#------------------------------------------------------------------------------ #$Date: 2022-01-07 01:08:03 +0200 (Fri, 07 Jan 2022) $ #$Revision: 271903 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/39/2243983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2243983 _cell_angle_alpha 80.147 _cell_angle_beta 81.815 _cell_angle_gamma 85.494 _cell_length_a 9.2401 _cell_length_b 11.3301 _cell_length_c 19.4144 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7206 _cod_data_source_file yk2158MOF2sup3.hkl _cod_data_source_block MOF2 _shelx_title ' 4_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 233.01 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 29.04 56.45 1.66 o 2 0 0 29295.03 30282.40 312.84 o 3 0 0 2722.65 2682.17 32.53 o 4 0 0 960.20 1082.26 15.36 o 5 0 0 747.09 853.38 17.27 o 6 0 0 2412.26 2407.56 29.20 o 7 0 0 232.97 251.33 10.38 o 8 0 0 71.61 67.10 8.63 o 9 0 0 3013.79 3065.08 43.72 o 10 0 0 257.81 259.31 14.69 o 11 0 0 84.63 97.71 23.03 o 12 0 0 924.61 1029.25 86.41 o -12 1 0 1259.12 1289.27 58.78 o -11 1 0 34.80 25.06 12.59 o -10 1 0 259.53 267.10 17.74 o -9 1 0 2600.77 2548.18 48.85 o -8 1 0 111.94 116.11 9.98 o -7 1 0 804.16 803.27 15.61 o -6 1 0 2808.89 2864.55 33.11 o -5 1 0 177.98 133.17 12.54 o -4 1 0 88.94 64.75 4.62 o -3 1 0 10087.56 10333.94 108.55 o -2 1 0 5860.69 5707.01 60.54 o -1 1 0 404.72 549.27 7.60 o 0 1 0 11768.10 11859.34 151.13 o 1 1 0 380.52 421.97 5.15 o 2 1 0 30474.78 33524.24 308.00 o 3 1 0 4019.67 4166.90 45.40 o 4 1 0 606.56 596.92 10.25 o 5 1 0 52.43 83.19 5.94 o 6 1 0 6399.52 6512.23 86.30 o 7 1 0 1211.12 1217.89 20.79 o 8 1 0 51.62 51.21 10.01 o 9 1 0 1933.17 1941.00 31.41 o 10 1 0 265.77 263.05 19.28 o 11 1 0 965.94 1020.77 60.68 o 12 1 0 393.35 433.70 34.84 o -12 2 0 488.73 453.99 30.58 o -11 2 0 371.02 371.53 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16.57 9.59 28.71 o 10 7 0 41.32 48.86 21.24 o 11 7 0 1243.54 1440.70 131.90 o -10 8 0 394.95 330.31 22.09 o -9 8 0 175.52 165.44 15.49 o -8 8 0 745.00 746.38 22.72 o -7 8 0 899.81 873.73 22.47 o -6 8 0 1283.84 1233.91 52.31 o -5 8 0 673.33 614.09 20.50 o -4 8 0 731.09 688.90 24.16 o -3 8 0 187.79 130.29 9.65 o -2 8 0 300.28 324.98 10.80 o -1 8 0 3582.16 3427.20 43.08 o 0 8 0 1162.44 993.02 14.41 o 1 8 0 2.24 2.94 5.00 o 2 8 0 2715.19 2948.47 37.41 o 3 8 0 37.73 37.37 5.22 o 4 8 0 17.76 20.33 14.63 o 5 8 0 3322.11 3384.97 65.88 o 6 8 0 381.37 372.85 22.48 o 7 8 0 36.76 18.79 15.31 o 8 8 0 1077.71 1108.61 40.42 o 9 8 0 90.12 114.89 37.92 o 10 8 0 242.39 236.66 26.99 o 11 8 0 720.26 690.37 40.02 o -9 9 0 424.02 423.79 20.65 o -8 9 0 39.31 61.97 13.58 o -7 9 0 1501.22 1429.62 28.72 o -6 9 0 24.52 19.79 11.18 o -5 9 0 199.28 182.75 13.46 o -4 9 0 2699.56 2558.29 39.04 o -3 9 0 10.86 2.70 8.15 o -2 9 0 941.49 921.17 17.88 o -1 9 0 5091.88 4896.26 52.67 o 0 9 0 110.27 82.68 6.20 o 1 9 0 7.56 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264.83 12.97 o -2 11 0 176.07 168.69 9.83 o -1 11 0 1884.53 1813.20 22.94 o 0 11 0 18.57 31.53 8.42 o 1 11 0 233.34 216.08 