#------------------------------------------------------------------------------
#$Date: 2021-08-11 05:14:50 +0300 (Wed, 11 Aug 2021) $
#$Revision: 268022 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243891.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243891
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   8.4006
_cell_length_b                   8.4006
_cell_length_c                   30.1113
_exptl_crystal_F_000             1152.00
_reflns_d_resolution_high        0.7225
_cod_data_source_file            ru2076Na3_Li_2SO4_6H2O-180Ksup3.hkl
_cod_data_source_block           Na3_Li_2SO4_6H2O-180K
_shelx_title                     ' Na-Li-SO4 - 180K'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            167.25
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-y, -x, z+1/2'
'-x+y, -x, z'
'x, x-y, z+1/2'
'-x+y, y, z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-y+2/3, -x+1/3, z+5/6'
'-x+y+2/3, -x+1/3, z+1/3'
'x+2/3, x-y+1/3, z+5/6'
'-x+y+2/3, y+1/3, z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-y+1/3, -x+2/3, z+7/6'
'-x+y+1/3, -x+2/3, z+2/3'
'x+1/3, x-y+2/3, z+7/6'
'-x+y+1/3, y+2/3, z+7/6'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 -40 4399.04 4209.96 66.49 o
-2 2 -40 5957.97 5416.84 68.33 o
-1 3 -40 5440.05 5056.22 62.38 o
-1 2 -39 566.55 528.79 5.05 o
-2 4 -39 299.19 287.72 5.57 o
-1 1 -38 650.09 643.83 13.75 o
0 2 -38 134.92 139.45 2.57 o
-2 3 -38 188.15 175.58 2.80 o
-4 4 -38 562.12 514.03 7.54 o
-1 4 -38 931.93 858.83 14.95 o
-1 3 -37 2722.01 2624.65 46.79 o
-3 4 -37 128.91 123.25 4.66 o
-2 5 -37 1447.69 1329.20 17.80 o
0 0 -36 2162.45 2190.57 56.69 o
-1 2 -36 4365.92 4255.23 48.86 o
-3 3 -36 6692.30 6501.47 62.39 o
0 3 -36 7707.84 7633.08 200.30 o
-2 4 -36 6901.73 6718.76 60.13 o
-4 5 -36 5972.65 5639.66 74.18 o
-1 5 -36 3680.78 3467.37 43.49 o
-2 3 -35 1312.95 1244.00 18.11 o
-1 4 -35 739.49 703.74 8.71 o
-3 5 -35 751.59 702.30 15.49 o
-2 6 -35 122.41 117.94 3.43 o
0 1 -34 61.78 62.14 3.22 o
-2 2 -34 1272.47 1211.57 20.34 o
-1 3 -34 931.08 925.87 15.12 o
-3 4 -34 312.36 297.10 4.75 o
0 4 -34 1240.43 1177.93 19.81 o
-5 5 -34 727.82 686.84 20.41 o
-2 5 -34 103.02 95.54 1.84 o
-4 6 -34 1023.18 971.07 26.69 o
-1 6 -34 286.84 266.96 1.85 o
-1 2 -33 3311.96 3270.54 45.51 o
-2 4 -33 2056.33 2022.19 22.08 o
-4 5 -33 242.81 243.56 6.11 o
-1 5 -33 870.85 839.16 12.07 o
-3 6 -33 1333.09 1243.84 22.29 o
-1 1 -32 622.13 536.07 6.63 o
0 2 -32 3339.41 3383.67 78.23 o
-2 3 -32 7841.96 7815.96 99.93 o
-4 4 -32 2790.05 2633.00 71.22 o
-1 4 -32 4108.27 4022.29 68.90 o
-3 5 -32 2228.28 2112.43 47.39 o
0 5 -32 57.52 75.66 10.51 o
-5 6 -32 1417.11 1345.65 54.72 o
-2 6 -32 2818.22 2682.03 39.74 o
-4 7 -32 1137.79 1019.26 27.09 o
-1 3 -31 956.96 911.02 10.45 o
-3 4 -31 1586.83 1547.08 27.17 o
-2 5 -31 845.13 795.60 12.15 o
-4 6 -31 335.95 322.75 12.42 o
-1 6 -31 796.59 741.03 7.20 o
-6 7 -31 525.65 496.22 29.22 o
-3 7 -31 334.96 333.13 6.66 o
0 0 -30 1967.68 1910.33 41.96 o
