#------------------------------------------------------------------------------ #$Date: 2021-10-14 05:30:14 +0300 (Thu, 14 Oct 2021) $ #$Revision: 269940 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/24/39/2243937.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243937 loop_ _publ_author_name 'Domasevitch, Kostiantyn V.' 'Ponomarova, Vira V.' _publ_section_title ; Isostructural rubidium and caesium 4-(3,5-dinitropyrazol-4-yl)-3,5-dinitropyrazolates: crystal engineering with polynitro energetic species ; _journal_coeditor_code HB7988 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first ; ; _journal_paper_doi 10.1107/S2056989021010227 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac '[Rb (C6 H N8 O8)]' _chemical_formula_moiety 'C6 H N8 O8 Rb' _chemical_formula_sum 'C6 H N8 O8 Rb' _chemical_formula_weight 398.62 _chemical_name_systematic ; Poly[[\m~4~-4-(3,5-dinitropyrazol-4-yl)-3,5-dinitropyrazol-1-ido]rubidium] ; _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 90 _cell_angle_beta 115.264(7) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 19.4400(15) _cell_length_b 8.6070(4) _cell_length_c 16.0977(10) _cell_measurement_reflns_used 8000 _cell_measurement_temperature 213(2) _cell_measurement_theta_max 27.898 _cell_measurement_theta_min 2.317 _cell_volume 2435.8(3) _computing_cell_refinement ; IPDS Software (Stoe & Cie, 2000) ; _computing_data_collection ; IPDS Software (Stoe & Cie, 2000) ; _computing_data_reduction ; IPDS Software (Stoe & Cie, 2000) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 1999) ; _computing_publication_material ; WinGX (Farrugia, 2012) ; _computing_structure_refinement ; SHELXL2018/1 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 213(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Stoe IPDS' _diffrn_measurement_method '\f oscillation scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0330 _diffrn_reflns_av_unetI/netI 0.0373 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 9925 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.898 _diffrn_reflns_theta_min 2.317 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 4.134 _exptl_absorpt_correction_T_max 0.7892 _exptl_absorpt_correction_T_min 0.6720 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; [X-RED (Stoe & Cie, 2001) and X-SHAPE (Stoe & Cie, 1999)] ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 2.174 _exptl_crystal_description prism _exptl_crystal_F_000 1552 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.160 _exptl_crystal_size_min 0.140 _refine_diff_density_max 0.373 _refine_diff_density_min -0.392 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.885 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 210 _refine_ls_number_reflns 2890 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.885 _refine_ls_R_factor_all 0.0379 _refine_ls_R_factor_gt 0.0256 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0326P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0535 _refine_ls_wR_factor_ref 0.0552 _reflns_number_gt 2186 _reflns_number_total 2890 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb7988sup1.cif _cod_data_source_block 1 _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 2243937 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.492 _shelx_estimated_absorpt_t_max 0.595 _shelx_hkl_file ; -25 -1 6 29.98 6.50 25 1 -6 31.29 4.97 -25 1 6 23.41 4.36 25 -1 -6 27.30 4.38 25 1 -7 16.88 4.36 -25 1 7 16.91 4.33 25 -1 -7 18.22 6.14 -25 -1 7 14.69 4.40 -25 -1 8 3.31 4.30 25 1 -8 3.49 6.09 25 -1 -8 4.17 4.32 -25 1 8 4.36 6.03 -25 1 9 2.68 4.31 -25 -1 9 6.82 4.32 25 -1 -9 0.82 6.14 25 1 -9 1.21 4.35 -25 1 10 49.97 4.44 -25 -1 10 50.02 4.47 25 -1 -10 49.39 6.23 25 1 -10 49.49 4.47 -25 1 11 11.18 6.04 25 -1 -11 11.69 6.16 -25 -1 11 6.14 6.08 25 1 -11 13.28 4.37 25 -1 -12 0.71 4.93 -25 1 12 3.33 4.79 25 1 -12 4.51 4.87 -25 -1 12 -4.27 4.88 24 0 -2 0.96 4.89 24 0 -3 9.90 6.08 -24 0 3 3.75 4.29 -24 0 4 141.57 4.77 24 0 -4 144.52 4.88 24 0 -5 4.45 4.34 -24 0 5 0.68 4.34 24 0 -6 1.21 4.42 -24 0 6 -1.37 6.18 -24 0 7 2.48 4.34 24 0 -7 -3.47 5.85 -24 0 8 10.66 4.35 24 0 -8 11.26 4.40 -24 0 9 -2.78 5.82 24 0 -9 0.59 5.85 24 0 -10 -1.29 5.86 -24 0 10 -5.17 4.43 -24 0 11 0.16 4.35 24 0 -11 -0.99 4.45 -24 0 12 60.08 6.28 24 0 -12 58.36 4.61 -24 0 13 -1.61 6.13 24 0 -13 1.80 4.38 -24 0 14 4.74 6.08 24 0 -14 12.12 6.21 24 0 -15 2.25 5.02 -24 0 15 1.32 6.80 -24 2 3 20.63 4.93 -24 -2 4 20.80 6.14 24 -2 -4 22.37 6.21 24 2 -4 20.75 4.38 -24 2 4 21.79 4.39 -24 -2 5 46.92 4.51 24 -2 -5 42.48 6.33 -24 2 5 51.56 4.46 24 2 -5 44.04 4.47 24 2 -6 7.58 4.34 24 -2 -6 5.40 6.24 -24 2 6 4.02 4.36 -24 -2 6 -1.66 6.23 -24 -2 7 22.93 4.43 24 2 -7 23.82 4.41 24 -2 -7 23.19 4.44 -24 2 7 28.56 6.19 -24 2 8 38.92 4.52 24 -2 -8 39.17 6.35 -24 -2 8 40.89 4.50 24 2 -8 37.12 4.44 -24 2 9 2.91 4.35 24 -2 -9 1.80 4.43 -24 -2 9 4.83 4.38 24 2 -9 3.08 4.42 -24 -2 10 2.84 6.19 24 -2 -10 4.07 4.44 24 2 -10 6.52 4.33 -24 2 10 6.41 4.35 24 -2 -11 32.81 4.53 -24 -2 11 34.34 4.49 -24 2 11 31.45 4.42 24 2 -11 34.18 4.52 24 -2 -12 8.63 6.33 -24 2 12 17.91 6.16 -24 -2 12 18.06 4.35 24 2 -12 21.28 6.19 24 2 -13 25.66 4.45 -24 -2 13 18.52 4.38 -24 2 13 20.39 4.34 24 -2 -13 20.64 4.45 24 -2 -14 5.49 4.95 -24 2 14 0.81 4.86 -24 -2 14 1.43 4.93 23 -1 -1 21.89 4.44 23 1 -1 22.24 6.19 -23 -1 1 15.25 6.19 -23 1 1 18.91 4.44 -23 -1 2 45.80 4.49 23 1 -2 49.62 4.62 -23 1 2 35.70 4.48 23 -1 -2 57.27 6.32 23 1 -3 9.54 4.45 -23 -1 3 10.26 4.46 -23 1 3 15.21 6.19 23 -1 -3 10.02 4.43 -23 -1 4 0.56 5.45 -23 1 4 -2.18 5.47 23 1 -4 1.46 3.83 23 -1 -4 -1.14 3.84 23 1 -5 -3.72 3.97 -23 1 5 -0.88 5.48 23 -1 -5 0.46 3.88 -23 -1 5 -3.25 3.91 23 1 -6 109.46 4.30 -23 1 6 106.69 4.22 -23 -1 6 107.49 4.22 23 -1 -6 102.73 4.26 23 1 -7 2.22 3.91 23 -1 -7 2.30 5.49 -23 1 7 -2.42 5.50 -23 -1 7 1.22 3.93 23 -1 -8 2.54 3.92 -23 -1 8 -2.73 3.90 23 1 -8 1.91 3.89 -23 1 8 -1.07 3.90 23 1 -9 8.27 5.53 -23 -1 9 5.14 3.87 -23 1 9 8.41 3.83 23 -1 -9 2.64 3.93 -23 -1 10 71.90 4.15 23 1 -10 79.17 5.77 -23 1 10 70.57 4.10 23 -1 -10 68.57 4.23 -23 1 11 3.27 5.47 23 -1 -11 3.33 5.51 23 1 -11 2.80 5.54 -23 -1 11 3.36 5.48 -23 -1 12 1.14 3.85 23 -1 -12 1.46 3.93 -23 1 12 1.07 3.85 23 1 -12 1.76 3.90 23 1 -13 24.44 4.53 23 -1 -13 24.53 4.58 -23 -1 13 20.23 5.88 -23 1 13 24.16 3.92 23 -1 -14 19.08 4.54 -23 -1 14 21.09 6.18 23 1 -14 19.41 4.51 -23 1 14 18.35 4.39 23 1 -15 8.61 4.50 23 -1 -15 9.28 4.48 -23 1 15 9.22 4.33 -23 -1 15 7.39 4.37 -23 1 16 0.06 6.47 23 1 -16 1.89 4.98 23 -1 -16 -3.94 6.72 -23 -1 16 -0.37 4.85 23 3 -2 6.62 6.49 -23 -3 2 3.15 6.49 -23 3 2 -0.06 4.38 23 -3 -2 3.53 4.35 23 -3 -3 38.31 4.52 -23 -3 3 35.05 4.45 23 3 -3 39.41 4.46 -23 3 3 37.80 4.48 -23 3 4 11.01 4.41 -23 -3 4 10.20 4.39 23 3 -4 5.33 6.26 23 -3 -4 9.07 4.47 23 -3 -5 37.00 4.55 23 3 -5 33.13 4.49 -23 -3 5 33.05 6.22 -23 3 5 30.55 4.44 23 3 -6 0.73 4.42 -23 -3 6 -1.90 4.36 23 -3 -6 2.96 4.41 -23 3 6 0.88 4.37 23 3 -7 -1.87 5.84 23 -3 -7 0.19 5.94 -23 3 7 -5.28 5.84 -23 -3 7 0.52 3.84 23 -3 -8 11.75 3.96 -23 3 8 16.48 3.86 -23 -3 8 13.14 3.92 23 3 -8 15.11 3.85 -23 3 9 1.20 3.86 -23 -3 9 2.89 3.87 23 3 -9 0.92 5.82 23 -3 -9 -1.51 3.90 -23 -3 10 7.02 4.36 -23 3 10 3.07 4.41 23 3 -10 4.63 6.16 23 -3 -10 -0.56 4.47 23 -3 -11 43.82 6.39 -23 -3 11 37.99 6.32 23 3 -11 41.17 6.34 -23 3 11 34.65 4.54 -23 3 12 22.42 6.19 23 -3 -12 19.39 4.53 -23 -3 12 20.71 6.31 23 3 -12 18.62 4.43 23 -3 -13 19.14 4.48 -23 -3 13 22.10 6.22 23 3 -13 16.06 4.52 -23 3 13 16.60 4.42 -23 -3 14 7.72 4.35 23 3 -14 5.90 4.42 -23 3 14 7.14 4.34 23 -3 -14 5.00 4.41 22 0 -1 -1.78 5.55 -22 0 1 -0.78 3.89 22 0 -2 3.82 3.93 -22 0 2 -0.24 3.91 -22 0 3 1.54 3.90 22 0 -3 4.65 3.93 -22 0 4 46.28 4.09 22 0 -4 45.78 5.72 -22 0 5 2.86 3.35 22 0 -5 -2.51 5.23 -22 0 6 -1.01 4.81 22 0 -6 2.97 3.38 -22 0 7 1.47 3.39 22 0 -7 2.05 3.39 -22 0 8 82.57 3.75 22 0 -8 94.40 3.76 -22 0 9 1.18 3.38 22 0 -9 -3.18 3.40 -22 0 10 2.90 3.41 22 0 -10 3.06 3.42 -22 0 11 -1.38 3.97 22 0 -11 1.36 3.97 22 0 -12 118.19 4.42 -22 0 12 123.80 5.92 22 0 -13 -0.93 3.98 -22 0 13 3.38 5.48 -22 0 14 1.28 3.84 22 0 -14 1.16 3.97 -22 0 15 -0.64 3.84 22 0 -15 2.41 6.00 -22 0 16 35.04 4.52 22 0 -16 42.15 6.42 -22 0 17 1.83 6.09 22 0 -17 8.15 6.23 -22 2 1 29.55 6.42 -22 -2 1 29.77 6.27 22 -2 -1 27.29 6.39 22 2 -1 25.06 4.59 -22 2 2 28.95 4.01 -22 -2 2 29.15 5.55 22 -2 -2 35.21 4.04 22 2 -2 36.11 5.60 -22 -2 3 38.54 5.57 22 2 -3 27.35 4.06 -22 2 3 31.18 4.02 22 -2 -3 31.47 4.06 -22 2 4 79.10 4.16 -22 -2 4 76.94 4.12 22 -2 -4 69.56 4.22 22 2 -4 75.33 5.69 22 -2 -5 60.25 4.17 -22 2 5 59.02 4.09 22 2 -5 64.81 5.68 -22 -2 5 66.19 4.08 22 2 -6 8.84 5.54 -22 -2 6 9.44 3.97 22 -2 -6 8.18 4.00 -22 2 6 5.15 3.98 -22 2 7 55.68 4.13 22 -2 -7 57.27 5.73 -22 -2 7 54.49 4.13 22 2 -7 53.86 4.14 22 2 -8 4.44 5.60 -22 -2 8 10.77 3.99 -22 2 8 5.54 5.61 22 -2 -8 9.66 5.63 -22 2 9 42.50 4.04 22 -2 -9 43.94 5.75 -22 -2 9 42.58 4.14 22 2 -9 47.31 4.04 -22 -2 10 39.83 5.71 22 2 -10 35.50 4.06 -22 2 10 40.05 5.64 22 -2 -10 40.66 5.72 22 2 -11 43.58 5.70 -22 2 11 30.95 4.03 22 -2 -11 34.15 4.11 -22 -2 11 37.19 4.08 22 -2 -12 24.62 5.66 22 2 -12 19.95 3.97 -22 -2 12 15.81 3.99 -22 2 12 14.60 4.01 -22 -2 13 16.01 3.95 22 -2 -13 21.63 5.68 -22 2 13 14.47 3.92 22 2 -13 19.65 4.04 -22 -2 14 -0.11 5.49 22 -2 -14 -4.07 5.67 22 2 -14 -2.13 4.02 -22 2 14 3.76 3.81 -22 -2 15 1.95 6.20 22 2 -15 0.78 4.47 22 -2 -15 0.77 4.54 -22 2 15 1.74 4.32 -22 2 16 5.10 4.30 22 -2 -16 6.12 4.44 22 2 -16 4.63 4.43 -22 -2 16 2.25 6.21 22 -4 -1 3.63 4.97 -22 4 1 2.10 4.96 -22 -4 1 0.80 4.88 22 4 -1 -1.83 4.99 -22 4 2 43.16 6.31 22 4 -2 40.84 6.30 -22 -4 2 39.27 6.20 22 -4 -2 38.64 4.52 22 -4 -3 11.63 4.48 -22 4 3 12.50 4.42 -22 -4 3 10.13 6.18 22 4 -3 10.86 4.42 22 -4 -4 13.88 4.54 -22 4 4 9.17 4.47 22 4 -4 5.14 6.24 -22 -4 4 7.23 4.44 -22 -4 5 24.24 4.41 -22 4 5 14.98 4.47 22 -4 -5 19.07 4.57 22 4 -5 15.58 5.89 22 -4 -6 99.76 5.87 -22 4 6 90.18 4.19 -22 -4 6 92.32 5.77 22 4 -6 108.20 5.64 22 -4 -7 35.56 4.03 22 4 -7 29.83 3.96 -22 -4 7 35.63 5.60 -22 4 7 33.13 5.53 -22 4 8 0.19 3.87 -22 -4 8 4.26 3.86 22 4 -8 4.64 3.78 22 -4 -8 0.10 3.95 22 4 -9 1.37 3.84 22 -4 -9 -1.07 3.96 -22 4 9 0.32 3.83 -22 -4 9 0.06 3.90 -22 -4 10 15.04 3.91 22 -4 -10 15.53 3.97 22 4 -10 15.80 5.51 -22 4 10 11.58 3.92 22 -4 -11 2.89 4.49 22 4 -11 3.03 4.39 -22 -4 11 2.16 6.27 -22 4 11 0.30 4.39 -22 -4 12 9.65 4.41 22 -4 -12 11.54 4.52 22 4 -12 11.24 4.39 -22 4 12 7.78 4.37 22 4 -13 20.57 6.28 -22 -4 13 13.83 4.43 22 -4 -13 9.66 4.58 -22 4 13 10.57 4.40 -22 4 14 28.00 6.15 -22 -4 14 31.67 6.27 22 -4 -14 21.74 4.58 22 4 -14 33.81 6.23 21 -1 -1 17.87 3.97 21 1 -1 15.76 4.01 -21 1 1 13.97 5.67 -21 -1 1 13.85 3.99 -21 1 2 88.87 3.76 -21 -1 2 83.93 4.29 21 -1 -2 77.96 3.73 21 1 -2 82.77 3.73 -21 1 3 3.06 3.40 21 -1 -3 0.08 3.45 -21 -1 3 1.60 3.41 21 1 -3 3.59 3.38 21 -1 -4 -1.28 3.44 -21 -1 4 0.94 3.41 21 1 -4 1.44 3.37 -21 1 4 5.38 3.42 -21 1 5 11.20 3.45 21 1 -5 10.59 3.42 -21 -1 5 8.93 4.86 21 -1 -5 8.89 3.47 21 -1 -6 250.91 5.59 -21 1 6 243.53 5.50 21 1 -6 242.22 4.28 -21 -1 6 232.96 4.30 21 1 -7 30.13 4.92 -21 -1 7 25.79 3.55 -21 1 7 25.93 3.59 21 -1 -7 28.07 3.56 21 1 -8 6.38 3.47 21 -1 -8 7.06 3.46 -21 1 8 3.11 3.48 -21 -1 8 3.06 3.49 -21 1 9 12.41 3.49 -21 -1 9 11.07 3.49 21 1 -9 13.97 3.50 21 -1 -9 16.92 3.47 -21 1 10 15.57 3.54 21 -1 -10 17.74 3.44 21 1 -10 18.74 3.52 -21 -1 10 16.30 4.93 21 1 -11 18.57 