#------------------------------------------------------------------------------ #$Date: 2023-03-14 05:11:18 +0200 (Tue, 14 Mar 2023) $ #$Revision: 281861 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/42/2244224.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244224 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 27.7071 _cell_length_b 27.7071 _cell_length_c 9.4575 _exptl_crystal_F_000 2880.00 _reflns_d_resolution_high 0.7851 _cod_data_source_file pk2679IIsup3.hkl _cod_data_source_block II _shelx_title ' MH271_3 I -4 R = 0.05 New: I41/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 445.36 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+3/4, x+1/4, z+1/4' '-x+1/2, -y, z+1/2' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-y+5/4, x+3/4, z+3/4' '-x+1, -y+1/2, z+1' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'y-3/4, -x-1/4, -z-1/4' 'x-1/2, y, -z-1/2' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'y-1/4, -x+1/4, -z+1/4' 'x, y+1/2, -z' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 4 0 18825.30 15705.63 149.46 o 0 4 0 2970.03 3088.96 62.07 o 2 4 0 20218.97 19232.21 116.10 o 4 4 0 72322.49 70283.66 574.24 o -4 6 0 9806.85 8915.34 83.01 o -2 6 0 106727.13 106094.21 1650.11 o 0 6 0 65502.14 60038.18 523.40 o 2 6 0 74919.70 72792.73 565.98 o 4 6 0 198344.86 194826.61 307.43 o 6 6 0 1126.18 880.83 34.06 o -6 8 0 487.52 593.75 41.04 o -4 8 0 11330.42 11572.03 111.44 o -2 8 0 24493.83 23605.96 133.30 o 0 8 0 285.81 353.54 30.16 o 2 8 0 53008.09 52334.73 132.95 o 4 8 0 41753.31 40033.38 255.21 o 6 8 0 1585.36 1401.98 46.16 o 8 8 0 1.77 4.01 22.56 o -8 10 0 115.17 117.58 30.70 o -6 10 0 7067.78 6355.80 59.42 o -4 10 0 930.70 1106.91 32.85 o -2 10 0 2349.56 2454.12 29.14 o 0 10 0 582.77 465.22 29.22 o 2 10 0 14095.29 13742.31 84.35 o 4 10 0 72830.79 70837.92 1029.28 o 6 10 0 1019.21 1123.13 41.97 o 8 10 0 16695.77 15797.96 187.05 o 10 10 0 2635.89 2934.04 38.17 o -10 12 0 32.55 37.84 26.30 o -8 12 0 653.22 572.65 25.75 o -6 12 0 5839.45 6230.43 52.13 o -4 12 0 1633.23 1658.62 26.72 o -2 12 0 736.15 675.84 24.67 o 0 12 0 15356.82 15365.10 91.50 o 2 12 0 7989.00 8437.92 61.39 o 4 12 0 3193.04 3380.70 38.68 o 6 12 0 1168.02 1009.90 45.44 o 8 12 0 1523.26 1475.29 42.28 o 10 12 0 1649.83 1602.08 26.02 o 12 12 0 1422.91 1738.69 23.22 o -12 14 0 376.58 400.10 24.93 o -10 14 0 1484.45 1406.69 49.72 o -8 14 0 1005.14 934.63 25.98 o -6 14 0 38.45 45.24 23.31 o -4 14 0 312.90 238.87 23.92 o -2 14 0 12663.11 