#------------------------------------------------------------------------------
#$Date: 2021-09-08 05:05:53 +0300 (Wed, 08 Sep 2021) $
#$Revision: 269046 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/24/39/2243911.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2243911
loop_
_publ_author_name
'Turgunov, Kambarali'
'Ziyadullaev, Mirjalol'
'Khoshimov, Farkhod'
'Karimov, Rikhsiboy'
'Elmuradov, Burkhon'
_publ_section_title
;
 Crystal structures of 6-nitroquinazolin-4(3<i>H</i>)-one,
 6-aminoquinazolin-4(3<i>H</i>)-one and 4-aminoquinazoline
 hemihydrochloride dihydrate
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2056989021008823
_journal_volume                  77
_journal_year                    2021
_chemical_formula_iupac          'C8 H8 N3 +, Cl -, C8 H7 N3, 2H2 O'
_chemical_formula_moiety         'C8 H8 N3 +, Cl -, C8 H7 N3, 2(H2 O)'
_chemical_formula_sum            'C16 H19 Cl N6 O2'
_chemical_formula_weight         362.82
_chemical_name_common
'bis(Hemi-4-aminoquinazoline)chloride dihydrate'
_chemical_name_systematic
;
4-Aminoquinazolin-1-ium chloride--4-aminoquinazoline--water (1/1/2)
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 93.544(7)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.3512(12)
_cell_length_b                   7.5867(6)
_cell_length_c                   16.2282(9)
_cell_measurement_reflns_used    1071
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      71.1960
_cell_measurement_theta_min      3.9830
_cell_volume                     1763.5(2)
_computing_cell_refinement
;
CrysAlisPro (Rigaku OD, 2018)
;
_computing_data_collection
;
CrysAlisPro (Rigaku OD, 2018)
;
_computing_data_reduction
;
CrysAlisPro (Rigaku OD, 2018)
;
_computing_molecular_graphics
;
XP in SHELXTL (Sheldrick, 2008)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement
;
<i>SHELXL2014/7</i> (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT2018/2</i> (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      298(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 10.2576
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.967
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'Rigaku Xcalibur, Ruby'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0520
_diffrn_reflns_av_unetI/netI     0.0681
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            6703
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         75.799
_diffrn_reflns_theta_min         3.992
_diffrn_source                   'Enhance (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    2.118
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.93394
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2018)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.367
_exptl_crystal_description       needle
_exptl_crystal_F_000             760
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.231
_refine_diff_density_min         -0.215
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.005
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     261
_refine_ls_number_reflns         3563
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      1.004
_refine_ls_R_factor_all          0.0931
_refine_ls_R_factor_gt           0.0541
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0514P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1258
_refine_ls_wR_factor_ref         0.1505
_reflns_number_gt                2207
_reflns_number_total             3563
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            dj2030sup1.cif
_cod_data_source_block           III
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2243911
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
   0   0   2 196770. 2184.67   3
   0   0   3 47.3425 97.0196   3
   0   0   4 103058. 2277.60   3
   0   0   5-239.241 238.017   3
   0   0   6 60259.3 2183.49   3
   0   0   7 189.737 249.877   3
   0   0  -7 382.577 319.182   1
   0   0  -8-18.4385 247.629   1
   0   0   8 289.802 382.704   3
   0   0   9-399.661 343.622   3
   0   0  -9 29.0230 232.738   1
   0   0 -10 17708.9 1652.92   1
   0   0 -11-362.561 293.990   1
   0   0  12 12123.3 745.803  12
   0   0  12 12885.2 758.079  11
   0   0  13-83.1071 131.387  11
   0   0  13 120.167 106.792  13
   0   0  13-97.8557 130.006  12
   0   0  14 679.068 232.213  11
   0   0  14 887.372 244.621  12
   0   0  14 991.914 227.691  13
   0   0  15-194.597 183.204  12
   0   0  15 36.8478 157.341  11
   0   0  16 81.4710 124.761  12
   0   0  16 352.347 187.633  11
   0   0  17-52.3669 144.566  11
   0   0  17 16.4741 139.226  12
   0   0  18-144.766 126.397  11
   0   0  18 52.0439 125.569  12
   0   0  19-61.2880 99.1853  11
   0   1   0 341.969 107.268   2
   0   1   1 1290.16 164.091   3
   0   1   1 1332.56 200.512   2
   0  -1  -2 19.0599 54.8266   1
   0   1   2-98.4541 78.9368   3
   0   1   3 21491.9 899.364   3
   0  -1  -3 20273.9 680.608   1
   0   1   4 2119.19 373.198   3
   0  -1  -4 1586.61 241.928   1
   0  -1   4 1564.49 340.108   3
   0   1   5 47795.1 1787.66   3
   0  -1   5 45550.6 1792.74   3
   0  -1  -5 44266.2 1452.77   1
   0   1   6 4288.84 604.542   3
   0  -1  -6 3754.09 511.683   1
   0  -1  -7 4238.92 606.675   1
   0   1   7 4222.97 641.517   3
   0  -1  -8 760.914 362.670   1
   0   1   8 121.993 219.415   3
   0   1   9 12343.1 1311.99   3
   0   1 -10-46.3613 396.545   1
   0   1  10-44.6110 251.982   3
   0   1 -11 6335.75 1152.83   1
   0   1 -12 11850.1 1612.43   1
   0  -1  12 11463.9 729.242  11
   0   1  12 11544.8 722.514  12
   0  -1  12 12029.1 724.121  13
   0   1  12 11932.5 740.788  11
   0  -1  12 12288.5 758.952  12
   0   1  13 116.285 105.907  12
   0  -1  13-68.7045 122.811  12
   0   1  13 127.040 111.150  13
   0  -1  13 37.4862 126.431  11
   0  -1  13 189.166 148.602  13
   0   1 -13 532.605 411.259   1
   0   1  13 282.647 174.101  11
   0  -1  14 93.2478 129.087  11
   0  -1  14-191.758 119.586  12
   0  -1  14-24.2339 174.075  13
   0   1  14 358.589 178.177  12
   0   1  14-2.16672 154.248  11
   0  -1  15 2727.50 387.114  11
   0   1  15 3075.85 415.727  11
   0   1  15 2560.21 366.437  12
   0  -1  15 2947.12 412.039  12
   0   1  16 539.578 215.495  11
   0  -1  16 842.445 237.909  12
   0  -1  16 681.792 188.094  11
   0   1  16 520.650 186.401  12
   0   1  17 629.572 214.688  11
   0  -1  17 988.790 251.208  12
   0  -1  17 686.794 201.315  11
   0   1  17 893.939 222.432  12
   0  -1  18 302.103 167.835  12
   0  -1  18 424.457 181.890  11
   0  -1  19 6440.08 440.225  12
   0  -1  19 7496.07 472.549  11
   0   2   0 326830. 4326.21   2
   0   2   1 1793.20 369.876   2
   0   2   1 1914.46 272.613   3
   0   2  -1 1689.20 353.120   2
   0   2   2 36912.5 1434.31   2
   0   2   2 38974.4 1133.48   3
   0   2   3 37152.8 1250.47   3
   0   2   4 1375.74 319.065   3
   0   2   5 93508.9 2526.40   3
   0   2   6 8031.76 828.846   3
   0   2   7 83935.1 2871.60   3
   0   2   8 13233.8 1246.53   3
   0   2   9 553.971 354.408   3
   0   2  10 488.224 368.095   3
   0   2  11 8088.47 1177.82   3
   0   2 -11 6556.56 1207.49   1
   0   2 -12 1293.13 575.939   1
   0   2  12 1801.09 320.197  11
   0  -2  12 1904.18 327.900  13
   0  -2  12 2064.03 344.415  12
   0   2  12 2230.47 332.140  12
   0   2  13 2620.08 367.661  11
   0  -2  13 2506.26 361.535  12
   0   2  13 3112.26 392.842  12
   0  -2  13 2916.78 406.139  13
   0   2  14 5333.79 535.733  11
   0  -2  14 5296.85 548.819  12
   0  -2  14 5262.48 519.069  13
   0   2  14 5425.87 514.322  12
   0  -2  14 5647.06 555.149  11
   0   2  15 10483.1 697.158  12
   0  -2  15 10175.3 737.606  12
   0  -2  15 10118.5 721.429  11
   0   2  15 9598.38 707.457  11
   0  -2  16 451.877 203.597  12
   0   2  16 613.043 200.396  11
   0  -2  16 612.647 206.332  11
   0  -2  17 197.200 176.185  12
   0  -2  17 114.301 131.238  11
   0  -2  18-35.4646 108.707  11
   0  -2  18 0.94368 118.306  12
   0  -2  19 143.962 77.6781  11
   0  -2  19-31.9189 96.4172  12
   0   3   0 145.321 258.823   2
   0   3   0 128.520 160.212   3
   0   3   1 1826.91 465.875   2
   0   3   1 1517.38 251.610   3
   0   3  -1 1287.44 440.347   2
   0   3   2 4801.84 451.152   3
   0   3  -2 4099.24 673.614   2
   0   3   2 4616.15 686.285   2
   0   3  -3 602.887 317.996   2
   0   3   3 1018.06 263.627   3
   0   3   4 3141.88 435.654   3
   0   3  -4 1963.51 510.514   2
   0   3  -5 6750.49 894.053   2
   0   3   5 6237.55 673.992   3
   0   3   6 851.875 284.087   3
   0   3  -6 941.156 407.211   2
   0   3  -7 3146.74 616.307   2
   0   3   7 3081.08 579.915   3
   0   3   8 9128.00 1060.16   3
   0   3  -8 9366.29 1168.55   2
   0   3  -9 378.393 389.806   2
   0   3   9-482.068 307.136   3
   0   3  10 717.696 232.429  11
   0   3  10 1044.57 371.292   3
   0  -3  11 3102.07 387.675  13
   0   3 -11 3310.12 957.001   1
   0   3  11 3465.92 414.784  11
   0  -3  11 3715.16 428.485  12
   0  -3  12 19605.9 977.484  13
   0  -3  12 21283.8 1043.56  12
   0   3 -12 19971.3 2340.46   1
   0  -3  13 3050.45 393.858  13
   0  -3  13 3183.54 428.012  12
   0  -3  14 86.7390 165.122  12
   0  -3  15 1238.14 295.742  12
   0  -3  15 1627.49 315.644  11
   0  -3  16 294.697 143.557  11
   0  -3  16 276.466 192.763  12
   0  -3  17 520.531 145.432  11
   0  -3  17 653.952 201.007  12
   0  -3  18 390.175 154.939  12
   0  -3  18 61.9218 96.2000  11
   0  -3  19 111.773 87.9282  12
   0   4   0 43892.6 2459.14   2
   0   4  -1 202.070 425.408   2
   0   4   1 119.923 337.546   2
   0   4  -2 3304.35 707.347   2
   0   4  -3 116.747 281.836   2
   0   4  -4 7365.23 1048.07   2
   0   4  -5 1615.38 578.320   2
   0   4  -6 220.018 340.179   2
   0   4  -7 21105.5 1915.18   2
   0   4  -8 268.905 450.575   2
   0  -4   9 1345.42 286.023  12
   0   4  -9 1321.67 541.627   2
   0  -4   9 1497.61 249.060  13
   0   4 -10 10993.2 1724.98   1
   0  -4  10 11183.0 726.657  12
   0  -4  11 2660.60 374.586  12
   0   4 -11 2060.01 793.679   1
   0  -4  12 13411.5 828.419  12
   0  -4  12 14184.5 810.557  14
   0  -4  13 1584.93 304.484  12
   0  -4  13 1728.34 279.776  14
   0  -4  14 549.159 220.048  12
   0  -4  15 107.141 142.979  12
   0  -4  15-60.2100 133.153  11
   0  -4  16 1397.73 247.378  11
   0  -4  16 1824.68 282.442  12
   0  -4  17 66.0616 114.959  12
   0  -4  17 169.508 102.421  11
   0  -4  18 4.50527 64.8952  12
   0  -4  18 108.954 70.7801  11
   0   5   0 131.336 395.066   2
   0   5  -1 1321.81 614.923   2
   0   5  -2-98.7569 372.552   2
   0   5  -3-140.314 430.216   2
   0   5  -4-32.1771 356.996   2
   0   5  -5 224.890 313.390   2
   0   5   6 1501.05 272.683  10
   0   5  -6 754.295 430.452   2
   0   5   7 4279.17 439.802  10
   0   5  -7 4055.35 949.358   2
   0   5  -8-378.483 386.649   2
   0   5   8 268.923 162.601  10
   0   5   9-22.6635 120.616  10
   0  -5   9 25.7409 146.909  12
   0  -5  10 2239.23 339.592  12
   0   5  10 1489.25 278.458  10
   0   5  10 2117.59 325.612   6
   0  -5  11 320.422 155.437  14
   0  -5  11 647.435 173.814  12
   0  -5  12 305.382 172.286  14
   0  -5  12 96.1982 142.444  12
   0  -5  13 3328.71 375.711  14
   0  -5  13 3742.68 420.613  12
   0  -5  14 94.1102 93.7944  14
   0  -5  14-114.526 112.261  12
   0  -5  15 331.776 137.110  11
   0  -5  15 260.467 118.975  12
   0  -5  16 850.092 147.878  12
   0  -5  16 1244.52 183.550  11
   0   6   0 385.431 170.782   6
   0   6  -1 2154.72 327.106   6
   0   6   2 1019.15 239.106  10
   0   6  -2 1619.97 272.257   6
   0   6  -3 1374.49 461.907   2
   0   6   3 1217.01 265.229  10
   0   6  -4 2323.01 731.462   2
   0   6   4 3252.75 407.186  10
   0   6  -5 17924.4 2130.16   2
   0   6   5 16792.5 890.255  10
   0   6   6 5217.72 506.674  10
   0   6   7 190.158 136.817  10
   0   6   7 152.943 169.722   6
   0   6   8 666.920 204.697   6
   0   6   9 64.1242 146.355   6
   0   6  10-76.2730 119.457   6
   0   6  11 471.636 164.163   6
   0  -6  11 940.907 254.053  14
   0  -6  12 146.052 140.974  14
   0  -6  13 228.767 128.453  14
   0  -6  14 1083.96 195.118  11
   0  -6  14 1207.09 176.714  14
   0  -6  15 480.403 110.662  11
   0   7   0 425.494 211.292   6
   0   7   1 260.467 205.834   6
   0   7  -1 56.5164 127.567   6
   0   7  -2 64.4100 104.373   6
   0   7   2 257.080 172.168   6
   0   7   3 456.837 214.234   6
   0   7   4 162.795 169.583   6
   0   7   5 128.424 144.116   6
   0   7   6-44.9336 136.678   6
   0   7   7 512.931 174.863   6
   0   7   8 546.573 182.959   6
   0   7   9 285.149 153.378   6
   0  -7  10-19.7652 113.881  14
   0   7  10 175.679 132.831   6
   0   7  11 583.363 153.047   6
   0  -7  11 800.681 192.381  14
   0  -7  12-212.520 131.712  14
   0  -7  13 6.25454 63.3044  14
   0   8   0 1440.96 275.423   6
   0   8  -1 404.914 181.245   6
   0   8   1 577.721 182.533   6
   0   8   2 27.5420 154.862   6
   0   8  -2 203.862 155.092   6
   0   8   3 892.272 220.808   6
   0   8   4 2277.57 319.669   6
   0   8   5 1030.09 234.884   6
   0   8   6 333.122 175.940   6
   0   8   7 143.872 121.115   6
   0  -8   7 147.422 154.850  14
   0   8   8 377.368 165.818   6
   0  -8   8 343.121 166.799  14
   0  -8   9 139.622 103.037  14
   0   8   9 249.529 119.375   6
   0   8   9-122.339 107.039   7
   0  -8  10 121.101 91.3010  14
   0   9   0-70.2236 127.156   7
   0   9  -1 201.086 125.310   7
   0   9  -2 162.476 112.967   7
   0  -9   2 168.324 82.8941  14
   0  -9   3-0.80669 69.2072  14
   0  -9   4-68.5327 86.4519  14
   0   9   4-273.646 127.631   7
   0   9   5 44.8193 91.5779   7
   0  -9   5-172.039 91.9637  14
   0  -9   6 51.4980 70.8983  14
   0   9   6 174.953 93.6989   7
