#------------------------------------------------------------------------------ #$Date: 2021-10-14 05:24:56 +0300 (Thu, 14 Oct 2021) $ #$Revision: 269934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/39/2243931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243931 _cell_angle_alpha 90.000 _cell_angle_beta 90.310 _cell_angle_gamma 90.000 _cell_length_a 15.7976 _cell_length_b 5.9184 _cell_length_c 19.5340 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7705 _cod_data_source_file wm5618Isup2.hkl _cod_data_source_block I _shelx_title ' p21_a.res in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 173.53 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -7 0 8.59 -5.09 10.82 o 2 -7 0 17.36 24.50 13.93 o 3 -7 0 40.87 36.88 14.23 o 4 -7 0 6.07 -0.78 13.41 o 5 -7 0 9.36 3.18 15.47 o 6 -7 0 57.60 104.66 30.76 o 7 -7 0 17.97 -11.54 20.38 o 8 -7 0 54.34 -0.65 20.12 o 0 -6 0 820.87 780.17 70.83 o 1 -6 0 3.99 0.55 9.88 o 2 -6 0 83.83 64.63 21.25 o 3 -6 0 71.46 61.00 14.13 o 4 -6 0 33.00 42.37 11.54 o 5 -6 0 134.47 94.35 15.95 o 6 -6 0 15.88 24.84 13.56 o 8 -6 0 25.22 56.32 23.02 o 9 -6 0 37.18 47.81 22.03 o 10 -6 0 41.96 34.82 17.46 o 11 -6 0 98.33 70.77 23.31 o 12 -6 0 53.29 77.27 34.38 o 1 -5 0 644.41 591.33 35.89 o 2 -5 0 421.66 498.82 29.88 o 3 -5 0 65.08 80.07 12.30 o 4 -5 0 337.81 372.13 33.41 o 5 -5 0 208.70 255.67 20.28 o 6 -5 0 98.49 44.86 15.05 o 7 -5 0 120.29 106.19 11.58 o 8 -5 0 125.98 154.55 15.47 o 9 -5 0 23.98 23.71 18.93 o 10 -5 0 17.29 29.96 20.22 o 11 -5 0 111.37 133.66 29.70 o 12 -5 0 3.82 16.33 14.42 o 13 -5 0 54.60 60.85 18.66 o 14 -5 0 18.66 23.60 15.66 o 15 -5 0 3.31 -13.12 13.12 o 0 -4 0 116.88 183.13 22.55 o 1 -4 0 92.24 67.37 10.07 o 2 -4 0 236.72 254.07 20.19 o 3 -4 0 21.24 25.56 9.27 o 4 -4 0 104.22 119.09 14.49 o 5 -4 0 267.74 242.72 15.59 o 6 -4 0 205.04 204.32 16.76 o 7 -4 0 372.47 362.26 21.78 o 8 -4 0 669.97 685.82 30.68 o 9 -4 0 18.49 15.58 13.98 o 10 -4 0 412.11 449.83 33.98 o 11 -4 0 26.09 46.91 16.65 o 12 -4 0 24.42 41.83 20.46 o 13 -4 0 30.81 90.44 21.69 o 14 -4 0 5.25 2.94 12.49 o 15 -4 0 6.63 -0.70 11.87 o 16 -4 0 32.58 20.31 18.17 o 17 -4 0 5.16 40.48 25.77 o 1 -3 0 1525.61 1516.97 70.71 o 2 -3 0 1.60 6.72 5.65 o 3 -3 0 1334.61 1538.88 84.23 o 4 -3 0 276.21 285.07 24.70 o 5 -3 0 1437.93 1568.92 70.23 o 6 -3 0 441.76 