#------------------------------------------------------------------------------ #$Date: 2024-05-17 05:02:20 +0300 (Fri, 17 May 2024) $ #$Revision: 291900 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312507.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312507 loop_ _publ_author_name 'Chinchan, Kunlanit' 'Jiajaroen, Suwadee' 'Theppitak, Chatphorn' 'Laksee, Sakchai' 'Sukwattanasinitt, Mongkol' 'Chainok, Kittipong' _publ_section_title ; Synthesis, structure and photoluminescence properties of heterometallic-based coordination polymers of trimesic acid. ; _journal_coeditor_code JX3081 _journal_issue 6 _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_paper_doi 10.1107/S2053229624003528 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Ca Co (C6 H4 O6)2 (H2 O)8]' _chemical_formula_moiety 'C18 H24 Ca Co O20' _chemical_formula_sum 'C18 H24 Ca Co O20' _chemical_formula_weight 659.38 _chemical_name_systematic catena-Poly[[tetraaquacobalt(II)]-\m-5-carboxybenzene-1,3-dicarboxylato-[tetraaquacalcium(II)]-\m-5-carboxybenzene-1,3-dicarboxylato] _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary geom _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 98.557(9) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.875(5) _cell_length_b 20.192(4) _cell_length_c 6.5339(16) _cell_measurement_reflns_used 1029 _cell_measurement_temperature 296 _cell_measurement_theta_max 25.242 _cell_measurement_theta_min 3.063 _cell_volume 2332.0(10) _computing_cell_refinement ; SAINT (Bruker, 2021) ; _computing_data_collection ; APEX4 (Bruker, 2021) ; _computing_data_reduction ; SAINT (Bruker, 2021) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296 _diffrn_detector 'Bruker PHOTON 200 area detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'four-circle KAPPA diffractometer' _diffrn_measurement_device_type 'Bruker D8 QUEST CMOS PHOTON II' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0490 _diffrn_reflns_av_unetI/netI 0.0296 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 15563 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.405 _diffrn_reflns_theta_min 3.063 _diffrn_source 'sealed x-ray tube' _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 1.059 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6894 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2021) ; _exptl_crystal_colour 'light pink' _exptl_crystal_density_diffrn 1.878 _exptl_crystal_description Block _exptl_crystal_F_000 1356 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.333 _refine_diff_density_min -0.279 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 207 _refine_ls_number_reflns 2391 _refine_ls_number_restraints 17 _refine_ls_restrained_S_all 1.046 _refine_ls_R_factor_all 0.0410 _refine_ls_R_factor_gt 0.0278 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0313P)^2^+2.5603P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0623 _refine_ls_wR_factor_ref 0.0684 _reflns_number_gt 1996 _reflns_number_total 2391 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 2.res in C2/c 2.res created by SHELXL-2018/3 at 15:07:50 on 18-Apr-2024 CELL 0.71073 17.8748 20.1921 6.5339 90 98.557 90 ZERR 4 0.0045 0.0041 0.0016 0 0.009 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Ca O Co UNIT 72 96 4 80 4 EQIV $1 -X,+Y,0.5-Z EQIV $2 -1-X,-Y,-Z EQIV $3 -0.5-X,-0.5+Y,-0.5-Z EQIV $4 +X,-Y,-0.5+Z EQIV $5 -0.5-X,-0.5-Y,-Z EQIV $6 -X,-Y,-Z EQIV $7 -0.5-X,0.5-Y,-Z EQIV $8 0.5+X,0.5+Y,+Z DFIX 0.85 O10 H10a O10 H10b DANG 1.34 H10a H10b SADI Ca1 H10a Ca1 H10b DFIX 0.85 O8 H8a O8 H8b DANG 1.34 H8a H8b SADI Co1 H8a Co1 H8b DFIX 0.85 O7 H7a O7 H7b DANG 1.34 H7a H7b SADI Co1 H7a Co1 H7b DFIX 0.82 O6 H6 RIGU 0.0001 0.0001 Ca1 Ca1 DFIX 0.85 O9 H9a DFIX 0.85 O9 H9b DFIX 1.4 H9b H9a DFIX 2.24 O5 H6 L.S. 10 PLAN 5 SIZE 0.18 0.39 0.41 TEMP 22.85 CONF HTAB O6 O2_$2 HTAB O7 O4_$3 HTAB O7 O5_$4 HTAB O8 O2_$5 HTAB O8 O4_$4 HTAB O8 O5_$3 HTAB O9 O3_$6 HTAB O10 O5_$7 HTAB O10 O7_$8 FREE Ca1 C8_$1 FREE Ca1 C8 FREE Ca1 H9b_$1 FREE Ca1 H9b LIST 4 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.031300 2.560300 FVAR 0.05813 CO1 5 -0.250000 -0.250000 0.000000 10.50000 0.01398 0.00937 = 0.02114 0.00086 0.00395 0.00099 CA1 3 0.000000 0.126354 0.250000 10.50000 0.01179 0.01356 = 0.02707 0.00000 -0.00009 0.00000 O1 4 -0.261533 -0.148445 -0.015913 11.00000 0.01647 0.00996 = 0.03622 0.00125 0.00694 0.00259 O2 4 -0.385042 -0.139060 -0.018092 11.00000 0.01520 0.01157 = 0.06774 -0.00222 0.00828 -0.00116 O3 4 -0.091328 0.040806 0.106578 11.00000 0.01591 0.01770 = 0.05630 -0.00650 -0.00436 0.00134 O4 4 -0.133762 0.142651 0.063030 11.00000 0.01721 0.01282 = 0.03428 -0.00102 0.00293 -0.00255 O5 4 -0.420375 0.176999 -0.028137 11.00000 0.01986 0.01022 = 0.05870 0.00103 0.00456 0.00223 O6 4 -0.487774 0.085710 -0.003894 11.00000 0.01660 0.01496 = 0.09386 0.00092 0.01876 0.00132 H6 2 -0.523404 0.112461 0.002477 11.00000 0.08675 O7 4 -0.352906 -0.268950 -0.211645 11.00000 0.02337 0.01772 = 0.02570 -0.00073 -0.00047 0.00221 H7A 2 -0.349407 -0.297205 -0.299553 11.00000 -1.50000 