4.97 -21 -1 11 15.05 3.48 -21 1 11 13.59 4.88 21 -1 -11 14.96 3.54 -21 -1 12 -1.35 3.43 21 -1 -12 0.85 4.87 -21 1 12 3.13 3.38 21 1 -12 0.34 4.89 21 -1 -13 2.38 4.04 -21 -1 13 -0.35 3.45 21 1 -13 7.99 5.32 -21 1 13 6.59 3.37 -21 -1 14 62.35 4.15 21 1 -14 62.24 4.28 21 -1 -14 64.29 4.28 -21 1 14 68.51 5.73 -21 1 15 9.04 3.92 -21 -1 15 9.41 5.49 21 -1 -15 7.94 4.03 21 1 -15 9.75 5.64 21 -1 -16 0.00 4.54 21 1 -16 3.80 5.97 -21 1 16 1.56 3.85 -21 -1 16 -0.78 4.39 -21 -1 17 15.65 6.22 -21 1 17 15.03 6.17 21 -1 -17 13.68 6.38 21 1 -17 10.27 4.49 -21 1 18 10.47 4.93 21 1 -18 8.48 5.02 21 -1 -18 11.08 6.64 -21 -1 18 10.51 6.61 -21 -3 1 71.94 4.14 -21 3 1 77.28 4.25 21 -3 -1 84.70 5.82 21 3 -1 88.53 5.76 21 3 -2 -1.09 3.95 -21 3 2 -0.28 3.92 -21 -3 2 3.17 5.50 21 -3 -2 -0.66 3.98 21 3 -3 28.98 5.57 -21 3 3 22.40 5.60 -21 -3 3 19.55 5.57 21 -3 -3 18.67 4.03 -21 3 4 11.87 3.96 -21 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1 1.06 4.45 -13 -9 1 4.41 6.09 13 9 -1 2.26 4.35 -13 9 2 56.90 6.39 13 9 -2 53.51 4.51 -13 9 2 56.08 4.60 -13 -9 2 62.25 6.27 -13 -9 3 -0.32 4.35 13 9 -3 2.04 4.31 -13 9 3 -0.81 4.47 -13 9 3 2.44 6.23 -13 -9 4 0.81 4.43 -13 9 4 5.86 6.16 -13 9 4 2.47 4.52 13 9 -4 0.07 4.36 13 9 -5 20.30 6.13 -13 9 5 23.53 4.43 -13 9 5 16.13 6.43 -13 -9 5 18.54 4.41 13 9 -6 34.86 4.35 -13 -9 6 31.99 4.46 -13 9 6 36.03 6.39 -13 9 6 27.12 4.44 13 9 -7 4.46 4.24 -13 9 7 1.26 4.33 -13 9 7 -3.37 6.43 -13 -9 7 2.23 4.42 -13 -9 8 -0.09 4.38 13 9 -8 -0.18 4.27 -13 9 8 0.86 4.50 -13 9 8 -0.88 4.28 13 9 -9 0.49 6.04 -13 9 9 2.33 4.49 -13 -9 9 7.21 4.36 -13 9 9 1.65 4.26 -13 9 10 30.21 4.34 -13 9 10 31.75 4.65 -13 -9 10 37.81 6.27 13 9 -10 35.07 6.14 -12 0 1 0.26 2.96 12 0 -1 -0.37 2.09 -12 0 2 2.20 2.09 12 0 -2 1.11 2.10 -12 0 3 -1.61 3.00 12 0 -3 0.17 2.07 -12 0 4 114.89 3.53 12 0 -4 111.38 2.88 -12 0 5 -0.94 2.11 12 0 -5 -0.81 2.10 -12 0 6 126.26 3.00 12 0 -6 133.99 3.70 -12 0 7 0.70 2.98 12 0 -7 0.20 2.99 -12 0 8 625.60 5.92 12 0 -8 620.17 5.44 12 0 -9 0.06 2.66 -12 0 9 -0.35 3.71 -12 0 10 204.82 4.77 12 0 -10 215.34 4.87 -12 0 11 -0.40 3.70 12 0 -11 0.34 2.62 -12 0 12 29.64 3.87 12 0 -12 27.08 2.87 12 0 -13 2.18 3.64 -12 0 13 1.20 3.62 12 0 -14 25.63 4.50 -12 0 14 21.54 3.28 -12 0 15 1.91 4.31 12 0 -15 -0.44 4.27 -12 0 16 120.92 5.25 12 0 -16 108.79 5.20 -12 0 17 0.65 5.05 -12 0 20 20.29 5.28 -12 2 1 30.60 2.77 -12 -2 1 27.09 2.74 12 2 -1 28.49 2.73 12 -2 -1 28.64 2.79 -12 -2 2 131.39 3.56 12 2 -2 138.71 3.55 -12 2 2 127.34 2.89 12 -2 -2 129.20 2.91 12 -2 -3 105.04 2.78 -12 2 3 106.18 2.76 12 2 -3 114.13 3.49 -12 -2 3 110.84 2.78 12 -2 -4 84.29 2.69 12 2 -4 84.40 2.64 -12 2 4 82.00 3.36 -12 -2 4 81.18 2.63 12 2 -5 47.56 3.19 12 -2 -5 48.21 2.48 -12 -2 5 46.11 2.42 -12 2 5 45.30 2.42 -12 2 6 45.11 3.17 12 -2 -6 44.85 2.45 12 2 -6 45.76 3.15 -12 -2 6 43.84 3.16 -12 -2 7 16.62 3.75 12 -2 -7 19.32 2.76 12 2 -7 16.18 2.67 -12 2 7 16.93 2.65 12 -2 -8 105.10 4.27 12 2 -8 99.73 3.19 -12 -2 8 100.63 3.21 -12 2 8 103.71 4.12 -12 -2 9 82.25 4.05 12 -2 -9 80.46 4.15 -12 2 9 77.00 3.08 12 2 -9 82.10 4.11 -12 -2 10 1.89 2.54 12 -2 -10 4.72 2.67 -12 2 10 0.64 2.57 12 2 -10 2.67 3.69 12 -2 -11 243.50 4.11 -12 2 11 242.92 4.83 12 2 -11 238.49 4.13 -12 -2 11 245.59 4.13 12 2 -12 42.83 3.93 -12 2 12 42.38 3.85 12 -2 -12 44.49 4.01 -12 -2 12 43.23 3.90 12 -2 -13 97.83 4.60 -12 2 13 98.46 4.50 -12 -2 13 98.47 4.65 12 2 -13 93.59 4.63 12 -2 -14 93.01 3.72 -12 -2 14 106.12 5.01 -12 2 14 101.17 4.86 12 2 -14 102.87 5.02 12 2 -15 8.01 4.29 -12 2 15 6.00 4.25 -12 -2 15 7.06 4.41 -12 2 16 42.15 5.29 -12 -2 16 44.01 5.52 12 2 -16 41.42 5.29 12 2 -17 19.01 6.17 -12 2 17 22.36 5.07 -12 -2 17 22.47 6.48 -12 2 17 19.79 5.09 -12 2 18 3.19 5.76 -12 2 18 5.63 5.71 -12 2 19 5.35 7.01 -12 2 19 5.88 6.81 -12 2 20 0.26 6.52 -12 4 1 105.92 4.13 12 -4 -1 105.84 3.17 -12 -4 1 107.29 3.05 12 4 -1 106.73 3.11 12 4 -2 800.10 6.03 -12 -4 2 762.88 5.27 -12 4 2 764.69 5.41 12 -4 -2 742.75 5.33 12 -4 -3 12.38 3.76 -12 -4 3 13.33 2.64 12 4 -3 15.36 2.62 -12 4 3 12.86 2.64 -12 -4 4 -1.04 2.57 12 -4 -4 0.31 3.66 12 4 -4 0.06 2.51 -12 4 4 0.68 2.56 12 -4 -5 3.38 3.68 -12 -4 5 0.90 3.63 12 4 -5 2.02 3.57 -12 4 5 0.91 2.59 12 -4 -6 206.68 3.62 -12 -4 6 210.18 4.42 -12 4 6 203.88 3.52 12 4 -6 215.84 3.58 -12 -4 7 9.94 3.63 12 -4 -7 8.57 2.71 -12 4 7 7.99 3.65 12 4 -7 9.19 2.56 12 -4 -8 11.59 2.69 -12 -4 8 13.69 2.63 -12 4 8 12.88 3.67 12 4 -8 12.42 2.63 -12 -4 9 33.25 2.75 12 4 -9 35.62 2.75 12 -4 -9 37.90 2.85 -12 4 9 39.21 3.77 -12 -4 10 326.63 4.30 12 4 -10 326.73 4.28 12 -4 -10 342.21 5.10 -12 4 10 327.70 4.20 12 -4 -11 66.56 3.50 -12 -4 11 64.02 3.44 12 4 -11 65.34 4.58 -12 4 11 66.02 3.37 -12 4 12 1.73 4.26 12 4 -12 0.67 3.03 -12 -4 12 0.50 4.29 -12 4 13 29.49 3.15 -12 -4 13 31.12 4.45 12 4 -13 31.89 4.41 12 4 -14 26.05 4.38 -12 -4 14 30.94 4.44 -12 4 14 27.63 3.13 12 4 -15 2.44 4.97 -12 4 15 1.40 3.63 -12 -4 15 0.61 5.17 -12 4 15 -0.01 4.90 12 4 -16 -0.14 3.50 -12 -4 16 1.76 3.57 -12 4 16 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-8 9 11.77 5.67 -12 8 10 -0.86 4.16 -12 8 10 2.32 3.83 12 8 -10 3.34 3.83 -12 -8 10 2.65 5.62 -12 8 11 46.81 5.55 -12 8 11 39.96 4.26 -12 -8 11 41.79 4.15 12 8 -11 41.38 5.60 -12 -8 12 18.05 6.12 -12 8 12 18.20 4.64 -12 8 12 17.50 3.89 12 8 -12 19.85 5.87 12 8 -13 -2.99 4.41 -12 8 13 2.91 4.63 -12 -8 13 -2.47 4.55 -12 8 13 -0.30 4.27 12 8 -14 13.57 6.17 -12 -8 14 10.91 6.84 -12 8 14 13.96 6.45 -12 8 14 10.99 4.59 -12 10 4 49.60 5.06 -12 -10 5 -1.46 4.88 -11 -1 1 63.61 2.52 -11 1 1 63.41 2.55 11 1 -1 66.68 3.35 11 -1 -1 64.13 2.63 -11 -1 2 470.21 4.51 11 -1 -2 490.08 5.16 -11 1 2 481.44 5.10 11 1 -2 502.47 5.18 -11 -1 3 44.13 2.44 11 -1 -3 42.32 2.45 -11 1 3 40.98 3.25 11 1 -3 46.86 3.23 -11 1 4 4.46 3.00 11 -1 -4 4.05 2.18 11 1 -4 3.38 2.14 -11 -1 4 2.44 2.12 -11 1 5 7.86 2.17 11 1 -5 8.50 3.03 11 -1 -5 9.66 2.22 -11 -1 5 7.87 2.18 -11 -1 6 675.61 5.63 -11 1 6 687.48 6.02 11 1 -6 690.00 5.71 11 -1 -6 698.28 5.63 11 -1 -7 149.54 3.89 11 1 -7 150.83 3.22 -11 1 7 148.79 3.19 -11 -1 7 148.52 3.22 -11 1 8 -0.62 2.96 11 1 -8 1.24 2.96 -11 -1 8 1.31 2.96 11 -1 -8 2.12 3.00 -11 -1 9 3.90 2.96 11 -1 -9 2.97 2.16 11 1 -9 3.80 2.11 -11 1 9 2.73 2.99 11 -1 -10 145.19 3.69 -11 1 10 138.21 3.55 -11 -1 10 144.76 3.63 11 1 -10 136.96 3.63 11 -1 -11 25.77 2.89 11 1 -11 25.44 3.91 -11 1 11 25.49 2.77 -11 -1 11 27.49 2.85 11 -1 -12 0.14 3.75 -11 1 12 1.75 2.59 11 1 -12 1.42 2.61 -11 -1 12 0.77 2.63 11 1 -13 13.66 3.78 -11 1 13 13.29 3.71 11 -1 -13 13.43 2.78 -11 -1 13 13.24 3.71 -11 -1 14 116.60 5.23 11 -1 -14 109.93 5.17 -11 1 14 102.82 3.91 11 1 -14 106.18 5.12 11 1 -15 22.37 4.50 -11 1 15 23.88 4.51 -11 -1 15 24.67 4.56 -11 -1 16 1.68 4.31 -11 1 16 1.17 4.26 11 1 -16 0.31 5.09 -11 1 17 2.15 6.23 -11 1 17 0.90 5.05 -11 1 18 34.44 6.41 -11 1 20 0.54 4.36 11 3 -1 33.80 2.76 11 -3 -1 34.02 2.82 -11 3 1 31.52 3.85 -11 -3 1 35.27 2.75 11 -3 -2 52.96 2.46 -11 -3 2 52.99 2.43 11 3 -2 58.17 3.22 -11 3 2 54.27 2.46 11 3 -3 131.26 3.57 11 -3 -3 130.16 2.97 -11 -3 3 129.77 2.88 -11 3 3 123.23 3.59 11 -3 -4 572.89 5.31 -11 -3 4 571.98 5.27 11 3 -4 596.13 5.32 -11 3 4 536.47 4.69 11 -3 -5 376.87 4.14 11 3 -5 384.12 4.09 -11 -3 5 363.84 4.10 -11 3 5 370.79 4.60 11 -3 -6 39.49 2.90 11 3 -6 42.31 2.83 -11 -3 6 39.02 2.37 -11 3 6 39.00 2.83 11 3 -7 78.92 4.00 -11 3 7 77.97 4.05 -11 -3 7 79.96 4.05 11 -3 -7 79.59 3.11 11 3 -8 42.59 2.82 -11 -3 8 49.45 3.90 -11 3 8 43.73 2.85 11 -3 -8 44.84 2.90 11 -3 -9 11.12 2.76 11 3 -9 14.07 3.69 -11 -3 9 11.28 3.69 -11 3 9 9.94 2.66 11 3 -10 81.34 4.10 -11 3 10 81.80 3.08 11 -3 -10 82.21 4.15 -11 -3 10 85.40 4.10 -11 3 11 88.41 4.08 -11 -3 11 87.11 3.23 11 -3 -11 90.62 4.22 11 3 -11 83.92 3.18 11 -3 -12 105.16 3.35 11 3 -12 99.11 3.35 -11 3 12 103.21 3.26 -11 -3 12 107.72 4.30 11 3 -13 3.24 3.13 -11 3 13 2.19 4.32 -11 -3 13 3.17 4.40 -11 3 14 0.53 3.01 11 3 -14 0.80 4.31 -11 -3 14 0.68 3.08 -11 -3 15 -0.70 4.39 -11 3 15 0.59 4.18 11 3 -15 1.40 4.25 -11 3 15 1.62 4.35 -11 3 16 7.50 3.66 -11 -3 16 8.14 5.25 -11 3 16 10.37 5.01 11 3 -16 10.31 6.11 11 3 -17 3.45 5.89 -11 3 17 1.74 4.97 -11 3 17 2.08 3.56 -11 3 18 26.47 5.89 -11 3 18 26.00 5.77 -11 3 19 8.20 6.19 -11 3 19 8.58 5.59 11 5 -1 2.99 2.57 -11 -5 1 1.53 2.50 11 -5 -1 3.79 2.57 -11 5 1 1.02 2.60 11 -5 -2 58.88 3.91 11 5 -2 60.53 3.78 -11 -5 2 56.50 2.81 -11 5 2 62.37 3.85 -11 -5 3 7.78 3.63 11 -5 -3 8.01 2.64 11 5 -3 7.84 2.59 -11 5 3 10.28 2.61 11 -5 -4 293.21 3.89 -11 -5 4 284.79 3.81 11 5 -4 294.49 3.80 -11 5 4 288.58 3.88 -11 -5 5 18.28 2.64 -11 5 5 15.31 2.64 11 5 -5 17.01 2.60 11 -5 -5 14.53 3.73 -11 -5 6 44.69 2.78 11 -5 -6 45.01 2.85 11 5 -6 47.72 2.76 -11 5 6 46.86 2.76 -11 5 7 8.87 3.55 11 -5 -7 7.06 2.65 11 5 -7 6.64 3.56 -11 -5 7 8.77 3.61 11 -5 -8 111.31 3.19 11 5 -8 115.90 3.11 -11 -5 8 117.81 4.10 -11 5 8 115.77 4.01 11 5 -9 27.07 3.61 -11 5 9 27.27 2.64 -11 -5 9 26.73 3.73 11 5 -10 9.86 4.23 -11 -5 10 8.99 3.12 -11 5 10 7.79 3.03 11 5 -11 1.22 3.00 -11 -5 11 -0.37 4.32 -11 5 11 0.82 2.99 -11 -5 12 135.99 3.85 11 5 -12 141.89 4.87 -11 5 12 139.07 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112.88 3.88 11 7 -9 108.18 3.87 -11 7 9 104.18 4.04 -11 -7 10 2.12 5.00 -11 7 10 0.54 5.14 11 7 -10 -0.99 3.43 -11 7 10 -1.35 3.46 11 7 -11 54.32 3.64 -11 7 11 51.57 3.59 -11 -7 11 52.11 3.75 -11 7 11 56.19 3.91 -11 -7 12 -1.49 4.99 11 7 -12 2.68 4.82 -11 7 12 2.05 3.34 -11 7 12 1.13 3.62 -11 7 13 4.75 4.10 11 7 -13 0.80 3.98 -11 -7 13 1.12 4.12 -11 7 13 0.80 3.94 11 7 -14 12.12 4.03 -11 -7 14 13.39 4.15 -11 7 14 12.21 4.14 -11 7 14 9.33 5.52 -11 7 15 4.61 6.45 11 7 -15 2.41 6.28 -11 7 15 -1.59 4.42 11 7 -16 9.70 6.24 -11 7 16 11.28 6.36 -11 7 16 11.58 6.13 11 9 -1 5.92 3.90 -11 9 1 2.36 3.97 -11 -9 1 4.13 3.87 -11 9 1 4.80 3.94 11 9 -2 128.66 4.31 -11 -9 2 133.59 4.31 -11 9 2 131.28 5.90 -11 9 2 124.01 4.30 -11 9 3 2.16 3.97 -11 -9 3 0.16 5.56 -11 9 3 -1.46 3.94 11 9 -3 1.65 3.87 -11 -9 4 2.83 3.91 -11 9 4 -3.83 3.91 -11 9 4 1.00 5.65 11 9 -4 1.44 5.44 11 9 -5 20.02 5.51 -11 -9 5 20.13 4.00 -11 9 5 23.13 5.55 -11 9 5 19.03 5.72 -11 9 6 165.07 6.08 -11 -9 6 151.61 4.46 -11 9 6 154.36 4.39 11 9 -6 159.61 4.33 -11 9 7 23.20 3.94 -11 9 7 25.04 4.11 -11 -9 7 21.25 4.03 11 9 -7 23.68 3.93 11 9 -8 4.79 3.82 -11 9 8 7.96 3.83 -11 9 8 3.64 4.08 -11 -9 8 5.54 3.95 -11 9 9 0.39 4.59 -11 -9 9 1.94 4.45 11 9 -9 -2.02 4.31 -11 9 9 4.24 4.34 -11 9 10 39.03 4.48 -11 -9 10 44.20 4.56 11 9 -10 44.85 4.38 -11 9 10 35.75 6.60 -11 9 11 -1.95 4.26 11 9 -11 -2.05 6.05 -11 -9 11 0.01 4.48 -11 9 11 0.30 6.48 -11 9 12 2.80 5.10 -10 0 1 0.72 2.14 10 0 -1 -0.63 2.16 -10 0 2 129.32 3.77 10 0 -2 130.69 3.76 10 0 -3 -0.53 2.16 -10 0 3 0.34 3.04 10 0 -4 242.02 4.38 -10 0 4 237.94 3.75 -10 0 5 -1.44 3.07 10 0 -5 -0.96 2.18 10 0 -6 114.19 3.07 -10 0 6 116.38 3.06 -10 0 7 -0.08 3.03 10 0 -7 0.17 2.13 -10 0 8 59.70 2.68 10 0 -8 61.57 3.50 -10 0 9 0.17 3.00 10 0 -9 -0.47 3.06 -10 0 10 281.21 4.36 10 0 -10 309.18 5.29 -10 0 11 0.62 3.68 10 0 -11 0.20 3.75 -10 0 12 172.69 4.94 10 0 -12 188.45 5.08 -10 0 13 -1.31 3.69 10 0 -13 -0.22 3.73 -10 0 14 12.61 3.71 10 0 -14 10.80 3.77 -10 0 15 -1.01 5.33 -10 0 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10 -2 -12 68.34 3.22 10 2 -12 68.62 4.23 -10 2 13 19.07 3.75 -10 -2 13 22.06 3.84 10 2 -13 17.82 3.80 -10 2 14 23.84 4.51 10 2 -14 26.68 4.62 -10 -2 14 27.69 4.65 10 2 -15 39.48 5.60 -10 -2 15 37.67 4.86 -10 2 15 39.99 4.54 -10 2 15 39.17 