#------------------------------------------------------------------------------ #$Date: 2021-10-20 05:24:09 +0300 (Wed, 20 Oct 2021) $ #$Revision: 270046 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/39/2243941.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243941 _cell_angle_alpha 90.000 _cell_angle_beta 99.076 _cell_angle_gamma 90.000 _cell_length_a 5.3708 _cell_length_b 15.2200 _cell_length_c 11.8014 _exptl_crystal_F_000 434.00 _reflns_d_resolution_high 0.7880 _cod_data_source_file hb7987Form_Isup2.hkl _cod_data_source_block Form_I _shelx_title ' imk4_Co in P2(1)/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.43 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 566.43 587.77 3.74 o 2 0 0 2907.29 2704.72 67.25 o 3 0 0 4.80 3.32 1.32 o 4 0 0 78.18 92.56 1.12 o 5 0 0 249.66 245.35 2.26 o 6 0 0 169.24 187.49 9.03 o 1 1 0 195.51 171.48 2.03 o 2 1 0 1301.57 1268.05 9.73 o 3 1 0 37.50 39.10 1.07 o 4 1 0 2369.63 2241.83 15.35 o 5 1 0 45.67 44.24 0.92 o 6 1 0 308.84 349.20 8.15 o 0 2 0 1924.92 2015.97 16.08 o 1 2 0 399.21 409.83 3.38 o 2 2 0 784.56 703.97 5.59 o 3 2 0 261.40 230.78 3.73 o 4 2 0 61.35 63.21 0.73 o 5 2 0 169.74 163.15 2.54 o 6 2 0 838.96 889.70 14.11 o 1 3 0 6549.41 6307.94 25.18 o 2 3 0 268.01 213.73 2.33 o 3 3 0 32.56 35.93 1.15 o 4 3 0 1112.27 1054.14 4.30 o 5 3 0 24.57 23.09 1.06 o 6 3 0 544.95 602.62 20.50 o 0 4 0 9079.59 9167.78 49.82 o 1 4 0 124.48 126.92 3.56 o 2 4 0 2751.32 2772.22 16.29 o 3 4 0 608.06 594.52 3.32 o 4 4 0 36.99 34.95 0.73 o 5 4 0 122.39 126.95 1.45 o 6 4 0 64.22 77.36 1.48 o 1 5 0 1797.79 2001.18 19.58 o 2 5 0 5106.52 5040.96 47.52 o 3 5 0 22.74 26.32 0.94 o 4 5 0 1483.56 1470.38 9.54 o 5 5 0 183.08 182.01 1.85 o 6 5 0 664.17 711.48 5.29 o 0 6 0 15130.44 15095.88 67.48 o 1 6 0 987.36 1068.26 9.91 o 2 6 0 1750.20 1634.32 11.83 o 3 6 0 130.29 133.75 1.19 o 4 6 0 48.54 52.54 0.94 o 5 6 0 11.38 15.31 1.06 o 6 6 0 356.49 356.95 5.88 o 1 7 0 22.74 28.65 0.62 o 2 7 0 234.56 193.13 2.49 o 3 7 0 190.91 191.37 1.75 o 4 7 0 1587.93 1563.10 14.74 o 5 7 0 28.85 33.44 1.25 o 6 7 0 291.76 287.56 2.79 o 0 8 0 8907.78 9121.52 42.05 o 1 8 0 232.41 237.02 1.87 o 2 8 0 822.36 801.92 6.75 o 3 8 0 90.73 77.41 1.19 o 4 8 0 9.40 10.64 0.95 o 5 8 0 495.02 508.07 3.51 o 6 8 0 352.40 327.06 42.63 o 1 9 0 99.00 113.63 1.38 o 2 9 0 