  -1   0  19 851.215 182.252  12
  -1   0  18 126.135 113.365  12
  -1   0  18-223.679 136.234  11
  -1   0  17 474.036 186.092  11
  -1   0  17 40.6102 145.606  12
  -1   0  16 152.323 133.180  11
  -1   0  16-123.401 143.714  12
  -1   0  15 25851.7 1152.56  11
  -1   0  15 26009.5 1113.49  13
  -1   0  15 24481.4 1106.61  12
  -1   0  14 36.9465 165.063  13
  -1   0  14-61.3011 154.858  12
  -1   0  14 170.925 158.247  11
  -1   0  13 19188.9 963.851  11
  -1   0  13 19377.3 942.365  13
  -1   0  13 19478.5 965.171  12
  -1   0  12-3.76159 100.197  11
  -1   0  12 45.8207 126.254  12
  -1   0  11 23914.9 2051.00   3
   1   0 -11 21900.3 1883.23   1
  -1   0  10 1086.65 531.835   3
   1   0 -10 129.103 232.378   1
  -1   0   9 49967.6 2574.64   3
   1   0  -9 48455.3 2494.61   1
  -1   0   8 60.9141 239.282   3
  -1   0   7 12689.4 1141.14   3
  -1   0   6 22.6035 218.143   3
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   1   1   6 5733.26 682.030   3
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   1   2 -13 1401.32 557.582   1
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   1   2 -12 23147.5 2368.32   1
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   1   2   0 236569. 1736.18   3
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   1   2   1 74058.9 868.969   3
   1   2   1 78599.4 2056.38   2
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   1   2  14 10449.0 755.646  11
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   1   3  -1 21706.1 1437.38   2
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   1   3   3 18820.8 1266.57   2
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   1   3   5 11618.7 849.361   3
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   1   3   6 4205.67 566.338   3
   1   3   7 38241.3 1904.03   3
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   1   3   8 3084.03 597.328   3
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   1   3  10 2026.68 313.096  11
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   1  -3  11 10518.2 687.151  13
   1   3  11 10137.8 701.016  11
   1  -3  11 10449.5 661.656  14
   1  -3  12 6519.79 585.434  12
   1   3  12 5752.67 552.187  11
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   1  -3  12 7003.89 549.538  14
   1  -3  13 1993.93 327.665  12
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   1  -3  15 4295.21 467.647  11
   1  -3  16 4395.75 437.780  12
   1  -3  16 4437.74 452.902  11
   1  -3  17 3554.90 365.144  12
   1  -3  17 3780.12 382.841  11
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   1   4  -8-500.345 483.769   2
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   1   4  -6 9623.44 1296.23   2
   1   4  -5 6137.86 978.754   2
   1   4  -4 4962.59 867.239   2
   1   4  -3 465.689 392.475   2
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   1   4  -1 5774.33 920.705   2
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   1   4   1 5036.19 822.065   2
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   1   4   9 276.697 155.111  10
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   1  -4  10 1249.66 228.822  12
   1   4  10 1773.89 267.484  10
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   1  -4  12 1856.31 318.586  12
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   1  -4  13 556.201 216.331  12
   1  -4  13 666.994 182.675  14
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   1  -4  15 20.9273 136.666  12
   1  -4  15 180.670 128.340  11
   1  -4  16 219.135 131.537  12
   1  -4  16 448.803 169.878  11
   1  -4  17-31.1773 84.1101  12
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  -1   5   8 4909.31 477.844   6
  -1  -5   7 4326.80 443.636  12
  -1   5   7 4019.83 431.522  10
  -1   5   6 3337.84 383.972  10
   1   5  -6 3568.76 873.388   2
   1   5  -5 863.316 602.339   2
   1   5  -4 3370.49 818.086   2
   1   5  -3 682.146 459.965   2
   1   5  -2 6002.06 1115.89   2
   1   5  -1 2226.10 726.532   2
   1   5   0 805.757 434.751   2
   1   5   1 3888.86 785.000   2
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  -1   5  -6 127.275 403.076   1
  -1   5  -6 141.876 422.922   2
   1   5   6 438.991 159.860  10
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   1   5   7 284.689 145.220  10
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  -1   5  -8 3212.59 871.671   2
   1   5   8 1751.79 308.416  10
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   1  -9   4 56.6284 82.0744  14
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   1   9   5 37.5005 89.1925   7
   1   9   5 178.913 91.5325   6
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   2   0  13 54.1223 149.845  12
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   2   1   3 22274.4 620.034   2
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   2   1  12 2684.07 363.733  12
   2  -1  12 3034.63 384.757  12
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   2   1  12 2866.66 376.870  11
   2  -1  13 4303.16 474.438  12
   2   1  13 4908.03 509.779  11
   2   1  13 4577.97 474.814  12
   2  -1  13 3963.92 458.165  11
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   2   1  14 605.182 217.500  12
   2  -1  14 619.323 213.619  11
   2   1  14 414.904 200.501  11
   2  -1  14 905.581 242.073  12
   2   1  15 1393.94 291.571  12
   2  -1  15 1239.06 276.573  11
   2  -1  15 1477.85 299.120  12
   2   1  15 1602.69 300.713  11
   2  -1  16 372.334 189.474  11
   2   1  16 198.144 129.033  12
   2  -1  16 62.6200 144.747  12
   2   1  16 364.097 171.343  11
   2   1  17 290.373 181.190  11
   2  -1  17 212.819 173.916  11
   2  -1  17 373.789 194.786  12
   2  -1  18 161.627 153.342  11
   2  -1  18 183.244 172.039  12
   2   1  18 286.313 141.844  11
   2  -1  19 3093.31 308.842  11
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   2   2 -13 1810.10 686.888   1
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  -2   2   8 28674.7 1923.12   3
  -2   2   7 29465.9 1822.54   3
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  -2   2   6 18491.8 1334.42   3
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  -2   2   5 864.288 325.862   3
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  -2   2   4 65.4672 232.047   3
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  -2   2   2 79906.8 1112.47   1
  -2   2   1 999999. 5773.45   1
  -2   2   1 986521. 8409.76   3
  -2   2   0 511817. 4923.06   1
  -2   2  -1 378255. 4747.23   1
  -2   2  -1 371543. 5035.26   2
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   2   2   2 6516.21 589.777   2
  -2   2  -3 4202.39 583.922   2
   2   2   3 5401.03 527.079   2
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  -2   2  -8 10941.9 1392.22   1
  -2   2  -9 31637.9 2472.96   1
  -2   2 -10 456.908 443.060   1
   2   2  11 6863.95 554.804  11
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   2  -2  11 7233.64 583.392  12
   2   2  11 6857.56 557.161  12
   2  -2  12 574.679 214.866  12
   2   2  12 420.830 153.678  12
   2   2  12 331.571 176.569   9
   2   2  12 291.266 161.489  11
   2   2  13-49.9567 153.677  12
   2  -2  13-266.644 170.564  12
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   2   2  13 104.988 189.894  11
   2   2  14 127.453 138.382  11
   2   2  14 77.3721 133.218  12
   2  -2  14 99.5264 133.315  12
   2  -2  14 54.8372 137.232  11
   2   2  15 6648.11 582.628  11
   2  -2  15 6647.68 593.647  11
   2  -2  15 6412.22 568.569  12
   2  -2  16 919.723 244.924  11
   2   2  16 1163.42 276.836  11
   2  -2  16 957.190 265.977  12
   2  -2  17 916.392 202.574  11
   2  -2  17 817.954 210.434  12
   2  -2  18 362.711 137.900  12
   2  -2  18 459.156 153.122  11
   2  -2  19 929.203 169.864  11
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  -2  -3  15 272.885 138.204  11
  -2  -3  15 298.647 164.314  13
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   2   3   1 24544.1 1476.64   2
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   2   4 -10 6632.51 1214.10   2
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   2   4   9 1030.02 224.823  10
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   2  -4  14 9670.17 643.839  12
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   2   5  -8 4829.69 1147.94   2
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   2   5  -7 1613.08 493.104   2
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   2   5  -5 3562.03 872.801   2
   2   5  -4 4175.33 928.085   2
   2   5  -3 10513.5 1422.32   2
   2   5  -2 1803.86 688.462   2
   2   5  -1 12206.9 1474.82   2
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   2   5   2 3014.16 816.569   2
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   2   5   5 1643.06 255.009  10
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   2   5   6 371.500 184.763  10
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   2   5   7 1203.38 258.799  10
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   2   6  -2 356.656 472.667   2
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   2   8   4 288.454 191.083   6
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   2   8   5 928.367 215.802   6
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   2   8   6 1511.93 267.603   6
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   2   9   2 68.3405 106.971   6
   2   9   3 121.737 102.615   6
   2   9   4 31.3851 89.7351   6
   2   9   5 60.1391 81.6484   6
   2   9   6 102.403 83.4256   6
   2   9   6-132.381 81.9507   7
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   3   0  12 173.448 136.943   9
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   3   0  12 50.1375 112.034  11
   3   0  12-94.1813 131.940  12
   3   0  13 201.495 172.099  12
   3   0  13 218.137 166.562  11
   3   0  13-59.2731 99.7830   9
   3   0  14 121.022 135.005   9
   3   0  14 47.7760 130.510  11
   3   0  14 128.943 156.881  12
   3   0  15 10256.3 721.224  12
   3   0  15 9991.66 730.118  11
   3   0  16 61.9759 143.596  11
   3   0  16 101.221 133.893  12
   3   0  17 701.816 215.829  11
   3   0  17 600.870 219.509  12
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  -3   1  13 873.844 214.650  13
  -3   1  13 611.340 179.964  11
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  -3   1  13 789.844 214.872  12
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  -3   1  12 5043.72 479.725  11
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  -3   1  11 2952.82 757.732   3
  -3   1  10 12768.5 1485.21   3
  -3  -1  10 12060.3 1410.33   3
  -3  -1   9 2214.83 634.806   3
  -3   1   9 2466.78 624.099   3
  -3  -1   8 23112.1 1698.33   3
  -3   1   8 24523.0 1796.83   3
  -3  -1   7 204.374 278.494   3
  -3   1   7 401.719 247.452   3
  -3   1   6-58.4301 222.149   3
  -3  -1   6 139.165 310.329   3
  -3  -1   5 16873.1 1140.72   3
  -3   1   5 17384.0 1253.19   3
  -3  -1   4 1033.46 275.212   3
  -3   1   4 751.287 334.213   3
  -3   1   3 26990.8 1374.60   3
  -3  -1   3 28602.5 1174.16   3
  -3  -1   2 466.145 165.898   3
  -3   1   2 791.503 348.027   3
  -3   1   1 18682.8 954.672   1
  -3  -1   1 21204.7 792.095   3
  -3   1   0 1817.04 324.638   1
  -3  -1   0 1347.26 225.518   3
  -3  -1  -1 52985.7 1881.79   1
  -3   1  -1 52962.9 1808.08   1
  -3   1  -2 373.586 230.800   1
  -3  -1  -2 243.080 223.920   1
  -3   1  -3 28884.5 1559.89   1
  -3  -1  -3 28829.9 1517.98   1
  -3  -1  -4 422.194 250.943   1
  -3   1  -4 198.567 280.611   1
  -3  -1  -5 8350.55 897.190   1
  -3   1  -5 9049.14 1062.19   1
  -3  -1  -6 31398.7 1872.29   1
  -3   1  -6 31078.6 1988.78   1
  -3   1  -7 1920.79 571.022   1
  -3  -1  -7 1892.58 515.192   1
  -3   1  -8 37088.6 2464.40   1
  -3  -1  -8 41754.1 2446.76   1
  -3  -1  -9-233.445 387.441   1
  -3   1  -9 538.809 305.457   1
  -3  -1 -10 545.973 370.826   1
  -3   1 -10 1331.64 556.210   1
  -3   1 -11 354.476 451.241   1
   3   1  11 826.750 237.626  12
   3   1  11 492.306 159.384  11
   3  -1  12 846.339 212.285  11
  -3   1 -12 1278.41 690.834   1
   3  -1  12 1027.53 238.649  12
   3   1  12 1334.91 284.406  11
   3   1  12 1105.75 272.119  12
   3   1  12 1158.57 247.649   9
   3  -1  13 307.071 135.294  12
   3   1  13 332.347 196.266  11
   3  -1  13 68.6482 136.263  11
   3   1  13 149.710 110.109   9
   3   1  13 236.278 174.892  12
   3   1  14 292.581 184.131  12
   3   1  14 537.911 204.002  11
   3  -1  14 842.136 219.697   9
   3  -1  14 333.138 165.056  11
   3   1  14 821.245 207.124   9
   3  -1  14 457.095 200.007  12
   3  -1  15 3202.38 405.110  12
   3   1  15 3950.50 456.564  12
   3   1  15 3734.44 443.319  11
   3  -1  15 3427.85 439.232  11
   3  -1  16 1908.82 321.869  12
   3   1  16 1883.58 327.144  11
   3  -1  16 1905.04 346.215  11
   3   1  17 228.836 192.956  11
   3  -1  17-48.2782 126.796  12
   3  -1  17-46.3658 161.323  11
   3  -1  18 320.582 150.303  11
   3  -1  19-68.4575 87.4487  11
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  -3  -2  17 590.815 222.874  12
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  -3  -2  16 1683.64 300.253  13
  -3   2  16 2231.88 300.970  12
  -3  -2  16 2589.92 333.074  11
  -3   2  15 227.099 162.708  12
  -3  -2  15 271.221 180.501  12
  -3  -2  15 125.706 144.157  13
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  -3  -2  14 12187.7 803.771  13
  -3  -2  14 12548.9 830.309  12
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  -3  -2  14 13935.0 807.668  11
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   3   2 -13 4507.71 1086.04   1