4.71 10 2 -16 9.77 6.82 -10 2 16 12.75 4.32 -10 2 16 10.82 4.39 -10 2 17 16.90 5.18 -10 2 17 16.32 5.22 -10 2 18 16.91 6.96 -10 2 18 17.63 6.88 -10 2 19 13.79 7.54 -10 2 20 25.10 7.50 -10 -4 1 41.83 3.81 10 -4 -1 43.70 2.91 10 4 -1 42.85 2.82 -10 4 1 42.31 2.87 10 -4 -2 259.60 3.82 -10 -4 2 285.42 4.65 -10 4 2 268.45 4.70 10 4 -2 281.16 3.82 10 4 -3 40.93 3.79 10 -4 -3 35.33 2.80 -10 -4 3 40.97 3.82 -10 4 3 37.02 2.84 10 -4 -4 3.44 2.66 -10 -4 4 2.16 2.60 10 4 -4 2.77 3.62 -10 4 4 4.34 2.60 10 4 -5 209.38 3.63 10 -4 -5 208.59 4.54 -10 -4 5 208.19 3.63 -10 4 5 203.63 3.60 -10 -4 6 247.10 4.68 -10 4 6 251.03 4.62 10 4 -6 251.19 4.63 10 -4 -6 258.33 4.75 -10 -4 7 5.94 3.67 10 -4 -7 5.07 2.74 -10 4 7 9.10 3.67 10 4 -7 7.31 2.59 -10 -4 8 12.84 3.72 10 4 -8 13.47 3.65 10 -4 -8 17.98 3.82 -10 4 8 13.56 3.68 -10 -4 9 15.43 3.74 10 4 -9 15.58 3.68 10 -4 -9 18.40 3.88 -10 4 9 16.97 2.66 10 4 -10 166.13 3.61 -10 4 10 159.11 3.47 -10 -4 10 164.25 4.50 -10 4 11 1.26 2.54 10 4 -11 0.01 2.54 -10 -4 11 0.92 3.65 -10 4 12 0.45 4.30 10 4 -12 0.33 3.03 -10 -4 12 0.79 3.09 -10 4 13 17.37 4.53 -10 -4 13 17.33 4.53 10 4 -13 18.04 4.43 -10 4 13 18.72 4.36 10 4 -14 167.36 5.40 -10 4 14 175.24 4.07 -10 -4 14 177.61 5.53 -10 4 14 170.38 4.14 -10 -4 15 16.40 5.30 10 4 -15 13.34 3.69 -10 4 15 18.75 5.14 -10 4 15 17.85 3.61 -10 4 16 0.66 4.91 -10 4 16 0.06 3.56 10 4 -16 0.23 4.93 10 4 -17 1.49 7.95 -10 4 17 1.46 5.70 -10 4 17 2.98 4.02 10 4 -17 2.76 6.86 -10 4 18 33.79 5.87 -10 4 18 33.14 5.80 -10 4 19 3.63 6.39 -10 4 19 3.78 6.28 -10 -6 1 79.31 2.86 10 6 -1 77.50 2.87 -10 6 1 70.56 2.90 -10 -6 2 23.15 2.62 10 6 -2 24.74 2.64 -10 6 2 26.52 2.67 10 6 -3 52.86 2.74 -10 6 3 53.95 3.73 -10 -6 3 53.17 2.77 10 6 -4 33.29 3.60 -10 -6 4 29.57 3.67 -10 6 4 36.40 3.67 10 6 -5 58.78 2.77 -10 -6 5 59.79 3.82 -10 6 5 61.23 2.81 10 6 -6 251.48 3.65 -10 6 6 261.27 4.46 -10 -6 6 250.79 3.66 -10 6 7 84.58 3.38 -10 -6 7 91.74 4.60 10 6 -7 80.88 3.33 -10 6 8 47.09 3.19 -10 -6 8 50.05 4.45 10 6 -8 50.32 3.15 10 6 -9 7.71 4.19 -10 6 9 6.44 4.48 -10 6 9 5.75 4.22 -10 -6 9 8.86 3.03 -10 6 10 31.62 3.08 -10 6 10 27.04 3.29 10 6 -10 28.36 3.08 -10 -6 10 29.75 4.45 -10 6 11 5.45 2.95 -10 6 11 8.32 3.12 10 6 -11 6.09 4.15 -10 -6 11 4.60 3.08 -10 -6 12 35.78 5.28 -10 6 12 41.63 5.32 -10 6 12 34.11 3.61 10 6 -12 34.85 3.68 -10 6 13 5.31 3.65 10 6 -13 3.89 4.90 -10 -6 13 5.52 3.66 -10 6 13 3.78 4.90 -10 6 14 103.36 3.88 -10 -6 14 99.03 4.28 10 6 -14 99.64 4.05 -10 6 14 93.57 4.01 10 6 -15 15.52 5.72 -10 6 15 17.39 4.13 -10 6 15 15.15 5.61 10 6 -16 9.56 3.99 -10 6 16 11.97 5.71 -10 6 16 12.04 4.00 10 6 -17 -0.59 4.47 10 6 -17 1.21 6.20 -10 6 17 -2.42 6.40 -10 6 17 2.32 4.39 -10 -8 1 74.48 3.71 -10 8 1 72.69 5.21 -10 8 1 75.65 3.73 10 8 -1 76.11 3.75 -10 8 2 17.33 3.53 -10 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14.63 5.13 -9 7 12 15.20 4.84 -9 7 12 18.19 5.15 9 7 -12 14.92 3.51 -9 7 13 126.65 5.59 -9 7 13 119.02 4.63 9 7 -13 119.70 4.50 9 7 -14 -2.94 5.64 -9 7 14 1.07 5.51 -9 7 14 2.06 5.80 9 7 -15 10.14 4.45 -9 7 15 8.28 6.47 -9 7 15 9.37 6.27 9 7 -15 8.53 6.44 9 7 -16 0.57 4.48 -9 7 16 -2.59 6.36 9 7 -16 0.62 4.41 -9 7 16 -0.13 4.38 -9 9 1 22.94 4.08 9 9 -1 21.37 3.99 -9 9 1 21.39 5.70 -9 -9 1 24.03 3.97 -9 9 2 154.62 3.95 -9 9 2 167.35 5.27 -9 -9 2 150.91 3.95 9 9 -2 151.84 5.12 -9 9 3 -0.01 3.43 -9 9 3 0.82 3.45 -9 -9 3 2.08 3.42 9 9 -3 -0.48 3.30 -9 9 4 0.59 3.48 -9 -9 4 3.00 4.84 9 9 -4 -0.09 3.37 -9 9 4 2.88 4.79 -9 -9 5 18.66 5.30 -9 9 5 15.73 3.99 -9 9 5 13.94 3.51 9 9 -5 9.85 3.39 -9 -9 6 98.79 4.35 -9 9 6 99.62 5.80 -9 9 6 95.31 4.40 9 9 -6 108.94 5.68 -9 9 7 1.28 5.56 -9 -9 7 1.81 5.61 -9 9 7 3.18 5.80 9 9 -7 4.02 3.87 -9 9 8 1.03 4.07 -9 9 8 -0.48 5.44 -9 -9 8 4.04 3.97 9 9 -8 -0.20 3.80 -9 9 9 62.10 4.30 -9 9 9 64.29 4.06 9 9 -9 61.78 4.07 -9 -9 9 55.23 5.84 -9 9 10 61.51 4.28 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3.64 8 4 -2 120.73 2.84 8 -4 -3 98.81 2.80 -8 4 3 99.54 3.50 -8 -4 3 100.17 3.43 8 4 -3 103.25 3.44 -8 -4 4 27.89 3.10 8 4 -4 29.28 3.07 8 -4 -4 28.10 3.18 -8 4 4 30.63 3.13 8 -4 -5 1.33 3.08 -8 4 5 4.10 2.12 -8 -4 5 4.18 2.13 8 4 -5 2.81 2.09 8 4 -6 165.75 3.17 -8 -4 6 164.84 3.21 -8 4 6 169.51 3.19 8 -4 -6 169.40 3.26 -8 4 7 14.48 2.71 -8 -4 7 11.48 3.75 8 4 -7 13.25 2.63 -8 4 8 30.91 3.78 -8 -4 8 30.61 3.84 8 4 -8 30.88 2.74 -8 4 9 0.44 2.59 8 4 -9 3.70 3.58 -8 -4 9 1.77 2.62 -8 4 10 169.23 3.58 -8 -4 10 171.96 4.74 8 4 -10 178.14 4.64 -8 -4 11 6.14 3.77 8 4 -11 6.59 3.62 -8 4 11 6.95 2.78 -8 4 11 6.57 3.63 -8 -4 12 32.15 2.91 8 4 -12 29.60 2.83 -8 4 12 31.63 2.87 -8 4 12 33.14 3.77 -8 4 13 8.70 3.08 -8 -4 13 8.36 4.45 8 4 -13 8.85 4.37 -8 4 13 7.68 4.47 -8 4 14 145.92 4.08 8 4 -14 144.44 5.50 -8 4 14 153.04 3.99 8 4 -15 0.28 5.47 -8 4 15 -1.13 5.13 8 4 -15 -1.58 5.48 -8 4 15 -0.33 5.04 8 4 -16 0.49 6.79 -8 4 16 0.72 4.96 -8 4 16 3.06 4.90 8 4 -16 0.82 7.67 -8 4 17 5.03 5.66 -8 4 17 6.10 5.81 -8 4 18 14.87 5.77 -8 4 18 14.05 5.64 -8 4 19 3.11 7.59 -8 4 19 3.41 7.67 -8 6 1 131.19 3.20 -8 -6 1 135.28 3.19 8 6 -1 138.83 4.10 -8 6 2 378.58 4.12 -8 -6 2 401.24 4.91 8 6 -2 400.38 4.18 -8 6 3 168.77 3.37 -8 -6 3 165.92 4.27 8 6 -3 174.61 4.20 -8 -6 4 47.65 3.80 8 6 -4 48.97 3.70 -8 6 4 44.98 2.79 8 6 -5 4.16 2.51 -8 -6 5 0.94 2.59 -8 6 5 1.47 3.61 -8 -6 6 103.87 4.06 -8 6 6 102.55 3.04 8 6 -6 105.09 3.03 -8 6 6 102.45 3.13 -8 -6 7 61.06 3.91 -8 6 7 58.88 2.82 -8 6 7 60.23 2.97 8 6 -7 60.51 2.83 -8 6 8 2.81 2.65 -8 -6 8 2.31 2.59 -8 6 8 1.62 2.51 8 6 -8 2.81 2.47 -8 6 9 13.40 3.28 -8 6 9 11.66 4.26 -8 -6 9 12.90 3.19 8 6 -9 14.04 3.00 -8 6 10 129.16 4.67 -8 -6 10 123.29 4.91 -8 6 10 118.83 3.70 8 6 -10 122.27 3.56 8 6 -11 29.00 4.28 -8 6 11 25.62 3.28 -8 -6 11 28.53 4.48 -8 6 11 31.70 4.25 -8 6 12 28.50 3.06 8 6 -12 32.25 4.29 -8 -6 12 27.24 3.25 -8 6 12 31.11 4.48 8 6 -13 2.00 3.48 -8 6 13 3.26 4.91 -8 6 13 -0.34 5.15 8 6 -14 32.29 5.05 -8 6 14 31.84 5.10 -8 6 14 30.69 5.00 8 6 -15 26.58 5.87 -8 6 15 26.28 4.31 8 6 -15 35.46 5.78 -8 6 15 35.72 4.14 8 6 -16 1.41 5.63 8 6 -16 3.88 5.61 -8 6 16 4.95 3.95 -8 6 16 4.91 3.99 8 6 -17 8.14 7.65 -8 6 17 8.94 6.41 8 6 -17 7.70 6.27 -8 6 17 8.73 6.28 -8 8 1 222.16 3.88 -8 8 1 225.93 3.83 -8 -8 1 237.07 4.84 8 8 -1 233.74 3.80 -8 8 2 4.93 3.00 -8 -8 2 7.93 2.94 8 8 -2 6.30 4.14 -8 8 2 10.83 4.25 -8 8 3 56.55 3.15 -8 -8 3 52.67 3.21 8 8 -3 51.68 3.14 -8 8 3 52.43 3.23 -8 -8 4 49.43 3.17 -8 8 4 48.11 3.15 8 8 -4 48.81 3.11 -8 8 4 50.41 3.21 -8 8 5 58.33 4.40 -8 -8 5 49.26 3.21 8 8 -5 54.19 3.10 -8 8 5 55.11 4.32 -8 -8 6 7.44 4.61 -8 8 6 7.96 2.88 -8 8 6 4.55 3.01 8 8 -6 6.07 4.46 -8 -8 7 21.09 5.07 -8 8 7 21.97 3.50 -8 8 7 21.91 5.13 8 8 -7 18.90 3.46 -8 8 8 114.75 3.87 -8 -8 8 116.53 5.35 8 8 -8 117.78 3.83 -8 8 8 122.67 5.50 -8 8 9 55.92 4.97 -8 -8 9 57.44 3.75 8 8 -9 52.96 3.60 -8 8 9 61.46 5.32 -8 8 10 0.51 3.66 -8 8 10 0.70 3.40 -8 -8 10 3.30 4.97 8 8 -10 5.75 3.32 8 8 -11 4.67 5.48 -8 8 11 2.72 3.89 -8 8 11 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330.19 4.63 7 -1 -3 341.06 5.22 -7 -1 3 343.96 4.71 7 1 -4 13.04 3.14 -7 -1 4 14.10 3.22 -7 1 4 14.81 2.34 7 -1 -4 13.61 2.35 -7 -1 5 460.83 5.97 7 1 -5 444.60 5.48 -7 1 5 450.61 5.84 7 -1 -5 454.79 5.47 -7 -1 6 9.00 3.17 7 1 -6 8.29 2.27 -7 1 6 7.87 2.27 7 -1 -6 9.05 2.32 7 1 -7 3.16 3.11 -7 -1 7 3.16 2.20 -7 1 7 2.62 3.10 7 -1 -7 4.73 2.27 7 -1 -8 22.07 2.52 7 1 -8 21.70 3.28 -7 1 8 20.93 2.40 -7 -1 8 21.74 2.43 7 -1 -9 10.42 3.23 -7 1 9 10.68 3.08 7 1 -9 9.95 3.18 -7 -1 9 10.52 3.10 7 -1 -10 447.26 6.65 -7 1 10 434.00 6.39 -7 -1 10 447.96 6.90 7 1 -10 448.65 7.09 7 1 -11 18.14 4.03 -7 -1 11 17.35 3.97 -7 1 11 17.57 3.90 7 1 -12 10.24 4.76 -7 1 12 9.83 3.77 -7 -1 12 11.75 4.78 -7 1 13 37.07 4.22 -7 1 13 31.89 4.24 -7 1 14 64.23 5.75 -7 1 14 71.39 6.35 -7 1 15 2.41 3.76 -7 1 16 10.98 4.64 -7 1 17 6.48 3.39 -7 1 18 47.98 5.39 -7 1 19 4.90 4.43 -7 1 20 0.04 4.12 -7 -3 1 1.46 2.13 7 -3 -1 2.86 2.15 -7 3 1 2.05 2.17 7 3 -1 2.29 2.11 7 -3 -2 95.32 2.93 -7 -3 2 89.68 2.82 -7 3 2 88.99 2.86 7 3 -2 92.53 2.79 7 -3 -3 281.83 4.01 -7 3 3 282.80 3.99 -7 -3 3 281.57 3.95 7 3 -3 272.40 3.87 -7 -3 4 435.81 5.20 7 -3 -4 418.69 4.62 7 3 -4 423.27 4.68 -7 3 4 420.14 4.66 -7 -3 5 9.60 2.20 7 -3 -5 2.43 2.21 7 3 -5 8.30 2.16 -7 3 5 7.66 2.22 7 3 -6 37.44 2.44 -7 -3 6 37.81 2.49 7 -3 -6 39.84 2.50 -7 3 6 38.61 2.46 7 3 -7 31.19 3.15 7 -3 -7 32.37 2.50 -7 -3 7 30.58 2.43 -7 3 7 29.80 2.38 7 3 -8 362.26 4.71 -7 -3 8 343.86 4.66 -7 3 8 362.02 5.02 -7 3 9 383.14 5.16 7 3 -9 370.59 5.45 -7 -3 9 369.33 5.49 7 3 -10 9.84 2.73 -7 -3 10 10.79 3.88 -7 3 10 9.78 2.67 -7 3 11 70.76 3.30 7 3 -11 74.86 3.42 -7 -3 11 74.38 3.46 -7 3 11 76.62 3.20 -7 -3 12 47.93 4.29 -7 3 12 50.62 3.98 -7 3 12 50.19 4.10 7 3 -12 46.48 4.15 7 3 -13 38.21 4.92 -7 3 13 41.11 2.91 -7 3 13 38.87 4.04 7 3 -14 1.43 5.32 -7 3 14 0.81 4.42 -7 3 14 1.93 4.25 7 3 -14 0.73 5.31 -7 3 15 51.05 4.61 -7 3 15 45.28 4.69 -7 3 16 60.93 5.63 -7 3 16 64.64 5.48 -7 3 17 33.46 5.27 -7 3 17 35.76 6.50 -7 3 18 9.01 4.76 -7 3 19 0.25 4.47 -7 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5 16 53.50 6.05 7 5 -16 40.98 5.96 7 5 -16 46.32 6.14 -7 5 16 60.92 5.93 -7 5 17 3.84 4.08 -7 5 17 4.01 4.00 -7 5 18 11.02 4.62 -7 5 18 15.07 6.36 -7 7 1 175.70 3.76 7 7 -1 182.23 3.73 -7 7 1 182.27 3.82 -7 -7 1 186.38 4.52 -7 7 2 27.82 3.71 7 7 -2 25.90 2.66 -7 7 2 24.01 3.67 -7 -7 2 21.69 2.62 -7 7 3 256.67 4.45 -7 7 3 267.13 4.50 7 7 -3 269.54 3.64 -7 -7 3 259.42 3.68 7 7 -4 116.82 3.45 -7 7 4 117.07 3.52 -7 -7 4 111.28 3.53 -7 7 4 111.98 4.30 -7 7 5 1.28 3.04 -7 -7 5 2.45 3.07 7 7 -5 0.03 3.02 -7 7 5 1.95 3.16 -7 7 6 134.48 3.68 -7 7 6 137.50 3.56 -7 -7 6 138.09 4.77 7 7 -6 140.21 4.61 -7 7 7 1.92 3.00 -7 7 7 3.96 3.11 7 7 -7 2.01 2.95 -7 -7 7 -0.62 3.07 -7 7 8 107.32 3.60 -7 -7 8 108.80 3.58 -7 7 8 109.33 3.41 7 7 -8 108.03 4.53 -7 7 9 158.45 4.68 7 7 -9 152.16 3.64 -7 7 9 152.38 4.95 -7 -7 9 151.93 3.81 -7 7 10 45.61 3.32 -7 7 10 41.55 3.14 7 7 -10 45.46 4.27 -7 -7 10 42.72 3.29 -7 7 11 5.67 3.67 -7 7 11 5.35 3.47 7 7 -11 5.02 3.43 -7 7 12 10.45 4.86 -7 7 12 13.12 5.11 7 7 -12 11.60 4.84 -7 7 13 1.31 3.36 7 7 -13 2.51 3.45 -7 7 13 -1.09 3.57 7 7 -13 -0.25 3.42 7 7 -14 40.95 5.84 -7 7 14 44.38 5.91 -7 7 14 45.76 4.12 7 7 -14 46.85 5.82 -7 7 15 6.82 5.93 7 7 -15 6.01 6.05 -7 7 15 2.90 6.10 7 7 -15 5.72 5.95 -7 7 16 22.31 4.53 -7 7 16 24.41 6.42 7 7 -16 25.91 6.35 7 7 -16 20.25 4.53 -7 9 1 5.10 4.88 -7 -9 1 4.03 4.82 7 9 -1 1.19 4.85 -7 9 1 2.45 3.50 -7 9 2 61.09 3.73 -7 -9 2 71.33 3.66 7 9 -2 71.43 3.67 -7 9 2 59.74 3.71 -7 9 3 29.94 4.94 7 9 -3 26.65 3.46 -7 9 3 25.77 3.58 -7 -9 3 23.87 3.55 -7 9 4 -0.56 3.44 7 9 -4 0.65 4.76 -7 9 4 0.63 3.50 -7 -9 4 -1.03 3.48 -7 9 5 2.45 4.81 -7 -9 5 4.43 3.45 7 9 -5 3.56 3.36 -7 9 5 6.17 3.50 -7 9 6 43.34 3.57 -7 -9 6 41.53 5.07 7 9 -6 47.39 3.50 -7 9 6 48.63 5.09 -7 9 7 0.63 3.36 -7 9 7 1.47 3.54 7 9 -7 3.45 3.33 -7 -9 7 -2.83 3.47 -7 9 8 21.35 3.97 -7 9 8 21.58 4.19 7 9 -8 19.67 3.94 -7 9 9 0.79 3.85 -7 9 9 1.25 4.10 7 9 -9 -1.93 3.88 -7 9 10 34.03 4.23 -7 9 10 34.93 3.95 7 9 -10 36.30 5.46 -7 9 11 1.71 4.35 -7 9 11 2.85 4.62 7 9 -11 1.97 4.32 -7 9 12 0.20 4.29 7 9 -12 -0.56 4.53 -7 9 12 1.94 4.55 7 9 -12 0.15 4.33 -6 0 1 0.27 2.24 6 0 -1 0.69 3.18 6 0 -2 283.27 5.61 -6 0 2 278.54 5.90 -6 0 3 -0.64 3.24 6 0 -3 0.77 2.29 -6 0 4 4013.31 7.38 -6 0 5 0.09 3.34 6 0 -5 0.47 2.26 6 0 -6 189.78 4.92 -6 0 6 181.43 5.16 -6 0 7 -0.32 3.13 6 0 -7 1.14 2.26 -6 0 8 341.05 