#------------------------------------------------------------------------------ #$Date: 2023-03-16 05:28:11 +0200 (Thu, 16 Mar 2023) $ #$Revision: 281912 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/42/2244242.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2244242 _cell_angle_alpha 90.000 _cell_angle_beta 98.776 _cell_angle_gamma 90.000 _cell_length_a 10.8564 _cell_length_b 9.1857 _cell_length_c 13.3100 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7891 _cod_data_source_file yz20301asup2.hkl _cod_data_source_block 1a _shelx_title ' elg_m6 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.27 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5736.47 5551.69 131.29 o 4 0 0 1232.63 1183.17 14.43 o 6 0 0 133.84 131.18 3.62 o 8 0 0 1611.56 1578.72 18.89 o 10 0 0 35.52 35.88 2.37 o 12 0 0 246.84 264.95 3.91 o 1 1 0 375.05 383.77 4.47 o 2 1 0 754.74 738.84 10.25 o 3 1 0 121.63 104.87 2.06 o 4 1 0 663.07 667.67 6.34 o 5 1 0 471.76 565.52 5.60 o 6 1 0 250.41 243.97 3.22 o 7 1 0 798.98 792.01 5.78 o 8 1 0 39.90 38.68 0.99 o 9 1 0 528.30 514.78 3.86 o 10 1 0 323.63 322.40 3.10 o 11 1 0 239.54 239.38 2.54 o 12 1 0 122.10 120.88 1.74 o 13 1 0 141.22 146.00 2.32 o 0 2 0 10.08 9.06 2.60 o 1 2 0 1204.23 1238.59 10.99 o 2 2 0 1751.69 1607.12 14.59 o 3 2 0 1180.75 1175.30 13.24 o 4 2 0 6197.53 6460.62 59.98 o 5 2 0 187.51 248.61 3.39 o 6 2 0 18.36 17.35 1.26 o 7 2 0 103.28 88.11 1.18 o 8 2 0 14.62 9.79 0.65 o 9 2 0 1.00 1.87 0.69 o 10 2 0 639.42 610.28 4.96 o 11 2 0 15.90 14.06 0.90 o 12 2 0 88.62 90.01 1.37 o 13 2 0 21.02 18.44 0.71 o 1 3 0 958.32 936.63 10.24 o 2 3 0 3131.40 3097.81 24.18 o 3 3 0 1114.53 1184.40 10.75 o 4 3 0 285.41 302.71 4.16 o 5 3 0 505.26 547.65 6.53 o 6 3 0 995.96 975.65 5.89 o 7 3 0 819.37 809.87 5.12 o 8 3 0 42.87 29.57 0.90 o 9 3 0 980.81 932.90 7.42 o 10 3 0 854.44 896.43 7.35 o 11 3 0 583.96 573.15 5.18 o 12 3 0 0.87 0.95 0.75 o 13 3 0 0.76 0.64 0.50 o 0 4 0 719.84 676.71 10.46 o 1 4 0 1441.66 1421.70 12.93 o 2 4 0 918.25 917.54 8.78 o 3 4 0 78.52 65.14 1.75 o 4 4 0 2713.79 2685.52 27.15 o 5 4 0 2.55 9.66 0.57 o 6 4 0 54.89 57.57 0.80 o 7 4 0 162.60 174.09 2.03 o 8 4 0 383.61 351.27 3.09 o 9 4 0 185.22 150.04 2.39 o 10 4 0 270.17 266.60 3.41 o 11 4 0 356.24 344.49 3.55 o 12 4 0 76.18 84.13 1.52 o 1 5 0 2352.74 2472.81 22.82 