  -3   2  13 8070.47 1373.64   3
  -3   2  13 6478.93 592.001  11
  -3  -2  13 6505.06 595.866  13
  -3  -2  13 6408.75 595.714  12
  -3  -2  12 2291.38 357.501  13
  -3  -2  12 2505.38 368.004   8
  -3   2  12 2383.02 360.622  11
  -3   2  12 2530.68 784.444   3
  -3  -2  12 2078.94 320.151  11
  -3  -2  12 2539.00 392.289  12
  -3   2  11 2912.98 806.314   3
  -3  -2  11 1308.52 251.071  12
  -3   2  10 4403.37 910.278   3
  -3   2   9 340.819 263.694   3
  -3  -2   8 4330.20 770.372   3
  -3   2   8 5101.93 840.260   3
  -3   2   7 596.595 305.056   3
  -3  -2   7 748.769 381.747   3
  -3   2   6 85889.3 3047.38   3
  -3  -2   6 82633.0 2742.81   3
  -3   2   5 3232.02 556.227   3
  -3  -2   5 3429.58 530.401   3
  -3  -2   4 4745.18 559.396   3
  -3   2   4 4479.82 642.479   3
  -3  -2   3 10468.7 681.210   3
  -3   2   3 12471.1 1032.96   3
  -3   2   2 13957.4 1112.07   3
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  -3   2   2 14899.6 705.263   1
  -3   2   1 1874.21 329.507   1
  -3   2   1 1937.51 492.360   3
  -3   2   0 29343.3 1332.20   1
  -3   2  -1 51708.9 1934.98   1
  -3   2  -2 65681.2 2353.04   1
  -3   2  -3 4913.97 733.429   1
   3   2   3 6080.87 571.066   2
   3   2   4 55207.3 1504.19   2
  -3  -2  -4 51612.0 2134.81   1
  -3   2  -5 21209.5 1687.13   1
  -3  -2  -5 23390.8 1496.37   1
  -3   2  -6 29266.9 2111.33   1
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  -3  -2  -7-112.911 204.301   1
  -3   2  -7-115.452 359.134   1
  -3   2  -8 1586.68 666.151   1
  -3   2  -9-447.311 495.012   1
  -3   2 -10 11010.3 1653.90   1
  -3   2 -11 75.2702 285.147   1
   3  -2  11 434.177 154.080  14
   3   2  11 380.051 187.462  12
   3  -2  11 378.875 149.861  12
   3   2  11 513.286 194.380  11
   3   2  11 401.009 165.727   9
   3  -2  12 7446.73 551.561  14
   3   2  12 6003.99 557.921  12
   3   2  12 6417.44 584.130  11
   3  -2  12 6823.39 590.868  12
   3  -2  12 7099.66 566.772   5
   3   2  12 7555.46 599.532   9
  -3   2 -12 4909.84 1131.69   1
   3   2  13 1321.01 267.523   9
   3   2  13 1052.16 262.480  11
   3  -2  13 1116.86 276.679  12
   3  -2  14 1311.92 277.583  12
   3  -2  14 825.333 238.121  11
   3   2  14 886.457 247.919  11
   3  -2  15 423.698 206.278  12
   3  -2  15 248.225 117.581   9
   3   2  15 319.543 166.389  11
   3  -2  15 271.637 196.304  11
   3  -2  16 1691.81 291.663  12
   3   2  16 2054.08 320.856  11
   3  -2  16 1703.24 308.901  11
   3  -2  17 278.831 165.198  12
   3  -2  17-103.923 133.249  11
   3  -2  18 773.980 184.675  12
   3  -2  18 850.628 187.569  11
   3  -2  19 115.551 91.4918  11
  -3  -3  19-62.1263 67.6163  12
  -3  -3  18-3.54918 104.873  12
  -3  -3  17 347.686 142.712  12
  -3  -3  16 146.513 118.589  11
  -3  -3  16 92.8967 148.824  12
  -3  -3  15 7554.26 601.289  13
  -3  -3  15 8428.95 588.154  11
  -3  -3  15 7446.78 616.946  12
  -3  -3  14 673.337 180.301  11
  -3  -3  14 436.717 196.894  13
  -3  -3  14 758.510 224.650  12
  -3  -3  13 2358.53 340.142  11
  -3  -3  13 2146.44 353.747  13
  -3  -3  13 2242.21 388.942  12
  -3  -3  12 760.931 243.241  13
  -3   3  12 1419.30 507.476   3
  -3  -3  12 674.138 238.019  12
  -3  -3  11 8478.39 668.659  12
  -3  -3  11 8595.96 639.960  13
  -3   3  11 8548.52 1307.92   3
  -3  -3  10 1355.01 262.328  12
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  -3   3  10 1683.44 606.763   3
  -3   3   9 2608.25 693.263   3
  -3   3   8 1376.82 547.460   3
  -3   3   7 819.331 375.633   3
  -3   3   6 11668.7 1201.51   3
  -3   3   5 3427.42 640.542   3
  -3   3   4 15168.1 1262.72   3
  -3   3   3 456.342 230.023   3
  -3   3   2 9313.26 1001.39   3
  -3   3   1 5509.74 829.398   3
  -3   3   1 5578.69 572.507   1
  -3   3   0 5604.26 672.179   1
  -3   3  -1 1533.43 367.925   1
  -3   3  -2 30893.2 1824.60   1
   3   3   2 32939.2 1694.67   2
   3   3   3 1782.88 420.273   2
  -3   3  -3 1277.33 403.325   1
  -3   3  -4 1046.65 426.423   1
   3   3   4 1481.04 348.532   2
  -3   3  -5 588.254 381.980   1
  -3   3  -6 1175.40 492.028   1
  -3   3  -7 1121.22 625.778   1
  -3   3  -8 1428.21 658.124   1
  -3   3  -9 1303.18 623.490   1
  -3   3 -10 2925.38 921.538   1
   3  -3  10 2280.92 323.574  14
   3   3  10 2178.35 333.793  11
   3  -3  11 303.505 164.372  14
   3  -3  11 213.206 139.095  12
  -3   3 -11 380.212 327.840   1
   3   3  11 421.055 192.342  11
   3  -3  12 81.5751 124.999  14
   3  -3  12 4.67188 176.263  12
   3  -3  13 408.491 190.898  14
   3  -3  13 704.643 225.664  12
   3  -3  13 505.278 186.062   5
   3  -3  14 1641.52 290.943  12
   3  -3  15 232.330 153.148  12
   3  -3  15 161.039 164.535  11
   3  -3  16-89.2923 121.407  12
   3  -3  16 143.639 152.900  11
   3  -3  17 943.046 187.210  11
   3  -3  17 862.894 177.369  12
   3  -3  18 278.693 115.621  11
  -3  -4  18 164.831 81.3143  12
  -3  -4  17 207.481 137.750  12
  -3  -4  16 22.7441 147.179  12
  -3  -4  15 677.591 176.463  12
  -3  -4  14 610.441 173.158  11
  -3  -4  14 833.473 245.464  12
  -3  -4  14 833.545 224.981  13
  -3  -4  13 247.956 177.960  12
  -3  -4  13 651.885 202.416  13
  -3  -4  13 344.881 141.292  11
  -3  -4  12 409.656 215.083  12
  -3  -4  12 657.159 249.264  13
  -3  -4  11 575.602 245.426  13
  -3  -4  11 279.356 203.651  12
  -3  -4  10-133.788 189.305  12
   3   4 -10 421.596 278.457   2
  -3  -4  10 91.3273 131.298  13
   3   4  -9 153.366 458.485   2
  -3  -4   9 441.140 198.356  13
  -3  -4   9 257.680 167.919  12
  -3   4   8 2823.09 723.671   3
  -3  -4   8 2710.93 363.728  12
  -3   4   7 12149.6 1366.89   3
  -3   4   6 552.055 378.505   3
  -3   4   5 680.550 391.520   3
  -3   4   4 669.492 393.569   3
  -3   4   3 13124.5 1237.82   3
  -3   4   2 2046.09 486.510   3
  -3   4   1 15933.9 1416.18   3
   3   4  -1 14473.1 1412.94   2
  -3   4   0 116102. 3986.16   3
   3   4   0 109485. 3837.10   2
  -3   4  -1 1858.69 486.020   1
   3   4   1 2346.63 649.118   2
   3   4   2 24151.7 1741.99   2
  -3   4  -2 22475.8 1745.52   1
  -3   4  -3 12276.2 1360.50   1
   3   4   3 12643.4 1254.34   2
  -3   4  -4 11218.7 1373.45   1
   3   4   4 13236.4 1273.21   2
  -3   4  -5 20553.4 1981.50   1
  -3   4  -6 1167.48 603.730   1
  -3   4  -7 12772.9 1704.86   1
  -3   4  -8 3825.39 1045.41   1
  -3   4  -9 8426.82 1533.71   1
   3  -4   9 7671.63 597.357  14
   3   4   9 8735.23 602.994  10
   3   4  10 273.549 160.908  10
   3  -4  10 218.713 149.528  14
   3  -4  11 12303.3 782.877  14
   3   4  11 12947.8 745.682  10
   3  -4  12 3346.30 396.030  14
   3  -4  13 172.237 139.853  12
   3  -4  13 136.586 112.982  14
   3  -4  13 314.777 162.472   5
   3  -4  14 1984.20 293.912  14
   3  -4  14 2077.31 295.909  12
   3  -4  14 2512.51 317.624   5
   3  -4  15 4408.34 439.274  11
   3  -4  15 4662.19 388.273  12
   3  -4  16-70.2772 109.190  11
   3  -4  17 107.477 93.1094  11
  -3  -5  16 152.259 94.9747  12
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  -3  -5  14-65.4078 130.833  12
  -3  -5  13 468.362 242.897  12
  -3  -5  12 499.159 173.194  12
  -3  -5  11 723.024 240.151  12
  -3   5  10 749.070 199.017   6
  -3  -5  10 373.343 154.264  12
  -3   5   9 296.736 130.905   6
  -3  -5   9-23.6455 145.898  12
  -3  -5   8 4050.74 475.464  12
   3   5  -8 3308.80 901.612   2
  -3   5   8 3993.35 428.538   6
   3   5  -7 3504.23 893.018   2
  -3   5   7 3147.98 390.816   6
  -3   5   6 5381.89 490.819   6
   3   5  -6 4599.96 1119.00   2
   3   5  -5 1932.68 772.294   2
  -3   5   5 951.052 217.455   6
   3   5  -4 3348.94 879.042   2
   3   5  -3 2094.19 713.163   2
   3   5  -2 1545.56 605.121   2
   3   5  -1-106.650 372.728   2
   3   5   0 172.965 467.520   2
   3   5   1 1107.15 475.179   2
   3   5   2 8366.84 1225.49   2
   3   5   3 1463.99 535.975   2
   3   5   4-142.017 96.4673  10
  -3   5  -4 1059.54 552.083   1
  -3   5  -5 71.3677 396.766   1
   3   5   5-30.2061 105.755  10
  -3   5  -6 1514.11 738.629   1
   3   5   6 36.6260 154.296  10
   3   5   7 286.066 176.459  10
  -3   5  -7 579.459 594.698   1
  -3   5  -8 855.211 527.884   1
   3   5   8 150.976 157.235  10
   3  -5   9 324.764 194.185  14
   3   5   9 413.857 168.271  10
   3  -5  10 301.607 186.519  14
   3   5  10 157.185 110.866  10
   3   5  11 1733.01 297.449  10
   3  -5  11 1681.61 307.423  14
   3   5  12 1911.57 288.327  10
   3  -5  12 1797.46 315.443  14
   3  -5  13 3929.58 405.666  14
   3  -5  14 2457.65 285.426  14
   3  -5  14 2365.14 276.503   5
   3  -5  15 1180.16 220.328  11
   3  -5  16-21.5423 91.7463  11
  -3  -6  15 53.0934 68.7365  12
  -3  -6  14 228.255 113.675  12
  -3  -6  13 83.1908 87.1715  14
  -3  -6  13 174.685 157.301  12
  -3  -6  12 102.390 129.668  12
  -3  -6  12 167.459 110.161  14
  -3  -6  11 294.990 154.949  12
  -3  -6  10 311.196 131.907  12
  -3   6  10 271.014 133.830   6
  -3   6   9-265.988 224.529   7
  -3  -6   9 224.774 143.849  12
  -3   6   9-55.1870 131.302   6
  -3   6   8 3490.96 414.348   6
  -3  -6   8 3549.37 443.546  12
  -3  -6   7 1200.17 269.987  12
  -3   6   7 1117.64 278.593   6
  -3   6   6 1269.20 278.534   6
  -3   6   5-22.1862 150.013   6
   3   6  -4-292.595 466.633   2
  -3   6   4 14.0284 151.225   6
   3   6  -3 1000.57 633.220   2
  -3   6   3 529.947 212.644   6
  -3   6   2 595.208 229.179   6
   3   6  -2-418.263 517.527   2
   3   6  -1 148.290 467.491   2
  -3   6   1 662.882 226.913   6
   3   6  -1 478.218 181.315  10
   3   6   0 11263.2 1513.67   2
   3   6   0 10273.9 674.896  10
  -3   6   0 9938.79 676.507   6
  -3   6  -1 3763.78 420.969   6
   3   6   1 4044.32 419.582  10
  -3   6  -2 387.458 215.989   6
   3   6   2-50.8698 130.339  10
  -3   6  -3 405.912 189.118   6
   3   6   3 450.881 183.621  10
   3   6   4 1142.07 278.842  10
   3   6   5 296.502 156.870  10
   3   6   6 814.658 210.283  10
   3   6   7 601.775 205.083  10
   3   6   8 3422.75 427.821  10
   3  -6   8 3564.37 453.195  14
   3  -6   9 395.259 191.694  14
   3   6   9 260.976 148.913  10
   3  -6  10 345.886 209.206  14
   3   6  10 314.295 138.579  10
   3   6  11 3496.27 354.681   6
   3  -6  11 3024.07 381.503  14
   3   6  11 2743.37 334.871  10
   3  -6  12 1574.20 273.730  14
   3  -6  13 138.207 102.445  14
   3  -6  13 234.730 120.153   5
   3  -6  14 1466.94 226.129  11
   3  -6  15 225.823 82.2648  11
  -3  -7  12 572.882 147.115  14
  -3  -7  11 2075.22 269.015  14
  -3   7  10 418.139 138.588   7
  -3  -7  10 416.440 143.123  12
  -3   7   9-65.4343 106.109   7
  -3   7   9 124.210 99.4495   6
  -3  -7   9 74.5830 122.495  12
  -3  -7   8-235.810 143.374  12
  -3   7   8 76.6562 133.067   6
  -3   7   8-101.743 206.055   7
  -3  -7   7 355.067 175.616  12
  -3   7   7 502.263 203.524   6
  -3   7   6-162.263 137.566   6
  -3   7   5 966.025 249.728   6
  -3   7   4-46.9552 139.444   6
  -3   7   3 927.814 250.337   6
  -3   7   2-18.0199 165.242   6
   3   7  -2 326.383 167.569   6
  -3   7   1 1691.16 314.060   6
   3   7  -1 1735.52 284.101   6
  -3   7   0-8.51257 144.762   6
  -3   7  -1 253.712 147.669   6
   3   7   2 271.611 140.470  10
   3   7   3 37.1574 127.902  10
   3   7   4 6.48233 154.949  10
   3   7   5 734.277 231.271  10
   3   7   6 139.393 141.136  10
   3  -7   6-96.5423 162.920  14
   3  -7   7 67.1286 164.877  14
   3   7   7 46.7253 132.440  10
   3  -7   8 616.222 195.604  14
   3   7   8 570.101 184.047  10
   3   7   8 806.006 223.782   6
   3  -7   9 1784.72 303.912  14
   3   7   9 1804.72 272.738   6
   3  -7  10 1867.91 268.496  14
   3   7  10 1919.29 251.064   6
   3  -7  11 4948.04 391.137  14
   3   7  11 4938.13 336.024   6
   3  -7  12 383.200 128.228  14
   3  -7  12-55.0203 88.5483   5
   3  -7  13 405.606 106.239  11
  -3  -8  10 160.184 88.5684  14
  -3  -8   9 284.433 130.886  14
  -3   8   9 9.86197 80.4457   7
  -3   8   8 900.349 185.046   7
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   3  -8   6 360.525 160.947  14
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   3   8   7 2791.34 303.998   6
   3   8   8 1494.97 216.902   6
   3  -8   8 1557.46 227.669  14
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   3   8   9 280.668 99.6737   6
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   4   0  13 70.4201 129.943  12
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   4   0  15 19.5303 129.200  11
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   4   1  11 2930.52 377.706  12
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   4   1  11 3234.62 375.076  11
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   4   1  12 6288.16 560.108  11
   4  -1  12 6334.97 561.719  12
   4   1  12 6622.43 566.593   9
   4  -1  12 5655.58 552.379  11
   4   1  12 6548.34 560.218  12
   4  -1  12 6677.07 550.537   5
   4   1  13 5518.80 526.856  12
   4  -1  13 5676.65 526.450  12
   4   1  13 5761.11 536.427  11
   4  -1  13 6144.92 568.542  11
   4   1  13 6306.03 556.174   9
   4   1  14 223.670 182.334  12
   4  -1  14 21.2288 131.511  12
   4  -1  14-87.3591 164.816  11
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   4   1  14-0.71471 152.439  11
   4  -1  14-21.5426 133.856   9
   4  -1  15 487.324 194.607  12
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   4   1  15 443.467 167.952   9
   4  -1  15 447.780 178.409   9
   4   1  16 2613.17 352.555  11
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   4  -1  16 2665.93 352.837  12
   4  -1  16 2606.47 364.606  11
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  -4   2   6 14627.8 1338.42   3
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  -4  -2   5 118322. 3059.95   3