H7B 2 -0.370498 -0.235008 -0.275628 11.00000 -1.50000 O8 4 -0.190738 -0.248511 -0.250148 11.00000 0.02336 0.01772 = 0.03009 0.00394 0.01191 0.00339 H8A 2 -0.180001 -0.212991 -0.300505 11.00000 -1.50000 H8B 2 -0.152559 -0.272606 -0.245970 11.00000 -1.50000 O9 4 0.055394 0.089551 -0.052269 11.00000 0.04105 0.02362 = 0.04426 -0.00570 0.01296 0.00733 AFIX 3 H9A 2 0.065634 0.051501 -0.092519 11.00000 0.07337 H9B 2 0.073504 0.120881 -0.116119 11.00000 0.28647 AFIX 0 O10 4 0.024521 0.220936 0.047305 11.00000 0.02913 0.02201 = 0.05303 0.01195 0.01896 0.00698 H10A 2 0.000086 0.257714 0.045992 11.00000 -1.50000 H10B 2 0.061279 0.227223 -0.015676 11.00000 -1.50000 C1 1 -0.320398 -0.114262 -0.014825 11.00000 0.01856 0.01172 = 0.01782 0.00046 0.00286 0.00073 C2 1 -0.309697 -0.039881 -0.009757 11.00000 0.01728 0.01125 = 0.01583 0.00049 0.00343 0.00009 C3 1 -0.236983 -0.013709 0.015502 11.00000 0.01638 0.01407 = 0.01649 0.00032 0.00172 0.00285 AFIX 43 H3 2 -0.195739 -0.042261 0.027325 11.00000 -1.20000 AFIX 0 C4 1 -0.224625 0.054457 0.023469 11.00000 0.01491 0.01309 = 0.01464 -0.00072 0.00190 -0.00105 C5 1 -0.286231 0.097328 0.005046 11.00000 0.01687 0.00936 = 0.01753 -0.00011 0.00300 -0.00164 AFIX 43 H5 2 -0.278678 0.142906 0.006890 11.00000 -1.20000 AFIX 0 C6 1 -0.359359 0.071535 -0.016198 11.00000 0.01383 0.01273 = 0.01915 0.00071 0.00276 0.00152 C7 1 -0.370859 0.003332 -0.024721 11.00000 0.01464 0.01312 = 0.02213 -0.00038 0.00250 -0.00195 AFIX 43 H7 2 -0.419827 -0.013462 -0.040546 11.00000 -1.20000 AFIX 0 C8 1 -0.145106 0.080406 0.064590 11.00000 0.01686 0.01548 = 0.01985 -0.00281 0.00229 0.00048 C9 1 -0.425258 0.116761 -0.018338 11.00000 0.01573 0.01369 = 0.02563 -0.00099 0.00123 0.00075 HKLF 4 REM 2.res in C2/c REM wR2 = 0.068379, GooF = S = 1.04690, Restrained GooF = 1.04634 for all data REM R1 = 0.027793 for 1996 Fo > 4sig(Fo) and 0.040954 for all 2391 data REM 207 parameters refined using 17 restraints END WGHT 0.0312 2.5667 REM Highest difference peak 0.333, deepest hole -0.279, 1-sigma level 0.065 Q1 1 -0.2543 0.0734 0.0192 11.00000 0.05 0.33 Q2 1 -0.2770 -0.0279 -0.0275 11.00000 0.05 0.32 Q3 1 -0.3826 0.0934 0.0290 11.00000 0.05 0.32 Q4 1 -0.3181 -0.0714 -0.0016 11.00000 0.05 0.31 Q5 1 -0.3271 0.0806 -0.0225 11.00000 0.05 0.29 REM The information below was added by Olex2. REM REM R1 = 0.027793 for 1996 Fo > 4sig(Fo) and 0.040954 for all 15824 data REM 207 parameters refined using n/a restraints REM Highest difference peak 0.33, deepest hole -0.28 