#------------------------------------------------------------------------------
#$Date: 2024-05-11 04:46:09 +0300 (Sat, 11 May 2024) $
#$Revision: 291814 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312501.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2312501
loop_
_publ_author_name
'Gollé-Leidreiter, Philipp'
'Bhat, Shrikant'
'Wiehl, Leonore'
'Wen, Qingbo'
'Kroll, Peter'
'Ishikawa, Ryo'
'Etter, Martin'
'Farla, Robert'
'Ikuhara, Yuichi'
'Riedel, Ralf'
'Kolb, Ute'
_publ_section_title
;
 Crystal structures of two new high-pressure oxynitrides with composition
 SnGe<sub>4</sub>N<sub>4</sub>O<sub>4</sub>, from single-crystal electron
 diffraction.
;
_journal_coeditor_code           JE5053SUP1
_journal_issue                   3
_journal_name_full
'Acta crystallographica Section B, Structural science, crystal engineering and materials'
_journal_paper_doi               10.1107/S2052520624002683
_journal_volume                  80
_journal_year                    2024
_chemical_formula_moiety         'Ge4 N4 O4 Sn'
_chemical_formula_sum            'Ge24 N24 O24 Sn6'
_chemical_formula_weight         3174.6
_space_group_IT_number           166
_space_group_name_Hall           '-R 3 2"'
_space_group_name_H-M_alt        'R -3 m :H'
_symmetry_cell_setting           trigonal
_symmetry_Int_Tables_number      166
_symmetry_space_group_name_Hall  '-R 3 2"'
_symmetry_space_group_name_H-M   'R -3 m :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   5.846(1)
_cell_length_b                   5.846(1)
_cell_length_c                   28.230(5)
_cell_measurement_reflns_used    none
_cell_measurement_temperature    ?
_cell_measurement_theta_max      none
_cell_measurement_theta_min      none
_cell_volume                     835.5(3)
_diffrn_ambient_temperature      293
_diffrn_detector                 'gatan ultrascan 4000'
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.99
_diffrn_measurement_device       'transmission electron microscope'
_diffrn_measurement_device_type  'Tecnai F30 ST'
_diffrn_measurement_method       'ADT with precession'
_diffrn_radiation_probe          electron
_diffrn_radiation_type           electron
_diffrn_radiation_wavelength     0.0197
_diffrn_reflns_av_unetI/netI     0.1149
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       56
_diffrn_reflns_limit_l_min       -56
_diffrn_reflns_number            32673
_diffrn_reflns_theta_full        1.15
_diffrn_reflns_theta_max         1.15
_diffrn_reflns_theta_min         0.06
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    0
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    6.3092
_exptl_crystal_F_000             342.882
_refine_diff_density_max         1.08
_refine_diff_density_min         -1.12
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    4.3835
_refine_ls_goodness_of_fit_ref   3.6465
_refine_ls_number_constraints    0
_refine_ls_number_parameters     88
_refine_ls_number_reflns         2279
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1651
_refine_ls_R_factor_gt           0.1452
_refine_ls_shift/su_max          0.0469
_refine_ls_shift/su_mean         0.0111
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo)+(0.01P)^2^+0.0000P] where P=(Fo+2Fc)/3'
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.1591
_refine_ls_wR_factor_ref         0.1624
_reflns_number_gt                1504
_reflns_number_total             2279
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            je5053.cif
_cod_data_source_block           Cr4_HH266
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_cell_measurement_temperature' value 'none' was changed to
'?' -- the value is undefined or not given.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 
;
_cod_original_cell_volume        835.5244
_cod_original_sg_symbol_H-M      'R -3 m'
_cod_database_code               2312501
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -y,x-y,z
3 -x+y,-x,z
4 y,x,-z
5 x-y,-y,-z
6 -x,-x+y,-z
7 -x,-y,-z
8 y,-x+y,-z
9 x-y,x,-z
10 -y,-x,z
11 -x+y,y,z
12 x,x-y,z
13 x+2/3,y+1/3,z+1/3
14 -y+2/3,x-y+1/3,z+1/3
15 -x+y+2/3,-x+1/3,z+1/3
16 y+2/3,x+1/3,-z+1/3
17 x-y+2/3,-y+1/3,-z+1/3
18 -x+2/3,-x+y+1/3,-z+1/3
19 -x+2/3,-y+1/3,-z+1/3
20 y+2/3,-x+y+1/3,-z+1/3
21 x-y+2/3,x+1/3,-z+1/3
22 -y+2/3,-x+1/3,z+1/3
23 -x+y+2/3,y+1/3,z+1/3
24 x+2/3,x-y+1/3,z+1/3
25 x+1/3,y+2/3,z+2/3
26 -y+1/3,x-y+2/3,z+2/3
27 -x+y+1/3,-x+2/3,z+2/3
28 y+1/3,x+2/3,-z+2/3
29 x-y+1/3,-y+2/3,-z+2/3
30 -x+1/3,-x+y+2/3,-z+2/3
31 -x+1/3,-y+2/3,-z+2/3
32 y+1/3,-x+y+2/3,-z+2/3
33 x-y+1/3,x+2/3,-z+2/3
34 -y+1/3,-x+2/3,z+2/3
35 -x+y+1/3,y+2/3,z+2/3
36 x+1/3,x-y+2/3,z+2/3
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_site_symmetry_multiplicity
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn1 Sn -0.333333 0.333333 0.76046(7) Uiso 0.0053(6) 6 1 d . . .
Ge1 Ge 0.333333 0.666667 0.72874(11) Uiso 0.0081(8) 6 1 d . . .
Ge2 Ge -0.166667 0.666667 0.666667 Uiso 0.0080(6) 9 1 d . . .
Ge3 Ge 0.166667 0.333333 0.833333 Uiso 0.0065(6) 9 1 d . . .
N2 N -0.0166(13) 0.4917(7) 0.7084(2) Uiso 0.0055(12) 18 1 d . . .
O2 O -0.1553(8) 0.1553(8) 0.7962(2) Uiso 0.0188(16) 18 1 d . . .
O1 O 0 1 0.7004(3) Uiso 0.0022(18) 6 1 d . . .
