#------------------------------------------------------------------------------ #$Date: 2021-08-11 05:15:44 +0300 (Wed, 11 Aug 2021) $ #$Revision: 268023 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/38/2243896.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243896 loop_ _publ_author_name 'Whited, Matthew T.' 'Ball, Margaret A.' 'Block, Alison' 'Brewster, Benjamin A.' 'Ferrer, LouLou' 'Jin-Lee, Helen J.' 'King, Colby J.' 'North, Jamie D.' 'Shelton, Inger L.' 'Wilson, David G.' _publ_section_title ; Crystal structures of phosphine-supported (\h^5^-cyclopentadienyl)molybdenum(II) propionyl complexes ; _journal_coeditor_code JQ2008 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989021008008 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac '[Mo (C5 H5) (C3 H5 O) (C18 H12 F3 P) (C O)2]' _chemical_formula_moiety 'C28 H22 F3 Mo O3 P' _chemical_formula_sum 'C28 H22 F3 Mo O3 P' _chemical_formula_weight 590.36 _chemical_name_common CpMo(CO)2(P(4-FPh)3(COEt) _chemical_name_systematic Dicarbonyl(\h^5^-cyclopentadienyl)propionyl[tris(4-fluorophenyl)phosphane-\kP]molybdenum(II) _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 97.256(2) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 11.7991(4) _cell_length_b 18.6907(8) _cell_length_c 22.4744(8) _cell_measurement_reflns_used 9718 _cell_measurement_temperature 170.(2) _cell_measurement_theta_max 30.5150 _cell_measurement_theta_min 2.3352 _cell_volume 4916.7(3) _computing_cell_refinement ; SAINT (Bruker, 2019) ; _computing_data_collection ; BIS (Bruker, 2019) ; _computing_data_reduction ; SAINT (Bruker, 2019) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2020) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 170.(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'Fixed--\c Diffractometer' _diffrn_measurement_device_type 'Bruker D8 QUEST ECO' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'Curved Graphite' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0418 _diffrn_reflns_av_unetI/netI 0.0270 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 73758 _diffrn_reflns_theta_full 25.24 _diffrn_reflns_theta_max 26.37 _diffrn_reflns_theta_min 2.33 _diffrn_source 'sealed tube' _diffrn_source_current 20.0 _diffrn_source_power 1.00 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.650 _exptl_absorpt_correction_T_max 0.97 _exptl_absorpt_correction_T_min 0.86 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (Krause et al., 2015) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.595 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 2384 _exptl_crystal_size_max 0.050 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.373 _refine_diff_density_min -0.393 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.068 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 651 _refine_ls_number_reflns 10047 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.068 _refine_ls_R_factor_all 0.0386 _refine_ls_R_factor_gt 0.0292 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0211P)^2^+4.4865P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0605 _refine_ls_wR_factor_ref 0.0633 _reflns_number_gt 8547 _reflns_number_total 10047 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jq2008sup1.cif _cod_data_source_block 2 _cod_database_code 2243896 _shelx_hkl_file ; 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0 0 3.93 0.87 -13 0 0 15.02 1.35 -13 0 0 13.19 1.38 13 0 0 13.61 1.46 14 0 0 6.78 1.06 14 -1 0 0.27 0.73 -14 1 0 -0.18 0.65 13 -1 0 35.69 2.08 -13 1 0 35.76 2.03 -13 1 0 37.32 1.96 12 -1 0 0.43 0.72 -12 1 0 0.58 0.64 -12 1 0 0.98 0.66 11 -1 0 15.05 1.38 -11 1 0 13.25 1.30 -11 1 0 14.03 1.23 10 -1 0 10.60 1.13 -10 1 0 11.56 1.09 -10 1 0 10.60 1.12 9 -1 0 34.53 1.62 9 -1 0 37.05 1.75 -9 1 0 35.77 1.66 -9 1 0 38.04 1.72 8 -1 0 25.77 1.29 8 -1 0 26.24 1.32 8 -1 0 25.08 1.32 8 -1 0 26.12 1.37 -8 1 0 25.58 1.33 -8 1 0 26.85 1.33 7 -1 0 28.79 1.34 7 -1 0 29.11 1.31 7 -1 0 29.13 1.34 -7 1 0 29.18 1.34 -7 1 0 29.40 1.33 6 -1 0 2.49 0.48 6 -1 0 1.26 0.45 6 -1 0 1.65 0.44 -6 1 0 1.39 0.49 -6 1 0 1.77 0.48 -6 1 0 1.52 0.44 5 -1 0 4.30 0.54 5 -1 0 4.71 0.53 5 -1 0 4.44 0.56 -5 1 0 3.70 0.49 -5 1 0 3.95 0.53 -5 1 0 3.53 0.48 4 -1 0 26.68 1.06 4 -1 0 25.44 1.10 4 -1 0 26.28 1.09 -4 1 0 27.08 1.08 -4 1 0 25.56 1.08 -4 1 0 26.76 1.09 3 -1 0 240.82 6.88 3 -1 0 240.84 6.89 3 -1 0 245.66 6.91 -3 1 0 242.79 6.90 -3 1 0 247.29 6.89 -3 1 0 246.38 6.90 2 -1 0 472.89 12.73 2 -1 0 479.47 12.73 -2 1 0 429.77 12.72 -2 1 0 459.26 12.73 -1 -1 0 0.05 0.09 -1 -1 0 0.06 0.07 -2 -1 0 479.56 13.26 -2 -1 0 487.58 13.26 2 1 0 483.05 13.25 2 1 0 475.50 13.26 -3 -1 0 219.18 6.73 -3 -1 0 243.82 6.80 -3 -1 0 241.54 6.76 3 1 0 247.90 6.76 3 1 0 248.26 6.76 3 1 0 243.77 6.79 -4 -1 0 26.15 1.05 -4 -1 0 26.80 1.03 -4 -1 0 25.40 1.00 4 1 0 25.22 1.01 4 1 0 26.48 1.01 4 1 0 25.69 1.05 -5 -1 0 4.22 0.50 -5 -1 0 4.57 0.55 -5 -1 0 5.36 0.58 5 1 0 3.97 0.45 5 1 0 6.05 0.59 5 1 0 4.31 0.51 -6 -1 0 2.12 0.49 -6 -1 0 1.72 0.41 -6 -1 0 1.32 0.40 6 1 0 1.91 0.44 6 1 0 1.61 0.41 6 1 0 2.04 0.48 -7 -1 0 27.76 1.24 -7 -1 0 27.98 1.27 -7 -1 0 28.93 1.33 7 1 0 26.95 1.25 7 1 0 27.88 1.23 7 1 0 28.07 1.30 -8 -1 0 26.04 1.25 -8 -1 0 25.68 1.33 -8 -1 0 26.46 1.27 8 1 0 27.35 1.26 8 1 0 24.55 1.28 8 1 0 22.15 1.22 -9 -1 0 34.04 1.55 -9 -1 0 34.20 1.57 -9 -1 0 32.29 1.62 9 1 0 36.55 1.57 9 1 0 29.07 1.47 -10 -1 0 14.03 1.14 -10 -1 0 10.63 1.11 -10 -1 0 10.06 1.00 10 1 0 12.54 1.05 -11 -1 0 15.09 1.26 -11 -1 0 13.08 1.16 11 1 0 15.92 1.30 -12 -1 0 0.63 0.64 -12 -1 0 0.20 0.60 12 1 0 0.43 0.65 -13 -1 0 35.40 1.96 13 1 0 35.53 2.04 14 1 0 -0.20 0.65 14 1 0 0.02 0.65 14 -2 0 2.82 0.91 -14 2 0 4.77 0.98 -14 2 0 3.27 0.87 13 -2 0 -0.06 0.76 -13 2 0 1.02 0.72 -13 2 0 0.52 0.69 12 -2 0 -0.33 0.64 -12 2 0 0.87 0.70 -12 2 0 0.32 0.64 11 -2 0 55.90 2.49 -11 2 0 56.04 2.44 -11 2 0 55.81 2.38 10 -2 0 -0.22 0.55 -10 2 0 -0.07 0.57 -10 2 0 1.08 0.65 9 -2 0 0.24 0.55 9 -2 0 -0.42 0.46 -9 2 0 -0.01 0.49 -9 2 0 -0.32 0.51 8 -2 0 13.29 1.01 8 -2 0 13.97 1.00 8 -2 0 13.90 1.01 8 -2 0 10.33 0.97 -8 2 0 10.48 0.98 -8 2 0 12.95 1.02 7 -2 0 33.40 1.50 7 -2 0 34.08 1.48 7 -2 0 34.70 1.51 7 -2 0 32.36 1.45 -7 2 0 34.55 1.49 -7 2 0 34.25 1.50 6 -2 0 6.23 0.69 6 -2 0 7.22 0.74 6 -2 0 6.93 0.74 6 -2 0 5.83 0.62 -6 2 0 5.67 0.60 -6 2 0 6.25 0.73 5 -2 0 111.44 3.46 5 -2 0 110.92 3.48 5 -2 0 112.51 3.48 5 -2 0 113.16 3.50 -5 2 0 113.17 3.48 -5 2 0 114.39 3.49 4 -2 0 65.38 2.15 4 -2 0 66.68 2.15 4 -2 0 66.80 2.17 4 -2 0 64.76 2.16 -4 2 0 66.16 2.16 -4 2 0 68.45 2.17 3 -2 0 30.39 1.13 3 -2 0 26.73 1.10 3 -2 0 27.20 1.11 3 -2 0 28.15 1.10 -3 2 0 30.94 1.12 -3 2 0 31.94 1.13 2 -2 0 0.72 0.31 2 -2 0 0.47 0.32 2 -2 0 0.88 0.26 -2 2 0 0.06 0.30 -2 2 0 0.95 0.31 -2 2 0 0.26 0.26 1 -2 0 10.49 0.50 1 -2 0 10.66 0.46 -1 2 0 10.48 0.49 -1 2 0 10.41 0.46 -1 2 0 11.19 0.49 0 -2 0 -0.16 0.10 0 -2 0 -0.03 0.07 -1 -2 0 11.62 0.35 -1 -2 0 10.83 0.45 -1 -2 0 11.16 0.41 -2 -2 0 0.52 0.26 -2 -2 0 0.30 0.20 2 2 0 0.70 0.20 2 2 0 0.91 0.22 2 2 0 0.42 0.27 2 2 0 0.83 0.22 -3 -2 0 30.32 1.11 -3 -2 0 28.91 1.04 3 2 0 30.83 1.04 3 2 0 31.08 1.11 3 2 0 31.15 1.04 -4 -2 0 67.25 2.13 -4 -2 0 67.05 2.07 -4 -2 0 67.20 2.06 4 2 0 67.23 2.06 4 2 0 64.34 2.05 4 2 0 64.91 2.11 -5 -2 0 111.29 3.36 -5 -2 0 112.16 3.44 -5 -2 0 110.07 3.37 5 2 0 114.32 3.36 5 2 0 112.22 3.37 5 2 0 113.01 3.43 -6 -2 0 6.80 0.71 -6 -2 0 5.98 0.65 -6 -2 0 7.34 0.64 6 2 0 6.67 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2 3 0 7.44 0.45 2 3 0 7.52 0.52 -3 -3 0 86.66 2.51 -3 -3 0 84.54 2.60 3 3 0 87.25 2.61 3 3 0 86.34 2.52 3 3 0 86.92 2.52 3 3 0 85.79 2.51 -4 -3 0 14.36 0.69 -4 -3 0 15.72 0.79 4 3 0 14.33 0.68 4 3 0 14.21 0.77 4 3 0 14.55 0.68 4 3 0 13.50 0.66 -5 -3 0 0.05 0.30 -5 -3 0 0.02 0.34 5 3 0 0.41 0.31 5 3 0 0.43 0.36 5 3 0 0.41 0.30 5 3 0 0.34 0.31 -6 -3 0 4.81 0.50 -6 -3 0 4.87 0.58 6 3 0 4.04 0.48 6 3 0 3.41 0.52 6 3 0 5.23 0.59 6 3 0 4.57 0.50 -7 -3 0 15.46 0.88 -7 -3 0 15.66 0.98 7 3 0 14.70 0.85 7 3 0 13.96 0.84 7 3 0 13.54 0.93 -8 -3 0 6.29 0.67 -8 -3 0 6.05 0.75 8 3 0 6.31 0.71 8 3 0 6.18 0.72 8 3 0 6.42 0.66 8 3 0 6.79 0.71 -9 -3 0 12.32 1.05 -9 -3 0 12.42 0.96 9 3 0 11.16 0.89 9 3 0 9.92 0.90 9 3 0 11.35 0.89 9 3 0 10.08 1.03 -10 -3 0 9.64 1.08 -10 -3 0 11.52 1.04 10 3 0 10.24 0.99 10 3 0 9.45 0.93 -11 -3 0 -1.00 0.54 -11 -3 0 -0.32 0.53 11 3 0 0.52 0.63 11 3 0 0.42 0.55 -12 -3 0 13.43 1.34 -12 -3 0 12.16 1.25 12 3 0 14.60 1.23 -13 -3 0 5.44 0.88 13 3 0 7.27 0.95 13 3 0 6.93 1.04 14 3 0 0.67 0.68 14 3 0 1.07 0.67 14 3 0 1.59 0.76 14 -4 0 4.21 1.00 -14 4 0 2.68 0.92 13 -4 0 5.67 1.02 -13 4 0 4.54 0.92 -13 4 0 6.83 1.02 12 -4 0 14.89 1.44 -12 4 0 15.34 1.45 -12 4 0 15.45 1.48 11 -4 0 0.53 0.69 -11 4 0 1.14 0.75 -11 4 0 -0.25 0.60 10 -4 0 1.01 0.67 -10 4 0 0.75 0.60 -10 4 0 1.21 0.65 9 -4 0 0.11 0.53 -9 4 0 0.33 0.57 -9 4 0 0.34 0.59 8 -4 0 27.98 1.45 8 -4 0 26.23 1.60 8 -4 0 26.49 1.42 -8 4 0 29.19 1.46 -8 4 0 23.77 1.37 7 -4 0 0.05 0.45 7 -4 0 0.86 0.46 7 -4 0 0.17 0.45 7 -4 0 -0.48 0.39 -7 4 0 0.32 0.47 -7 4 0 0.58 0.49 6 -4 0 8.01 0.81 6 -4 0 8.12 0.79 6 -4 0 7.06 0.82 6 -4 0 7.69 0.79 -6 4 0 7.59 0.77 -6 4 0 7.09 0.79 5 -4 0 -0.08 0.41 5 -4 0 -0.14 0.37 5 -4 0 -0.18 0.37 5 -4 0 0.49 0.45 -5 4 0 0.66 0.44 -5 4 0 -0.11 0.44 4 -4 0 7.99 0.72 4 -4 0 7.38 0.74 4 -4 0 8.69 0.72 4 -4 0 8.50 0.71 -4 4 0 7.21 0.70 -4 4 0 8.09 0.75 3 -4 0 1.54 0.38 3 -4 0 1.24 0.38 3 -4 0 1.19 0.39 -3 4 0 1.93 0.38 -3 4 0 1.37 0.35 -3 4 0 1.64 0.40 2 -4 0 40.42 1.38 2 -4 0 36.19 1.39 2 -4 0 41.09 1.36 -2 4 0 40.39 1.40 -2 4 0 36.66 1.36 -2 4 0 40.81 1.35 1 -4 0 32.71 1.11 1 -4 0 31.23 1.04 1 -4 0 31.10 1.12 -1 4 0 30.57 1.09 -1 4 0 25.87 1.01 -1 4 0 30.37 1.11 0 -4 0 295.30 9.11 0 -4 0 345.81 9.13 0 -4 0 351.23 9.05 0 4 0 303.55 9.11 0 4 0 343.25 9.13 -1 -4 0 30.60 0.86 -1 -4 0 30.44 1.01 -1 -4 0 24.69 1.02 1 4 0 31.01 1.05 1 4 0 30.14 0.85 1 4 0 30.71 1.02 -2 -4 0 40.35 1.33 -2 -4 0 39.26 1.25 -2 -4 0 40.67 1.16 2 4 0 39.35 1.16 2 4 0 39.23 1.26 2 4 0 40.85 1.34 -3 -4 0 1.71 0.23 -3 -4 0 1.68 0.27 -3 -4 0 1.45 0.35 3 4 0 1.21 0.28 3 4 0 1.64 0.24 3 4 0 1.12 0.33 -4 -4 0 7.93 0.50 -4 -4 0 7.81 0.63 4 4 0 7.52 