o 2 5 0 327.48 312.42 3.49 o 3 5 0 2386.65 2354.98 18.31 o 4 5 0 256.43 293.90 2.10 o 5 5 0 14.89 6.45 0.52 o 6 5 0 79.18 83.09 1.57 o 7 5 0 662.49 655.77 4.34 o 8 5 0 21.62 23.25 0.88 o 9 5 0 36.12 39.81 1.37 o 10 5 0 0.27 0.76 0.68 o 11 5 0 173.70 164.28 2.07 o 12 5 0 2.26 2.98 0.55 o 0 6 0 5.39 17.73 0.98 o 1 6 0 65.87 70.60 1.01 o 2 6 0 1045.32 1100.35 6.57 o 3 6 0 3.48 4.40 0.51 o 4 6 0 289.10 286.13 2.02 o 5 6 0 18.72 16.55 0.63 o 6 6 0 2.42 3.04 0.61 o 7 6 0 462.09 454.58 3.47 o 8 6 0 389.24 388.63 3.43 o 9 6 0 30.68 30.34 0.92 o 10 6 0 28.97 26.80 0.92 o 11 6 0 48.28 44.24 1.27 o 1 7 0 423.45 423.46 3.25 o 2 7 0 843.49 827.66 5.37 o 3 7 0 1716.33 1713.29 10.33 o 4 7 0 1735.48 1732.59 11.08 o 5 7 0 1587.37 1587.38 9.86 o 6 7 0 1.75 2.33 0.60 o 7 7 0 135.65 141.05 1.61 o 8 7 0 15.75 11.70 0.68 o 9 7 0 2.28 4.05 0.72 o 10 7 0 23.00 24.42 0.85 o 0 8 0 0.12 1.08 1.04 o 1 8 0 58.57 60.16 1.03 o 2 8 0 9.17 9.04 0.66 o 3 8 0 55.95 52.90 0.91 o 4 8 0 213.19 212.92 1.91 o 5 8 0 1448.03 1438.32 9.45 o 6 8 0 2.48 1.61 0.69 o 7 8 0 290.80 300.11 3.01 o 8 8 0 68.57 71.04 1.30 o 9 8 0 312.10 325.73 4.07 o 1 9 0 0.96 0.96 0.70 o 2 9 0 118.59 125.44 1.69 o 3 9 0 0.99 1.97 0.65 o 4 9 0 18.58 16.18 0.75 o 5 9 0 503.64 507.07 4.30 o 6 9 0 68.00 65.37 1.79 o 7 9 0 3.89 4.58 0.59 o 8 9 0 151.44 170.67 2.92 o 0 10 0 14.80 17.02 1.07 o 1 10 0 273.57 271.62 2.32 o 2 10 0 45.78 49.06 1.09 o 3 10 0 171.06 188.24 1.98 o 4 10 0 286.55 280.84 2.93 o 5 10 0 857.73 848.01 8.90 o 6 10 0 430.62 412.81 6.02 o 1 11 0 275.14 282.23 4.12 o 2 11 0 9.02 7.90 0.58 o 3 11 0 58.30 48.48 1.17 o 4 11 0 35.12 34.52 1.45 o -13 0 1 236.64 229.81 3.77 o -11 0 1 271.73 279.32 3.68 o -9 0 1 126.56 131.36 2.49 o -7 0 1 128.14 106.78 1.98 o -5 0 1 2349.55 2460.84 27.53 o -3 0 1 422.65 425.17 6.20 o -1 0 1 11723.07 10973.15 258.59 o 1 0 1 297.56 301.79 11.12 o 3 0 1 538.58 551.26 13.11 o 5 0 1 590.51 546.98 12.12 o 7 0 1 1578.09 1563.67 14.49 o 9 0 1 158.59 154.48 3.65 o 11 0 1 108.69 119.44 2.98 o 13 0 1 67.66 65.81 2.95 o -13 1 1 22.55 25.75 0.83 o -12 1 1 5.32 5.39 0.73 o -11 1 1 95.85 92.94 1.56 o -10 1 1 878.17 862.52 6.74 o -9 1 1 473.77 473.62 4.07 o -8 1 1 129.67 145.66 2.10 o -7 1 1 1525.15 1565.05 10.27 o -6 1 1 276.04 258.66 3.18 o -5 1 1 189.68 230.07 2.93 o -4 1 1 58.94 60.06 1.49 o -3 1 1 