N1 N 0.333333 0.666667 0.7957(3) Uiso -0.0035(17) 6 1 d . . .
loop_
_atom_type_symbol
_atom_type_scat_source
Ge International_Tables_Vol_C
N International_Tables_Vol_C
O International_Tables_Vol_C
Sn International_Tables_Vol_C
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
? ? ?
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
? ? ? ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N2 Sn1 N2 . . 2_565 79.4(2) ?
N2 Sn1 N2 . . 3_455 79.4(2) ?
N2 Sn1 O2 . . . 90.5(2) ?
N2 Sn1 O2 . . 2_565 90.50(18) ?
N2 Sn1 O2 . . 3_455 166.8(2) ?
N2 Sn1 N2 2_565 . 3_455 79.4(3) ?
N2 Sn1 O2 2_565 . . 166.8(3) ?
N2 Sn1 O2 2_565 . 2_565 90.5(3) ?
N2 Sn1 O2 2_565 . 3_455 90.5(2) ?
N2 Sn1 O2 3_455 . . 90.5(3) ?
N2 Sn1 O2 3_455 . 2_565 166.8(2) ?
N2 Sn1 O2 3_455 . 3_455 90.5(2) ?
O2 Sn1 O2 . . 2_565 98.1(2) ?
O2 Sn1 O2 . . 3_455 98.1(2) ?
O2 Sn1 O2 2_565 . 3_455 98.1(2) ?
N2 Ge1 N2 . . 2_665 110.9(2) ?
N2 Ge1 N2 . . 3_565 110.9(3) ?
N2 Ge1 N1 . . . 108.0(2) ?
N2 Ge1 N2 2_665 . 3_565 110.9(3) ?
N2 Ge1 N1 2_665 . . 108.0(2) ?
N2 Ge1 N1 3_565 . . 108.0(2) ?
Ge2 Ge2 Ge2 2_565 . 2_675 180 ?
Ge2 Ge2 Ge2 2_565 . 3_455 60 ?
Ge2 Ge2 Ge2 2_565 . 3_465 120 ?
Ge2 Ge2 N2 2_565 . . 87.94(13) ?
Ge2 Ge2 N2 2_565 . 2_565 43.80(19) ?
Ge2 Ge2 N2 2_565 . 17_566 136.20(12) ?
Ge2 Ge2 N2 2_565 . 18_456 92.06(16) ?
Ge2 Ge2 O1 2_565 . . 138.97(13) ?
Ge2 Ge2 O1 2_565 . 16_356 41.03(13) ?
Ge2 Ge2 Ge2 2_675 . 3_455 120 ?
Ge2 Ge2 Ge2 2_675 . 3_465 60 ?
Ge2 Ge2 N2 2_675 . . 92.06(13) ?
Ge2 Ge2 N2 2_675 . 2_565 136.20(19) ?
Ge2 Ge2 N2 2_675 . 17_566 43.80(12) ?
Ge2 Ge2 N2 2_675 . 18_456 87.94(16) ?
Ge2 Ge2 O1 2_675 . . 41.03(13) ?
Ge2 Ge2 O1 2_675 . 16_356 138.97(13) ?
Ge2 Ge2 Ge2 3_455 . 3_465 180 ?
Ge2 Ge2 N2 3_455 . . 43.80(12) ?
Ge2 Ge2 N2 3_455 . 2_565 87.9(3) ?
Ge2 Ge2 N2 3_455 . 17_566 92.06(17) ?
Ge2 Ge2 N2 3_455 . 18_456 136.20(19) ?
Ge2 Ge2 O1 3_455 . . 138.97(13) ?
Ge2 Ge2 O1 3_455 . 16_356 41.03(13) ?
Ge2 Ge2 N2 3_465 . . 136.20(12) ?
Ge2 Ge2 N2 3_465 . 2_565 92.1(3) ?
Ge2 Ge2 N2 3_465 . 17_566 87.94(17) ?
Ge2 Ge2 N2 3_465 . 18_456 43.80(19) ?
Ge2 Ge2 O1 3_465 . . 41.03(13) ?
Ge2 Ge2 O1 3_465 . 16_356 138.97(13) ?
N2 Ge2 N2 . . 2_565 86.6(3) ?
N2 Ge2 N2 . . 17_566 93.4(3) ?
N2 Ge2 N2 . . 18_456 180 ?
N2 Ge2 O1 . . . 95.47(19) ?
N2 Ge2 O1 . . 16_356 84.53(19) ?
N2 Ge2 N2 2_565 . 17_566 180 ?
N2 Ge2 N2 2_565 . 18_456 93.4(3) ?
N2 Ge2 O1 2_565 . . 95.5(3) ?
N2 Ge2 O1 2_565 . 16_356 84.5(3) ?
N2 Ge2 N2 17_566 . 18_456 86.6(3) ?
N2 Ge2 O1 17_566 . . 84.53(19) ?
N2 Ge2 O1 17_566 . 16_356 95.47(19) ?
N2 Ge2 O1 18_456 . . 84.5(2) ?
N2 Ge2 O1 18_456 . 16_356 95.5(2) ?
O1 Ge2 O1 . . 16_356 180 ?
Ge3 Ge3 Ge3 2_555 . 2_665 180 ?
Ge3 Ge3 Ge3 2_555 . 3_555 60 ?
Ge3 Ge3 Ge3 2_555 . 3_565 120 ?
Ge3 Ge3 O2 2_555 . . 41.12(15) ?
Ge3 Ge3 O2 2_555 . 3_555 87.05(12) ?
Ge3 Ge3 O2 2_555 . 28_556 138.88(15) ?
Ge3 Ge3 O2 2_555 . 29_556 92.95(12) ?
Ge3 Ge3 N1 2_555 . . 137.11(13) ?
Ge3 Ge3 N1 2_555 . 28_446 42.89(13) ?
Ge3 Ge3 Ge3 2_665 . 3_555 120 ?
Ge3 Ge3 Ge3 2_665 . 3_565 60 ?
Ge3 Ge3 O2 2_665 . . 138.88(15) ?
Ge3 Ge3 O2 2_665 . 3_555 92.95(12) ?
Ge3 Ge3 O2 2_665 . 28_556 41.12(15) ?