0.49 4 4 0 8.95 0.65 4 4 0 7.20 0.52 4 4 0 8.28 0.54 -5 -4 0 0.33 0.36 -5 -4 0 0.28 0.29 5 4 0 0.24 0.28 5 4 0 0.08 0.30 5 4 0 -0.07 0.29 5 4 0 -0.06 0.36 -6 -4 0 8.23 0.75 -6 -4 0 7.64 0.63 6 4 0 7.75 0.61 6 4 0 8.24 0.64 6 4 0 8.40 0.64 6 4 0 7.55 0.73 -7 -4 0 0.12 0.41 -7 -4 0 0.80 0.36 7 4 0 0.15 0.39 7 4 0 0.57 0.36 7 4 0 0.17 0.33 7 4 0 0.27 0.35 -8 -4 0 27.43 1.27 -8 -4 0 26.88 1.38 8 4 0 28.20 1.37 8 4 0 28.81 1.27 8 4 0 27.52 1.25 8 4 0 29.40 1.27 -9 -4 0 2.44 0.53 -9 -4 0 0.42 0.51 9 4 0 0.11 0.45 9 4 0 1.05 0.54 9 4 0 -0.09 0.41 9 4 0 0.53 0.43 -10 -4 0 1.45 0.61 -10 -4 0 1.01 0.53 10 4 0 1.06 0.50 10 4 0 0.34 0.48 10 4 0 2.26 0.58 -11 -4 0 0.42 0.60 -11 -4 0 0.54 0.55 11 4 0 0.31 0.47 11 4 0 -0.12 0.51 -12 -4 0 14.05 1.33 -12 -4 0 13.66 1.23 12 4 0 15.09 1.19 -13 -4 0 5.61 0.97 13 4 0 6.69 0.93 14 4 0 4.90 0.94 14 4 0 3.02 0.77 14 4 0 2.79 0.75 14 -5 0 -0.43 0.76 -14 5 0 0.35 0.74 13 -5 0 4.17 1.02 -13 5 0 3.78 0.93 -13 5 0 4.91 1.00 12 -5 0 14.70 1.45 -12 5 0 13.10 1.40 -12 5 0 13.70 1.47 11 -5 0 9.41 1.18 -11 5 0 8.82 1.12 -11 5 0 8.40 1.04 10 -5 0 25.25 1.62 -10 5 0 27.13 1.65 9 -5 0 1.91 0.65 -9 5 0 2.36 0.73 -9 5 0 1.99 0.65 8 -5 0 0.68 0.51 8 -5 0 0.90 0.58 -8 5 0 1.09 0.52 -8 5 0 0.21 0.49 7 -5 0 10.46 0.95 7 -5 0 9.95 0.94 7 -5 0 11.11 0.93 7 -5 0 9.57 0.88 -7 5 0 8.98 0.95 -7 5 0 7.95 0.88 6 -5 0 41.07 1.68 6 -5 0 41.11 1.70 6 -5 0 40.99 1.66 6 -5 0 40.11 1.70 -6 5 0 42.12 1.71 -6 5 0 41.69 1.70 5 -5 0 19.44 1.07 5 -5 0 21.73 1.10 5 -5 0 19.97 1.09 5 -5 0 20.35 1.12 -5 5 0 20.15 1.08 -5 5 0 21.52 1.13 4 -5 0 5.33 0.56 4 -5 0 4.66 0.60 4 -5 0 4.69 0.62 -4 5 0 4.18 0.54 -4 5 0 3.71 0.47 -4 5 0 4.19 0.54 3 -5 0 3.23 0.47 3 -5 0 4.25 0.54 3 -5 0 3.72 0.45 -3 5 0 4.05 0.54 -3 5 0 3.44 0.45 -3 5 0 2.98 0.41 2 -5 0 0.32 0.35 2 -5 0 0.44 0.33 2 -5 0 -0.02 0.37 -2 5 0 0.54 0.36 -2 5 0 0.29 0.36 -2 5 0 0.94 0.34 1 -5 0 253.91 7.18 1 -5 0 260.73 7.18 1 -5 0 259.60 7.11 -1 5 0 225.36 7.14 -1 5 0 257.67 7.18 -1 5 0 264.32 7.12 0 -5 0 0.10 0.20 0 -5 0 0.26 0.33 0 -5 0 -0.12 0.20 0 -5 0 0.04 0.30 0 5 0 -0.12 0.30 0 5 0 0.13 0.31 -1 -5 0 260.02 6.92 -1 -5 0 254.94 7.04 -1 -5 0 257.64 6.92 -1 -5 0 259.83 7.09 1 5 0 221.10 7.02 1 5 0 255.57 7.08 -2 -5 0 0.57 0.31 -2 -5 0 0.51 0.26 2 5 0 0.25 0.27 2 5 0 0.27 0.31 -3 -5 0 4.23 0.44 -3 -5 0 3.97 0.30 -3 -5 0 3.88 0.35 3 5 0 3.01 0.35 3 5 0 3.52 0.30 3 5 0 4.72 0.54 -4 -5 0 4.45 0.40 -4 -5 0 3.88 0.47 4 5 0 5.14 0.59 4 5 0 4.15 0.46 4 5 0 4.63 0.41 4 5 0 4.57 0.49 -5 -5 0 20.74 0.84 -5 -5 0 19.60 0.99 5 5 0 19.21 0.83 5 5 0 17.48 0.85 5 5 0 22.66 1.03 5 5 0 21.27 0.89 -6 -5 0 41.45 1.46 -6 -5 0 42.93 1.62 6 5 0 39.64 1.45 6 5 0 41.20 1.46 6 5 0 41.86 1.60 6 5 0 41.20 1.47 -7 -5 0 9.45 0.85 -7 -5 0 10.94 0.73 7 5 0 10.92 0.74 7 5 0 9.18 0.69 7 5 0 9.85 0.73 7 5 0 10.75 0.84 -8 -5 0 0.40 0.47 -8 -5 0 0.43 0.40 8 5 0 0.56 0.39 8 5 0 0.96 0.47 8 5 0 0.68 0.38 8 5 0 0.73 0.42 -9 -5 0 1.90 0.59 -9 -5 0 1.58 0.49 9 5 0 2.20 0.65 9 5 0 1.70 0.52 9 5 0 2.71 0.52 9 5 0 2.11 0.49 -10 -5 0 21.34 1.28 -10 -5 0 24.93 1.46 10 5 0 24.47 1.28 10 5 0 26.60 1.33 10 5 0 25.27 1.31 -11 -5 0 7.14 0.83 -11 -5 0 8.56 1.01 11 5 0 8.30 0.91 11 5 0 6.23 0.81 -12 -5 0 11.01 1.25 -12 -5 0 13.02 1.15 12 5 0 12.29 1.13 -13 -5 0 4.02 0.89 13 5 0 4.07 0.74 13 5 0 3.42 0.74 14 5 0 -0.30 0.59 14 5 0 -0.18 0.63 14 -6 0 3.55 1.01 14 -6 0 3.25 1.01 -14 6 0 3.20 1.01 13 -6 0 3.56 0.96 -13 6 0 3.37 0.93 -13 6 0 1.27 0.87 12 -6 0 15.42 1.51 -12 6 0 15.78 1.45 -12 6 0 11.62 1.25 11 -6 0 20.93 1.57 -11 6 0 19.92 1.53 -11 6 0 20.72 1.56 10 -6 0 13.10 1.29 -10 6 0 13.14 1.33 -10 6 0 11.23 1.24 9 -6 0 1.23 0.62 -9 6 0 1.09 0.63 -9 6 0 2.06 0.69 8 -6 0 7.87 0.93 -8 6 0 7.96 0.86 -8 6 0 6.73 0.83 7 -6 0 13.96 1.10 7 -6 0 17.37 1.11 7 -6 0 14.01 1.04 7 -6 0 15.35 1.10 -7 6 0 15.28 1.08 -7 6 0 12.60 1.06 6 -6 0 28.87 1.39 6 -6 0 26.79 1.38 6 -6 0 25.96 1.31 6 -6 0 29.22 1.38 -6 6 0 31.44 1.44 -6 6 0 28.18 1.36 5 -6 0 140.60 4.30 5 -6 0 134.77 4.29 5 -6 0 139.73 4.26 -5 6 0 139.57 4.28 -5 6 0 139.56 4.31 -5 6 0 134.35 4.26 4 -6 0 2.90 0.51 4 -6 0 2.38 0.46 4 -6 0 3.09 0.51 -4 6 0 1.94 0.47 -4 6 0 2.35 0.47 -4 6 0 3.12 0.58 3 -6 0 96.98 3.02 3 -6 0 93.37 3.03 3 -6 0 96.31 2.97 -3 6 0 93.64 2.99 -3 6 0 97.40 2.98 2 -6 0 3.45 0.49 2 -6 0 3.98 0.45 2 -6 0 3.32 0.46 -2 6 0 4.61 0.54 -2 6 0 3.49 0.42 -2 6 0 4.15 0.49 1 -6 0 1.34 0.31 1 -6 0 1.06 0.36 1 -6 0 1.37 0.38 -1 6 0 1.39 0.30 -1 6 0 0.79 0.34 -1 6 0 1.98 0.43 0 -6 0 156.67 4.38 0 -6 0 157.18 4.50 0 -6 0 156.08 4.50 0 -6 0 156.21 4.37 0 6 0 146.36 4.48 0 6 0 158.06 4.50 -1 -6 0 1.75 0.18 -1 -6 0 1.86 0.39 -1 -6 0 1.48 0.36 -1 -6 0 1.77 0.18 1 6 0 1.62 0.35 1 6 0 0.81 0.33 -2 -6 0 3.86 0.38 -2 -6 0 3.06 0.42 2 6 0 3.83 0.39 2 6 0 3.65 0.42 -3 -6 0 96.40 2.68 -3 -6 0 97.16 2.93 -3 -6 0 94.52 2.81 3 6 0 95.57 2.82 3 6 0 93.46 2.91 3 6 0 94.72 2.68 -4 -6 0 2.35 0.33 -4 -6 0 2.64 0.45 -4 -6 0 2.93 0.28 4 6 0 2.80 0.39 4 6 0 2.62 0.28 -5 -6 0 138.49 3.90 -5 -6 0 138.79 4.10 5 6 0 134.75 3.95 5 6 0 136.88 3.90 5 6 0 124.91 3.93 5 6 0 135.09 4.08 -6 -6 0 31.02 1.31 -6 -6 0 29.62 1.11 6 6 0 29.46 1.14 6 6 0 28.97 1.16 6 6 0 28.73 1.11 6 6 0 28.75 1.29 -7 -6 0 15.17 0.82 -7 -6 0 14.93 0.98 7 6 0 15.88 0.86 7 6 0 14.65 0.83 7 6 0 15.20 0.82 7 6 0 14.93 0.98 -8 -6 0 6.91 0.70 -8 -6 0 8.42 0.89 8 6 0 6.48 0.73 8 6 0 7.25 0.69 8 6 0 7.39 0.70 8 6 0 7.25 0.83 -9 -6 0 0.75 0.44 -9 -6 0 1.41 0.57 9 6 0 0.65 0.48 9 6 0 0.92 0.44 9 6 0 0.87 0.44 -10 -6 0 14.14 1.18 -10 -6 0 12.33 0.98 10 6 0 12.39 1.01 10 6 0 12.06 0.95 10 6 0 12.14 0.97 -11 -6 0 18.96 1.23 -11 -6 0 19.19 1.40 11 6 0 20.30 1.25 11 6 0 18.86 1.19 -12 -6 0 14.31 1.34 12 6 0 14.87 1.17 -13 -6 0 3.53 0.87 13 6 0 4.22 0.76 13 6 0 5.10 0.81 -14 -6 0 4.22 0.96 14 6 0 2.90 0.79 14 6 0 4.08 0.81 13 -7 0 15.24 1.59 -13 7 0 15.24 1.54 -13 7 0 16.46 1.56 12 -7 0 3.55 0.93 -12 7 0 3.30 0.87 -12 7 0 2.52 0.90 11 -7 0 8.49 1.12 -11 7 0 6.81 1.03 -11 7 0 5.54 0.95 10 -7 0 2.97 0.79 -10 7 0 6.06 0.92 -10 7 0 5.62 0.89 9 -7 0 12.06 1.24 -9 7 0 12.74 1.23 -9 7 0 10.77 1.15 8 -7 0 1.12 0.57 -8 7 0 3.29 0.70 -8 7 0 1.36 0.59 7 -7 0 26.94 1.42 7 -7 0 26.59 1.46 7 -7 0 25.02 1.65 7 -7 0 24.25 1.59 -7 7 0 26.38 1.39 -7 7 0 24.93 1.44 6 -7 0 7.23 0.81 6 -7 0 6.48 0.70 6 -7 0 5.37 0.65 6 -7 0 6.73 0.73 -6 7 0 6.85 0.72 -6 7 0 7.61 0.88 5 -7 0 11.44 0.85 5 -7 0 9.26 0.93 5 -7 0 10.82 0.93 -5 7 0 10.42 0.84 -5 7 0 11.47 0.89 -5 7 0 11.14 0.93 4 -7 0 22.83 1.24 4 -7 0 24.43 1.16 4 -7 0 23.59 1.20 -4 7 0 25.64 1.17 -4 7 0 24.92 1.24 -4 7 0 24.69 1.17 3 -7 0 18.07 0.94 3 -7 0 18.71 1.04 3 -7 0 17.92 1.05 -3 7 0 19.92 1.06 -3 7 0 18.02 0.95 -3 7 0 17.71 0.99 2 -7 0 194.35 5.78 2 -7 0 195.34 5.79 2 -7 0 199.59 5.70 -2 7 0 198.63 5.77 -2 7 0 198.89 5.71 -2 7 0 200.76 5.81 1 -7 0 44.00 1.55 1 -7 0 41.16 1.42 1 -7 0 42.93 1.57 -1 7 0 42.94 1.54 -1 7 0 44.05 1.43 -1 7 0 42.34 1.56 0 -7 0 -0.15 0.22 0 -7 0 -0.08 0.37 0 -7 0 -0.41 0.21 0 -7 0 0.52 0.37 0 7 0 0.34 0.32 0 7 0 -0.20 0.34 -1 -7 0 42.48 1.25 -1 -7 0 37.37 1.44 -1 -7 0 43.23 1.50 -1 -7 0 42.93 1.25 1 7 0 41.16 1.47 1 7 0 44.52 1.46 -2 -7 0 198.63 5.70 -2 -7 0 193.30 5.61 2 7 0 199.98 5.69 2 7 0 196.90 5.62 -3 -7 0 17.40 0.92 -3 -7 0 19.03 0.81 3 7 0 17.97 0.92 3 7 0 19.63 0.84 -4 -7 0 24.43 0.94 -4 -7 0 24.60 1.10 -4 -7 0 23.57 0.79 4 7 0 24.66 0.98 4 7 0 23.49 1.09 4 7 0 23.74 0.81 -5 -7 0 9.98 0.77 -5 -7 0 11.94 0.54 5 7 0 9.62 0.53 5 7 0 12.35 0.82 5 7 0 9.56 0.61 5 7 0 9.94 0.68 -6 -7 0 7.13 0.75 -6 -7 0 6.95 0.52 6 7 0 7.10 0.58 6 7 0 7.81 0.64 6 7 0 8.25 0.77 6 7 0 7.40 0.53 -7 -7 0 24.86 1.06 -7 -7 0 25.77 1.29 7 7 0 24.97 1.26 7 7 0 26.70 1.08 7 7 0 27.16 1.14 7 7 0 25.93 1.10 -8 -7 0 2.68 0.46 -8 -7 0 2.02 0.54 8 7 0 1.87 0.43 8 7 0 0.97 0.50 8 7 0 1.35 0.40 8 7 0 2.14 0.48 -9 -7 0 11.61 0.87 -9 -7 0 10.45 1.04 9 7 0 11.10 0.90 9 7 0 11.50 0.83 9 7 0 10.69 0.85 -10 -7 0 4.33 0.77 -10 -7 0 5.42 0.68 10 7 0 4.82 0.63 10 7 0 4.16 0.60 10 7 0 5.43 0.71 -11 -7 0 6.52 0.75 -11 -7 0 6.92 0.95 11 7 0 8.07 0.86 11 7 0 8.47 0.85 11 7 0 5.92 0.73 -12 -7 0 2.11 0.75 12 7 0 1.36 0.60 12 7 0 4.06 0.72 12 7 0 3.68 0.64 -13 -7 0 16.62 1.46 13 7 0 15.55 1.25 13 7 0 13.53 1.22 13 -8 0 0.32 0.82 -13 8 0 0.44 0.81 12 -8 0 1.03 0.86 -12 8 0 0.31 0.77 -12 8 0 -0.24 0.71 11 -8 0 28.63 1.88 -11 8 0 30.52 1.89 -11 8 0 30.86 1.90 10 -8 0 0.60 0.71 -10 8 0 0.05 0.64 -10 8 0 -0.03 0.67 9 -8 0 2.73 0.76 -9 8 0 2.15 0.69 -9 8 0 2.88 0.77 8 -8 0 6.32 0.86 -8 8 0 7.03 0.94 -8 8 0 5.95 0.81 7 -8 0 0.49 0.56 -7 8 0 -0.24 0.55 -7 8 0 -0.49 0.47 6 -8 0 20.72 1.13 6 -8 0 18.96 1.24 6 -8 0 17.59 1.18 -6 8 0 15.90 1.12 -6 8 0 16.89 1.22 5 -8 0 68.03 2.51 5 -8 0 72.26 2.53 5 -8 0 69.87 2.45 -5 8 0 66.48 2.46 -5 8 0 73.75 2.57 -5 8 0 71.69 2.48 4 -8 0 1.83 0.50 4 -8 0 2.49 0.59 4 -8 0 1.94 0.46 -4 8 0 1.24 0.53 -4 8 0 2.38 0.52 -4 8 0 1.97 0.45 3 -8 0 3.54 0.58 3 -8 0 3.26 0.49 3 -8 0 3.90 0.62 -3 8 0 2.34 0.49 -3 8 0 3.10 0.47 -3 8 0 2.64 0.55 2 -8 0 35.87 1.32 2 -8 0 35.28 1.47 2 -8 0 34.91 1.45 -2 8 0 35.91 1.33 -2 8 0 34.43 1.45 -2 8 0 33.04 1.39 1 -8 0 -0.13 0.39 1 -8 0 0.28 0.30 1 -8 0 0.83 0.45 -1 8 0 -0.09 0.36 -1 8 0 0.49 0.42 0 -8 0 319.71 8.83 0 -8 0 320.02 8.83 0 -8 0 317.47 9.00 0 -8 0 315.57 8.97 0 8 0 312.48 8.97 0 8 0 315.29 8.99 -1 -8 0 0.03 0.39 -1 -8 0 -0.03 0.18 -1 -8 0 0.27 0.19 -1 -8 0 -0.11 0.38 1 8 0 0.28 0.37 1 8 0 0.17 0.35 -2 -8 0 31.97 1.27 -2 -8 0 34.49 1.35 2 8 0 35.53 1.29 2 8 0 35.24 1.34 -3 -8 0 3.12 0.49 -3 -8 0 2.32 0.38 3 8 0 3.61 0.45 3 8 0 3.01 0.48 -4 -8 0 1.80 0.44 -4 -8 0 1.83 0.35 4 8 0 2.30 0.41 4 8 0 2.25 0.25 4 8 0 2.43 0.46 -5 -8 0 68.61 2.05 -5 -8 0 71.79 2.37 -5 -8 0 69.76 2.18 5 8 0 69.17 2.21 5 8 0 68.46 2.06 5 8 0 69.78 2.36 -6 -8 0 20.98 1.11 -6 -8 0 20.44 0.83 6 8 0 21.52 0.84 6 8 0 21.83 0.98 6 8 0 20.96 1.12 6 8 0 20.75 0.92 -7 -8 0 -0.03 0.28 -7 -8 0 -0.20 0.42 7 8 0 -0.15 0.36 7 8 0 0.03 0.31 7 8 0 -0.17 0.39 7 8 0 0.27 0.30 -8 -8 0 6.84 0.65 -8 -8 0 6.35 0.78 8 8 0 8.30 0.71 8 8 0 7.47 0.87 8 8 0 7.26 0.66 8 8 0 7.06 0.76 -9 -8 0 0.97 0.58 9 8 0 1.64 0.44 9 8 0 2.89 0.54 -10 -8 0 0.21 0.56 -10 -8 0 0.07 0.42 10 8 0 0.52 0.50 10 8 0 0.63 0.42 10 8 0 -0.02 0.41 -11 -8 0 30.10 1.69 11 8 0 25.32 1.37 11 8 0 29.69 