448.60 431.94 5.92 o 3 9 0 22.42 29.13 0.84 o 4 9 0 574.01 591.74 9.21 o 5 9 0 9.10 12.99 1.08 o 0 10 0 6205.60 6344.43 32.15 o 1 10 0 55.80 63.79 0.85 o 2 10 0 496.59 487.26 4.92 o 3 10 0 200.25 194.69 2.02 o 4 10 0 37.09 32.74 1.09 o 5 10 0 9.37 11.03 0.94 o 1 11 0 45.73 49.84 0.82 o 2 11 0 617.03 618.05 6.29 o 3 11 0 65.90 61.13 0.96 o 4 11 0 1073.55 1088.09 8.11 o 5 11 0 45.47 44.67 1.08 o 0 12 0 3319.73 3383.34 15.76 o 1 12 0 14.95 17.82 0.87 o 2 12 0 445.81 439.94 3.71 o 3 12 0 31.68 25.30 0.98 o 4 12 0 6.45 7.49 0.87 o 5 12 0 88.72 83.12 3.00 o 1 13 0 310.08 329.35 3.76 o 2 13 0 258.75 274.60 3.32 o 3 13 0 21.58 20.67 1.00 o 4 13 0 622.22 658.60 12.39 o 0 14 0 921.77 917.97 5.76 o 1 14 0 59.68 61.17 1.17 o 2 14 0 462.75 459.77 7.87 o 3 14 0 409.91 400.93 9.33 o 4 14 0 0.38 1.13 1.12 o 1 15 0 43.83 39.16 1.24 o 2 15 0 527.69 536.07 9.71 o 3 15 0 77.82 72.60 0.94 o 4 15 0 134.06 144.79 1.24 o 0 16 0 2395.69 2488.39 10.60 o 1 16 0 11.84 13.84 0.91 o 2 16 0 320.70 331.06 5.04 o 3 16 0 17.13 19.85 1.03 o 1 17 0 73.36 71.43 1.12 o 2 17 0 101.75 109.00 1.95 o 3 17 0 11.46 11.45 0.63 o 0 18 0 811.98 792.81 5.39 o 1 18 0 56.00 63.31 1.53 o 2 18 0 112.57 93.29 1.04 o 1 19 0 8.99 6.32 0.51 o -6 0 1 21.71 22.56 1.88 o -5 0 1 929.17 926.16 13.05 o -4 0 1 533.40 507.86 5.37 o -3 0 1 482.03 442.47 4.89 o -2 0 1 261.83 293.12 4.66 o -1 0 1 119.04 130.72 2.22 o 0 0 1 277.27 270.70 7.23 o 1 0 1 287.11 262.10 2.05 o 2 0 1 1080.82 1105.17 9.58 o 3 0 1 61.68 52.22 1.30 o 4 0 1 282.82 285.61 1.62 o 5 0 1 688.36 683.20 8.15 o 6 0 1 7.03 5.83 2.44 o -6 1 1 213.43 220.66 4.74 o -5 1 1 304.65 299.86 3.12 o -4 1 1 14.61 18.74 0.58 o -3 1 1 235.12 218.77 4.29 o -2 1 1 24.32 23.39 0.67 o -1 1 1 407.99 399.51 2.14 o 0 1 1 3758.29 3630.56 62.71 o 1 1 1 560.29 551.90 8.31 o 2 1 1 439.33 440.27 5.99 o 3 1 1 1311.47 1246.62 5.16 o 4 1 1 280.63 268.11 1.68 o 5 1 1 15.18 16.48 0.94 o 6 1 1 108.05 114.49 2.49 o -6 2 1 63.38 68.61 1.64 o -5 2 1 24.32 25.79 0.80 o -4 2 1 285.64 281.10 1.69 o -3 2 1 1343.73 1307.24 39.23 o -2 2 1 92.79 75.74 1.69 o -1 2 1 3095.83 3008.56 17.87 o 0 2 1 4.09 5.33 0.37 o 1 2 1 2148.95 2052.03 15.23 o 2 2 1 16.34 21.39 0.72 o 3 2 1 2773.85 2682.03 16.41 o 4 2 1 24.32 25.92 0.57 o 5 2 1 1093.14 1119.05 12.55 o 6 2 1 11.34 12.65 1.19 o -6 3 1 78.26 84.31 1.36 o -5 3 1 55.92 