#------------------------------------------------------------------------------
#$Date: 2021-08-11 05:14:50 +0300 (Wed, 11 Aug 2021) $
#$Revision: 268022 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/38/2243894.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243894
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   8.4570
_cell_length_b                   8.4570
_cell_length_c                   30.3317
_exptl_crystal_F_000             1152.00
_reflns_d_resolution_high        0.7802
_cod_data_source_file            ru2076Na3_Li_2SO4_6H2O-293Ksup6.hkl
_cod_data_source_block           Na3_Li_2SO4_6H2O-293K
_shelx_title                     ' Li-Na-SO4 293K in R3c'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            285.00
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-y, -x, z+1/2'
'-x+y, y, z+1/2'
'x, x-y, z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'-y+2/3, -x+1/3, z+5/6'
'-x+y+2/3, y+1/3, z+5/6'
'x+2/3, x-y+1/3, z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-y+1/3, -x+2/3, z+7/6'
'-x+y+1/3, y+2/3, z+7/6'
'x+1/3, x-y+2/3, z+7/6'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 1 -38 221.66 245.00 21.30 o
-1 3 -37 923.68 902.68 44.87 o
0 0 -36 1312.12 1037.49 25.14 o
-1 2 -36 2296.64 2289.82 105.36 o
-3 3 -36 3414.94 3623.31 203.72 o
0 3 -36 3559.77 3819.88 248.56 o
-2 4 -36 3231.30 3360.53 129.36 o
-2 3 -35 500.18 464.96 11.81 o
-1 4 -35 247.04 223.30 14.16 o
0 1 -34 25.27 18.03 10.40 o
-2 2 -34 595.70 613.15 35.23 o
-1 3 -34 390.34 324.42 9.52 o
-3 4 -34 116.48 100.85 7.52 o
0 4 -34 473.35 413.89 35.30 o
-2 5 -34 33.71 15.13 8.41 o
-1 2 -33 1531.91 1562.68 41.66 o
-2 4 -33 956.82 1018.35 19.73 o
-4 5 -33 84.21 49.24 9.82 o
-1 5 -33 292.94 275.70 18.35 o
-1 1 -32 295.50 277.93 8.72 o
0 2 -32 1882.97 1969.84 119.01 o
-2 3 -32 4044.52 4125.96 113.37 o
-4 4 -32 1557.35 1590.01 51.18 o
-1 4 -32 2252.97 2340.28 123.93 o
-3 5 -32 1304.80 1295.07 52.55 o
0 5 -32 86.79 28.87 22.15 o
-2 6 -32 1317.85 1283.98 104.06 o
-1 3 -31 502.90 466.53 14.30 o
-3 4 -31 709.85 681.69 23.54 o
-2 5 -31 335.64 292.64 20.11 o
-4 6 -31 105.33 79.62 10.00 o
-1 6 -31 262.37 227.21 17.35 o
0 0 -30 1138.50 1114.32 22.06 o
-1 2 -30 366.01 383.01 7.54 o
-3 3 -30 104.12 97.25 10.05 o
0 3 -30 466.46 425.67 47.08 o
-2 4 -30 241.48 210.05 12.66 o
-4 5 -30 441.32 455.37 12.31 o
-1 5 -30 274.38 228.11 10.23 o
-3 6 -30 313.50 274.24 16.07 o
-2 3 -29 961.71 1018.70 25.07 o
-1 4 -29 977.39 925.44 23.56 o
-3 5 -29 33.99 11.20 6.57 o
-5 6 -29 563.27 558.24 25.56 o
-2 6 -29 875.77 766.66 31.24 o
-4 7 -29 18.23 0.75 16.18 o