-1 2 -30 603.10 607.14 8.41 o
-3 3 -30 378.91 375.12 9.38 o
0 3 -30 865.56 809.02 13.19 o
-2 4 -30 493.05 485.73 6.05 o
-4 5 -30 1135.14 1100.34 24.80 o
-1 5 -30 578.24 581.17 7.66 o
-6 6 -30 3410.55 3566.42 282.68 o
-3 6 -30 803.41 770.31 12.14 o
0 6 -30 986.19 960.98 18.52 o
-5 7 -30 35.84 38.14 1.21 o
-2 7 -30 462.59 429.89 7.32 o
-4 8 -30 158.93 153.35 2.86 o
-2 3 -29 1921.38 1891.86 32.54 o
-1 4 -29 1884.76 1887.61 26.28 o
-3 5 -29 74.28 83.10 4.77 o
-5 6 -29 1323.48 1333.02 49.95 o
-2 6 -29 1926.37 1874.33 40.73 o
-4 7 -29 46.90 48.00 2.94 o
-1 7 -29 79.57 75.51 2.66 o
-6 8 -29 1798.25 1651.24 82.36 o
-3 8 -29 2136.49 2040.54 65.11 o
0 1 -28 2992.11 3029.74 26.40 o
-2 2 -28 5531.49 5225.47 98.38 o
-1 3 -28 6533.80 6411.81 40.26 o
-3 4 -28 12581.65 12997.46 312.38 o
0 4 -28 15832.42 16063.05 238.67 o
-5 5 -28 3068.05 3098.56 217.25 o
-2 5 -28 3273.27 3111.83 58.23 o
-4 6 -28 2280.77 2195.85 85.79 o
-1 6 -28 2437.89 2385.03 27.35 o
-6 7 -28 1518.92 1415.18 83.11 o
-3 7 -28 2323.07 2237.46 62.70 o
0 7 -28 1281.35 1201.70 30.20 o
-5 8 -28 2498.16 2269.85 73.32 o
-2 8 -28 2395.20 2217.83 63.60 o
-1 2 -27 1946.47 1898.05 29.33 o
-2 4 -27 1066.60 1110.97 26.09 o
-4 5 -27 1.88 97.80 36.38 o
-1 5 -27 132.90 137.50 4.70 o
-3 6 -27 243.17 234.99 6.78 o
-5 7 -27 629.66 603.69 21.38 o
-2 7 -27 2767.96 2694.88 79.79 o
-7 8 -27 1084.06 932.50 31.48 o
-4 8 -27 55.91 57.37 3.75 o
-1 8 -27 227.03 212.80 5.23 o
-1 1 -26 1012.72 980.56 9.20 o
0 2 -26 391.68 385.05 4.95 o
-2 3 -26 3313.25 3271.52 58.00 o
-4 4 -26 2162.58 2171.29 93.30 o
-1 4 -26 2778.10 2825.31 38.55 o
-3 5 -26 61.28 63.21 2.69 o
0 5 -26 1656.76 1660.40 20.36 o
-5 6 -26 175.82 155.70 4.95 o
-2 6 -26 1430.68 1442.92 32.39 o
-7 7 -26 872.69 821.94 3.85 o
-4 7 -26 1311.35 1297.21 38.61 o
-1 7 -26 355.07 351.47 8.15 o
-6 8 -26 436.72 411.48 10.29 o
-3 8 -26 454.89 442.45 12.09 o
-5 9 -26 516.70 465.08 15.22 o
-1 3 -25 651.80 649.66 9.49 o
-3 4 -25 4569.83 4741.32 145.51 o
-2 5 -25 1132.59 1086.90 23.50 o
-4 6 -25 1123.20 1142.44 44.64 o
-1 6 -25 344.03 329.68 8.16 o
-6 7 -25 519.08 469.30 19.99 o
-3 7 -25 326.06 330.22 10.51 o
-5 8 -25 4247.05 4113.80 170.53 o
-2 8 -25 667.07 649.97 21.16 o
-4 9 -25 999.03 932.16 27.04 o
0 0 -24 12567.87 12065.56 282.03 o
-1 2 -24 14966.45 14998.97 212.85 o
-3 3 -24 8676.03 8768.54 289.00 o
0 3 -24 14902.23 15314.50 394.79 o
-2 4 -24 19523.71 19509.77 459.08 o
-4 5 -24 5695.85 5721.44 229.95 o
-1 5 -24 5269.10 5324.70 96.96 o
-6 6 -24 6408.99 6175.99 7.75 o
-3 6 -24 9876.06 9842.17 292.80 o
0 6 -24 7377.41 7324.39 108.77 o
-5 7 -24 6992.99 6472.74 139.99 o
-2 7 -24 3753.39 3691.11 105.49 o
-7 8 -24 2201.66 1960.00 88.70 o
-4 8 -24 1962.90 1953.49 62.93 o
-1 8 -24 5605.34 5659.88 168.33 o
-6 9 -24 7340.01 6521.89 43.41 o
-3 9 -24 4446.94 4283.13 155.18 o
-2 3 -23 1226.11 1239.21 27.99 o
-1 4 -23 219.42 223.85 4.34 o
-3 5 -23 4801.03 4886.22 180.10 o
-5 6 -23 36.69 34.36 1.29 o
-2 6 -23 185.72 183.22 4.88 o