57.97 1.03 o -4 3 1 92.32 84.78 0.78 o -3 3 1 332.40 344.69 2.46 o -2 3 1 726.62 750.85 7.45 o -1 3 1 14423.27 14174.76 59.87 o 0 3 1 871.08 850.04 4.60 o 1 3 1 25100.45 23454.31 148.33 o 2 3 1 19.09 20.33 0.82 o 3 3 1 65.19 44.58 0.85 o 4 3 1 127.85 121.63 1.10 o 5 3 1 86.93 98.61 1.19 o 6 3 1 43.33 51.82 2.29 o -6 4 1 89.45 93.80 1.45 o -5 4 1 141.13 150.01 1.22 o -4 4 1 93.51 89.91 0.86 o -3 4 1 1448.59 1364.96 7.79 o -2 4 1 1601.40 1520.13 30.30 o -1 4 1 66.42 55.67 0.99 o 0 4 1 11.90 11.76 0.96 o 1 4 1 4476.69 4529.86 20.86 o 2 4 1 2506.32 2468.55 37.38 o 3 4 1 901.15 840.65 10.98 o 4 4 1 60.82 59.61 1.03 o 5 4 1 1210.08 1255.85 16.34 o 6 4 1 4.75 7.24 1.25 o -6 5 1 151.27 160.08 1.69 o -5 5 1 208.76 211.89 2.35 o -4 5 1 248.61 236.65 1.96 o -3 5 1 71.74 77.46 1.40 o -2 5 1 43.26 52.68 0.99 o -1 5 1 1669.08 1619.80 14.87 o 0 5 1 112.55 116.94 1.26 o 1 5 1 960.40 882.63 8.52 o 2 5 1 751.15 806.65 8.02 o 3 5 1 258.28 243.80 3.05 o 4 5 1 216.62 202.70 1.84 o 5 5 1 32.53 32.11 1.18 o 6 5 1 90.29 99.76 1.88 o -6 6 1 35.95 38.74 1.42 o -5 6 1 44.16 50.21 1.18 o -4 6 1 535.32 540.15 4.37 o -3 6 1 418.61 392.92 3.87 o -2 6 1 27.37 29.46 0.66 o -1 6 1 267.81 224.43 2.68 o 0 6 1 57.36 62.54 1.31 o 1 6 1 33.69 35.93 0.80 o 2 6 1 604.34 660.19 6.26 o 3 6 1 829.43 815.02 6.83 o 4 6 1 37.87 38.50 0.97 o 5 6 1 254.39 289.09 2.02 o 6 6 1 3.80 4.75 1.65 o -6 7 1 94.96 97.27 2.65 o -5 7 1 39.01 46.91 1.21 o -4 7 1 16.75 15.93 0.84 o -3 7 1 19.17 15.80 0.62 o -2 7 1 49.95 49.69 0.79 o -1 7 1 2590.52 2699.80 12.13 o 0 7 1 750.43 757.89 3.64 o 1 7 1 2750.54 2757.29 9.47 o 2 7 1 300.51 318.56 4.94 o 3 7 1 395.56 403.09 4.30 o 4 7 1 340.15 322.27 2.55 o 5 7 1 11.93 10.13 1.19 o 6 7 1 22.09 20.93 1.22 o -6 8 1 20.32 17.42 1.13 o -5 8 1 254.85 258.26 2.65 o -4 8 1 30.66 36.38 1.06 o -3 8 1 838.26 827.61 7.94 o -2 8 1 62.75 67.42 1.09 o -1 8 1 843.01 859.02 4.31 o 0 8 1 66.68 75.77 1.26 o 1 8 1 261.71 273.29 2.60 o 2 8 1 154.13 147.78 2.72 o 3 8 1 941.07 940.19 5.08 o 4 8 1 34.63 35.45 1.17 o 5 8 1 948.17 1003.68 6.18 o 6 8 1 3.66 3.53 0.56 o -6 9 1 79.34 65.72 1.48 o -5 9 1 191.27 195.16 2.15 o -4 9 1 41.72 31.75 1.07 o -3 9 1 1.93 2.36 0.80 o -2 9 1 520.08 535.96 4.05 o -1 9 1 600.98 561.70 3.27 o 0 9 1 1665.21 1752.47 11.80 o 1 9 1 2040.32 2076.87 27.64 o 2 9 1 43.21 49.35 0.91 o 