Ge3 Ge3 O2 2_665 . 29_556 87.05(12) ?
Ge3 Ge3 N1 2_665 . . 42.89(13) ?
Ge3 Ge3 N1 2_665 . 28_446 137.11(13) ?
Ge3 Ge3 Ge3 3_555 . 3_565 180 ?
Ge3 Ge3 O2 3_555 . . 87.05(15) ?
Ge3 Ge3 O2 3_555 . 3_555 41.12(14) ?
Ge3 Ge3 O2 3_555 . 28_556 92.95(15) ?
Ge3 Ge3 O2 3_555 . 29_556 138.88(14) ?
Ge3 Ge3 N1 3_555 . . 137.11(13) ?
Ge3 Ge3 N1 3_555 . 28_446 42.89(13) ?
Ge3 Ge3 O2 3_565 . . 92.95(15) ?
Ge3 Ge3 O2 3_565 . 3_555 138.88(14) ?
Ge3 Ge3 O2 3_565 . 28_556 87.05(15) ?
Ge3 Ge3 O2 3_565 . 29_556 41.12(14) ?
Ge3 Ge3 N1 3_565 . . 42.89(13) ?
Ge3 Ge3 N1 3_565 . 28_446 137.11(13) ?
O2 Ge3 O2 . . 3_555 89.2(2) ?
O2 Ge3 O2 . . 28_556 180 ?
O2 Ge3 O2 . . 29_556 90.8(2) ?
O2 Ge3 N1 . . . 96.0(2) ?
O2 Ge3 N1 . . 28_446 84.0(2) ?
O2 Ge3 O2 3_555 . 28_556 90.8(2) ?
O2 Ge3 O2 3_555 . 29_556 180 ?
O2 Ge3 N1 3_555 . . 96.04(19) ?
O2 Ge3 N1 3_555 . 28_446 83.96(19) ?
O2 Ge3 O2 28_556 . 29_556 89.2(2) ?
O2 Ge3 N1 28_556 . . 84.0(2) ?
O2 Ge3 N1 28_556 . 28_446 96.0(2) ?
O2 Ge3 N1 29_556 . . 83.96(19) ?
O2 Ge3 N1 29_556 . 28_446 96.04(19) ?
N1 Ge3 N1 . . 28_446 180 ?
Sn1 N2 Ge1 . . . 119.5(3) ?
Sn1 N2 Ge2 . . . 96.7(3) ?
Sn1 N2 Ge2 . . 3_455 96.68(17) ?
Sn1 N2 N2 . . 2_565 50.3(2) ?
Sn1 N2 N2 . . 3_455 50.32(17) ?
Sn1 N2 N2 . . 16_456 139.60(18) ?
Sn1 N2 N2 . . 17_566 139.6(4) ?
Sn1 N2 O1 . . 1_545 94.20(16) ?
Sn1 N2 O1 . . . 94.2(3) ?
Sn1 N2 O1 . . 16_356 95.5(3) ?
Ge1 N2 Ge2 . . . 122.44(19) ?
Ge1 N2 Ge2 . . 3_455 122.4(4) ?
Ge1 N2 N2 . . 2_565 145.5(3) ?
Ge1 N2 N2 . . 3_455 145.5(3) ?
Ge1 N2 N2 . . 16_456 87.7(3) ?
Ge1 N2 N2 . . 17_566 87.7(2) ?
Ge1 N2 O1 . . 1_545 89.8(3) ?
Ge1 N2 O1 . . . 89.81(13) ?
Ge1 N2 O1 . . 16_356 145.0(3) ?
Ge2 N2 Ge2 . . 3_455 92.4(2) ?
Ge2 N2 N2 . . 2_565 46.7(2) ?
Ge2 N2 N2 . . 3_455 92.1(3) ?
Ge2 N2 N2 . . 16_456 91.3(2) ?
Ge2 N2 N2 . . 17_566 43.3(2) ?
Ge2 N2 O1 . . 1_545 133.2(3) ?
Ge2 N2 O1 . . . 41.11(15) ?
Ge2 N2 O1 . . 16_356 46.34(13) ?
Ge2 N2 N2 3_455 . 2_565 92.1(3) ?
Ge2 N2 N2 3_455 . 3_455 46.70(18) ?
Ge2 N2 N2 3_455 . 16_456 43.30(15) ?
Ge2 N2 N2 3_455 . 17_566 91.3(2) ?
Ge2 N2 O1 3_455 . 1_545 41.11(16) ?
Ge2 N2 O1 3_455 . . 133.2(3) ?
Ge2 N2 O1 3_455 . 16_356 46.34(12) ?
N2 N2 N2 2_565 . 3_455 60.0(3) ?
N2 N2 N2 2_565 . 16_456 121.4(3) ?
N2 N2 N2 2_565 . 17_566 90.0(3) ?
N2 N2 O1 2_565 . 1_545 121.5(2) ?
N2 N2 O1 2_565 . . 61.7(2) ?
N2 N2 O1 2_565 . 16_356 58.6(2) ?
N2 N2 N2 3_455 . 16_456 90.0(2) ?
N2 N2 N2 3_455 . 17_566 121.4(3) ?
N2 N2 O1 3_455 . 1_545 61.7(2) ?
N2 N2 O1 3_455 . . 121.5(3) ?
N2 N2 O1 3_455 . 16_356 58.60(19) ?
N2 N2 N2 16_456 . 17_566 62.7(2) ?
N2 N2 O1 16_456 . 1_545 53.9(2) ?
N2 N2 O1 16_456 . . 116.6(3) ?
N2 N2 O1 16_456 . 16_356 62.76(17) ?
N2 N2 O1 17_566 . 1_545 116.6(3) ?
N2 N2 O1 17_566 . . 53.9(2) ?
N2 N2 O1 17_566 . 16_356 62.76(19) ?
O1 N2 O1 1_545 . . 170.5(3) ?
O1 N2 O1 1_545 . 16_356 87.45(17) ?
O1 N2 O1 . . 16_356 87.5(2) ?
Sn1 O2 Ge3 . . . 126.3(2) ?
Sn1 O2 Ge3 . . 2_555 126.3(2) ?
Sn1 O2 O2 . . 2_555 139.1(3) ?
