 2.40 0 4 -3 37 59.42 1.50 0 1 -4 -37 46.72 1.57 0 -1 -3 -37 60.52 1.48 0 -3 4 -37 49.14 1.06 0 3 1 -37 52.50 1.13 0 3 1 -37 60.34 1.63 0 -4 3 -37 67.53 1.50 0 4 -1 -37 50.06 1.41 0 4 -1 -37 49.95 1.23 0 -4 3 -37 49.90 1.42 0 5 -2 37 645.85 1.97 0 3 2 37 629.33 2.45 0 -3 -2 -37 576.62 1.94 0 3 -5 -37 604.12 1.92 0 -5 2 -37 554.38 1.84 0 2 3 -37 605.40 2.07 0 -5 2 -37 550.74 2.08 0 5 -3 -37 570.96 1.85 0 -2 5 -37 551.48 1.72 0 6 -1 37 14.76 1.06 0 5 1 37 14.00 1.09 0 -6 1 -37 11.22 1.03 0 1 5 -37 18.60 1.04 0 -1 6 -37 17.65 1.00 0 -6 1 -37 11.64 1.06 0 6 -5 -37 18.91 1.11 0 -5 -1 -37 15.34 1.34 0 5 -6 -37 13.19 1.11 0 6 -4 37 62.64 1.49 0 -6 4 -37 61.34 1.12 0 -4 6 -37 56.91 1.39 0 4 2 -37 61.92 1.36 0 6 -2 -37 67.53 1.60 0 6 -2 -37 64.15 1.54 0 6 -2 -37 60.95 1.52 0 7 -3 37 32.44 1.32 0 4 3 37 31.87 1.46 0 -3 7 -37 23.49 1.38 0 4 -7 -37 37.68 1.16 0 -4 -3 -37 39.33 1.47 0 3 4 -37 31.96 1.41 0 7 -4 -37 30.94 1.50 0 -7 3 -37 31.10 1.01 0 0 -1 -38 313.49 2.20 0 1 0 -38 274.96 1.88 0 -1 1 -38 274.33 1.54 0 -1 1 -38 263.63 1.47 0 1 0 -38 275.32 1.47 0 0 -1 -38 295.04 1.75 0 0 2 -38 58.24 1.39 0 2 -2 -38 64.45 2.16 0 -2 0 -38 63.39 1.38 0 0 2 -38 57.77 1.48 0 -2 0 -38 60.50 1.13 0 2 -2 -38 63.74 1.60 0 3 -2 38 85.28 1.56 0 -2 3 -38 69.02 1.13 0 -2 3 -38 70.66 1.17 0 2 1 -38 74.04 1.23 0 -3 2 -38 77.57 1.17 0 -3 2 -38 79.05 1.51 0 3 -1 -38 82.39 1.27 0 2 1 -38 74.77 1.51 0 -1 -2 -38 81.78 1.69 0 1 -3 -38 77.37 1.18 0 -1 -2 -38 85.71 1.42 0 3 -1 -38 75.96 1.49 0 3 1 38 393.45 1.86 0 4 -1 38 419.26 2.04 0 -3 -1 -38 410.49 2.22 0 -4 1 -38 356.49 1.69 0 1 3 -38 367.62 1.60 0 -4 1 -38 365.86 1.99 0 4 -3 -38 388.68 1.99 0 -1 4 -38 349.94 1.53 0 -3 -1 -38 361.41 1.72 0 3 -4 -38 394.63 1.66 0 4 -4 38 261.09 1.45 0 0 -4 -38 231.43 1.40 0 -4 4 -38 215.15 1.36 0 4 0 -38 228.37 1.80 0 4 0 -38 221.89 1.46 0 5 0 38 163.06 1.70 0 -5 0 -38 167.07 1.69 0 0 5 -38 154.05 1.24 0 -5 0 -38 142.20 1.71 0 5 -5 -38 150.18 1.71 0 2 3 38 55.09 1.57 0 5 -3 38 62.03 1.51 0 -5 3 -38 40.20 1.14 0 2 -5 -38 40.11 1.20 0 -2 -3 -38 46.76 1.51 0 -3 5 -38 44.02 1.42 0 3 2 -38 46.79 1.15 0 -5 3 -38 39.20 1.19 0 5 -2 -38 42.32 1.57 0 5 -2 -38 49.01 1.59 0 5 -2 -38 44.20 1.48 0 6 -2 38 276.98 1.79 0 4 2 38 262.42 1.92 0 -4 -2 -38 242.56 1.79 0 4 -6 -38 259.90 1.81 0 -6 2 -38 238.06 1.66 