#------------------------------------------------------------------------------ #$Date: 2022-11-08 21:23:43 +0200 (Tue, 08 Nov 2022) $ #$Revision: 279108 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/42/2244208.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244208 _cell_angle_alpha 90.000 _cell_angle_beta 96.825 _cell_angle_gamma 90.000 _cell_length_a 18.7990 _cell_length_b 11.3033 _cell_length_c 15.8639 _exptl_crystal_F_000 1320.00 _reflns_d_resolution_high 0.7836 _cod_data_source_file hb80362sup3.hkl _cod_data_source_block 2 _shelx_title ' 3pic1_auto_a.res in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.61 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 36105.20 29398.34 141.15 o 4 0 0 2320.82 2385.44 20.12 o 6 0 0 1667.10 2201.47 39.04 o 8 0 0 2333.04 1778.29 27.52 o 10 0 0 4445.42 3664.35 34.14 o 12 0 0 1965.64 1684.18 10.00 o 14 0 0 14668.11 14048.81 88.76 o 16 0 0 482.16 414.33 5.42 o 18 0 0 2452.95 2268.43 17.39 o 20 0 0 123.22 153.60 2.78 o 22 0 0 113.95 131.49 3.60 o 1 1 0 86.63 8.16 0.26 o 3 1 0 34.49 32.34 0.73 o 5 1 0 42703.29 41751.12 142.77 o 7 1 0 2605.06 2758.45 26.99 o 9 1 0 770.17 615.35 9.93 o 11 1 0 1289.14 1750.23 27.62 o 13 1 0 5.63 1.49 1.04 o 15 1 0 11.14 4.71 0.63 o 17 1 0 9.06 2.47 0.71 o 19 1 0 58.79 70.81 1.12 o 21 1 0 244.65 186.78 2.42 o 23 1 0 1.20 2.70 0.69 o 0 2 0 729.81 724.63 17.16 o 2 2 0 1592.64 2074.34 8.21 o 4 2 0 39348.08 34468.73 263.66 o 6 2 0 4790.26 6058.12 35.80 o 8 2 0 1410.77 1116.75 11.88 o 10 2 0 9212.13 9045.79 42.60 o 12 2 0 18.82 28.62 1.48 o 14 2 0 11981.03 11381.20 116.91 o 16 2 0 21.72 31.97 1.24 o 18 2 0 812.80 819.11 8.22 o 20 2 0 187.54 177.75 2.11 o 22 2 0 75.62 95.78 2.46 o 1 3 0 3784.61 2596.93 22.11 o 3 3 0 1370.94 1381.18 8.79 o 5 3 0 4240.55 4623.50 19.97 o 7 3 0 7.21 1.88 0.76 o 9 3 0 3029.03 2914.64 17.60 o 11 3 0 274.43 320.60 2.74 o 13 3 0 0.06 0.27 1.01 o 15 3 0 0.04 0.06 0.61 o 17 3 0 49.01 50.29 1.02 o 19 3 0 24.99 25.12 1.03 o 21 3 0 94.67 119.62 2.24 o 23 3 0 46.44 34.00 3.11 o 0 4 0 23260.75 26096.57 131.90 o 2 4 0 398.42 410.64 5.17 o 4 4 0 3984.64 3412.77 19.47 o 6 4 0 2467.46 2836.77 21.27 o 8 4 0 6097.65 6140.10 55.16 o 10 4 0 18494.57 17959.25 165.63 o 12 4 0 1405.72 1488.01 22.79 o 14 4 0 5690.15 