11.89 o 2 11 0 631.91 713.13 27.61 o 3 11 0 44.01 59.28 13.73 o 4 11 0 1360.72 1351.43 39.32 o 5 11 0 411.56 466.84 57.70 o 6 11 0 401.90 404.11 37.92 o 7 11 0 376.04 401.94 40.09 o 8 11 0 1066.44 1093.20 66.10 o 9 11 0 40.10 41.18 33.59 o -7 12 0 608.26 530.97 19.98 o -6 12 0 70.57 75.16 12.84 o -5 12 0 133.70 126.14 12.34 o -4 12 0 161.58 102.42 10.96 o -3 12 0 7.78 5.46 9.97 o -2 12 0 1030.40 1012.96 20.57 o -1 12 0 1180.46 1303.27 22.06 o 0 12 0 555.91 553.67 30.98 o 1 12 0 1.68 6.32 15.44 o 2 12 0 978.76 1032.64 34.32 o 3 12 0 59.34 66.94 15.27 o 4 12 0 286.97 366.19 35.22 o 5 12 0 505.91 548.77 43.34 o 6 12 0 137.20 134.36 30.88 o 7 12 0 379.03 367.81 41.72 o 8 12 0 368.72 397.61 44.97 o -6 13 0 36.91 63.61 13.45 o -5 13 0 2.93 -8.75 11.24 o -4 13 0 554.87 572.39 18.84 o -3 13 0 109.71 101.80 11.34 o -2 13 0 145.58 147.49 11.39 o -1 13 0 2413.79 2360.40 41.53 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806.65 57.97 o -7 -11 1 40.98 48.22 28.17 o -6 -11 1 17.23 23.51 16.46 o -5 -11 1 1953.61 1790.72 47.64 o -4 -11 1 10.17 12.48 13.56 o -3 -11 1 39.71 64.69 14.17 o -2 -11 1 2126.00 2160.82 48.43 o -1 -11 1 9.47 5.49 6.84 o 0 -11 1 74.34 56.63 7.07 o 1 -11 1 2324.26 2265.05 26.33 o 2 -11 1 181.82 149.63 8.92 o 3 -11 1 50.35 62.72 10.06 o 4 -11 1 190.43 158.59 12.43 o 5 -11 1 10.51 7.32 10.98 o 6 -11 1 52.53 53.20 12.81 o 7 -11 1 980.00 986.61 27.97 o 8 -11 1 60.12 72.43 17.13 o -9 -10 1 4.34 13.16 22.95 o -8 -10 1 2367.39 2187.22 62.03 o -7 -10 1 5.62 7.07 24.11 o -6 -10 1 0.00 -2.45 14.54 o -5 -10 1 540.43 568.79 42.26 o -4 -10 1 3.93 14.82 12.83 o -3 -10 1 961.92 880.80 29.49 o -2 -10 1 2614.06 2763.33 36.55 o -1 -10 1 110.54 97.20 7.11 o 0 -10 1 50.52 40.19 6.78 o 1 -10 1 1991.21 1838.24 23.96 o 2 -10 1 475.77 453.66 14.55 o 3 -10 1 132.11 140.27 11.76 o 4 -10 1 2592.82 2498.84 35.44 o 5 -10 1 58.76 50.87 10.58 o 6 -10 1 272.43 252.14 14.86 o 7 -10 1 354.61 360.36 17.64 o 8 -10 1 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5 25 270.82 295.39 30.79 o 2 5 25 138.03 179.77 43.34 o 3 5 25 439.08 461.85 35.41 o 4 5 25 245.28 246.59 45.48 o 5 5 25 905.80 984.04 51.50 o -1 6 25 500.09 536.40 49.30 o 0 6 25 9.45 -7.87 24.11 o 1 6 25 760.27 759.29 40.94 o 2 6 25 827.91 893.97 46.62 o 3 6 25 50.81 79.89 27.30 o 4 6 25 37.25 25.40 26.46 o 5 6 25 135.56 131.89 29.38 o -1 7 25 534.70 538.47 55.80 o 0 7 25 28.97 11.98 24.72 o 1 7 25 735.65 778.30 46.29 o 2 7 25 118.57 105.11 27.13 o 3 7 25 13.66 -15.28 25.11 o 4 7 25 1381.20 1627.06 61.22 o 1 8 25 479.08 450.62 35.86 o 2 8 25 135.44 112.14 41.72 o 3 8 25 13.28 29.26 42.80 o 1 -1 26 2.43 1.02 27.90 o 2 -1 26 1902.77 2030.83 64.74 o 3 -1 26 4.76 14.63 37.38 o 0 0 26 66.57 56.86 23.28 o 1 0 26 2.67 -9.64 22.99 o 2 0 26 1329.57 1365.87 52.24 o 3 0 26 4.54 1.96 23.81 o 4 0 26 402.09 440.64 69.89 o -1 1 26 716.27 808.92 41.94 o 0 1 26 123.45 107.60 38.47 o 1 1 26 72.85 74.68 24.37 o 2 1 26 1192.68 1141.86 49.97 o 3 1 26 147.58 131.20 27.13 o 4 1 26 99.66 100.73 27.23 o -1 2 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