12950.33 132.50 o 0 14 0 204.37 261.54 30.00 o 2 14 0 1233.44 1434.09 58.80 o 4 14 0 1986.42 2131.43 33.70 o 6 14 0 321.23 377.93 28.21 o 8 14 0 2633.62 2575.72 59.05 o 10 14 0 521.67 777.17 33.06 o 12 14 0 1440.61 1303.84 21.56 o 14 14 0 1905.11 1805.54 39.10 o -14 16 0 2871.15 2947.64 44.13 o -12 16 0 3721.84 3961.01 45.71 o -10 16 0 193.57 176.35 70.11 o -8 16 0 1695.40 1781.85 52.09 o -6 16 0 725.44 750.99 22.88 o -4 16 0 20848.42 22099.87 161.17 o -2 16 0 11592.62 11646.60 122.44 o 0 16 0 4664.67 4534.35 67.44 o 2 16 0 8152.49 9168.64 154.54 o 4 16 0 2101.05 2368.76 34.20 o 6 16 0 78.86 41.11 23.97 o 8 16 0 2252.46 2471.15 35.30 o 10 16 0 201.47 162.89 22.16 o 12 16 0 228.16 286.23 21.35 o 14 16 0 1293.46 1182.75 23.97 o 16 16 0 5055.08 5269.22 55.11 o -16 18 0 6902.98 7443.89 89.43 o -14 18 0 2833.24 2819.22 61.00 o -12 18 0 759.83 643.68 30.03 o -10 18 0 1040.06 1065.05 28.33 o -8 18 0 55.64 74.10 21.93 o -6 18 0 131.59 155.75 23.90 o -4 18 0 171.16 186.11 20.43 o -2 18 0 6834.79 7269.38 120.05 o 0 18 0 6191.31 6425.09 87.43 o 2 18 0 5553.57 6339.71 70.21 o 4 18 0 419.30 418.34 37.88 o 6 18 0 17.23 20.60 25.75 o 8 18 0 1053.24 992.99 33.04 o 10 18 0 83.31 94.16 21.66 o 12 18 0 0.00 -32.49 22.37 o 14 18 0 170.73 233.06 24.60 o 16 18 0 9622.02 10123.98 120.75 o 18 18 0 15.45 6.31 20.72 o -18 20 0 169.58 165.70 23.97 o -16 20 0 23.21 -3.16 20.52 o -14 20 0 34.91 2.79 24.65 o -12 20 0 3.65 7.41 31.19 o -10 20 0 4997.49 5355.83 151.70 o -8 20 0 7383.47 7371.06 184.64 o -6 20 0 3385.89 3607.81 54.53 o -4 20 0 348.79 373.90 47.21 o -2 20 0 70.15 101.08 22.86 o 0 20 0 2007.46 2002.74 49.48 o 2 20 0 423.25 476.19 26.92 o 4 20 0 2515.86 2436.37 410.87 o 6 20 0 320.60 364.44 31.33 o 8 20 0 34.88 23.45 24.31 o 10 20 0 599.88 741.59 26.89 o 12 20 0 43.50 -6.29 24.39 o 14 20 0 2118.54 2309.74 41.16 o 16 20 0 203.45 134.18 22.31 o 18 20 0 299.01 161.37 22.10 o 20 20 0 1454.97 1531.62 46.33 o -20 22 0 714.53 735.20 43.21 o -18 22 0 146.08 122.75 37.25 o -16 22 0 32.09 40.04 20.68 o -14 22 0 415.03 402.29 38.11 o -12 22 0 3225.84 3417.70 71.92 o -10 22 0 255.78 237.41 46.10 o -8 22 0 12818.93 13574.98 248.80 o -6 22 0 14.78 28.44 71.38 o -4 22 0 128.21 145.46 24.31 o -2 22 0 548.17 490.55 33.07 o 0 22 0 51.14 48.06 33.47 o 2 22 0 0.11 13.08 36.26 o 4 22 0 5.41 2.62 24.21 o 6 22 0 82.90 116.09 26.04 o 8 22 0 276.44 197.59 25.36 o 10 22 0 25.88 -3.46 25.36 o 12 22 0 972.80 956.82 26.54 o 14 22 0 79.07 200.74 41.57 o 16 22 0 162.85 239.05 21.44 o 18 22 