5646.46 25.68 o 16 4 0 1226.55 1173.37 9.46 o 18 4 0 5.95 8.17 0.91 o 20 4 0 27.77 30.22 1.11 o 22 4 0 118.79 123.04 3.17 o 1 5 0 237.35 179.88 2.21 o 3 5 0 831.22 906.55 5.07 o 5 5 0 268.62 271.35 4.18 o 7 5 0 417.08 344.34 6.71 o 9 5 0 181.21 154.38 2.13 o 11 5 0 8.06 4.60 1.12 o 13 5 0 1.52 5.39 0.59 o 15 5 0 12.05 18.92 1.20 o 17 5 0 24.32 23.17 1.07 o 19 5 0 1.21 1.31 0.89 o 21 5 0 3.40 3.64 0.78 o 0 6 0 31387.47 31935.14 320.09 o 2 6 0 1.54 2.64 1.04 o 4 6 0 1353.84 1391.93 9.86 o 6 6 0 60.00 28.84 0.90 o 8 6 0 483.42 479.71 4.01 o 10 6 0 3009.68 2996.13 29.40 o 12 6 0 451.32 378.27 3.27 o 14 6 0 4668.35 4427.08 35.00 o 16 6 0 326.61 402.82 3.39 o 18 6 0 1038.60 1089.19 11.63 o 20 6 0 151.57 158.98 2.31 o 1 7 0 337.85 291.40 3.23 o 3 7 0 159.89 167.05 1.91 o 5 7 0 0.85 5.40 0.65 o 7 7 0 1141.52 1277.66 10.26 o 9 7 0 1569.59 1549.52 10.59 o 11 7 0 44.88 47.79 0.94 o 13 7 0 96.78 99.42 1.21 o 15 7 0 0.09 2.80 0.86 o 17 7 0 24.14 22.53 1.04 o 19 7 0 0.08 2.51 0.76 o 0 8 0 13015.56 12469.53 49.10 o 2 8 0 1462.75 1688.33 23.57 o 4 8 0 4942.74 5119.58 25.55 o 6 8 0 92.34 107.51 2.72 o 8 8 0 197.38 200.92 1.48 o 10 8 0 629.41 570.88 2.54 o 12 8 0 14.36 16.62 0.78 o 14 8 0 5662.22 5804.05 35.89 o 16 8 0 174.12 161.58 1.85 o 18 8 0 406.74 415.23 8.84 o 1 9 0 402.03 417.63 5.77 o 3 9 0 289.86 315.01 6.57 o 5 9 0 676.48 647.37 4.18 o 7 9 0 496.44 469.04 3.63 o 9 9 0 420.55 399.99 2.79 o 11 9 0 2.84 8.13 0.70 o 13 9 0 211.23 222.91 1.80 o 15 9 0 41.25 46.55 1.37 o 17 9 0 12.23 8.38 0.61 o 0 10 0 11676.09 11654.90 82.55 o 2 10 0 35.37 70.38 2.95 o 4 10 0 196.98 220.94 2.75 o 6 10 0 869.26 879.19 6.00 o 8 10 0 1558.12 1760.06 7.65 o 10 10 0 1860.05 1742.22 10.45 o 12 10 0 1.81 1.38 0.61 o 14 10 0 1904.11 1997.19 30.38 o 16 10 0 2.61 1.83 1.22 o 1 11 0 0.58 1.33 0.90 o 3 11 0 5.17 5.56 1.07 o 5 11 0 5.57 11.19 0.72 o 7 11 0 18.33 31.63 1.56 o 9 11 0 192.36 227.97 3.43 o 11 11 0 19.33 28.67 0.82 o 13 11 0 20.40 14.73 0.76 o 15 11 0 0.02 -0.37 0.85 o 0 12 0 178.68 162.59 2.62 o 2 12 0 26.54 24.45 0.92 o 4 12 0 1342.80 1417.99 11.66 o 6 12 0 536.78 581.86 3.29 o 8 12 0 516.39 543.72 5.01 o 10 12 0 1493.08 1413.81 25.49 o 12 12 0 82.13 61.96 1.53 o 1 13 0 0.72 1.06 0.57 o 3 13 0 30.86 27.79 1.05 o 5 13 0 83.39 75.74 1.56 