1.39 11 8 0 26.87 1.35 11 8 0 30.80 1.46 -12 -8 0 0.13 0.63 12 8 0 0.82 0.50 12 8 0 0.23 0.55 12 8 0 0.79 0.54 -13 -8 0 0.86 0.71 13 8 0 -0.25 0.56 13 8 0 -0.26 0.54 13 -9 0 15.25 1.65 13 -9 0 15.43 1.70 -13 9 0 13.43 1.59 12 -9 0 8.86 1.21 -12 9 0 9.05 1.21 -12 9 0 10.44 1.22 11 -9 0 0.19 0.76 -11 9 0 -0.46 0.70 -11 9 0 -0.29 0.65 10 -9 0 11.43 1.34 -10 9 0 11.22 1.24 -10 9 0 9.96 1.16 9 -9 0 4.58 0.93 -9 9 0 5.51 0.88 8 -9 0 7.46 0.91 -8 9 0 9.99 1.05 -8 9 0 8.90 1.02 7 -9 0 1.09 0.60 -7 9 0 1.56 0.59 -7 9 0 1.47 0.66 6 -9 0 13.85 1.11 6 -9 0 12.36 1.30 -6 9 0 15.03 1.09 -6 9 0 14.69 1.16 5 -9 0 19.95 1.17 5 -9 0 24.79 1.31 5 -9 0 23.20 1.30 -5 9 0 24.90 1.33 -5 9 0 23.74 1.24 -5 9 0 22.63 1.23 4 -9 0 -0.10 0.43 4 -9 0 0.31 0.49 4 -9 0 0.91 0.43 -4 9 0 0.79 0.44 -4 9 0 -0.01 0.49 -4 9 0 0.22 0.44 3 -9 0 57.65 2.10 3 -9 0 56.19 2.00 3 -9 0 58.44 2.14 -3 9 0 57.61 2.13 -3 9 0 56.82 2.08 -3 9 0 58.81 2.01 2 -9 0 44.25 1.70 2 -9 0 41.76 1.54 2 -9 0 42.68 1.71 -2 9 0 42.19 1.55 -2 9 0 43.17 1.70 -2 9 0 43.19 1.66 1 -9 0 12.66 0.89 1 -9 0 12.84 0.95 1 -9 0 13.63 0.72 1 -9 0 12.52 0.71 -1 9 0 13.18 0.85 -1 9 0 13.43 0.90 0 -9 0 -0.29 0.42 0 -9 0 0.08 0.25 0 -9 0 0.41 0.41 0 -9 0 -0.15 0.25 0 9 0 0.31 0.41 0 9 0 0.43 0.39 -1 -9 0 12.26 0.86 -1 -9 0 12.49 0.52 -1 -9 0 12.74 0.53 -1 -9 0 11.11 0.84 1 9 0 11.52 0.81 1 9 0 12.50 0.82 -2 -9 0 42.05 1.53 -2 -9 0 42.94 1.60 2 9 0 42.00 1.58 2 9 0 42.50 1.53 -3 -9 0 55.75 1.85 -3 -9 0 55.47 1.97 3 9 0 58.17 1.97 3 9 0 55.84 1.87 -4 -9 0 0.43 0.29 -4 -9 0 0.14 0.38 4 9 0 0.31 0.36 4 9 0 0.18 0.38 -5 -9 0 22.60 0.94 -5 -9 0 23.64 1.15 5 9 0 22.00 1.12 5 9 0 21.51 0.98 5 9 0 22.63 0.76 -6 -9 0 13.43 0.94 6 9 0 12.88 0.61 6 9 0 12.45 0.80 6 9 0 13.24 0.73 6 9 0 13.47 0.93 -7 -9 0 1.97 0.54 -7 -9 0 1.18 0.31 7 9 0 1.21 0.50 7 9 0 1.06 0.36 7 9 0 1.43 0.33 7 9 0 1.17 0.44 -8 -9 0 9.59 0.96 8 9 0 10.01 0.82 8 9 0 7.73 0.71 8 9 0 8.70 0.67 8 9 0 7.43 0.81 -9 -9 0 5.29 0.76 9 9 0 5.67 0.60 9 9 0 5.97 0.60 9 9 0 5.40 0.65 -10 -9 0 10.04 1.11 10 9 0 9.26 0.83 10 9 0 10.24 0.84 10 9 0 9.43 0.82 10 9 0 11.77 0.94 -11 -9 0 0.34 0.61 11 9 0 0.84 0.44 11 9 0 0.77 0.53 11 9 0 1.17 0.50 11 9 0 1.18 0.46 -12 -9 0 8.57 1.06 12 9 0 10.39 0.92 12 9 0 9.20 1.00 12 9 0 9.80 0.96 -13 -9 0 12.94 1.35 13 9 0 12.82 1.14 13 9 0 13.36 1.11 13 -10 0 2.43 1.07 13 -10 0 1.33 0.94 -13 10 0 0.08 0.85 12 -10 0 3.81 1.00 -12 10 0 1.88 0.94 11 -10 0 9.33 1.27 -11 10 0 9.97 1.15 -11 10 0 10.58 1.29 10 -10 0 15.60 1.47 -10 10 0 15.33 1.45 -10 10 0 16.29 1.52 9 -10 0 0.93 0.70 -9 10 0 0.25 0.67 -9 10 0 1.52 0.76 8 -10 0 48.08 2.22 -8 10 0 48.97 2.25 -8 10 0 46.76 2.17 7 -10 0 62.26 2.54 -7 10 0 65.44 2.51 -7 10 0 61.50 2.57 6 -10 0 0.08 0.51 -6 10 0 -0.20 0.45 -6 10 0 -0.46 0.51 5 -10 0 0.47 0.52 5 -10 0 0.53 0.45 5 -10 0 0.06 0.47 -5 10 0 0.94 0.48 -5 10 0 0.57 0.45 -5 10 0 0.73 0.57 4 -10 0 10.49 0.94 4 -10 0 9.13 0.79 4 -10 0 9.86 0.92 -4 10 0 9.34 0.82 -4 10 0 10.16 0.87 -4 10 0 9.05 0.94 3 -10 0 137.81 4.35 3 -10 0 147.15 4.50 3 -10 0 141.99 4.50 -3 10 0 144.25 4.38 -3 10 0 145.78 4.47 -3 10 0 146.29 4.52 2 -10 0 47.42 1.84 2 -10 0 46.82 1.67 2 -10 0 48.18 1.85 -2 10 0 48.39 1.81 -2 10 0 46.23 1.86 1 -10 0 5.46 0.65 1 -10 0 5.93 0.64 1 -10 0 5.96 0.56 1 -10 0 6.03 0.56 -1 10 0 5.53 0.62 -1 10 0 6.38 0.63 0 -10 0 66.69 2.28 0 -10 0 67.70 2.29 0 -10 0 68.11 2.06 0 -10 0 65.87 2.05 0 10 0 66.59 2.28 0 10 0 64.95 2.25 -1 -10 0 5.68 0.40 -1 -10 0 7.12 0.75 -1 -10 0 7.74 0.78 -1 -10 0 6.38 0.40 1 10 0 5.95 0.69 1 10 0 6.63 0.62 -2 -10 0 48.27 1.76 -2 -10 0 46.01 1.67 2 10 0 46.54 1.67 2 10 0 46.55 1.72 -3 -10 0 138.61 4.17 -3 -10 0 143.41 4.30 3 10 0 140.92 4.18 3 10 0 140.02 4.27 -4 -10 0 10.58 0.84 -4 -10 0 9.84 0.66 4 10 0 9.81 0.72 4 10 0 9.98 0.80 -5 -10 0 0.27 0.30 -5 -10 0 0.13 0.40 5 10 0 0.35 0.39 5 10 0 0.85 0.43 -6 -10 0 0.23 0.44 6 10 0 0.05 0.39 6 10 0 0.51 0.44 6 10 0 0.63 0.19 6 10 0 0.17 0.22 -7 -10 0 62.69 2.31 7 10 0 61.52 2.08 7 10 0 62.54 1.89 7 10 0 58.77 2.26 7 10 0 59.39 1.89 7 10 0 60.41 2.03 -8 -10 0 46.44 1.94 8 10 0 47.30 1.55 8 10 0 43.62 1.94 8 10 0 44.50 1.65 8 10 0 44.53 1.70 8 10 0 44.47 1.56 -9 -10 0 1.07 0.60 9 10 0 1.81 0.42 9 10 0 0.33 0.40 9 10 0 1.06 0.50 9 10 0 1.09 0.39 -10 -10 0 14.14 1.24 10 10 0 14.86 1.04 10 10 0 14.27 0.91 10 10 0 14.97 0.91 10 10 0 15.74 0.91 -11 -10 0 9.94 1.15 11 10 0 13.48 0.89 11 10 0 11.96 0.99 11 10 0 11.29 0.89 11 10 0 9.96 0.88 -12 -10 0 2.92 0.80 12 10 0 3.67 0.58 12 10 0 3.90 0.60 12 10 0 3.14 0.65 12 10 0 3.10 0.60 -13 -10 0 1.63 0.73 13 10 0 1.85 0.60 13 10 0 2.05 0.62 12 -11 0 16.86 1.63 12 -11 0 15.99 1.73 -12 11 0 15.69 1.70 11 -11 0 1.73 0.86 -11 11 0 0.41 0.75 -11 11 0 0.94 0.72 10 -11 0 39.16 2.20 -10 11 0 39.07 2.11 -10 11 0 39.81 2.20 9 -11 0 0.96 0.75 -9 11 0 1.69 0.84 -9 11 0 1.31 0.70 8 -11 0 0.12 0.68 -8 11 0 0.30 0.69 -8 11 0 0.83 0.70 7 -11 0 9.87 1.11 -7 11 0 10.24 1.12 -7 11 0 9.92 1.06 6 -11 0 46.87 2.10 -6 11 0 44.71 2.11 -6 11 0 51.19 2.06 5 -11 0 49.90 2.09 5 -11 0 49.47 1.96 -5 11 0 44.34 1.95 -5 11 0 52.65 2.14 4 -11 0 10.41 0.83 4 -11 0 9.60 0.99 4 -11 0 10.17 1.01 -4 11 0 9.87 0.87 -4 11 0 8.13 0.88 -4 11 0 9.35 0.89 3 -11 0 6.57 0.69 3 -11 0 7.67 0.89 3 -11 0 6.47 0.73 -3 11 0 6.82 0.80 -3 11 0 6.41 0.73 -3 11 0 7.68 0.81 2 -11 0 4.01 0.48 2 -11 0 4.03 0.48 2 -11 0 3.31 0.60 2 -11 0 4.23 0.63 -2 11 0 2.77 0.58 -2 11 0 3.47 0.55 1 -11 0 103.70 3.30 1 -11 0 97.53 3.08 1 -11 0 104.56 3.30 1 -11 0 99.67 3.08 -1 11 0 100.31 3.27 -1 11 0 102.00 3.29 0 -11 0 -0.27 0.24 0 -11 0 -0.53 0.42 0 -11 0 0.48 0.43 0 -11 0 0.24 0.27 0 11 0 -0.56 0.35 0 11 0 0.15 0.43 -1 -11 0 88.76 2.85 -1 -11 0 101.02 3.14 -1 -11 0 99.63 2.87 -1 -11 0 101.59 3.20 1 11 0 101.67 3.17 1 11 0 100.71 3.14 -2 -11 0 2.94 0.53 -2 -11 0 2.94 0.49 2 11 0 3.64 0.51 2 11 0 2.83 0.51 -3 -11 0 7.56 0.80 -3 -11 0 7.15 0.69 3 11 0 6.58 0.71 3 11 0 8.18 0.76 -4 -11 0 10.88 0.88 -4 -11 0 9.67 0.70 4 11 0 9.90 0.76 4 11 0 9.86 0.82 -5 -11 0 48.55 1.72 -5 -11 0 50.43 1.94 5 11 0 51.52 1.78 5 11 0 50.60 1.93 -6 -11 0 48.61 1.92 -6 -11 0 45.65 1.63 6 11 0 45.65 1.87 6 11 0 47.61 1.70 -7 -11 0 8.55 0.92 7 11 0 7.38 0.44 7 11 0 9.49 0.80 7 11 0 8.68 0.69 7 11 0 11.35 0.97 7 11 0 8.70 0.50 -8 -11 0 0.14 0.52 8 11 0 -0.18 0.25 8 11 0 -0.49 0.29 8 11 0 -0.41 0.43 8 11 0 -0.11 0.35 -9 -11 0 1.07 0.61 9 11 0 1.13 0.50 9 11 0 1.11 0.37 9 11 0 1.95 0.37 9 11 0 1.28 0.43 -10 -11 0 36.35 1.86 10 11 0 39.01 1.52 10 11 0 38.35 1.59 10 11 0 37.92 1.44 10 11 0 36.16 1.44 -11 -11 0 1.03 0.64 11 11 0 0.93 0.43 11 11 0 0.59 0.53 11 11 0 0.12 0.39 11 11 0 0.60 0.40 -12 -11 0 16.15 1.42 12 11 0 15.13 0.97 12 11 0 13.82 1.00 12 11 0 15.07 1.11 12 11 0 16.85 1.03 12 -12 0 7.89 1.23 12 -12 0 7.61 1.24 -12 12 0 8.09 1.27 11 -12 0 0.15 0.76 11 -12 0 0.43 0.75 -11 12 0 0.24 0.84 10 -12 0 26.53 1.83 -10 12 0 24.68 1.83 -10 12 0 25.58 1.75 9 -12 0 2.71 0.88 -9 12 0 2.32 0.87 -9 12 0 2.56 0.82 8 -12 0 59.42 2.58 -8 12 0 55.52 2.46 -8 12 0 57.87 2.60 7 -12 0 37.89 1.99 -7 12 0 37.50 2.00 -7 12 0 38.43 1.88 6 -12 0 0.06 0.60 -6 12 0 -0.59 0.52 -6 12 0 -0.26 0.61 5 -12 0 9.68 0.93 5 -12 0 9.63 1.11 -5 12 0 8.64 0.92 -5 12 0 9.40 1.04 4 -12 0 20.08 1.12 4 -12 0 20.05 1.28 -4 12 0 18.95 1.29 -4 12 0 15.74 1.48 -4 12 0 20.11 1.15 3 -12 0 62.69 2.38 3 -12 0 65.50 2.21 3 -12 0 61.56 2.34 3 -12 0 61.77 2.18 -3 12 0 60.82 2.30 -3 12 0 57.01 2.34 2 -12 0 0.60 0.53 2 -12 0 1.47 0.40 2 -12 0 1.62 0.40 2 -12 0 1.18 0.52 -2 12 0 1.07 0.47 -2 12 0 0.92 0.52 1 -12 0 31.52 1.44 1 -12 0 29.02 1.19 1 -12 0 30.48 1.45 1 -12 0 30.23 1.19 -1 12 0 29.61 1.42 -1 12 0 29.45 1.38 0 -12 0 16.59 1.08 0 -12 0 19.09 1.11 0 -12 0 18.58 0.81 0 -12 0 18.39 0.81 0 12 0 17.66 1.08 0 12 0 17.82 1.04 -1 -12 0 29.30 1.02 -1 -12 0 28.14 1.34 -1 -12 0 31.16 1.02 -1 -12 0 31.76 1.41 1 12 0 28.49 1.34 1 12 0 28.60 1.33 -2 -12 0 1.39 0.47 -2 -12 0 1.08 0.48 2 12 0 0.93 0.45 2 12 0 0.83 0.45 -3 -12 0 63.30 2.26 -3 -12 0 63.03 2.13 3 12 0 61.65 2.13 3 12 0 58.87 2.19 -4 -12 0 19.79 1.17 -4 -12 0 19.76 0.99 4 12 0 21.21 1.15 4 12 0 18.89 1.02 -5 -12 0 8.07 0.67 -5 -12 0 7.51 0.88 5 12 0 8.53 0.77 5 12 0 7.59 0.77 -6 -12 0 0.83 0.51 -6 -12 0 0.15 0.32 6 12 0 -0.66 0.41 6 12 0 -0.03 0.47 -7 -12 0 36.17 1.68 7 12 0 35.16 1.68 7 12 0 35.26 1.39 7 12 0 38.94 1.50 -8 -12 0 60.14 2.31 8 12 0 56.05 1.95 8 12 0 59.35 2.02 8 12 0 50.74 1.67 8 12 0 56.71 1.70 -9 -12 0 1.88 0.66 9 12 0 2.13 0.37 9 12 0 2.04 0.55 9 12 0 2.84 0.48 9 12 0 2.86 0.35 -10 -12 0 27.51 1.59 10 12 0 24.80 1.08 10 12 0 25.68 1.05 10 12 0 26.36 1.27 10 12 0 24.64 1.19 -11 -12 0 0.95 0.65 11 12 0 1.25 0.42 11 12 0 2.06 0.47 11 12 0 0.97 0.52 11 12 0 1.63 0.42 -12 -12 0 8.87 1.10 12 12 0 8.43 0.77 12 12 0 8.28 0.92 12 -13 0 15.22 1.75 12 -13 0 16.95 1.70 -12 13 0 17.57 1.83 11 -13 0 3.24 1.02 11 -13 0 2.71 0.96 -11 13 0 3.21 1.02 10 -13 0 28.77 1.94 10 -13 0 26.57 1.83 -10 13 0 32.32 2.01 9 -13 0 7.36 1.15 -9 13 0 6.71 1.10 8 -13 0 5.19 0.93 -8 13 0 5.29 1.01 -8 13 0 4.76 0.87 7 -13 0 10.93 1.26 -7 13 0 12.01 1.32 -7 13 0 12.04 1.20 -6 13 0 32.32 1.70 -6 13 0 33.31 1.88 5 -13 0 47.74 2.14 5 -13 0 47.17 1.99 -5 13 0 48.15 2.17 4 -13 0 2.77 0.58 4 -13 0 3.41 0.70 4 -13 0 3.11 0.60 -4 13 0 2.25 0.70 3 -13 0 5.48 0.81 3 -13 0 6.31 0.84 3 -13 0 4.76 0.62 3 -13 0 6.48 0.67 -3 13 0 6.69 0.95 -3 13 0 5.69 0.82 2 -13 0 0.23 0.50 2 -13 0 0.88 0.59 2 -13 0 -0.04 0.33 2 -13 0 0.06 0.37 -2 13 0 0.18 0.51 -2 13 0 -0.02 0.43 1 -13 0 63.80 2.13 1 -13 0 65.58 2.41 1 -13 0 64.87 2.13 1 -13 0 62.02 2.37 -1 13 0 65.73 2.40 -1 13 0 62.15 2.33 0 -13 0 -0.32 0.49 0 -13 0 0.34 0.29 0 -13 0 -0.21 0.27 0 -13 0 0.35 0.50 0 13 0 0.17 0.41 0 13 0 1.06 0.51 -1 -13 0 62.60 1.96 -1 -13 0 63.67 2.30 -1 -13 0 65.15 1.96 -1 -13 0 64.53 2.35 1 13 0 64.37 2.31 1 13 0 64.23 2.31 -2 -13 0 -0.25 0.44 -2 -13 0 0.26 0.46 2 13 0 -0.70 0.41 2 13 0 0.50 0.44 -3 -13 0 7.04 0.78 -3 -13 0 6.36 0.67 3 13 0 5.21 0.68 3 13 0 5.95 0.66 -4 -13 0 2.96 0.63 -4 -13 0 3.22 0.50 4 13 0 2.37 0.53 4 13 0 2.91 0.59 -5 -13 0 42.50 1.62 -5 -13 0 46.32 1.89 5 13 0 44.35 1.69 5 13 0 45.51 1.84 -6 -13 0 27.08 1.49 -6 -13 0 32.07 1.26 6 13 0 30.76 1.34 6 13 0 31.57 1.54 -7 -13 0 11.26 1.07 7 13 