0 2 4 -38 228.35 1.42 0 -6 2 -38 234.08 1.92 0 6 -4 -38 236.63 1.49 0 -2 6 -38 239.07 1.34 0 6 -5 38 99.61 1.20 0 6 -1 -38 70.91 1.47 0 5 1 -38 98.36 1.55 0 -5 6 -38 83.02 1.11 0 6 -1 -38 83.20 1.29 0 6 -1 -38 83.18 1.49 0 -6 5 -38 82.28 1.17 0 1 -2 -39 244.64 2.42 0 -1 2 -39 232.50 1.43 0 2 -1 -39 232.43 1.99 0 -1 -1 -39 241.84 2.04 0 -1 2 -39 221.47 1.74 0 1 1 -39 213.87 1.72 0 -2 1 -39 229.08 1.72 0 2 -1 -39 234.17 1.48 0 -2 1 -39 235.76 1.82 0 -1 -1 -39 222.09 1.45 0 1 -2 -39 239.17 1.76 0 1 1 -39 226.16 1.49 0 2 2 39 143.61 1.78 0 4 -2 39 144.16 1.34 0 -4 2 -39 129.97 1.53 0 -2 4 -39 112.32 1.20 0 4 -2 -39 134.93 2.35 0 2 2 -39 126.49 1.29 0 -4 2 -39 118.46 1.64 0 2 2 -39 133.48 1.45 0 4 -2 -39 134.07 1.69 0 2 -4 -39 120.51 1.35 0 -2 -2 -39 131.26 1.61 0 5 -1 39 132.46 1.54 0 4 1 39 136.84 1.70 0 -5 1 -39 119.37 1.57 0 1 4 -39 117.85 1.50 0 -5 1 -39 113.17 1.70 0 5 -4 -39 130.80 1.35 0 -1 5 -39 119.37 1.49 0 -4 -1 -39 124.72 1.55 0 4 -5 -39 124.92 1.34 0 5 -4 39 372.52 1.66 0 -1 -4 -39 331.07 1.59 0 1 -5 -39 335.69 1.86 0 -4 5 -39 338.87 1.51 0 4 1 -39 337.79 1.74 0 5 -1 -39 350.42 2.18 0 5 -1 -39 350.65 1.99 0 -5 4 -39 330.50 1.91 0 6 -3 39 97.92 1.24 0 -3 -3 -39 87.49 1.22 0 3 -6 -39 90.97 1.60 0 -3 6 -39 86.88 1.50 0 3 3 -39 85.23 1.40 0 -6 3 -39 89.68 1.50 0 6 -3 -39 90.01 1.30 0 -1 0 -40 1810.91 3.83 0 0 1 -40 1720.85 3.40 0 0 1 -40 1696.25 2.92 0 1 -1 -40 1718.76 2.83 0 -1 0 -40 1775.47 3.07 0 1 -1 -40 1921.58 4.66 0 2 0 -40 2160.71 4.01 0 0 -2 -40 2399.70 6.06 0 -2 2 -40 2225.67 3.49 0 -2 2 -40 2145.29 3.28 0 2 0 -40 2247.12 3.21 0 0 -2 -40 2257.97 3.22 0 3 -1 40 2409.13 3.75 0 -1 3 -40 2030.15 3.33 0 -3 1 -40 2116.40 3.64 0 -1 3 -40 2001.90 3.06 0 1 2 -40 2011.68 3.01 0 -2 -1 -40 2327.31 4.62 0 -3 1 -40 2067.53 3.44 0 3 -2 -40 2101.30 3.14 0 -2 -1 -40 2072.49 3.21 0 2 -3 -40 2164.49 3.19 0 1 2 -40 2048.39 3.47 0 3 -2 -40 2330.51 7.41 0 4 0 40 2566.40 3.89 0 -4 0 -40 2395.01 3.93 0 -4 0 -40 2253.65 3.62 0 0 4 -40 2304.45 3.42 0 4 -4 -40 2426.69 3.39 0 4 -3 40 3089.75 3.93 0 -3 4 -40 2633.16 3.61 0 3 1 -40 2782.23 3.61 0 -4 3 -40 2559.51 3.78 0 4 -1 -40 2719.39 3.61 0 3 1 -40 2690.98 4.01 0 -4 3 -40 2682.85 3.80 0 4 -1 -40 2659.23 5.01 0 1 -4 -40 2713.37 3.56 0 -1 -3 -40 2715.81 3.80 0 3 2 40 1666.78 3.82 0 5 -2 40 1640.78 2.93 0 -2 5 -40 1448.28 2.74 0 -5 2 -40 1388.38 2.73 0 2 3 -40 1425.85 2.81 0 -5 2 -40 1415.23 3.09 0 5 -3 -40 1480.05 2.74 0 -3 -2 -40 1457.34 2.85 0 3 -5 -40 1547.01 2.78 0 3 -1 -41 588.79 2.81 0 -2 3 -41 574.12 2.13 0 -2 3 -41 530.24 1.85 0 2 1 -41 563.87 2.12 0 -3 2 -41 529.43 1.92 0 3 -1 -41 577.00 1.94 0 -3 2 -41 550.61 2.00 0 2 1 -41 532.99 2.03 0 1 -3 -41 564.45 1.90 0 -1 -2 -41 541.13 2.15 0 3 1 41 175.06 1.79 0 4 -1 41 171.16 1.39 0 -1 4 -41 155.87 1.29 0 -3 -1 -41 168.17 1.60 0 -4 1 -41 147.64 1.34 0 -4 1 -41 140.06 1.39 0 1 3 -41 160.04 1.30 0 4 -3 -41 169.85 1.62 0 -3 -1 -41 149.71 1.37 0 3 -4 -41 177.79 1.76 0 5 -3 41 435.47 1.89 0 -2 -3 -41 404.32 1.98 0 -5 3 -41 370.39 1.68 0 -3 5 -41 373.50 1.61 0 -5 3 -41 357.54 1.78 0 3 2 -41 374.10 1.90 0 5 -2 -41 387.40 1.70 0 2 -5 -41 395.54 1.72 0 0 0 -42 1223.60 3.36 0 0 0 -42 1140.15 2.69 0 -1 -1 -42 124.24 1.88 0 1 -2 -42 119.48 2.52 0 1 1 -42 111.72 1.56 0 -1 2 -42 112.31 1.44 0 2 -1 -42 128.99 2.15 0 -1 2 -42 118.07 1.59 0 1 1 -42 107.93 1.63 0 -2 1 -42 112.59 1.47 0 2 -1 -42 114.57 1.28 0 1 -2 -42 113.58 1.29 0 -1 -1 -42 121.59 1.60 0 -2 1 -42 113.11 1.33 0 3 0 42 334.18 1.75 0 -3 0 -42 300.06 1.74 0 -3 0 -42 277.34 1.84 0 3 -3 -42 315.36 1.90 0 0 3 -42 294.18 1.54 0 -3 3 -42 146.90 1.34 0 -3 3 -42 153.34 1.55 0 3 0 -42 179.59 1.82 0 0 -3 -42 162.59 1.70 0 3 0 -42 164.84 1.77 0 4 -2 42 85.57 1.56 0 -2 4 -42 71.68 1.49 0 -4 2 -42 64.09 1.40 0 4 -2 -42 61.89 2.12 0 -4 2 -42 72.80 1.58 0 4 -2 -42 73.38 2.68 0 4 -2 -42 75.19 1.49 0 2 2 -42 71.12 1.50 0 -2 -2 -42 73.07 1.54 0 2 -4 -42 69.93 1.61 0 -1 3 -43 141.38 1.63 0 -3 1 -43 135.84 1.40 0 -2 -1 -43 159.69 1.99 0 1 2 -43 141.92 1.32 0 3 -2 -43 221.70 5.35 0 -3 1 -43 136.05 1.32 0 3 -2 -43 160.51 1.36 0 -2 -1 -43 144.02 1.66 0 2 -3 -43 150.05 1.74 0 1 2 -43 134.85 1.36 0 1 0 -44 2108.51 4.54 0 -1 1 -44 2049.84 3.21 0 1 0 -44 2033.20 3.10 0 -1 1 -44 2086.59 3.84 0 0 -1 -44 2139.40 3.39 0 0 -1 -44 2309.81 5.54 0 0 2 -44 1481.09 3.08 0 0 2 -44 1460.76 2.75 0 -2 0 -44 1592.48 3.62 0 -2 0 -44 1505.53 2.91 0 2 -2 -44 1548.08 2.79 0 ; _shelx_hkl_checksum 42033 _shelx_res_file ; TITL Na-Li-SO4 - 180K Na3_Li_2SO4_6H2O-180K.res created by SHELXL-2018/3 at 10:27:31 on 01-Jul-2021 CELL 0.71073 8.4006 8.4006 30.1113 90.00000 90.00000 120.00000 ZERR 6 