Sn1 O2 O2 . . 3_555 139.1(3) ?
Sn1 O2 O2 . . 29_556 94.9(2) ?
Sn1 O2 O2 . . 30_446 94.9(2) ?
Sn1 O2 N1 . . 1_445 87.87(16) ?
Sn1 O2 N1 . . . 87.87(16) ?
Sn1 O2 N1 . . 28_446 155.9(3) ?
Ge3 O2 Ge3 . . 2_555 97.8(3) ?
Ge3 O2 O2 . . 2_555 92.9(2) ?
Ge3 O2 O2 . . 3_555 45.42(15) ?
Ge3 O2 O2 . . 29_556 44.58(18) ?
Ge3 O2 O2 . . 30_446 98.0(3) ?
Ge3 O2 N1 . . 1_445 140.4(3) ?
Ge3 O2 N1 . . . 42.70(14) ?
Ge3 O2 N1 . . 28_446 48.91(13) ?
Ge3 O2 O2 2_555 . 2_555 45.42(15) ?
Ge3 O2 O2 2_555 . 3_555 92.9(2) ?
Ge3 O2 O2 2_555 . 29_556 98.0(3) ?
Ge3 O2 O2 2_555 . 30_446 44.58(18) ?
Ge3 O2 N1 2_555 . 1_445 42.70(14) ?
Ge3 O2 N1 2_555 . . 140.4(3) ?
Ge3 O2 N1 2_555 . 28_446 48.91(13) ?
O2 O2 O2 2_555 . 3_555 60.00(16) ?
O2 O2 O2 2_555 . 29_556 124.4(3) ?
O2 O2 O2 2_555 . 30_446 90.0(2) ?
O2 O2 N1 2_555 . 1_445 62.26(11) ?
O2 O2 N1 2_555 . . 122.26(19) ?
O2 O2 N1 2_555 . 28_446 58.85(19) ?
O2 O2 O2 3_555 . 29_556 90.0(2) ?
O2 O2 O2 3_555 . 30_446 124.4(3) ?
O2 O2 N1 3_555 . 1_445 122.26(19) ?
O2 O2 N1 3_555 . . 62.26(11) ?
O2 O2 N1 3_555 . 28_446 58.85(19) ?
O2 O2 O2 29_556 . 30_446 68.8(2) ?
O2 O2 N1 29_556 . 1_445 123.8(3) ?
O2 O2 N1 29_556 . . 55.03(19) ?
O2 O2 N1 29_556 . 28_446 65.6(2) ?
O2 O2 N1 30_446 . 1_445 55.03(19) ?
O2 O2 N1 30_446 . . 123.8(3) ?
O2 O2 N1 30_446 . 28_446 65.6(2) ?
N1 O2 N1 1_445 . . 175.4(2) ?
N1 O2 N1 1_445 . 28_446 91.61(18) ?
N1 O2 N1 . . 28_446 91.61(18) ?
Ge2 O1 Ge2 . . 2_675 97.9(3) ?
Ge2 O1 Ge2 . . 3_465 97.9(3) ?
Ge2 O1 N2 . . . 43.42(12) ?
Ge2 O1 N2 . . 1_565 141.0(2) ?
Ge2 O1 N2 . . 2_565 43.42(13) ?
Ge2 O1 N2 . . 2_675 141.0(3) ?
Ge2 O1 N2 . . 3_465 93.60(14) ?
Ge2 O1 N2 . . 3_565 93.60(14) ?
Ge2 O1 N2 . . 16_466 97.6(3) ?
Ge2 O1 N2 . . 17_566 49.13(17) ?
Ge2 O1 N2 . . 18_456 49.1(2) ?
Ge2 O1 Ge2 2_675 . 3_465 97.9(3) ?
Ge2 O1 N2 2_675 . . 93.60(14) ?
Ge2 O1 N2 2_675 . 1_565 93.60(14) ?
Ge2 O1 N2 2_675 . 2_565 141.0(3) ?
Ge2 O1 N2 2_675 . 2_675 43.42(13) ?
Ge2 O1 N2 2_675 . 3_465 141.0(2) ?
Ge2 O1 N2 2_675 . 3_565 43.42(12) ?
Ge2 O1 N2 2_675 . 16_466 49.13(18) ?
Ge2 O1 N2 2_675 . 17_566 49.13(18) ?
Ge2 O1 N2 2_675 . 18_456 97.6(3) ?
Ge2 O1 N2 3_465 . . 141.0(2) ?
Ge2 O1 N2 3_465 . 1_565 43.42(12) ?
Ge2 O1 N2 3_465 . 2_565 93.60(16) ?
Ge2 O1 N2 3_465 . 2_675 93.60(17) ?
Ge2 O1 N2 3_465 . 3_465 43.42(12) ?
Ge2 O1 N2 3_465 . 3_565 141.0(2) ?
Ge2 O1 N2 3_465 . 16_466 49.13(18) ?
Ge2 O1 N2 3_465 . 17_566 97.6(3) ?
Ge2 O1 N2 3_465 . 18_456 49.1(2) ?
N2 O1 N2 . . 1_565 170.5(3) ?
N2 O1 N2 . . 2_565 56.5(2) ?
N2 O1 N2 . . 2_675 119.4(2) ?
N2 O1 N2 . . 3_465 119.41(19) ?
N2 O1 N2 . . 3_565 63.08(19) ?
N2 O1 N2 . . 16_466 126.1(3) ?
N2 O1 N2 . . 17_566 63.33(17) ?
N2 O1 N2 . . 18_456 92.5(3) ?
N2 O1 N2 1_565 . 2_565 119.4(2) ?
N2 O1 N2 1_565 . 2_675 63.1(2) ?
N2 O1 N2 1_565 . 3_465 56.53(18) ?
N2 O1 N2 1_565 . 3_565 119.41(19) ?
N2 O1 N2 1_565 . 16_466 63.3(2) ?
N2 O1 N2 1_565 . 17_566 126.1(3) ?
N2 O1 N2 1_565 . 18_456 92.5(3) ?
N2 O1 N2 2_565 . 2_675 170.5(3) ?
N2 O1 N2 2_565 . 3_465 63.1(2) ?