6.28 6 0 -8 348.36 6.37 6 0 -9 -0.01 2.19 -6 0 9 0.04 3.05 6 0 -10 12.05 3.33 -6 0 10 7.86 3.13 -6 0 11 1.26 4.53 -6 0 12 613.92 6.37 -6 0 14 13.81 4.86 -6 0 16 44.89 5.48 -6 0 18 2.69 3.98 -6 0 20 62.90 6.31 6 2 -1 181.21 3.60 6 -2 -1 186.48 4.30 -6 -2 1 178.93 4.18 -6 2 1 189.03 4.30 6 2 -2 17.01 2.35 6 -2 -2 15.45 2.42 -6 -2 2 16.92 2.36 -6 2 2 16.22 2.37 6 2 -3 947.66 7.28 6 -2 -3 916.48 7.19 -6 -2 3 943.15 7.25 -6 2 3 928.14 7.53 6 2 -4 421.42 5.12 6 -2 -4 407.05 5.06 -6 2 4 405.18 4.99 -6 -2 4 414.29 5.13 6 2 -5 553.92 5.93 6 -2 -5 547.38 5.82 -6 -2 5 540.47 6.32 -6 2 5 540.92 6.16 6 2 -6 40.75 2.64 -6 -2 6 40.49 2.63 -6 2 6 42.33 2.63 6 -2 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540.56 5.40 -6 -4 6 510.68 5.55 6 4 -6 529.28 5.53 -6 -4 7 150.87 3.30 -6 4 7 152.87 3.82 6 4 -7 149.60 3.23 -6 4 8 2.31 2.63 -6 -4 8 2.34 2.67 -6 4 8 3.78 2.71 6 4 -8 2.83 2.55 -6 4 9 100.36 3.27 -6 4 9 100.64 3.34 -6 -4 9 93.81 3.45 6 4 -9 101.56 3.35 -6 -4 10 147.31 4.75 -6 4 10 147.59 4.59 -6 4 10 155.05 4.42 6 4 -10 152.88 4.58 -6 4 11 8.61 2.62 6 4 -11 8.68 3.67 -6 4 11 7.00 3.79 -6 -4 11 11.17 3.83 -6 4 12 7.16 2.69 -6 4 12 7.32 3.62 6 4 -12 7.19 2.60 6 4 -13 0.49 4.33 -6 4 13 0.25 3.09 -6 4 13 -1.31 4.30 6 4 -13 1.36 4.34 6 4 -14 39.82 5.58 6 4 -14 43.60 5.63 -6 4 14 42.78 4.59 -6 4 14 48.42 4.51 6 4 -15 4.24 7.92 -6 4 15 6.28 5.13 -6 4 15 3.86 3.54 6 4 -15 4.53 8.53 -6 4 16 24.39 5.17 -6 4 16 21.66 5.13 -6 4 17 23.69 5.82 -6 4 17 22.14 5.94 -6 4 18 12.52 5.62 -6 4 18 13.03 6.91 -6 4 19 16.02 12.36 -6 4 19 12.32 10.83 -6 6 1 11.83 2.68 -6 -6 1 10.04 3.69 6 6 -1 12.53 3.65 -6 6 1 11.50 3.70 -6 -6 2 401.91 5.03 -6 6 2 396.95 4.34 6 6 -2 406.07 4.30 -6 6 2 413.30 4.35 -6 6 3 105.69 3.12 -6 6 3 110.89 3.16 6 6 -3 111.33 4.01 -6 -6 3 106.42 4.13 -6 6 4 12.58 3.78 -6 6 4 15.32 2.61 6 6 -4 15.86 3.65 -6 -6 4 16.09 2.69 -6 6 5 170.89 4.22 6 6 -5 172.21 3.40 -6 6 5 170.02 4.37 -6 -6 5 171.13 3.46 -6 6 6 79.62 3.86 -6 -6 6 75.34 3.02 6 6 -6 77.12 3.89 -6 6 6 76.36 4.07 -6 -6 7 26.41 3.81 -6 6 7 25.71 2.83 6 6 -7 27.50 3.66 -6 6 7 27.15 3.66 -6 6 8 0.71 3.73 6 6 -8 2.70 2.51 -6 -6 8 3.57 3.68 -6 6 8 1.94 2.49 -6 6 9 45.12 4.39 6 6 -9 41.12 4.37 -6 6 9 40.81 4.67 -6 -6 9 40.90 3.41 -6 6 10 138.59 5.01 -6 6 10 140.59 4.77 -6 -6 10 130.59 3.86 6 6 -10 136.88 3.68 -6 6 11 47.87 3.21 6 6 -11 48.76 4.40 -6 6 11 47.23 3.36 -6 6 12 32.48 4.30 -6 6 12 30.05 3.22 6 6 -12 27.97 3.15 -6 6 13 67.84 5.17 6 6 -13 54.24 3.89 -6 6 13 56.52 3.96 6 6 -13 66.11 5.24 -6 6 14 20.08 4.90 6 6 -14 19.18 5.00 6 6 -14 14.19 4.99 -6 6 14 19.90 5.08 -6 6 15 17.37 5.71 -6 6 15 18.39 5.79 6 6 -15 12.31 4.08 6 6 -15 14.26 5.65 -6 6 16 2.65 5.52 6 6 -16 1.10 5.45 6 6 -16 -0.15 5.47 -6 6 16 -0.19 5.63 -6 6 17 -2.70 6.38 6 6 -17 -0.01 8.76 6 6 -17 0.59 8.75 -6 6 17 -1.48 6.29 -6 8 1 8.12 3.07 -6 8 1 8.41 4.29 6 8 -1 11.34 4.24 -6 -8 1 12.90 3.01 -6 8 2 9.13 3.00 -6 8 2 8.44 3.05 6 8 -2 7.08 2.98 -6 -8 2 7.70 3.06 -6 8 3 290.86 4.03 6 8 -3 313.28 4.05 -6 8 3 306.48 4.13 -6 -8 3 309.71 4.16 -6 8 4 65.40 3.22 -6 -8 4 61.86 3.27 6 8 -4 66.61 3.20 -6 8 4 65.82 3.35 -6 8 5 10.81 3.02 6 8 -5 14.98 2.95 -6 -8 5 14.57 4.24 -6 8 5 12.74 4.32 -6 8 6 -0.56 2.92 -6 -8 6 1.83 2.98 6 8 -6 2.01 4.07 -6 8 6 0.46 3.07 -6 -8 7 33.12 3.15 -6 8 7 40.76 3.24 6 8 -7 43.15 3.05 -6 8 7 40.30 3.10 -6 8 8 78.34 5.02 -6 8 8 67.75 3.93 6 8 -8 70.25 3.68 -6 8 9 -3.08 3.42 -6 8 9 1.58 3.60 6 8 -9 -0.13 4.80 -6 8 10 0.30 3.40 -6 8 10 -0.03 5.12 6 8 -10 2.67 3.38 -6 8 11 68.02 4.14 -6 8 11 71.17 6.08 6 8 -11 65.70 4.20 6 8 -12 10.49 5.79 -6 8 12 11.94 3.95 -6 8 12 15.01 4.16 6 8 -12 10.42 3.93 -6 8 13 8.68 5.46 6 8 -13 2.65 4.03 6 8 -13 3.59 5.48 -6 8 13 3.47 5.72 -6 8 14 3.80 4.53 -6 8 14 7.09 6.23 6 8 -14 9.48 4.53 6 8 -14 10.73 6.24 -6 10 1 17.56 3.97 6 10 -1 13.07 3.96 -6 10 1 14.59 3.95 -6 10 2 4.73 5.54 -6 10 2 0.21 3.94 6 10 -2 1.25 5.46 -6 10 3 -1.23 3.94 6 10 -3 7.97 5.37 -6 10 3 0.38 3.98 -6 10 4 82.27 5.65 -6 10 4 80.20 4.27 6 10 -4 87.63 5.61 -6 10 5 -1.24 3.89 -6 10 5 3.98 3.97 6 10 -5 -2.84 5.44 -6 10 6 1.39 3.85 -6 10 6 3.42 5.62 6 10 -6 -0.83 3.78 -6 10 7 0.61 4.39 -6 10 7 -0.77 4.57 6 10 -7 5.49 6.09 -6 10 8 76.17 6.20 6 10 -8 79.46 6.18 -6 10 8 81.45 6.52 -6 10 9 1.86 4.20 6 10 -9 -2.78 4.44 6 10 -9 6.94 5.97 -6 10 9 0.56 4.52 -5 -1 1 280.76 4.96 5 1 -1 286.16 5.05 -5 1 1 293.14 5.11 5 -1 -1 287.48 5.11 -5 1 2 931.55 8.29 -5 -1 2 910.86 8.23 5 1 -2 961.74 8.41 5 -1 -2 946.33 8.38 -5 1 3 401.35 5.65 5 1 -3 390.11 5.89 -5 -1 3 398.24 5.75 5 -1 -3 399.98 5.91 5 1 -4 234.32 4.72 5 -1 -4 241.47 4.74 -5 1 4 234.82 4.63 -5 -1 4 240.49 5.23 5 1 -5 1084.92 10.00 5 -1 -5 1085.14 9.69 -5 1 5 1084.07 9.60 -5 -1 5 1094.49 9.67 5 1 -6 935.02 9.68 5 -1 -6 934.07 8.92 -5 1 6 958.11 9.19 -5 -1 6 970.35 9.51 5 -1 -7 22.46 2.63 5 1 -7 19.25 3.39 -5 -1 7 18.38 2.51 -5 1 7 18.53 2.50 -5 -1 8 1.07 3.05 5 -1 -8 0.35 3.19 5 1 -8 -0.02 3.09 -5 1 8 0.63 3.03 -5 -1 9 4.40 3.14 -5 1 9 3.41 3.03 5 1 -9 3.59 3.84 5 1 -10 151.29 7.18 -5 -1 10 134.20 6.89 -5 1 10 133.19 4.79 -5 1 10 122.48 4.80 -5 1 11 50.05 4.59 -5 1 11 53.76 4.54 -5 1 12 54.00 5.63 -5 1 12 54.31 6.14 -5 1 13 11.51 4.38 -5 1 14 53.59 6.03 -5 1 15 72.06 6.38 -5 1 16 0.36 4.22 -5 1 17 0.49 3.66 -5 1 18 11.95 4.88 -5 1 19 12.31 4.33 -5 1 20 11.87 4.28 -5 3 1 192.13 4.26 -5 -3 1 194.89 3.61 5 -3 -1 193.45 3.66 5 3 -1 199.59 3.60 5 -3 -2 212.51 3.74 -5 3 2 206.09 4.34 5 3 -2 215.63 3.72 -5 -3 2 210.52 3.73 -5 -3 3 27.74 3.26 5 -3 -3 25.68 2.50 -5 3 3 28.09 2.46 5 3 -3 27.97 2.43 -5 3 4 211.56 4.33 -5 -3 4 213.77 3.83 5 -3 -4 210.70 4.40 5 3 -4 219.78 4.41 -5 3 5 1.98 2.18 5 3 -5 2.81 2.97 -5 -3 5 2.74 2.19 -5 3 6 144.24 3.33 -5 -3 6 152.85 4.14 5 3 -6 151.56 3.45 -5 3 7 47.37 2.59 -5 -3 7 45.46 3.47 5 3 -7 49.08 3.35 -5 -3 8 348.72 5.12 -5 3 8 356.01 4.65 -5 3 8 363.11 5.33 5 3 -8 362.14 5.55 -5 3 9 15.54 3.09 -5 -3 9 13.98 2.35 5 3 -9 14.83 2.29 -5 3 9 14.38 2.35 -5 -3 10 7.58 3.88 5 3 -10 7.38 3.75 -5 3 10 7.84 2.79 -5 3 10 6.57 3.72 -5 3 11 37.00 2.95 -5 3 11 38.18 4.07 5 3 -11 38.32 4.15 -5 3 12 15.68 3.76 5 3 -12 14.25 4.71 5 3 -12 14.39 4.70 -5 3 12 15.46 2.77 5 3 -13 20.99 6.74 5 3 -13 21.77 6.21 -5 3 13 20.01 2.83 -5 3 13 25.11 3.81 -5 3 14 31.60 4.69 -5 3 14 36.35 4.56 -5 3 15 34.27 4.65 -5 3 15 33.54 4.56 -5 3 16 63.99 5.65 -5 3 16 63.60 5.73 -5 3 17 28.37 9.03 -5 3 17 28.05 9.07 -5 3 18 0.99 6.79 -5 3 19 4.80 5.01 -5 -5 1 54.80 2.47 5 5 -1 54.19 3.24 -5 5 1 49.12 2.48 -5 5 2 23.48 3.12 5 5 -2 23.33 2.27 -5 -5 2 24.06 2.25 -5 -5 3 0.51 2.11 -5 5 3 -0.26 2.17 5 5 -3 1.16 2.94 -5 5 3 0.47 2.99 -5 -5 4 498.66 4.74 5 5 -4 501.39 5.11 -5 5 4 503.84 4.69 -5 5 4 514.84 5.09 -5 5 5 7.09 2.19 5 5 -5 7.18 2.10 -5 5 5 7.63 2.13 -5 -5 5 6.22 2.15 5 5 -6 7.18 3.62 -5 -5 6 7.93 2.67 -5 5 6 8.33 2.63 -5 5 6 9.05 2.72 -5 5 7 95.46 3.28 5 5 -7 105.46 3.21 -5 5 7 106.82 3.18 -5 -5 7 104.43 4.28 -5 5 8 548.32 5.75 5 5 -8 546.61 6.03 -5 5 8 509.49 5.10 -5 -5 8 510.78 5.38 -5 5 9 12.56 3.68 5 5 -9 13.14 2.67 -5 -5 9 13.66 3.82 -5 5 9 12.91 3.86 -5 5 10 23.00 2.69 -5 5 10 26.33 3.84 5 5 -10 24.17 2.69 -5 5 11 38.84 4.45 -5 5 11 33.88 4.62 5 5 -11 38.38 4.49 -5 5 12 78.63 4.59 5 5 -12 63.56 4.77 5 5 -12 73.82 3.61 -5 5 12 67.34 3.54 -5 5 13 0.82 3.04 5 5 -13 1.95 3.00 -5 5 13 1.91 3.09 5 5 -13 3.28 4.20 -5 5 14 11.06 5.17 5 5 -14 9.85 5.06 5 5 -14 15.06 5.01 -5 5 14 14.01 3.57 -5 5 15 17.19 5.12 5 5 -15 17.27 6.11 -5 5 15 18.58 5.03 5 5 -15 14.71 6.05 -5 5 16 79.46 6.06 -5 5 16 66.37 6.14 -5 5 17 3.73 5.71 -5 5 17 1.56 5.58 -5 5 18 10.98 6.28 -5 5 18 9.16 4.51 -5 -7 1 20.86 2.62 -5 7 1 17.60 2.65 5 7 -1 23.01 3.62 -5 7 1 22.73 3.70 -5 -7 2 77.03 2.93 -5 7 2 76.93 2.93 -5 7 2 82.33 3.91 5 7 -2 77.37 2.88 -5 7 3 82.96 2.91 5 7 -3 78.28 3.82 -5 7 3 79.33 3.90 -5 -7 3 78.12 2.96 -5 7 4 34.15 3.69 5 7 -4 38.70 3.63 -5 7 4 33.96 2.75 -5 -7 4 32.78 2.72 -5 7 5 168.44 3.30 -5 -7 5 168.15 4.27 5 7 -5 171.71 3.30 -5 7 5 168.21 4.34 5 7 -6 22.64 4.27 -5 -7 6 21.68 4.50 -5 7 6 20.20 3.10 -5 7 6 18.22 3.23 -5 7 7 5.47 4.45 -5 7 7 6.97 3.01 5 7 -7 5.48 2.92 -5 -7 7 5.29 3.11 -5 7 8 1.18 4.19 5 7 -8 0.95 4.12 -5 7 8 1.56 3.12 -5 7 9 14.51 4.42 -5 7 9 11.97 3.00 5 7 -9 12.85 2.93 -5 7 10 73.85 3.28 -5 7 10 75.65 4.61 5 7 -10 75.53 3.29 -5 7 11 43.27 3.57 5 7 -11 45.74 5.08 5 7 -11 39.01 3.79 -5 7 11 41.10 5.32 -5 7 12 53.59 3.66 5 7 -12 46.48 3.80 5 7 -12 56.78 5.12 -5 7 12 50.53 3.85 -5 7 13 118.62 5.63 5 7 -13 98.49 5.77 5 7 -13 110.36 4.06 -5 7 13 108.44 5.78 -5 7 14 4.41 3.96 -5 7 14 7.80 5.71 5 7 -14 5.75 5.64 5 7 -14 6.56 5.59 -5 7 15 -1.06 4.49 5 7 -15 0.89 4.44 -5 7 15 2.27 6.39 5 7 -15 -1.64 4.47 5 7 -16 5.77 6.13 5 7 -16 7.02 6.12 -5 7 16 7.57 6.28 -5 7 16 4.60 4.42 -5 9 1 7.50 3.50 -5 9 1 5.55 3.52 -5 -9 1 3.36 3.50 5 9 -1 2.63 4.88 5 9 -2 101.98 3.75 -5 -9 2 100.58 5.24 -5 9 2 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4 0 -5 1.07 3.27 -4 0 5 0.56 3.19 -4 0 6 22.75 3.59 4 0 -6 22.76 3.62 -4 0 7 0.25 3.13 4 0 -7 9.07 3.43 -4 0 8 513.21 10.49 4 0 -8 478.93 10.46 -4 0 9 0.39 4.90 -4 0 9 0.31 4.23 -4 0 12 101.56 6.52 -4 0 14 85.62 6.87 -4 0 16 240.44 7.18 -4 0 18 17.05 6.12 -4 0 20 0.79 4.76 -4 2 1 37.98 2.72 4 -2 -1 32.43 2.67 -4 -2 1 31.09 2.63 4 2 -1 32.27 3.41 -4 2 2 425.61 5.52 4 -2 -2 444.19 5.63 -4 -2 2 437.28 5.65 4 2 -2 440.93 5.59 -4 2 3 746.03 7.11 -4 -2 3 782.33 7.45 4 2 -3 764.76 7.37 4 -2 -3 761.19 7.23 -4 2 4 575.25 6.36 -4 -2 4 568.95 6.98 4 -2 -4 546.76 6.24 4 2 -4 571.29 6.63 4 -2 -5 515.41 6.57 -4 2 5 527.39 6.14 -4 -2 5 504.48 6.53 4 2 -5 535.87 6.56 -4 2 6 297.29 4.84 -4 -2 6 294.64 5.76 4 2 -6 289.69 5.17 -4 2 7 27.29 2.53 -4 -2 7 28.04 3.46 4 2 -7 29.97 3.40 -4 2 7 27.52 2.60 -4 2 8 125.74 4.20 -4 2 8 121.34 4.27 -4 -2 8 116.56 4.64 4 2 -8 126.40 4.59 -4 2 9 342.19 5.74 -4 -2 9 303.60 6.89 4 2 -9 329.28 6.93 -4 2 9 323.88 5.81 -4 2 10 101.51 4.12 4 2 -10 97.94 5.55 4 2 -10 96.34 5.60 -4 2 10 105.87 4.08 -4 2 11 240.95 5.85 -4 2 11 256.81 5.85 -4 2 12 140.42 5.09 -4 2 12 134.76 5.12 -4 2 13 4.02 3.74 -4 2 13 3.52 3.66 -4 2 14 109.60 7.52 -4 2 14 94.79 6.63 -4 2 15 0.31 3.97 -4 2 16 47.30 5.54 -4 2 17 26.40 5.16 -4 2 18 0.32 3.49 -4 2 19 1.07 4.46 -4 2 20 15.06 4.62 -4 4 1 202.77 3.53 4 4 -1 211.50 3.54 -4 -4 1 198.80 3.50 -4 4 2 1155.19 7.20 4 4 -2 1182.80 7.57 -4 -4 2 1142.59 7.52 -4 4 3 199.70 3.46 -4 -4 3 205.58 3.59 4 4 -3 211.44 3.61 -4 4 4 11.14 2.23 4 4 -4 11.71 2.21 -4 -4 4 11.23 2.28 -4 4 4 10.45 2.30 4 4 -5 26.58 2.32 -4 4 5 26.24 2.39 -4 -4 5 23.89 2.40 -4 4 5 26.21 3.14 -4 4 6 178.44 3.93 4 4 -6 177.32 3.48 -4 -4 6 173.20 4.13 -4 4 6 175.64 3.45 -4 4 7 135.27 3.10 -4 4 7 138.72 3.20 4 4 -7 147.42 3.92 -4 -4 7 138.67 3.38 -4 4 8 2.71 3.28 4 4 -8 1.34 2.59 -4 4 8 3.44 2.69 -4 -4 8 2.22 2.71 -4 4 9 8.46 3.87 -4 4 9 6.88 2.64 4 4 -9 8.09 2.66 -4 4 10 500.07 6.02 -4 4 10 450.86 6.00 4 4 -10 491.12 6.58 -4 4 11 39.22 3.82 4 4 -11 35.08 3.99 -4 4 11 34.33 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6 9 6.70 3.16 -4 6 9 5.60 3.01 -4 6 10 77.37 3.33 4 6 -10 69.89 3.49 4 6 -10 80.26 3.41 -4 6 10 69.35 3.46 4 6 -11 27.05 3.26 -4 6 11 29.02 3.12 4 6 -11 27.53 3.20 -4 6 11 30.31 3.24 -4 6 12 23.47 4.29 4 6 -12 20.64 4.29 4 6 -12 18.94 4.29 -4 6 12 20.06 3.09 -4 6 13 0.73 3.48 4 6 -13 -0.39 3.52 -4 6 13 1.19 3.57 4 6 -13 1.00 4.91 4 6 -14 57.26 5.19 -4 6 14 57.08 3.82 -4 6 14 70.47 5.21 4 6 -14 65.40 5.27 -4 6 15 -0.14 5.65 -4 6 15 3.09 4.07 4 6 -15 4.10 5.56 4 6 -15 2.34 5.53 -4 6 16 1.43 4.43 4 6 -16 -0.60 