0.00190 0.00190 0.00910 0.00000 0.00000 0.00000 LATT -3 SYMM -Y, X-Y, Z SYMM -Y, -X, Z+ 0.50000 SYMM -X+Y, -X, Z SYMM X, X-Y, Z+ 0.50000 SYMM -X+Y, Y, Z+ 0.50000 SFAC Na Li S O H UNIT 18 6 12 84 72 OMIT -4 4 -2 OMIT -2 59 L.S. 12 ACTA BOND FMAP 2 PLAN 1 WGHT 0.041300 EXTI 0.055125 FVAR 0.66203 MOLE 1 LI1 2 0.666667 0.333333 0.153968 10.33333 0.01248 0.01248 = 0.00867 0.00000 0.00000 0.00624 NA1 1 0.234553 0.265845 0.060646 11.00000 0.01177 0.01387 = 0.01187 0.00357 0.00347 0.00675 S1 3 0.666667 0.333333 0.043137 10.33333 0.00683 0.00683 = 0.00335 0.00000 0.00000 0.00342 S2 3 0.333333 0.666667 0.125634 10.33333 0.00641 0.00641 = 0.00458 0.00000 0.00000 0.00320 O1 4 0.392315 0.538352 0.109028 11.00000 0.01192 0.00992 = 0.01074 -0.00204 -0.00016 0.00725 O2 4 0.518014 0.362994 0.026147 11.00000 0.00948 0.01533 = 0.01310 0.00222 0.00015 0.00851 O3 4 0.666667 0.333333 0.091240 10.33333 0.02532 0.02532 = 0.00392 0.00000 0.00000 0.01266 O4 4 0.333333 0.666667 0.174600 10.33333 0.01428 0.01428 = 0.00542 0.00000 0.00000 0.00714 O5 4 0.145430 0.429310 0.009949 11.00000 0.01169 0.00987 = 0.01032 -0.00115 0.00103 0.00512 H5A 5 0.057190 0.430534 0.020475 11.00000 0.01872 H5B 5 0.105611 0.359487 -0.010562 11.00000 0.02085 O6 4 -0.029696 0.209205 0.101794 11.00000 0.01499 0.01221 = 0.00965 -0.00003 0.00073 0.00637 H6B 5 -0.010856 0.311467 0.101527 11.00000 0.02947 H6A 5 -0.022855 0.189309 0.127543 11.00000 0.01858 HKLF 4 REM Na-Li-SO4 - 180K REM wR2 = 0.0534, GooF = S = 1.176, Restrained GooF = 1.175 for all data REM R1 = 0.0214 for 1087 Fo > 4sig(Fo) and 0.0214 for all 1088 data REM 78 parameters refined using 1 restraints END WGHT 0.0422 0.2986 REM Highest difference peak 0.227, deepest hole -0.327, 1-sigma level 0.046 Q1 1 0.3333 0.6667 0.2320 10.33333 0.05 0.21 ; _shelx_res_checksum 88547 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-y, -x, z+1/2' '-x+y, -x, z' 'x, x-y, z+1/2' '-x+y, y, z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-y+2/3, -x+1/3, z+5/6' '-x+y+2/3, -x+1/3, z+1/3' 'x+2/3, x-y+1/3, z+5/6' '-x+y+2/3, y+1/3, z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-y+1/3, -x+2/3, z+7/6' '-x+y+1/3, -x+2/3, z+2/3' 'x+1/3, x-y+2/3, z+7/6' '-x+y+1/3, y+2/3, z+7/6' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Li Li1 0.666667 