N2 O1 N2 2_565 . 3_565 119.4(2) ?
N2 O1 N2 2_565 . 16_466 126.1(3) ?
N2 O1 N2 2_565 . 17_566 92.5(2) ?
N2 O1 N2 2_565 . 18_456 63.33(18) ?
N2 O1 N2 2_675 . 3_465 119.4(2) ?
N2 O1 N2 2_675 . 3_565 56.5(2) ?
N2 O1 N2 2_675 . 16_466 63.33(16) ?
N2 O1 N2 2_675 . 17_566 92.5(2) ?
N2 O1 N2 2_675 . 18_456 126.1(3) ?
N2 O1 N2 3_465 . 3_565 170.5(3) ?
N2 O1 N2 3_465 . 16_466 92.5(2) ?
N2 O1 N2 3_465 . 17_566 126.1(3) ?
N2 O1 N2 3_465 . 18_456 63.3(2) ?
N2 O1 N2 3_565 . 16_466 92.5(2) ?
N2 O1 N2 3_565 . 17_566 63.3(2) ?
N2 O1 N2 3_565 . 18_456 126.1(3) ?
N2 O1 N2 16_466 . 17_566 62.8(3) ?
N2 O1 N2 16_466 . 18_456 62.8(2) ?
N2 O1 N2 17_566 . 18_456 62.8(3) ?
Ge1 N1 Ge3 . . . 122.22(19) ?
Ge1 N1 Ge3 . . 2_665 122.22(19) ?
Ge1 N1 Ge3 . . 3_565 122.22(19) ?
Ge1 N1 O2 . . . 90.32(19) ?
Ge1 N1 O2 . . 1_665 90.32(19) ?
Ge1 N1 O2 . . 2_565 90.32(19) ?
Ge1 N1 O2 . . 2_665 90.32(19) ?
Ge1 N1 O2 . . 3_555 90.32(19) ?
Ge1 N1 O2 . . 3_565 90.32(19) ?
Ge1 N1 O2 . . 28_556 143.32(16) ?
Ge1 N1 O2 . . 29_556 143.32(16) ?
Ge1 N1 O2 . . 30_556 143.32(16) ?
Ge3 N1 Ge3 . . 2_665 94.2(3) ?
Ge3 N1 Ge3 . . 3_565 94.2(3) ?
Ge3 N1 O2 . . . 41.26(12) ?
Ge3 N1 O2 . . 1_665 135.4(3) ?
Ge3 N1 O2 . . 2_565 91.74(14) ?
Ge3 N1 O2 . . 2_665 91.74(14) ?
Ge3 N1 O2 . . 3_555 41.26(12) ?
Ge3 N1 O2 . . 3_565 135.4(3) ?
Ge3 N1 O2 . . 28_556 47.13(15) ?
Ge3 N1 O2 . . 29_556 47.13(17) ?
Ge3 N1 O2 . . 30_556 94.5(3) ?
Ge3 N1 Ge3 2_665 . 3_565 94.2(3) ?
Ge3 N1 O2 2_665 . . 135.4(3) ?
Ge3 N1 O2 2_665 . 1_665 41.26(12) ?
Ge3 N1 O2 2_665 . 2_565 135.4(3) ?
Ge3 N1 O2 2_665 . 2_665 41.26(12) ?
Ge3 N1 O2 2_665 . 3_555 91.74(14) ?
Ge3 N1 O2 2_665 . 3_565 91.74(14) ?
Ge3 N1 O2 2_665 . 28_556 47.13(15) ?
Ge3 N1 O2 2_665 . 29_556 94.5(3) ?
Ge3 N1 O2 2_665 . 30_556 47.13(17) ?
Ge3 N1 O2 3_565 . . 91.74(14) ?
Ge3 N1 O2 3_565 . 1_665 91.74(14) ?
Ge3 N1 O2 3_565 . 2_565 41.26(12) ?
Ge3 N1 O2 3_565 . 2_665 135.4(3) ?
Ge3 N1 O2 3_565 . 3_555 135.4(3) ?
Ge3 N1 O2 3_565 . 3_565 41.26(12) ?
Ge3 N1 O2 3_565 . 28_556 94.5(3) ?
Ge3 N1 O2 3_565 . 29_556 47.13(18) ?
Ge3 N1 O2 3_565 . 30_556 47.13(18) ?
O2 N1 O2 . . 1_665 175.44(16) ?
O2 N1 O2 . . 2_565 64.51(15) ?
O2 N1 O2 . . 2_665 120.00(15) ?
O2 N1 O2 . . 3_555 55.48(15) ?
O2 N1 O2 . . 3_565 120.00(15) ?
O2 N1 O2 . . 28_556 88.39(18) ?
O2 N1 O2 . . 29_556 59.36(16) ?
O2 N1 O2 . . 30_556 121.6(3) ?
O2 N1 O2 1_665 . 2_565 120.00(15) ?
O2 N1 O2 1_665 . 2_665 55.48(15) ?
O2 N1 O2 1_665 . 3_555 120.00(15) ?
O2 N1 O2 1_665 . 3_565 64.51(15) ?
O2 N1 O2 1_665 . 28_556 88.39(18) ?
O2 N1 O2 1_665 . 29_556 121.6(3) ?
O2 N1 O2 1_665 . 30_556 59.36(16) ?
O2 N1 O2 2_565 . 2_665 175.44(16) ?
O2 N1 O2 2_565 . 3_555 120.00(15) ?
O2 N1 O2 2_565 . 3_565 55.48(15) ?
O2 N1 O2 2_565 . 28_556 121.6(3) ?
O2 N1 O2 2_565 . 29_556 59.4(2) ?
O2 N1 O2 2_565 . 30_556 88.4(2) ?
O2 N1 O2 2_665 . 3_555 64.51(15) ?
O2 N1 O2 2_665 . 3_565 120.00(15) ?
O2 N1 O2 2_665 . 28_556 59.36(17) ?
O2 N1 O2 2_665 . 29_556 121.6(3) ?
O2 N1 O2 2_665 . 30_556 88.4(2) ?
O2 N1 O2 3_555 . 3_565 175.44(16) ?
O2 N1 O2 3_555 . 28_556 59.36(17) ?