o 7 13 0 47.76 40.86 1.04 o 9 13 0 44.87 48.11 1.04 o 0 14 0 2465.26 2272.76 27.31 o 2 14 0 257.40 270.63 5.98 o 4 14 0 211.14 202.83 1.87 o -23 1 1 1747.82 1821.82 11.55 o -21 1 1 68.68 49.77 1.27 o -19 1 1 1114.71 1147.48 4.73 o -17 1 1 389.90 367.90 3.85 o -15 1 1 582.90 650.97 4.20 o -13 1 1 8235.04 8209.71 80.93 o -11 1 1 1191.45 1577.00 10.46 o -9 1 1 1992.26 2371.46 17.53 o -7 1 1 86.23 55.15 3.13 o -5 1 1 9871.15 8435.57 89.16 o -3 1 1 15295.99 17368.87 84.85 o -1 1 1 18517.01 22006.43 193.87 o 1 1 1 57724.49 52797.87 195.20 o 3 1 1 1836.76 2370.37 46.72 o 5 1 1 3017.70 2678.23 29.24 o 7 1 1 604.67 805.37 6.08 o 9 1 1 1075.13 1028.70 15.87 o 11 1 1 3886.05 3823.21 51.88 o 13 1 1 935.21 886.25 7.29 o 15 1 1 12134.50 12219.84 32.03 o 17 1 1 181.52 188.69 1.71 o 19 1 1 1057.83 1051.59 9.79 o 21 1 1 7.48 7.43 0.76 o 23 1 1 219.64 203.84 2.67 o -22 2 1 147.97 141.94 3.10 o -20 2 1 138.92 178.08 1.76 o -18 2 1 26.40 30.34 0.94 o -16 2 1 79.88 66.06 1.08 o -14 2 1 143.83 153.24 2.41 o -12 2 1 91.82 66.79 1.32 o -10 2 1 541.98 583.61 11.98 o -8 2 1 1597.75 1809.83 20.15 o -6 2 1 0.49 2.11 0.59 o -4 2 1 37398.82 36983.60 170.52 o -2 2 1 117.25 104.74 1.16 o 0 2 1 2776.20 1437.68 6.27 o 2 2 1 55.86 36.04 1.17 o 4 2 1 1156.59 1126.98 7.04 o 6 2 1 3844.45 3578.90 11.99 o 8 2 1 2568.39 3123.06 16.37 o 10 2 1 759.67 1045.06 7.97 o 12 2 1 28.50 15.57 1.18 o 14 2 1 234.72 223.27 3.15 o 16 2 1 6.97 7.86 0.66 o 18 2 1 51.73 45.66 1.20 o 20 2 1 20.31 12.79 0.90 o 22 2 1 169.44 173.30 2.88 o -21 3 1 53.46 56.17 1.43 o -19 3 1 183.76 217.70 2.00 o -17 3 1 227.42 222.46 3.09 o -15 3 1 309.01 338.53 2.03 o -13 3 1 6342.78 6539.24 27.38 o -11 3 1 143.06 145.72 7.30 o -9 3 1 36304.58 36854.66 177.10 o -7 3 1 783.10 906.99 7.59 o -5 3 1 545.16 378.84 2.99 o -3 3 1 1995.24 1571.18 15.48 o -1 3 1 1001.62 1303.68 4.66 o 1 3 1 42130.04 41077.63 290.26 o 3 3 1 1677.38 1733.65 11.16 o 5 3 1 28442.79 28056.46 73.85 o 7 3 1 3595.86 3174.95 36.52 o 9 3 1 6215.42 6800.76 58.03 o 11 3 1 2363.83 2328.62 27.70 o 13 3 1 594.49 515.39 7.05 o 15 3 1 7276.80 7455.93 21.85 o 17 3 1 863.14 856.13 6.72 o 19 3 1 755.59 775.35 12.37 o 21 3 1 78.70 93.84 1.70 o -22 4 1 69.94 82.07 2.68 o -20 4 1 76.31 84.82 2.27 o -18 4 1 142.46 156.65 2.03 o -16 