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.040954 REM R1_gt = 0.027793 REM wR_ref = 0.068379 REM GOOF = 1.04690 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 15824 REM Reflections_gt = 1996 REM Parameters = 207 REM Hole = -0.28 REM Peak = 0.33 REM Flack = n/a ; _cod_data_source_file jx3081sup1.cif _cod_data_source_block 2 _cod_original_cell_volume 2332.0(9) _cod_database_code 2312507 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.671 _shelx_estimated_absorpt_t_max 0.832 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co Co1 -0.250000 -0.250000 0.000000 0.01469(11) Uani d 1 . . Ca Ca1 0.000000 0.12635(3) 0.250000 0.01778(14) Uani d 1 . . O O1 -0.26153(7) -0.14844(6) -0.0159(2) 0.0206(3) Uani d 1 . . O O2 -0.38504(8) -0.13906(7) -0.0181(3) 0.0313(4) Uani d 1 . . O O3 -0.09133(8) 0.04081(7) 0.1066(3) 0.0310(4) Uani d 1 . . O O4 -0.13376(8) 0.14265(6) 0.0630(2) 0.0215(3) Uani d 1 . . O O5 -0.42037(8) 0.17700(7) -0.0281(3) 0.0297(4) Uani d 1 . . O O6 -0.48777(9) 0.08571(7) -0.0039(3) 0.0407(5) Uani d 1 . . H H6 -0.5234(11) 0.1125(10) 0.002(6) 0.087(13) Uiso d 1 . . O O7 -0.35291(8) -0.26895(7) -0.2116(2) 0.0227(3) Uani d 1 . . H H7A -0.3494(13) -0.2972(10) -0.300(3) 0.034 Uiso d 1 . . H H7B -0.3705(12) -0.2350(9) -0.276(3) 0.034 Uiso d 1 . . O O8 -0.19074(8) -0.24851(7) -0.2501(2) 0.0229(3) Uani d 1 . . H H8A -0.1800(13) -0.2130(9) -0.301(3) 0.034 Uiso d 1 . . H H8B -0.1526(11) -0.2726(11) -0.246(4) 0.034 Uiso d 1 . . O O9 0.05539(10) 0.08955(8) -0.0523(3) 0.0356(4) Uani d 1 . . H H9A 0.065634 0.051501 -0.092519 0.073(11) Uiso d 1 . . H H9B 0.073504 0.120881 -0.116119 0.29(4) Uiso d 1 . . O O10 0.02452(9) 0.22094(8) 0.0473(3) 0.0334(4) Uani d 1 . . H H10A 0.0001(14) 0.2577(9) 0.046(4) 0.050 Uiso d 1 . . H H10B 0.0613(13) 0.2272(12) -0.016(4) 0.050 Uiso d 1 . . C C1 -0.32040(11) -0.11426(9) -0.0148(3) 0.0160(4) Uani d 1 . . C C2 -0.30970(11) -0.03988(9) -0.0098(3) 0.0147(4) Uani d 1 . . C C3 -0.23698(11) -0.01371(9) 0.0155(3) 0.0157(4) Uani d 1 . . H H3 -0.195739 -0.042261 0.027325 0.019 Uiso calc 1 . . C C4 -0.22463(11) 0.05446(9) 0.0235(3) 0.0142(4) Uani d 1 . . C C5 -0.28623(11) 0.09733(9) 0.0050(3) 0.0145(4) Uani d 1 . . H H5 -0.278678 0.142906 0.006890 0.017 Uiso calc 1 . . C C6 -0.35936(11) 0.07153(9) -0.0162(3) 0.0152(4) Uani d 1 . . C C7 -0.37086(11) 0.00333(9) -0.0247(3) 0.0167(4) Uani d 1 . . H H7 -0.419827 -0.013462 -0.040546 0.020 Uiso calc 1 . . C C8 -0.14511(11) 0.08041(9) 0.0646(3) 0.0174(4) Uani d 1 . . C C9 -0.42526(11) 0.11676(9) -0.0183(3) 