482.66 27.39 o 7 -3 0 641.24 654.84 32.60 o 8 -3 0 35.65 35.05 6.03 o 9 -3 0 731.19 757.16 42.62 o 10 -3 0 45.37 66.22 10.07 o 11 -3 0 240.62 183.72 28.30 o 12 -3 0 102.63 160.80 24.82 o 13 -3 0 25.11 42.73 17.45 o 14 -3 0 13.04 15.87 15.52 o 15 -3 0 60.43 29.94 17.71 o 16 -3 0 37.22 41.95 15.23 o 17 -3 0 80.20 72.87 23.15 o 18 -3 0 16.00 -11.68 11.68 o 0 -2 0 1176.69 1230.29 56.49 o 1 -2 0 197.85 176.28 12.59 o 2 -2 0 3943.12 4030.50 124.54 o 3 -2 0 275.17 269.48 11.19 o 4 -2 0 124.81 147.69 7.46 o 5 -2 0 327.75 306.25 11.39 o 6 -2 0 3712.36 3859.95 124.27 o 7 -2 0 26.03 33.30 5.32 o 8 -2 0 62.49 52.90 3.97 o 9 -2 0 1.83 2.56 2.41 o 10 -2 0 272.49 282.16 19.83 o 11 -2 0 120.01 109.61 11.55 o 12 -2 0 110.90 103.79 12.11 o 13 -2 0 9.77 18.49 9.71 o 14 -2 0 403.33 310.15 35.35 o 15 -2 0 124.72 92.22 19.16 o 16 -2 0 185.34 161.18 21.44 o 17 -2 0 12.55 13.06 7.91 o 18 -2 0 89.93 63.98 12.41 o 1 -1 0 30113.97 29359.88 822.56 o 2 -1 0 150.06 148.36 9.00 o 3 -1 0 1042.47 951.43 22.40 o 4 -1 0 52.95 42.33 2.90 o 5 -1 0 47.57 56.26 2.73 o 6 -1 0 47.43 38.88 2.53 o 7 -1 0 1920.53 1800.61 48.45 o 8 -1 0 35.74 43.24 3.76 o 9 -1 0 1242.39 1335.48 54.15 o 10 -1 0 55.54 53.13 5.03 o 11 -1 0 496.14 519.42 30.36 o 12 -1 0 8.06 1.08 5.46 o 13 -1 0 1087.69 1083.02 49.33 o 14 -1 0 108.93 97.31 14.53 o 15 -1 0 22.43 42.75 7.69 o 16 -1 0 54.55 48.35 9.03 o 17 -1 0 7.27 23.67 11.71 o 18 -1 0 69.47 53.79 8.61 o 19 -1 0 85.16 96.02 14.30 o 20 -1 0 33.93 36.73 13.80 o 2 0 0 4390.75 4084.11 138.44 o 3 0 0 2.10 3.28 0.92 o 4 0 0 984.27 925.85 22.85 o 5 0 0 9.50 14.39 1.30 o 6 0 0 232.45 247.27 6.61 o 7 0 0 48.75 49.40 2.91 o 8 0 0 3104.53 3090.79 124.82 o 9 0 0 78.88 78.16 4.69 o 10 0 0 2799.53 2864.54 138.75 o 11 0 0 2.97 4.40 5.16 o 12 0 0 43.10 57.24 5.63 o 13 0 0 1.66 -2.70 3.44 o 14 0 0 374.76 333.86 36.75 o 15 0 0 29.37 48.56 6.96 o 16 0 0 0.31 6.20 5.84 o 17 0 0 3.36 6.71 5.77 o 18 0 0 323.67 285.92 37.88 o 19 0 0 0.02 26.15 11.60 o 1 1 0 30110.84 28766.20 821.51 o 2 1 0 150.18 142.06 5.91 o 3 1 0 1041.15 985.15 27.08 o 4 1 0 52.98 55.38 4.45 o 5 1 0 47.52 51.90 2.89 o 6 1 0 47.46 48.83 2.61 o 7 1 0 1921.93 1925.88 56.03 o 8 1 0 35.78 38.04 4.11 o 9 1 0 1241.43 1272.87 49.41 o 10 1 0 55.64 55.83 5.22 o 11 1 0 496.16 515.41 29.27 o 12 1 0 8.05 5.93 3.08 o 13 1 0 1086.55 1072.94 62.98 o 15 1 0 