4 1 7.23 4.59 0.71 o -14 4 1 31.67 33.25 0.91 o -12 4 1 60.02 39.77 1.34 o -10 4 1 261.87 314.14 6.49 o -8 4 1 6008.65 5999.40 56.16 o -6 4 1 1677.51 1498.72 10.18 o -4 4 1 1733.65 1948.71 7.38 o -2 4 1 552.64 653.70 5.99 o 0 4 1 1405.81 1095.39 6.10 o 2 4 1 1689.89 1463.30 13.06 o 4 4 1 1068.16 1489.72 20.21 o 6 4 1 944.57 941.89 10.04 o 8 4 1 280.88 271.69 9.51 o 10 4 1 5.75 2.42 0.74 o 12 4 1 150.99 126.53 3.13 o 14 4 1 77.59 108.09 1.47 o 16 4 1 98.03 118.16 1.69 o 18 4 1 111.65 110.09 1.87 o 20 4 1 51.01 61.00 1.89 o 22 4 1 13.82 15.34 1.04 o -21 5 1 14.74 17.55 1.12 o -19 5 1 184.16 219.04 2.41 o -17 5 1 623.31 604.24 5.04 o -15 5 1 40.81 34.25 1.97 o -13 5 1 24250.29 24100.17 71.43 o -11 5 1 3090.34 2886.82 30.21 o -9 5 1 6996.54 7037.28 44.43 o -7 5 1 1279.82 1169.88 11.28 o -5 5 1 9565.82 8807.01 45.23 o -3 5 1 506.70 274.15 3.14 o -1 5 1 27.07 39.74 2.58 o 1 5 1 28481.36 26710.51 149.37 o 3 5 1 2081.06 2645.29 28.61 o 5 5 1 14565.24 14890.39 87.07 o 7 5 1 364.24 469.59 8.49 o 9 5 1 7956.15 7741.98 68.24 o 11 5 1 5247.23 5393.97 58.67 o 13 5 1 1147.95 996.09 7.70 o 15 5 1 677.13 730.19 4.50 o 17 5 1 30.28 41.48 1.19 o 19 5 1 987.40 987.50 6.05 o 21 5 1 61.33 68.03 6.34 o -20 6 1 26.75 14.83 1.14 o -18 6 1 72.02 79.84 1.54 o -16 6 1 14.56 8.52 0.87 o -14 6 1 28.86 15.49 0.83 o -12 6 1 68.65 104.17 2.52 o -10 6 1 111.92 157.00 2.45 o -8 6 1 326.08 370.72 2.69 o -6 6 1 2997.15 3491.89 25.07 o -4 6 1 214.33 268.55 3.50 o -2 6 1 71.77 100.85 3.47 o 0 6 1 41.27 34.92 1.54 o 2 6 1 337.35 397.00 4.66 o 4 6 1 1544.27 1727.08 11.31 o 6 6 1 1.66 0.88 0.66 o 8 6 1 699.57 630.70 7.41 o 10 6 1 172.49 236.92 2.65 o 12 6 1 249.60 261.70 1.96 o 14 6 1 166.89 134.05 3.47 o 16 6 1 50.96 63.34 1.66 o 18 6 1 21.03 19.21 1.15 o 20 6 1 100.72 104.73 2.06 o -19 7 1 929.19 969.82 6.35 o -17 7 1 2083.45 2103.14 27.02 o -15 7 1 743.31 709.44 8.16 o -13 7 1 262.68 324.50 2.68 o -11 7 1 2239.94 2246.04 15.66 o -9 7 1 5483.49 5359.87 27.67 o -7 7 1 288.91 294.31 5.05 o -5 7 1 1749.21 1707.86 11.41 o -3 7 1 3314.64 3033.34 23.10 o -1 7 1 4253.91 4583.71 44.80 o 1 7 1 23802.66 24456.13 106.28 o 3 7 1 39.33 75.85 3.66 o 5 7 1 1196.77 781.37 4.39 o 7 7 1 225.88 171.15 2.34 o 9 7 1 60.81 79.27 0.96 o 11 7 1 297.33 308.96 2.87 o 13 