2868.20 2830.13 26.98 o -2 1 1 4454.84 4397.69 46.82 o -1 1 1 298.54 290.30 4.10 o 0 1 1 6231.45 6007.98 71.03 o 1 1 1 497.25 522.00 8.46 o 2 1 1 5028.15 4899.97 60.87 o 3 1 1 5045.29 5077.07 54.32 o 4 1 1 12.30 9.60 1.17 o 5 1 1 100.14 108.59 2.95 o 6 1 1 162.42 134.60 2.57 o 7 1 1 143.66 144.81 1.66 o 8 1 1 29.55 32.56 0.78 o 9 1 1 1.56 1.95 0.67 o 10 1 1 700.83 698.54 5.22 o 11 1 1 81.79 92.03 1.65 o 12 1 1 8.99 8.71 0.72 o 13 1 1 24.48 25.47 0.93 o -13 2 1 7.72 6.11 0.62 o -12 2 1 184.34 180.98 2.15 o -11 2 1 32.02 37.54 1.33 o -10 2 1 720.10 765.84 6.26 o -9 2 1 8.83 5.32 0.73 o -8 2 1 2466.90 2424.84 15.41 o -7 2 1 30.40 22.21 0.76 o -6 2 1 48.64 48.49 2.52 o -5 2 1 215.99 257.16 3.44 o -4 2 1 3698.53 3690.56 28.81 o -3 2 1 8.60 7.33 0.86 o -2 2 1 4127.34 4153.34 44.71 o -1 2 1 128.94 139.08 2.70 o 0 2 1 9866.46 9623.20 107.05 o 1 2 1 1840.82 1866.22 17.84 o 2 2 1 1548.09 1529.79 19.05 o 3 2 1 176.94 167.77 3.62 o 4 2 1 100.25 68.95 2.64 o 5 2 1 637.64 697.76 7.62 o 6 2 1 57.40 64.67 1.73 o 7 2 1 90.46 91.21 1.09 o 8 2 1 67.97 59.84 1.07 o 9 2 1 194.00 183.83 1.93 o 10 2 1 183.83 181.20 2.10 o 11 2 1 177.84 207.86 2.48 o 12 2 1 167.14 172.79 2.26 o 13 2 1 49.37 45.46 1.88 o -13 3 1 293.60 298.83 3.48 o -12 3 1 0.29 1.19 0.83 o -11 3 1 655.69 700.54 6.10 o -10 3 1 447.32 415.52 4.05 o -9 3 1 216.58 179.94 2.38 o -8 3 1 11.18 8.90 0.68 o -7 3 1 486.02 480.88 3.24 o -6 3 1 32.90 41.42 0.78 o -5 3 1 17.46 7.27 0.80 o -4 3 1 206.28 220.01 2.39 o -3 3 1 954.02 978.24 9.46 o -2 3 1 386.91 401.93 4.63 o -1 3 1 14526.89 14694.49 163.84 o 0 3 1 0.15 0.30 1.27 o 1 3 1 25.74 37.04 1.08 o 2 3 1 481.16 504.68 4.99 o 3 3 1 95.64 67.61 1.55 o 4 3 1 117.90 105.68 2.37 o 5 3 1 178.31 156.42 2.62 o 6 3 1 2.77 4.00 0.51 o 7 3 1 649.42 634.07 4.95 o 8 3 1 18.70 20.05 0.86 o 9 3 1 212.72 227.17 2.35 o 10 3 1 194.55 186.04 2.07 o 11 3 1 103.28 108.68 1.69 o 12 3 1 11.50 7.88 0.68 o -12 4 1 349.54 338.46 4.22 o -11 4 1 113.34 107.39 1.55 o -10 4 1 64.29 53.56 1.69 o -9 4 1 1610.03 1524.03 11.23 o -8 4 1 221.51 220.98 2.19 o -7 4 1 5.14 5.07 0.62 o -6 4 1 995.64 1044.39 5.88 o -5 4 1 461.43 439.00 3.02 o -4 4 1 1849.53 1931.20 17.30 o -3 4 1 5.00 5.59 0.82 o -2 4 1 63.91 63.10 1.38 o -1 4 1 20.74 16.42 1.43 o 0 4 1 1261.67 1262.54 13.04 o 1 4 1 1019.62 992.62 8.54 o 2 4 1 397.88 