22.55 34.54 8.22 o 16 1 0 54.59 52.57 9.04 o 0 2 0 1178.60 1145.33 54.88 o 1 2 0 197.62 168.54 7.53 o 2 2 0 3943.46 4020.06 119.56 o 3 2 0 275.04 301.30 12.81 o 4 2 0 124.35 123.03 7.17 o 5 2 0 327.57 339.89 13.60 o 6 2 0 3712.67 3949.90 119.98 o 7 2 0 26.09 43.92 5.00 o 8 2 0 62.52 75.02 7.08 o 9 2 0 1.83 1.12 2.46 o 10 2 0 272.35 265.96 15.61 o 11 2 0 120.23 95.00 7.75 o 12 2 0 110.88 106.53 7.46 o 13 2 0 9.67 18.47 4.57 o 14 2 0 402.84 348.09 23.30 o 15 2 0 124.65 132.60 14.57 o 16 2 0 185.25 139.64 14.14 o 17 2 0 12.55 10.86 9.42 o 1 3 0 1527.01 1506.82 73.51 o 2 3 0 1.61 5.46 5.88 o 3 3 0 1334.93 1507.39 62.36 o 4 3 0 275.83 295.32 15.04 o 5 3 0 1439.11 1526.84 53.48 o 6 3 0 441.16 442.15 17.56 o 7 3 0 642.72 696.55 26.53 o 8 3 0 35.52 47.53 7.53 o 9 3 0 731.27 728.00 33.87 o 10 3 0 45.34 42.84 6.54 o 11 3 0 240.41 286.73 23.41 o 12 3 0 102.66 83.02 14.22 o 13 3 0 25.08 25.22 4.72 o 14 3 0 13.08 7.79 10.28 o 15 3 0 60.06 53.09 9.58 o 16 3 0 37.15 27.59 7.73 o 17 3 0 80.71 92.18 16.26 o 18 3 0 15.99 56.65 15.22 o 0 4 0 116.54 106.33 16.78 o 1 4 0 92.24 108.11 13.90 o 2 4 0 236.40 229.45 19.74 o 3 4 0 21.22 23.67 9.34 o 4 4 0 104.20 147.32 13.95 o 5 4 0 267.96 293.44 25.76 o 6 4 0 205.69 207.99 22.38 o 7 4 0 372.41 386.66 25.67 o 8 4 0 670.87 668.23 29.77 o 9 4 0 18.42 19.96 7.02 o 10 4 0 411.70 436.61 27.48 o 11 4 0 26.04 51.61 8.17 o 12 4 0 24.40 37.88 8.70 o 13 4 0 30.89 11.80 6.47 o 14 4 0 5.28 -4.25 5.85 o 15 4 0 6.62 25.02 8.00 o 16 4 0 32.46 33.54 7.93 o 17 4 0 5.15 6.31 12.54 o 1 5 0 645.23 461.08 47.22 o 2 5 0 422.28 331.34 43.19 o 3 5 0 65.23 84.60 16.46 o 4 5 0 337.42 342.37 27.46 o 5 5 0 208.83 228.97 48.70 o 6 5 0 99.00 126.08 12.50 o 7 5 0 120.48 121.07 13.56 o 8 5 0 125.95 109.78 21.99 o 9 5 0 23.91 14.19 7.79 o 10 5 0 17.28 14.65 10.90 o 11 5 0 111.31 149.33 17.74 o 12 5 0 3.85 4.94 11.82 o 13 5 0 54.79 80.27 12.79 o 14 5 0 18.80 9.68 11.56 o 15 5 0 3.24 18.38 8.44 o 0 6 0 820.70 892.54 73.19 o 1 6 0 3.96 -13.81 13.81 o 2 6 0 83.82 73.05 23.30 o 4 6 0 32.96 41.74 23.70 o 5 6 0 134.11 146.83 21.24 o 6 6 0 15.82 21.09 11.80 o 7 6 0 96.36 111.29 15.01 o 8 6 0 25.26 34.12 11.22 o 9 6 0 37.01 53.38 16.75 o 10 6 0 41.90 38.81 10.96 o 11 6 0 98.47 103.49 14.30 o 12 6 0 53.29 41.61 13.09 o 1 7 0 8.67 9.62 19.41 o 2 7 0 17.32 42.42 17.64 o 3 7 0 40.99 50.94 