3 9 1 423.60 429.91 4.35 o 4 9 1 15.77 23.48 1.17 o 5 9 1 69.31 75.09 1.26 o -5 10 1 154.14 159.66 1.75 o -4 10 1 354.91 349.16 3.01 o -3 10 1 434.07 449.96 3.85 o -2 10 1 28.46 28.32 0.91 o -1 10 1 253.39 247.51 1.64 o 0 10 1 233.87 257.67 2.82 o 1 10 1 14.81 12.83 0.62 o 2 10 1 39.73 45.79 1.09 o 3 10 1 303.39 311.48 2.84 o 4 10 1 247.81 244.90 1.99 o 5 10 1 636.75 707.01 3.37 o -5 11 1 114.20 121.81 3.83 o -4 11 1 304.24 309.68 2.21 o -3 11 1 46.30 44.64 0.92 o -2 11 1 125.59 129.74 1.27 o -1 11 1 962.21 991.72 5.01 o 0 11 1 145.72 135.74 1.66 o 1 11 1 1313.86 1339.80 11.22 o 2 11 1 12.83 18.82 1.14 o 3 11 1 267.40 262.50 2.98 o 4 11 1 102.42 102.90 1.34 o 5 11 1 36.40 35.47 0.89 o -5 12 1 10.38 13.58 0.78 o -4 12 1 117.85 117.01 1.70 o -3 12 1 205.87 203.94 2.89 o -2 12 1 309.27 301.40 2.70 o -1 12 1 421.18 401.24 4.15 o 0 12 1 3.18 3.85 0.85 o 1 12 1 39.80 48.56 0.94 o 2 12 1 146.61 157.90 1.80 o 3 12 1 346.83 350.45 5.91 o 4 12 1 16.70 19.43 0.87 o 5 12 1 219.01 219.74 2.33 o -5 13 1 67.27 61.34 2.87 o -4 13 1 2.47 2.95 0.87 o -3 13 1 5.28 6.59 1.02 o -2 13 1 68.23 72.39 1.23 o -1 13 1 949.03 958.36 4.92 o 0 13 1 392.20 403.23 3.08 o 1 13 1 962.52 944.15 8.21 o 2 13 1 10.71 13.63 1.15 o 3 13 1 43.31 44.67 0.99 o 4 13 1 94.85 103.84 1.65 o -4 14 1 55.38 66.88 1.20 o -3 14 1 314.40 306.44 2.70 o -2 14 1 20.51 22.74 1.05 o -1 14 1 62.74 70.20 1.13 o 0 14 1 63.81 67.50 1.14 o 1 14 1 6.57 5.72 0.95 o 2 14 1 17.82 20.30 1.12 o 3 14 1 461.81 476.84 3.34 o 4 14 1 13.87 15.90 0.83 o -4 15 1 2.16 3.33 0.63 o -3 15 1 6.87 7.65 0.81 o -2 15 1 193.51 179.82 2.32 o -1 15 1 465.98 465.12 2.34 o 0 15 1 82.91 89.49 1.26 o 1 15 1 651.59 646.14 8.27 o 2 15 1 12.83 14.51 0.96 o 3 15 1 89.65 86.37 1.01 o 4 15 1 18.09 17.11 0.69 o -3 16 1 200.78 214.04 2.28 o -2 16 1 121.75 118.07 1.84 o -1 16 1 35.96 35.82 0.93 o 0 16 1 119.97 123.31 1.35 o 1 16 1 32.89 32.63 0.86 o 2 16 1 7.61 8.98 0.77 o 3 16 1 109.39 105.46 1.72 o -3 17 1 10.39 9.94 0.87 o -2 17 1 6.40 6.35 0.68 o -1 17 1 49.03 47.88 0.81 o 0 17 1 518.17 506.17 7.78 o 1 17 1 157.01 158.75 2.48 o 2 17 1 8.22 9.72 0.57 o 3 17 1 73.30 66.72 3.14 o -2 18 1 11.77 11.36 0.87 o -1 18 1 600.21 594.76 3.35 o 0 18 1 1.12 1.98 0.68 o 1 18 1 109.32 115.22 1.39 o 2 18 1 6.62 6.03 0.61 o -1 19 1 379.89 272.10 9.15 o 0 19 1 90.69 64.47 0.65 o 