  -4   2   5 116683. 3593.47   3
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  -4   2   4 24911.4 1602.40   3
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   4   2   4 905.049 214.483   2
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   4  -2  11 2604.15 351.949  14
   4  -2  11 2357.17 340.504  12
   4   2  11 2453.32 331.469  11
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   4   2  11 2194.64 333.336   9
   4  -2  11 2077.96 323.716   5
   4  -2  12 1620.40 265.808  14
   4  -2  12 1813.82 317.378  12
   4   2  12 1921.00 335.721  11
   4   2  12 1597.63 277.209   9
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   4  -2  12 1797.63 303.335   5
   4  -2  13 993.249 275.966  12
   4   2  13 1007.29 230.003   9
   4  -2  13 821.784 218.342   5
   4   2  13 1204.10 268.048  11
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   4  -2  14-48.0187 117.989  12
   4  -2  15 519.451 177.000  12
   4   2  15 759.682 219.331  11
   4  -2  15 763.425 221.198  11
   4  -2  15 620.131 173.870   9
   4  -2  16 172.114 143.104  12
   4  -2  16 257.854 153.482  11
   4  -2  16 229.725 133.250   9
   4  -2  17 114.504 132.190  12
   4  -2  17-103.478 120.141  11
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   4   3   3 1559.03 435.567   2
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   4   3   4 6390.59 729.811   2
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  -4   3  -5 1363.16 572.047   1
  -4   3  -6 399.774 309.430   1
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  -4   3  -8 1656.08 558.066   1
  -4   3  -9 596.145 342.768   1
   4   3   9 230.388 144.330  11
   4  -3   9 178.031 137.842  14
   4  -3  10 108.656 131.486  14
   4   3  10 69.7242 148.303  11
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   4  -3  11 371.785 159.822  14
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   4  -3  12 923.519 227.720  14
   4  -3  12 516.333 166.701   5
   4  -3  12 896.157 222.249  12
   4  -3  13 477.118 200.950  14
   4  -3  13 344.401 154.973  12
   4  -3  13 629.872 208.424   5
   4  -3  14 158.940 153.301  12
   4  -3  14-153.508 128.120   5
   4  -3  14-215.846 179.413  11
   4  -3  15 5100.85 457.703  12
   4  -3  15 4213.62 454.648  11
   4  -3  16 1494.13 252.882  11
   4  -3  16 1579.61 244.546  12
   4  -3  16 1610.35 237.534   9
   4  -3  17 228.114 136.110  11
   4  -3  18 2637.27 246.480  11
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  -4  -4  13 1186.82 265.499  12
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  -4  -4  12 405.990 193.336  12
  -4  -4  12 306.842 159.274  13
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  -4  -4  11 82.5986 176.190  13
  -4  -4  10 3002.49 388.072  13
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  -4  -4   9 695.124 221.346  13
  -4   4   9 975.949 490.371   3
  -4  -4   9 628.393 196.471  12
  -4   4   8 1596.35 567.932   3
  -4   4   7 1651.28 585.830   3
  -4   4   6 1363.59 477.196   3
  -4   4   5 157.844 237.987   3
  -4   4   4 15950.0 1500.22   3
  -4   4   3 7747.40 1061.97   3
  -4   4   2 53694.2 2733.22   3
  -4   4   1 124234. 4233.98   3
  -4   4   0 206527. 5744.48   3
   4   4   1 781.176 459.465   2
  -4   4  -1 603.622 269.634   1
   4   4   2 2199.33 579.501   2
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  -4   4  -3 8329.85 1145.19   1
   4   4   3 9945.55 1122.94   2
  -4   4  -4 21507.6 1955.76   1
  -4   4  -5 834.764 513.013   1
  -4   4  -6 5637.52 1170.87   1
  -4   4  -7 209.957 345.187   1
   4  -4   7-8.12839 153.472  14
   4  -4   8 4624.25 489.427  14
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  -4   4  -9 1750.18 739.555   1
   4  -4   9 1958.73 331.325  14
   4  -4  10 1108.22 254.490  14
   4   4  10 1714.28 292.920  10
   4  -4  11 902.016 238.237  14
   4   4  11 917.883 228.275  10
   4  -4  12 3314.57 403.384  14
   4   4  12 3398.71 371.185  10
   4  -4  13 106.611 162.016  14
   4  -4  13 198.626 156.976   5
   4  -4  14 9.66203 100.149   5
   4  -4  15 150.213 140.455  11
   4  -4  16 257.384 139.751  11
   4  -4  17-47.6710 80.4431  11
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  -4  -5  14 903.070 213.693  12
  -4  -5  13-91.5396 170.185  12
  -4  -5  12 77.8923 165.088  12
  -4  -5  11 471.143 250.225  12
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   4   5  -8 469.320 375.839   2
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   4   5  -7 387.374 576.253   2
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   4   5  -6 1131.74 553.757   2
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   4   5  -3-30.7098 373.098   2
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   4   5   5 67.5171 113.483  10
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   4  -7   8 7932.05 577.645  14
   4   7   8 8164.18 565.945  10
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   5   0  12 38.7436 113.742   9
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   5   1  10 1650.30 274.990   9
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   5   1  11 3968.66 452.933  12
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   5  -1  11 4968.36 479.474   5
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   5   1  12 3116.67 421.103  12
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   5  -1  13 3811.04 444.533  12
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   5   1  13 3285.86 420.867   9
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   5   1  16 9034.62 614.539  11
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   5   1  17 86.3382 119.032  11
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   5  -2  10 48.8333 126.350  14
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   5   2  10 227.482 138.710  11
   5   2  10 558.061 194.287   9
   5  -2  10 203.038 108.990   5
   5  -2  11 338.326 171.149  14
   5  -2  11 269.521 153.660  12
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   5   2  11 317.948 167.522  11
   5   2  11 120.831 148.785   9
   5  -2  11 119.633 149.309   5
   5   2  12 241.559 191.540  11
   5  -2  12 38.4522 145.070   5
   5  -2  12-74.2181 176.630  12
   5   2  12 42.4853 134.349   9
   5   2  13 1830.82 309.536  11
   5  -2  13 1538.19 294.365  12
   5  -2  13 1376.38 291.859  11
   5   2  13 1689.45 303.297   9
   5  -2  13 1625.27 294.632   5
   5  -2  14 3983.87 424.790  12
   5   2  14 4068.50 444.670  11
   5  -2  14 3476.35 439.530  11
   5  -2  14 4161.53 436.475   5
   5  -2  15 17.0885 133.992  12
   5   2  15 60.9137 137.334  11
   5  -2  15 187.521 185.899  11
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   5   5  -6 1341.32 726.901   2
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   6   0  10 9455.83 659.154  12
   6   0  10 10572.7 679.311  11
   6   0  10 10588.3 684.091   5
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   6   0  11 67.7787 140.803  12
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   6   0  12 10149.6 710.823  12
   6   0  12 10512.7 748.904   9
   6   0  12 10806.1 725.128  11
   6   0  13-22.6798 139.610  11
   6   0  13 51.9841 107.513   9
   6   0  14 3626.49 420.026  11
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   6   0  15-20.4123 135.214  11
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   6   0  16 2431.69 322.564  11
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   6  -1  10-31.8673 131.808  12
   6   1  10 50.2562 116.201  11
   6  -1  10-59.8711 111.636   5
   6   1  10 202.873 146.652   9
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   6  -1  11 2224.58 357.133  12
   6   1  11 2014.55 304.742  11
   6  -1  11 2020.34 351.996  11
   6  -1  11 1880.09 314.327   5
   6   1  11 2152.85 341.318   9
   6  -1  12 445.812 200.563  12
   6   1  12 542.251 210.358  11
   6  -1  12 543.400 216.625  11
   6  -1  12 541.876 190.066   5
   6   1  12 225.878 156.334   9
   6  -1  13 7186.74 595.371  12
   6   1  13 6787.51 579.195  11
   6  -1  13 6988.01 605.544  11
   6  -1  13 7000.16 584.595   5
   6   1  13 6577.61 584.116   9
   6  -1  14 665.168 208.433  12
   6   1  14 260.222 164.987  11
   6  -1  14 376.235 175.007  11
   6   1  14 260.607 164.661   9
   6  -1  14 277.304 159.026   9
   6   1  15 1350.85 277.542  11
   6  -1  15 1403.05 279.928  11
   6   1  15 1693.31 287.001   9
   6  -1  15 1294.61 247.268   9
   6   1  16 76.7236 121.630  11
   6  -1  16 201.787 167.569  11
   6  -1  16 173.917 140.574   9
   6  -1  17 379.352 161.323  11
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   6  -1  18 147.675 92.9741  11
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   6  -2   9 3834.65 409.580  14
   6  -2   9 3843.90 440.000   5
   6   2   9 3947.07 432.521   9
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   6  -2  10 263.542 145.736  14
   6   2  10 274.966 164.076  11
   6   2  10 140.118 113.383   9
   6  -2  10 264.480 170.327   5
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   6   2  11 3462.34 406.032  11
   6  -2  11 3351.91 428.918   5
   6   2  11 3199.21 424.073   9
   6  -2  12-258.514 124.091  12
   6   2  12 67.9848 147.603  11
   6   2  12-176.667 160.364   9
   6  -2  12-113.704 129.926   5
   6   2  13 74.7203 122.502  11
   6  -2  13 73.5748 144.774  11
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   6   2  13-97.4171 114.030   9
   6  -2  13 192.147 137.852  12
   6  -2  14 805.862 206.809  12
   6   2  14 607.702 208.957  11
   6  -2  14 467.765 193.711  11
   6  -2  14 636.439 186.808   5
   6  -2  15 5680.60 502.831  11
   6  -2  15 5707.33 496.944   9
   6  -2  16 359.741 165.790  11
   6  -2  16 160.238 114.759   9
   6  -2  17 1055.07 189.647  11
   6  -2  17 951.144 159.579   9
   6  -2  18 83.6216 66.6946  11
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  -6   3   8 214.664 325.914   3
  -6   3   7 2258.99 667.654   3
  -6   3   6 3332.66 777.579   3
  -6   3   5 6101.94 1031.32   3
  -6   3   4 2061.57 644.699   3
  -6   3   3 5703.95 942.462   3
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  -6   3  -3 890.078 383.471   1
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  -6   3  -5 131.173 395.462   1
  -6   3  -6 10145.0 1549.07   1
   6  -3   7 2394.96 344.747  14
  -6   3  -7 2071.64 687.745   1
   6   3   7 1625.39 276.063   9
   6  -3   8 561.273 177.237  14
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   6   3   8 707.489 222.385   9
   6  -3   9 136.053 125.757  14
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   6  -3  10 2218.56 353.897  14
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   6  -3  11 100.840 136.817  14
   6  -3  11 11.5714 115.857   5
   6  -3  12 215.500 162.619   5
   6  -3  13 85.8217 118.445   5
   6  -3  14 2080.62 294.090   5
   6  -3  14 1808.82 312.421  11
   6  -3  15 79.6263 136.235  11
   6  -3  15 115.658 106.469   5
   6  -3  15 361.432 138.350   9
   6  -3  16 326.148 129.085  11
   6  -3  16-20.0076 78.4409   9
   6  -3  17 46.2146 87.7833  11
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  -6  -4  11 884.657 269.253  12
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  -6   4   7-248.533 394.463   3
  -6   4   6-465.063 452.977   3
  -6   4   6-144.124 156.789   7
  -6   4   6 4.76944 131.541   6
  -6   4   5 315.314 363.134   3
  -6   4   4 502.094 499.472   3
  -6   4   3 1627.85 618.112   3
  -6   4   2 912.849 420.992   3
  -6   4   1 3155.00 781.875   3
  -6   4   0 4100.59 978.362   3
  -6   4  -1 145.327 519.466   3
   6   4   2 10824.2 1263.27   2
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  -6   4  -3 2635.11 722.349   1
  -6   4  -4 2016.57 755.745   1
   6  -4   5 11956.9 719.964  14
  -6   4  -5 10880.6 1599.82   1
   6  -4   6 16764.4 871.635  14
  -6   4  -6 15671.1 1991.92   1
   6  -4   7 377.175 151.478  14
  -6   4  -7 357.302 539.430   1
   6  -4   8 3243.45 427.116  14
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   6  -4   9 4520.15 480.303  14
   6  -4  10 7342.46 627.691  14
   6  -4  11 367.020 185.798  14
   6  -4  11 282.095 172.392   5
   6  -4  12 469.352 193.850  14
   6   4  12 580.267 198.637  10
   6  -4  12 641.961 208.582   5
   6   4  13 416.276 148.481  10
   6  -4  13 555.122 176.044   5
   6  -4  14 666.002 197.430  11
   6  -4  14 421.325 156.962   5
   6  -4  15 65.9806 103.985  11
   6  -4  15 277.107 124.877   5
   6  -4  16-20.3102 92.0499  11
   6  -4  16 52.5829 54.9187   9
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  -6   5   8 1011.18 255.138   7
  -6   5   7 5728.25 548.631   7
  -6   5   6 188.695 174.918   7
  -6   5   5 78.2909 119.232   6
  -6   5   5 80.7035 156.622   7
  -6   5   4 884.140 255.467   7
  -6   5   4 971.480 246.375   6
  -6   5   4 1401.45 561.313   3
  -6   5   3 1252.14 238.781   7
  -6   5   3 1297.90 267.869   6
   6   5  -3 957.909 505.862   2
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  -6   5   2 67.5065 140.757   7
  -6   5   2-48.7284 150.412   6
   6   5  -2-114.277 458.974   2
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   6   5  -1 4805.58 1065.93   2
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   6   5   0 261.512 412.112   2
   6   5   0 246.615 169.455  10
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   6   5   1-58.7266 308.086   2
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   6  -5   2 724.651 210.607  14
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   6  -5   3 1119.75 251.037  14
   6  -5   4 208.453 195.842  14
   6  -5   5 2408.77 365.696  14
   6  -5   6 856.090 232.535  14