383.12 5.06 o 3 4 1 852.37 850.86 7.35 o 4 4 1 10.15 7.53 1.09 o 5 4 1 37.90 38.32 0.74 o 6 4 1 247.96 280.83 1.96 o 7 4 1 21.81 21.28 0.89 o 8 4 1 422.27 397.46 4.22 o 9 4 1 189.87 210.52 2.60 o 10 4 1 119.99 123.05 1.66 o 11 4 1 365.66 378.87 3.70 o 12 4 1 1.53 1.18 0.74 o -12 5 1 28.30 27.86 1.22 o -11 5 1 20.49 24.66 0.86 o -10 5 1 289.57 297.46 3.27 o -9 5 1 23.44 27.20 1.02 o -8 5 1 40.54 36.14 1.14 o -7 5 1 8.31 6.87 0.67 o -6 5 1 379.96 322.86 2.37 o -5 5 1 618.33 621.12 3.71 o -4 5 1 8.11 9.53 0.50 o -3 5 1 986.17 946.83 8.83 o -2 5 1 1136.52 1066.33 10.68 o -1 5 1 216.66 234.47 3.36 o 0 5 1 13.49 16.45 0.92 o 1 5 1 40.89 46.88 1.20 o 2 5 1 1965.42 1950.87 16.14 o 3 5 1 839.85 861.41 6.46 o 4 5 1 275.71 260.22 1.87 o 5 5 1 20.24 21.88 0.58 o 6 5 1 985.12 967.95 5.59 o 7 5 1 0.16 0.66 0.66 o 8 5 1 73.08 68.02 1.34 o 9 5 1 113.64 119.14 1.81 o 10 5 1 2.96 4.50 0.71 o 11 5 1 109.34 105.24 1.63 o 12 5 1 0.03 0.22 0.54 o -11 6 1 4.43 3.77 0.51 o -10 6 1 1.70 0.31 0.72 o -9 6 1 70.60 64.04 1.34 o -8 6 1 417.56 403.58 3.67 o -7 6 1 203.58 192.30 1.76 o -6 6 1 12.58 13.96 0.68 o -5 6 1 949.92 945.38 5.71 o -4 6 1 195.72 202.99 1.68 o -3 6 1 379.77 371.12 2.71 o -2 6 1 83.71 81.29 1.46 o -1 6 1 15.99 27.61 0.79 o 0 6 1 91.25 87.96 1.13 o 1 6 1 1383.68 1417.27 8.98 o 2 6 1 154.01 162.89 1.40 o 3 6 1 43.80 41.10 0.70 o 4 6 1 254.11 261.41 1.94 o 5 6 1 333.79 328.97 2.38 o 6 6 1 668.03 650.76 4.34 o 7 6 1 278.74 296.18 2.42 o 8 6 1 3.25 2.27 0.68 o 9 6 1 68.95 71.80 1.20 o 10 6 1 1.30 2.18 0.66 o 11 6 1 39.93 34.10 1.08 o -10 7 1 14.04 13.95 0.83 o -9 7 1 7.95 11.91 0.87 o -8 7 1 7.80 6.07 0.70 o -7 7 1 38.58 38.81 0.85 o -6 7 1 593.16 586.97 3.94 o -5 7 1 2059.69 2053.54 12.19 o -4 7 1 65.58 70.26 1.00 o -3 7 1 221.95 220.08 2.01 o -2 7 1 891.50 895.90 6.20 o -1 7 1 4.45 4.28 0.60 o 0 7 1 144.93 150.64 1.62 o 1 7 1 36.39 31.55 0.79 o 2 7 1 6.31 8.59 0.60 o 3 7 1 455.81 442.30 2.98 o 4 7 1 39.29 40.16 0.75 o 5 7 1 21.30 21.68 0.73 o 6 7 1 4.97 5.36 0.67 o 7 7 1 33.10 32.49 0.94 o 8 7 1 47.93 53.59 1.23 o 9 7 1 28.73 30.78 1.05 o 10 7 1 443.40 449.51 5.14 o -9 8 1 9.49 9.99 0.73 o -8 8 1 60.95 62.66 1.27 o -7 8 1 164.59 162.87 1.89 o -6 8 1 36.57 36.84 0.85 o -5 8 1 187.26 195.75 2.10 o -4 8 1 713.35 713.65 4.93 o -3 8 1 995.62 1006.29 6.48 o -2 8 1 125.97 124.33 