O2 N1 O2 3_555 . 29_556 88.4(2) ?
O2 N1 O2 3_555 . 30_556 121.6(3) ?
O2 N1 O2 3_565 . 28_556 121.6(3) ?
O2 N1 O2 3_565 . 29_556 88.4(2) ?
O2 N1 O2 3_565 . 30_556 59.4(2) ?
O2 N1 O2 28_556 . 29_556 62.3(2) ?
O2 N1 O2 28_556 . 30_556 62.3(2) ?
O2 N1 O2 29_556 . 30_556 62.3(2) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn1 N2 . . 2.175(6) ?
Sn1 N2 . 2_565 2.175(7) ?
Sn1 N2 . 3_455 2.175(6) ?
Sn1 O2 . . 2.067(6) ?
Sn1 O2 . 2_565 2.067(6) ?
Sn1 O2 . 3_455 2.067(6) ?
Ge1 N2 . . 1.862(7) ?
Ge1 N2 . 2_665 1.862(8) ?
Ge1 N2 . 3_565 1.862(7) ?
Ge1 N1 . . 1.889(8) ?
Ge2 Ge2 . 2_565 2.923 ?
Ge2 Ge2 . 2_675 2.923 ?
Ge2 Ge2 . 3_455 2.923 ?
Ge2 Ge2 . 3_465 2.923 ?
Ge2 N2 . . 2.025(7) ?
Ge2 N2 . 2_565 2.025(4) ?
Ge2 N2 . 17_566 2.025(7) ?
Ge2 N2 . 18_456 2.025(9) ?
Ge2 O1 . . 1.937(4) ?
Ge2 O1 . 16_356 1.937(4) ?
Ge3 Ge3 . 2_555 2.923 ?
Ge3 Ge3 . 2_665 2.923 ?
Ge3 Ge3 . 3_555 2.923 ?
Ge3 Ge3 . 3_565 2.923 ?
Ge3 O2 . . 1.940(5) ?
Ge3 O2 . 3_555 1.940(6) ?
Ge3 O2 . 28_556 1.940(5) ?
Ge3 O2 . 29_556 1.940(6) ?
Ge3 N1 . . 1.995(4) ?
Ge3 N1 . 28_446 1.995(4) ?
N2 N2 . 2_565 2.778(10) ?
N2 N2 . 3_455 2.778(7) ?
N2 N2 . 16_456 2.948(9) ?
N2 N2 . 17_566 2.948(7) ?
N2 O1 . 1_545 2.933(6) ?
N2 O1 . . 2.933(5) ?
N2 O1 . 16_356 2.666(9) ?
O2 O2 . 2_555 2.723(8) ?
O2 O2 . 3_555 2.723(8) ?
O2 O2 . 29_556 2.763(8) ?
O2 O2 . 30_446 2.763(8) ?
O2 N1 . 1_445 2.925(3) ?
O2 N1 . . 2.925(3) ?
O2 N1 . 28_446 2.632(9) ?
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_intensity_calc
_refln_intensity_meas
_refln_intensity_sigma
_refln_scale_group_code
_refln_observed_status
-8 8 -7 670.06 184.10 175.40 1 <
-7 6 8 4193.80 3413.80 494.10 1 o
-7 7 -5 359.63 339.40 237.30 1 <
-6 4 23 255.18 331.90 214.40 1 <
-6 5 10 2566.10 3313.00 409.70 1 o
-6 7 -19 583.52 458.10 256.30 1 <
-5 6 -17 696.46 337.50 239.10 1 <
-4 1 37 124.03 231.10 181.90 1 <
-4 2 24 12366.00 15494.60 711.20 1 o
-4 3 11 5296.20 4720.40 535.20 1 o
-4 6 -31 1196.00 729.20 290.70 1 <
-3 4 -16 3560.70 2818.60 427.00 1 o
-2 -1 38 1000.40 1508.70 276.20 1 o
-2 2 -1 394.35 1128.50 559.30 1 <
-2 4 -30 12483.00 9498.70 675.70 1 o
0 -3 39 348.15 683.40 215.90 1 o
0 2 -29 3232.70 1780.50 344.70 1 o
2 -4 27 2420.60 3715.80 416.50 1 o
2 -3 14 2470.20 3112.60 461.80 1 o
2 -2 1 389.29 1676.20 613.80 1 <
4 -6 28 3309.10 2888.70 438.90 1 o
4 -5 15 544.66 649.90 291.80 1 <
4 -2 -27 2792.60 2903.10 422.40 1 o
5 -4 -12 413.93 487.30 311.50 1 <
6 -4 -26 1591.60 989.10 294.70 1 o
7 -8 15 65.25 -83.00 117.00 1 <
7 -7 2 54.40 271.30 263.60 1 <
7 -6 -11 347.73 146.80 222.60 1 <
8 -7 -12 18.69 57.80 128.30 1 <
-8 8 -7 891.52 225.20 258.90 2 <
-7 5 21 142.41 87.50 185.80 2 <
-7 6 8 4839.00 3977.90 513.30 2 o
-6 4 23 306.31 292.50 236.40 2 <
-6 7 -19 817.85 461.40 282.20 2 <
-5 5 -4 2825.30 1752.90 371.50 2 o
-4 1 37 186.78 235.70 207.50 2 <
-4 2 24 18542.00 19878.30 770.90 2 o
-4 3 11 5675.40 5342.50 545.60 2 o
-4 5 -18 1901.80 816.40 333.00 2 <
-3 5 -32 227.03 208.90 238.60 2 <
-2 4 -30 19698.00 12114.30 746.10 2 o
-1 -2 40 70.03 406.50 191.70 2 <
-1 -1 27 6528.30 6190.10 470.00 2 o
-1 2 -15 3218.10 2061.60 417.40 2 o
0 2 -29 4028.80 2664.00 365.70 2 o
1 -3 28 28.21 365.80 226.00 2 <
2 -2 1 607.61 3010.20 651.50 2 o
2 0 -28 15869.00 16773.30 730.50 2 o
3 -5 29 115.58 241.10 239.70 2 <
4 -4 2 46006.00 56136.50 1096.80 2 o
4 -2 -27 3596.50 3331.10 450.90 2 o
5 -4 -12 59.89 340.80 247.80 2 <
6 -7 16 674.33 468.20 206.20 2 <
6 -6 3 73.86 306.20 360.50 2 <
6 -4 -26 2110.00 1174.10 299.80 2 o