0.0185(4) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.0140(2) 0.00937(18) 0.0211(2) 0.00099(13) 0.00395(15) 0.00086(14) Ca1 0.0118(3) 0.0136(3) 0.0271(3) 0.000 -0.0001(2) 0.000 O1 0.0165(7) 0.0100(6) 0.0362(9) 0.0026(5) 0.0069(6) 0.0012(6) O2 0.0152(8) 0.0116(7) 0.0677(12) -0.0012(6) 0.0083(7) -0.0022(7) O3 0.0159(8) 0.0177(7) 0.0563(11) 0.0013(6) -0.0044(7) -0.0065(7) O4 0.0172(7) 0.0128(7) 0.0343(8) -0.0026(5) 0.0029(6) -0.0010(6) O5 0.0199(8) 0.0102(7) 0.0587(11) 0.0022(6) 0.0046(7) 0.0010(7) O6 0.0166(8) 0.0150(7) 0.0939(15) 0.0013(6) 0.0188(9) 0.0009(8) O7 0.0234(8) 0.0177(7) 0.0257(8) 0.0022(6) -0.0005(6) -0.0007(6) O8 0.0234(8) 0.0177(7) 0.0301(8) 0.0034(6) 0.0119(6) 0.0039(6) O9 0.0410(10) 0.0236(9) 0.0443(10) 0.0073(7) 0.0130(8) -0.0057(8) O10 0.0291(9) 0.0220(8) 0.0530(11) 0.0070(7) 0.0190(8) 0.0120(8) C1 0.0186(10) 0.0117(9) 0.0178(10) 0.0007(7) 0.0029(8) 0.0005(7) C2 0.0173(10) 0.0112(9) 0.0158(10) 0.0001(7) 0.0034(8) 0.0005(7) C3 0.0164(10) 0.0141(9) 0.0165(10) 0.0029(7) 0.0017(8) 0.0003(7) C4 0.0149(9) 0.0131(9) 0.0146(9) -0.0010(7) 0.0019(7) -0.0007(7) C5 0.0169(10) 0.0094(8) 0.0175(10) -0.0016(7) 0.0030(8) -0.0001(7) C6 0.0138(10) 0.0127(9) 0.0191(10) 0.0015(7) 0.0028(8) 0.0007(7) C7 0.0146(10) 0.0131(9) 0.0221(10) -0.0019(7) 0.0025(8) -0.0004(8) C8 0.0169(10) 0.0155(9) 0.0199(10) 0.0005(8) 0.0023(8) -0.0028(8) C9 0.0157(10) 0.0137(10) 0.0256(11) 0.0008(7) 0.0012(8) -0.0010(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l 4 0 0 -4 0 0 -4 0 0 4 0 0 6 0 0 6 0 0 -6 0 0 -6 0 0 -8 0 0 8 0 0 8 0 0 -8 0 0 -10 0 0 10 0 0 -10 0 0 10 0 0 -12 0 0 12 0 0 -12 0 0 12 0 0 14 0 0 -14 0 0 14 0 0 16 0 0 -16 0 0 -16 0 0 16 0 0 18 0 0 -18 0 0 18 0 0 -18 0 0 -20 0 0 -20 0 0 20 0 0 20 0 0 -22 0 0 -22 0 0 22 0 0 3 -1 0 -3 -1 0 -3 -1 0 3 -1 0 -3 1 0 3 1 0 3 1 0 5 -1 0 -5 -1 0 5 -1 0 -5 -1 0 5 1 0 -5 1 0 -5 1 0 5 1 0 -7 -1 0 -7 -1 0 7 -1 0 7 -1 0 7 1 0 -7 1 0 -7 1 0 7 1 0 -9 -1 0 -9 -1 0 9 -1 0 9 -1 0 9 1 0 -9 1 0 9 1 0 -9 1 0 11 -1 0 -11 -1 0 11 -1 0 -11 -1 0 11 1 0 11 1 0 -11 1 0 -11 1 0 -13 -1 0 -13 -1 0 13 -1 0 13 -1 0 -13 1 0 -13 1 0 13 1 0 15 -1 0 -15 -1 0 15 -1 0 15 1 0 -15 1 0 -15 1 0 15 1 0 -17 -1 0 -17 -1 0 17 -1 0 17 -1 0 -17 1 0 -17 1 0 17 1 0 17 1 0 -19 -1 0 -19 -1 0 19 -1 0 19 -1 0 19 1 0 -19 1 0 -19 1 0 19 1 0 -21 -1 0 21 -1 0 -21 -1 0 21 -1 0 -21 1 0 -21 1 0 21 1 0 21 1 0 2 -2 0 -2 -2 0 -2 -2 0 2 -2 0 4 -2 0 4 -2 0 -4 -2 0 -4 -2 0 4 2 0 -4 2 0 -4 2 0 4 2 0 -6 -2 0 -6 -2 0 6 -2 0 6 -2 0 6 2 0 -6 2 0 -6 2 0 -8 -2 0 8 -2 0 8 -2 0 -8 -2 0 -8 2 0 8 2 0 -8 