0.333333 0.15397(15) 0.0112(7) Uani d 1 . . Na Na1 0.23455(8) 0.26585(8) 0.06065(3) 0.0123(2) Uani d 1 . . S S1 0.666667 0.333333 0.04314(2) 0.00567(18) Uani d 1 . . S S2 0.333333 0.666667 0.12563(2) 0.00580(18) Uani d 1 . . O O1 0.39232(16) 0.53835(14) 0.10903(4) 0.0101(2) Uani d 1 . . O O2 0.51801(14) 0.36299(14) 0.02615(4) 0.0116(2) Uani d 1 . . O O3 0.666667 0.333333 0.09124(10) 0.0182(6) Uani d 1 . . O O4 0.333333 0.666667 0.17460(9) 0.0113(5) Uani d 1 . . O O5 0.14543(15) 0.42931(14) 0.00995(4) 0.0107(2) Uani d 1 . . H H5A 0.057(4) 0.431(3) 0.0205(10) 0.019(6) Uiso d 1 . . H H5B 0.106(4) 0.359(4) -0.0106(11) 0.021(5) Uiso d 1 . . O O6 -0.02970(15) 0.20921(15) 0.10179(4) 0.0125(2) Uani d 1 . . H H6B -0.011(4) 0.311(5) 0.1015(12) 0.029(8) Uiso d 1 . . H H6A -0.023(4) 0.189(4) 0.1275(11) 0.019(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Li1 0.0125(11) 0.0125(11) 0.0087(17) 0.0062(5) 0.000 0.000 Na1 0.0118(3) 0.0139(3) 0.0119(3) 0.0068(2) 0.00347(19) 0.00357(19) S1 0.0068(2) 0.0068(2) 0.0033(3) 0.00342(11) 0.000 0.000 S2 0.0064(2) 0.0064(2) 0.0046(3) 0.00320(11) 0.000 0.000 O1 0.0119(4) 0.0099(4) 0.0107(5) 0.0073(3) -0.0002(3) -0.0020(3) O2 0.0095(4) 0.0153(5) 0.0131(4) 0.0085(4) 0.0002(3) 0.0022(3) O3 0.0253(9) 0.0253(9) 0.0039(11) 0.0127(4) 0.000 0.000 O4 0.0143(7) 0.0143(7) 0.0054(11) 0.0071(4) 0.000 0.000 O5 0.0117(4) 0.0099(4) 0.0103(5) 0.0051(3) 0.0010(4) -0.0011(3) O6 0.0150(5) 0.0122(5) 0.0096(5) 0.0064(4) 0.0007(3) 0.0000(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O3 Li1 O5 . 17_554 110.52(13) ? O3 Li1 O5 . 15_654 110.52(13) ? O5 Li1 O5 17_554 15_654 108.41(13) ? O3 Li1 O5 . 18_544 110.52(13) ? O5 Li1 O5 17_554 18_544 108.41(13) ? O5 Li1 O5 15_654 18_544 108.40(13) ? O3 Li1 Na1 . 15_654 126.01(6) ? O5 Li1 Na1 17_554 15_654 118.70(17) ? O5 Li1 Na1 15_654 15_654 34.19(6) ? O5 Li1 Na1 18_544 15_654 74.26(9) ? O3 Li1 Na1 . 18_544 126.01(6) ? O5 Li1 Na1 17_554 18_544 74.26(9) ? O5 Li1 Na1 15_654 18_544 118.70(17) ? O5 Li1 Na1 18_544 18_544 34.19(6) ? Na1 Li1 Na1 15_654 18_544 88.94(8) ? O3 Li1 Na1 . 17_554 126.01(6) ? O5 Li1 Na1 17_554 17_554 34.19(6) ? O5 Li1 Na1 15_654 17_554 74.27(9) ? O5 Li1 Na1 18_544 17_554 118.70(17) ? Na1 Li1 Na1 15_654 17_554 88.94(8) ? Na1 Li1 Na1 18_544 17_554 88.94(8) ? O2 Na1 O6 . 