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Information card for entry 2243966
Preview
| Coordinates | 2243966.cif |
|---|---|
| Structure factors | 2243966.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis{2-[(diisopropylphosphanyl)methyl]quinoline-8-thiolato}palladium(II) bis(hexafluoridoantimonate) dichloromethane monosolvate) |
|---|---|
| Formula | C33 H44 Cl2 F12 N2 P2 Pd2 S2 Sb2 |
| Calculated formula | C33 H44 Cl2 F12 N2 P2 Pd2 S2 Sb2 |
| Title of publication | Crystal structure of a dicationic Pd^II^ dimer containing a 2-[(diisopropylphosphanyl)methyl]quinoline-8-thiolate pincer ligand |
| Authors of publication | Clerc, Arnaud; Saffon-Merceron, Nathalie; Monot, Julien; Martin Vaca, Blanca; Bourissou, Didier |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2022 |
| Journal volume | 78 |
| Journal issue | 1 |
| Pages of publication | 18 - 22 |
| a | 23.5167 ± 0.0019 Å |
| b | 16.1492 ± 0.0014 Å |
| c | 24.0414 ± 0.0018 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 9130.3 ± 1.3 Å3 |
| Cell temperature | 193 ± 2 K |
| Ambient diffraction temperature | 193 ± 2 K |
| Number of distinct elements | 9 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.0959 |
| Residual factor for significantly intense reflections | 0.0458 |
| Weighted residual factors for significantly intense reflections | 0.0928 |
| Weighted residual factors for all reflections included in the refinement | 0.1132 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 271671 (current) | 2022-01-01 | cif/ hkl/ Adding structures of 2243966 via cif-deposit CGI script. |
2243966.cif 2243966.hkl |
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Users of the data should acknowledge the original authors of the
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