1 19 1 501.99 352.91 11.54 o -6 0 2 715.05 725.04 7.93 o -5 0 2 1329.05 1280.47 10.46 o -4 0 2 7.43 10.12 0.73 o -3 0 2 3.56 8.01 1.44 o -2 0 2 299.51 311.25 7.17 o -1 0 2 466.79 430.41 17.89 o 0 0 2 12850.81 12136.79 82.66 o 1 0 2 3464.95 3310.97 14.95 o 2 0 2 428.72 405.92 3.58 o 3 0 2 989.20 938.10 7.25 o 4 0 2 367.32 380.65 4.07 o 5 0 2 1.62 2.03 1.17 o 6 0 2 39.52 42.69 2.84 o -6 1 2 249.17 252.00 2.49 o -5 1 2 739.38 714.89 6.43 o -4 1 2 18.74 21.26 0.58 o -3 1 2 1928.41 1722.95 9.45 o -2 1 2 312.88 292.11 2.75 o -1 1 2 8452.68 8205.79 36.34 o 0 1 2 8.92 8.86 0.47 o 1 1 2 2278.36 2238.49 27.26 o 2 1 2 47.81 53.31 0.96 o 3 1 2 305.57 291.23 2.01 o 4 1 2 1016.68 994.61 6.33 o 5 1 2 328.33 335.87 5.13 o 6 1 2 94.41 115.24 6.20 o -6 2 2 79.24 82.12 1.37 o -5 2 2 488.80 468.60 3.52 o -4 2 2 8.57 9.54 0.51 o -3 2 2 1.33 3.03 0.96 o -2 2 2 780.27 768.70 6.18 o -1 2 2 548.97 565.62 5.55 o 0 2 2 2988.70 3031.41 22.20 o 1 2 2 9167.94 9072.89 37.95 o 2 2 2 78.33 79.04 0.95 o 3 2 2 523.53 508.95 2.54 o 4 2 2 11.90 15.64 0.67 o 5 2 2 2.67 3.83 0.91 o 6 2 2 77.05 75.30 3.54 o -6 3 2 122.64 122.41 1.73 o -5 3 2 756.06 725.99 4.62 o -4 3 2 111.51 109.52 1.05 o -3 3 2 3479.19 3320.17 20.20 o -2 3 2 72.66 69.33 1.22 o -1 3 2 2914.17 2855.99 14.26 o 0 3 2 666.46 707.12 4.64 o 1 3 2 1377.88 1428.40 8.30 o 2 3 2 48.92 46.39 0.93 o 3 3 2 143.05 132.13 1.44 o 4 3 2 69.82 66.90 0.92 o 5 3 2 673.03 721.93 6.46 o 6 3 2 25.07 24.79 1.02 o -6 4 2 120.76 123.92 1.57 o -5 4 2 344.48 342.67 3.12 o -4 4 2 79.35 85.35 0.87 o -3 4 2 9.48 10.12 0.75 o -2 4 2 597.93 587.20 9.20 o -1 4 2 1117.11 1054.03 17.25 o 0 4 2 75.54 82.78 0.88 o 1 4 2 1989.64 1949.40 12.87 o 2 4 2 662.66 705.88 4.68 o 3 4 2 24.92 24.71 0.87 o 4 4 2 58.87 52.50 0.91 o 5 4 2 7.41 6.91 1.12 o 6 4 2 22.53 20.95 1.16 o -6 5 2 7.35 8.75 1.04 o -5 5 2 410.83 422.45 2.15 o -4 5 2 239.02 227.95 1.44 o -3 5 2 2408.11 2344.41 15.75 o -2 5 2 656.20 723.34 4.57 o -1 5 2 2375.49 2299.32 12.31 o 0 5 2 2177.46 2201.32 15.32 o 1 5 2 63.89 58.86 1.32 o 2 5 2 1546.02 1570.99 9.47 o 3 5 2 493.12 453.62 3.97 o 4 5 2 336.81 334.48 4.24 o 5 5 2 98.73 108.61 1.83 o 6 5 2 152.06 146.36 2.41 o -6 6 2 80.68 86.44 1.31 o -5 6 2 187.25 192.69 1.81 o -4 6 2 58.25 55.04 0.86 o -3 6 2 0.68 0.52 0.55 o -2 6 2 6.50 9.01 0.79 o -1 6 2 3323.01 3388.63 30.93 