1.71 o -1 8 1 580.49 592.09 4.85 o 0 8 1 229.99 235.04 2.29 o 1 8 1 0.03 0.22 0.65 o 2 8 1 70.45 67.52 1.29 o 3 8 1 315.99 310.96 2.54 o 4 8 1 517.24 511.26 3.88 o 5 8 1 187.88 197.36 1.82 o 6 8 1 1.80 2.24 0.70 o 7 8 1 20.84 19.81 0.81 o 8 8 1 198.46 199.26 2.40 o 9 8 1 19.77 18.57 0.97 o -8 9 1 9.70 6.59 0.66 o -7 9 1 66.89 71.61 1.40 o -6 9 1 316.24 328.73 3.06 o -5 9 1 554.93 558.51 4.39 o -4 9 1 14.56 12.50 0.65 o -3 9 1 156.45 160.16 1.81 o -2 9 1 49.09 48.23 0.99 o -1 9 1 179.75 172.49 1.75 o 0 9 1 134.96 131.76 1.67 o 1 9 1 11.93 12.86 0.80 o 2 9 1 185.05 182.52 1.83 o 3 9 1 144.23 135.02 1.47 o 4 9 1 20.26 21.79 0.79 o 5 9 1 1.78 2.07 0.69 o 6 9 1 8.93 8.99 0.66 o 7 9 1 186.12 184.48 2.56 o 8 9 1 4.25 4.30 0.57 o -6 10 1 1.67 1.69 0.61 o -5 10 1 217.39 212.92 3.20 o -4 10 1 65.41 61.04 1.11 o -3 10 1 145.40 153.16 1.63 o -2 10 1 54.05 52.96 1.01 o -1 10 1 202.44 204.40 1.87 o 0 10 1 72.88 73.18 1.09 o 1 10 1 48.03 41.97 0.83 o 2 10 1 2.04 1.84 0.59 o 3 10 1 24.54 28.45 0.74 o 4 10 1 291.16 295.89 2.96 o 5 10 1 590.48 567.98 5.62 o 6 10 1 17.07 18.27 0.79 o -4 11 1 20.22 21.55 0.91 o -3 11 1 28.08 28.11 0.84 o -2 11 1 322.43 339.75 3.19 o -1 11 1 38.43 32.05 0.73 o 0 11 1 115.26 105.09 1.18 o 1 11 1 8.46 7.41 0.61 o 2 11 1 2.22 2.28 0.55 o 3 11 1 0.95 0.57 0.57 o 4 11 1 34.89 26.54 0.84 o -12 0 2 146.49 138.99 2.77 o -10 0 2 15.31 10.65 1.10 o -8 0 2 339.19 334.43 3.77 o -6 0 2 7.17 13.92 1.61 o -4 0 2 3797.35 3843.45 46.73 o -2 0 2 2492.82 2538.72 43.53 o 0 0 2 827.49 787.24 14.07 o 2 0 2 2340.24 2319.95 56.71 o 4 0 2 7021.07 6935.57 135.69 o 6 0 2 1911.79 2174.72 27.93 o 8 0 2 319.90 272.60 4.33 o 10 0 2 4.93 4.41 1.01 o 12 0 2 55.68 65.06 1.73 o -13 1 2 230.46 236.29 3.99 o -12 1 2 17.69 18.80 0.92 o -11 1 2 1.56 3.15 0.87 o -10 1 2 1900.05 1877.21 13.41 o -9 1 2 2118.07 2046.75 13.90 o -8 1 2 377.77 396.71 2.96 o -7 1 2 136.64 144.34 1.69 o -6 1 2 60.32 52.40 1.69 o -5 1 2 815.94 787.07 7.90 o -4 1 2 141.18 176.91 2.68 o -3 1 2 86.45 99.74 1.93 o -2 1 2 2121.20 2082.80 19.33 o -1 1 2 405.68 410.79 4.21 o 0 1 2 550.69 520.32 6.13 o 1 1 2 9452.56 9347.48 96.98 o 2 1 2 171.31 194.29 2.97 o 3 1 2 52.45 56.87 1.73 o 4 1 2 1427.04 1485.33 19.27 o 5 1 2 4.67 1.49 1.27 o 6 1 2 4.44 3.15 1.03 o 7 1 2 188.02 188.56 1.69 o 8 1 2 252.78 245.74 2.26 o 9 1 2 