0 3752.15 4117.87 102.40 o 20 22 0 124.96 173.00 21.97 o 22 22 0 115.00 66.48 30.13 o -22 24 0 145.29 123.25 24.31 o -20 24 0 110.20 75.00 27.73 o -18 24 0 0.44 22.01 21.22 o -16 24 0 20.60 50.83 18.67 o -14 24 0 573.46 613.88 38.25 o -12 24 0 252.62 257.16 39.30 o -10 24 0 6532.25 6452.09 193.63 o -8 24 0 17.64 9.81 38.09 o -6 24 0 1056.78 1055.35 45.14 o -4 24 0 115.28 96.01 25.31 o -2 24 0 8.13 -18.45 57.21 o 0 24 0 688.02 648.08 28.40 o 2 24 0 321.30 351.18 45.05 o 4 24 0 3790.69 3654.60 87.43 o 6 24 0 0.04 -13.79 27.31 o 8 24 0 961.56 1056.70 35.28 o 10 24 0 184.02 178.90 24.41 o 12 24 0 37.32 73.89 23.36 o 14 24 0 80.62 24.26 25.47 o 16 24 0 1508.93 1588.76 29.13 o 18 24 0 1829.73 1608.37 39.59 o 20 24 0 62.02 168.07 19.89 o 22 24 0 28.20 20.37 21.47 o 24 24 0 209.70 240.00 22.68 o -22 26 0 111.58 90.54 31.20 o -20 26 0 21.94 18.86 25.71 o -18 26 0 99.63 199.14 43.81 o -16 26 0 37.42 10.05 21.83 o -14 26 0 633.25 558.99 25.50 o -12 26 0 1319.98 1346.03 104.05 o -10 26 0 114.50 264.07 97.63 o -8 26 0 24.56 20.69 25.70 o -6 26 0 417.57 399.59 27.30 o -4 26 0 385.74 455.04 26.10 o -2 26 0 73.53 58.22 32.43 o 0 26 0 1986.42 1890.36 30.10 o 2 26 0 10.84 4.90 24.43 o 4 26 0 1433.92 1617.12 36.67 o 6 26 0 1956.64 2146.86 146.58 o 8 26 0 2694.80 2642.18 88.93 o 10 26 0 474.41 494.09 22.99 o 12 26 0 576.02 573.62 25.85 o 14 26 0 108.37 115.92 21.36 o 16 26 0 253.30 182.38 21.08 o 18 26 0 343.61 284.88 26.80 o 20 26 0 2.20 -29.13 19.42 o 22 26 0 3.53 -8.33 19.91 o -20 28 0 62.27 28.08 26.89 o -18 28 0 13.31 25.18 24.63 o -16 28 0 115.39 61.13 22.73 o -14 28 0 11.74 -24.98 22.22 o -12 28 0 593.24 766.27 68.93 o -10 28 0 20.36 2.44 23.88 o -8 28 0 80.71 1.73 29.84 o -6 28 0 445.63 525.67 27.59 o -4 28 0 90.51 252.53 56.40 o -2 28 0 233.44 192.66 44.72 o 0 28 0 627.70 650.59 63.90 o 2 28 0 463.03 439.60 24.32 o 4 28 0 375.18 387.60 29.75 o 6 28 0 447.28 412.24 27.07 o 8 28 0 19.72 10.78 26.46 o 10 28 0 183.01 164.07 26.45 o 12 28 0 88.36 35.64 39.93 o 14 28 0 199.02 176.03 21.81 o 16 28 0 11.66 1.79 21.03 o 18 28 0 34.48 28.55 21.54 o 20 28 0 8.64 19.47 22.91 o -18 30 0 1.91 11.30 28.65 o -16 30 0 0.93 8.21 23.05 o -14 30 0 6.38 -29.09 24.24 o -12 30 0 2.93 9.70 29.11 o -10 30 0 3.38 109.71 75.87 o -8 30 0 256.88 253.22 66.49 o -6 30 0 985.72 933.86 46.46 o -4 30 0 9.01 -5.09 23.47 o -2 30 0 4.90 68.59 22.92 o 0 30 0 45.14 65.68 22.30 o 2 30 0 5.33 -0.81 40.42 o 4 30 0 16.29 28.71 33.29 o 6 30 0 243.86 391.46 74.75 o 8 30 0 210.76 138.57 26.19 o 