   6  -5   7 4022.39 454.200  14
   6  -5   8 13694.7 833.273  14
   6   5   8 12786.6 787.315  10
   6  -5   9 7654.28 610.632  14
   6   5   9 8327.32 625.908  10
   6  -5  10 330.292 160.590  14
   6   5  10 400.941 137.550  10
   6  -5  11 53.8448 145.760  14
   6   5  11 3.82129 122.383  10
   6   5  12 80.8145 103.974  10
   6  -5  12-149.421 152.065   5
   6   5  13 177.613 101.687  10
   6  -5  13 115.982 107.311   5
   6  -5  14 218.188 145.761  11
   6  -5  14 98.4924 99.7290   5
   6  -5  15 140.795 94.2286  11
   6  -5  15 26.7875 48.5345   9
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  -6   6   7 2866.45 389.054   7
  -6   6   6 9510.93 708.465   7
  -6   6   5 14203.6 858.302   7
  -6   6   4 5657.46 551.242   7
  -6   6   3 18900.3 992.284   7
  -6   6   2 11584.1 793.212   7
  -6   6   1 19568.9 1016.92   7
   6   6  -1 17885.8 876.115  10
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   6   6   0 3625.98 416.140  10
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   6   6   1-191.986 133.650  10
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   6   6   2-43.3916 128.642  10
   6  -6   2 72.8229 109.439  14
   6  -6   3 327.261 195.122  14
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   6   6   3-16.9999 134.921  10
   6  -6   4 667.693 215.648  14
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   6   6   4 677.991 230.260  10
   6  -6   5 117.800 146.463  14
   6   6   5 172.125 138.317  10
   6  -6   6 93.8620 164.904  14
   6   6   6 268.231 175.291  10
   6  -6   7 1643.21 292.026  14
   6   6   7 1844.06 303.370  10
   6  -6   8 367.766 205.945  14
   6   6   8 437.622 212.515  10
   6  -6   9 1076.26 234.445  14
   6   6   9 1510.44 270.340  10
   6  -6  10 735.053 234.889  14
   6   6  10 1049.50 234.858  10
   6  -6  11 365.970 168.256  14
   6   6  11 623.131 176.275  10
   6  -6  11 447.262 191.286   5
   6   6  12 35.1595 98.5772  10
   6  -6  12 243.221 132.318   5
   6  -6  13 248.186 120.675  11
   6  -6  13-12.2829 75.1902   5
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  -6   7   8 371.755 147.626   7
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  -6   7   7 186.704 148.060   7
  -6  -7   7 189.319 165.433  12
  -6   7   6 803.966 267.790   7
  -6  -7   6 668.654 237.421  12
  -6   7   5-50.1644 158.002   7
  -6   7   4 225.429 166.819   7
  -6   7   3 183.819 166.344   7
  -6   7   2 1171.28 284.639   7
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  -6   7   0 325.354 201.518   7
   6   7   0 332.108 132.592  10
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   6   7   1 180.695 164.010  10
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   6   7   2 269.434 182.550  10
   6  -7   3 438.503 186.542  14
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   6   7   3 392.339 168.351  10
   6  -7   4 160.856 155.252  14
   6   7   4 335.913 194.468  10
   6  -7   5-277.425 165.977  14
   6   7   5-70.6838 128.835  10
   6  -7   6 134.866 134.983  14
   6   7   6 98.5399 151.545  10
   6  -7   7 384.022 161.437  14
   6   7   7 664.269 202.234  10
   6  -7   8 451.527 146.374  14
   6   7   8 565.466 180.293  10
   6  -7   9 227.294 136.021  14
   6   7   9 172.301 117.906  10
   6   7   9 241.213 130.422   6
   6   7  10 24.2035 75.1183   6
   6  -7  10 146.464 122.763   5
   6  -7  11-16.6806 76.0706   5
  -6   8   8 76.6632 76.0003   7
  -6   8   7 71.3002 134.111   7
  -6   8   6 1265.07 218.250   7
  -6  -8   6 885.336 146.616  12
  -6   8   5 3766.03 351.427   7
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  -6   8   4 2220.72 295.382   7
  -6   8   3 10635.1 625.046   7
  -6  -8   3 11491.9 556.550  12
  -6   8   2 631.811 199.240   7
  -6   8   1 1461.33 259.284   7
  -6   8   0 144.144 155.110   7
   6   8   0 63.2734 95.6282   6
  -6   8  -1-85.4557 129.091   7
   6   8   1 193.746 115.934   6
  -6   8  -2 353.688 152.882   7
   6   8   2 102.656 109.478   6
   6   8   3 285.882 155.748   6
   6   8   4-131.432 108.160   6
   6  -8   5 27.9655 67.4879  14
   6   8   5-11.9305 94.4951   6
   6   8   6 36.0300 107.852   6
   6   8   7 141.124 92.6239   6
   6   8   8-71.9349 60.8558   6
   6  -8   8-30.5796 69.3624   5
  -7   0  18-65.3788 98.2904  13
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  -7   0  16 258.831 181.186  13
  -7   0  15 4436.16 486.903  13
  -7   0  15 4804.04 501.546   8
  -7   0  14 67.9433 154.141   8
  -7   0  13 147.231 150.930   8
  -7   0  12 178.842 182.062   8
  -7   0  12-600.367 415.067   3
  -7   0  11 4145.34 974.141   3
  -7   0  11 5283.03 521.018   8
  -7   0  10 330.075 168.146   8
  -7   0  10-98.0992 298.765   3
  -7   0   9 11202.6 1473.25   3
  -7   0   8-48.8137 389.795   3
  -7   0   7 517.047 421.071   3
  -7   0   6-200.867 407.435   3
  -7   0   5 84.6708 296.516   3
  -7   0   4 39.4064 230.475   3
  -7   0   3 1178.61 441.396   3
  -7   0   2-171.633 258.164   3
  -7   0   1 38724.5 2215.15   3
  -7   0   0 18.7981 290.992   3
  -7   0   0 149.909 279.655   1
  -7   0  -1 186.978 310.376   1
  -7   0  -2-115.034 289.277   1
  -7   0  -3 28855.9 2237.12   1
  -7   0  -4 551.641 489.706   1
  -7   0  -5 1990.37 582.309   1
  -7   0  -6-215.494 516.521   1
  -7   0  -7 15212.4 1887.51   1
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   7   0   9 1005.84 229.793   5
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   7   0  10-10.2183 123.685   5
   7   0  11 5125.06 487.536  11
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   7   0  11 4327.25 480.257   9
   7   0  12 108.376 153.673  11
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   7   0  14-57.6683 148.407  11
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   7  -1   9 3710.77 411.351   5
   7   1   9 3881.46 449.758   9
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   7  -1  10 240.588 177.417  12
   7  -1  10 206.383 134.194  11
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   7   1  10-9.13591 128.479   9
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   7  -1  11 1049.67 262.429  11
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   7   1  11 1021.63 265.749   9
   7   1  12 371.926 146.073  11
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   7   1  12 320.848 150.015   9
   7   1  13 247.913 112.550  11
   7  -1  13 82.6616 125.002  11
   7   1  13 68.4186 143.861   9
   7  -1  13 132.692 158.127   9
   7   1  14 433.741 182.427  11
   7  -1  14 1028.70 234.908  11
   7   1  14 595.917 189.919   9
   7  -1  14 560.834 186.155   9
   7   1  15 1914.34 273.686  11
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   7   1  15 1591.42 264.190   9
   7  -1  15 1586.62 255.268   9
   7  -1  16 941.543 191.561  11
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   7  -1  17 248.871 103.770  11
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   7  -2   8 895.969 229.902  14
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   7   2   8 749.660 223.881   9
   7  -2   8 770.135 203.478   5
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   7   2   9 462.764 195.772   9
   7  -2   9 505.881 228.373   5
   7  -2  10 13334.3 832.014   5
   7   2  10 13796.2 845.985   9
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   7   2  11 675.027 209.816   9
   7  -2  11 941.274 241.647   5
   7  -2  12 4719.69 482.359  11
   7  -2  12 4279.90 481.615   5
   7   2  12 4739.82 507.959   9
   7  -2  13 421.085 189.545  11
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   7   2  13 54.1917 108.823   9
   7  -2  14 118.193 137.776  11
   7  -2  14 33.2432 126.194   5
   7  -2  14 342.423 158.536   9
   7  -2  15 80.0779 126.051  11
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   7  -2  16 548.569 148.302  11
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   7  -3   6 8841.92 624.805  14
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   7  -3   7 753.617 213.711  14
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   7  -3   9 20011.4 1003.52  14
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   7  -3  10 15168.5 870.574  14
   7  -3  10 14831.8 890.887   5
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   7  -3  12 1079.16 260.397   5
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   7  -3  14 1118.00 239.915  11
   7  -3  14 1039.93 199.054   5
   7  -3  15 2359.42 293.016  11
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   7  -3  16 1302.45 194.503  11
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  -7   4   6 1337.06 268.847   7
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  -7   4   4 4944.51 493.467   7
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   7  -4   4 1719.33 274.635  14
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   7  -4   5 1047.62 246.178  14
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   7  -4   6 2104.99 356.256  14
   7  -4   7 13448.5 811.473  14
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   7  -4   8 10466.9 732.900  14
   7  -4   9 200.765 179.808  14
   7  -4  10-43.5563 134.273  14
   7  -4  10 222.263 178.765   5
   7  -4  11 402.504 203.394   5
   7   4  12 457.778 162.819  10
   7  -4  12 601.082 209.599   5
   7  -4  13 103.556 140.297  11
   7   4  13-109.219 108.050  10
   7  -4  13 3.27056 115.049   5
   7  -4  14 1055.13 220.028  11
   7  -4  14 877.875 194.871   5
   7  -4  15 799.297 157.632  11
   7  -4  15 594.087 143.857   9
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   7   5  -2 3738.21 970.661   2
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   7   5  -1 53.3993 433.399   2
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   7   5   0 281.225 346.577   2
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  -7   5  -1 641.299 422.954   3
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   7  -5   2-57.9463 143.006  14
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   7  -5   3 549.889 190.177  14
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   7  -5   4 2302.23 348.819  14
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   7  -5   5 1053.10 257.101  14
   7  -5   6 1679.41 317.757  14
   7  -5   7 148.635 136.093  14
   7  -5   8 1894.81 338.566  14
   7  -5   9 2120.90 352.586  14
   7   5   9 2047.92 320.641  10
   7  -5  10 5007.15 492.078  14
   7   5  10 5820.40 491.270  10
   7   5  11 132.756 145.158  10
   7  -5  11 107.789 168.276   5
   7   5  12 190.920 133.297  10
   7  -5  12 64.2203 118.381   5
   7  -5  13-118.235 105.158  11
   7   5  13 30.1429 74.4879  10
   7  -5  13 61.6527 97.0437   5
   7  -5  14-6.82029 79.7913  11
   7  -5  14 0.87818 74.1285   5
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  -7   6   7 4248.94 464.640   7
  -7   6   6 652.351 206.342   7
  -7   6   5 1131.74 297.063   7
  -7   6   4 254.685 223.610   7
  -7   6   3 3461.53 466.483   7
  -7   6   2 4291.14 504.627   7
  -7   6   1-33.5379 194.541   7
  -7   6   0-163.426 146.822   7
   7   6   0 51.1643 150.651  10
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   7   6   1 3375.61 395.483  10
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   7   6   2 1493.39 273.429  10
   7  -6   3 2182.93 326.834  14
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   7   6   3 1951.55 315.133  10
   7  -6   4 2655.88 347.511  14
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   7   6   4 1656.22 305.282  10
   7  -6   5 488.688 217.251  14
   7   6   5 300.578 181.775  10
   7  -6   6 2032.71 332.020  14
   7   6   6 1743.24 283.436  10
   7  -6   7 278.644 168.272  14
   7   6   7 79.7988 129.736  10
   7   6   8 211.992 139.514  10
   7  -6   8 98.5981 175.966  14
   7  -6   9 56.7701 124.938  14
   7   6   9 196.449 133.103  10
   7   6  10 686.857 177.576  10
   7  -6  10 507.597 198.861   5
   7   6  11 160.536 123.891  10
   7  -6  11 113.765 104.249   5
   7   6  12 150.835 89.2279  10
   7  -6  12 69.4863 90.2581   5
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  -7   7   9 61.5801 90.8358   7
  -7  -7   9 4.98986 110.832  12
  -7   7   8 292.444 155.104   7
  -7  -7   8 99.8999 139.504  12
  -7   7   7 850.136 249.926   7
  -7  -7   7 648.928 209.939  12
  -7   7   6 265.139 170.617   7
  -7  -7   6 28.4251 157.461  12
  -7   7   5 129.132 170.149   7
  -7   7   4 190.319 194.680   7
  -7   7   3 795.122 274.833   7
  -7   7   2 744.465 253.319   7
  -7   7   1 66.8915 170.069   7
  -7   7   0 249.426 210.816   7
   7   7   0 235.039 152.621  10
  -7   7  -1 251.324 185.668   7
   7   7   1 211.466 155.941  10
  -7   7  -2 356.142 214.998   7
   7   7   2 416.138 186.652  10
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   7   7   3 293.468 168.927  10
   7  -7   4 214.752 147.874  14
   7   7   4 139.605 149.404  10
   7  -7   5 263.744 142.978  14
   7   7   5 219.853 160.140  10
   7  -7   6 324.175 138.944  14
   7   7   6-52.1404 122.207  10
   7  -7   7 589.910 163.227  14
   7   7   7 573.388 175.202  10
   7   7   8 51.4423 94.6912  10
   7   7   9 9.89515 102.996  10
   7   7   9-132.299 97.9214   6
   7  -7   9 231.474 119.879   5
   7   7  10-104.821 55.8589   6
   7  -7  10-20.8915 85.5463   5
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  -7   8   6-10.0245 74.8596   4
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  -7   8   5 115.440 132.685   7
  -7  -8   5 187.450 85.0316  12
  -7   8   4 214.254 144.064   7
  -7  -8   4 144.511 78.7758  12
  -7   8   3 359.747 175.343   7
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  -7   8   2 5776.79 432.769   7