7 1 1918.13 1831.61 12.32 o 15 7 1 9936.34 10164.42 60.94 o 17 7 1 1.55 1.31 0.85 o 19 7 1 387.46 412.78 5.37 o -18 8 1 54.90 54.01 1.75 o -16 8 1 0.06 0.78 0.78 o -14 8 1 0.41 2.29 0.78 o -12 8 1 231.26 267.99 1.96 o -10 8 1 219.13 187.51 1.33 o -8 8 1 801.78 810.80 5.51 o -6 8 1 597.11 641.83 9.22 o -4 8 1 139.09 183.91 1.95 o -2 8 1 307.40 312.01 9.61 o 0 8 1 60.57 63.62 1.66 o 2 8 1 160.49 144.82 2.62 o 4 8 1 883.74 903.06 5.63 o 6 8 1 191.95 234.36 1.87 o 8 8 1 702.59 769.22 5.24 o 10 8 1 27.77 16.67 1.04 o 12 8 1 0.10 1.12 0.70 o 14 8 1 77.25 93.23 1.44 o 16 8 1 0.35 0.42 1.00 o 18 8 1 13.06 6.48 0.73 o -17 9 1 49.52 62.29 1.43 o -15 9 1 80.19 86.39 1.58 o -13 9 1 2670.40 2672.32 16.01 o -11 9 1 33.97 53.66 1.37 o -9 9 1 2571.57 2730.78 9.67 o -7 9 1 0.25 1.97 0.64 o -5 9 1 749.33 733.38 4.73 o -3 9 1 3251.06 3229.87 22.19 o -1 9 1 6050.22 6263.20 65.34 o 1 9 1 13076.70 13981.88 87.11 o 3 9 1 254.88 272.68 6.22 o 5 9 1 537.42 580.61 4.46 o 7 9 1 10.58 10.03 1.14 o 9 9 1 1672.69 1790.41 11.07 o 11 9 1 765.72 802.36 3.44 o 13 9 1 0.01 1.04 0.62 o 15 9 1 2195.22 2314.83 54.42 o 17 9 1 53.94 43.34 1.28 o -16 10 1 23.98 32.68 1.29 o -14 10 1 17.25 16.68 0.69 o -12 10 1 21.51 33.03 0.98 o -10 10 1 24.60 50.01 0.98 o -8 10 1 248.62 253.92 1.87 o -6 10 1 745.69 710.44 6.13 o -4 10 1 2.93 11.23 0.90 o -2 10 1 5.34 11.36 0.94 o 0 10 1 49.26 52.19 1.38 o 2 10 1 36.86 52.98 1.29 o 4 10 1 288.54 277.64 2.25 o 6 10 1 39.60 40.29 1.03 o 8 10 1 17.68 14.07 0.76 o 10 10 1 549.26 462.03 3.78 o 12 10 1 16.22 20.10 0.71 o 14 10 1 66.83 71.67 1.80 o 16 10 1 1.59 1.54 0.61 o -15 11 1 46.75 25.00 1.34 o -13 11 1 2267.77 2313.56 36.14 o -11 11 1 166.77 142.52 1.28 o -9 11 1 1683.25 1639.54 10.23 o -7 11 1 248.81 225.85 2.47 o -5 11 1 300.52 331.80 2.13 o -3 11 1 380.75 382.08 2.73 o -1 11 1 1520.45 1599.51 7.03 o 1 11 1 1221.00 1329.18 9.25 o 3 11 1 564.54 539.82 8.01 o 5 11 1 3591.03 3623.83 21.27 o 7 11 1 529.16 474.64 4.45 o 9 11 1 1512.50 1491.38 12.18 o 11 11 1 965.84 1016.42 8.45 o 13 11 1 3.95 5.39 0.63 o 15 11 1 371.32 339.49 4.15 o -12 12 1 11.17 22.68 1.25 o -10 12 1 2.45 1.11 0.58 o -8 12 1 76.24 78.26 1.05 o -6 12 1 103.60 121.34 1.78 o -4 12 1 442.02 473.12 2.93 o -2 12 1 37.16 30.78 1.21 o 0 12 1 13.80 23.30 