10 30 0 26.90 -9.72 27.89 o 12 30 0 245.95 223.71 27.87 o 14 30 0 9.83 -12.74 22.43 o 16 30 0 0.00 -9.65 22.27 o 18 30 0 218.42 183.09 28.07 o -14 32 0 35.82 5.90 27.25 o -12 32 0 0.29 40.94 35.85 o -10 32 0 243.87 231.35 33.94 o -8 32 0 83.75 63.80 23.51 o -6 32 0 133.04 165.05 23.74 o -4 32 0 382.84 404.54 23.35 o -2 32 0 636.91 715.57 32.59 o 0 32 0 967.25 909.96 27.33 o 2 32 0 87.49 60.65 23.80 o 4 32 0 100.07 60.22 23.45 o 6 32 0 8.90 0.74 22.68 o 8 32 0 0.16 33.17 23.44 o 10 32 0 122.30 83.22 41.08 o 12 32 0 142.45 107.79 23.79 o 14 32 0 152.10 144.09 25.03 o -8 34 0 232.93 196.87 26.60 o -6 34 0 27.85 24.19 25.83 o -4 34 0 506.63 522.30 58.96 o -2 34 0 170.50 134.34 34.76 o 0 34 0 13.80 25.98 23.94 o 2 34 0 512.12 571.57 51.82 o 4 34 0 22.05 -17.69 22.88 o 6 34 0 36.98 -0.74 24.27 o 8 34 0 495.98 479.80 25.29 o -1 2 1 4009.27 4029.41 37.50 o 1 2 1 7568.75 6899.44 48.78 o -2 3 1 8062.70 7892.07 40.99 o 0 3 1 30662.10 29750.28 133.25 o 2 3 1 706.68 694.80 22.41 o -3 4 1 22370.50 21746.19 186.60 o -1 4 1 2534.41 2160.69 28.05 o 1 4 1 45307.97 44801.98 279.59 o 3 4 1 20690.34 19957.63 160.60 o -4 5 1 98811.37 91921.94 658.86 o -2 5 1 60270.08 58554.61 263.09 o 0 5 1 12215.63 10877.05 55.23 o 2 5 1 7783.60 7016.55 47.90 o 4 5 1 8329.79 7757.58 61.16 o -5 6 1 92101.57 86423.84 649.60 o -3 6 1 16417.80 17337.03 73.63 o -1 6 1 8187.13 7672.32 35.74 o 1 6 1 40115.00 36159.93 213.54 o 3 6 1 25785.10 24760.48 148.77 o 5 6 1 98120.28 95920.78 874.82 o -6 7 1 7869.93 7790.63 52.62 o -4 7 1 1099.53 868.49 22.77 o -2 7 1 2.18 83.83 21.40 o 0 7 1 1215.28 1420.04 24.73 o 2 7 1 403.45 442.86 23.95 o 4 7 1 73935.91 70167.55 740.43 o 6 7 1 27095.26 25977.04 187.32 o -7 8 1 574.22 465.82 23.29 o -5 8 1 20791.00 19767.56 109.72 o -3 8 1 1916.87 1686.29 21.98 o -1 8 1 3012.51 2914.47 24.13 o 1 8 1 42.40 24.92 20.19 o 3 8 1 8152.88 8493.19 33.79 o 5 8 1 8289.24 8162.45 58.50 o 7 8 1 1526.06 1423.39 28.80 o -8 9 1 8910.31 8501.65 64.07 o -6 9 1 2095.46 2111.67 22.75 o -4 9 1 4372.73 4337.78 25.88 o -2 9 1 0.29 11.92 17.15 o 0 9 1 1040.21 931.54 21.02 o 2 9 1 308.69 390.55 19.54 o 4 9 1 4798.17 4993.66 39.31 o 6 9 1 11163.01 10197.33 41.87 o 8 9 1 1278.86 1581.45 28.84 o -9 10 1 2572.30 2402.71 28.06 o -7 10 1 4082.02 3679.18 38.62 o -5 10 1 956.09 934.86 19.67 o -3 10 1 348.59 474.36 18.12 o -1 10 1 3239.21 3122.95 28.76 o 1 10 1 1370.66 1340.42 18.73 o 3 10 1 75.02 43.34 18.31 o 5 10 1 42.28 154.94 19.38 o 7 10 1 6757.42 6854.69 47.50 o 9 10 1 3509.01 