0 1 -28 2127.97 2234.37 50.71 o
-2 2 -28 3735.20 3707.93 199.18 o
-1 3 -28 4484.02 4521.47 191.49 o
-3 4 -28 7743.73 7855.84 331.39 o
0 4 -28 8600.78 8072.81 176.99 o
-5 5 -28 1796.71 1811.49 65.90 o
-2 5 -28 2104.88 1958.76 34.42 o
-4 6 -28 1453.74 1557.40 122.77 o
-1 6 -28 1421.63 1262.88 24.27 o
-3 7 -28 1377.32 1349.08 23.60 o
-1 2 -27 1136.93 1161.26 37.47 o
-2 4 -27 478.20 504.46 25.78 o
-4 5 -27 3.65 10.36 6.74 o
-1 5 -27 81.56 77.62 31.47 o
-3 6 -27 107.82 72.68 11.17 o
-5 7 -27 220.97 207.72 14.09 o
-2 7 -27 1080.86 1128.68 24.49 o
-1 1 -26 713.51 694.83 34.03 o
0 2 -26 134.25 167.56 15.27 o
-2 3 -26 1955.48 2206.43 79.99 o
-4 4 -26 1225.70 1306.44 15.42 o
-1 4 -26 1487.47 1317.42 36.41 o
-3 5 -26 31.84 23.24 11.00 o
0 5 -26 711.34 635.25 16.72 o
-5 6 -26 55.75 42.21 8.33 o
-2 6 -26 657.03 672.16 20.82 o
-4 7 -26 501.80 523.33 22.29 o
-1 7 -26 143.98 123.12 16.58 o
-1 3 -25 412.19 395.97 9.82 o
-3 4 -25 2760.42 3140.72 123.61 o
-2 5 -25 483.15 453.50 27.97 o
-4 6 -25 466.76 493.49 21.59 o
-1 6 -25 194.25 157.21 10.07 o
-6 7 -25 163.11 193.01 14.03 o
-3 7 -25 138.49 100.58 19.08 o
-5 8 -25 1605.88 1852.60 26.17 o
0 0 -24 7073.99 7168.13 45.44 o
-1 2 -24 11350.42 11410.38 324.52 o
-3 3 -24 6348.72 6099.10 416.01 o
0 3 -24 10219.93 9383.93 108.53 o
-2 4 -24 13072.23 11756.68 365.42 o
-4 5 -24 4076.08 4426.13 207.99 o
-1 5 -24 3695.81 3308.24 174.54 o
-6 6 -24 3582.33 4040.50 27.64 o
-3 6 -24 5929.06 5544.78 265.46 o
0 6 -24 4105.40 3541.26 32.18 o
-5 7 -24 3773.28 3956.41 306.52 o
-2 7 -24 2115.66 1789.35 25.10 o
-4 8 -24 1175.02 1171.89 23.46 o
-2 3 -23 925.39 962.12 36.64 o
-1 4 -23 132.25 137.75 13.89 o
-3 5 -23 2608.02 2725.45 51.99 o
-5 6 -23 10.05 1.22 11.51 o
-2 6 -23 86.87 64.73 11.84 o
-4 7 -23 274.70 268.83 15.18 o
-1 7 -23 523.40 482.80 17.23 o
-6 8 -23 35.39 22.60 21.45 o
-3 8 -23 153.62 136.25 21.19 o
0 1 -22 1681.16 1588.87 51.29 o
-2 2 -22 1446.69 1532.68 90.62 o
-1 3 -22 2333.60 2191.40 35.36 o
-3 4 -22 1351.86 1311.64 39.92 o
0 4 -22 4078.10 3879.64 33.63 o
-5 5 -22 1750.07 2081.95 36.71 o
-2 5 -22 773.62 747.10 20.40 o
-4 6 -22 323.52 358.71 11.87 o
-1 6 -22 111.77 80.64 11.44 o
-6 7 -22 696.08 782.77 16.35 o
-3 7 -22 119.30 99.81 13.25 o
-5 8 -22 301.32 319.55 21.13 o
-2 8 -22 57.95 32.59 20.55 o
-1 2 -21 2128.09 2197.52 77.55 o
-2 4 -21 1836.06 1783.80 86.60 o
-4 5 -21 2501.79 2827.69 32.77 o
-1 5 -21 3685.57 3555.95 43.94 o
-3 6 -21 195.16 200.01 21.74 o
-5 7 -21 58.98 43.28 13.76 o
-2 7 -21 263.36 258.20 18.96 o
-7 8 -21 683.60 867.95 90.77 o
-4 8 -21 160.65 144.96 18.12 o
-1 1 -20 27788.38 28818.96 759.41 o