o 0 6 2 37.67 49.91 0.88 o 1 6 2 2460.44 2405.63 8.47 o 2 6 2 1497.73 1524.69 14.20 o 3 6 2 35.28 30.22 0.72 o 4 6 2 105.70 105.92 1.60 o 5 6 2 29.49 26.66 1.11 o 6 6 2 67.81 50.28 1.28 o -6 7 2 30.87 29.20 1.14 o -5 7 2 385.82 395.77 3.34 o -4 7 2 70.05 71.76 1.11 o -3 7 2 1219.14 1145.27 10.27 o -2 7 2 161.08 153.10 3.34 o -1 7 2 2936.41 2953.28 13.32 o 0 7 2 3.07 2.96 0.45 o 1 7 2 12.01 13.86 0.59 o 2 7 2 269.83 331.27 3.31 o 3 7 2 794.71 788.19 4.67 o 4 7 2 421.43 427.38 3.94 o 5 7 2 452.01 462.35 14.45 o 6 7 2 59.85 47.13 6.46 o -6 8 2 21.84 18.88 1.08 o -5 8 2 1051.70 1099.19 4.98 o -4 8 2 11.60 12.43 1.06 o -3 8 2 51.95 47.20 0.79 o -2 8 2 224.43 262.63 2.55 o -1 8 2 155.10 204.15 2.02 o 0 8 2 193.82 191.92 1.41 o 1 8 2 2713.61 2665.51 17.51 o 2 8 2 32.25 32.10 0.83 o 3 8 2 1749.15 1743.67 18.86 o 4 8 2 40.39 40.93 1.18 o 5 8 2 4.51 6.05 1.04 o -6 9 2 55.19 41.53 1.00 o -5 9 2 728.98 777.31 6.67 o -4 9 2 30.60 33.67 1.15 o -3 9 2 1709.19 1664.78 13.06 o -2 9 2 60.28 60.62 1.12 o -1 9 2 2430.10 2435.52 12.72 o 0 9 2 22.11 19.22 0.64 o 1 9 2 34.78 35.39 0.76 o 2 9 2 244.40 244.86 3.71 o 3 9 2 36.34 38.44 0.93 o 4 9 2 326.97 339.15 5.38 o 5 9 2 250.63 284.27 2.29 o -5 10 2 167.19 187.83 3.81 o -4 10 2 3.93 5.91 1.07 o -3 10 2 0.61 1.40 0.73 o -2 10 2 77.73 89.42 1.16 o -1 10 2 673.60 677.02 4.11 o 0 10 2 159.33 151.39 0.99 o 1 10 2 2145.83 2142.65 16.50 o 2 10 2 18.21 23.13 1.41 o 3 10 2 26.71 28.83 0.89 o 4 10 2 0.33 1.32 1.08 o 5 10 2 1.05 1.47 0.68 o -5 11 2 213.17 238.49 4.71 o -4 11 2 25.05 25.38 1.08 o -3 11 2 511.02 539.54 3.06 o -2 11 2 47.85 49.50 1.01 o -1 11 2 769.33 780.37 5.81 o 0 11 2 83.37 85.94 0.87 o 1 11 2 682.55 694.47 4.81 o 2 11 2 58.08 60.00 1.49 o 3 11 2 161.83 167.18 1.72 o 4 11 2 187.82 190.64 2.12 o 5 11 2 138.54 144.75 1.63 o -5 12 2 243.44 250.43 11.35 o -4 12 2 10.04 10.58 1.04 o -3 12 2 306.32 278.36 3.14 o -2 12 2 4.88 5.98 0.90 o -1 12 2 408.23 405.43 2.97 o 0 12 2 32.62 35.20 0.85 o 1 12 2 320.31 327.32 2.68 o 2 12 2 246.59 246.14 2.05 o 3 12 2 171.47 163.48 2.71 o 4 12 2 29.47 32.02 0.94 o 5 12 2 0.92 1.19 1.27 o -5 13 2 239.63 212.29 6.98 o -4 13 2 19.31 21.55 1.14 o -3 13 2 759.95 718.05 13.42 o -2 13 2 30.48 34.67 0.98 o -1 13 2 1148.88 1165.76 4.72 o 0 13 2 372.14 375.20 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