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  -7   8   0 2659.45 308.144   7
   7   8   0 1744.61 210.614   6
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   7   8   1 2042.59 241.274   6
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   7   8   2-93.7768 95.9227   6
   7   8   3-15.3088 108.994   6
   7   8   4 37.1929 105.959   6
  -7   8  -5 67.9934 84.1816   4
   7   8   5 121.307 108.218   6
   7  -8   5 287.807 100.791   5
   7   8   6 277.658 106.776   6
   7  -8   6 193.549 89.3072   5
   7   8   7 213.518 92.3429   6
  -8   0  18 200.030 84.0444  13
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  -8   0  14 3920.71 446.503   8
  -8   0  13-99.2021 143.027   8
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  -8   0  11-204.049 174.424   8
  -8   0  11-71.3974 263.998   3
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  -8   0  -5-148.825 452.221   1
  -8   0  -6-526.336 344.407   1
  -8   0  -7-401.373 584.427   1
   8   0   8 16371.1 879.367   5
  -8   0  -8 14855.9 2027.95   1
  -8   0  -9-406.829 433.452   1
   8   0   9 70.1265 127.969   5
  -8   0 -10 990.539 600.135   1
   8   0  10 1343.40 301.827   9
   8   0  11-53.4050 140.044   9
   8   0  12 1282.24 286.034   9
   8   0  13-24.5575 121.331  11
   8   0  13 34.4041 116.725   9
   8   0  14 1008.76 215.218  11
   8   0  14 746.541 193.029   9
   8   0  15 31.6894 117.067  11
   8   0  15 208.306 125.597   9
   8   0  16 122.915 107.307   9
  -8  -1  18 88.2706 85.6891  13
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  -8   1  16 490.452 166.588  13
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  -8   1  10 162.933 149.937   8
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  -8   1   9 511.578 431.916   3
  -8  -1   8 103.083 128.654   8
  -8  -1   8 68.2996 216.124   3
  -8   1   8 99.6021 375.004   3
  -8  -1   7 222.251 300.217   3
  -8   1   7 153.223 357.721   3
  -8  -1   6 299.676 265.478   3
  -8   1   6 423.004 392.690   3
  -8  -1   5 3495.59 753.823   3
  -8   1   5 3103.14 735.771   3
  -8  -1   4 2061.63 568.695   3
  -8   1   4 2628.79 685.242   3
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  -8   1   3 3271.88 732.515   3
  -8  -1   2 2518.95 576.463   3
  -8   1   2 2759.04 699.861   3
  -8   1   1 1992.63 703.841   3
  -8  -1   1 2539.58 614.621   3
  -8   1   0 4796.23 1015.70   3
  -8   1   0 5837.20 996.808   1
  -8  -1   0 5486.92 843.238   3
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  -8   1  -1 3231.41 778.799   1
  -8  -1  -2 4823.12 856.839   3
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  -8   1  -3 9376.91 1411.71   1
  -8  -1  -4 2447.57 808.010   1
  -8   1  -4 1917.14 660.764   1
  -8  -1  -5 4492.86 983.982   1
  -8   1  -5 4361.77 1038.25   1
  -8  -1  -6 6.49303 317.291   1
  -8   1  -6-667.928 542.942   1
  -8  -1  -7 1698.86 524.748   1
   8  -1   7 2727.36 365.630   5
  -8   1  -7 3046.38 1025.76   1
   8   1   7 2683.94 358.885   9
  -8  -1  -8 2129.15 826.180   1
   8  -1   8 3390.50 408.656   5
  -8   1  -8 3215.22 997.403   1
   8   1   8 3083.42 391.612   9
  -8   1  -9-173.022 554.682   1
   8  -1   9 448.973 178.601   5
   8   1   9 433.141 184.021   9
  -8   1 -10 2356.41 792.577   1
   8  -1  10 1777.73 335.589   5
   8  -1  11 680.852 199.976  11
   8  -1  11 399.701 200.876   5
   8   1  11 484.146 187.854   9
   8  -1  12 1778.22 287.492  11
   8  -1  12 1379.12 297.789   5
   8   1  12 1313.64 273.128   9
   8  -1  12 1318.21 308.099   9
   8  -1  13 599.530 169.846  11
   8   1  13 882.907 250.552   9
   8  -1  13 669.974 190.596   9
   8  -1  14 761.424 198.204  11
   8   1  14 501.762 190.691   9
   8  -1  14 530.155 194.169   9
   8   1  15 309.465 149.481   9
   8  -1  15 148.029 106.943   9
   8  -1  16 272.695 117.660  11
   8  -1  16 37.8122 84.3234   9
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  -8  -2  15 6440.79 510.774  12
  -8  -2  14 768.710 218.768  12
  -8  -2  14 592.424 177.640   8
  -8  -2  13 240.189 167.633   8
  -8  -2  13 599.736 219.447  12
  -8   2  13 319.115 190.848   8
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  -8  -2  12-44.7377 128.895  12
  -8   2  12 204.074 178.766   8
  -8  -2  11 3960.41 476.498  12
  -8   2  11 4603.46 485.596   8
  -8  -2  11 4176.44 470.933   8
  -8   2  10 2476.45 360.390   8
  -8  -2  10 2563.59 379.463   8
  -8  -2  10 1713.64 329.700  12
  -8   2  10 2020.05 709.995   3
  -8   2   9 11909.2 1642.06   3
  -8  -2   9 12979.7 811.009  12
  -8   2   9 13094.2 770.567   8
  -8  -2   9 12586.9 762.042   8
  -8   2   8 1959.22 291.898   8
  -8  -2   8 1800.24 288.653   8
  -8   2   8 1787.12 648.199   3
  -8   2   7 376.043 459.970   3
  -8   2   6 12461.7 1545.86   3
  -8   2   5 7450.52 1208.84   3
  -8   2   4 1322.85 433.284   3
  -8   2   3 15004.2 1631.42   3
  -8   2   2 1618.75 508.050   3
  -8   2   1 8601.71 1337.04   3
  -8   2   1 7578.25 1125.86   1
  -8   2   0 5685.10 1157.84   3
  -8   2   0 5899.72 1027.25   1
  -8   2  -1 31820.1 2648.09   3
  -8   2  -1 32239.1 2434.62   1
  -8   2  -2 19133.7 1957.06   1
  -8   2  -3 4022.04 924.471   1
  -8   2  -4 6480.72 1329.25   1
  -8   2  -5 2740.36 862.597   1
   8   2   6 750.688 198.703   9
  -8   2  -6 434.455 551.698   1
   8  -2   6 889.510 230.217   5
   8  -2   7 23846.3 1056.79   5
  -8   2  -7 23868.9 2596.19   1
   8   2   7 22048.2 1023.04   9
   8  -2   8 2816.73 394.357   5
   8   2   8 2627.81 379.124   9
  -8   2  -8 2625.41 956.923   1
   8  -2   9 7448.55 619.977   5
   8   2   9 6964.13 601.297   9
  -8   2  -9 5815.08 1390.64   1
   8   2  10 2097.70 369.552   9
   8  -2  10 2079.62 336.761   5
   8  -2  11 18.3929 115.422  11
   8  -2  11 227.264 199.092   5
   8   2  11 37.2136 133.808   9
   8  -2  12 19.5479 117.797  11
   8  -2  12-95.0584 143.986   5
   8   2  12 64.6842 167.578   9
   8  -2  13 672.244 208.237  11
   8  -2  13 678.000 212.191   5
   8  -2  14-164.188 131.511  11
   8  -2  14 24.8835 116.435   9
   8  -2  15 183.774 115.478  11
   8  -2  15 256.573 140.039   9
   8  -2  16-66.2494 73.3403  11
   8  -2  16 139.538 100.663   9
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  -8  -3  13 908.859 231.767  12
  -8  -3  13 1162.64 258.573   8
  -8  -3  12 470.308 202.423   8
  -8  -3  12 852.907 237.299  12
  -8  -3  11 75.8257 147.592   8
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  -8  -3  10 266.743 187.133   8
  -8  -3  10 262.378 154.539  12
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  -8  -3   9 34.4721 146.816  12
  -8   3   9 282.079 351.510   3
  -8  -3   8 990.181 243.176   8
  -8   3   8 1322.95 278.915   7
  -8   3   8 1140.16 582.185   3
  -8  -3   7 976.244 225.211   8
  -8   3   7 1166.32 272.697   7
  -8   3   6 7093.01 577.405   7
  -8  -3   6 6158.99 527.810   8
  -8   3   5-42.5884 363.401   3
  -8   3   4-250.743 252.756   3
  -8   3   3-353.417 407.809   3
  -8   3   2-227.321 416.792   3
  -8   3   1 861.138 608.709   3
  -8   3   0 992.145 509.848   3
  -8   3  -1 2352.80 900.975   3
  -8   3  -1 1496.21 615.938   1
  -8   3  -2 1752.88 719.159   1
  -8   3  -3 38.6842 493.917   1
  -8   3  -4 555.572 504.148   1
   8  -3   5 85.9319 101.012  14
  -8   3  -5-332.465 462.097   1
   8  -3   6 1328.04 287.723  14
  -8   3  -6 2327.50 982.026   1
   8  -3   7 18896.4 953.645  14
  -8   3  -7 19397.3 2422.63   1
   8  -3   8 14904.6 874.357  14
   8  -3   8 15614.0 918.427   5
  -8   3  -8 17282.7 2316.10   1
   8  -3   9 776.191 254.700   5
   8  -3  10 1254.61 312.247   5
   8  -3  11-3.50961 140.527   5
   8  -3  12 2753.96 358.324  11
   8  -3  12 2113.78 343.102   5
   8  -3  13 1549.91 262.732  11
   8  -3  13 1380.74 270.124   5
   8   3  13 1315.96 216.205  10
   8  -3  14 359.750 139.947  11
   8  -3  14 385.769 166.083   5
   8  -3  14 572.683 179.813   9
   8  -3  15 840.240 159.464  11
   8  -3  15 1362.93 206.990   9
   8  -3  16 128.785 71.7324   9
  -8  -4  16 159.624 93.3264  12
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  -8  -4  13-62.7053 122.786  13
  -8  -4  13-117.081 140.470  12
  -8  -4  12 469.435 191.886  12
  -8  -4  12 611.180 178.717  13
  -8  -4  11 1118.76 249.603  13
  -8  -4  11 645.051 222.589  12
  -8  -4  10 140.316 169.434  12
  -8   4   9 2319.82 341.080   7
  -8  -4   9 2188.06 386.975  12
  -8   4   8 21293.5 1011.37   7
  -8   4   7 6428.05 583.208   7
  -8   4   7 7574.34 1329.60   3
  -8   4   6 19656.0 2097.74   3
  -8   4   6 15571.1 901.220   7
  -8   4   5 23169.8 2257.74   3
  -8   4   5 22997.5 1075.62   7
  -8   4   4 37136.9 2838.99   3
  -8   4   4 36042.7 1327.29   7
  -8   4   3 836.272 218.522   7
  -8   4   3 1609.52 754.093   3
  -8   4   2 124.845 147.199   7
  -8   4   2 257.022 370.708   3
  -8   4   1 1938.72 336.297   7
  -8   4   1 875.722 433.839   3
  -8   4   0 6712.41 1311.05   3
  -8   4   0 7937.44 601.091   7
  -8   4  -1 215.881 644.788   3
  -8   4  -1-56.1667 129.183   7
  -8   4  -2 3153.59 1032.47   3
   8  -4   2 2495.73 328.106  14
  -8   4  -2 2577.10 370.730   7
  -8   4  -3 449.838 516.968   3
   8  -4   3 425.731 199.979  14
  -8   4  -3 394.678 206.336   7
   8  -4   4-218.890 142.716  14
  -8   4  -4 47.7017 155.232   7
  -8   4  -4-188.433 351.349   1
   8  -4   5 1486.20 309.437  14
  -8   4  -5 848.428 575.434   1
   8  -4   6 1618.63 306.383  14
  -8   4  -6 2263.15 844.830   1
   8  -4   7 2351.56 379.792  14
   8  -4   8 54.6124 165.989  14
   8  -4   9-24.4818 158.031  14
   8  -4   9-10.8486 149.848   5
   8  -4  10 1167.41 278.218   5
   8  -4  11 280.310 181.237   5
   8   4  12 1406.77 244.497  10
   8  -4  12 453.957 190.371   5
   8  -4  13 133.351 133.616  11
   8   4  13 135.276 124.026  10
   8  -4  13 226.139 135.551   5
   8  -4  14-5.85882 93.0730  11
   8  -4  14 90.8892 87.3494   5
   8  -4  15 414.321 111.049   9
  -8  -5  15 628.984 120.912  12
  -8  -5  14 976.995 185.901  12
  -8  -5  13 1434.74 258.753  12
  -8  -5  12 58.7462 127.900  12
  -8  -5  11 196.819 149.012  12
  -8  -5  10 516.281 220.016  12
  -8   5   9 206.177 152.581   7
  -8  -5   9 640.364 235.296  12
  -8   5   8 1166.14 265.475   7
  -8   5   7 625.643 254.363   7
  -8   5   6-78.2252 169.566   7
  -8   5   5 791.658 217.405   7
  -8   5   4 295.046 227.279   7
  -8   5   3 33.1894 175.087   7
  -8   5   3 1183.80 581.380   3
  -8   5   2 129.321 160.918   7
   8   5  -2-108.377 248.329   2
  -8   5   2-401.572 353.926   3
  -8   5   1 139.462 208.659   7
   8   5  -1 831.628 490.181   2
  -8   5   0-125.506 165.419   7
  -8   5   0 186.717 393.328   3
  -8   5  -1 195.287 225.884   7
  -8   5  -1 577.104 454.864   3
  -8   5  -2-29.6552 196.059   7
   8  -5   3 500.559 175.293  14
  -8   5  -3 669.505 232.002   7
   8  -5   4 48.8925 119.667  14
  -8   5  -4 255.516 227.915   7
   8  -5   5 587.207 212.883  14
   8  -5   6 810.823 246.314  14
   8  -5   7 266.117 204.656  14
   8  -5   8-38.5543 145.203  14
   8   5   9 741.297 220.255  10
   8  -5   9 649.284 220.733   5
   8   5  10 384.446 147.362  10
   8  -5  10 493.334 234.492   5
   8   5  11 227.759 129.203  10
   8  -5  11 90.1097 151.954   5
   8  -5  12 337.765 115.753  11
   8   5  12 186.981 111.436  10
   8  -5  12 104.106 109.311   5
   8  -5  13 245.068 103.483  11
   8   5  13 100.746 85.9464  10
   8  -5  13 94.5981 109.845   5
   8  -5  14 1393.79 167.704   9
  -8  -6  13 222.364 95.9701  12
  -8  -6  12 227.386 150.773  12
  -8  -6  11 34.3960 124.657  12
  -8  -6  10 370.928 170.638  12
  -8   6   9-89.7151 121.700   7
  -8  -6   9 89.2764 171.564  12
  -8   6   8-9.66496 149.040   7
  -8  -6   8 115.121 179.984  12
  -8   6   7 179.883 186.403   7
  -8   6   6 2462.19 366.895   7
  -8   6   5 12376.9 804.129   7
  -8   6   4 11260.5 774.104   7
  -8   6   3 368.242 178.655   7
  -8   6   2 111.759 157.874   7
  -8   6   1 753.839 256.226   7
  -8   6   0 219.163 229.006   7
   8   6   0-106.740 163.161  10
  -8   6  -1 246.148 204.305   7
   8   6   1 177.639 121.226  10
  -8   6  -2-12.1504 175.283   7
   8   6   2 18.9834 126.733  10
   8  -6   3 2120.38 322.155  14
  -8   6  -3 1999.25 338.033   7
   8   6   3 1743.75 303.587  10
   8  -6   4-44.8612 143.009  14
  -8   6  -4 6.51947 153.250   7
   8   6   4 23.8753 114.824  10
   8  -6   5 386.589 166.388  14
   8   6   5 152.633 133.327  10
   8  -6   6 4373.11 428.722  14
   8   6   6 3616.18 401.749  10
   8  -6   7 1957.83 302.304  14
   8   6   7 1627.36 290.656  10
   8   6   8 339.988 165.839  10
   8  -6   8 423.929 183.489   5
   8   6   9-85.7243 109.060  10
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   9   0   7 4950.03 499.607   5
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   9   0   9 23930.7 1110.93   9
   9   0  10-79.6733 163.395   9
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   9   0  12 26.4943 142.409   9
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   9  -1   6 1964.73 319.576   5
   9   1   6 2027.58 317.966   9
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   9  -1   7 8967.11 658.309   5
   9   1   7 7603.60 610.365   9
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   9  -1   8 58707.4 1749.35   5
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   9   1   8 59417.7 1729.86   9
   9  -1   9 5765.34 552.247   5
   9   1   9 5959.74 551.736   9
   9  -1  10 7094.08 616.301   5
   9   1  10 7095.99 629.685   9
   9  -1  11 875.197 248.852   5
   9   1  11 717.943 209.569   9
   9   1  12 648.824 194.477   9
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   9  -1  13 1405.74 291.488   9
   9   1  14 63.9241 129.567   9
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   9   2   5-135.057 118.792   9