6.28 -4 6 16 1.31 6.44 4 6 -16 1.59 7.23 -4 6 17 1.49 6.25 -4 6 17 1.60 6.30 -4 8 1 2.84 3.03 -4 8 1 0.81 4.28 -4 -8 1 0.23 4.28 4 8 -1 2.00 2.96 -4 8 2 39.16 4.33 4 8 -2 34.81 4.28 -4 -8 2 34.95 4.38 -4 8 2 35.48 4.42 -4 8 3 14.99 4.37 4 8 -3 15.25 3.02 -4 -8 3 18.20 4.31 -4 8 3 16.73 3.03 4 8 -4 143.22 3.51 -4 8 4 135.27 3.54 -4 8 4 138.33 3.60 -4 8 5 0.39 2.94 4 8 -5 0.49 4.12 -4 8 5 1.27 4.32 4 8 -6 -1.21 2.93 -4 8 6 -0.48 2.94 -4 8 6 0.89 3.04 -4 8 7 122.02 3.43 4 8 -7 129.71 3.51 -4 8 7 123.74 3.60 -4 8 8 34.63 4.93 4 8 -8 34.65 3.56 -4 8 8 31.83 3.80 -4 8 9 2.45 3.42 4 8 -9 4.85 3.57 4 8 -9 3.34 4.79 -4 8 9 4.40 5.13 4 8 -10 7.93 5.03 4 8 -10 9.27 4.72 -4 8 10 6.93 3.49 -4 8 10 7.99 3.60 -4 8 11 34.02 5.65 4 8 -11 34.06 5.84 4 8 -11 33.21 5.63 -4 8 11 29.82 4.21 -4 8 12 82.26 4.39 -4 8 12 86.11 4.22 4 8 -12 71.37 4.40 4 8 -12 81.11 4.27 4 8 -13 3.05 6.38 -4 8 13 0.14 4.58 4 8 -13 -0.13 6.25 -4 8 13 -0.33 6.24 4 8 -14 3.16 6.30 -4 8 14 6.78 6.17 -4 8 14 6.29 4.47 4 8 -14 5.39 6.22 -4 10 1 34.27 4.09 4 10 -1 34.86 4.01 -4 10 1 33.64 4.09 -4 10 2 9.83 5.58 4 10 -2 6.12 5.50 -4 10 2 4.28 3.93 4 10 -3 12.70 3.84 -4 10 3 10.79 5.57 -4 10 3 12.13 3.92 -4 10 4 23.44 5.63 4 10 -4 20.59 3.95 -4 10 4 33.34 5.69 -4 10 5 0.00 3.87 4 10 -5 -2.72 5.41 -4 10 5 3.28 3.97 -4 10 6 -3.07 3.84 4 10 -6 1.92 3.93 4 10 -6 -0.07 3.81 -4 10 6 1.01 4.00 -4 10 7 1.85 6.16 4 10 -7 5.57 4.48 4 10 -7 0.29 4.30 -4 10 7 4.57 6.04 -4 10 8 52.78 4.51 4 10 -8 54.04 6.46 4 10 -8 58.87 4.43 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384.68 5.39 -3 3 3 279.86 4.82 3 3 -3 278.41 4.32 -3 -3 3 276.93 4.43 -3 3 4 651.39 6.17 -3 -3 4 640.93 6.44 -3 3 4 661.75 6.50 3 3 -4 669.17 6.42 -3 3 5 46.70 3.46 -3 3 5 45.00 2.62 -3 -3 5 42.49 2.71 3 3 -5 44.84 2.65 -3 -3 6 2.87 3.13 -3 3 6 4.20 3.01 3 3 -6 3.08 3.02 -3 3 6 2.44 2.26 -3 3 7 22.89 2.35 3 3 -7 22.87 2.41 -3 3 7 21.93 2.42 -3 -3 7 22.00 2.52 -3 3 8 105.58 3.90 3 3 -8 110.84 4.03 -3 3 8 112.45 3.84 -3 3 9 3.07 2.08 -3 3 9 3.00 3.04 3 3 -9 3.44 2.95 3 3 -9 2.70 3.06 -3 3 10 150.51 4.68 3 3 -10 132.93 5.23 3 3 -10 149.22 5.17 -3 3 10 144.68 4.74 3 3 -11 108.16 5.23 -3 3 11 125.79 4.59 -3 3 11 118.94 4.62 3 3 -11 123.67 5.28 -3 3 12 86.77 4.33 3 3 -12 81.09 6.70 -3 3 12 83.07 4.38 3 3 -12 74.82 6.10 -3 3 13 2.48 4.32 -3 3 13 0.40 4.47 -3 3 14 11.30 4.37 -3 3 14 9.81 4.47 -3 3 15 26.87 4.55 -3 3 15 27.60 5.39 -3 3 16 18.11 6.40 -3 3 16 19.91 6.24 -3 3 17 0.19 5.37 -3 3 18 14.00 4.45 -3 3 19 10.36 4.42 3 5 -1 10.52 2.14 -3 5 1 7.44 3.05 -3 -5 1 10.34 2.99 -3 5 1 10.21 2.20 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16 40.58 4.20 -3 5 16 37.19 4.34 -3 5 17 2.17 6.35 -3 5 17 1.51 6.39 -3 5 18 2.63 6.98 -3 5 18 2.54 6.96 3 7 -1 275.12 3.69 -3 7 1 271.18 3.76 -3 -7 1 279.59 4.57 -3 7 1 273.72 3.78 -3 7 2 22.34 2.71 3 7 -2 18.95 2.64 -3 7 2 21.08 2.63 -3 -7 2 23.54 2.68 -3 7 3 38.01 3.76 3 7 -3 42.55 2.75 -3 -7 3 39.16 2.77 -3 7 3 39.30 2.79 3 7 -4 7.20 2.52 -3 7 4 7.73 2.52 -3 7 4 7.56 2.58 3 7 -5 4.19 3.53 -3 7 5 6.54 3.65 -3 7 5 6.54 2.52 -3 7 6 39.16 3.14 -3 7 6 36.24 4.14 3 7 -6 34.39 3.15 -3 7 7 137.21 3.61 -3 7 7 139.49 3.66 3 7 -7 148.30 3.63 -3 7 8 38.83 3.15 -3 7 8 34.20 3.34 3 7 -8 36.44 4.29 -3 7 9 189.07 3.76 3 7 -9 188.18 3.86 -3 7 9 179.46 3.88 3 7 -9 174.71 5.07 -3 7 10 2.61 2.93 3 7 -10 2.06 2.88 3 7 -10 1.82 4.26 -3 7 10 3.26 3.03 -3 7 11 30.73 3.74 3 7 -11 32.01 3.70 -3 7 11 38.58 4.97 3 7 -11 36.69 3.61 3 7 -12 5.44 4.95 -3 7 12 10.21 3.42 3 7 -12 5.71 3.44 -3 7 12 9.36 3.57 -3 7 13 14.22 4.02 3 7 -13 10.60 5.71 3 7 -13 13.40 4.02 -3 7 13 13.13 5.80 -3 7 14 24.65 5.69 3 7 -14 23.33 5.63 -3 7 14 26.54 5.77 3 7 -14 26.11 5.67 -3 7 15 2.62 4.48 3 7 -15 -1.15 6.30 -3 7 15 4.30 4.48 3 7 -15 2.32 6.17 3 9 -1 6.15 3.42 -3 9 1 2.44 3.52 -3 9 1 1.39 3.51 3 9 -2 247.87 4.30 -3 9 2 304.40 5.69 -3 9 2 300.81 4.46 3 9 -3 17.11 3.47 -3 9 3 12.53 3.59 -3 9 3 16.02 3.48 3 9 -4 5.12 3.39 -3 9 4 -0.93 4.86 -3 9 4 0.78 3.53 -3 9 5 102.15 3.81 3 9 -5 103.20 5.06 -3 9 5 92.62 3.89 -3 9 6 133.55 3.92 3 9 -6 122.26 4.00 3 9 -6 138.96 3.90 -3 9 6 137.23 4.07 3 9 -7 -1.04 3.33 3 9 -7 -1.61 4.97 -3 9 7 -1.58 4.98 -3 9 7 4.01 4.73 -3 9 8 -1.61 3.89 3 9 -8 3.17 3.88 3 9 -8 1.01 4.06 -3 9 8 -3.68 5.82 -3 9 9 11.01 4.14 3 9 -9 12.54 4.10 3 9 -9 11.64 5.48 -3 9 9 12.31 3.91 -3 9 10 79.19 4.37 -3 9 10 76.43 4.10 3 9 -10 82.44 4.16 3 9 -10 71.49 4.30 -3 9 11 -0.96 4.57 -3 9 11 2.89 4.37 3 9 -11 3.24 4.53 3 9 -11 7.86 6.09 -3 9 12 6.92 4.38 -3 9 12 5.52 6.37 3 9 -12 8.66 4.33 3 9 -12 8.07 4.52 3 11 -1 13.83 4.32 3 11 -1 16.72 4.38 -3 11 1 15.74 4.42 -3 11 1 12.56 6.17 -3 11 2 40.45 6.24 3 11 -2 41.41 6.18 -3 11 2 41.59 4.54 3 11 -2 40.10 4.51 -3 11 3 18.70 4.34 3 11 -3 14.63 4.36 3 11 -3 20.33 6.02 -3 11 3 19.94 4.38 3 11 -4 5.13 6.41 -3 11 4 -0.78 4.86 3 11 -4 0.28 6.59 -3 11 4 -0.06 4.36 -2 0 2 1.18 1.96 2 0 -2 1.16 2.74 -2 0 3 0.12 2.56 2 0 -3 0.24 2.60 -2 0 4 4146.28 8.42 2 0 -5 0.55 4.12 -2 0 5 0.04 3.93 -2 0 6 31.32 5.21 -2 0 8 206.09 6.53 -2 0 12 299.26 7.03 -2 0 14 54.36 5.72 -2 0 16 17.34 3.97 -2 0 18 1.08 3.51 2 2 -1 301.64 5.38 -2 2 1 286.24 5.00 -2 -2 1 289.12 5.43 -2 -2 2 742.42 7.94 2 2 -2 743.84 7.88 -2 2 2 708.13 7.84 2 2 -3 6.40 1.98 -2 2 3 6.42 1.98 -2 2 3 6.63 2.63 -2 -2 3 7.58 1.93 -2 2 4 43.24 3.59 2 2 -4 41.51 3.62 -2 2 4 37.91 2.78 -2 -2 4 38.39 3.70 2 2 -5 228.83 4.97 -2 2 5 233.96 4.59 -2 2 5 219.85 4.55 -2 -2 5 221.19 5.12 -2 2 6 32.90 3.51 2 2 -6 31.91 2.77 -2 -2 6 12.10 2.48 -2 2 6 32.21 3.44 -2 2 7 120.20 3.59 2 2 -7 117.70 4.70 -2 2 7 110.71 3.58 2 2 -7 112.66 4.77 2 2 -8 210.18 6.69 -2 2 8 218.84 4.46 2 2 -8 226.04 6.18 -2 2 8 218.69 5.05 -2 2 9 75.82 3.90 -2 2 9 78.23 3.20 2 2 -9 78.62 5.27 2 2 -9 77.36 5.42 -2 2 10 377.39 6.03 -2 2 10 369.50 6.68 -2 2 11 125.00 4.95 -2 2 11 130.98 5.03 -2 2 12 20.91 3.94 -2 2 12 21.02 3.96 -2 2 13 45.52 5.02 -2 2 13 44.59 5.07 -2 2 14 1.39 6.89 -2 2 14 1.29 6.09 -2 2 15 6.40 5.42 -2 2 16 40.10 6.41 -2 2 17 9.43 5.53 -2 2 18 17.79 4.97 -2 2 19 30.25 5.36 -2 4 1 28.37 2.40 -2 -4 1 27.18 2.40 2 4 -1 26.00 2.37 -2 4 1 25.53 3.26 -2 4 2 594.30 5.80 -2 -4 2 575.06 5.44 -2 4 2 589.08 5.37 2 4 -2 594.16 5.44 -2 4 3 0.30 2.15 2 4 -3 0.25 2.12 -2 -4 3 0.26 3.08 -2 -4 4 2.78 2.19 -2 4 4 2.14 2.17 2 4 -4 3.09 2.11 -2 4 5 6.31 2.23 -2 -4 5 5.78 3.10 2 4 -5 5.31 2.99 -2 4 6 353.00 4.94 2 4 -6 361.29 5.11 -2 4 7 4.87 3.06 2 4 -7 4.33 2.93 2 4 -8 217.00 4.23 -2 4 8 217.67 4.78 2 4 -8 200.30 5.08 -2 4 8 204.38 4.84 2 4 -9 39.53 2.98 -2 4 9 39.41 2.90 2 4 -9 37.07 4.09 -2 4 9 37.18 2.96 -2 4 10 350.79 4.83 -2 4 10 388.17 4.86 2 4 -10 397.49 6.26 2 4 -10 342.55 6.15 2 4 -11 30.65 3.94 -2 4 11 35.06 3.80 2 4 -11 34.00 3.90 -2 4 11 32.86 3.88 2 4 -12 0.62 4.28 -2 4 12 2.43 4.25 -2 4 12 0.32 4.38 2 4 -12 0.59 4.31 -2 4 13 3.93 4.38 -2 4 13 2.46 3.02 2 4 -13 2.10 4.26 2 4 -13 2.74 5.24 -2 4 14 146.27 5.21 -2 4 14 137.42 5.17 -2 4 15 20.33 5.11 -2 4 15 17.54 5.15 -2 4 16 1.05 5.67 -2 4 16 2.00 5.69 -2 4 17 14.36 5.67 -2 4 17 13.62 6.98 -2 4 18 58.26 9.40 -2 4 18 59.22 9.43 -2 6 1 4.10 2.66 -2 6 1 8.63 3.73 -2 -6 1 4.69 2.64 2 6 -1 6.27 2.61 -2 6 2 417.74 4.44 -2 6 2 418.02 4.38 -2 -6 2 414.66 4.48 2 6 -2 413.48 5.10 -2 6 3 15.21 3.70 -2 -6 3 10.80 2.73 -2 6 3 14.56 2.71 2 6 -3 12.56 2.66 -2 6 4 37.08 2.81 -2 6 4 36.01 2.76 2 6 -4 36.53 2.77 -2 6 5 0.43 2.53 -2 6 5 0.80 2.62 2 6 -5 2.20 3.57 -2 6 6 142.46 3.37 -2 6 6 145.94 3.29 2 6 -6 152.73 4.21 -2 6 7 58.40 2.87 -2 6 7 57.30 2.96 2 6 -7 61.71 3.82 2 6 -8 19.99 2.60 -2 6 8 20.98 3.64 -2 6 8 19.17 2.72 2 6 -8 16.73 3.79 -2 6 9 -1.46 3.04 2 6 -9 0.90 2.96 2 6 -9 1.52 3.11 -2 6 9 1.64 3.10 -2 6 10 41.83 4.49 2 6 -10 42.16 3.20 -2 6 10 41.10 3.19 2 6 -10 35.06 3.33 -2 6 11 27.70 3.09 2 6 -11 22.89 4.38 -2 6 11 21.57 3.17 2 6 -11 26.01 3.14 2 6 -12 3.71 3.54 -2 6 12 2.31 5.11 2 6 -12 4.85 4.95 -2 6 12 2.96 3.55 2 6 -13 0.46 4.92 -2 6 13 0.82 4.88 -2 6 13 -0.31 3.59 2 6 -13 -1.51 4.96 -2 6 14 72.32 5.96 -2 6 14 64.53 6.05 2 6 -14 63.14 6.03 2 6 -14 57.53 5.89 -2 6 15 48.24 5.81 -2 6 15 38.93 5.89 2 6 -15 36.82 5.74 2 6 -15 41.36 5.80 -2 6 16 10.83 6.40 2 6 -16 8.93 7.59 2 6 -16 7.46 7.77 -2 6 16 13.04 6.43 2 8 -1 18.33 3.00 -2 8 1 11.95 3.06 -2 8 1 16.36 3.06 2 8 -2 22.72 3.02 -2 8 2 18.99 4.34 -2 8 2 23.37 3.06 2 8 -3 3.42 2.96 -2 8 3 2.44 3.05 -2 8 3 4.49 2.98 2 8 -4 108.34 3.38 -2 8 4 104.90 3.40 -2 8 4 104.00 3.47 2 8 -5 104.31 3.38 -2 8 5 102.83 3.35 -2 8 5 95.97 3.43 2 8 -6 7.94 2.94 -2 8 6 7.38 2.94 2 8 -6 7.04 3.01 -2 8 6 7.22 4.30 2 8 -7 11.47 2.93 2 8 -7 11.43 3.06 -2 8 7 14.24 4.08 -2 8 7 14.28 4.28 2 8 -8 91.42 3.97 2 8 -8 100.72 3.79 -2 8 8 101.34 3.78 -2 8 8 94.53 3.92 2 8 -9 3.41 4.72 2 8 -9 2.99 3.57 -2 8 9 2.95 3.39 -2 8 9 3.32 3.54 -2 8 10 -4.18 3.54 -2 8 10 3.08 3.39 2 8 -10 0.34 3.50 2 8 -10 -0.19 4.70 2 8 -11 7.06 4.11 -2 8 11 12.30 5.58 -2 8 11 10.15 4.11 2 8 -11 12.02 3.93 2 8 -12 33.76 4.17 -2 8 12 39.66 4.20 -2 8 12 40.85 4.09 2 8 -12 47.86 5.63 2 8 -13 0.45 4.48 -2 8 13 2.21 6.38 2 8 -13 0.90 4.41 -2 8 13 4.00 4.38 -2 8 14 9.26 5.02 2 8 -14 10.21 6.99 -2 8 14 10.67 5.06 2 8 -14 9.56 7.05 2 10 -1 13.40 5.54 -2 10 1 10.91 5.60 -2 10 1 9.31 4.01 2 10 -2 -2.79 3.93 2 10 -2 -1.35 5.59 -2 10 2 0.86 3.96 -2 10 2 1.66 3.95 2 10 -3 -2.14 5.68 2 10 -3 2.25 3.95 -2 10 3 2.73 3.95 -2 10 3 5.30 3.96 -2 10 4 49.75 5.60 2 10 -4 42.56 4.12 2 10 -4 51.22 5.58 -2 10 4 37.83 4.13 2 10 -5 8.14 3.90 -2 10 5 15.38 5.44 2 10 -5 8.46 4.00 -2 10 5 12.24 5.65 -2 10 6 1.56 3.96 -2 10 6 -3.75 5.47 2 10 -6 1.01 3.81 2 10 -6 -1.27 3.97 -2 10 7 0.69 4.41 -2 10 7 2.79 4.59 2 10 -7 5.99 4.52 2 10 -7 3.67 4.31 -2 10 8 40.34 6.49 2 10 -8 34.81 6.46 2 10 -8 34.39 4.44 -2 10 8 44.92 6.14 2 10 -9 28.22 4.58 -2 10 9 36.77 6.40 2 10 -9 31.17 6.12 -2 10 9 28.58 4.36 1 1 -1 223.10 6.07 -1 1 1 214.91 5.88 -1 -1 1 215.32 6.07 -1 1 2 50.71 3.24 -1 -1 2 52.41 3.51 1 1 -2 54.54 3.50 -1 1 3 111.60 4.72 -1 -1 3 104.36 4.83 1 1 -3 112.44 4.92 -1 1 4 109.16 4.63 1 1 -4 113.30 5.52 -1 1 6 1433.76 14.01 -1 1 7 30.36 3.65 -1 1 8 1.83 3.05 -1 1 8 1.92 3.70 -1 1 9 17.74 3.99 -1 1 9 18.20 3.40 -1 1 10 468.23 9.85 -1 1 10 453.36 9.69 -1 1 11 1.61 5.88 -1 1 11 1.67 5.93 -1 1 12 0.45 5.45 -1 1 13 58.96 5.45 -1 1 14 148.58 7.39 -1 1 15 1.40 5.41 -1 1 16 2.25 5.96 -1 1 17 6.24 5.92 -1 1 18 18.32 6.66 -1 1 19 18.30 6.45 -1 -3 1 249.97 4.35 -1 3 1 251.66 4.28 1 3 -1 256.27 4.27 1 3 -2 12.33 2.33 -1 3 2 12.66 2.35 -1 -3 2 11.39 2.39 1 3 -3 72.39 2.95 -1 -3 3 70.61 3.73 -1 3 3 68.68 2.86 -1 3 4 1001.29 7.70 1 3 -4 1007.77 8.18 -1 3 5 454.25 5.82 1 3 -5 453.67 5.77 1 3 -6 100.16 4.03 1 3 -6 106.45 3.94 -1 3 6 99.45 3.16 1 3 -7 47.87 3.64 1 3 -7 52.38 2.83 -1 3 7 47.99 2.67 1 3 -8 41.37 3.56 1 3 -8 45.16 3.49 -1 3 8 46.58 3.43 1 3 -9 48.49 4.13 1 3 -9 43.54 4.27 -1 3 9 43.77 4.07 1 3 -10 5.90 3.72 -1 3 10 5.28 3.78 1 3 -10 5.38 3.83 -1 3 11 113.48 4.48 1 3 -11 112.11 5.83 -1 3 11 108.51 4.52 1 3 -11 96.49 5.10 1 3 -12 174.41 9.32 -1 3 12 191.15 5.00 1 3 -12 160.87 9.27 -1 3 12 179.07 5.01 -1 3 13 23.90 4.43 -1 3 13 21.43 4.53 -1 3 14 42.25 3.53 -1 3 14 47.94 4.69 -1 3 15 2.46 6.20 -1 3 15 2.55 4.99 -1 3 16 21.48 6.37 -1 3 16 21.74 6.27 -1 3 17 0.08 5.60 -1 3 18 11.26 5.37 -1 -5 1 5.20 2.16 -1 5 1 5.72 2.16 1 5 -1 4.46 2.12 -1 5 2 28.86 2.32 -1 -5 2 26.18 2.35 1 5 -2 26.16 3.14 -1 5 3 141.73 3.08 1 5 -3 142.71 3.08 -1 5 4 263.19 3.68 1 5 -4 262.12 3.77 -1 5 5 74.94 2.66 1 5 -5 81.57 3.38 1 5 -6 81.19 4.05 -1 5 6 76.89 3.10 1 5 -6 76.27 4.18 