3327.22 40.45 o -10 11 1 312.80 397.10 22.53 o -8 11 1 31459.35 32415.36 293.19 o -6 11 1 4491.79 4422.55 30.82 o -4 11 1 2744.55 3005.53 22.79 o -2 11 1 2243.68 2163.88 20.55 o 0 11 1 33.97 12.70 17.45 o 2 11 1 8846.33 8384.69 58.65 o 4 11 1 20032.18 19627.07 75.11 o 6 11 1 13883.55 14192.93 101.59 o 8 11 1 6310.64 6195.71 56.00 o 10 11 1 50.02 125.21 26.09 o -11 12 1 3566.10 3547.74 28.95 o -9 12 1 5088.56 5713.68 47.66 o -7 12 1 74.36 191.79 23.63 o -5 12 1 6318.51 6214.68 73.87 o -3 12 1 3896.59 3975.45 24.85 o -1 12 1 3187.30 2864.41 23.77 o 1 12 1 14.87 31.14 16.75 o 3 12 1 2.86 42.75 16.78 o 5 12 1 23619.49 23679.83 116.96 o 7 12 1 7099.79 6960.11 65.63 o 9 12 1 30289.46 29947.56 280.80 o 11 12 1 5083.72 5313.98 33.41 o -12 13 1 1321.82 1410.93 22.08 o -10 13 1 284.31 321.40 18.72 o -8 13 1 1925.36 1885.95 25.14 o -6 13 1 3218.95 3335.98 26.28 o -4 13 1 44.21 72.51 17.31 o -2 13 1 5580.52 5592.04 24.92 o 0 13 1 2641.61 2776.39 21.00 o 2 13 1 13295.45 13223.57 64.89 o 4 13 1 7900.43 8005.03 84.08 o 6 13 1 161.17 231.02 18.81 o 8 13 1 23204.28 22311.17 205.44 o 10 13 1 1301.29 1251.34 24.35 o 12 13 1 301.76 268.36 18.78 o -13 14 1 251.12 330.82 20.76 o -11 14 1 0.03 47.61 17.38 o -9 14 1 5853.44 6060.05 42.54 o -7 14 1 1601.38 1939.00 30.02 o -5 14 1 4351.51 4569.01 39.65 o -3 14 1 2908.74 2870.16 23.12 o -1 14 1 491.51 611.78 17.79 o 1 14 1 132.03 76.99 16.13 o 3 14 1 7341.80 7448.06 50.79 o 5 14 1 268.99 308.74 19.15 o 7 14 1 7065.71 7137.72 47.62 o 9 14 1 5555.22 5383.93 38.00 o 11 14 1 537.38 559.72 19.66 o 13 14 1 1214.18 1119.32 17.89 o -14 15 1 209.12 245.88 17.61 o -12 15 1 3019.27 3240.94 24.30 o -10 15 1 1417.87 1267.65 20.51 o -8 15 1 0.35 25.15 18.34 o -6 15 1 2223.91 2014.92 21.38 o -4 15 1 715.62 781.86 19.05 o -2 15 1 140.91 141.94 16.48 o 0 15 1 751.29 686.53 17.33 o 2 15 1 382.85 336.47 16.74 o 4 15 1 14.59 2.53 17.37 o 6 15 1 14.68 12.58 19.45 o 8 15 1 5304.59 5418.05 54.09 o 10 15 1 27.38 50.07 19.74 o 12 15 1 135.28 98.32 17.26 o 14 15 1 37.50 21.45 17.00 o -15 16 1 1530.17 1585.61 37.79 o -13 16 1 1394.56 1423.48 28.38 o -11 16 1 16.69 8.32 16.53 o -9 16 1 1146.70 1147.86 19.55 o -7 16 1 1150.34 1318.89 24.44 o -5 16 1 7974.08 7572.61 54.16 o -3 16 1 417.55 445.59 18.84 o -1 16 1 349.28 456.96 18.13 o 1 16 1 208.09 200.96 15.77 o 3 16 1 7777.00 8148.51 48.33 o 5 16 1 512.02 483.28 20.17 o 7 16 1 225.69 254.93 22.18 o 9 16 1 1630.15 1573.52 22.01 o 11 16 1 4.01 8.56 16.90 o 13 16 1 236.56 295.27 18.10 o 15 16 1 5618.43 