7 -6 -11 564.07 181.30 219.70 2 <
-8 7 6 2753.40 1216.50 341.50 3 o
-7 5 21 27.58 -16.10 128.30 3 <
-7 6 8 4640.90 4706.70 503.30 3 o
-7 7 -8 3008.40 1421.40 377.00 3 o
-6 4 23 266.80 223.60 233.30 3 <
-6 6 -6 1365.10 1176.80 321.10 3 o
-6 7 -22 2811.00 1300.90 353.80 3 o
-5 2 38 547.01 389.00 231.50 3 <
-5 6 -20 3309.50 1591.80 348.50 3 o
-4 3 11 5091.80 5245.30 521.90 3 o
-4 6 -34 1157.20 605.00 201.80 3 <
-3 0 39 528.45 725.50 242.80 3 <
-3 1 26 46.85 269.50 278.40 3 <
-3 3 -3 709.16 1041.50 448.40 3 <
-2 -1 41 2257.10 1632.50 296.00 3 o
-2 3 -17 4422.70 3570.60 482.40 3 o
-2 4 -33 1006.80 728.40 269.90 3 <
-1 3 -31 505.09 90.00 217.90 3 <
1 -2 15 3370.60 2453.20 462.70 3 o
1 0 -14 23879.00 26543.80 819.50 3 o
1 1 -30 485.09 627.40 262.60 3 <
2 -4 30 18532.00 23651.80 753.30 3 o
3 -4 16 5101.00 4527.40 412.10 3 o
3 -2 -13 6796.70 5216.70 457.30 3 o
4 -6 31 1872.10 1664.50 309.30 3 o
4 -2 -27 4766.20 4033.10 459.50 3 o
5 -6 17 969.64 1153.80 255.10 3 o
6 -4 -26 1958.00 1227.60 274.90 3 o
7 -6 -11 751.14 309.30 210.60 3 <
8 -8 4 778.56 535.10 287.50 3 <
-8 6 19 42.07 232.90 170.50 4 <
-7 5 21 138.06 268.30 205.00 4 <
-7 6 5 516.83 234.10 264.00 4 <
-7 7 -11 219.46 166.70 208.10 4 <
-6 4 23 255.56 362.80 265.80 4 <
-6 5 7 1228.60 461.20 314.70 4 <
-6 6 -9 167.76 289.60 210.40 4 <
-6 7 -25 887.00 388.40 196.80 4 <
-5 2 38 921.88 663.50 278.00 4 <
-5 4 9 122.10 551.00 304.60 4 <
-5 5 -7 1761.00 620.50 321.50 4 <
-5 6 -23 284.63 122.00 194.60 4 <
-4 1 40 80.82 114.20 186.80 4 <
-4 4 -5 9174.40 8676.90 609.60 4 o
-4 5 -21 472.13 233.60 218.90 4 <
-3 5 -38 835.87 524.40 241.10 4 <
-2 0 28 17520.00 18729.90 735.80 4 o
-2 4 -36 137.06 243.80 209.20 4 <
-1 0 14 26809.00 29098.60 826.40 4 o
-1 3 -34 2442.90 1300.20 309.70 4 o
0 1 -16 19689.00 20497.20 783.70 4 o
0 2 -32 8374.70 6612.70 518.40 4 o
1 -3 31 430.08 799.60 250.70 4 o
3 -4 19 4678.00 5312.70 486.20 4 o
3 -3 3 983.53 899.30 485.80 4 <
3 -1 -29 900.37 494.50 283.00 4 <
4 -6 34 938.36 787.80 239.20 4 o
5 -6 20 2778.10 2361.30 345.90 4 o
6 -6 6 1281.80 1389.40 339.90 4 o
6 -5 -10 3434.40 2921.60 381.50 4 o
6 -4 -26 2058.00 1118.20 296.60 4 o
8 -8 7 865.68 461.10 252.60 4 <
8 -7 -9 75.28 75.60 204.50 4 <
-8 6 19 98.13 139.20 223.10 5 <
-8 7 3 41.97 112.70 231.70 5 <
-7 5 21 60.74 116.90 192.40 5 <
-7 6 5 218.75 109.70 169.00 5 <
-7 7 -11 368.57 310.90 240.60 5 <
-6 4 23 508.34 363.80 245.60 5 <
-6 5 7 934.59 533.60 308.00 5 <
-5 4 9 317.12 329.50 314.10 5 <
-5 6 -26 112.24 531.80 263.50 5 <
-4 1 40 33.02 103.40 180.20 5 <
-4 5 -24 2338.20 2442.60 380.30 5 o
-3 4 -22 12372.00 9452.40 610.20 5 o
-2 3 -20 13692.00 12180.40 630.00 5 o
-1 -1 30 669.56 987.20 346.30 5 <
-1 2 -18 7431.50 8328.70 578.50 5 o
0 -1 16 17001.00 20832.10 774.80 5 o
1 1 -33 5603.00 3794.40 432.50 5 o
2 -4 33 1343.30 1308.60 286.80 5 o
2 0 -31 6769.60 7026.30 505.90 5 o
3 -5 35 589.60 861.70 250.80 5 o
3 -4 19 4380.60 6467.70 476.50 5 o
3 -1 -29 1060.80 664.10 281.20 5 <
4 -5 21 457.92 428.10 254.80 5 <
4 -4 5 8036.60 11071.30 584.40 5 o
4 -3 -11 6147.50 4330.50 492.20 5 o
5 -3 -28 123.01 379.10 186.90 5 <
6 -7 22 2745.10 2353.10 320.90 5 o
6 -4 -26 2250.20 1175.20 314.70 5 o
7 -7 8 4017.80 2356.60 370.00 5 o
7 -6 -8 3632.10 3180.40 385.30 5 o
7 -5 -24 1038.50 700.40 245.60 5 <
-8 6 19 89.09 144.80 201.70 6 <
-7 5 21 36.54 211.40 209.20 6 <
-7 7 -14 1796.30 1205.40 293.30 6 o
-6 4 23 417.58 344.50 252.30 6 <
-5 3 25 2207.80 1009.60 349.80 6 <
-5 6 -26 96.67 334.10 210.50 6 <
-4 5 -24 2201.40 1707.60 351.80 6 o
