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Information card for entry 2312316
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| Coordinates | 2312316.cif |
|---|---|
| Structure factors | 2312316.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis(μ-anthracene-κ^2^<i>C</i>^9^:<i>C</i>^10^)dicopper bis[bis(tetrahydrofuran-κ<i>O</i>)potassium] |
|---|---|
| Formula | C44 H52 Cu2 K2 O4 |
| Calculated formula | C44 H52 Cu2 K2 O4 |
| Title of publication | Crystal structure and synthesis of the bis(anthracene)dicuprate dianion as the dipotassium salt, [K(tetrahydrofuran)<sub>2</sub>]<sub>2</sub>[{Cu(9,10-η<sup>2</sup>-anthracene)}<sub>2</sub>], the first anionic arene complex of copper. |
| Authors of publication | Young, Jr, Victor G; Brennessel, William W.; Ellis, John E. |
| Journal of publication | Acta crystallographica. Section C, Structural chemistry |
| Year of publication | 2023 |
| Journal volume | 79 |
| Journal issue | Pt 11 |
| Pages of publication | 456 - 463 |
| a | 9.6864 ± 0.0019 Å |
| b | 10.484 ± 0.002 Å |
| c | 10.658 ± 0.002 Å |
| α | 66.22 ± 0.03° |
| β | 89.67 ± 0.03° |
| γ | 82.73 ± 0.03° |
| Cell volume | 981.3 ± 0.4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0356 |
| Residual factor for significantly intense reflections | 0.0287 |
| Weighted residual factors for significantly intense reflections | 0.0687 |
| Weighted residual factors for all reflections included in the refinement | 0.0726 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288126 (current) | 2023-12-07 | cif/ Updating files of 2312316 Original log message: Adding full bibliography for 2312316.cif. |
2312316.cif 2312316.hkl |
| 286648 | 2023-10-04 | cif/ hkl/ Adding structures of 2312316 via cif-deposit CGI script. |
2312316.cif 2312316.hkl |
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Users of the data should acknowledge the original authors of the
structural data.