2 0 8 2 0 10 -2 0 10 -2 0 -10 -2 0 -10 -2 0 10 2 0 10 2 0 -10 2 0 -10 2 0 -12 -2 0 12 -2 0 12 -2 0 -12 -2 0 -12 2 0 12 2 0 -12 2 0 12 2 0 -14 -2 0 14 -2 0 -14 -2 0 14 -2 0 14 2 0 -14 2 0 14 2 0 -14 2 0 16 -2 0 16 -2 0 -16 -2 0 16 2 0 -16 2 0 -16 2 0 16 2 0 -18 -2 0 18 -2 0 -18 -2 0 18 -2 0 18 2 0 -18 2 0 18 2 0 -18 2 0 20 -2 0 20 -2 0 -20 -2 0 -20 -2 0 20 2 0 -20 2 0 -20 2 0 20 2 0 -22 -2 0 22 -2 0 22 2 0 -22 2 0 -1 3 0 1 3 0 -1 3 0 3 -3 0 -3 -3 0 -3 -3 0 3 -3 0 3 3 0 -3 3 0 5 -3 0 -5 -3 0 -5 -3 0 5 -3 0 5 3 0 -5 3 0 -5 3 0 -7 -3 0 7 -3 0 -7 -3 0 7 -3 0 7 3 0 -7 3 0 7 3 0 -7 3 0 -9 -3 0 9 -3 0 9 -3 0 9 3 0 -9 3 0 -9 3 0 9 3 0 -11 -3 0 11 -3 0 -11 -3 0 11 -3 0 11 3 0 -11 3 0 -11 3 0 11 3 0 13 -3 0 -13 -3 0 -13 -3 0 13 -3 0 -13 3 0 13 3 0 13 3 0 -13 3 0 -15 -3 0 15 -3 0 15 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7 -3 -7 -7 3 -7 7 3 7 7 3 7 7 -3 7 -7 5 -7 7 -5 -7 -7 -5 -7 -7 5 7 7 5 7 7 10 -8 -7 -10 -8 7 10 -8 -7 -10 -8 7 -10 8 7 -10 8 7 10 8 -7 -8 -8 7 8 -8 -7 -8 -8 7 8 -8 -7 -8 8 7 -8 8 7 -6 -8 7 -6 -8 7 6 -8 -7 6 -8 -7 6 8 -7 -6 8 7 -6 8 7 4 -8 -7 -4 -8 7 -4 -8 7 4 -8 -7 4 8 -7 -4 8 7 -4 8 7 2 -8 -7 2 -8 -7 -2 -8 7 -2 -8 7 2 8 -7 -2 8 7 -2 8 7 0 -8 -7 0 -8 7 0 -8 7 0 -8 -7 0 8 7 0 8 7 0 8 -7 2 -8 7 -2 -8 -7 -2 -8 -7 2 -8 7 -2 8 -7 2 8 7 2 8 7 -4 -8 -7 4 -8 7 -4 -8 -7 4 -8 7 4 8 7 -4 8 -7 4 8 7 -6 -8 -7 -6 -8 -7 6 -8 7 6 8 7 6 8 7 11 -9 -7 11 9 -7 -11 9 7 -11 9 7 9 -9 -7 9 -9 -7 -9 -9 7 -9 -9 7 -9 9 7 -9 9 7 9 9 -7 -7 -9 7 7 -9 -7 7 -9 -7 -7 -9 7 -7 9 7 7 9 -7 -7 9 7 5 -9 -7 5 -9 -7 -5 -9 7 -5 -9 7 5 9 -7 -5 9 7 -5 9 7 3 -9 -7 -3 -9 7 3 -9 -7 -3 -9 7 -3 9 7 3 9 -7 -3 9 7 1 -9 -7 -1 -9 7 1 -9 -7 -1 -9 7 1 9 -7 -1 9 7 -1 -9 -7 1 -9 7 1 -9 7 -1 -9 -7 -1 9 -7 1 9 7 -3 -9 -7 -3 -9 -7 3 -9 7 3 -9 7 -3 9 -7 3 9 7 3 9 7 -5 -9 -7 -5 -9 -7 5 -9 7 5 9 7 5 9 7 10 -10 -7 -10 -10 7 10 -10 -7 -10 10 7 10 10 -7 -10 10 7 -8 -10 7 8 -10 -7 8 -10 -7 -8 -10 7 8 10 -7 -8 10 7 -8 10 7 -6 -10 7 6 -10 -7 -6 -10 7 6 -10 -7 -6 10 7 -6 10 7 6 10 -7 4 -10 -7 4 -10 -7 -4 -10 7 -4 -10 7 4 10 -7 -4 10 7 2 -10 -7 -2 -10 7 2 -10 -7 -2 -10 7 -2 10 7 2 10 -7 -2 10 7 0 -10 -7 0 -10 7 0 -10 7 0 -10 -7 0 10 7 0 10 -7 0 10 7 -2 -10 -7 2 -10 7 -2 -10 -7 2 -10 7 -2 10 -7 2 10 7 2 10 7 -4 -10 -7 -4 -10 -7 4 -10 7 4 10 7 9 -11 -7 -9 11 7 9 11 -7 -7 -11 7 7 -11 -7 -7 -11 7 7 -11 -7 -7 11 7 7 11 -7 -7 11 7 5 -11 -7 -5 -11 7 5 -11 -7 -5 -11 7 -5 11 7 5 11 -7 -5 11 7 3 -11 -7 -3 -11 7 3 -11 -7 -3 -11 7 3 11 -7 -3 11 7 -3 11 7 -1 -11 7 1 -11 -7 1 -11 -7 -1 -11 7 -1 11 7 1 11 -7 -1 11 7 -1 -11 -7 1 -11 