   9  -2   5-134.638 181.796   5
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   9  -2   6 8942.81 662.963   5
   9   2   6 7890.94 618.185   9
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   9  -2   7 6725.56 589.392   5
   9   2   7 6112.62 573.877   9
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   9  -2   8 6506.65 595.862   5
   9   2   8 6554.56 586.328   9
   9  -2   9-24.2708 136.208   5
   9   2   9 3.66544 130.961   9
   9  -2  10 107.089 144.717   5
   9   2  10 72.2116 169.760   9
   9  -2  11 330.571 182.877   5
   9   2  11 485.849 214.409   9
   9  -2  12 416.130 195.517   5
   9   2  12 420.039 161.117   9
   9  -2  13 188.256 150.000   9
   9  -2  14 1001.24 215.297   9
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   9  -2  16 955.142 141.164   9
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   9  -3   5 535.700 165.065   5
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   9  -3   6 250.906 207.861   5
   9  -3   7 7153.70 632.074   5
   9  -3   8 155.010 126.702   5
   9  -3   9 728.791 239.567   5
   9  -3  10 2940.29 409.245   5
   9  -3  11 1428.45 279.203  11
   9  -3  11 1337.16 280.015   5
   9  -3  12 1783.21 282.826  11
   9  -3  12 1275.22 250.993   5
   9  -3  13 572.666 174.472  11
   9  -3  13 574.353 206.064   5
   9   3  13 433.877 158.657  10
   9  -3  14 182.421 130.979   9
   9  -3  15 3730.87 301.085   9
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  -9   4   8 6089.24 553.449   7
  -9   4   7 163.384 191.923   4
  -9   4   7 476.992 204.184   7
  -9   4   6 12980.8 829.480   7
  -9   4   5 3961.34 483.123   7
  -9   4   5 3857.00 975.932   3
  -9   4   4 4118.45 494.009   7
  -9   4   4 3822.00 887.349   3
  -9   4   3 4669.24 532.086   7
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  -9   4   2 5339.90 1169.19   3
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   9  -4   3 123.623 137.567  14
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   9  -4   4 38.4847 157.523  14
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   9  -4   5 158.505 176.941  14
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   9  -4   7 1721.23 325.931   5
   9  -4   8 98.9732 134.422   5
   9  -4   9 861.183 257.478   5
   9  -4  10 43.2300 164.328   5
   9  -4  11 12.3260 132.826   5
   9  -4  12 287.506 118.501  11
   9   4  12 200.581 123.023  10
   9  -4  12 248.838 158.591   5
   9  -4  13 90.0075 83.6653  11
   9   4  13 19.2711 90.2490  10
   9  -4  13 173.419 131.849   5
   9  -4  14 63.3485 71.0805   9
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  -9   5   7-210.719 194.036   7
  -9   5   6 183.729 176.137   7
  -9   5   5 50.9379 172.504   7
  -9   5   4 1369.34 329.646   7
  -9   5   3 260.482 232.186   7
  -9   5   2-110.586 163.026   7
  -9   5   1 508.341 238.833   7
  -9   5   0 528.032 242.315   7
  -9   5  -1 120.586 187.059   7
  -9   5  -2 153.234 184.914   7
   9  -5   3 2466.70 341.630  14
  -9   5  -3 2979.22 395.880   7
   9  -5   4 512.389 193.845  14
   9  -5   5 243.479 180.127  14
  -9   5  -6 913.816 258.588   4
   9  -5   7 1648.34 294.681   5
   9  -5   8 2219.01 372.475   5
   9   5   9 163.267 156.813  10
   9  -5   9 73.0019 153.519   5
   9   5  10 167.166 141.980  10
   9  -5  10 209.798 167.745   5
   9  -5  11 114.395 92.3076  11
   9   5  11 12.5304 93.1493  10
   9  -5  11 82.2937 122.890   5
   9  -5  12 1395.22 182.967  11
   9   5  12 997.301 173.386  10
   9  -5  12 1049.79 204.240   5
   9  -5  13 287.483 109.485   5
   9  -5  13 431.298 111.816   9
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  -9  -6   8 1212.39 256.662  12
  -9   6   7 470.543 178.562   4
  -9   6   7 439.522 201.302   7
  -9  -6   7 935.070 266.519  12
  -9   6   6 908.869 275.063   7
  -9   6   5 267.834 190.206   7
  -9   6   4 280.942 219.262   7
  -9   6   3 920.081 306.593   7
  -9   6   2 270.062 186.587   7
  -9   6   1 954.549 278.994   7
  -9   6   0 1568.46 344.701   7
   9   6   0 990.362 223.719  10
  -9   6  -1 1321.62 287.582   7
   9   6   1 1103.42 231.267  10
  -9   6  -2 314.550 208.656   7
   9   6   2 378.373 173.805  10
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   9   6   3 703.060 200.892  10
   9   6   4 91.1806 175.277  10
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   9   6   5 110.787 177.149  10
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   9   6   6-133.952 138.891  10
   9  -6   6 76.7314 150.366   5
   9   6   7 287.354 163.209  10
   9  -6   7 218.388 149.211   5
   9   6   8 209.663 130.895  10
   9  -6   8-49.0609 141.870   5
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 -17   0   3 152.730 116.961   8
 -17   0   2 106.923 117.987   8
 -17   0   1 311.981 139.044   8
 -17   0   0 202.209 128.004   8
 -17   0  -1 266.212 123.670   8
 -17   0  -2 6.29526 112.864   8
 -17   0  -3-63.1166 94.7453   8
 -17   0  -4 34.2415 69.6811   8
 -17  -1   7 567.455 128.947   8
 -17  -1   6 96.1618 84.2154   8
 -17   1   5 228.803 84.4157   8
 -17  -1   5 107.224 97.1802   8
 -17   1   4 11.9537 68.9750   8
 -17  -1   4 120.172 123.123   8
 -17   1   3 298.482 99.4140   8
 -17  -1   3 340.337 141.932   8
 -17   1   2 842.181 148.426   8
 -17  -1   2 185.152 127.528   8
 -17   1   1 777.387 142.203   8
 -17  -1   1 743.491 161.990   8
 -17   1   0 219.117 86.9116   8
 -17  -1   0 311.887 155.649   8
 -17   1  -1 847.989 134.879   8
 -17  -1  -1 748.778 173.184   8
 -17  -1  -2-44.8335 103.580   8
 -17  -1  -3 729.561 151.651   8
 -17  -1  -4 499.696 122.670   8
 -17  -1  -5 106.845 84.0906   8
 -17  -2   6 220.857 85.3780   8
 -17  -2   5 416.713 114.431   8
 -17  -2   4 337.271 131.728   8
 -17  -2   3 454.098 151.902   8
 -17  -2   2 1709.96 223.005   8
 -17  -2   1 156.811 114.772   8
 -17  -2   0-150.195 115.636   8
 -17  -2  -1 264.466 117.909   8
 -17  -2  -2 618.635 133.157   8
 -17  -2  -3 207.095 89.8144   8
 -17  -2  -4 58.2919 92.5719   8
 -17  -3   1 138.634 73.9517   8
   0   0   0    0.00    0.00   0
TITL e2672kam in P2(1)/n
REM P2(1)/n (#14 in standard setting)
CELL 1.54184  14.351249   7.586707  16.228237  90.0000  93.5444  90.0000
ZERR    8.00   0.001192   0.000625   0.000950   0.0000   0.0068   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H N O
UNIT 88.00 80.00 8.00 8.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              67375
_shelx_res_file
;
    2672.res created by SHELXL-2014/7
TITL SIR92 run in space group P 1 21/n 1
CELL 1.54184 14.3512 7.5867 16.2282 90 93.544 90
ZERR 4 0.0012 0.0006 0.0009 0 0.007 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H N O Cl
UNIT 64 76 24 8 4
L.S. 4
PLAN  20
TEMP 25
BOND $H
CONF
MORE -1
fmap 2
acta
DFIX 0.90 O1w H1W1
DFIX 0.90 O1w H2W1
DFIX 0.90 O2w H1W2
DFIX 0.90 O2w H2W2
WGHT    0.051400
FVAR       4.11957
CL1   5    0.382995    0.884037    0.760440    11.00000    0.08809    0.08412 =
         0.04310   -0.00391    0.00152   -0.00308
O1W   4    0.329288    0.488511    0.720131    11.00000    0.08203    0.08066 =
         0.05655   -0.00629    0.00212    0.00590
O2W   4    0.478937    0.265925    0.780576    11.00000    0.06118    0.09713 =
         0.10920   -0.01102   -0.00510    0.00334
N1A   3    0.288517    0.917599    0.342963    11.00000    0.04045    0.05302 =
         0.03286    0.00069   -0.00213   -0.00071
C2A   1    0.370835    0.842973    0.355624    11.00000    0.04001    0.05173 =
         0.04093   -0.00313    0.00754   -0.00345
AFIX  43
H2AA  2    0.400716    0.805221    0.309540    11.00000   -1.20000
AFIX   0
N3A   3    0.414598    0.817351    0.429149    11.00000    0.03332    0.04983 =
         0.03962    0.00065    0.00506    0.00553
C4A   1    0.371311    0.871731    0.497124    11.00000    0.03920    0.04152 =
         0.03820   -0.00207    0.00376   -0.00007
C4AA  1    0.280135    0.955920    0.489074    11.00000    0.03458    0.03797 =
         0.04387    0.00211    0.00127    0.00013
C5A   1    0.231334    1.013458    0.555948    11.00000    0.05241    0.05280 =
         0.03989    0.00103    0.00296    0.00336
AFIX  43
H5AA  2    0.257794    1.001001    0.609403    11.00000   -1.20000
AFIX   0
C6A   1    0.145581    1.087378    0.543316    11.00000    0.05462    0.05545 =
         0.05686   -0.00469    0.01651    0.00846
AFIX  43
H6AA  2    0.113268    1.124804    0.588075    11.00000   -1.20000
AFIX   0
C7A   1    0.105605    1.107406    0.462762    11.00000    0.03445    0.04887 =
         0.07511   -0.00002    0.00585    0.01046
AFIX  43
H7AA  2    0.046840    1.158440    0.454592    11.00000   -1.20000
AFIX   0
C8A   1    0.151974    1.052770    0.395866    11.00000    0.04685    0.04733 =
         0.04528    0.00402   -0.00747   -0.00296
AFIX  43
H8AA  2    0.125254    1.066354    0.342563    11.00000   -1.20000
AFIX   0
C8AA  1    0.239952    0.976488    0.409425    11.00000    0.03767    0.03732 =
         0.04094    0.00185    0.00680   -0.00319
N9A   3    0.415345    0.842183    0.567702    11.00000    0.04058    0.07159 =
         0.03905   -0.00449    0.00092    0.01333
N1B   3    0.284227    0.426529    0.320158    11.00000    0.04435    0.05366 =
         0.03200   -0.00110   -0.00133    0.00249
C2B   1    0.365710    0.357848    0.342015    11.00000    0.04228    0.05274 =
         0.03967   -0.00323    0.00603    0.00290
AFIX  43
H2BA  2    0.400964    0.320320    0.299130    11.00000   -1.20000
AFIX   0
N3B   3    0.404701    0.334830    0.418439    11.00000    0.03381    0.05629 =
         0.03906   -0.00416    0.00101    0.00663
C4B   1    0.356378    0.391555    0.481858    11.00000    0.03401    0.04364 =
         0.03685   -0.00406    0.00082   -0.00079
C4AB  1    0.265213    0.469549    0.466621    11.00000    0.03368    0.03460 =
         0.03920    0.00011    0.00105   -0.00103
C5B   1    0.208647    0.526947    0.529241    11.00000    0.04178    0.04989 =
         0.03667   -0.00001    0.00652    0.00156
AFIX  43
H5BA  2    0.230446    0.518080    0.584254    11.00000   -1.20000
AFIX   0
C6B   1    0.122149    0.595445    0.509905    11.00000    0.04202    0.05054 =
         0.05457   -0.00334    0.01377    0.00293
AFIX  43
H6BA  2    0.085635    0.634530    0.551631    11.00000   -1.20000
AFIX   0
C7B   1    0.088343    0.606934    0.427373    11.00000    0.03140    0.04870 =
         0.06427    0.00733    0.00312    0.00598
AFIX  43
H7BA  2    0.028968    0.652157    0.414604    11.00000   -1.20000
AFIX   0
C8B   1    0.141888    0.552172    0.365118    11.00000    0.03980    0.04705 =
         0.04407    0.00641   -0.00418    0.00026
AFIX  43
H8BA  2    0.118903    0.561535    0.310444    11.00000   -1.20000
AFIX   0
C8AB  1    0.231122    0.482140    0.383541    11.00000    0.03605    0.04023 =
         0.03881   -0.00123    0.00275   -0.00187
N9B   3    0.395419    0.370915    0.557244    11.00000    0.03908    0.07158 =
         0.03663   -0.00582   -0.00150    0.01120
H1A   2    0.259357    0.929019    0.283534    11.00000    0.05989
H9AA  2    0.472249    0.788612    0.569475    11.00000    0.06218
H9AB  2    0.389617    0.880081    0.616861    11.00000    0.10255
H9BA  2    0.452866    0.308351    0.564774    11.00000    0.05745
H9BB  2    0.369588    0.405994    0.596426    11.00000    0.04731
H1W1  2    0.344721    0.601320    0.733188    11.00000    0.10905
H2W1  2    0.271018    0.497300    0.735684    11.00000    0.18996
H1W2  2    0.436690    0.345906    0.758959    11.00000   -1.00000
H2W2  2    0.436640    0.183098    0.766387    11.00000    0.14989
HKLF 4
REM  SIR92 run in space group P 1 21/n 1
REM R1 =  0.0541 for    2207 Fo > 4sig(Fo)  and  0.0931 for all    3563 data
REM    261 parameters refined using      4 restraints
END
WGHT      0.0516      0.0000
REM Highest difference peak  0.231,  deepest hole -0.215,  1-sigma level  0.047
Q1    1   0.2398  0.4391  0.4220  11.00000  0.05    0.23
Q2    1   0.2648  0.9644  0.4569  11.00000  0.05    0.22
Q3    1   0.3274  0.9210  0.5643  11.00000  0.05    0.20
Q4    1   0.3483  0.9871  0.7217  11.00000  0.05    0.18
Q5    1   0.2569  0.5138  0.4315  11.00000  0.05    0.18
Q6    1   0.1796  0.9623  0.4032  11.00000  0.05    0.18
Q7    1   0.4584  0.7485  0.4441  11.00000  0.05    0.18
Q8    1   0.1192  0.6530  0.4803  11.00000  0.05    0.17
Q9    1   0.1186  1.0533  0.5028  11.00000  0.05    0.16
Q10   1   0.2747  0.7039  0.4224  11.00000  0.05    0.16
Q11   1   0.4671  0.3043  0.4334  11.00000  0.05    0.16
Q12   1   0.3372  0.8329  0.7179  11.00000  0.05    0.16
Q13   1   0.3119  0.9180  0.4984  11.00000  0.05    0.16
Q14   1   0.2458  0.7482  0.5225  11.00000  0.05    0.16
Q15   1   0.2372  0.2678  0.6992  11.00000  0.05    0.15
Q16   1   0.3144  0.4422  0.4795  11.00000  0.05    0.15
Q17   1   0.1962  0.5289  0.3758  11.00000  0.05    0.15
Q18   1   0.1725  1.0017  0.5459  11.00000  0.05    0.15
Q19   1   0.2620  1.2459  0.5436  11.00000  0.05    0.15
Q20   1   0.2375  0.3238  0.7597  11.00000  0.05    0.15
;
_shelx_res_checksum              63090
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cl Cl1 0.38300(8) 0.88404(15) 0.76044(5) 0.0719(3) Uani d 1 . .
O O1W 0.3293(2) 0.4885(5) 0.72013(16) 0.0732(8) Uani d 1 . .
O O2W 0.4789(2) 0.2659(6) 0.7806(2) 0.0896(10) Uani d 1 . .
N N1A 0.28852(17) 0.9176(4) 0.34296(12) 0.0423(6) Uani d 1 . .
C C2A 0.3708(2) 0.8430(4) 0.35562(16) 0.0440(7) Uani d 1 . .
H H2AA 0.4007 0.8052 0.3095 0.053 Uiso calc 1 . .
N N3A 0.41460(17) 0.8174(4) 0.42915(13) 0.0408(5) Uani d 1 . .
C C4A 0.3713(2) 0.8717(4) 0.49712(16) 0.0396(6) Uani d 1 . .
C C4AA 0.28014(19) 0.9559(4) 0.48907(16) 0.0389(6) Uani d 1 . .