0 2 -20 6223.33 5737.79 37.00 o
-2 3 -20 14677.64 14115.06 791.25 o
-4 4 -20 25486.35 28697.75 88.05 o
-1 4 -20 19911.19 18767.74 484.85 o
-3 5 -20 5113.03 5270.36 67.51 o
0 5 -20 9120.39 7890.87 48.61 o
-5 6 -20 3666.87 3903.41 41.16 o
-2 6 -20 7797.02 7629.93 48.44 o
-7 7 -20 7808.44 9564.34 51.34 o
-4 7 -20 3798.71 3997.04 36.75 o
-1 7 -20 1449.98 1348.07 25.66 o
-6 8 -20 2892.26 3106.18 32.77 o
-3 8 -20 6871.32 6869.62 48.11 o
-5 9 -20 3490.19 3589.33 37.74 o
-1 3 -19 7992.07 7432.44 167.83 o
-3 4 -19 632.51 664.25 15.15 o
-2 5 -19 754.07 749.41 31.12 o
-4 6 -19 591.36 665.45 28.42 o
-1 6 -19 73.10 77.08 16.45 o
-6 7 -19 279.16 314.03 13.93 o
-3 7 -19 840.03 764.35 21.98 o
-5 8 -19 263.12 239.88 20.04 o
-2 8 -19 213.63 197.67 16.01 o
-7 9 -19 437.85 465.12 25.88 o
-4 9 -19 132.89 105.13 16.71 o
0 0 -18 24459.44 25799.62 93.98 o
-1 2 -18 1609.47 1530.87 51.87 o
-3 3 -18 1621.28 1705.24 239.47 o
0 3 -18 2447.60 2162.62 80.40 o
-2 4 -18 355.28 359.46 14.34 o
-4 5 -18 482.18 554.97 18.39 o
-1 5 -18 1728.33 1496.04 55.85 o
-6 6 -18 243.34 323.45 17.80 o
-3 6 -18 114.00 121.33 16.90 o
0 6 -18 2388.98 2346.49 30.06 o
-5 7 -18 197.63 187.42 13.64 o
-2 7 -18 325.84 301.46 19.34 o
-7 8 -18 331.02 360.61 17.14 o
-4 8 -18 880.69 821.89 22.88 o
-6 9 -18 224.81 207.40 20.75 o
-3 9 -18 13.92 -1.60 19.27 o
-2 3 -17 1750.68 1644.44 98.15 o
-1 4 -17 217.04 208.12 10.04 o
-3 5 -17 7744.71 8326.29 428.45 o
-5 6 -17 416.45 481.53 14.71 o
-2 6 -17 1260.84 1236.09 22.64 o
-4 7 -17 1218.14 1319.25 22.12 o
-1 7 -17 251.24 252.43 20.49 o
-6 8 -17 1566.37 1705.28 27.65 o
-3 8 -17 416.49 369.44 20.50 o
-5 9 -17 324.23 328.78 22.29 o
0 1 -16 27750.83 28872.62 74.31 o
-2 2 -16 5250.16 5055.88 392.41 o
-1 3 -16 24346.93 22391.51 618.21 o
-3 4 -16 3874.12 3946.43 105.94 o
0 4 -16 4547.95 4153.42 36.22 o
-2 5 -16 6795.29 6446.32 47.04 o
-4 6 -16 18429.48 20073.90 1057.70 o
-1 6 -16 7260.07 6531.65 47.26 o
-6 7 -16 3550.20 4021.69 68.78 o
-3 7 -16 2349.53 2112.85 27.82 o
-8 8 -16 1384.45 1496.88 172.59 o
-5 8 -16 4328.71 4541.31 40.76 o
-2 8 -16 2073.79 1819.33 29.08 o
-7 9 -16 3408.62 3883.30 40.82 o
-4 9 -16 2833.68 2837.18 36.36 o
-1 2 -15 6289.42 6022.05 200.86 o
-2 4 -15 2522.24 2564.49 132.24 o
-4 5 -15 1016.97 1175.71 28.76 o
-1 5 -15 1036.30 968.50 64.36 o
-3 6 -15 1765.68 1797.54 28.06 o
-5 7 -15 815.14 881.46 21.53 o
-2 7 -15 2888.62 2738.82 33.17 o
-7 8 -15 154.07 188.18 17.80 o
-4 8 -15 267.07 290.86 19.98 o
-6 9 -15 206.75 207.40 19.27 o
-3 9 -15 6.35 -2.37 18.24 o
-5 10 -15 69.95 42.57 23.43 o
-1 1 -14 4106.44 4233.82 171.63 o