-4 7 -23 594.62 577.12 8.54 o
-1 7 -23 1393.79 1452.10 25.70 o
-6 8 -23 77.38 79.03 7.43 o
-3 8 -23 451.64 456.51 11.00 o
-5 9 -23 44.30 52.04 2.97 o
-2 9 -23 1211.62 1211.95 50.07 o
0 1 -22 2058.71 1996.69 17.82 o
-2 2 -22 2191.82 2147.17 42.28 o
-1 3 -22 3795.06 3758.33 49.00 o
-3 4 -22 2011.04 2005.86 49.03 o
0 4 -22 6534.35 6698.53 14.73 o
-5 5 -22 3083.18 2902.59 84.05 o
-2 5 -22 1569.71 1566.55 37.85 o
-4 6 -22 731.34 723.33 18.09 o
-1 6 -22 207.86 204.52 5.47 o
-6 7 -22 1730.98 1634.20 34.67 o
-3 7 -22 250.80 238.00 7.71 o
0 7 -22 659.85 701.32 36.76 o
-8 8 -22 308.53 267.58 20.22 o
-5 8 -22 627.16 601.22 8.06 o
-2 8 -22 138.30 136.55 4.96 o
-7 9 -22 95.96 99.09 9.84 o
-4 9 -22 167.05 162.05 6.01 o
-1 9 -22 639.04 635.62 37.21 o
-1 2 -21 2738.15 2733.92 45.04 o
-2 4 -21 2752.34 2782.36 43.12 o
-4 5 -21 4502.19 4333.52 129.25 o
-1 5 -21 6307.14 6608.54 142.00 o
-3 6 -21 375.19 363.70 14.49 o
-5 7 -21 84.43 82.13 2.36 o
-2 7 -21 659.93 641.03 16.71 o
-7 8 -21 1809.98 1674.56 77.57 o
-4 8 -21 306.61 301.02 6.63 o
-1 8 -21 1199.23 1238.58 34.89 o
-6 9 -21 668.27 638.38 2.00 o
-3 9 -21 1654.03 1653.92 54.82 o
-5 10 -21 800.32 724.48 3.11 o
0 2 -20 7405.33 7267.11 87.10 o
-2 3 -20 18920.62 20828.24 466.67 o
-3 5 -20 6990.92 6705.57 87.17 o
0 5 -20 13832.19 15051.52 77.12 o
-5 6 -20 5349.80 4957.84 42.74 o
-2 6 -20 12116.75 12192.74 390.02 o
-7 7 -20 15927.16 14256.17 1141.98 o
-4 7 -20 6144.29 5912.39 107.34 o
-1 7 -20 2099.63 2204.42 45.14 o
-6 8 -20 5298.92 4883.31 124.39 o
-3 8 -20 14338.55 14636.02 544.04 o
0 8 -20 7367.49 7558.16 378.95 o
-8 9 -20 6553.05 5751.82 193.82 o
-5 9 -20 7505.59 7049.27 84.40 o
-2 9 -20 7212.05 7559.77 327.33 o
-4 10 -20 3270.67 3228.04 115.70 o
-1 3 -19 11593.51 12272.06 278.73 o
-3 4 -19 1020.58 990.13 39.10 o
-2 5 -19 1234.59 1256.85 26.73 o
-4 6 -19 917.91 865.02 10.77 o
-1 6 -19 138.81 139.25 3.31 o
-6 7 -19 588.42 554.64 12.25 o
-3 7 -19 1641.33 1610.41 32.08 o
-5 8 -19 767.54 755.06 7.77 o
-2 8 -19 456.01 455.48 18.02 o
-7 9 -19 1395.59 1261.42 33.92 o
-4 9 -19 318.99 317.91 2.94 o
-1 9 -19 45.39 49.61 3.33 o
-6 10 -19 25.14 24.92 3.23 o
-3 10 -19 141.18 145.42 7.51 o
-1 2 -18 1818.11 1766.77 35.28 o
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-2 4 -18 454.78 451.05 13.52 o
-4 5 -18 731.56 717.98 13.58 o
-1 5 -18 2733.49 2746.30 58.52 o
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-2 7 -18 779.55 765.22 19.57 o
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0 9 -18 757.70 780.01 67.65 o
-5 10 -18 241.74 215.90 2.05 o
-2 3 -17 2133.58 2162.39 41.07 o
-1 4 -17 366.83 365.86 8.75 o
-3 5 -17 11361.34 10758.93 160.07 o
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-2 6 -17 1787.28 1950.78 66.14 o
-4 7 -17 2244.68 2135.78 30.78 o
-1 7 -17 647.77 659.56 15.88 o
-6 8 -17 3540.48 3295.16 53.29 o
-3 8 -17 952.48 959.83 18.32 o
-8 9 -17 1597.84 1459.04 70.88 o
-5 9 -17 748.34 706.37 3.72 o
-2 9 -17 118.72 132.45 7.17 o
-7 10 -17 463.56 416.68 7.93 o