0 10.77 0.88 7 13 0 10.03 0.74 -8 -13 0 5.45 0.82 8 13 0 6.23 0.66 8 13 0 5.95 0.67 -9 -13 0 6.14 0.87 9 13 0 6.15 0.60 9 13 0 6.56 0.69 -10 -13 0 27.27 1.62 10 13 0 26.44 1.28 10 13 0 26.70 1.21 10 13 0 27.75 0.99 10 13 0 28.10 1.01 11 13 0 4.05 0.55 11 13 0 3.75 0.45 11 13 0 2.86 0.60 -12 -13 0 15.31 1.41 12 13 0 17.95 1.11 12 13 0 17.89 0.91 11 -14 0 -0.45 0.78 11 -14 0 -0.49 0.72 -11 14 0 0.00 0.84 10 -14 0 13.66 1.56 10 -14 0 10.71 1.28 -10 14 0 11.94 1.37 9 -14 0 0.27 0.66 9 -14 0 0.42 0.78 -9 14 0 -0.60 0.67 8 -14 0 18.77 1.46 8 -14 0 16.14 1.54 -8 14 0 18.69 1.63 7 -14 0 1.23 0.77 7 -14 0 2.14 0.72 -7 14 0 3.27 0.85 6 -14 0 2.14 0.83 6 -14 0 1.71 0.64 -6 14 0 1.83 0.74 5 -14 0 24.29 1.56 5 -14 0 23.12 1.37 -5 14 0 21.76 1.57 4 -14 0 28.55 1.59 4 -14 0 22.21 1.31 4 -14 0 24.53 1.33 -4 14 0 27.62 1.59 3 -14 0 19.09 1.33 3 -14 0 17.22 1.07 3 -14 0 18.89 1.10 -3 14 0 19.09 1.34 2 -14 0 5.87 0.83 2 -14 0 5.39 0.60 2 -14 0 5.50 0.63 2 -14 0 5.34 0.77 -2 14 0 4.91 0.76 -2 14 0 6.51 1.07 1 -14 0 15.49 1.18 1 -14 0 14.50 0.85 1 -14 0 11.87 1.13 1 -14 0 14.77 0.85 -1 14 0 15.56 1.17 -1 14 0 15.23 1.07 0 -14 0 33.22 1.58 0 -14 0 28.28 1.52 0 -14 0 31.58 1.21 0 -14 0 31.72 1.20 0 14 0 33.40 1.51 0 14 0 30.49 1.52 -1 -14 0 14.51 0.66 -1 -14 0 14.34 1.12 -1 -14 0 15.30 0.68 -1 -14 0 14.25 1.10 1 14 0 13.72 1.09 1 14 0 13.66 1.01 -2 -14 0 5.02 0.73 -2 -14 0 5.34 0.69 2 14 0 5.41 0.69 2 14 0 5.63 0.67 -3 -14 0 18.43 1.10 -3 -14 0 21.39 1.26 3 14 0 18.69 1.13 3 14 0 18.26 1.15 -4 -14 0 25.42 1.23 -4 -14 0 26.88 1.44 4 14 0 27.77 1.30 4 14 0 26.51 1.38 -5 -14 0 20.14 1.31 -5 -14 0 21.12 1.08 5 14 0 23.68 1.32 5 14 0 23.77 1.19 -6 -14 0 2.88 0.65 -6 -14 0 2.45 0.45 6 14 0 2.91 0.57 -7 -14 0 1.75 0.63 7 14 0 1.61 0.54 -8 -14 0 19.07 1.33 8 14 0 16.65 0.93 8 14 0 19.45 1.09 -9 -14 0 0.52 0.60 9 14 0 -0.12 0.47 9 14 0 0.99 0.39 -10 -14 0 10.75 1.13 10 14 0 11.34 0.80 10 14 0 11.28 0.92 -11 -14 0 0.25 0.64 11 14 0 -0.31 0.46 11 -15 0 2.89 0.98 11 -15 0 1.98 0.98 -11 15 0 2.39 0.93 10 -15 0 0.73 0.85 10 -15 0 1.86 0.84 -10 15 0 2.01 0.98 9 -15 0 14.37 1.55 9 -15 0 13.07 1.44 -9 15 0 12.17 1.39 8 -15 0 6.52 1.04 8 -15 0 5.58 1.04 -8 15 0 5.34 1.01 7 -15 0 2.95 0.88 7 -15 0 1.98 0.76 -7 15 0 2.67 0.87 6 -15 0 19.17 1.52 6 -15 0 19.33 1.37 -6 15 0 20.79 1.57 5 -15 0 10.95 1.26 5 -15 0 9.74 1.05 -5 15 0 9.13 1.14 4 -15 0 0.37 0.62 4 -15 0 0.05 0.49 4 -15 0 0.30 0.49 -4 15 0 0.39 0.65 3 -15 0 2.40 0.56 3 -15 0 1.74 0.52 3 -15 0 0.80 0.66 -3 15 0 2.26 0.69 2 -15 0 1.94 0.48 2 -15 0 2.25 0.51 2 -15 0 1.36 0.69 -2 15 0 1.68 0.70 1 -15 0 15.54 0.91 1 -15 0 15.34 1.24 1 -15 0 15.65 1.24 1 -15 0 15.82 0.90 -1 15 0 16.08 1.25 0 -15 0 0.07 0.31 0 -15 0 0.08 0.54 0 -15 0 -0.59 0.54 0 -15 0 0.16 0.32 0 15 0 0.34 0.48 0 15 0 -0.35 0.54 -1 -15 0 15.65 0.72 -1 -15 0 15.25 0.70 -1 -15 0 13.97 1.18 -1 -15 0 15.75 1.22 1 15 0 14.14 1.08 1 15 0 16.47 1.18 -2 -15 0 0.10 0.57 -2 -15 0 1.85 0.61 2 15 0 2.80 0.63 2 15 0 1.40 0.57 -3 -15 0 1.83 0.64 -3 -15 0 2.74 0.60 3 15 0 2.32 0.59 3 15 0 1.24 0.55 -4 -15 0 -0.04 0.55 -4 -15 0 0.12 0.45 4 15 0 0.02 0.49 4 15 0 0.20 0.49 -5 -15 0 10.16 0.83 -5 -15 0 9.89 1.07 5 15 0 10.07 0.94 -6 -15 0 20.90 1.34 -6 -15 0 20.59 1.02 6 15 0 18.12 1.11 -7 -15 0 2.51 0.46 -7 -15 0 4.76 0.79 7 15 0 3.13 0.59 -8 -15 0 5.04 0.82 8 15 0 5.53 0.56 8 15 0 5.67 0.66 -9 -15 0 10.82 1.17 9 15 0 11.25 0.91 9 15 0 11.37 0.79 -10 -15 0 2.03 0.74 10 15 0 1.98 0.44 10 15 0 2.29 0.54 -11 -15 0 0.84 0.67 11 15 0 1.85 0.54 10 -16 0 1.56 0.83 10 -16 0 0.84 0.89 -10 16 0 -0.53 0.82 9 -16 0 8.99 1.27 9 -16 0 8.49 1.12 -9 16 0 9.63 1.34 8 -16 0 2.93 0.92 8 -16 0 2.06 0.79 -8 16 0 4.04 0.99 7 -16 0 2.22 0.84 7 -16 0 0.68 0.63 -7 16 0 1.65 0.85 6 -16 0 0.86 0.64 6 -16 0 0.05 0.74 -6 16 0 0.10 0.72 5 -16 0 4.25 0.93 5 -16 0 5.37 0.81 -5 16 0 6.32 0.97 4 -16 0 9.14 1.05 4 -16 0 8.81 0.99 -4 16 0 8.64 1.10 3 -16 0 -0.58 0.62 3 -16 0 0.07 0.46 3 -16 0 0.15 0.49 -3 16 0 -0.18 0.66 2 -16 0 6.93 0.81 2 -16 0 8.51 1.05 2 -16 0 7.39 0.79 -2 16 0 7.93 1.00 1 -16 0 8.83 0.96 1 -16 0 8.35 0.73 1 -16 0 9.34 0.78 -1 16 0 8.85 0.98 0 -16 0 0.13 0.62 0 -16 0 0.99 0.68 0 -16 0 0.20 0.36 0 -16 0 0.89 0.35 0 16 0 0.06 0.58 -1 -16 0 7.78 0.57 -1 -16 0 9.73 1.01 -1 -16 0 8.88 0.56 -1 -16 0 9.21 0.93 1 16 0 9.90 0.95 -2 -16 0 10.02 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5.26 0.51 7 6 -9 17.56 0.79 7 6 -9 17.26 1.23 7 6 -9 16.70 0.78 7 6 -9 19.35 0.98 7 6 -9 17.32 0.93 6 6 -9 48.41 1.95 6 6 -9 45.07 1.41 6 6 -9 45.13 1.64 6 6 -9 41.23 1.39 -6 -6 9 44.25 1.84 -6 -6 9 45.94 1.61 5 6 -9 7.29 0.81 5 6 -9 8.37 0.67 -5 -6 9 5.45 0.65 -5 -6 9 7.71 0.61 4 6 -9 26.59 1.36 4 6 -9 24.53 1.08 -4 -6 9 24.84 1.26 -4 -6 9 24.29 1.03 3 6 -9 50.28 2.00 3 6 -9 50.52 1.75 -3 -6 9 50.81 1.93 -3 -6 9 50.87 1.72 2 6 -9 36.84 1.39 2 6 -9 37.05 1.61 -2 -6 9 35.46 1.36 -2 -6 9 35.81 1.56 1 6 -9 2.74 0.60 1 6 -9 3.14 0.49 -1 -6 9 4.42 0.54 -1 -6 9 3.02 0.33 -1 -6 9 3.18 0.33 -1 -6 9 3.02 0.60 0 6 -9 98.65 3.03 0 6 -9 99.15 3.20 0 -6 9 96.25 2.84 0 -6 9 93.38 2.84 0 -6 9 93.00 3.13 0 -6 9 94.06 3.02 -1 6 -9 101.42 3.33 -1 6 -9 100.38 3.20 1 -6 9 103.10 3.08 1 -6 9 99.87 3.20 1 -6 9 101.76 3.07 1 -6 9 99.84 3.30 -2 6 -9 55.90 2.05 -2 6 -9 56.68 2.16 2 -6 9 56.77 2.14 2 -6 9 57.31 1.95 2 -6 9 56.94 2.07 2 -6 9 56.79 1.95 -3 6 -9 8.85 0.84 -3 6 -9 9.35 0.95 3 -6 9 13.35 0.92 3 -6 9 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6.39 0.64 9 5 -9 6.79 0.78 9 5 -9 6.54 0.72 9 5 -9 7.09 0.74 9 5 -9 8.46 0.96 8 5 -9 30.94 1.24 8 5 -9 31.92 1.26 8 5 -9 33.46 1.68 8 5 -9 30.83 1.39 8 5 -9 31.06 1.38 7 5 -9 60.83 1.94 7 5 -9 62.00 2.13 7 5 -9 61.23 2.29 7 5 -9 59.62 2.36 7 5 -9 60.63 1.95 7 5 -9 59.75 2.10 6 5 -9 12.62 1.04 6 5 -9 12.49 0.58 6 5 -9 13.05 0.81 6 5 -9 11.31 0.58 -6 -5 9 13.25 0.95 -6 -5 9 12.42 0.77 5 5 -9 38.02 1.17 5 5 -9 38.16 1.68 5 5 -9 39.18 1.17 5 5 -9 39.73 1.46 -5 -5 9 38.31 1.43 -5 -5 9 37.35 1.62 4 5 -9 0.80 0.38 4 5 -9 0.86 0.54 -4 -5 9 0.39 0.32 -4 -5 9 0.77 0.47 3 5 -9 23.33 1.28 3 5 -9 23.16 1.07 -3 -5 9 23.95 1.20 -3 -5 9 22.70 1.02 2 5 -9 33.46 1.32 -2 -5 9 32.09 1.44 -2 -5 9 33.86 1.30 1 5 -9 124.80 3.77 1 5 -9 123.45 3.91 -1 -5 9 123.60 3.52 -1 -5 9 124.62 3.77 -1 -5 9 124.39 3.88 -1 -5 9 125.08 3.53 0 5 -9 47.31 1.73 0 5 -9 48.38 1.87 0 -5 9 47.04 1.73 0 -5 9 46.94 1.83 0 -5 9 48.49 1.54 -1 5 -9 122.79 3.79 -1 5 -9 117.22 3.69 -1 5 -9 120.18 3.56 1 -5 9 117.46 3.76 1 -5 9 118.85 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18.95 0.68 4 3 -9 20.33 1.16 4 3 -9 18.96 0.68 -4 -3 9 18.44 1.07 -4 -3 9 19.66 0.95 3 3 -9 15.59 1.03 3 3 -9 15.19 0.90 -3 -3 9 14.88 0.85 -3 -3 9 15.36 0.98 2 3 -9 60.82 1.78 2 3 -9 61.48 2.09 2 3 -9 62.53 2.19 -2 -3 9 61.67 2.16 -2 -3 9 60.37 2.06 -2 -3 9 63.66 1.79 1 3 -9 21.10 1.15 1 3 -9 22.21 0.79 1 3 -9 23.58 1.09 -1 -3 9 21.96 1.12 -1 -3 9 21.44 0.80 -1 -3 9 23.47 1.07 0 3 -9 113.56 3.51 0 3 -9 114.00 3.33 0 3 -9 114.73 3.56 0 -3 9 113.37 3.53 0 -3 9 113.94 3.33 0 -3 9 113.64 3.50 -1 3 -9 166.02 4.91 -1 3 -9 166.28 4.78 -1 3 -9 164.73 4.93 1 -3 9 166.91 4.78 1 -3 9 161.56 4.90 1 -3 9 160.32 4.90 -2 3 -9 0.02 0.43 -2 3 -9 0.33 0.34 -2 3 -9 0.00 0.48 2 -3 9 -0.18 0.47 2 -3 9 0.22 0.35 2 -3 9 0.89 0.51 -3 3 -9 35.26 1.52 -3 3 -9 36.30 1.53 -3 3 -9 36.82 1.46 3 -3 9 35.10 1.50 3 -3 9 37.65 1.46 3 -3 9 35.32 1.54 -4 3 -9 55.32 2.04 -4 3 -9 52.09 1.98 -4 3 -9 54.38 1.98 4 -3 9 51.08 1.95 4 -3 9 52.17 1.97 4 -3 9 53.07 2.02 -5 3 -9 14.23 1.00 -5 3 -9 12.84 0.97 -5 3 -9 13.64 1.02 5 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1 4 -27 3.00 0.61 1 4 -27 1.47 0.97 0 4 -27 0.50 0.91 0 4 -27 1.97 1.06 -1 4 -27 4.10 1.12 -1 4 -27 2.76 0.68 -1 4 -27 4.26 1.16 5 3 -27 2.44 1.06 5 3 -27 5.14 0.55 5 3 -27 6.42 1.32 4 3 -27 5.48 1.18 4 3 -27 1.35 1.10 4 3 -27 1.94 0.45 3 3 -27 1.09 0.47 3 3 -27 0.72 0.87 3 3 -27 0.06 0.95 2 3 -27 25.04 2.05 2 3 -27 27.45 2.08 2 3 -27 23.71 1.30 -2 -3 27 29.21 1.69 1 3 -27 3.30 1.12 1 3 -27 4.87 0.72 1 3 -27 4.27 1.07 0 3 -27 16.62 1.75 0 3 -27 13.80 1.51 0 3 -27 16.31 1.21 -1 3 -27 1.69 0.98 -1 3 -27 3.16 0.74 -1 3 -27 0.75 0.94 5 2 -27 6.56 1.24 5 2 -27 5.66 1.22 5 2 -27 5.63 0.59 4 2 -27 21.02 1.98 4 2 -27 23.68 1.94 4 2 -27 21.64 1.14 3 2 -27 0.50 0.96 3 2 -27 0.48 0.90 3 2 -27 1.38 0.51 -3 -2 27 0.74 0.59 2 2 -27 2.63 0.61 2 2 -27 -1.02 0.88 2 2 -27 1.94 0.98 1 2 -27 0.25 0.92 1 2 -27 1.06 0.94 0 2 -27 3.96 1.05 0 2 -27 3.21 0.70 0 2 -27 1.51 0.96 -1 2 -27 8.23 0.96 -1 2 -27 8.12 1.32 -1 2 -27 7.53 1.27 -2 2 -27 10.35 1.34 -2 2 -27 16.50 1.78 -2 2 -27 15.17 1.35 5 1 -27 0.51 1.01 5 1 -27 0.93 0.48 5 1 -27 1.58 0.99 4 1 -27 1.61 1.03 4 1 -27 0.95 0.50 4 1 -27 1.12 0.98 3 1 -27 0.16 0.88 3 1 -27 -0.75 0.86 3 1 -27 0.11 0.48 2 1 -27 5.23 0.73 2 1 -27 5.74 1.15 2 1 -27 4.45 1.14 1 1 -27 -0.64 0.82 1 1 -27 -0.15 0.87 1 1 -27 -0.01 0.54 0 1 -27 2.67 1.00 0 1 -27 3.05 1.02 0 1 -27 3.45 0.75 -1 1 -27 5.61 1.11 -1 1 -27 4.06 0.82 -1 1 -27 4.00 1.14 -2 1 -27 -0.32 0.83 -2 1 -27 1.17 0.68 -2 1 -27 1.32 0.87 5 0 -27 -0.52 0.93 5 0 -27 -0.64 0.44 5 0 -27 0.40 0.97 4 0 -27 -0.22 0.47 4 0 -27 -1.12 0.86 4 0 -27 0.17 0.94 3 0 -27 0.79 0.94 3 0 -27 0.70 0.92 3 0 -27 -0.10 0.51 2 0 -27 0.62 0.87 2 0 -27 0.11 0.88 2 0 -27 0.46 0.54 1 0 -27 0.94 0.92 1 0 -27 -0.64 0.84 1 0 -27 0.76 0.61 0 0 -27 1.29 1.02 0 0 -27 0.37 0.59 0 0 -27 -0.03 0.82 -1 0 -27 3.84 1.01 -1 0 -27 1.52 0.91 -1 0 -27 -0.87 0.55 -2 0 -27 1.38 0.88 -2 0 -27 -0.40 0.61 -2 0 -27 -0.87 0.87 5 -1 -27 1.32 1.01 5 -1 -27 1.59 0.59 5 -1 -27 0.53 0.98 4 -1 -27 1.63 0.60 4 -1 -27 1.73 0.99 4 -1 -27 1.75 0.99 3 -1 -27 0.16 0.55 3 -1 -27 -0.29 0.82 3 -1 -27 -0.44 0.94 2 -1 -27 6.03 1.22 2 -1 -27 4.87 0.82 2 -1 -27 3.72 1.02 1 -1 -27 0.39 0.62 1 -1 -27 0.48 0.96 1 -1 -27 0.69 0.87 0 -1 -27 3.35 1.06 0 -1 -27 2.32 0.92 -1 -1 -27 3.59 0.82 -1 -1 -27 3.81 1.01 -1 -1 -27 3.61 1.15 -2 -1 -27 0.57 0.80 -2 -1 -27 0.89 0.73 -2 -1 -27 1.54 0.96 5 -2 -27 7.40 0.90 5 -2 -27 6.02 1.28 5 -2 -27 6.21 1.21 4 -2 -27 27.27 2.06 4 -2 -27 22.98 1.96 4 -2 -27 20.12 1.39 3 -2 -27 0.25 0.58 3 -2 -27 1.06 0.94 3 -2 -27 0.83 0.90 2 -2 -27 1.45 0.89 2 -2 -27 -0.17 0.57 2 -2 -27 0.14 0.82 1 -2 -27 0.39 0.85 1 -2 -27 -0.62 