0 2 -14 9043.34 8320.39 140.05 o
-2 3 -14 888.33 943.23 51.27 o
-1 4 -14 2351.79 2194.04 176.78 o
-3 5 -14 1337.60 1486.81 94.18 o
0 5 -14 144.75 139.97 15.75 o
-5 6 -14 1166.92 1298.17 22.26 o
-2 6 -14 253.37 282.17 18.89 o
-4 7 -14 1003.77 1169.10 22.38 o
-6 8 -14 144.04 137.85 17.16 o
-3 8 -14 573.89 585.75 23.13 o
-8 9 -14 192.57 184.33 16.72 o
-5 9 -14 556.78 583.59 22.10 o
-1 3 -13 34114.27 32531.42 876.58 o
-3 4 -13 609.61 704.40 16.48 o
-2 5 -13 600.08 552.13 20.96 o
-4 6 -13 2942.82 3082.91 33.97 o
-1 6 -13 2358.01 2091.46 30.53 o
-6 7 -13 429.15 465.26 38.27 o
-3 7 -13 395.70 430.63 20.75 o
-5 8 -13 53.80 14.60 16.45 o
-7 9 -13 445.12 497.03 21.84 o
-4 9 -13 91.70 79.64 18.05 o
-6 10 -13 209.78 187.74 23.56 o
0 0 -12 52974.59 60429.47 176.66 o
-1 2 -12 10752.18 9974.84 407.30 o
0 3 -12 11325.18 10519.70 61.96 o
-2 4 -12 3524.12 3671.91 135.83 o
-4 5 -12 190.10 187.50 16.71 o
-1 5 -12 7028.58 6316.45 47.29 o
-3 6 -12 3848.78 3922.53 40.47 o
-5 7 -12 745.79 801.68 21.79 o
-2 7 -12 8404.03 7759.94 53.88 o
-7 8 -12 2929.17 3470.22 149.97 o
-4 8 -12 2918.26 2990.22 37.28 o
-6 9 -12 1068.78 1104.70 26.92 o
-5 10 -12 1057.24 1059.21 30.70 o
-2 3 -11 19339.74 19035.07 1716.81 o
-1 4 -11 1358.19 1148.67 95.87 o
-3 5 -11 34.12 52.16 19.91 o
-5 6 -11 3785.74 4608.57 41.88 o
-2 6 -11 1125.04 1047.95 27.26 o
-4 7 -11 323.33 352.13 16.46 o
-6 8 -11 103.01 123.31 17.35 o
-3 8 -11 1736.49 1456.63 28.49 o
-8 9 -11 134.22 106.02 15.39 o
-5 9 -11 480.48 480.03 22.74 o
-7 10 -11 32.14 8.39 19.78 o
0 1 -10 864.62 839.99 50.77 o
-2 2 -10 6975.50 5926.62 51.77 o
-1 3 -10 1965.65 1852.53 118.25 o
-3 4 -10 559.28 678.43 20.77 o
0 4 -10 8752.47 7549.62 53.10 o
-2 5 -10 1824.44 1734.87 30.97 o
-4 6 -10 1130.15 1241.65 26.36 o
-1 6 -10 1164.79 1036.05 26.30 o
-6 7 -10 24.52 12.72 12.68 o
-3 7 -10 1400.57 1341.19 27.78 o
-8 8 -10 67.11 59.41 23.37 o
-5 8 -10 299.66 315.28 21.33 o
-7 9 -10 23.89 18.18 17.09 o
-4 9 -10 180.57 137.22 18.95 o
-6 10 -10 416.20 396.52 27.48 o
-1 2 -9 27141.22 25376.20 1194.67 o
-2 4 -9 1866.34 2165.62 220.27 o
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-1 5 -9 4503.47 4086.07 42.77 o
-3 6 -9 5099.92 5059.69 48.72 o
-5 7 -9 5200.04 6372.90 52.99 o
-2 7 -9 1837.44 1653.87 30.95 o
-7 8 -9 809.16 962.84 64.33 o
-4 8 -9 607.74 598.30 22.49 o
-6 9 -9 47.94 38.80 20.17 o
-1 1 -8 81223.37 84775.49 253.93 o
0 2 -8 9676.20 8615.03 520.70 o
-2 3 -8 9664.78 12013.56 76.45 o
-1 4 -8 8488.47 7787.30 59.81 o
-3 5 -8 7609.04 8404.33 62.20 o
-5 6 -8 5623.17 5231.34 78.81 o
-2 6 -8 1062.62 1034.07 28.93 o
-7 7 -8 520.61 469.14 23.38 o