-2 4 -39 666.62 317.10 184.30 6 <
-1 3 -37 117.97 321.80 188.50 6 <
0 -2 32 5863.80 7073.40 492.60 6 o
0 2 -35 852.59 612.90 265.70 6 <
1 -3 34 2000.00 1922.40 318.30 6 o
1 -2 18 5895.70 8874.80 587.00 6 o
1 1 -33 5706.20 4489.30 420.00 6 o
3 -2 -13 4111.20 5123.00 465.80 6 o
4 -3 -11 4773.00 5022.00 475.80 6 o
5 -6 23 208.86 264.00 178.90 6 <
5 -5 7 1594.10 936.50 291.90 6 o
5 -3 -28 267.62 171.40 165.50 6 <
6 -7 25 836.17 493.70 236.80 6 <
6 -4 -26 1664.50 1347.00 297.30 6 o
7 -6 -8 4894.00 4031.90 388.20 6 o
7 -5 -24 1084.90 706.60 239.50 6 <
8 -7 -6 2131.40 1453.20 301.80 6 o
-8 7 0 1551.80 878.70 294.50 7 <
-7 6 2 311.95 1304.90 344.30 7 o
-7 7 -17 78.63 135.50 220.90 7 <
-6 4 23 513.38 385.70 253.80 7 <
-6 5 4 3244.10 3439.00 429.50 7 o
-6 6 -15 370.21 128.80 253.70 7 <
-5 3 25 2012.20 1189.40 355.60 7 o
-5 6 -32 147.94 11.00 108.70 7 <
-4 2 27 4077.00 3995.00 442.30 7 o
-3 1 29 1084.30 804.10 267.90 7 o
-2 0 31 6691.70 7333.70 526.60 7 o
-2 3 -23 1007.80 1275.60 322.50 7 o
-1 -1 33 5332.10 4760.60 431.40 7 o
-1 2 -21 2909.20 1642.10 360.80 7 o
0 -2 35 554.20 696.30 283.50 7 <
0 1 -19 17494.00 18863.50 830.30 7 o
0 2 -38 5172.40 3746.60 405.80 7 o
1 -3 37 228.38 487.20 248.60 7 <
1 -1 2 42335.00 28810.50 1158.20 7 o
1 0 -17 3920.40 5502.00 478.00 7 o
1 1 -36 1697.80 1477.30 317.30 7 o
2 -4 39 1008.00 966.50 228.70 7 o
2 -2 4 97638.00 100325.00 1493.40 7 o
2 -1 -15 2607.70 3463.90 473.50 7 o
2 0 -34 2243.70 2759.20 362.40 7 o
3 -3 6 81043.00 83327.40 1286.60 7 o
3 -2 -13 3931.90 5932.40 504.00 7 o
3 -1 -32 246.80 544.60 222.80 7 <
4 -4 8 3268.20 6509.70 545.00 7 o
4 -3 -11 5893.10 5156.10 476.30 7 o
4 -2 -30 14531.00 14042.80 650.00 7 o
5 -6 26 76.30 988.60 250.40 7 o
5 -5 10 2549.90 5711.90 470.10 7 o
5 -4 -9 219.54 667.70 246.60 7 <
5 -3 -28 152.19 406.10 190.90 7 <
6 -6 12 2025.90 2450.30 352.90 7 o
6 -5 -7 878.24 532.40 248.00 7 <
6 -4 -26 1600.00 1570.90 276.90 7 o
7 -6 -5 222.92 473.20 257.00 7 <
7 -5 -24 991.21 917.40 236.10 7 o
8 -7 -3 95.69 78.20 182.60 7 <
-8 6 16 4968.30 3079.60 446.50 8 o
-8 7 -3 175.88 195.30 168.00 8 <
-7 7 -20 1415.60 536.40 242.50 8 <
-6 5 4 2866.20 3051.90 428.20 8 o
-5 3 25 1650.30 1851.50 322.40 8 o
-5 4 6 17521.00 15621.00 656.70 8 o
-5 5 -13 1218.80 756.30 286.60 8 <
-4 2 27 3554.80 4509.80 483.50 8 o
-4 4 -11 8715.90 9887.70 665.10 8 o
-4 5 -30 297.91 330.00 231.10 8 <
-3 1 29 982.47 1482.40 318.20 8 o
-3 4 -28 124.57 582.20 224.60 8 <
0 -1 19 21598.00 24923.60 811.50 8 o
0 2 -41 1140.10 961.60 259.10 8 o
1 -2 21 2747.90 2840.10 376.00 8 o
1 0 -17 5178.00 8070.60 589.10 8 o
1 1 -39 925.06 679.50 245.40 8 <
2 -3 23 453.08 1998.80 365.60 8 o
2 -1 -15 1784.30 4712.90 496.00 8 o
3 -4 25 3207.20 4955.30 396.40 8 o
3 -1 -32 664.50 670.80 257.30 8 <
4 -5 27 1867.70 965.30 256.60 8 o
4 -2 -30 19739.00 13864.30 669.00 8 o
5 -6 29 308.66 433.50 223.10 8 <
5 -3 -28 428.14 485.80 246.80 8 <
6 -4 -26 2103.20 1596.40 317.50 8 o
7 -7 14 1422.50 1318.60 287.50 8 o
7 -5 -24 1024.60 843.80 283.80 8 <
8 -7 -3 90.34 185.40 163.50 8 <
-8 7 -6 1769.50 1691.20 359.20 9 o
-7 5 18 925.23 1298.00 324.00 9 o
-6 5 1 3701.50 4218.40 480.20 9 o
-6 6 -21 814.57 5826.00 488.10 9 o
-5 3 25 2580.30 1537.30 355.40 9 o
-5 5 -16 796.93 607.60 316.80 9 <
-4 2 27 3671.20 4115.80 436.50 9 o
-4 3 8 44268.00 37486.60 962.40 9 o
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loop_
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1 1924.295
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