1 5 -7 0.79 2.57 -1 5 7 3.06 2.62 1 5 -7 0.60 2.67 -1 5 8 229.13 4.74 1 5 -8 238.88 4.04 1 5 -8 211.26 4.05 -1 5 9 16.42 2.75 1 5 -9 18.54 3.81 1 5 -9 19.86 3.65 1 5 -10 6.68 3.56 1 5 -10 7.06 2.64 -1 5 10 7.24 3.68 1 5 -11 3.63 3.09 1 5 -11 4.53 4.26 -1 5 11 4.89 3.11 -1 5 11 6.03 3.03 -1 5 12 138.84 4.88 1 5 -12 135.20 5.21 -1 5 12 127.01 4.93 1 5 -12 113.63 5.06 -1 5 13 17.44 5.10 1 5 -13 16.09 5.12 -1 5 13 14.59 5.20 1 5 -13 13.08 5.04 -1 5 14 33.74 5.12 1 5 -14 29.41 5.21 1 5 -14 26.34 5.09 -1 5 14 28.79 5.20 1 5 -15 6.79 8.78 -1 5 15 6.90 5.78 1 5 -15 5.47 7.96 -1 5 15 7.51 5.77 -1 5 16 9.81 5.67 -1 5 16 6.99 5.71 -1 5 17 21.09 6.38 -1 5 17 16.40 4.45 -1 7 1 4.59 2.57 1 7 -1 4.10 2.57 -1 7 2 142.75 3.23 1 7 -2 153.12 4.15 -1 7 3 8.52 2.62 1 7 -3 12.07 3.58 -1 7 4 115.39 3.13 1 7 -4 120.73 4.01 1 7 -5 229.32 4.55 -1 7 5 235.79 3.68 1 7 -5 237.07 3.65 1 7 -6 9.63 4.40 -1 7 6 6.35 3.11 1 7 -6 8.41 3.01 1 7 -7 180.78 5.05 1 7 -7 190.17 3.82 -1 7 7 188.62 4.97 -1 7 8 68.78 3.37 1 7 -8 65.95 3.27 1 7 -8 64.41 3.44 1 7 -9 15.25 2.98 1 7 -9 12.44 3.15 -1 7 9 14.56 3.11 -1 7 9 16.33 4.22 1 7 -10 59.96 5.08 1 7 -10 54.08 5.23 -1 7 10 54.37 3.83 -1 7 10 58.40 3.75 1 7 -11 -2.38 5.03 -1 7 11 2.59 4.87 1 7 -11 2.05 3.44 -1 7 11 3.39 3.53 1 7 -12 18.00 3.48 1 7 -12 19.68 4.89 -1 7 12 18.46 3.57 -1 7 12 19.36 4.91 1 7 -13 35.93 5.76 -1 7 13 31.28 4.18 -1 7 13 38.23 4.12 1 7 -13 31.83 5.73 1 7 -14 26.32 6.45 -1 7 14 27.29 4.61 -1 7 14 29.61 6.36 1 7 -14 21.23 6.34 -1 7 15 28.58 6.36 1 7 -15 20.79 4.54 -1 7 15 28.27 6.35 1 7 -15 21.66 6.25 1 9 -1 62.67 3.69 -1 9 1 57.80 3.73 -1 9 1 58.79 5.13 -1 9 2 104.60 5.16 1 9 -2 107.10 5.25 -1 9 2 99.98 3.85 1 9 -2 104.43 5.20 -1 9 3 -0.97 3.48 1 9 -3 -2.39 3.58 -1 9 3 -0.18 3.51 1 9 -3 0.71 4.91 1 9 -4 12.27 3.44 1 9 -4 9.35 4.97 -1 9 4 13.83 3.45 -1 9 4 8.30 4.97 1 9 -5 14.84 3.45 -1 9 5 17.24 3.43 1 9 -5 14.68 5.00 -1 9 5 17.49 3.53 -1 9 6 93.81 5.24 1 9 -6 84.71 3.86 1 9 -6 95.43 3.69 -1 9 6 91.38 3.74 1 9 -7 -2.43 3.40 -1 9 7 -2.50 4.98 1 9 -7 -1.20 3.52 -1 9 7 4.83 4.70 1 9 -8 0.64 3.91 -1 9 8 4.00 5.78 -1 9 8 4.04 3.88 1 9 -8 1.96 4.04 1 9 -9 46.99 5.60 -1 9 9 47.13 4.02 -1 9 9 43.83 4.21 1 9 -9 45.66 4.22 -1 9 10 39.77 4.53 -1 9 10 44.21 4.74 1 9 -10 37.71 6.18 1 9 -10 42.60 4.47 1 9 -11 1.71 6.36 -1 9 11 1.12 4.48 1 9 -11 -2.01 6.12 -1 9 11 3.75 6.13 -1 11 1 32.58 4.44 1 11 -1 32.47 4.43 -1 11 1 36.84 6.21 1 11 -1 34.65 6.23 -1 11 2 11.07 6.20 1 11 -2 12.47 4.33 1 11 -2 11.59 6.23 -1 11 2 9.69 4.38 -1 11 3 42.22 4.52 -1 11 3 44.68 6.15 1 11 -3 38.06 4.42 1 11 -3 38.58 4.51 -1 11 4 -2.86 4.43 1 11 -4 -0.67 4.26 1 11 -4 0.96 4.37 -1 11 4 -3.20 6.49 0 0 2 16.62 4.35 0 0 4 21.65 5.08 0 0 5 0.43 3.94 0 0 -5 1.08 3.86 0 0 -6 5.78 3.94 0 0 6 5.23 4.00 0 0 -7 0.26 4.25 0 0 7 1.34 4.34 0 0 8 1271.74 8.35 0 0 12 12.54 5.22 0 0 14 0.14 4.35 0 0 16 92.49 6.84 0 0 18 0.91 5.24 0 -2 0 30.65 2.98 0 2 0 29.89 2.39 0 2 1 154.63 4.34 0 -2 1 156.38 4.07 0 2 -1 154.68 4.03 0 -2 -1 167.88 4.45 0 2 -2 20.78 2.27 0 -2 -2 22.51 2.24 0 2 2 20.06 2.20 0 2 -3 5.83 2.36 0 -2 -3 6.87 2.40 0 2 3 6.35 3.28 0 2 -4 695.68 8.65 0 2 -4 747.31 8.52 0 -2 -4 742.00 7.97 0 2 4 700.42 7.85 0 2 5 453.65 6.45 0 2 -5 462.78 7.43 0 -2 -5 486.32 6.61 0 2 -5 494.90 7.45 0 2 -6 142.82 5.00 0 2 -6 147.96 4.84 0 -2 -6 148.07 3.80 0 2 6 142.69 4.39 0 2 7 286.48 4.94 0 -2 -7 296.50 4.97 0 2 -7 302.68 6.38 0 2 -7 283.06 6.47 0 2 -8 94.67 4.96 0 2 8 86.78 3.28 0 2 -8 91.15 5.10 0 -2 -8 92.85 3.27 0 2 -9 136.09 5.49 0 2 -9 155.18 6.02 0 -2 -9 152.32 4.44 0 2 9 145.83 4.41 0 2 -10 1.11 5.19 0 2 -10 1.01 4.60 0 2 10 1.59 3.72 0 2 11 3.79 3.73 0 2 12 52.40 4.93 0 2 12 49.72 4.23 0 2 13 8.20 4.41 0 2 13 7.26 5.45 0 2 14 36.40 5.78 0 2 14 35.43 5.83 0 2 15 42.94 5.92 0 2 16 8.81 3.41 0 2 17 2.19 3.36 0 2 18 8.72 3.63 0 4 0 592.07 5.44 0 -4 0 588.32 5.49 0 4 -1 27.90 2.39 0 4 1 28.64 2.41 0 -4 -1 25.68 3.25 0 4 -2 390.02 4.61 0 4 2 364.10 4.42 0 -4 -2 370.40 4.44 0 4 -3 2.83 3.07 0 4 3 3.75 2.17 0 -4 -3 3.50 3.06 0 4 -4 14.57 2.29 0 4 4 17.01 3.17 0 -4 -4 15.82 3.12 0 4 -5 282.44 4.70 0 4 -5 257.37 4.17 0 -4 -5 280.02 3.94 0 4 5 265.27 4.51 0 4 -6 466.89 5.65 0 4 -6 421.05 5.18 0 -4 -6 474.25 5.33 0 4 6 428.41 4.78 0 4 7 -0.27 2.14 0 4 -7 -0.07 2.17 0 4 -7 -0.28 2.89 0 -4 -7 0.55 2.93 0 4 -8 28.55 3.98 0 4 8 27.20 2.86 0 -4 -8 30.27 2.81 0 4 -8 29.83 2.85 0 4 -9 1.50 3.76 0 4 9 1.56 2.66 0 4 -9 1.31 2.53 0 4 10 35.18 3.93 0 4 -10 35.26 3.90 0 4 -10 33.36 3.97 0 4 -11 1.03 3.62 0 4 11 1.34 2.60 0 4 -11 0.87 3.53 0 4 -12 3.89 4.28 0 4 -12 2.82 4.24 0 4 12 3.30 4.36 0 4 13 108.71 4.94 0 4 -13 100.70 5.48 0 4 -13 87.90 5.32 0 4 13 98.24 4.93 0 4 14 171.10 6.07 0 4 14 187.80 6.13 0 4 15 8.22 5.11 0 4 15 12.36 5.03 0 4 16 7.97 5.74 0 4 16 9.29 5.70 0 4 17 -0.58 6.34 0 4 17 1.33 6.26 0 6 0 -0.41 2.60 0 6 -1 94.10 3.11 0 6 1 90.90 3.05 0 6 -2 619.54 5.77 0 6 2 599.54 5.04 0 6 -3 6.25 2.64 0 6 3 4.57 2.68 0 6 -4 1.20 2.61 0 6 -4 1.96 3.61 0 6 4 2.02 2.63 0 6 -5 82.93 3.12 0 6 -5 91.11 3.02 0 6 5 85.67 3.09 0 6 -6 32.53 3.91 0 6 -6 34.01 2.72 0 6 6 33.24 3.84 0 6 7 153.14 3.44 0 6 -7 146.95 4.40 0 6 -7 152.01 3.41 0 6 -8 33.53 3.87 0 6 8 31.21 2.79 0 6 -8 33.90 3.70 0 6 9 91.69 4.71 0 6 -9 84.90 4.79 0 6 -9 93.13 3.51 0 6 -10 77.08 4.68 0 6 10 76.60 3.47 0 6 -10 84.00 4.58 0 6 11 29.94 4.41 0 6 -11 27.06 4.37 0 6 -11 32.62 4.27 0 6 -12 70.24 5.26 0 6 12 76.84 5.22 0 6 12 63.56 3.83 0 6 -12 62.11 5.21 0 6 13 2.34 4.92 0 6 -13 0.38 4.87 0 6 13 1.26 3.54 0 6 -13 -0.11 4.83 0 6 14 41.45 5.78 0 6 -14 33.40 5.79 0 6 -14 30.09 5.67 0 6 14 30.77 4.17 0 6 15 1.34 4.50 0 6 -15 0.61 6.20 0 6 -15 0.09 7.64 0 6 15 0.25 4.54 0 6 16 0.94 6.30 0 6 -16 0.29 9.53 0 6 16 -0.20 4.45 0 6 -16 0.92 9.72 0 8 0 165.20 3.67 0 8 -1 106.47 3.44 0 8 -1 110.02 3.42 0 8 1 110.23 3.47 0 8 -2 7.95 4.33 0 8 -2 11.83 4.22 0 8 2 9.67 3.04 0 8 -3 34.39 3.19 0 8 -3 32.71 3.13 0 8 3 33.13 3.18 0 8 -4 74.04 3.34 0 8 -4 78.13 4.40 0 8 4 73.99 3.32 0 8 5 27.75 4.34 0 8 -5 24.71 3.14 0 8 -5 26.99 3.08 0 8 6 17.41 3.14 0 8 -6 20.61 3.06 0 8 -6 22.60 4.16 0 8 7 53.73 5.20 0 8 -7 45.22 3.82 0 8 -7 51.39 4.99 0 8 8 55.14 5.21 0 8 -8 55.56 3.83 0 8 -8 56.01 3.60 0 8 9 14.28 3.45 0 8 -9 16.18 5.02 0 8 9 17.73 3.59 0 8 -9 16.60 3.41 0 8 -10 5.27 3.88 0 8 -10 1.71 5.80 0 8 10 5.90 3.91 0 8 10 3.42 4.10 0 8 -11 1.68 3.98 0 8 -11 0.20 5.45 0 8 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5.14 14 4 1 201.92 3.82 -14 -4 -1 227.39 4.92 -14 4 -1 216.81 5.12 14 -4 2 395.26 4.62 14 4 2 386.45 4.48 -14 -4 -2 389.15 4.38 -14 4 -2 377.51 4.58 14 -4 3 -1.91 3.05 -14 -4 -3 5.36 2.93 14 4 3 4.97 4.23 -14 4 -3 0.61 3.08 14 -4 4 1.01 3.53 -14 -4 -4 -1.77 3.48 14 4 4 -0.73 3.51 -14 4 -4 -2.61 3.63 14 -4 5 7.79 4.93 -14 -4 -5 11.16 4.87 14 4 5 5.83 3.53 -14 4 -5 4.88 3.55 14 -4 6 42.80 3.63 -14 -4 -6 40.82 3.59 -14 4 -6 32.95 3.68 14 4 6 39.31 3.60 -14 -4 -7 0.63 3.95 14 -4 7 1.59 3.97 -14 4 -7 -1.90 4.02 14 4 7 -0.68 5.67 -14 -4 -8 -3.43 5.93 14 -4 8 1.81 4.43 -14 4 -8 0.12 5.95 14 4 8 0.38 4.59 14 -4 9 24.33 6.38 -14 4 -9 27.50 6.22 14 4 9 25.32 4.61 -14 -4 -9 25.84 6.32 -14 -6 0 -1.15 3.44 14 6 0 2.43 3.45 14 -6 0 2.34 3.50 -14 6 0 1.84 3.53 14 6 1 50.11 3.60 14 -6 1 42.71 3.68 -14 6 -1 42.49 3.74 -14 -6 -1 45.69 4.97 14 6 2 27.53 3.51 14 -6 2 24.26 3.50 -14 6 -2 23.89 3.65 -14 -6 -2 22.69 3.48 14 6 3 34.33 5.00 14 -6 3 40.25 4.88 -14 6 -3 27.74 5.10 -14 -6 -3 35.05 4.82 14 -6 4 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236.93 5.71 -15 -1 -6 217.77 4.36 15 -1 6 230.12 4.51 -15 1 -7 0.69 4.00 -15 -1 -7 1.76 4.01 15 1 7 2.89 5.36 15 -1 7 -1.74 5.35 -15 -1 -8 3.87 5.61 15 1 8 3.87 4.05 15 -1 8 6.92 4.02 -15 1 -8 6.84 5.60 15 -1 9 27.76 4.66 -15 -1 -9 28.75 4.53 15 1 9 30.01 4.67 -15 1 -9 30.34 6.35 15 -1 10 63.14 5.34 -15 -1 -10 65.55 7.16 -15 1 -10 63.56 7.15 15 -3 0 29.55 3.12 15 3 0 28.80 4.28 -15 3 0 23.95 4.42 -15 -3 0 25.94 3.06 15 -3 1 10.89 3.11 15 3 1 16.42 4.26 -15 3 -1 9.20 3.13 -15 -3 -1 12.22 3.05 15 -3 2 1.80 3.02 -15 3 -2 0.11 3.02 15 3 2 2.16 2.99 -15 -3 -2 -1.02 4.20 15 -3 3 18.26 3.02 -15 3 -3 17.88 4.28 15 3 3 15.36 2.99 -15 -3 -3 14.40 3.04 15 -3 4 80.45 3.87 -15 3 -4 74.24 3.85 15 3 4 77.08 3.87 -15 -3 -4 83.62 3.74 15 -3 5 60.68 5.20 -15 3 -5 60.46 3.77 -15 -3 -5 60.46 3.70 15 3 5 64.88 3.73 15 -3 6 7.58 5.37 -15 3 -6 5.37 5.34 -15 -3 -6 8.27 3.47 15 3 6 10.81 4.10 15 -3 7 3.67 5.68 -15 3 -7 5.04 5.65 -15 -3 -7 6.34 5.59 15 3 7 6.27 5.69 15 -3 8 13.84 4.55 -15 3 -8 12.83 6.33 -15 -3 -8 19.06 6.31 15 3 8 17.56 4.56 15 -3 9 11.84 6.30 -15 3 -9 12.86 6.17 -15 -3 -9 19.18 6.21 15 3 9 10.22 6.39 15 -5 0 274.89 5.10 -15 -5 0 273.41 4.95 15 5 0 273.58 3.99 -15 5 0 257.09 5.08 15 -5 1 5.39 3.58 -15 -5 -1 6.30 4.86 15 5 1 9.68 3.50 -15 5 -1 7.54 5.06 15 -5 2 5.42 4.98 -15 -5 -2 2.30 4.86 15 5 2 5.05 3.52 -15 5 -2 5.88 3.57 -15 -5 -3 2.34 3.40 15 -5 3 5.37 3.51 15 5 3 3.72 4.93 -15 5 -3 3.68 3.57 -15 -5 -4 157.63 4.42 15 -5 4 149.28 4.56 15 5 4 163.47 4.58 -15 5 -4 163.99 4.70 -15 -5 -5 15.50 4.02 15 -5 5 24.25 5.61 15 5 5 15.50 4.08 -15 5 -5 16.54 4.14 -15 -5 -6 0.68 4.42 15 -5 6 -0.63 4.51 15 5 6 -3.98 4.59 -15 5 -6 0.52 4.51 15 -5 7 -1.32 4.41 -15 5 -7 1.13 4.40 15 5 7 7.76 6.25 -15 -5 -7 1.24 4.37 15 7 0 8.89 4.03 15 -7 0 15.18 4.04 -15 7 0 13.04 5.75 -15 -7 0 15.15 3.91 15 7 1 30.73 4.05 15 -7 1 35.52 4.10 -15 -7 -1 31.28 3.97 -15 7 -1 31.97 4.11 15 7 2 17.54 5.56 -15 -7 -2 19.57 3.89 -15 7 -2 19.01 5.72 15 7 3 6.87 4.47 -15 -7 -3 -0.41 4.40 -15 7 -3 6.98 6.48 15 7 4 9.81 6.30 -15 -7 -4 10.85 4.35 -15 7 -4 12.94 4.54 -16 0 0 124.42 3.53 16 0 0 118.17 3.58 -16 0 -1 2.49 2.99 16 0 1 -1.04 4.31 -16 0 -2 0.95 4.25 16 0 2 6.69 4.25 -16 0 -3 0.31 3.00 16 0 3 1.75 2.98 -16 0 -4 401.16 5.03 16 0 4 396.08 5.06 -16 0 -5 -0.89 4.91 16 0 5 -1.61 3.50 16 0 6 16.82 3.52 -16 0 -6 10.67 5.32 -16 0 -7 -0.94 5.60 16 0 7 2.07 4.03 -16 0 -8 22.97 4.50 16 0 8 24.23 4.63 -16 0 -9 -2.97 6.15 16 0 9 4.20 6.21 -16 2 0 249.50 4.05 16 2 0 262.71 4.10 -16 -2 0 262.49 5.03 16 -2 0 267.49 4.14 -16 2 -1 80.88 3.39 16 2 1 84.32 3.37 -16 -2 -1 85.14 3.38 16 -2 1 90.15 4.60 -16 2 -2 44.84 4.39 16 2 2 43.94 3.23 -16 -2 -2 43.98 4.30 16 -2 2 49.57 4.38 -16 2 -3 47.19 3.79 16 2 3 45.30 4.72 -16 -2 -3 49.64 5.07 16 -2 3 48.10 4.79 -16 2 -4 10.48 5.06 16 2 4 11.62 3.52 -16 -2 -4 12.05 4.92 16 -2 4 11.54 3.58 16 -2 5 50.40 5.12 -16 2 -5 47.56 3.73 -16 -2 -5 47.42 3.66 16 2 5 49.67 3.63 16 -2 6 42.93 5.85 -16 2 -6 41.04 4.14 -16 -2 -6 41.38 4.15 16 2 6 42.61 4.15 16 -2 7 17.50 5.72 -16 2 -7 13.88 5.63 -16 -2 -7 15.96 3.99 16 2 7 16.06 5.69 16 -2 8 39.94 4.60 -16 2 -8 36.74 4.50 -16 -2 -8 35.37 4.48 16 2 8 38.97 4.62 16 -4 0 25.77 3.16 16 4 0 24.93 3.00 -16 -4 0 25.77 4.22 -16 4 0 30.18 4.28 16 -4 1 -0.29 5.05 16 4 1 0.39 3.52 -16 -4 -1 3.09 3.40 -16 4 -1 -4.85 5.11 16 -4 2 112.02 3.98 -16 -4 -2 114.29 3.86 16 4 2 111.99 3.89 -16 4 -2 111.76 4.02 16 -4 3 2.20 3.53 -16 -4 -3 3.13 4.84 16 4 3 6.27 4.88 -16 4 -3 1.40 3.55 16 -4 4 2.74 4.06 -16 -4 -4 5.88 3.95 -16 4 -4 5.26 4.07 16 4 4 8.24 4.02 16 -4 5 45.06 4.13 -16 -4 -5 47.40 4.10 -16 4 -5 46.96 4.14 16 4 5 50.02 4.17 16 -4 6 47.52 6.45 -16 -4 -6 44.58 4.57 -16 4 -6 40.08 4.61 16 4 6 47.83 4.65 -16 -4 -7 5.47 6.15 16 -4 7 -0.49 6.27 -16 4 -7 0.72 4.40 16 4 7 2.37 4.50 -16 -6 0 -0.22 3.38 16 -6 0 -1.60 3.48 16 6 0 2.26 3.40 -16 6 0 -1.13 3.52 -16 -6 -1 21.48 3.91 16 -6 1 19.90 5.74 16 6 1 15.69 4.07 -16 6 -1 17.63 4.11 -16 -6 -2 52.61 4.05 16 -6 2 58.18 