0.55 1 -2 -27 0.25 0.88 0 -2 -27 2.51 1.05 0 -2 -27 3.94 0.97 0 -2 -27 2.55 0.77 -1 -2 -27 8.80 1.20 -1 -2 -27 7.75 1.32 -1 -2 -27 9.68 1.12 -2 -2 -27 14.03 1.51 -2 -2 -27 14.82 1.58 -2 -2 -27 13.43 1.35 5 -3 -27 4.67 1.12 5 -3 -27 2.16 1.10 5 -3 -27 2.95 0.73 4 -3 -27 1.23 0.97 4 -3 -27 2.23 1.08 4 -3 -27 1.89 0.69 3 -3 -27 0.46 0.94 3 -3 -27 -0.01 0.82 3 -3 -27 0.42 0.64 2 -3 -27 25.35 1.60 2 -3 -27 24.87 2.05 2 -3 -27 29.54 1.95 1 -3 -27 5.19 0.87 1 -3 -27 3.02 1.07 1 -3 -27 3.53 0.99 0 -3 -27 15.11 1.67 0 -3 -27 18.72 1.47 0 -3 -27 17.04 1.59 -1 -3 -27 2.94 0.92 -1 -3 -27 2.72 1.10 -1 -3 -27 3.13 0.84 4 -4 -27 30.71 2.25 4 -4 -27 33.97 2.15 4 -4 -27 32.31 1.77 3 -4 -27 3.52 1.02 3 -4 -27 1.99 0.74 3 -4 -27 3.67 1.09 2 -4 -27 1.99 0.74 2 -4 -27 2.15 0.92 2 -4 -27 0.48 0.93 1 -4 -27 1.92 0.79 1 -4 -27 3.11 1.10 1 -4 -27 3.57 0.96 0 -4 -27 2.44 0.81 0 -4 -27 1.40 1.03 0 -4 -27 3.52 0.95 -1 -4 -27 3.91 0.88 -1 -4 -27 0.63 1.01 -1 -4 -27 2.96 0.89 4 -5 -27 0.44 0.87 4 -5 -27 1.04 0.70 4 -5 -27 -0.33 0.97 3 -5 -27 6.75 1.18 3 -5 -27 9.68 1.43 3 -5 -27 10.32 1.14 2 -5 -27 20.21 1.95 2 -5 -27 19.29 1.53 2 -5 -27 16.86 1.65 1 -5 -27 1.02 0.71 1 -5 -27 0.19 0.77 1 -5 -27 -0.53 0.96 0 -5 -27 17.05 1.88 0 -5 -27 18.29 1.56 0 -5 -27 16.18 1.48 3 -6 -27 0.49 0.66 3 -6 -27 1.12 1.02 3 -6 -27 -0.17 0.81 2 -6 -27 7.38 1.34 2 -6 -27 7.70 1.11 2 -6 -27 7.02 1.10 1 -6 -27 4.21 0.94 1 -6 -27 4.53 0.97 1 -6 -27 3.94 1.10 2 1 -28 2.47 1.04 2 1 -28 1.50 1.02 2 1 -28 2.22 0.64 1 1 -28 6.81 1.23 1 1 -28 4.96 1.22 1 1 -28 7.01 0.87 2 0 -28 5.93 0.83 2 0 -28 7.85 1.27 2 0 -28 7.66 1.36 1 0 -28 35.08 2.26 1 0 -28 25.17 1.97 1 0 -28 24.28 1.51 2 -1 -28 1.56 1.00 2 -1 -28 0.88 0.95 2 -1 -28 0.39 0.59 1 -1 -28 4.41 0.82 1 -1 -28 5.49 1.22 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 11193 _shelx_res_file ; TITL CC2109_0m_a.res in P2(1)/c CC2109_0m.res created by SHELXL-2018/3 at 12:40:45 on 20-Jul-2021 REM Old TITL CC2109_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.093, Rweak 0.005, Alpha 0.088 REM 0.337 for 226 systematic absences, Orientation as input REM Formula found by SHELXT: C56 F4 Mo2 O8 P2 CELL 0.71073 11.7991 18.6907 22.4744 90.000 97.256 90.000 ZERR 8.000 0.0004 0.0008 0.0008 0.000 0.002 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H F MO O P UNIT 224 176 24 8 24 8 ACTA TEMP -103.150 SIZE 0.05 0.05 0.05 L.S. 10 BOND $H CONF LIST 4 OMIT 0 2 0 OMIT 0 1 2 OMIT 1 1 0 OMIT -1 1 1 OMIT 0 0 2 HTAB C15 O6 EQIV $1 x+1, y, z HTAB C49 F4_$1 EQIV $2 x-1, y, z HTAB C55 O3_$2 EQIV $3 x, -y+1/2, z+1/2 HTAB C34 O1_$3 FMAP 2 PLAN 20 WGHT 0.021100 4.486500 FVAR 0.07030 MO1 4 0.683589 0.167436 0.310967 11.00000 0.02038 0.01882 = 0.01827 -0.00050 -0.00004 0.00364 P1 6 0.507280 0.186022 0.357910 11.00000 0.02031 0.01899 = 0.01997 0.00104 0.00047 0.00069 F1 3 0.549080 0.085106 0.610777 11.00000 0.05696 0.10401 = 0.02973 0.03130 0.00338 -0.00345 F2 3 0.081206 0.036493 0.257172 11.00000 0.03603 0.06815 = 0.05538 -0.01778 0.00491 -0.02743 F3 3 0.365089 0.490636 0.352388 11.00000 0.04538 0.02046 = 0.06691 -0.00373 0.00870 0.00493 O1 5 0.510706 0.182663 0.194899 11.00000 0.03736 0.05060 = 0.02840 -0.00348 -0.00926 0.00652 O2 5 0.746333 0.311990 0.376278 11.00000 0.03754 0.03308 = 0.03775 -0.01276 0.00494 -0.00742 O3 5 0.881322 0.222386 0.246953 11.00000 0.02757 0.03920 = 0.03413 -0.00003 0.00794 0.00252 C1 1 0.573384 0.181925 0.238756 11.00000 0.02677 0.02469 = 0.02544 -0.00305 0.00369 0.00379 C2 1 0.718366 0.259552 0.351333 11.00000 0.01991 0.02901 = 0.02428 0.00017 0.00421 -0.00013 C3 1 0.782653 0.236625 0.252825 11.00000 0.02865 0.02711 = 0.01826 -0.00388 0.00150 -0.00149 C4 1 0.729406 0.303235 0.220838 11.00000 0.03986 0.03302 = 0.03161 0.00387 0.00747 0.00569 AFIX 23 H4A 2 0.666050 0.287860 0.190403 11.00000 -1.20000 H4B 2 0.696117 0.333204 0.250547 11.00000 -1.20000 AFIX 0 C5 1 0.811066 0.348825 0.190213 11.00000 0.04945 0.03556 = 0.03807 0.00635 0.00729 -0.00205 AFIX 137 H5A 2 0.842510 0.320370 0.159538 11.00000 -1.50000 H5B 2 0.873425 0.365392 0.219977 11.00000 -1.50000 H5C 2 0.770080 0.390200 0.171316 11.00000 -1.50000 AFIX 0 C6 1 0.698736 0.043649 0.294013 11.00000 0.05607 0.01915 = 0.04701 -0.00391 -0.00092 0.01138 AFIX 13 H6 2 0.647429 0.014715 0.264404 11.00000 -1.20000 AFIX 0 C7 1 0.687181 0.052334 0.355025 11.00000 0.03705 0.02067 = 0.04557 0.00961 0.00492 0.00743 AFIX 13 H7 2 0.625273 0.031156 0.376022 11.00000 -1.20000 AFIX 0 C8 1 0.781809 0.090858 0.382604 11.00000 0.03364 0.03544 = 0.03258 0.01229 -0.00243 0.01344 AFIX 13 H8 2 0.799791 0.100797 0.426502 11.00000 -1.20000 AFIX 0 C9 1 0.852329 0.106731 0.338290 11.00000 0.02544 0.04278 = 0.04149 0.01326 0.00120 0.01613 AFIX 13 H9 2 0.930101 0.128742 0.345501 11.00000 -1.20000 AFIX 0 C10 1 0.800784 0.077307 0.283248 11.00000 0.05441 0.03258 = 0.04141 0.00234 0.01463 0.02653 AFIX 13 H10 2 0.835835 0.075189 0.245032 11.00000 -1.20000 AFIX 0 C11 1 0.518011 0.154570 0.435856 11.00000 0.02425 0.02540 = 0.02163 0.00326 0.00417 0.00503 C12 1 0.608918 0.177240 0.477179 11.00000 0.02661 0.04961 = 0.02843 0.00584 0.00188 -0.00416 AFIX 43 H12 2 0.664562 0.208646 0.464597 11.00000 -1.20000 AFIX 0 C13 1 0.619406 0.154703 0.536293 11.00000 0.03176 0.07135 = 0.02551 0.00771 -0.00419 -0.00255 AFIX 43 H13 2 0.680534 0.171027 0.564616 11.00000 -1.20000 AFIX 0 C14 1 0.539032 0.108102 0.552882 11.00000 0.03939 0.05863 = 0.02486 0.01485 0.00646 0.01023 C15 1 0.449660 0.083290 0.513936 11.00000 0.03703 0.03551 = 0.03563 0.01296 0.01177 0.00223 AFIX 43 H15 2 0.395996 0.050678 0.526812 11.00000 -1.20000 AFIX 0 C16 1 0.439232 0.107063 0.454803 11.00000 0.02804 0.02439 = 0.03110 0.00204 0.00479 0.00411 AFIX 43 H16 2 0.377406 0.090595 0.426987 11.00000 -1.20000 AFIX 0 C17 1 0.374866 0.143128 0.323792 11.00000 0.02441 0.02486 = 0.02154 0.00282 0.00072 -0.00477 C18 1 0.379766 0.074024 0.301203 11.00000 0.03150 0.02933 = 0.03217 -0.00379 0.00193 -0.00128 AFIX 43 H18 2 0.451868 0.051639 0.300493 11.00000 -1.20000 AFIX 0 C19 1 0.280765 0.037407 0.279713 11.00000 0.04173 0.03453 = 0.03241 -0.00767 0.00378 -0.01084 AFIX 43 H19 2 0.284022 -0.010424 0.265731 11.00000 -1.20000 AFIX 0 C20 1 0.178084 0.071908 0.279135 11.00000 0.03115 0.05084 = 0.02611 -0.00260 0.00400 -0.01819 C21 1 0.168770 0.140336 0.299694 11.00000 0.02436 0.04317 = 0.02920 0.00126 0.00521 -0.00541 AFIX 43 H21 2 0.096469 0.163162 0.297831 11.00000 -1.20000 AFIX 0 C22 1 0.268210 0.175446 0.323379 11.00000 0.02783 0.02890 = 0.02596 0.00259 0.00403 -0.00272 AFIX 43 H22 2 0.263447 0.222164 0.339530 11.00000 -1.20000 AFIX 0 C23 1 0.463012 0.279417 0.360212 11.00000 0.01589 0.02120 = 0.02626 0.00022 0.00137 -0.00065 C24 1 0.423427 0.311634 0.305395 11.00000 0.03171 0.02247 = 0.02599 -0.00064 0.00042 0.00204 AFIX 43 H24 2 0.421085 0.284722 0.269401 11.00000 -1.20000 AFIX 0 C25 1 0.387707 0.381965 0.302823 11.00000 0.03424 0.02431 = 0.03548 0.00533 -0.00123 0.00176 AFIX 43 H25 2 0.358032 0.403262 0.265723 11.00000 -1.20000 AFIX 0 C26 1 0.396098 0.420190 0.354975 11.00000 0.02155 0.01873 = 0.05262 -0.00250 0.00707 0.00069 C27 1 0.434766 0.391217 0.409831 11.00000 0.02732 0.03109 = 0.03445 -0.01059 0.00836 -0.00376 AFIX 43 H27 2 0.439161 0.419233 0.445318 11.00000 -1.20000 AFIX 0 C28 1 0.467334 0.319773 0.412083 11.00000 0.02228 0.02888 = 0.02553 -0.00134 0.00393 -0.00037 AFIX 43 H28 2 0.492908 0.298322 0.449712 11.00000 -1.20000 AFIX 0 MO2 4 0.137775 0.205034 0.571032 11.00000 0.01832 0.02103 = 0.01787 0.00333 0.00110 0.00077 P2 6 0.076261 0.326916 0.539871 11.00000 0.01800 0.02054 = 0.01817 0.00111 0.00262 0.00139 F4 3 -0.410945 0.384832 0.565359 11.00000 0.02067 0.06717 = 0.04682 -0.00497 0.01131 0.00748 F5 3 0.364886 0.551121 0.670187 11.00000 0.03328 0.03643 = 0.05154 -0.01189 0.00458 -0.01458 F6 3 0.087377 0.406591 0.284690 11.00000 0.06412 0.06045 = 0.02215 0.01105 0.01291 0.01080 O4 5 -0.115755 0.178233 0.518264 11.00000 0.02352 0.03883 = 0.05287 -0.00674 -0.00066 -0.00365 O5 5 0.283703 0.232457 0.466969 11.00000 0.03813 0.04209 = 0.04697 0.01361 0.02443 0.01184 O6 5 0.184253 0.047656 0.546479 11.00000 0.09869 0.02703 = 0.04338 0.00406 -0.01428 0.01102 C29 1 -0.020911 0.188245 0.536038 11.00000 0.02666 0.02094 = 0.02769 0.00137 0.00502 0.00184 C30 1 0.226759 0.221999 0.504188 11.00000 0.02384 0.02274 = 0.03144 0.00246 0.00191 0.00517 C31 1 0.140346 0.098678 0.521000 11.00000 0.02508 0.02272 = 0.03161 0.00348 0.00353 -0.00202 C32 1 0.091996 0.089593 0.455937 11.00000 0.04741 0.03792 = 0.03087 -0.00345 -0.00107 0.00879 AFIX 23 H32A 2 0.008542 0.097943 0.452191 11.00000 -1.20000 H32B 2 0.125178 0.127064 0.432240 11.00000 -1.20000 AFIX 0 C33 1 0.112474 0.017917 0.428551 11.00000 0.05905 0.03552 = 0.03831 -0.00555 0.00785 -0.00632 AFIX 137 H33A 2 0.073311 0.016208 0.387439 11.00000 -1.50000 H33B 2 0.082777 -0.020030 0.452393 11.00000 -1.50000 H33C 2 0.194657 0.010948 0.428005 11.00000 -1.50000 AFIX 0 C34 1 0.291018 0.219594 0.648018 11.00000 0.03610 0.06185 = 0.02251 0.00277 -0.00898 -0.01275 AFIX 13 H34 2 0.365723 0.243055 0.643730 11.00000 -1.20000 AFIX 0 C35 1 0.196770 0.252740 0.667990 11.00000 0.07257 0.03825 = 0.01603 -0.00039 -0.00681 0.00040 AFIX 13 H35 2 0.192359 0.304240 0.679536 11.00000 -1.20000 AFIX 0 C36 1 0.113513 0.200862 0.674250 11.00000 0.04199 0.06337 = 0.01806 0.01120 0.00722 0.01404 AFIX 13 H36 2 0.040367 0.208562 0.691483 11.00000 -1.20000 AFIX 0 C37 1 0.156275 0.134251 0.656453 11.00000 0.04834 0.03795 = 0.02388 0.01473 -0.00244 -0.00491 AFIX 13 H37 2 0.120101 0.086396 0.660455 11.00000 -1.20000 AFIX 0 C38 1 0.267043 0.146768 0.640665 11.00000 0.03733 0.04496 = 0.02294 0.00658 -0.00481 0.01429 AFIX 13 H38 2 0.322423 0.109088 0.631453 11.00000 -1.20000 AFIX 0 C39 1 -0.071608 0.351256 0.548936 11.00000 0.02013 0.02015 = 0.02000 -0.00036 0.00086 0.00189 C40 1 -0.114395 0.336215 0.602741 11.00000 0.02923 0.03477 = 0.02426 0.00515 0.00454 0.00495 AFIX 43 H40 2 -0.064987 0.316910 0.635460 11.00000 -1.20000 AFIX 0 C41 1 -0.228073 0.349079 0.609071 11.00000 0.03081 0.03838 = 0.02738 0.00463 0.01233 0.00503 AFIX 43 H41 2 -0.256614 0.339932 0.646011 11.00000 -1.20000 