4 94.92(4) ? O2 Na1 O6 . . 171.37(5) ? O6 Na1 O6 4 . 87.90(6) ? O2 Na1 O5 . . 94.13(4) ? O6 Na1 O5 4 . 162.50(5) ? O6 Na1 O5 . . 85.35(5) ? O2 Na1 O1 . . 87.57(4) ? O6 Na1 O1 4 . 104.10(4) ? O6 Na1 O1 . . 83.82(4) ? O5 Na1 O1 . . 91.21(4) ? O2 Na1 O4 . 9_554 103.11(6) ? O6 Na1 O4 4 9_554 85.59(5) ? O6 Na1 O4 . 9_554 85.22(5) ? O5 Na1 O4 . 9_554 77.78(5) ? O1 Na1 O4 . 9_554 165.06(3) ? O2 Na1 Na1 . 4 102.10(4) ? O6 Na1 Na1 4 4 39.43(3) ? O6 Na1 Na1 . 4 85.26(3) ? O5 Na1 Na1 . 4 123.70(3) ? O1 Na1 Na1 . 4 142.29(3) ? O4 Na1 Na1 9_554 4 46.17(4) ? O2 Na1 Na1 . 2 149.23(3) ? O6 Na1 Na1 4 2 85.51(3) ? O6 Na1 Na1 . 2 39.06(3) ? O5 Na1 Na1 . 2 79.08(3) ? O1 Na1 Na1 . 2 122.25(3) ? O4 Na1 Na1 9_554 2 46.17(4) ? Na1 Na1 Na1 4 2 60.0 ? O2 Na1 Li1 . 9_564 72.31(3) ? O6 Na1 Li1 4 9_564 167.18(4) ? O6 Na1 Li1 . 9_564 104.59(4) ? O5 Na1 Li1 . 9_564 26.99(3) ? O1 Na1 Li1 . 9_564 74.93(6) ? O4 Na1 Li1 9_554 9_564 98.14(7) ? Na1 Na1 Li1 4 9_564 142.78(5) ? Na1 Na1 Li1 2 9_564 105.95(2) ? O3 S1 O2 . . 110.20(6) ? O3 S1 O2 . 2_655 110.21(6) ? O2 S1 O2 . 2_655 108.73(6) ? O3 S1 O2 . 4_665 110.21(6) ? O2 S1 O2 . 4_665 108.73(6) ? O2 S1 O2 2_655 4_665 108.73(6) ? O4 S2 O1 . . 109.74(6) ? O4 S2 O1 . 4_565 109.74(6) ? O1 S2 O1 . 4_565 109.20(6) ? O4 S2 O1 . 2_665 109.74(6) ? O1 S2 O1 . 2_665 109.20(6) ? O1 S2 O1 4_565 2_665 109.20(6) ? S2 O1 Na1 . . 130.92(7) ? S1 O2 Na1 . . 125.78(7) ? S1 O3 Li1 . . 180.0 ? S2 O4 Na1 . 18_554 126.90(6) ? S2 O4 Na1 . 15_554 126.90(6) ? Na1 O4 Na1 18_554 15_554 87.67(9) ? S2 O4 Na1 . 17_554 126.90(6) ? Na1 O4 Na1 18_554 17_554 87.67(9) ? Na1 O4 Na1 15_554 17_554 87.67(9) ? Li1 O5 Na1 9_564 . 118.83(9) ? Na1 O6 Na1 2 . 101.51(5) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Li1 O3 . 1.889(6) ? Li1 O5 17_554 1.9454(19) ? Li1 O5 15_654 1.9455(19) ? Li1 O5 18_544 1.9455(19) ? Li1 Na1 15_654 3.756(3) ? Li1 Na1 18_544 3.756(3) ? Li1 Na1 17_554 3.756(3) ? Na1 O2 . 2.3393(12) ? Na1 O6 4 2.3546(13) ? Na1 O6 . 2.3734(13) ? Na1 O5 . 2.4093(13) ? Na1 O1 . 2.4669(12) ? Na1 O4 9_554 2.644(2) ? Na1 Na1 4 3.6617(13) ? Na1 Na1 2 3.6618(13) ? S1 O3 . 1.448(3) ? S1 O2 . 1.4813(11) ? S1 O2 2_655 1.4814(11) ? S1 O2 4_665 1.4814(11) ? S2 O4 . 1.474(3) ? S2 O1 . 1.4804(11) ? S2 O1 4_565 1.4804(11) ? S2 O1 2_665 1.4804(11) ? _cod_database_fobs_code 2243891