4.20 16 6 2 62.58 5.75 -16 6 -2 48.72 4.28 16 -6 3 3.37 3.91 16 6 3 2.69 3.99 -16 6 -3 1.56 4.04 -16 -6 -3 5.51 3.84 16 -6 4 8.10 4.46 16 6 4 10.78 6.28 -16 6 -4 8.16 6.43 -16 -6 -4 7.32 4.40 16 -6 5 -2.08 6.65 16 6 5 2.25 4.40 -16 6 -5 1.60 6.78 -16 -6 -5 3.94 4.90 16 8 0 45.95 4.55 -16 -8 0 43.31 6.61 -16 8 0 43.73 4.52 -17 -1 0 11.39 3.05 -17 1 0 13.34 3.05 17 1 0 13.54 4.24 17 -1 0 12.00 3.10 -17 1 -1 4.11 4.26 17 1 1 6.31 4.22 17 -1 1 6.88 3.05 -17 -1 -1 6.01 2.97 -17 1 -2 74.54 4.85 17 1 2 74.42 4.83 17 -1 2 75.57 3.85 -17 -1 -2 69.06 4.82 -17 1 -3 11.69 3.58 17 1 3 9.52 3.55 17 -1 3 11.98 3.57 -17 -1 -3 13.13 4.95 -17 1 -4 3.50 4.91 17 1 4 3.22 4.87 -17 -1 -4 1.00 4.87 17 -1 4 -0.31 4.92 -17 1 -5 20.62 4.09 17 1 5 24.32 4.13 -17 -1 -5 21.44 4.05 17 -1 5 21.55 4.11 -17 1 -6 78.59 4.24 -17 -1 -6 80.39 5.80 17 1 6 81.33 4.30 17 -1 6 79.61 4.31 -17 -1 -7 7.54 6.30 17 1 7 14.94 6.40 17 -1 7 6.96 6.40 -17 1 -7 8.76 4.47 17 -1 8 1.47 5.05 -17 -1 -8 2.92 6.59 17 1 8 5.50 5.01 -17 1 -8 -0.34 6.54 17 -3 0 66.43 3.25 -17 3 0 68.28 3.26 17 3 0 71.73 3.25 -17 -3 0 68.02 3.22 17 -3 1 7.54 3.55 -17 3 -1 6.67 3.58 17 3 1 7.96 3.54 -17 -3 -1 10.88 3.45 17 -3 2 3.87 3.50 -17 3 -2 4.52 3.54 17 3 2 6.14 3.47 -17 -3 -2 4.59 4.90 17 -3 3 15.19 3.59 -17 3 -3 19.23 5.02 17 3 3 17.53 4.95 -17 -3 -3 17.10 3.49 17 -3 4 66.85 5.91 -17 3 -4 63.10 4.24 -17 -3 -4 60.52 4.24 17 3 4 62.95 4.20 17 -3 5 12.57 3.98 -17 3 -5 10.01 4.02 -17 -3 -5 8.04 3.94 17 3 5 4.67 4.00 17 -3 6 7.65 4.58 -17 3 -6 10.81 4.49 -17 -3 -6 12.34 6.29 17 3 6 11.79 4.53 17 -3 7 16.27 4.48 -17 3 -7 10.13 6.18 -17 -3 -7 11.49 4.46 17 3 7 14.94 6.27 17 -5 0 115.57 3.95 -17 -5 0 122.66 5.15 17 5 0 119.17 3.86 -17 5 0 111.72 3.96 17 -5 1 5.10 5.81 -17 -5 -1 13.03 5.57 17 5 1 12.39 4.00 -17 5 -1 6.84 4.15 17 -5 2 4.59 5.67 -17 -5 -2 7.09 5.48 17 5 2 2.45 3.97 -17 5 -2 2.82 4.09 17 -5 3 7.05 5.65 -17 -5 -3 6.26 3.91 17 5 3 4.05 3.95 -17 5 -3 5.65 4.08 -17 -5 -4 109.49 6.44 17 -5 4 118.78 6.58 17 5 4 99.61 4.84 -17 5 -4 102.15 4.86 -17 -5 -5 0.71 4.36 17 -5 5 0.58 4.39 -17 5 -5 0.47 6.30 17 5 5 0.81 4.43 17 -7 0 21.84 4.55 17 7 0 23.19 4.47 -17 7 0 21.84 4.55 -17 -7 0 24.52 4.40 17 -7 1 23.87 6.28 17 7 1 16.00 4.48 -17 7 -1 15.26 6.43 -17 -7 -1 21.65 6.09 17 -7 2 15.99 5.03 -17 -7 -2 20.31 4.84 -18 0 0 604.60 5.11 18 0 0 630.84 6.10 -18 0 -1 -4.44 5.01 18 0 1 2.97 4.98 -18 0 -2 -4.72 4.94 18 0 2 -2.36 4.99 -18 0 -3 1.71 4.86 18 0 3 0.99 3.45 18 0 4 81.64 4.31 -18 0 -4 82.23 4.23 18 0 5 -1.25 4.01 -18 0 -5 0.62 3.90 -18 0 -6 0.21 4.45 18 0 6 0.15 4.49 -18 0 -7 -2.58 4.92 18 0 7 2.54 4.44 -18 2 0 38.34 3.60 18 2 0 29.06 5.07 -18 -2 0 37.31 4.98 18 -2 0 33.05 3.64 -18 2 -1 12.11 3.54 18 2 1 13.59 4.93 -18 -2 -1 15.66 3.48 18 -2 1 9.06 3.55 -18 2 -2 20.79 3.53 18 2 2 16.40 3.54 -18 -2 -2 19.61 3.50 18 -2 2 19.47 3.59 -18 2 -3 48.13 4.23 18 2 3 48.03 4.17 -18 -2 -3 48.11 5.38 18 -2 3 57.03 4.17 18 -2 4 66.17 4.27 -18 2 -4 67.13 5.83 18 2 4 68.24 5.78 -18 -2 -4 69.65 5.74 18 -2 5 80.97 4.28 -18 2 -5 75.96 6.19 -18 -2 -5 78.64 4.17 18 2 5 82.08 6.21 18 -2 6 18.51 4.52 -18 2 -6 13.71 4.50 -18 -2 -6 12.89 4.46 18 2 6 20.47 6.28 18 -4 0 -1.69 5.00 18 4 0 5.42 3.43 -18 -4 0 5.58 4.83 -18 4 0 5.82 3.48 18 -4 1 6.55 3.99 -18 -4 -1 4.36 5.53 -18 4 -1 0.57 4.12 18 4 1 1.66 3.96 18 -4 2 93.77 4.39 -18 -4 -2 89.64 4.19 -18 4 -2 75.82 4.28 18 4 2 97.22 5.89 18 -4 3 40.74 4.12 -18 -4 -3 31.91 4.01 -18 4 -3 33.45 5.74 18 4 3 37.30 4.06 18 -4 4 5.65 4.49 -18 -4 -4 8.68 4.39 -18 4 -4 5.81 4.52 18 4 4 6.55 6.38 18 -4 5 0.67 4.44 -18 -4 -5 0.92 4.35 -18 4 -5 2.86 4.43 18 4 5 2.61 6.25 -18 -6 0 -1.49 4.39 18 -6 0 2.85 4.53 18 6 0 7.69 4.43 -18 6 0 0.29 4.55 -18 -6 -1 5.33 4.33 18 -6 1 1.95 4.50 18 6 1 0.70 4.46 -18 6 -1 -0.08 4.59 -18 -6 -2 65.48 4.52 18 -6 2 73.78 4.65 18 6 2 78.39 6.35 -18 6 -2 67.63 4.73 -19 1 0 2.81 4.90 19 1 0 -0.21 3.47 19 -1 0 1.42 3.50 -19 -1 0 0.31 3.47 -19 1 -1 4.94 3.54 19 1 1 10.33 3.46 19 -1 1 6.60 3.53 -19 -1 -1 8.85 3.43 -19 1 -2 57.61 4.20 19 1 2 56.79 4.19 19 -1 2 65.21 4.20 -19 -1 -2 55.42 5.41 -19 1 -3 18.11 5.66 19 1 3 21.08 5.70 -19 -1 -3 26.60 5.60 19 -1 3 20.01 5.70 -19 1 -4 -2.70 4.00 19 1 4 1.33 3.96 -19 -1 -4 -2.21 5.54 19 -1 4 1.44 3.96 -19 1 -5 0.65 4.41 -19 -1 -5 0.00 4.44 19 1 5 -0.14 4.52 19 -1 5 0.89 6.33 19 1 6 33.87 6.27 19 -3 0 62.12 3.68 -19 3 0 61.88 3.66 19 3 0 54.94 3.65 -19 -3 0 56.14 4.99 19 -3 1 13.99 4.10 -19 3 -1 15.60 4.07 19 3 1 12.86 4.07 -19 -3 -1 14.64 4.02 19 -3 2 10.89 4.03 -19 3 -2 6.90 4.02 -19 -3 -2 9.99 3.93 19 3 2 8.21 3.97 19 -3 3 72.19 4.27 -19 3 -3 71.23 6.25 -19 -3 -3 71.34 4.17 19 3 3 80.00 6.18 19 -3 4 109.67 4.82 -19 3 -4 110.20 4.87 -19 -3 -4 119.16 4.79 19 3 4 109.93 4.89 -19 -3 -5 6.93 4.99 19 3 5 10.05 5.02 19 -5 0 76.08 5.76 -19 -5 0 69.42 4.07 19 5 0 64.08 5.72 -19 5 0 71.15 5.88 19 -5 1 3.78 4.48 -19 -5 -1 0.02 4.40 19 5 1 0.21 6.31 -19 5 -1 3.71 6.41 19 -5 2 0.42 4.44 -19 -5 -2 0.12 6.09 -19 5 -2 3.52 6.39 19 5 2 -2.85 4.42 -20 0 0 51.59 3.65 20 0 0 65.93 5.03 -20 0 -1 1.88 3.96 20 0 1 -0.09 5.61 -20 0 -2 1.46 3.90 20 0 2 3.40 5.60 20 0 3 -0.69 4.46 -20 0 -3 0.47 4.44 20 0 4 89.17 4.70 -20 0 -4 98.27 6.43 -20 2 0 75.85 4.28 20 2 0 71.41 4.24 -20 -2 0 76.26 4.18 20 -2 0 81.16 5.84 -20 2 -1 5.22 3.99 20 2 1 -2.95 3.99 -20 -2 -1 4.38 5.54 20 -2 1 7.60 5.62 20 -2 2 3.58 5.63 -20 2 -2 8.02 3.92 20 2 2 5.10 4.01 -20 -2 -2 6.75 3.92 20 -2 3 37.37 6.44 -20 2 -3 34.87 4.59 -20 -2 -3 35.82 4.51 20 2 3 41.74 6.32 20 -2 4 25.95 4.50 -20 2 -4 22.99 6.27 -20 -2 -4 26.84 4.45 20 2 4 28.81 4.43 20 -4 0 12.10 5.65 -20 4 0 12.44 5.63 -20 -4 0 12.32 5.47 20 4 0 11.74 4.00 20 -4 1 5.06 6.38 -20 4 -1 5.45 6.39 -20 -4 -1 1.91 4.36 20 4 1 0.82 6.32 20 -4 2 29.84 4.55 -20 4 -2 28.28 6.39 -20 -4 -2 32.23 4.42 20 4 2 30.31 6.28 -21 1 0 0.47 3.91 21 1 0 -3.36 5.58 21 -1 0 0.73 5.59 -21 -1 0 1.49 5.50 -21 1 -1 18.18 3.99 21 1 1 19.20 5.61 -21 -1 -1 18.57 3.99 21 -1 1 18.64 5.61 -21 1 -2 82.12 4.66 21 1 2 96.95 4.77 -21 -1 -2 88.22 4.69 21 -1 2 112.01 6.50 -21 1 -3 7.76 4.42 21 1 3 11.75 4.45 -21 -1 -3 11.75 4.96 21 -1 3 15.90 4.38 21 -3 0 60.05 4.70 -21 3 0 62.49 4.69 -21 -3 0 61.25 6.40 21 3 0 64.75 6.41 21 -3 1 100.21 4.80 -21 3 -1 100.05 4.76 -21 -3 -1 103.68 4.65 21 3 1 108.00 6.46 21 -3 2 8.09 5.03 -21 3 -2 10.36 5.06 -21 -3 -2 13.19 6.96 21 3 2 11.19 4.95 -22 0 0 100.74 6.45 22 0 0 103.40 6.54 -22 0 -1 -0.25 4.36 22 0 1 1.24 6.21 22 0 2 0.22 4.43 -22 2 0 20.92 4.43 22 2 0 22.84 4.42 -22 -2 0 18.67 4.43 22 -2 0 21.21 4.46 22 -2 1 12.48 4.45 -22 2 -1 15.05 4.41 22 2 1 17.53 4.93 -22 -2 -1 15.36 6.59 23 1 0 -2.88 4.93 23 -1 0 -0.20 4.91 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 78890 _shelx_res_file ; TITL ip2028 in C2/c shelx.res created by SHELXL-2018/1 at 11:04:18 on 18-Sep-2021 CELL 0.71073 19.4400 8.6070 16.0977 90.000 115.264 90.000 ZERR 8.00 0.0015 0.0004 0.0010 0.000 0.007 0.000 LATT 7 SYMM - X, Y, 1/2 - Z SFAC C H N O RB UNIT 48 8 64 64 8 MERG 2 FMAP 2 EQIV $1 X, -1+Y, Z EQIV $2 -0.5+X, 0.5+Y, Z EQIV $3 0.5-X, 0.5-Y, -Z EQIV $4 0.5-X, 0.5+Y, 0.5-Z EQIV $5 -0.5+X, 0.5-Y, -0.5+Z RTAB H..O H1 N4_$1 RTAB O..O N1 N4_$1 RTAB XHY N1 H1 N4_$1 BIND RB2 O2_$2 BIND RB2 O2_$3 FREE RB2 N7_$4 FREE RB2 N7_$5 PLAN 10 SIZE 0.14 0.16 0.20 ACTA BOND BOND $H CONF L.S. 5 TEMP -60.00 WGHT 0.032600 FVAR 0.13662 RB1 5 0.500000 0.392794 0.250000 10.50000 0.01707 0.01962 = 0.04422 0.00000 0.00897 0.00000 RB2 5 0.000000 0.500000 0.000000 10.50000 0.02226 0.03355 = 0.03067 -0.01165 0.00132 0.00090 O1 4 0.383299 -0.383041 0.161058 11.00000 0.03105 0.01883 = 0.07025 0.00381 0.01530 0.01281 O2 4 0.384889 -0.146109 0.116394 11.00000 0.02839 0.02785 = 0.05332 0.00341 0.02344 -0.00052 O3 4 0.036975 -0.160317 0.062145 11.00000 0.02116 0.02826 = 0.09411 0.00358 0.02140 -0.00112 O4 4 0.106810 0.032438 0.137918 11.00000 0.04114 0.02138 = 0.05192 -0.00027 0.02985 0.00709 O5 4 0.453192 0.098535 0.307178 11.00000 0.02058 0.03355 = 0.03271 0.00481 0.00006 -0.00437 O6 4 0.377967 -0.092937 0.295802 11.00000 0.03753 0.01548 = 0.02716 0.00461 0.00397 -0.00010 O7 4 0.131233 0.343696 -0.012928 11.00000 0.03132 0.01902 = 0.04703 0.01270 0.01113 0.01207 O8 4 0.122177 0.094170 -0.030945 11.00000 0.02254 0.02311 = 0.03048 0.00077 0.00373 -0.00460 N1 3 0.232223 -0.366118 0.107374 11.00000 0.02312 0.00895 = 0.02666 -0.00101 0.00978 0.00038 AFIX 43 H1 2 0.247444 -0.461154 0.107308 11.00000 -1.50000 AFIX 0 N2 3 0.162176 -0.326010 0.095322 11.00000 0.02221 0.01273 = 0.02834 0.00202 0.01093 -0.00043 N3 3 0.334704 0.270998 0.195471 11.00000 0.02200 0.01412 = 0.02304 -0.00103 0.00671 -0.00157 N4 3 0.269458 0.319349 0.126427 11.00000 0.02134 0.01025 = 0.02769 0.00086 0.00984 -0.00007 N5 3 0.353872 -0.256623 0.133487 11.00000 0.02115 0.01639 = 0.02297 -0.00506 0.00642 0.00306 N6 3 0.097899 -0.093546 0.100109 11.00000 0.02562 0.01738 = 0.04231 0.00773 0.01982 0.00298 N7 3 0.390832 0.034668 0.271521 11.00000 0.02409 0.01758 = 0.01963 -0.00145 0.00532 0.00101 N8 3 0.155088 0.210892 0.010623 11.00000 0.01869 0.01802 = 0.02629 0.00566 0.01075 0.00307 C1 1 0.276058 -0.239071 0.119649 11.00000 0.02030 0.01148 = 0.01930 0.00000 0.00697 0.00007 C2 1 0.235453 -0.106126 0.118136 11.00000 0.01868 0.01041 = 0.01876 0.00077 0.00747 0.00101 C3 1 0.164746 -0.171861 0.102512 11.00000 0.02029 0.01217 = 0.02235 0.00187 0.00947 0.00077 C4 1 0.329271 0.115929 0.199662 11.00000 0.02056 0.01194 = 0.01918 -0.00027 0.00702 0.00066 C5 1 0.261311 0.055291 0.134165 11.00000 0.01771 0.01090 = 0.02024 0.00027 0.00937 0.00141 C6 1 0.226506 0.192590 0.089412 11.00000 0.01845 0.01259 = 0.01982 0.00109 0.00893 0.00160 HKLF 4 REM ip2028 in C2/c REM R1 = 0.0256 for 2186 Fo > 4sig(Fo) and 0.0379 for all 2890 data REM 210 parameters refined using 0 restraints END WGHT 0.0322 0.0000 REM Highest difference peak 0.373, deepest hole -0.392, 1-sigma level 0.077 Q1 1 0.3063 0.0637 0.1683 11.00000 0.05 0.37 Q2 1 0.0479 0.5096 0.0445 11.00000 0.05 0.37 Q3 1 0.1964 0.1994 0.0495 11.00000 0.05 0.36 Q4 1 0.5286 0.4419 0.2281 11.00000 0.05 0.35 Q5 1 -0.0325 0.5508 0.0228 11.00000 0.05 0.35 Q6 1 0.4562 0.3683 0.2072 11.00000 0.05 0.33 Q7 1 0.5339 0.3443 0.2239 11.00000 0.05 0.32 Q8 1 0.1937 -0.1257 0.0903 11.00000 0.05 0.30 Q9 1 0.3595 0.3167 0.2258 11.00000 0.05 0.26 Q10 1 0.0799 0.0798 -0.0664 11.00000 0.05 0.26 ; _shelx_res_checksum 9287 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rb Rb1 0.500000 0.39279(3) 0.250000 0.02840(9) Uani d 1 . . Rb Rb2 0.000000 0.500000 0.000000 0.03230(9) Uani d 1 . . O O1 0.38330(9) -0.38304(18) 0.16106(14) 0.0422(5) Uani d 1 . . O O2 0.38489(9) -0.14611(18) 0.11639(13) 0.0344(4) Uani d 1 . . O O3 0.03697(9) -0.16032(19) 0.06215(16) 0.0490(5) Uani d 1 . . O O4 0.10681(9) 0.03244(17) 0.13792(13) 0.0347(4) Uani d 1 . . O O5 0.45319(8) 0.09854(18) 0.30718(12) 0.0329(4) Uani d 1 . . O O6 0.37797(9) -0.09294(16) 0.29580(11) 0.0301(4) Uani d 1 . . O O7 0.13123(9) 0.34370(17) -0.01293(13) 0.0344(4) Uani d 1 . . O O8 0.12218(8) 0.09417(17) -0.03095(11) 0.0280(3) Uani d 1 . . N N1 0.23222(9) -0.36612(17) 0.10737(13) 0.0199(4) Uani d 1 . . H H1 0.247444 -0.461154 0.107308 0.030 Uiso calc 1 . . N N2 0.16218(9) -0.32601(19) 0.09532(13) 0.0210(4) Uani d 1 . . N N3 0.33470(9) 0.27100(18) 0.19547(13) 0.0207(4) Uani d 1 . . N N4 0.26946(9) 0.31935(17) 0.12643(13) 0.0200(4) Uani d 1 . . N N5 0.35387(9) -0.25662(18) 0.13349(12) 0.0212(4) Uani d 1 . . N N6 0.09790(10) -0.0935(2) 0.10011(14) 