AFIX 0 C42 1 -0.298180 0.375312 0.560702 11.00000 0.01963 0.03228 = 0.03629 -0.00701 0.00821 0.00093 C43 1 -0.259760 0.392067 0.507477 11.00000 0.02335 0.04240 = 0.02757 0.00009 -0.00037 0.00743 AFIX 43 H43 2 -0.309978 0.411534 0.475153 11.00000 -1.20000 AFIX 0 C44 1 -0.145310 0.379874 0.501898 11.00000 0.02326 0.03466 = 0.02156 0.00172 0.00443 0.00267 AFIX 43 H44 2 -0.117090 0.391315 0.465296 11.00000 -1.20000 AFIX 0 C45 1 0.162107 0.397787 0.579761 11.00000 0.02361 0.02347 = 0.01888 0.00285 0.00103 -0.00172 C46 1 0.113580 0.456124 0.605047 11.00000 0.02100 0.02633 = 0.02481 0.00099 0.00047 0.00188 AFIX 43 H46 2 0.032784 0.460151 0.601914 11.00000 -1.20000 AFIX 0 C47 1 0.181904 0.508838 0.634963 11.00000 0.02993 0.02327 = 0.03107 -0.00220 0.00574 0.00218 AFIX 43 H47 2 0.148881 0.548962 0.652204 11.00000 -1.20000 AFIX 0 C48 1 0.297852 0.501318 0.638868 11.00000 0.02826 0.02565 = 0.03052 0.00097 -0.00033 -0.00856 C49 1 0.349968 0.444969 0.613768 11.00000 0.02077 0.03050 = 0.03828 0.00282 0.00462 -0.00270 AFIX 43 H49 2 0.430847 0.441860 0.616714 11.00000 -1.20000 AFIX 0 C50 1 0.281339 0.393242 0.584261 11.00000 0.02228 0.02770 = 0.03294 -0.00273 0.00628 0.00214 AFIX 43 H50 2 0.315441 0.353790 0.566651 11.00000 -1.20000 AFIX 0 C51 1 0.083103 0.351421 0.461382 11.00000 0.01869 0.02417 = 0.01835 0.00112 0.00288 0.00505 C52 1 0.126690 0.416983 0.446055 11.00000 0.02496 0.02520 = 0.02542 0.00150 0.00532 0.00261 AFIX 43 H52 2 0.155534 0.449472 0.476796 11.00000 -1.20000 AFIX 0 C53 1 0.128667 0.435747 0.386126 11.00000 0.02993 0.03140 = 0.02947 0.00762 0.01090 0.00520 AFIX 43 H53 2 0.158918 0.480455 0.375637 11.00000 -1.20000 AFIX 0 C54 1 0.085974 0.388152 0.342956 11.00000 0.03191 0.04336 = 0.02152 0.00883 0.01153 0.01425 C55 1 0.041003 0.322896 0.355840 11.00000 0.03601 0.03643 = 0.02317 -0.00329 0.00012 0.00956 AFIX 43 H55 2 0.011264 0.291174 0.324697 11.00000 -1.20000 AFIX 0 C56 1 0.040354 0.304773 0.415627 11.00000 0.03068 0.02443 = 0.02533 0.00137 0.00227 0.00333 AFIX 43 H56 2 0.010257 0.259799 0.425552 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM CC2109_0m_a.res in P2(1)/c REM wR2 = 0.063326, GooF = S = 1.06840, Restrained GooF = 1.06840 for all data REM R1 = 0.029163 for 8547 Fo > 4sig(Fo) and 0.038591 for all 10047 data REM 651 parameters refined using 0 restraints END WGHT 0.0211 4.4865 REM Highest difference peak 0.373, deepest hole -0.393, 1-sigma level 0.065 Q1 1 0.1928 -0.0173 0.4471 11.00000 0.05 0.37 Q2 1 0.5156 0.1760 0.4023 11.00000 0.05 0.35 Q3 1 0.4725 0.2425 0.3583 11.00000 0.05 0.32 Q4 1 0.0842 0.3418 0.4922 11.00000 0.05 0.31 Q5 1 0.4013 0.3999 0.3845 11.00000 0.05 0.31 Q6 1 0.4258 0.4012 0.3271 11.00000 0.05 0.31 Q7 1 -0.0036 0.3402 0.5461 11.00000 0.05 0.30 Q8 1 0.1241 0.3993 0.3715 11.00000 0.05 0.30 Q9 1 0.1126 0.0629 0.5472 11.00000 0.05 0.29 Q10 1 0.0607 0.1277 0.4409 11.00000 0.05 0.28 Q11 1 0.0160 0.3241 0.3847 11.00000 0.05 0.28 Q12 1 0.2262 0.4043 0.5649 11.00000 0.05 0.28 Q13 1 -0.2836 0.3642 0.5296 11.00000 0.05 0.28 Q14 1 0.7598 0.2796 0.2383 11.00000 0.05 0.26 Q15 1 0.2831 0.1755 0.6604 11.00000 0.05 0.26 Q16 1 0.6605 0.3141 0.2353 11.00000 0.05 0.26 Q17 1 0.4294 0.1620 0.3375 11.00000 0.05 0.26 Q18 1 0.2089 0.2039 0.5442 11.00000 0.05 0.25 Q19 1 0.0775 0.1568 0.6621 11.00000 0.05 0.25 Q20 1 0.7004 0.0276 0.3239 11.00000 0.05 0.25 ; _shelx_res_checksum 4554 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mo Mo1 0.68359(2) 0.16744(2) 0.31097(2) 0.01937(5) Uani d 1 . . P P1 0.50728(5) 0.18602(3) 0.35791(3) 0.01993(12) Uani d 1 . . F F1 0.54908(16) 0.08511(12) 0.61078(7) 0.0637(6) Uani d 1 . . F F2 0.08121(14) 0.03649(10) 0.25717(8) 0.0533(5) Uani d 1 . . F F3 0.36509(14) 0.49064(7) 0.35239(8) 0.0441(4) Uani d 1 . . O O1 0.51071(16) 0.18266(10) 0.19490(8) 0.0399(5) Uani d 1 . . O O2 0.74633(16) 0.31199(10) 0.37628(8) 0.0361(4) Uani d 1 . . O O3 0.88132(15) 0.22239(10) 0.24695(8) 0.0333(4) Uani d 1 . . C C1 0.5734(2) 0.18193(12) 0.23876(11) 0.0256(5) Uani d 1 . . C C2 0.71837(19) 0.25955(13) 0.35133(10) 0.0243(5) Uani d 1 . . C C3 0.7827(2) 0.23663(13) 0.25283(10) 0.0248(5) Uani d 1 . . C C4 0.7294(2) 0.30324(14) 0.22084(12) 0.0346(6) Uani d 1 . . H H4A 0.66605 0.28786 0.190403 0.041 Uiso calc 1 . . H H4B 0.696117 0.333204 0.250547 0.041 Uiso calc 1 . . C C5 0.8111(3) 0.34882(15) 0.19021(13) 0.0409(7) Uani d 1 . . H H5A 0.84251 0.32037 0.159538 0.061 Uiso calc 1 . . H H5B 0.873425 0.365392 0.219977 0.061 Uiso calc 1 . . H H5C 0.77008 0.3902 0.171316 0.061 Uiso calc 1 . . C C6 0.6987(3) 0.04365(14) 0.29401(13) 0.0414(7) Uani d 1 . . H H6 0.647429 0.014715 0.264404 0.05 Uiso calc 1 . . C C7 0.6872(2) 0.05233(13) 0.35502(13) 0.0345(6) Uani d 1 . . H H7 0.625273 0.031156 0.376022 0.041 Uiso calc 1 . . C C8 0.7818(2) 0.09086(14) 0.38260(12) 0.0345(6) Uani d 1 . . H H8 0.799791 0.100797 0.426502 0.041 Uiso calc 1 . . C C9 0.8523(2) 0.10673(15) 0.33829(12) 0.0368(6) Uani d 1 . . H H9 0.930101 0.128742 0.345501 0.044 Uiso calc 1 . . C C10 0.8008(3) 0.07731(15) 0.28325(13) 0.0421(7) Uani d 1 . . H H10 0.835835 0.075189 0.245032 0.05 Uiso calc 1 . . C C11 0.5180(2) 0.15457(12) 0.43586(10) 0.0236(5) Uani d 1 . . C C12 0.6089(2) 0.17724(15) 0.47718(12) 0.0350(6) Uani d 1 . . H H12 0.664562 0.208646 0.464597 0.042 Uiso calc 1 . . C C13 0.6194(2) 0.15470(18) 0.53629(12) 0.0435(7) Uani d 1 . . H H13 0.680534 0.171027 0.564616 0.052 Uiso calc 1 . . C C14 0.5390(2) 0.10810(17) 0.55288(12) 0.0408(7) Uani d 1 . . C C15 0.4497(2) 0.08329(14) 0.51394(12) 0.0354(6) Uani d 1 . . H H15 0.395996 0.050678 0.526812 0.043 Uiso calc 1 . . C C16 0.4392(2) 0.10706(13) 0.45480(11) 0.0278(5) Uani d 1 . . H H16 0.377406 0.090595 0.426987 0.033 Uiso calc 1 . . C C17 0.3749(2) 0.14313(12) 0.32379(10) 0.0238(5) Uani d 1 . . C C18 0.3798(2) 0.07402(13) 0.30120(11) 0.0312(6) Uani d 1 . . H H18 0.451868 0.051639 0.300493 0.037 Uiso calc 1 . . C C19 0.2808(2) 0.03741(15) 0.27971(12) 0.0363(6) Uani d 1 . . H H19 0.284022 -0.010424 0.265731 0.044 Uiso calc 1 . . C C20 0.1781(2) 0.07191(16) 0.27914(12) 0.0360(6) Uani d 1 . . C C21 0.1688(2) 0.14034(15) 0.29969(11) 0.0321(6) Uani d 1 . . H H21 0.096469 0.163162 0.297831 0.039 Uiso calc 1 . . C C22 0.2682(2) 0.17545(13) 0.32338(11) 0.0275(5) Uani d 1 . . H H22 0.263447 0.222164 0.33953 0.033 Uiso calc 1 . . C C23 0.46301(18) 0.27942(12) 0.36021(10) 0.0212(5) Uani d 1 . . C C24 0.4234(2) 0.31163(12) 0.30539(11) 0.0270(5) Uani d 1 . . H H24 0.421085 0.284722 0.269401 0.032 Uiso calc 1 . . C C25 0.3877(2) 0.38197(13) 0.30282(12) 0.0318(6) Uani d 1 . . H H25 0.358032 0.403262 0.265723 0.038 Uiso calc 1 . . C C26 0.3961(2) 0.42019(12) 0.35498(13) 0.0308(6) Uani d 1 . . C C27 0.4348(2) 0.39122(13) 0.40983(12) 0.0306(6) Uani d 1 . . H H27 0.439161 0.419233 0.445318 0.037 Uiso calc 1 . . C C28 0.4673(2) 0.31977(13) 0.41208(11) 0.0255(5) Uani d 1 . . H H28 0.492908 0.298322 0.449712 0.031 Uiso calc 1 . . Mo Mo2 0.13778(2) 0.20503(2) 0.57103(2) 0.01918(5) Uani d 1 . . P P2 0.07626(5) 0.32692(3) 0.53987(3) 0.01888(12) Uani d 1 . . F F4 -0.41095(12) 0.38483(9) 0.56536(7) 0.0443(4) Uani d 1 . . F F5 0.36489(13) 0.55112(8) 0.67019(7) 0.0405(4) Uani d 1 . . F F6 0.08738(15) 0.40659(9) 0.28469(7) 0.0483(4) Uani d 1 . . O O4 -0.11576(15) 0.17823(10) 0.51826(9) 0.0389(4) Uani d 1 . . O O5 0.28370(16) 0.23246(10) 0.46697(9) 0.0408(5) Uani d 1 . . O O6 0.1843(2) 0.04766(10) 0.54648(9) 0.0584(6) Uani d 1 . . C C29 -0.0209(2) 0.18824(12) 0.53604(11) 0.0250(5) Uani d 1 . . C C30 0.2268(2) 0.22200(12) 0.50419(11) 0.0261(5) Uani d 1 . . C C31 0.1403(2) 0.09868(12) 0.52100(11) 0.0265(5) Uani d 1 . . C C32 0.0920(3) 0.08959(15) 0.45594(12) 0.0392(7) Uani d 1 . . H H32A 0.008542 0.097943 0.452191 0.047 Uiso calc 1 . . H H32B 0.125178 0.127064 0.43224 0.047 Uiso calc 1 . . C C33 0.1125(3) 0.01792(15) 0.42855(13) 0.0441(7) Uani d 1 . . H H33A 0.073311 0.016208 0.387439 0.066 Uiso calc 1 . . H H33B 0.082777 -0.02003 0.452393 0.066 Uiso calc 1 . . H H33C 0.194657 0.010948 0.428005 0.066 Uiso calc 1 . . C C34 0.2910(2) 0.21959(17) 0.64802(12) 0.0412(7) Uani d 1 . . H H34 0.365723 0.243055 0.64373 0.049 Uiso calc 1 . . C C35 0.1968(3) 0.25274(16) 0.66799(11) 0.0433(7) Uani d 1 . . H H35 0.192359 0.30424 0.679536 0.052 Uiso calc 1 . . C C36 0.1135(3) 0.20086(17) 0.67425(11) 0.0408(7) Uani d 1 . . H H36 0.040367 0.208562 0.691483 0.049 Uiso calc 1 . . C C37 0.1563(2) 0.13425(15) 0.65645(11) 0.0373(6) Uani d 1 . . H H37 0.120101 0.086396 0.660455 0.045 Uiso calc 1 . . C C38 0.2670(2) 0.14677(15) 0.64067(11) 0.0358(6) Uani d 1 . . H H38 0.322423 0.109088 0.631453 0.043 Uiso calc 1 . . C C39 -0.07161(19) 0.35126(12) 0.54894(10) 0.0202(5) Uani d 1 . . C C40 -0.1144(2) 0.33622(13) 0.60274(11) 0.0293(5) Uani d 1 . . H H40 -0.064987 0.31691 0.63546 0.035 Uiso calc 1 . . C C41 -0.2281(2) 0.34908(14) 0.60907(11) 0.0314(6) Uani d 1 . . H H41 -0.256614 0.339932 0.646011 0.038 Uiso calc 1 . . C C42 -0.2982(2) 0.37531(13) 0.56070(12) 0.0290(5) Uani d 1 . . C C43 -0.2598(2) 0.39207(14) 0.50748(11) 0.0314(6) Uani d 1 . . H H43 -0.309978 0.411534 0.475153 0.038 Uiso calc 1 . . C C44 -0.1453(2) 0.37987(13) 0.50190(11) 0.0264(5) Uani d 1 . . H H44 -0.11709 0.391315 0.465296 0.032 Uiso calc 1 . . C C45 0.16211(19) 0.39779(12) 0.57976(10) 0.0221(5) Uani d 1 . . C C46 0.1136(2) 0.45612(12) 0.60505(10) 0.0243(5) Uani d 1 . . H H46 0.032784 0.460151 0.601914 0.029 Uiso calc 1 . . C C47 0.1819(2) 0.50884(13) 0.63496(11) 0.0279(5) Uani d 1 . . H H47 0.148881 0.548962 0.652204 0.034 Uiso calc 1 . . C C48 0.2979(2) 0.50132(13) 0.63887(11) 0.0285(5) Uani d 1 . . C C49 0.3500(2) 0.44497(13) 0.61377(11) 0.0298(6) Uani d 1 . . H H49 0.430847 0.44186 0.616714 0.036 Uiso calc 1 . . C C50 0.2813(2) 0.39324(13) 0.58426(11) 0.0274(5) Uani d 1 . . H H50 0.315441 0.35379 0.566651 0.033 Uiso calc 1 . . C C51 0.08310(18) 0.35142(12) 0.46138(10) 0.0204(5) Uani d 1 . . C C52 0.1267(2) 0.41698(12) 0.44605(11) 0.0250(5) Uani d 1 . . H H52 0.155534 0.449472 0.476796 0.03 Uiso calc 1 . . C C53 0.1287(2) 0.43575(14) 0.38613(11) 0.0297(5) Uani d 1 . . H H53 0.158918 0.480455 0.375637 0.036 