15.77 o 4 7 0 6.08 20.14 20.91 o 5 7 0 9.39 20.64 24.62 o 6 7 0 57.66 68.92 14.28 o 7 7 0 17.89 44.15 17.06 o 8 7 0 54.42 66.49 21.09 o -8 -7 1 5.30 12.96 19.42 o -7 -7 1 32.20 27.53 20.99 o -6 -7 1 20.20 19.03 26.67 o -5 -7 1 39.61 29.47 13.14 o -4 -7 1 23.78 17.57 13.08 o -3 -7 1 3.58 -1.85 11.78 o -2 -7 1 39.78 35.71 13.43 o -1 -7 1 10.96 44.77 15.83 o 0 -7 1 46.36 67.55 17.23 o 1 -7 1 19.84 26.55 16.26 o 2 -7 1 44.56 28.80 14.03 o 3 -7 1 2.74 -2.48 12.70 o 4 -7 1 50.33 80.13 17.14 o 5 -7 1 58.67 50.73 13.79 o 6 -7 1 32.07 11.54 25.37 o 7 -7 1 19.16 -17.81 17.81 o 8 -7 1 4.96 16.70 19.26 o -12 -6 1 6.66 33.28 20.69 o -11 -6 1 91.32 141.21 29.82 o -10 -6 1 51.12 43.67 20.64 o -9 -6 1 49.97 42.76 21.53 o -8 -6 1 7.78 72.89 30.41 o -7 -6 1 121.64 138.58 24.22 o -6 -6 1 44.76 21.80 9.74 o -5 -6 1 123.51 113.15 15.24 o -4 -6 1 41.84 44.22 19.83 o -3 -6 1 113.65 109.62 17.68 o -2 -6 1 93.70 89.28 14.58 o -1 -6 1 202.65 232.16 25.48 o 0 -6 1 36.94 23.46 19.96 o 1 -6 1 267.05 240.84 49.82 o 2 -6 1 46.66 47.74 13.02 o 3 -6 1 204.94 225.79 21.45 o 4 -6 1 39.96 48.46 19.63 o 5 -6 1 119.63 87.22 21.37 o 6 -6 1 58.97 55.30 20.84 o 7 -6 1 117.30 81.71 29.97 o 8 -6 1 12.17 5.50 17.61 o 9 -6 1 22.77 29.24 19.91 o 10 -6 1 27.42 39.78 19.94 o 11 -6 1 57.67 119.78 34.56 o 12 -6 1 7.78 12.14 16.64 o -15 -5 1 61.24 108.75 26.99 o -14 -5 1 31.81 44.62 20.07 o -13 -5 1 27.31 38.18 18.92 o -12 -5 1 52.49 80.23 21.62 o -11 -5 1 83.02 131.48 33.25 o -10 -5 1 76.17 110.16 24.50 o -9 -5 1 151.26 116.04 22.45 o -8 -5 1 68.74 71.37 12.66 o -7 -5 1 141.72 150.02 17.90 o -6 -5 1 187.80 231.02 19.81 o -5 -5 1 288.34 329.16 21.40 o -4 -5 1 996.05 990.55 51.16 o -3 -5 1 346.26 379.99 30.86 o -2 -5 1 93.97 42.04 17.72 o -1 -5 1 56.90 37.95 14.34 o 0 -5 1 234.96 220.49 24.68 o 1 -5 1 130.06 121.17 14.35 o 2 -5 1 69.07 54.58 12.43 o 3 -5 1 814.94 781.29 39.12 o 4 -5 1 535.16 525.47 42.91 o 5 -5 1 403.08 365.55 23.43 o 6 -5 1 307.55 332.02 24.01 o 7 -5 1 142.94 132.79 16.10 o 8 -5 1 87.41 108.65 17.31 o 9 -5 1 93.96 92.75 30.31 o 10 -5 1 60.63 70.32 19.71 o 11 -5 1 52.59 70.99 25.47 o 12 -5 1 41.55 33.73 18.41 o 13 -5 1 34.84 25.71 21.82 o 14 -5 1 58.49 39.05 18.26 o 15 -5 1 27.83 23.35 17.51 o -17 -4 1 45.91 50.45 18.90 o -16 -4 1 26.21 32.87 18.77 o -15 -4 1 23.06 3.14 13.81 o -14 -4 1 38.64 52.44 18.73 o -13 -4 1 128.49 102.61 21.55 o -12 -4 1 34.58 30.78 17.51 o -11 -4 1 90.29 111.43 19.99 o -10 -4 1 495.31 469.02 24.71 o -9 -4 1 9.89 4.31 3.64 o -8 -4 1 1201.16 1224.06 54.19 o -7 -4 1 322.62 330.20 28.74 o -6 -4 1 416.23 451.08 28.17 o -5 -4 1 185.12 191.48 14.34 o -4 -4 1 556.62 535.81 31.69 o -3 -4 1 588.53 580.29 33.27 o -2 -4 1 286.12 315.14 30.27 o -1 -4 1 36.27 36.30 10.95 o 0 -4 1 71.96 68.54 15.22 o 1 -4 1 62.65 72.68 14.86 o 2 -4 1 317.41 348.38 23.27 o 3 -4 1 250.73 311.66 44.42 o 4 -4 1 931.49 914.29 50.63 o 5 -4 1 165.56 133.82 23.08 o 6 -4 1 246.05 245.29 24.08 o 7 -4 1 715.82 653.61 29.90 o 8 -4 1 484.66 500.76 35.57 o 9 -4 1 9.26 9.92 5.87 o 10 -4 1 202.70 207.83 30.29 o 11 -4 1 41.19 39.18 14.13 o 12 -4 1 67.99 50.38 16.07 o 13 -4 1 76.86 101.98 24.47 o 14 -4 1 71.04 83.82 24.45 o 15 -4 1 36.91 131.29 29.55 o 16 -4 1 43.50 20.99 16.04 o 17 -4 1 53.27 71.97 25.46 o -18 -3 1 40.21 32.59 17.08 o -17 -3 1 48.33 50.78 17.56 o -16 -3 1 57.28 124.44 22.23 o -15 -3 1 141.34 185.64 22.91 o -14 -3 1 77.00 109.13 18.83 o -13 -3 1 69.68 92.13 21.92 o -12 -3 1 128.57 131.81 19.57 o -11 -3 1 66.77 58.81 6.01 o -10 -3 1 295.09 292.67 15.80 o -9 -3 1 438.95 432.61 21.14 o -8 -3 1 256.40 314.08 31.65 o -7 -3 1 186.44 189.87 9.62 o -6 -3 1 561.14 471.35 40.24 o -5 -3 1 684.07 704.47 34.74 o -4 -3 1 833.93 905.72 44.59 o -3 -3 1 452.95 465.15 25.22 o -2 -3 1 421.21 424.67 47.48 o -1 -3 1 232.22 316.65 22.02 o 0 -3 1 177.35 149.99 17.98 o 1 -3 1 184.62 211.48 14.10 o 2 -3 1 726.69 755.73 36.10 o 3 -3 1 278.15 273.09 37.62 o 4 -3 1 1190.52 1201.99 51.91 o 5 -3 1 527.83 531.79 27.87 o 6 -3 1 1158.41 1141.44 41.69 o 7 -3 1 107.48 125.09 8.50 o 8 -3 1 456.91 431.97 25.82 o 9 -3 1 327.83 333.01 24.74 o 10 -3 1 262.03 290.56 23.97 o 11 -3 1 75.26 61.44 9.34 o 12 -3 1 59.09 21.52 17.55 o 13 -3 1 53.30 33.90 13.65 o 14 -3 1 65.68 112.75 22.89 o 15 -3 1 78.26 48.85 21.09 o 16 -3 1 29.77 32.90 15.23 o 17 -3 1 44.70 36.15 14.25 o 18 -3 1 30.19 72.36 22.06 o -19 -2 1 101.70 77.01 16.09 o -18 -2 1 100.50 109.09 11.93 o -17 -2 1 132.92 101.95 12.08 o -16 -2 1 16.08 30.59 11.56 o -15 -2 1 156.08 163.78 21.18 o -14 -2 1 76.27 83.41 14.87 o -13 -2 1 181.99 87.33 14.04 o -12 -2 1 142.31 147.43 13.13 o -11 -2 1 43.33 26.24 3.77 o -10 -2 1 104.74 70.25 7.45 o -9 -2 1 19.38 21.34 3.96 o -8 -2 