0.0266(4) Uani d 1 . . N N7 0.39083(9) 0.03467(19) 0.27152(13) 0.0218(4) Uani d 1 . . N N8 0.15509(9) 0.21089(19) 0.01062(13) 0.0206(4) Uani d 1 . . C C1 0.27606(10) -0.2391(2) 0.11965(14) 0.0175(4) Uani d 1 . . C C2 0.23545(10) -0.1061(2) 0.11814(14) 0.0161(4) Uani d 1 . . C C3 0.16475(10) -0.1719(2) 0.10251(15) 0.0181(4) Uani d 1 . . C C4 0.32927(10) 0.1159(2) 0.19966(14) 0.0177(4) Uani d 1 . . C C5 0.26131(10) 0.0553(2) 0.13416(14) 0.0158(4) Uani d 1 . . C C6 0.22651(10) 0.1926(2) 0.08941(14) 0.0167(4) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Rb1 0.01707(13) 0.01962(14) 0.0442(2) 0.000 0.00897(13) 0.000 Rb2 0.02226(15) 0.03355(17) 0.0307(2) 0.00090(12) 0.00132(12) -0.01165(14) O1 0.0311(8) 0.0188(8) 0.0702(14) 0.0128(6) 0.0153(9) 0.0038(8) O2 0.0284(8) 0.0279(8) 0.0533(12) -0.0005(6) 0.0234(8) 0.0034(8) O3 0.0212(8) 0.0283(9) 0.0941(17) -0.0011(7) 0.0214(9) 0.0036(9) O4 0.0411(9) 0.0214(8) 0.0519(12) 0.0071(7) 0.0299(9) -0.0003(7) O5 0.0206(7) 0.0336(8) 0.0327(10) -0.0044(6) 0.0001(7) 0.0048(7) O6 0.0375(8) 0.0155(7) 0.0272(10) -0.0001(6) 0.0040(7) 0.0046(6) O7 0.0313(8) 0.0190(7) 0.0470(12) 0.0121(6) 0.0111(8) 0.0127(7) O8 0.0225(7) 0.0231(8) 0.0305(10) -0.0046(6) 0.0037(6) 0.0008(7) N1 0.0231(8) 0.0089(7) 0.0267(11) 0.0004(6) 0.0098(7) -0.0010(7) N2 0.0222(8) 0.0127(8) 0.0283(11) -0.0004(6) 0.0109(7) 0.0020(7) N3 0.0220(8) 0.0141(8) 0.0230(10) -0.0016(6) 0.0067(7) -0.0010(7) N4 0.0213(8) 0.0103(7) 0.0277(11) -0.0001(6) 0.0098(7) 0.0009(7) N5 0.0211(8) 0.0164(8) 0.0230(10) 0.0031(6) 0.0064(7) -0.0051(7) N6 0.0256(9) 0.0174(9) 0.0423(13) 0.0030(7) 0.0198(8) 0.0077(8) N7 0.0241(9) 0.0176(9) 0.0196(10) 0.0010(6) 0.0053(7) -0.0014(7) N8 0.0187(8) 0.0180(8) 0.0263(11) 0.0031(6) 0.0108(7) 0.0057(7) C1 0.0203(9) 0.0115(9) 0.0193(12) 0.0001(7) 0.0070(8) 0.0000(7) C2 0.0187(9) 0.0104(8) 0.0188(11) 0.0010(7) 0.0075(8) 0.0008(8) C3 0.0203(9) 0.0122(9) 0.0223(12) 0.0008(7) 0.0095(8) 0.0019(8) C4 0.0206(9) 0.0119(8) 0.0192(11) 0.0007(7) 0.0070(8) -0.0003(7) C5 0.0177(9) 0.0109(8) 0.0202(12) 0.0014(7) 0.0094(8) 0.0003(7) C6 0.0185(9) 0.0126(8) 0.0198(11) 0.0016(7) 0.0089(8) 0.0011(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Rb1 O1 2_665 1_565 94.94(7) ? O1 Rb1 O5 2_665 . 134.80(5) ? O1 Rb1 O5 1_565 . 116.69(4) ? O1 Rb1 O5 2_665 2_655 116.69(4) ? O1 Rb1 O5 1_565 2_655 134.80(5) ? O5 Rb1 O5 . 2_655 62.80(7) ? O1 Rb1 N3 2_665 . 150.29(5) ? O1 Rb1 N3 1_565 . 65.44(5) ? O5 Rb1 N3 . . 52.18(4) ? O5 Rb1 N3 2_655 . 92.36(4) ? O1 Rb1 N3 2_665 2_655 65.44(5) ? O1 Rb1 N3 1_565 2_655 150.29(5) ? O5 Rb1 N3 . 2_655 92.36(4) ? O5 Rb1 N3 2_655 2_655 52.18(4) ? N3 Rb1 N3 . 2_655 140.85(6) ? O1 Rb1 O8 2_665 8_556 52.19(5) ? O1 Rb1 O8 1_565 8_556 124.56(5) ? O5 Rb1 O8 . 8_556 82.76(4) ? O5 Rb1 O8 2_655 8_556 100.60(4) ? N3 Rb1 O8 . 8_556 119.65(4) ? N3 Rb1 O8 2_655 8_556 61.84(4) ? O1 Rb1 O8 2_665 7 124.56(5) ? O1 Rb1 O8 1_565 7 52.19(5) ? O5 Rb1 O8 . 7 100.60(4) ? O5 Rb1 O8 2_655 7 82.76(4) ? N3 Rb1 O8 . 7 61.84(4) ? N3 Rb1 O8 2_655 7 119.65(4) ? O8 Rb1 O8 8_556 7 176.11(5) ? O1 Rb1 O3 2_665 3 96.42(5) ? O1 Rb1 O3 1_565 3 93.94(5) ? O5 Rb1 O3 . 3 111.58(4) ? O5 Rb1 O3 2_655 3 53.44(4) ? N3 Rb1 O3 . 3 106.56(4) ? N3 Rb1 O3 2_655 3 68.00(4) ? O8 Rb1 O3 8_556 3 128.33(4) ? O8 Rb1 O3 7 3 52.33(4) ? O1 Rb1 O3 2_665 4 93.94(5) ? O1 Rb1 O3 1_565 4 96.42(5) ? O5 Rb1 O3 . 4 53.44(4) ? O5 Rb1 O3 2_655 4 111.58(4) ? N3 Rb1 O3 . 4 68.00(4) ? N3 Rb1 O3 2_655 4 106.56(4) ? O8 Rb1 O3 8_556 4 52.33(4) ? O8 Rb1 O3 7 4 128.33(4) ? O3 Rb1 O3 3 4 164.66(6) ? O1 Rb1 O4 2_665 3 60.41(5) ? O1 Rb1 O4 1_565 3 91.65(5) ? O5 Rb1 O4 . 3 141.47(4) ? O5 Rb1 O4 2_655 3 78.75(4) ? N3 Rb1 O4 . 3 137.39(5) ? N3 Rb1 O4 2_655 3 59.64(4) ? O8 Rb1 O4 8_556 3 102.96(4) ? O8 Rb1 O4 7 3 75.66(4) ? O3 Rb1 O4 3 3 36.38(4) ? O3 Rb1 O4 4 3 153.75(4) ? O1 Rb1 O4 2_665 4 91.65(5) ? O1 Rb1 O4 1_565 4 60.41(5) ? O5 Rb1 O4 . 4 78.75(4) ? O5 Rb1 O4 2_655 4 141.47(4) ? N3 Rb1 O4 . 4 59.64(4) ? N3 Rb1 O4 2_655 4 137.39(5) ? O8 Rb1 O4 8_556 4 75.66(4) ? O8 Rb1 O4 7 4 102.96(4) ? O3 Rb1 O4 3 4 153.75(4) ? O3 Rb1 O4 4 4 36.38(4) ? O4 Rb1 O4 3 4 139.76(5) ? O5 Rb2 O5 8_455 4 180.00(8) ? O5 Rb2 O7 8_455 5_565 108.32(4) ? O5 Rb2 O7 4 5_565 71.68(4) ? O5 Rb2 O7 8_455 . 71.68(4) ? O5 Rb2 O7 4 . 108.32(4) ? O7 Rb2 O7 5_565 . 180.0 ? O5 Rb2 O3 8_455 5 57.45(5) ? O5 Rb2 O3 4 5 122.55(5) ? O7 Rb2 O3 5_565 5 111.42(4) ? O7 Rb2 O3 . 5 68.58(4) ? O5 Rb2 O3 8_455 1_565 122.55(5) ? O5 Rb2 O3 4 1_565 57.45(5) ? O7 Rb2 O3 5_565 1_565 68.58(4) ? O7 Rb2 O3 . 1_565 111.42(4) ? O3 Rb2 O3 5 1_565 180.00(10) ? O5 Rb2 N2 8_455 5 64.39(4) ? O5 Rb2 N2 4 5 115.61(4) ? O7 Rb2 N2 5_565 5 63.20(4) ? O7 Rb2 N2 . 5 116.80(4) ? O3 Rb2 N2 5 5 50.09(4) ? O3 Rb2 N2 1_565 5 129.91(4) ? O5 Rb2 N2 8_455 1_565 115.61(4) ? O5 Rb2 N2 4 1_565 64.39(4) ? O7 Rb2 N2 5_565 1_565 116.80(4) ? O7 Rb2 N2 . 1_565 63.20(4) ? O3 Rb2 N2 5 1_565 129.91(4) ? O3 Rb2 N2 1_565 1_565 50.09(4) ? N2 Rb2 N2 5 1_565 180.0 ? O5 Rb2 O6 8_455 8_455 40.54(4) ? O5 Rb2 O6 4 8_455 139.46(4) ? O7 Rb2 O6 5_565 8_455 71.28(5) ? O7 Rb2 O6 . 8_455 108.72(5) ? O3 Rb2 O6 5 8_455 86.34(5) ? O3 Rb2 O6 1_565 8_455 93.66(5) ? N2 Rb2 O6 5 8_455 59.09(4) ? N2 Rb2 O6 1_565 8_455 120.91(4) ? O5 Rb2 O6 8_455 4 139.46(4) ? O5 Rb2 O6 4 4 40.54(4) ? O7 Rb2 O6 5_565 4 108.72(5) ? O7 Rb2 O6 . 4 71.28(5) ? O3 Rb2 O6 5 4 93.66(5) ? O3 Rb2 O6 1_565 4 86.34(5) ? N2 Rb2 O6 5 4 120.91(4) ? N2 Rb2 O6 1_565 4 59.09(4) ? O6 Rb2 O6 8_455 4 180.00(7) ? O5 Rb2 O2 8_455 7 63.14(4) ? O5 Rb2 O2 4 7 116.86(4) ? O7 Rb2 O2 5_565 7 127.24(4) ? O7 Rb2 O2 . 7 52.75(4) ? O3 Rb2 O2 5 7 105.45(5) ? O3 Rb2 O2 1_565 7 74.55(5) ? N2 Rb2 O2 5 7 126.63(4) ? N2 Rb2 O2 1_565 7 53.37(4) ? O6 Rb2 O2 8_455 7 74.96(4) ? O6 Rb2 O2 4 7 105.04(4) ? O5 Rb2 O2 8_455 3_455 116.86(4) ? O5 Rb2 O2 4 3_455 63.14(4) ? O7 Rb2 O2 5_565 3_455 52.76(4) ? O7 Rb2 O2 . 3_455 127.25(4) ? O3 Rb2 O2 5 3_455 74.55(5) ? O3 Rb2 O2 1_565 3_455 105.45(5) ? N2 Rb2 O2 5 3_455 53.37(4) ? N2 Rb2 O2 1_565 3_455 126.63(4) ? O6 Rb2 O2 8_455 3_455 105.04(4) ? O6 Rb2 O2 4 3_455 74.96(4) ? O2 Rb2 O2 7 3_455 180.00(3) ? N5 O1 Rb1 . 1_545 158.96(13) ? N6 O3 Rb2 . 1_545 130.77(13) ? N6 O3 Rb1 . 3_445 91.12(15) ? Rb2 O3 Rb1 1_545 3_445 107.84(5) ? N6 O4 Rb1 . 3_445 87.86(12) ? N7 O5 Rb2 . 4_545 99.33(12) ? N7 O5 Rb1 . . 127.55(12) ? Rb2 O5 Rb1 4_545 . 124.88(5) ? N7 O6 Rb2 . 4_545 86.64(11) ? N8 O7 Rb2 . . 128.40(13) ? N8 O8 Rb1 . 7 121.64(12) ? N2 N1 C1 . . 110.67(15) ? N2 N1 H1 . . 124.7 ? C1 N1 H1 . . 124.7 ? C3 N2 N1 . . 104.29(15) ? C3 N2 Rb2 . 1_545 119.80(12) ? N1 N2 Rb2 . 1_545 132.66(12) ? C4 N3 N4 . . 106.38(15) ? C4 N3 Rb1 . . 114.35(12) ? N4 N3 Rb1 . . 128.37(12) ? N3 N4 C6 . . 107.59(15) ? O2 N5 O1 . . 125.25(17) ? O2 N5 C1 . . 118.13(15) ? O1 N5 C1 . . 116.61(16) ? O4 N6 O3 . . 124.73(18) ? O4 N6 C3 . . 117.74(17) ? O3 N6 C3 . . 117.50(18) ? O4 N6 Rb1 . 3_445 72.68(11) ? O3 N6 Rb1 . 3_445 69.40(14) ? C3 N6 Rb1 . 3_445 132.87(13) ? O6 N7 O5 . . 123.15(18) ? O6 N7 C4 . . 118.54(16) ? O5 N7 C4 . . 118.29(16) ? O6 N7 Rb2 . 4_545 72.15(11) ? O5 N7 Rb2 . 4_545 59.69(11) ? C4 N7 Rb2 . 4_545 146.67(12) ? O8 N8 O7 . . 123.57(18) ? O8 N8 C6 . . 118.40(15) ? O7 N8 C6 . . 118.00(17) ? N1 C1 C2 . . 110.36(16) ? N1 C1 N5 . . 119.62(15) ? C2 C1 N5 . . 130.01(16) ? C1 C2 C3 . . 100.20(16) ? C1 C2 C5 . . 129.17(17) ? C3 C2 C5 . . 130.53(17) ? N2 C3 C2 . . 114.47(16) ? N2 C3 N6 . . 117.47(16) ? C2 C3 N6 . . 127.90(17) ? N3 C4 C5 . . 113.82(17) ? N3 C4 N7 . . 117.80(17) ? C5 C4 N7 . . 128.31(17) ? C4 C5 C6 . . 99.63(15) ? C4 C5 C2 . . 129.27(17) ? C6 C5 C2 . . 131.10(17) ? N4 C6 C5 . . 112.57(17) ? N4 C6 N8 . . 119.01(16) ? C5 C6 N8 . . 128.38(16) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Rb1 O1 2_665 2.8543(15) n Rb1 O1 1_565 2.8543(15) y Rb1 O5 . 2.9673(16) y Rb1 O5 2_655 2.9673(16) n Rb1 N3 . 3.1285(16) y Rb1 N3 2_655 3.1285(16) n Rb1 O8 8_556 3.3074(16) n Rb1 O8 7 3.3074(16) y Rb1 O3 3 3.424(2) n Rb1 O3 4 3.424(2) y Rb1 O4 3 3.4942(16) n Rb1 O4 4 3.4942(16) y Rb2 O5 8_455 2.9616(17) n Rb2 O5 4 2.9616(17) y Rb2 O7 5_565 2.9690(15) n Rb2 O7 . 2.9690(15) y Rb2 O3 5 3.0743(17) n Rb2 O3 1_565 3.0743(17) y Rb2 N2 5 3.2261(16) n Rb2 N2 1_565 3.2261(16) y Rb2 O6 8_455 3.2275(16) n Rb2 O6 4 3.2275(16) y Rb2 O2 7 3.6985(16) y Rb2 O2 3_455 3.6985(16) n O1 N5 . 1.221(2) n O2 N5 . 1.219(2) n O3 N6 . 1.220(2) n O4 N6 . 1.219(2) n O5 N7 . 1.228(2) n O6 N7 . 1.227(2) n O7 N8 . 1.231(2) n O8 N8 . 1.225(2) n N1 N2 . 1.336(2) n N1 C1 . 1.348(2) n N1 H1 . 0.8700 ? N2 C3 . 1.331(2) n N3 C4 . 1.343(2) n N3 N4 . 1.347(2) n N4 C6 . 1.348(2) n N5 C1 . 1.440(2) n N6 C3 . 1.450(2) n N7 C4 . 1.441(2) n N8 C6 . 1.435(3) n C1 C2 . 1.384(3) n C2 C3 . 1.406(3) n C2 C5 . 1.462(2) n C4 C5 . 1.393(3) n C5 C6 . 1.399(3) n loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1 N4 1_545 0.87 1.93 2.785(2) 166 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C1 N1 N2 C3 . . . . -1.3(2) ? C1 N1 N2 Rb2 . . . 1_545 157.43(14) ? C4 N3 N4 C6 . . . . -1.0(2) ? Rb1 N3 N4 C6 . . . . 140.39(14) ? Rb1 O1 N5 O2 1_545 . . . 26.7(6) ? Rb1 O1 N5 C1 1_545 . . . -153.8(4) ? Rb1 O4 N6 O3 3_445 . . . 48.3(2) ? Rb1 O4 N6 C3 3_445 . . . -129.88(17) ? Rb2 O3 N6 O4 1_545 . . . -164.56(17) ? Rb1 O3 N6 O4 3_445 . . . -49.6(2) ? Rb2 O3 N6 C3 1_545 . . . 13.7(3) ? Rb1 O3 N6 C3 3_445 . . . 128.59(17) ? Rb2 O3 N6 Rb1 1_545 . . 3_445 -114.92(19) ? Rb2 O6 N7 O5 4_545 . . . 32.5(2) ? Rb2 O6 N7 C4 4_545 . . . -145.49(16) ? Rb2 O5 N7 O6 4_545 . . . -36.3(2) ? Rb1 O5 N7 O6 . . . . 174.67(14) ? Rb2 O5 N7 C4 4_545 . . . 141.67(15) ? Rb1 O5 N7 C4 . . . . -7.3(3) ? Rb1 O5 N7 Rb2 . . . 4_545 -149.01(17) ? Rb1 O8 N8 O7 7 . . . 22.7(3) ? Rb1 O8 N8 C6 7 . . . -155.32(13) ? Rb2 O7 N8 O8 . . . . 72.4(3) ? Rb2 O7 N8 C6 . . . . -109.63(17) ? N2 N1 C1 C2 . . . . 1.4(2) ? N2 N1 C1 N5 . . . . -179.72(17) ? O2 N5 C1 N1 . . . . 157.8(2) ? O1 N5 C1 N1 . . . . -21.7(3) ? O2 N5 C1 C2 . . . . -23.6(3) ? O1 N5 C1 C2 . . . . 156.9(2) ? N1 C1 C2 C3 . . . . -0.8(2) ? N5 C1 C2 C3 . . . . -179.5(2) ? N1 C1 C2 C5 . . . . 175.8(2) ? N5 C1 C2 C5 . . . . -2.9(4) ? N1 N2 C3 C2 . . . . 0.8(2) ? Rb2 N2 C3 C2 1_545 . . . -161.31(14) ? N1 N2 C3 N6 . . . . -174.94(18) ? Rb2 N2 C3 N6 1_545 . . . 23.0(2) ? C1 C2 C3 N2 . . . . 0.0(2) ? C5 C2 C3 N2 . . . . -176.6(2) ? C1 C2 C3 N6 . . . . 175.2(2) ? C5 C2 C3 N6 . . . . -1.4(4) ? O4 N6 C3 N2 . . . . 154.3(2) ? O3 N6 C3 N2 . . . . -24.1(3) ? Rb1 N6 C3 N2 3_445 . . . 62.6(3) ? O4 N6 C3 C2 . . . . -20.8(3) ? O3 N6 C3 C2 . . . . 160.8(2) ? Rb1 N6 C3 C2 3_445 . . . -112.5(2) ? N4 N3 C4 C5 . . . . 0.3(2) ? Rb1 N3 C4 C5 . . . . -147.15(14) ? N4 N3 C4 N7 . . . . -177.06(17) ? Rb1 N3 C4 N7 . . . . 35.5(2) ? O6 N7 C4 N3 . . . . 156.77(19) ? O5 N7 C4 N3 . . . . -21.3(3) ? Rb2 N7 C4 N3 4_545 . . . 55.7(3) ? O6 N7 C4 C5 . . . . -20.2(3) ? O5 N7 C4 C5 . . . . 161.7(2) ? Rb2 N7 C4 C5 4_545 . . . -121.3(2) ? N3 C4 C5 C6 . . . . 0.4(2) ? N7 C4 C5 C6 . . . . 177.5(2) ? N3 C4 C5 C2 . . . . -179.85(19) ? N7 C4 C5 C2 . . . . -2.8(4) ? C1 C2 C5 C4 . . . . -41.0(4) ? C3 C2 C5 C4 . . . . 134.7(2) ? C1 C2 C5 C6 . . . . 138.7(2) ? C3 C2 C5 C6 . . . . -45.6(4) ? N3 N4 C6 C5 . . . . 1.3(2) ? N3 N4 C6 N8 . . . . -176.64(16) ? C4 C5 C6 N4 . . . . -1.0(2) ? C2 C5 C6 N4 . . . . 179.2(2) ? C4 C5 C6 N8 . . . . 176.7(2) ? C2 C5 C6 N8 . . . . -3.1(4) ? O8 N8 C6 N4 . . . . 168.87(18) ? O7 N8 C6 N4 . . . . -9.2(3) ? O8 N8 C6 C5 . . . . -8.7(3) ? O7 N8 C6 C5 . . . . 173.2(2) ? _cod_database_fobs_code 2243937