Uiso calc 1 . . C C54 0.0860(2) 0.38815(15) 0.34296(11) 0.0316(6) Uani d 1 . . C C55 0.0410(2) 0.32290(14) 0.35584(11) 0.0322(6) Uani d 1 . . H H55 0.011264 0.291174 0.324697 0.039 Uiso calc 1 . . C C56 0.0404(2) 0.30477(13) 0.41563(11) 0.0269(5) Uani d 1 . . H H56 0.010257 0.259799 0.425552 0.032 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mo1 0.02038(10) 0.01882(10) 0.01827(10) 0.00364(8) -0.00004(7) -0.00050(7) P1 0.0203(3) 0.0190(3) 0.0200(3) 0.0007(2) 0.0005(2) 0.0010(2) F1 0.0570(12) 0.1040(16) 0.0297(9) -0.0035(11) 0.0034(8) 0.0313(10) F2 0.0360(9) 0.0682(12) 0.0554(11) -0.0274(9) 0.0049(8) -0.0178(9) F3 0.0454(10) 0.0205(7) 0.0669(11) 0.0049(7) 0.0087(8) -0.0037(7) O1 0.0374(11) 0.0506(12) 0.0284(10) 0.0065(9) -0.0093(8) -0.0035(9) O2 0.0375(10) 0.0331(10) 0.0377(10) -0.0074(8) 0.0049(8) -0.0128(8) O3 0.0276(9) 0.0392(10) 0.0341(10) 0.0025(8) 0.0079(8) 0.0000(8) C1 0.0268(12) 0.0247(12) 0.0254(12) 0.0038(10) 0.0037(10) -0.0031(10) C2 0.0199(11) 0.0290(13) 0.0243(12) -0.0001(10) 0.0042(9) 0.0002(10) C3 0.0287(13) 0.0271(12) 0.0183(11) -0.0015(10) 0.0015(10) -0.0039(9) C4 0.0399(15) 0.0330(14) 0.0316(14) 0.0057(12) 0.0075(12) 0.0039(11) C5 0.0494(17) 0.0356(15) 0.0381(16) -0.0021(13) 0.0073(13) 0.0064(12) C6 0.0561(19) 0.0191(12) 0.0470(17) 0.0114(12) -0.0009(14) -0.0039(12) C7 0.0371(15) 0.0207(12) 0.0456(16) 0.0074(11) 0.0049(12) 0.0096(11) C8 0.0336(14) 0.0354(14) 0.0326(14) 0.0134(12) -0.0024(11) 0.0123(12) C9 0.0254(13) 0.0428(15) 0.0415(16) 0.0161(12) 0.0012(12) 0.0133(13) C10 0.0544(18) 0.0326(14) 0.0414(16) 0.0265(14) 0.0146(14) 0.0023(12) C11 0.0242(12) 0.0254(12) 0.0216(11) 0.0050(10) 0.0042(9) 0.0033(9) C12 0.0266(13) 0.0496(16) 0.0284(13) -0.0042(12) 0.0019(11) 0.0058(12) C13 0.0318(15) 0.071(2) 0.0255(14) -0.0025(14) -0.0042(11) 0.0077(14) C14 0.0394(16) 0.0586(19) 0.0249(14) 0.0102(14) 0.0065(12) 0.0149(13) C15 0.0370(15) 0.0355(14) 0.0356(15) 0.0022(12) 0.0118(12) 0.0130(12) C16 0.0280(13) 0.0244(12) 0.0311(13) 0.0041(10) 0.0048(10) 0.0020(10) C17 0.0244(12) 0.0249(12) 0.0215(12) -0.0048(10) 0.0007(9) 0.0028(9) C18 0.0315(14) 0.0293(13) 0.0322(14) -0.0013(11) 0.0019(11) -0.0038(11) C19 0.0417(16) 0.0345(14) 0.0324(14) -0.0108(12) 0.0038(12) -0.0077(12) C20 0.0312(14) 0.0508(17) 0.0261(13) -0.0182(13) 0.0040(11) -0.0026(12) C21 0.0244(13) 0.0432(15) 0.0292(14) -0.0054(11) 0.0052(10) 0.0013(12) C22 0.0278(13) 0.0289(13) 0.0260(12) -0.0027(10) 0.0040(10) 0.0026(10) C23 0.0159(10) 0.0212(11) 0.0263(12) -0.0006(9) 0.0014(9) 0.0002(9) C24 0.0317(13) 0.0225(12) 0.0260(12) 0.0020(10) 0.0004(10) -0.0006(10) C25 0.0342(14) 0.0243(12) 0.0355(14) 0.0018(11) -0.0012(11) 0.0053(11) C26 0.0216(12) 0.0187(11) 0.0526(17) 0.0007(10) 0.0071(11) -0.0025(11) C27 0.0273(13) 0.0311(13) 0.0345(14) -0.0038(11) 0.0084(11) -0.0106(11) C28 0.0223(12) 0.0289(12) 0.0255(12) -0.0004(10) 0.0039(10) -0.0013(10) Mo2 0.01832(10) 0.02103(10) 0.01787(10) 0.00077(8) 0.00110(7) 0.00333(8) P2 0.0180(3) 0.0205(3) 0.0182(3) 0.0014(2) 0.0026(2) 0.0011(2) F4 0.0207(7) 0.0672(11) 0.0468(10) 0.0075(7) 0.0113(7) -0.0050(8) F5 0.0333(8) 0.0364(8) 0.0515(10) -0.0146(7) 0.0046(7) -0.0119(7) F6 0.0641(11) 0.0604(11) 0.0221(8) 0.0108(9) 0.0129(8) 0.0110(7) O4 0.0235(10) 0.0388(11) 0.0529(12) -0.0036(8) -0.0007(9) -0.0067(9) O5 0.0381(11) 0.0421(11) 0.0470(12) 0.0118(9) 0.0244(9) 0.0136(9) O6 0.0987(19) 0.0270(10) 0.0434(12) 0.0110(11) -0.0143(12) 0.0041(9) C29 0.0267(13) 0.0209(11) 0.0277(12) 0.0018(10) 0.0050(10) 0.0014(10) C30 0.0238(12) 0.0227(12) 0.0314(13) 0.0052(10) 0.0019(11) 0.0025(10) C31 0.0251(12) 0.0227(12) 0.0316(13) -0.0020(10) 0.0035(10) 0.0035(10) C32 0.0474(17) 0.0379(15) 0.0309(14) 0.0088(13) -0.0011(12) -0.0035(12) C33 0.0590(19) 0.0355(15) 0.0383(16) -0.0063(14) 0.0078(14) -0.0056(13) C34 0.0361(15) 0.0618(19) 0.0225(13) -0.0127(14) -0.0090(11) 0.0028(13) C35 0.073(2) 0.0383(15) 0.0160(12) 0.0004(15) -0.0068(13) -0.0004(11) C36 0.0420(16) 0.0634(19) 0.0181(12) 0.0140(15) 0.0072(11) 0.0112(13) C37 0.0483(17) 0.0379(15) 0.0239(13) -0.0049(13) -0.0024(12) 0.0147(11) C38 0.0373(15) 0.0450(16) 0.0229(13) 0.0143(13) -0.0048(11) 0.0066(11) C39 0.0201(11) 0.0202(11) 0.0200(11) 0.0019(9) 0.0009(9) -0.0004(9) C40 0.0292(13) 0.0348(14) 0.0243(12) 0.0049(11) 0.0045(10) 0.0052(11) C41 0.0308(13) 0.0384(14) 0.0274(13) 0.0050(11) 0.0123(11) 0.0046(11) C42 0.0196(12) 0.0323(13) 0.0363(14) 0.0009(10) 0.0082(10) -0.0070(11) C43 0.0233(12) 0.0424(15) 0.0276(13) 0.0074(11) -0.0004(10) 0.0001(11) C44 0.0233(12) 0.0347(13) 0.0216(12) 0.0027(10) 0.0044(10) 0.0017(10) C45 0.0236(12) 0.0235(11) 0.0189(11) -0.0017(9) 0.0010(9) 0.0028(9) C46 0.0210(11) 0.0263(12) 0.0248(12) 0.0019(10) 0.0005(9) 0.0010(10) C47 0.0299(13) 0.0233(12) 0.0311(13) 0.0022(10) 0.0057(11) -0.0022(10) C48 0.0283(13) 0.0256(12) 0.0305(13) -0.0086(10) -0.0003(10) 0.0010(10) C49 0.0208(12) 0.0305(13) 0.0383(15) -0.0027(10) 0.0046(11) 0.0028(11) C50 0.0223(12) 0.0277(12) 0.0329(13) 0.0021(10) 0.0063(10) -0.0027(10) C51 0.0187(11) 0.0242(11) 0.0183(11) 0.0051(9) 0.0029(9) 0.0011(9) C52 0.0250(12) 0.0252(12) 0.0254(12) 0.0026(10) 0.0053(10) 0.0015(10) C53 0.0299(13) 0.0314(13) 0.0295(13) 0.0052(11) 0.0109(11) 0.0076(11) C54 0.0319(14) 0.0434(15) 0.0215(12) 0.0143(12) 0.0115(10) 0.0088(11) C55 0.0360(14) 0.0364(14) 0.0232(12) 0.0096(12) 0.0001(11) -0.0033(11) C56 0.0307(13) 0.0244(12) 0.0253(12) 0.0033(10) 0.0023(10) 0.0014(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 Mo1 C2 . . 109.77(10) y C1 Mo1 C3 . . 77.34(9) y C2 Mo1 C3 . . 70.93(9) y C2 Mo1 C9 . . 100.67(10) ? C1 Mo1 C9 . . 138.27(10) ? C3 Mo1 C9 . . 86.76(9) ? C2 Mo1 C10 . . 131.68(11) ? C1 Mo1 C10 . . 103.50(10) ? C3 Mo1 C10 . . 83.74(10) ? C9 Mo1 C10 . . 35.76(10) ? C2 Mo1 C8 . . 99.28(10) ? C1 Mo1 C8 . . 150.20(10) ? C3 Mo1 C8 . . 119.84(9) ? C9 Mo1 C8 . . 35.20(9) ? C10 Mo1 C8 . . 58.73(10) ? C2 Mo1 C6 . . 156.88(10) ? C1 Mo1 C6 . . 93.30(10) ? C3 Mo1 C6 . . 114.34(10) ? C9 Mo1 C6 . . 58.62(11) ? C10 Mo1 C6 . . 35.04(10) ? C8 Mo1 C6 . . 58.07(10) ? C2 Mo1 C7 . . 127.71(10) ? C1 Mo1 C7 . . 116.47(10) ? C3 Mo1 C7 . . 140.99(9) ? C9 Mo1 C7 . . 58.14(10) ? C10 Mo1 C7 . . 58.07(10) ? C8 Mo1 C7 . . 34.68(9) ? C6 Mo1 C7 . . 34.61(10) ? C1 Mo1 P1 . . 80.12(7) y C2 Mo1 P1 . . 79.50(7) y C3 Mo1 P1 . . 133.55(6) y C9 Mo1 P1 . . 134.42(7) ? C10 Mo1 P1 . . 141.31(8) ? C8 Mo1 P1 . . 99.33(7) ? C6 Mo1 P1 . . 106.98(8) ? C7 Mo1 P1 . . 85.46(7) ? C23 P1 C17 . . 101.43(10) ? C23 P1 C11 . . 105.34(11) ? C17 P1 C11 . . 102.19(11) ? C23 P1 Mo1 . . 113.94(7) ? C17 P1 Mo1 . . 118.55(8) ? C11 P1 Mo1 . . 113.67(8) ? O1 C1 Mo1 . . 172.5(2) ? O2 C2 Mo1 . . 175.3(2) ? O3 C3 C4 . . 117.9(2) ? O3 C3 Mo1 . . 120.52(18) ? C4 C3 Mo1 . . 121.58(17) ? C5 C4 C3 . . 115.1(2) ? C5 C4 H4A . . 108.5 ? C3 C4 H4A . . 108.5 ? C5 C4 H4B . . 108.5 ? C3 C4 H4B . . 108.5 ? H4A C4 H4B . . 107.5 ? C4 C5 H5A . . 109.5 ? C4 C5 H5B . . 109.5 ? H5A C5 H5B . . 109.5 ? C4 C5 H5C . . 109.5 ? H5A C5 H5C . . 109.5 ? H5B C5 H5C . . 109.5 ? C7 C6 C10 . . 107.9(3) ? C7 C6 Mo1 . . 73.13(14) ? C10 C6 Mo1 . . 70.88(15) ? C7 C6 H6 . . 125.9 ? C10 C6 H6 . . 125.9 ? Mo1 C6 H6 . . 125.9 ? C6 C7 C8 . . 108.7(3) ? C6 C7 Mo1 . . 72.26(14) ? C8 C7 Mo1 . . 71.94(14) ? C6 C7 H7 . . 125.6 ? C8 C7 H7 . . 125.6 ? Mo1 C7 H7 . . 125.6 ? C7 C8 C9 . . 107.7(3) ? C7 C8 Mo1 . . 73.38(14) ? C9 C8 Mo1 . . 70.80(14) ? C7 C8 H8 . . 126.0 ? C9 C8 H8 . . 126.0 ? Mo1 C8 H8 . . 126.0 ? C8 C9 C10 . . 108.0(3) ? C8 C9 Mo1 . . 74.01(14) ? C10 C9 Mo1 . . 72.42(14) ? C8 C9 H9 . . 125.8 ? C10 C9 H9 . . 125.8 ? Mo1 C9 H9 . . 125.8 ? C6 C10 C9 . . 107.8(3) ? C6 C10 Mo1 . . 74.08(15) ? C9 C10 Mo1 . . 71.82(14) ? C6 C10 H10 . . 125.9 ? C9 C10 H10 . . 125.9 ? Mo1 C10 H10 . . 125.9 ? C16 C11 C12 . . 118.6(2) ? C16 C11 P1 . . 121.88(18) ? C12 C11 P1 . . 119.53(18) ? C13 C12 C11 . . 121.0(2) ? C13 C12 H12 . . 119.5 ? C11 C12 H12 . . 119.5 ? C14 C13 C12 . . 118.2(3) ? C14 C13 H13 . . 120.9 ? C12 C13 H13 . . 120.9 ? F1 C14 C15 . . 118.2(3) ? F1 C14 C13 . . 118.7(3) ? C15 C14 C13 . . 123.1(2) ? C14 C15 C16 . . 118.2(2) ? C14 C15 H15 . . 120.9 ? C16 C15 H15 . . 120.9 ? C11 C16 C15 . . 121.0(2) ? C11 C16 H16 . . 119.5 ? C15 C16 H16 . . 119.5 ? C18 C17 C22 . . 118.6(2) ? C18 C17 P1 . . 119.04(18) ? C22 C17 P1 . . 122.22(18) ? C19 C18 C17 . . 120.9(2) ? C19 C18 H18 . . 119.6 ? C17 C18 H18 . . 119.6 ? C20 C19 C18 . . 118.4(2) ? C20 C19 H19 . . 120.8 ? C18 C19 H19 . . 120.8 ? F2 C20 C21 . . 118.6(3) ? F2 C20 C19 . . 118.4(3) ? C21 C20 C19 . . 123.0(2) ? C20 C21 C22 . . 118.1(2) ? C20 C21 H21 . . 121.0 ? C22 C21 H21 . . 121.0 ? C21 C22 C17 . . 121.0(2) ? C21 C22 H22 . . 119.5 ? C17 C22 H22 . . 119.5 ? C28 C23 C24 . . 118.7(2) ? C28 C23 P1 . . 124.40(18) ? C24 C23 P1 . . 116.89(17) ? C25 C24 C23 . . 120.9(2) ? C25 C24 H24 . . 119.5 ? C23 C24 H24 . . 119.5 ? C26 C25 C24 . . 118.3(2) ? C26 C25 H25 . . 120.9 ? C24 C25 H25 . . 120.9 ? C25 C26 F3 . . 118.5(2) ? C25 C26 C27 . . 123.0(2) ? F3 C26 C27 . . 118.4(2) ? C26 C27 C28 . . 118.1(2) ? C26 C27 H27 . . 120.9 ? C28 C27 H27 . . 120.9 ? C23 C28 C27 . . 120.8(2) ? C23 C28 H28 . . 119.6 ? C27 C28 H28 . . 119.6 ? C29 Mo2 C30 . . 107.12(10) y C29 Mo2 C31 . . 74.64(9) y C30 Mo2 C31 . . 73.89(9) y C29 Mo2 C38 . . 135.20(10) ? C30 Mo2 C38 . . 102.87(10) ? C31 Mo2 C38 . . 82.81(9) ? C29 Mo2 C37 . . 103.05(10) ? C30 Mo2 C37 . . 136.20(10) ? C31 Mo2 C37 . . 84.57(9) ? C38 Mo2 C37 . . 35.59(10) ? C29 Mo2 C34 . . 156.64(10) ? C30 Mo2 C34 . . 96.22(10) ? C31 Mo2 C34 . . 113.90(10) ? C38 Mo2 C34 . . 34.77(10) ? C37 Mo2 C34 . . 58.30(10) ? C29 Mo2 C36 . . 99.19(10) ? C30 Mo2 C36 . . 153.46(10) ? C31 Mo2 C36 . . 117.57(10) ? C38 Mo2 C36 . . 58.30(10) ? C37 Mo2 C36 . . 35.19(10) ? C34 Mo2 C36 . . 57.46(10) ? C29 Mo2 C35 . . 125.58(11) ? C30 Mo2 C35 . . 121.19(11) ? C31 Mo2 C35 . . 139.20(9) ? C38 Mo2 C35 . . 57.64(10) ? C37 Mo2 C35 . . 57.91(10) ? C34 Mo2 C35 . . 34.31(10) ? C36 Mo2 C35 . . 34.28(10) ? C29 Mo2 P2 . . 78.59(7) y C30 Mo2 P2 . . 78.48(7) y C31 Mo2 P2 . . 133.28(6) y C38 Mo2 P2 . . 140.53(7) ? C37 Mo2 P2 . . 139.10(7) ? C34 Mo2 P2 . . 105.85(8) ? C36 Mo2 P2 . . 103.91(7) ? C35 Mo2 P2 . . 87.44(7) ? C45 P2 C51 . . 