585.56 554.27 4.29 o 10 1 2 358.61 381.62 3.24 o 11 1 2 4.59 7.16 0.79 o 12 1 2 11.67 11.66 0.74 o 13 1 2 114.25 108.68 2.88 o -13 2 2 192.71 198.63 3.10 o -12 2 2 160.78 154.91 2.31 o -11 2 2 400.12 409.43 4.30 o -10 2 2 55.24 54.81 1.47 o -9 2 2 117.42 119.99 1.65 o -8 2 2 22.19 22.77 0.73 o -7 2 2 401.72 377.23 2.80 o -6 2 2 106.45 117.08 2.44 o -5 2 2 215.31 196.49 2.85 o -4 2 2 0.66 2.16 0.76 o -3 2 2 2977.67 3019.65 22.74 o -2 2 2 218.89 242.72 2.87 o -1 2 2 1125.75 1241.93 10.78 o 0 2 2 6963.19 7003.74 67.88 o 1 2 2 20527.26 20532.32 206.48 o 2 2 2 6.43 3.42 1.26 o 3 2 2 2897.86 2797.22 48.60 o 4 2 2 434.95 482.00 6.33 o 5 2 2 646.31 611.43 7.20 o 6 2 2 260.56 279.44 2.76 o 7 2 2 292.36 270.76 2.15 o 8 2 2 238.62 236.74 2.15 o 9 2 2 799.98 783.48 5.90 o 10 2 2 362.91 329.68 3.08 o 11 2 2 595.09 577.70 5.34 o 12 2 2 178.34 179.29 2.32 o -13 3 2 67.75 66.60 1.63 o -12 3 2 0.11 0.71 0.65 o -11 3 2 172.05 162.73 2.70 o -10 3 2 239.43 219.76 3.46 o -9 3 2 211.42 202.79 2.25 o -8 3 2 135.20 112.04 1.45 o -7 3 2 92.27 96.62 1.17 o -6 3 2 5174.60 5180.56 29.42 o -5 3 2 185.77 186.22 3.28 o -4 3 2 1690.35 1900.33 14.30 o -3 3 2 363.16 364.56 3.62 o -2 3 2 753.31 695.46 7.49 o -1 3 2 19.60 18.07 1.16 o 0 3 2 53.37 52.65 1.27 o 1 3 2 256.52 273.99 2.90 o 2 3 2 1478.84 1373.93 13.33 o 3 3 2 553.12 608.22 7.60 o 4 3 2 1.59 2.90 1.15 o 5 3 2 24.57 13.59 1.26 o 6 3 2 1383.64 1327.60 7.79 o 7 3 2 3.22 3.32 0.66 o 8 3 2 161.04 154.45 1.72 o 9 3 2 73.20 75.25 1.32 o 10 3 2 386.52 410.06 3.77 o 11 3 2 273.10 274.96 3.51 o 12 3 2 0.24 -0.17 0.55 o -12 4 2 52.32 49.08 0.98 o -11 4 2 171.28 172.10 2.17 o -10 4 2 188.97 195.55 2.94 o -9 4 2 298.81 302.92 2.89 o -8 4 2 900.72 873.85 5.91 o -7 4 2 475.44 492.26 3.53 o -6 4 2 24.02 20.40 0.60 o -5 4 2 279.05 269.45 2.11 o -4 4 2 69.37 88.27 1.90 o -3 4 2 1616.22 1667.44 14.61 o -2 4 2 8.28 10.20 0.87 o -1 4 2 465.67 466.89 5.34 o 0 4 2 8.26 21.49 1.09 o 1 4 2 195.85 238.05 3.19 o 2 4 2 1274.90 1298.87 11.19 o 3 4 2 26.50 37.92 1.35 o 4 4 2 19.54 17.85 0.92 o 5 4 2 24.79 20.44 0.60 o 6 4 2 502.68 540.62 3.75 o 7 4 2 622.83 632.56 4.66 o 8 4 2 21.89 23.88 1.14 o 9 4 2 117.34 123.71 1.64 o 10 4 2 502.38 495.10 4.33 o 11 4 2 155.67 146.22 1.86 o 12 4 2 30.11 26.88 0.97 o -12 5 2 4.09 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