-4 10 -17 596.41 576.83 10.12 o
-2 2 -16 6145.79 6126.56 294.11 o
-3 4 -16 4729.99 4526.46 158.23 o
0 4 -16 5490.69 5598.83 135.31 o
-5 5 -16 4722.90 4466.88 6.73 o
-2 5 -16 9169.18 8585.45 130.19 o
-1 6 -16 10905.08 11532.61 441.79 o
-6 7 -16 5552.08 5105.06 118.05 o
-3 7 -16 3500.03 3320.14 43.61 o
0 7 -16 16510.15 18266.65 13.21 o
-8 8 -16 2680.22 2425.78 53.07 o
-5 8 -16 7738.89 7285.13 128.18 o
-2 8 -16 3632.21 3820.42 147.93 o
-7 9 -16 7056.46 6718.51 168.30 o
-4 9 -16 5623.41 5441.24 46.97 o
-1 9 -16 1802.84 1901.84 97.88 o
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-1 2 -15 7536.50 7481.46 154.69 o
-2 4 -15 3069.94 2987.35 34.33 o
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-3 6 -15 2907.63 2817.34 23.31 o
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-2 7 -15 5794.19 5791.23 128.44 o
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-4 8 -15 601.67 604.58 16.59 o
-1 8 -15 2209.05 2301.86 94.40 o
-6 9 -15 552.51 531.44 8.39 o
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-8 10 -15 405.06 361.78 9.52 o
-5 10 -15 211.01 207.84 1.51 o
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-1 1 -14 4599.50 4327.75 87.22 o
0 2 -14 10928.59 10597.54 223.54 o
-2 3 -14 1078.38 1033.00 17.66 o
-4 4 -14 13756.91 13443.54 181.71 o
-1 4 -14 2961.18 3038.58 69.56 o
-3 5 -14 1891.56 1796.58 19.24 o
0 5 -14 198.66 250.77 15.63 o
-5 6 -14 1887.45 1680.03 37.50 o
-2 6 -14 398.39 415.51 7.18 o
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-4 7 -14 1774.91 1784.65 23.99 o
-1 7 -14 416.50 406.92 13.85 o
-6 8 -14 299.49 274.80 13.40 o
-3 8 -14 1190.43 1213.41 6.05 o
0 8 -14 649.35 753.38 54.25 o
-8 9 -14 608.45 574.08 12.96 o
-5 9 -14 1263.72 1218.10 14.82 o
-2 9 -14 440.82 486.79 19.54 o
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-3 4 -13 768.23 726.94 22.99 o
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-5 8 -13 106.41 101.96 5.91 o
-2 8 -13 717.65 772.70 27.40 o
-7 9 -13 1226.96 1145.75 19.92 o
-4 9 -13 170.11 160.29 3.56 o
-1 9 -13 293.22 305.90 13.08 o
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0 9 -12 1277.47 1338.12 61.89 o
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-7 11 -12 4490.24 4063.15 53.29 o
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-1 4 -11 1611.83 1568.73 11.70 o
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-6 8 -11 157.12 155.84 3.21 o
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-2 4 -9 2052.55 2127.15 37.38 o
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-1 5 -9 6111.25 6332.56 125.71 o
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-2 7 -9 3013.76 3045.17 51.73 o
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-2 10 -9 276.03 285.19 11.04 o
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0 2 -8 10027.25 9968.74 265.98 o
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-4 7 -8 12711.90 11826.37 132.85 o
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