0.98 o 2 12 1 18.52 15.50 0.83 o 4 12 1 29.12 30.86 1.00 o 6 12 1 49.87 64.30 1.09 o 8 12 1 25.23 17.89 0.95 o 10 12 1 8.44 6.18 0.62 o 12 12 1 75.99 70.79 1.77 o -9 13 1 1117.25 1019.62 9.44 o -7 13 1 90.66 86.24 1.73 o -5 13 1 198.33 191.04 1.63 o -3 13 1 218.56 236.27 1.53 o -1 13 1 486.17 469.86 4.95 o 1 13 1 2430.79 2506.73 14.92 o 3 13 1 0.13 2.12 0.60 o 5 13 1 336.83 426.91 7.86 o 7 13 1 30.78 36.93 1.36 o 9 13 1 205.45 195.10 4.89 o -4 14 1 136.81 114.21 1.42 o -2 14 1 45.48 41.61 1.53 o 0 14 1 100.17 82.39 3.05 o 2 14 1 0.98 1.33 0.48 o 4 14 1 0.07 0.20 0.55 o -22 0 2 2838.24 2850.98 17.16 o -20 0 2 73.29 79.69 1.77 o -18 0 2 4486.89 4407.31 19.77 o -16 0 2 1.11 8.29 1.51 o -14 0 2 329.08 280.87 3.58 o -12 0 2 3617.94 2929.67 14.10 o -10 0 2 22.38 4.93 2.14 o -8 0 2 41726.76 39700.71 254.99 o -6 0 2 2010.51 1585.59 11.08 o -4 0 2 93800.30 103997.42 355.35 o -2 0 2 58731.22 54926.28 490.36 o 0 0 2 13759.04 12191.97 153.28 o 4 0 2 28249.01 29343.40 209.38 o 6 0 2 9051.69 10535.77 75.21 o 8 0 2 20231.47 21244.38 188.43 o 10 0 2 5132.26 4230.06 56.92 o 12 0 2 3310.92 3337.98 24.22 o 14 0 2 5391.96 5544.58 47.74 o 16 0 2 7303.73 7335.62 33.84 o 18 0 2 908.03 891.14 6.97 o 20 0 2 526.04 556.50 7.23 o 22 0 2 132.35 118.37 2.46 o -23 1 2 61.65 63.43 1.77 o -21 1 2 1.33 2.64 0.75 o -19 1 2 183.41 186.08 2.73 o -17 1 2 0.21 0.77 0.72 o -15 1 2 35.09 29.79 0.84 o -13 1 2 4.37 7.69 0.84 o -11 1 2 22.28 9.60 0.71 o -9 1 2 4409.04 5195.97 42.22 o -7 1 2 2156.84 1884.50 9.53 o -5 1 2 1026.47 771.60 4.95 o -3 1 2 107.19 82.05 1.10 o -1 1 2 80.09 18.17 0.92 o 1 1 2 497.10 177.38 1.30 o 3 1 2 3605.64 2366.48 12.55 o 5 1 2 66.81 32.83 0.85 o 7 1 2 3532.02 3492.90 25.45 o 9 1 2 182.19 377.37 6.78 o 11 1 2 0.02 23.80 1.09 o 13 1 2 665.81 689.87 6.28 o 15 1 2 40.05 51.62 0.94 o 17 1 2 14.45 14.92 0.82 o 19 1 2 17.19 8.48 0.91 o 21 1 2 5.97 7.50 0.78 o 23 1 2 1.94 0.12 0.60 o -22 2 2 2534.26 2690.61 33.35 o -20 2 2 2.41 2.15 0.64 o -18 2 2 1512.22 1583.47 7.25 o -16 2 2 5.77 4.37 0.67 o -14 2 2 1187.83 1136.06 11.82 o -12 2 2 9555.32 8992.07 40.11 o -10 2 2 18.12 7.31 1.83 o -8 2 2 21595.57 20401.24 85.78 o -6 2 2 4.49 7.10 0.83 o -4 2 2 126.62 38.08 1.29 o -2 2 2 17139.02 21299.49 126.40 o 0 2 2 16581.42 18937.61 257.71 