101.62(10) ? C45 P2 C39 . . 103.92(10) ? C51 P2 C39 . . 101.68(10) ? C45 P2 Mo2 . . 113.86(7) ? C51 P2 Mo2 . . 117.18(7) ? C39 P2 Mo2 . . 116.52(7) ? O4 C29 Mo2 . . 176.6(2) ? O5 C30 Mo2 . . 176.6(2) ? O6 C31 C32 . . 117.5(2) ? O6 C31 Mo2 . . 119.32(19) ? C32 C31 Mo2 . . 123.17(17) ? C33 C32 C31 . . 115.8(2) ? C33 C32 H32A . . 108.3 ? C31 C32 H32A . . 108.3 ? C33 C32 H32B . . 108.3 ? C31 C32 H32B . . 108.3 ? H32A C32 H32B . . 107.4 ? C32 C33 H33A . . 109.5 ? C32 C33 H33B . . 109.5 ? H33A C33 H33B . . 109.5 ? C32 C33 H33C . . 109.5 ? H33A C33 H33C . . 109.5 ? H33B C33 H33C . . 109.5 ? C35 C34 C38 . . 108.2(3) ? C35 C34 Mo2 . . 73.66(16) ? C38 C34 Mo2 . . 71.04(14) ? C35 C34 H34 . . 125.7 ? C38 C34 H34 . . 125.7 ? Mo2 C34 H34 . . 125.7 ? C34 C35 C36 . . 108.8(3) ? C34 C35 Mo2 . . 72.03(15) ? C36 C35 Mo2 . . 72.80(15) ? C34 C35 H35 . . 125.5 ? C36 C35 H35 . . 125.5 ? Mo2 C35 H35 . . 125.5 ? C35 C36 C37 . . 107.5(3) ? C35 C36 Mo2 . . 72.92(15) ? C37 C36 Mo2 . . 70.28(14) ? C35 C36 H36 . . 126.2 ? C37 C36 H36 . . 126.2 ? Mo2 C36 H36 . . 126.2 ? C38 C37 C36 . . 107.3(3) ? C38 C37 Mo2 . . 72.04(14) ? C36 C37 Mo2 . . 74.53(14) ? C38 C37 H37 . . 126.0 ? C36 C37 H37 . . 126.0 ? Mo2 C37 H37 . . 126.0 ? C34 C38 C37 . . 108.1(3) ? C34 C38 Mo2 . . 74.19(15) ? C37 C38 Mo2 . . 72.36(14) ? C34 C38 H38 . . 125.7 ? C37 C38 H38 . . 125.7 ? Mo2 C38 H38 . . 125.7 ? C44 C39 C40 . . 118.5(2) ? C44 C39 P2 . . 121.51(17) ? C40 C39 P2 . . 119.86(17) ? C41 C40 C39 . . 120.9(2) ? C41 C40 H40 . . 119.5 ? C39 C40 H40 . . 119.5 ? C42 C41 C40 . . 118.4(2) ? C42 C41 H41 . . 120.8 ? C40 C41 H41 . . 120.8 ? F4 C42 C43 . . 118.2(2) ? F4 C42 C41 . . 119.0(2) ? C43 C42 C41 . . 122.8(2) ? C42 C43 C44 . . 118.3(2) ? C42 C43 H43 . . 120.8 ? C44 C43 H43 . . 120.8 ? C39 C44 C43 . . 121.1(2) ? C39 C44 H44 . . 119.5 ? C43 C44 H44 . . 119.5 ? C46 C45 C50 . . 118.8(2) ? C46 C45 P2 . . 122.54(18) ? C50 C45 P2 . . 118.68(18) ? C45 C46 C47 . . 120.7(2) ? C45 C46 H46 . . 119.6 ? C47 C46 H46 . . 119.6 ? C48 C47 C46 . . 118.2(2) ? C48 C47 H47 . . 120.9 ? C46 C47 H47 . . 120.9 ? F5 C48 C47 . . 118.4(2) ? F5 C48 C49 . . 118.4(2) ? C47 C48 C49 . . 123.2(2) ? C48 C49 C50 . . 118.0(2) ? C48 C49 H49 . . 121.0 ? C50 C49 H49 . . 121.0 ? C49 C50 C45 . . 121.1(2) ? C49 C50 H50 . . 119.4 ? C45 C50 H50 . . 119.4 ? C52 C51 C56 . . 118.7(2) ? C52 C51 P2 . . 121.43(17) ? C56 C51 P2 . . 119.85(17) ? C51 C52 C53 . . 120.9(2) ? C51 C52 H52 . . 119.6 ? C53 C52 H52 . . 119.6 ? C54 C53 C52 . . 118.2(2) ? C54 C53 H53 . . 120.9 ? C52 C53 H53 . . 120.9 ? F6 C54 C53 . . 118.2(2) ? F6 C54 C55 . . 118.7(2) ? C53 C54 C55 . . 123.1(2) ? C54 C55 C56 . . 118.0(2) ? C54 C55 H55 . . 121.0 ? C56 C55 H55 . . 121.0 ? C55 C56 C51 . . 121.1(2) ? C55 C56 H56 . . 119.4 ? C51 C56 H56 . . 119.4 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Mo1 P1 . 2.4730(6) y Mo1 C1 . 1.966(2) y Mo1 C2 . 1.965(2) y Mo1 C3 . 2.265(2) y Mo1 C9 . 2.306(2) ? Mo1 C10 . 2.314(2) ? Mo1 C8 . 2.348(2) ? Mo1 C6 . 2.355(3) ? Mo1 C7 . 2.366(2) ? P1 C23 . 1.825(2) ? P1 C17 . 1.835(2) ? P1 C11 . 1.837(2) ? F1 C14 . 1.361(3) ? F2 C20 . 1.359(3) ? F3 C26 . 1.366(3) ? O1 C1 . 1.155(3) ? O2 C2 . 1.156(3) ? O3 C3 . 1.218(3) ? C3 C4 . 1.532(3) ? C4 C5 . 1.515(4) ? C4 H4A . 0.99 ? C4 H4B . 0.99 ? C5 H5A . 0.98 ? C5 H5B . 0.98 ? C5 H5C . 0.98 ? C6 C7 . 1.404(4) ? C6 C10 . 1.406(4) ? C6 H6 . 1.0 ? C7 C8 . 1.405(4) ? C7 H7 . 1.0 ? C8 C9 . 1.408(4) ? C8 H8 . 1.0 ? C9 C10 . 1.419(4) ? C9 H9 . 1.0 ? C10 H10 . 1.0 ? C11 C16 . 1.391(3) ? C11 C12 . 1.393(3) ? C12 C13 . 1.384(4) ? C12 H12 . 0.95 ? C13 C14 . 1.373(4) ? C13 H13 . 0.95 ? C14 C15 . 1.364(4) ? C15 C16 . 1.392(3) ? C15 H15 . 0.95 ? C16 H16 . 0.95 ? C17 C18 . 1.392(3) ? C17 C22 . 1.395(3) ? C18 C19 . 1.387(4) ? C18 H18 . 0.95 ? C19 C20 . 1.371(4) ? C19 H19 . 0.95 ? C20 C21 . 1.369(4) ? C21 C22 . 1.390(3) ? C21 H21 . 0.95 ? C22 H22 . 0.95 ? C23 C28 . 1.384(3) ? C23 C24 . 1.398(3) ? C24 C25 . 1.379(3) ? C24 H24 . 0.95 ? C25 C26 . 1.366(4) ? C25 H25 . 0.95 ? C26 C27 . 1.371(4) ? C27 C28 . 1.389(3) ? C27 H27 . 0.95 ? C28 H28 . 0.95 ? Mo2 C29 . 1.962(2) y Mo2 C30 . 1.964(3) y Mo2 C31 . 2.286(2) y Mo2 C38 . 2.315(2) ? Mo2 C37 . 2.319(2) ? Mo2 C34 . 2.355(3) ? Mo2 C36 . 2.374(3) ? Mo2 C35 . 2.376(3) ? Mo2 P2 . 2.4654(6) y P2 C45 . 1.832(2) ? P2 C51 . 1.834(2) ? P2 C39 . 1.839(2) ? F4 C42 . 1.359(3) ? F5 C48 . 1.359(3) ? F6 C54 . 1.356(3) ? O4 C29 . 1.155(3) ? O5 C30 . 1.154(3) ? O6 C31 . 1.196(3) ? C31 C32 . 1.511(3) ? C32 C33 . 1.506(4) ? C32 H32A . 0.99 ? C32 H32B . 0.99 ? C33 H33A . 0.98 ? C33 H33B . 0.98 ? C33 H33C . 0.98 ? C34 C35 . 1.396(4) ? C34 C38 . 1.396(4) ? C34 H34 . 1.0 ? C35 C36 . 1.400(4) ? C35 H35 . 1.0 ? C36 C37 . 1.420(4) ? C36 H36 . 1.0 ? C37 C38 . 1.416(4) ? C37 H37 . 1.0 ? C38 H38 . 1.0 ? C39 C44 . 1.388(3) ? C39 C40 . 1.397(3) ? C40 C41 . 1.388(3) ? C40 H40 . 0.95 ? C41 C42 . 1.371(4) ? C41 H41 . 0.95 ? C42 C43 . 1.368(3) ? C43 C44 . 1.391(3) ? C43 H43 . 0.95 ? C44 H44 . 0.95 ? C45 C46 . 1.386(3) ? C45 C50 . 1.400(3) ? C46 C47 . 1.391(3) ? C46 H46 . 0.95 ? C47 C48 . 1.367(3) ? C47 H47 . 0.95 ? C48 C49 . 1.376(3) ? C49 C50 . 1.376(3) ? C49 H49 . 0.95 ? C50 H50 . 0.95 ? C51 C52 . 1.389(3) ? C51 C56 . 1.393(3) ? C52 C53 . 1.395(3) ? C52 H52 . 0.95 ? C53 C54 . 1.365(4) ? C53 H53 . 0.95 ? C54 C55 . 1.375(4) ? C55 C56 . 1.387(3) ? C55 H55 . 0.95 ? C56 H56 . 0.95 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C15 H15 O6 . 0.95 2.59 3.371(4) 139.4 y C49 H49 F4 1_655 0.95 2.55 3.344(3) 141.3 y C55 H55 O3 1_455 0.95 2.53 3.450(3) 164.3 y C34 H34 O1 4_566 1.00 2.38 3.237(3) 142.8 y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O3 C3 C4 C5 . . . . -6.1(3) ? Mo1 C3 C4 C5 . . . . 172.61(18) y C10 C6 C7 C8 . . . . -0.4(3) ? Mo1 C6 C7 C8 . . . . -63.15(17) ? C10 C6 C7 Mo1 . . . . 62.78(18) ? C6 C7 C8 C9 . . . . 0.4(3) ? Mo1 C7 C8 C9 . . . . -62.91(17) ? C6 C7 C8 Mo1 . . . . 63.36(18) ? C7 C8 C9 C10 . . . . -0.4(3) ? Mo1 C8 C9 C10 . . . . -64.96(17) ? C7 C8 C9 Mo1 . . . . 64.60(17) ? C7 C6 C10 C9 . . . . 0.1(3) ? Mo1 C6 C10 C9 . . . . 64.39(17) ? C7 C6 C10 Mo1 . . . . -64.24(18) ? C8 C9 C10 C6 . . . . 0.1(3) ? Mo1 C9 C10 C6 . . . . -65.88(18) ? C8 C9 C10 Mo1 . . . . 66.01(18) ? C23 P1 C11 C16 . . . . 108.3(2) ? C17 P1 C11 C16 . . . . 2.7(2) ? Mo1 P1 C11 C16 . . . . -126.24(18) ? C23 P1 C11 C12 . . . . -73.3(2) ? C17 P1 C11 C12 . . . . -178.9(2) ? Mo1 P1 C11 C12 . . . . 52.1(2) ? C16 C11 C12 C13 . . . . -1.7(4) ? P1 C11 C12 C13 . . . . 179.8(2) ? C11 C12 C13 C14 . . . . 1.4(4) ? C12 C13 C14 F1 . . . . 179.4(3) ? C12 C13 C14 C15 . . . . -0.1(5) ? F1 C14 C15 C16 . . . . 179.8(2) ? C13 C14 C15 C16 . . . . -0.7(4) ? C12 C11 C16 C15 . . . . 0.9(4) ? P1 C11 C16 C15 . . . . 179.29(19) ? C14 C15 C16 C11 . . . . 0.3(4) ? C23 P1 C17 C18 . . . . 164.88(19) ? C11 P1 C17 C18 . . . . -86.5(2) ? Mo1 P1 C17 C18 . . . . 39.3(2) ? C23 P1 C17 C22 . . . . -19.6(2) ? C11 P1 C17 C22 . . . . 89.0(2) ? Mo1 P1 C17 C22 . . . . -145.17(17) ? C22 C17 C18 C19 . . . . -1.2(4) ? P1 C17 C18 C19 . . . . 174.5(2) ? C17 C18 C19 C20 . . . . 2.4(4) ? C18 C19 C20 F2 . . . . 178.9(2) ? C18 C19 C20 C21 . . . . -1.1(4) ? F2 C20 C21 C22 . . . . 178.5(2) ? C19 C20 C21 C22 . . . . -1.5(4) ? C20 C21 C22 C17 . . . . 2.8(4) ? C18 C17 C22 C21 . . . . -1.5(4) ? P1 C17 C22 C21 . . . . -176.99(19) ? C17 P1 C23 C28 . . . . 121.0(2) ? C11 P1 C23 C28 . . . . 14.8(2) ? Mo1 P1 C23 C28 . . . . -110.42(19) ? C17 P1 C23 C24 . . . . -59.7(2) ? C11 P1 C23 C24 . . . . -165.84(18) ? Mo1 P1 C23 C24 . . . . 68.90(19) ? C28 C23 C24 C25 . . . . -0.9(4) ? P1 C23 C24 C25 . . . . 179.73(19) ? C23 C24 C25 C26 . . . . 2.5(4) ? C24 C25 C26 F3 . . . . 177.5(2) ? C24 C25 C26 C27 . . . . -2.2(4) ? C25 C26 C27 C28 . . . . 0.4(4) ? F3 C26 C27 C28 . . . . -179.3(2) ? C24 C23 C28 C27 . . . . -1.0(3) ? P1 C23 C28 C27 . . . . 178.31(18) ? C26 C27 C28 C23 . . . . 1.3(4) ? O6 C31 C32 C33 . . . . -4.5(4) ? Mo2 C31 C32 C33 . . . . 173.63(19) y C38 C34 C35 C36 . . . . 0.9(3) ? Mo2 C34 C35 C36 . . . . 63.96(19) ? C38 C34 C35 Mo2 . . . . -63.05(18) ? C34 C35 C36 C37 . . . . -1.3(3) ? Mo2 C35 C36 C37 . . . . 62.17(18) ? C34 C35 C36 Mo2 . . . . -63.47(18) ? C35 C36 C37 C38 . . . . 1.2(3) ? Mo2 C36 C37 C38 . . . . 65.08(17) ? C35 C36 C37 Mo2 . . . . -63.90(18) ? C35 C34 C38 C37 . . . . -0.2(3) ? Mo2 C34 C38 C37 . . . . -64.91(17) ? C35 C34 C38 Mo2 . . . . 64.75(19) ? C36 C37 C38 C34 . . . . -0.6(3) ? Mo2 C37 C38 C34 . . . . 66.12(18) ? C36 C37 C38 Mo2 . . . . -66.75(17) ? C45 P2 C39 C44 . . . . 105.6(2) ? C51 P2 C39 C44 . . . . 0.4(2) ? Mo2 P2 C39 C44 . . . . -128.27(18) ? C45 P2 C39 C40 . . . . -79.0(2) ? C51 P2 C39 C40 . . . . 175.70(19) ? Mo2 P2 C39 C40 . . . . 47.1(2) ? C44 C39 C40 C41 . . . . 0.4(4) ? P2 C39 C40 C41 . . . . -175.1(2) ? C39 C40 C41 C42 . . . . 1.6(4) ? C40 C41 C42 F4 . . . . 176.8(2) ? C40 C41 C42 C43 . . . . -2.8(4) ? F4 C42 C43 C44 . . . . -177.7(2) ? C41 C42 C43 C44 . . . . 1.9(4) ? C40 C39 C44 C43 . . . . -1.3(4) ? P2 C39 C44 C43 . . . . 174.10(19) ? C42 C43 C44 C39 . . . . 0.2(4) ? C51 P2 C45 C46 . . . . 101.2(2) ? C39 P2 C45 C46 . . . . -4.1(2) ? Mo2 P2 C45 C46 . . . . -131.89(18) ? C51 P2 C45 C50 . . . . -78.1(2) ? C39 P2 C45 C50 . . . . 176.65(19) ? Mo2 P2 C45 C50 . . . . 48.9(2) ? C50 C45 C46 C47 . . . . -0.7(3) ? P2 C45 C46 C47 . . . . -179.96(18) ? C45 C46 C47 C48 . . . . -0.2(4) ? C46 C47 C48 F5 . . . . -177.3(2) ? C46 C47 C48 C49 . . . . 1.2(4) ? F5 C48 C49 C50 . . . . 177.4(2) ? C47 C48 C49 C50 . . . . -1.2(4) ? C48 C49 C50 C45 . . . . 0.1(4) ? C46 C45 C50 C49 . . . . 0.8(4) ? P2 C45 C50 C49 . . . . -179.95(19) ? C45 P2 C51 C52 . . . . -10.9(2) ? C39 P2 C51 C52 . . . . 96.2(2) ? Mo2 P2 C51 C52 . . . . -135.61(17) ? C45 P2 C51 C56 . . . . 171.36(19) ? C39 P2 C51 C56 . . . . -81.6(2) ? Mo2 P2 C51 C56 . . . . 46.6(2) ? C56 C51 C52 C53 . . . . -0.5(3) ? P2 C51 C52 C53 . . . . -178.30(18) ? C51 C52 C53 C54 . . . . 0.4(4) ? C52 C53 C54 F6 . . . . 179.7(2) ? C52 C53 C54 C55 . . . . 0.2(4) ? F6 C54 C55 C56 . . . . 179.9(2) ? C53 C54 C55 C56 . . . . -0.6(4) ? C54 C55 C56 C51 . . . . 0.5(4) ? C52 C51 C56 C55 . . . . 0.1(3) ? P2 C51 C56 C55 . . . . 177.88(19) ? _cod_database_fobs_code 2243896