C C5A 0.2313(2) 1.0135(5) 0.55595(17) 0.0484(7) Uani d 1 . .
H H5AA 0.2578 1.0010 0.6094 0.058 Uiso calc 1 . .
C C6A 0.1456(2) 1.0874(5) 0.5433(2) 0.0551(8) Uani d 1 . .
H H6AA 0.1133 1.1248 0.5881 0.066 Uiso calc 1 . .
C C7A 0.1056(2) 1.1074(5) 0.4628(2) 0.0527(7) Uani d 1 . .
H H7AA 0.0468 1.1584 0.4546 0.063 Uiso calc 1 . .
C C8A 0.1520(2) 1.0528(4) 0.39587(17) 0.0469(7) Uani d 1 . .
H H8AA 0.1253 1.0664 0.3426 0.056 Uiso calc 1 . .
C C8AA 0.23995(19) 0.9765(4) 0.40943(16) 0.0385(6) Uani d 1 . .
N N9A 0.41535(19) 0.8422(4) 0.56770(14) 0.0505(7) Uani d 1 . .
N N1B 0.28423(18) 0.4265(4) 0.32016(12) 0.0435(6) Uani d 1 . .
C C2B 0.3657(2) 0.3578(4) 0.34201(16) 0.0447(7) Uani d 1 . .
H H2BA 0.4010 0.3203 0.2991 0.054 Uiso calc 1 . .
N N3B 0.40470(17) 0.3348(4) 0.41844(14) 0.0431(6) Uani d 1 . .
C C4B 0.35638(19) 0.3916(4) 0.48186(15) 0.0382(6) Uani d 1 . .
C C4AB 0.26521(19) 0.4695(4) 0.46662(15) 0.0359(5) Uani d 1 . .
C C5B 0.2086(2) 0.5269(4) 0.52924(16) 0.0426(6) Uani d 1 . .
H H5BA 0.2304 0.5181 0.5843 0.051 Uiso calc 1 . .
C C6B 0.1221(2) 0.5954(4) 0.50991(19) 0.0486(7) Uani d 1 . .
H H6BA 0.0856 0.6345 0.5516 0.058 Uiso calc 1 . .
C C7B 0.0883(2) 0.6069(4) 0.42737(19) 0.0481(7) Uani d 1 . .
H H7BA 0.0290 0.6522 0.4146 0.058 Uiso calc 1 . .
C C8B 0.1419(2) 0.5522(4) 0.36512(16) 0.0439(7) Uani d 1 . .
H H8BA 0.1189 0.5615 0.3104 0.053 Uiso calc 1 . .
C C8AB 0.23112(19) 0.4821(4) 0.38354(15) 0.0383(6) Uani d 1 . .
N N9B 0.39542(19) 0.3709(4) 0.55724(14) 0.0493(7) Uani d 1 . .
H H1A 0.259(3) 0.929(5) 0.284(2) 0.060(10) Uiso d 1 . .
H H9AA 0.472(3) 0.789(5) 0.569(2) 0.062(11) Uiso d 1 . .
H H9AB 0.390(4) 0.880(7) 0.617(3) 0.103(17) Uiso d 1 . .
H H9BA 0.453(3) 0.308(5) 0.565(2) 0.057(10) Uiso d 1 . .
H H9BB 0.370(3) 0.406(5) 0.596(2) 0.047(9) Uiso d 1 . .
H H1W1 0.345(4) 0.601(4) 0.733(3) 0.11(2) Uiso d 1 . .
H H2W1 0.271(2) 0.497(11) 0.736(4) 0.19(4) Uiso d 1 . .
H H1W2 0.437(5) 0.346(8) 0.759(5) 0.190 Uiso d 1 . .
H H2W2 0.437(4) 0.183(7) 0.766(4) 0.15(3) Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Cl1 0.0881(7) 0.0841(7) 0.0431(4) -0.0031(6) 0.0015(4) -0.0039(4)
O1W 0.082(2) 0.081(2) 0.0566(13) 0.0059(17) 0.0021(13) -0.0063(14)
O2W 0.0612(18) 0.097(3) 0.109(2) 0.0033(19) -0.0051(17) -0.011(2)
N1A 0.0404(13) 0.0530(16) 0.0329(10) -0.0007(11) -0.0021(9) 0.0007(10)
C2A 0.0400(15) 0.0517(18) 0.0409(12) -0.0035(13) 0.0075(11) -0.0031(12)
N3A 0.0333(11) 0.0498(15) 0.0396(10) 0.0055(10) 0.0051(9) 0.0006(10)
C4A 0.0392(14) 0.0415(15) 0.0382(12) -0.0001(12) 0.0038(10) -0.0021(11)
C4AA 0.0346(14) 0.0380(15) 0.0439(13) 0.0001(12) 0.0013(10) 0.0021(11)
C5A 0.0524(18) 0.0528(19) 0.0399(13) 0.0034(15) 0.0030(12) 0.0010(12)
C6A 0.0546(19) 0.055(2) 0.0569(16) 0.0085(16) 0.0165(14) -0.0047(15)
C7A 0.0345(15) 0.0489(18) 0.0751(19) 0.0105(14) 0.0058(13) 0.0000(16)
C8A 0.0469(17) 0.0473(18) 0.0453(13) -0.0030(14) -0.0075(12) 0.0040(12)
C8AA 0.0377(14) 0.0373(14) 0.0409(12) -0.0032(12) 0.0068(10) 0.0018(11)
N9A 0.0406(14) 0.072(2) 0.0390(11) 0.0133(13) 0.0009(10) -0.0045(11)
N1B 0.0443(13) 0.0537(16) 0.0320(9) 0.0025(12) -0.0013(9) -0.0011(10)
C2B 0.0423(15) 0.0527(18) 0.0397(12) 0.0029(13) 0.0060(11) -0.0032(12)
N3B 0.0338(12) 0.0563(16) 0.0391(10) 0.0066(11) 0.0010(9) -0.0042(10)
C4B 0.0340(13) 0.0436(15) 0.0368(11) -0.0008(12) 0.0008(10) -0.0041(11)
C4AB 0.0337(13) 0.0346(14) 0.0392(12) -0.0010(11) 0.0011(10) 0.0001(10)
C5B 0.0418(15) 0.0499(17) 0.0367(12) 0.0016(13) 0.0065(10) 0.0000(12)
C6B 0.0420(16) 0.0505(18) 0.0546(15) 0.0029(14) 0.0138(12) -0.0033(14)
C7B 0.0314(14) 0.0487(18) 0.0643(16) 0.0060(13) 0.0031(12) 0.0073(15)
C8B 0.0398(15) 0.0471(17) 0.0441(13) 0.0003(13) -0.0042(11) 0.0064(12)
C8AB 0.0360(14) 0.0402(15) 0.0388(12) -0.0019(12) 0.0028(10) -0.0012(11)
N9B 0.0391(14) 0.072(2) 0.0366(11) 0.0112(13) -0.0015(10) -0.0058(12)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
H1W1 O1W H2W1 . . 95(6) ?
H1W2 O2W H2W2 . . 87(6) ?
C2A N1A C8AA . . 120.3(2) ?
C2A N1A H1A . . 119(2) ?
C8AA N1A H1A . . 120(2) ?
N1A C2A N3A . . 125.0(3) ?
N1A C2A H2AA . . 117.5 ?
N3A C2A H2AA . . 117.5 ?
C2A N3A C4A . . 118.0(2) ?
N9A C4A N3A . . 116.2(3) ?
N9A C4A C4AA . . 122.9(3) ?
N3A C4A C4AA . . 120.8(2) ?
C8AA C4AA C5A . . 119.2(3) ?
C8AA C4AA C4A . . 116.8(2) ?
C5A C4AA C4A . . 124.0(2) ?
C6A C5A C4AA . . 120.4(3) ?
C6A C5A H5AA . . 119.8 ?
C4AA C5A H5AA . . 119.8 ?
C5A C6A C7A . . 120.0(3) ?
C5A C6A H6AA . . 120.0 ?
C7A C6A H6AA . . 120.0 ?
C8A C7A C6A . . 120.9(3) ?
C8A C7A H7AA . . 119.5 ?
C6A C7A H7AA . . 119.5 ?
C7A C8A C8AA . . 118.6(3) ?
C7A C8A H8AA . . 120.7 ?
C8AA C8A H8AA . . 120.7 ?
C4AA C8AA N1A . . 119.0(3) ?
C4AA C8AA C8A . . 120.8(3) ?
N1A C8AA C8A . . 120.2(2) ?
C4A N9A H9AA . . 120(2) ?
C4A N9A H9AB . . 120(3) ?
H9AA N9A H9AB . . 120(4) ?
C2B N1B C8AB . . 116.4(2) ?
N1B C2B N3B . . 128.1(3) ?
N1B C2B H2BA . . 115.9 ?
N3B C2B H2BA . . 115.9 ?
C2B N3B C4B . . 117.4(2) ?
N9B C4B N3B . . 117.4(3) ?
N9B C4B C4AB . . 122.3(3) ?
N3B C4B C4AB . . 120.3(2) ?
C5B C4AB C8AB . . 119.2(3) ?
C5B C4AB C4B . . 124.1(2) ?
C8AB C4AB C4B . . 116.7(2) ?
C6B C5B C4AB . . 120.6(2) ?
C6B C5B H5BA . . 119.7 ?
C4AB C5B H5BA . . 119.7 ?
C5B C6B C7B . . 120.1(3) ?
C5B C6B H6BA . . 120.0 ?
C7B C6B H6BA . . 120.0 ?
C8B C7B C6B . . 120.6(3) ?
C8B C7B H7BA . . 119.7 ?
C6B C7B H7BA . . 119.7 ?
C7B C8B C8AB . . 120.3(2) ?
C7B C8B H8BA . . 119.9 ?
C8AB C8B H8BA . . 119.9 ?
N1B C8AB C8B . . 119.7(2) ?
N1B C8AB C4AB . . 121.1(3) ?
C8B C8AB C4AB . . 119.2(3) ?
C4B N9B H9BA . . 119(2) ?
C4B N9B H9BB . . 120(3) ?
H9BA N9B H9BB . . 120(3) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
O1W H1W1 . 0.91(2) ?
O1W H2W1 . 0.89(2) ?
O2W H1W2 . 0.91(2) ?
O2W H2W2 . 0.89(2) ?
N1A C2A . 1.315(4) y
N1A C8AA . 1.393(4) ?
N1A H1A . 1.03(4) ?
C2A N3A . 1.328(4) y
C2A H2AA . 0.9300 ?
N3A C4A . 1.363(4) y
C4A N9A . 1.293(4) y
C4A C4AA . 1.455(4) ?
C4AA C8AA . 1.391(4) ?
C4AA C5A . 1.397(4) ?
C5A C6A . 1.356(5) ?
C5A H5AA . 0.9300 ?
C6A C7A . 1.403(5) ?
C6A H6AA . 0.9300 ?
C7A C8A . 1.372(5) ?
C7A H7AA . 0.9300 ?
C8A C8AA . 1.394(4) ?
C8A H8AA . 0.9300 ?
N9A H9AA . 0.91(4) ?
N9A H9AB . 0.94(5) ?
N1B C2B . 1.309(4) y
N1B C8AB . 1.383(4) ?
C2B N3B . 1.340(4) y
C2B H2BA . 0.9300 ?
N3B C4B . 1.347(4) y
C4B N9B . 1.323(4) y
C4B C4AB . 1.443(4) ?
C4AB C5B . 1.408(4) ?
C4AB C8AB . 1.409(4) ?
C5B C6B . 1.364(4) ?
C5B H5BA . 0.9300 ?
C6B C7B . 1.399(4) ?
C6B H6BA . 0.9300 ?
C7B C8B . 1.371(4) ?
C7B H7BA . 0.9300 ?
C8B C8AB . 1.402(4) ?
C8B H8BA . 0.9300 ?
N9B H9BA . 0.95(4) ?
N9B H9BB . 0.80(4) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N1A H1A N1B 2_555 1.03(3) 1.76(3) 2.786(3) 173(3) y
N9A H9AA N3B 3_666 0.91(4) 2.00(4) 2.907(4) 175(3) y
N9A H9AB Cl1 . 0.94(5) 2.34(5) 3.206(2) 153(5) y
N9B H9BA N3A 3_666 0.96(4) 2.12(4) 3.074(4) 174(3) y
N9B H9BB O1W . 0.79(4) 2.22(3) 2.999(4) 167(4) y
O1W H1W1 Cl1 . 0.90(3) 2.25(3) 3.157(4) 178(6) y
O1W H2W1 Cl1 2_546 0.89(4) 2.37(4) 3.183(3) 151(7) y
O2W H1W2 O1W . 0.91(7) 1.96(7) 2.857(5) 169(6) y
O2W H2W2 Cl1 1_545 0.89(5) 2.40(5) 3.215(4) 153(5) y
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
C8AA N1A C2A N3A . . . . -0.2(5) ?
N1A C2A N3A C4A . . . . 0.2(5) ?
C2A N3A C4A N9A . . . . 179.0(3) ?
C2A N3A C4A C4AA . . . . -0.3(4) ?
N9A C4A C4AA C8AA . . . . -178.8(3) ?
N3A C4A C4AA C8AA . . . . 0.4(4) ?
N9A C4A C4AA C5A . . . . 0.2(5) ?
N3A C4A C4AA C5A . . . . 179.4(3) ?
C8AA C4AA C5A C6A . . . . 0.4(5) ?
C4A C4AA C5A C6A . . . . -178.5(3) ?
C4AA C5A C6A C7A . . . . -0.4(6) ?
C5A C6A C7A C8A . . . . 0.1(6) ?
C6A C7A C8A C8AA . . . . 0.0(5) ?
C5A C4AA C8AA N1A . . . . -179.5(3) ?
C4A C4AA C8AA N1A . . . . -0.4(4) ?
C5A C4AA C8AA C8A . . . . -0.2(5) ?
C4A C4AA C8AA C8A . . . . 178.8(3) ?
C2A N1A C8AA C4AA . . . . 0.3(4) ?
C2A N1A C8AA C8A . . . . -178.9(3) ?
C7A C8A C8AA C4AA . . . . 0.0(5) ?
C7A C8A C8AA N1A . . . . 179.2(3) ?
C8AB N1B C2B N3B . . . . -0.2(5) ?
N1B C2B N3B C4B . . . . -1.5(5) ?
C2B N3B C4B N9B . . . . -179.1(3) ?
C2B N3B C4B C4AB . . . . 1.6(5) ?
N9B C4B C4AB C5B . . . . -1.5(5) ?
N3B C4B C4AB C5B . . . . 177.8(3) ?
N9B C4B C4AB C8AB . . . . -179.3(3) ?
N3B C4B C4AB C8AB . . . . 0.0(4) ?
C8AB C4AB C5B C6B . . . . -0.6(5) ?
C4B C4AB C5B C6B . . . . -178.4(3) ?
C4AB C5B C6B C7B . . . . 0.9(5) ?
C5B C6B C7B C8B . . . . -0.9(5) ?
C6B C7B C8B C8AB . . . . 0.6(5) ?
C2B N1B C8AB C8B . . . . -178.1(3) ?
C2B N1B C8AB C4AB . . . . 1.9(4) ?
C7B C8B C8AB N1B . . . . 179.7(3) ?
C7B C8B C8AB C4AB . . . . -0.3(5) ?
C5B C4AB C8AB N1B . . . . -179.7(3) ?
C4B C4AB C8AB N1B . . . . -1.8(4) ?
C5B C4AB C8AB C8B . . . . 0.3(4) ?
C4B C4AB C8AB C8B . . . . 178.2(3) ?

_cod_database_fobs_code 2243911