o 2 2 2 124332.40 119035.45 561.48 o 4 2 2 6048.67 5968.61 42.65 o 6 2 2 10041.83 9920.26 44.88 o 8 2 2 756.57 873.61 6.85 o 10 2 2 9395.46 9528.64 72.73 o 12 2 2 366.55 371.23 13.03 o 14 2 2 432.52 501.72 2.65 o 16 2 2 5495.43 5104.94 12.17 o 18 2 2 24.82 26.71 1.03 o 20 2 2 1469.90 1446.41 14.30 o 22 2 2 71.26 58.17 1.39 o -23 3 2 16.56 18.01 1.22 o -21 3 2 130.69 95.57 1.79 o -19 3 2 111.14 99.23 1.29 o -17 3 2 135.48 132.38 1.51 o -15 3 2 178.06 189.87 1.64 o -13 3 2 8.82 7.79 0.82 o -11 3 2 1.85 1.45 0.58 o -9 3 2 917.53 902.78 8.88 o -7 3 2 2448.03 2812.84 14.03 o -5 3 2 4096.19 4015.87 32.15 o -3 3 2 1328.84 1066.22 8.11 o -1 3 2 906.50 824.54 8.34 o 1 3 2 932.23 759.82 6.59 o 3 3 2 1664.22 1202.45 6.61 o 5 3 2 12.21 7.37 0.93 o 7 3 2 544.46 623.10 5.29 o 9 3 2 1017.79 1013.74 13.95 o 11 3 2 660.31 602.41 5.51 o 13 3 2 183.85 168.35 2.82 o 15 3 2 140.60 157.19 1.34 o 17 3 2 25.74 34.24 1.03 o 19 3 2 4.72 7.62 1.03 o 21 3 2 23.32 18.02 1.05 o -22 4 2 824.93 837.84 11.77 o -20 4 2 336.27 333.50 3.02 o -18 4 2 277.59 249.15 3.60 o -16 4 2 32.31 47.91 1.45 o -14 4 2 6495.02 6386.30 24.67 o -12 4 2 16699.75 16113.17 50.99 o -10 4 2 1195.76 1384.23 15.57 o -8 4 2 14628.92 14536.78 139.69 o -6 4 2 122.38 159.86 4.44 o -4 4 2 1542.41 1485.80 14.04 o -2 4 2 398.32 769.35 4.55 o 0 4 2 2528.51 2683.84 31.34 o 2 4 2 52867.65 51444.30 398.19 o 4 4 2 10072.50 10048.70 101.63 o 6 4 2 17209.10 17371.37 175.08 o 8 4 2 15.58 36.25 6.78 o 10 4 2 6334.31 5895.10 54.08 o 12 4 2 245.07 301.44 19.99 o 14 4 2 134.30 126.88 1.67 o 16 4 2 2025.16 2101.68 9.95 o 18 4 2 16.30 8.65 1.00 o 20 4 2 927.60 907.64 10.78 o 22 4 2 2.07 1.92 0.64 o -21 5 2 56.15 58.45 2.38 o -19 5 2 68.78 72.80 1.52 o -17 5 2 39.60 54.84 1.40 o -15 5 2 0.49 2.66 0.67 o -13 5 2 73.80 109.86 1.69 o -11 5 2 12.91 12.48 1.11 o -9 5 2 8.73 11.50 0.73 o -7 5 2 863.47 1093.19 8.84 o -5 5 2 229.53 201.17 2.59 o -3 5 2 7.68 1.90 0.93 o -1 5 2 22.92 28.51 1.11 o 1 5 2 928.13 884.35 9.94 o 3 5 2 67.85 56.78 1.40 o 5 5 2 227.79 121.84 2.38 o 7 5 2 152.05 190.68 2.22 o 9 5 2 21.81 17.09 1.44 o 11 5 2 0.87 2.85 1.20 o 13 5 2 36.79 14.40 0.86 o 15 5 2 313.83 361.57 3.55 o 17 5 2 1.20 2.19 0.85 o 19 5 2 15.04 17.81 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