5850.32 50.06 o -16 17 1 682.22 675.53 22.77 o -14 17 1 4332.40 4426.04 64.39 o -12 17 1 155.77 124.65 18.15 o -10 17 1 595.41 555.80 18.35 o -8 17 1 119.69 186.01 18.71 o -6 17 1 1019.66 1180.44 21.05 o -4 17 1 163.58 197.59 17.22 o -2 17 1 691.97 697.66 21.84 o 0 17 1 7.43 2.10 17.46 o 2 17 1 147.86 142.05 17.74 o 4 17 1 414.68 394.89 20.36 o 6 17 1 2736.25 2886.61 32.08 o 8 17 1 241.66 288.19 20.16 o 10 17 1 832.90 841.86 25.04 o 12 17 1 340.05 354.14 17.20 o 14 17 1 1205.48 1164.35 25.06 o 16 17 1 5.91 9.53 15.73 o -17 18 1 219.37 195.03 15.91 o -15 18 1 1080.63 1021.25 22.20 o -13 18 1 285.05 336.45 35.08 o -11 18 1 677.90 805.84 19.13 o -9 18 1 121.77 193.49 19.20 o -7 18 1 1.06 -26.57 17.72 o -5 18 1 1661.68 1546.41 22.64 o -3 18 1 2178.67 2362.86 25.37 o -1 18 1 3574.64 3610.12 46.22 o 1 18 1 245.47 230.32 16.80 o 3 18 1 1117.37 1236.65 20.56 o 5 18 1 321.74 397.44 22.69 o 7 18 1 336.23 365.35 18.01 o 9 18 1 559.20 687.02 25.19 o 11 18 1 260.47 285.86 22.13 o 13 18 1 0.85 14.13 26.18 o 15 18 1 964.36 919.19 17.90 o 17 18 1 17.72 44.90 14.42 o -18 19 1 1197.17 1118.70 19.61 o -16 19 1 226.91 255.07 18.34 o -14 19 1 577.44 611.52 20.95 o -12 19 1 446.89 502.48 19.04 o -10 19 1 212.20 201.60 17.72 o -8 19 1 917.26 964.33 22.25 o -6 19 1 16.68 16.10 17.55 o -4 19 1 88.22 84.56 31.95 o -2 19 1 3.81 -2.33 17.68 o 0 19 1 17.79 44.50 15.98 o 2 19 1 1071.91 1082.37 17.91 o 4 19 1 5.42 3.28 18.69 o 6 19 1 217.78 205.84 17.92 o 8 19 1 640.25 682.56 20.87 o 10 19 1 4.17 8.91 17.86 o 12 19 1 2097.17 1927.23 35.38 o 14 19 1 267.64 411.44 25.43 o 16 19 1 10.40 12.26 17.94 o 18 19 1 771.89 736.25 27.18 o -19 20 1 259.90 215.41 17.91 o -17 20 1 393.59 474.87 16.03 o -15 20 1 542.60 602.74 19.05 o -13 20 1 333.94 417.10 17.00 o -11 20 1 577.16 592.96 26.04 o -9 20 1 863.54 811.38 20.29 o -7 20 1 1784.35 1710.55 32.19 o -5 20 1 13.98 24.04 19.21 o -3 20 1 0.29 7.35 17.37 o -1 20 1 184.80 207.15 16.84 o 1 20 1 171.75 195.74 16.44 o 3 20 1 406.83 423.18 17.40 o 5 20 1 304.55 328.70 24.73 o 7 20 1 48.56 11.59 17.66 o 9 20 1 1904.10 1906.91 26.57 o 11 20 1 1140.25 1292.44 21.71 o 13 20 1 93.98 154.02 21.16 o 15 20 1 258.82 255.49 17.53 o 17 20 1 73.61 121.32 13.88 o 19 20 1 0.74 -4.51 14.97 o -20 21 1 657.78 576.64 24.25 o -18 21 1 905.66 943.95 19.08 o -16 21 1 813.23 918.20 25.92 o -14 21 1 829.53 822.49 20.55 o -12 21 1 115.33 102.48 15.60 o -10 21 1 3996.44 4275.89 54.66 o -8 21 1 30.13 83.32 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