-4 7 -8 8927.75 9170.77 66.19 o
-6 8 -8 4443.27 5068.02 49.03 o
-8 9 -8 2688.57 2977.24 211.81 o
-5 9 -8 1310.48 1177.27 30.20 o
-7 10 -8 1187.01 1144.31 20.84 o
-1 3 -7 1347.07 1342.50 71.78 o
-2 5 -7 9525.56 9474.32 69.33 o
-4 6 -7 72.17 111.78 17.29 o
-6 7 -7 633.46 729.94 52.13 o
-3 7 -7 1659.83 1659.81 34.54 o
-5 8 -7 969.86 925.38 28.14 o
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-6 10 -7 60.72 41.04 27.91 o
0 0 -6 9899.96 11268.11 100.78 o
-1 2 -6 2625.90 2785.46 190.13 o
0 3 -6 3639.46 3546.91 45.31 o
-2 4 -6 1019.29 1003.06 27.99 o
-4 5 -6 1826.56 1764.40 48.97 o
-1 5 -6 1579.32 1370.31 30.12 o
-6 6 -6 6888.35 6678.66 64.24 o
-3 6 -6 1162.90 1131.75 28.74 o
-5 7 -6 1147.66 1219.60 28.03 o
-7 8 -6 125.56 140.34 10.71 o
-4 8 -6 938.84 890.81 28.59 o
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-5 9 -5 300.69 269.16 25.68 o
-7 10 -5 211.35 208.08 17.09 o
0 1 -4 29016.44 28406.04 834.98 o
-1 3 -4 49189.03 46535.80 189.35 o
-3 4 -4 2162.88 1946.19 56.99 o
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-2 5 -4 17859.91 16010.68 103.02 o
-4 6 -4 9377.11 9833.74 76.89 o
-6 7 -4 17160.82 17212.42 1290.35 o
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-1 2 -3 2385.07 3033.18 59.84 o
-2 4 -3 1026.07 1167.80 33.51 o
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-3 6 -3 119.41 141.89 22.28 o
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-7 8 -3 1445.04 1705.10 97.44 o
-6 9 -3 632.09 596.45 34.63 o
-8 10 -3 172.89 140.81 17.39 o
-2 3 -2 10175.33 10488.42 150.91 o
-4 4 -2 1103.71 803.45 31.26 o
-3 5 -2 2965.24 3184.35 52.53 o
-5 6 -2 510.63 589.77 34.54 o
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-6 8 -2 279.22 299.97 34.93 o
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-1 3 -1 8167.22 7471.93 93.03 o
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-5 6 1 446.89 434.68 46.29 o
-6 8 1 272.95 282.59 17.61 o
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-2 2 2 3357.84 3079.57 56.54 o
-3 4 2 8706.78 8776.21 822.05 o
-5 5 2 3354.13 3311.34 42.41 o
-4 6 2 4317.21 3710.30 235.04 o
-6 7 2 1593.33 1644.82 156.63 o
-8 8 2 904.49 1114.52 26.92 o
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-1 2 3 2384.21 2240.82 44.93 o
-4 5 3 3520.26 3626.88 313.21 o
-5 7 3 1279.80 1247.95 25.79 o
-7 8 3 1078.78 1292.48 63.27 o
-4 8 3 946.95 879.04 20.39 o
-6 9 3 1041.11 1070.69 21.41 o
-8 10 3 252.59 236.29 23.56 o
-5 10 3 418.35 447.64 18.25 o
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-4 7 4 13245.81 12260.36 61.85 o
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