1 376.59 410.70 19.45 o -7 -2 1 242.31 245.21 10.53 o -6 -2 1 1402.10 1599.18 50.34 o -5 -2 1 1776.42 1819.91 73.11 o -4 -2 1 756.20 869.13 29.22 o -3 -2 1 1317.51 1394.56 43.77 o -2 -2 1 847.76 835.49 27.27 o -1 -2 1 1119.65 1170.59 36.96 o 0 -2 1 46.44 62.00 5.30 o 1 -2 1 1403.80 1496.30 46.92 o 2 -2 1 550.98 558.49 21.67 o 3 -2 1 1338.78 1345.00 41.80 o 4 -2 1 940.94 978.35 33.63 o 5 -2 1 2408.98 2357.78 67.95 o 6 -2 1 1575.74 1702.37 56.47 o 7 -2 1 195.41 209.90 11.30 o 8 -2 1 512.76 557.22 29.23 o 9 -2 1 16.21 4.42 5.21 o 10 -2 1 179.20 179.43 12.68 o 11 -2 1 52.31 51.76 5.92 o 12 -2 1 61.15 66.88 12.27 o 13 -2 1 320.83 355.33 31.73 o 14 -2 1 35.11 26.36 11.23 o 15 -2 1 87.92 62.23 18.70 o 16 -2 1 11.89 23.60 14.25 o 17 -2 1 151.56 168.21 14.29 o 18 -2 1 85.63 83.48 11.91 o 19 -2 1 138.34 110.15 21.93 o -20 -1 1 46.51 39.17 11.26 o -19 -1 1 6.82 15.34 10.10 o -18 -1 1 71.80 64.37 18.54 o -17 -1 1 156.51 118.39 14.33 o -16 -1 1 20.13 33.79 11.06 o -15 -1 1 87.26 115.67 10.36 o -14 -1 1 333.76 305.88 44.54 o -13 -1 1 187.06 164.42 16.65 o -12 -1 1 103.50 102.60 13.87 o -11 -1 1 109.72 113.95 7.64 o -10 -1 1 233.08 237.13 12.66 o -9 -1 1 482.77 446.25 18.38 o -8 -1 1 341.81 328.38 15.55 o -7 -1 1 494.12 496.09 15.66 o -6 -1 1 3050.98 3038.95 70.85 o -5 -1 1 4116.56 3957.57 86.84 o -4 -1 1 2558.68 2538.40 53.78 o -3 -1 1 4382.05 4334.86 101.40 o -2 -1 1 1159.48 1174.35 36.09 o -1 -1 1 2019.68 1945.33 55.04 o 0 -1 1 133.36 137.14 6.00 o 1 -1 1 1387.20 1405.03 41.25 o 2 -1 1 1763.35 1674.79 49.54 o 3 -1 1 3644.92 3622.76 103.13 o 4 -1 1 2432.35 2373.78 71.79 o 5 -1 1 3301.17 3205.44 92.58 o 6 -1 1 2654.61 2567.82 74.19 o 7 -1 1 416.44 432.63 13.35 o 8 -1 1 370.16 442.90 17.98 o 9 -1 1 470.74 528.11 30.28 o 10 -1 1 147.87 149.18 12.61 o 11 -1 1 66.59 71.74 8.84 o 12 -1 1 183.62 190.96 11.70 o 13 -1 1 244.11 274.09 16.35 o 14 -1 1 308.48 326.07 27.33 o 15 -1 1 47.34 33.43 8.02 o 16 -1 1 21.54 71.34 9.21 o 17 -1 1 150.84 144.51 14.78 o 18 -1 1 130.38 159.48 15.10 o 19 -1 1 4.20 0.29 8.83 o 20 -1 1 71.21 94.16 15.39 o -20 0 1 18.35 3.81 11.19 o -19 0 1 109.15 138.14 21.85 o -18 0 1 103.25 102.55 19.81 o -17 0 1 49.92 49.50 16.10 o -16 0 1 112.85 146.55 12.03 o -15 0 1 29.34 45.35 6.90 o -14 0 1 23.73 31.52 12.32 o -13 0 1 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