7 -1 -11 -7 1 -11 7 -1 11 -7 1 11 7 1 11 7 -3 -11 -7 -3 -11 -7 3 11 7 3 11 7 -3 11 -7 6 -12 -7 6 -12 -7 -6 -12 7 -6 -12 7 -6 12 7 -6 12 7 4 -12 -7 4 -12 -7 -4 -12 7 -4 -12 7 -4 12 7 -4 12 7 2 -12 -7 2 -12 -7 -2 -12 7 -2 -12 7 -2 12 7 -2 12 7 2 12 -7 0 -12 7 0 -12 -7 0 -12 7 0 -12 -7 0 12 7 0 12 7 0 12 -7 3 -13 -7 3 -13 -7 -3 -13 7 -3 13 7 -3 13 7 -6 0 8 -4 0 8 -2 0 8 0 0 8 -7 -1 8 -7 1 8 -5 -1 8 -5 1 8 -3 -1 8 -3 1 8 -1 -1 8 -1 1 8 1 -1 8 1 1 8 -6 -2 8 -6 2 8 -4 -2 8 -4 2 8 -2 -2 8 -2 2 8 0 -2 8 0 2 8 -7 -3 8 -7 3 8 -5 -3 8 -5 3 8 -3 -3 8 -3 3 8 -1 -3 8 -1 3 8 -6 -4 8 -6 4 8 -4 -4 8 -4 4 8 -2 -4 8 -2 4 8 -3 -5 8 -3 5 8 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Co1 O1 . 7_445 180.0 ? O1 Co1 O7 7_445 . 85.73(5) ? O1 Co1 O7 . 7_445 85.73(5) ? O1 Co1 O7 . . 94.27(5) ? O1 Co1 O7 7_445 7_445 94.27(5) ? O1 Co1 O8 . 7_445 89.72(5) ? O1 Co1 O8 . . 90.27(5) ? O1 Co1 O8 7_445 7_445 90.28(5) ? O1 Co1 O8 7_445 . 89.73(5) ? O7 Co1 O7 . 7_445 180.0 ? O8 Co1 O7 . . 89.10(6) ? O8 Co1 O7 7_445 . 90.90(6) ? O8 Co1 O7 . 7_445 90.90(6) ? O8 Co1 O7 7_445 7_445 89.10(6) ? O8 Co1 O8 7_445 . 180.0 ? O3 Ca1 O3 . 2 90.98(7) ? O3 Ca1 O4 2 2 52.03(5) ? O3 Ca1 O4 . . 52.03(5) ? O3 Ca1 O4 . 2 142.83(5) ? O3 Ca1 O4 2 . 142.83(5) ? O4 Ca1 O4 2 . 165.11(6) ? O9 Ca1 O3 . 2 76.69(6) ? O9 Ca1 O3 2 2 78.78(6) ? O9 Ca1 O3 2 . 76.69(6) ? O9 Ca1 O3 . . 78.78(6) ? O9 Ca1 O4 2 2 96.66(5) ? O9 Ca1 O4 2 . 87.86(6) ? O9 Ca1 O4 . . 96.66(5) ? O9 Ca1 O4 . 2 87.86(6) ? O9 Ca1 O9 2 . 144.73(8) ? O10 Ca1 O3 . 2 127.04(5) ? O10 Ca1 O3 2 2 120.85(6) ? O10 Ca1 O3 . . 120.85(6) ? O10 Ca1 O3 2 . 127.04(5) ? O10 Ca1 O4 . 2 85.77(5) ? O10 Ca1 O4 . . 82.40(5) ? O10 Ca1 O4 2 . 85.77(5) ? O10 Ca1 O4 2 2 82.40(5) ? O10 Ca1 O9 2 . 144.47(6) ? O10 Ca1 O9 . 2 144.47(6) ? O10 Ca1 O9 2 2 70.62(6) ? O10 Ca1 O9 . . 70.62(6) ? O10 Ca1 O10 2 . 74.63(9) ? C1 O1 Co1 . . 128.47(12) ? C8 O3 Ca1 . . 94.55(12) ? C8 O4 Ca1 . . 90.45(11) ? C9 O6 H6 . . 111.1(13) ? Co1 O7 H7A . . 115.2(16) ? Co1 O7 H7B . . 113.2(15) ? H7A O7 H7B . . 106(2) ? Co1 O8 H8A . . 120.2(15) ? Co1 O8 H8B . . 118.4(15) ? H8A O8 H8B . . 106(2) ? Ca1 O9 H9A . . 131.4 ? Ca1 O9 H9B . . 113.5 ? H9A O9 H9B . . 114.3 ? Ca1 O10 H10A . . 123.9(15) ? Ca1 O10 H10B . . 127.9(16) ? H10A O10 H10B . . 107(2) ? O1 C1 C2 . . 116.17(17) ? O2 C1 O1 . . 123.26(17) ? O2 C1 C2 . . 120.57(17) ? C3 C2 C1 . . 119.52(17) ? C3 C2 C7 . . 118.76(17) ? C7 C2 C1 . . 121.70(17) ? C2 C3 H3 . . 119.3 ? C2 C3 C4 . . 121.34(17) ? C4 C3 H3 . . 119.3 ? C3 C4 C8 . . 119.47(17) ? C5 C4 C3 . . 119.48(17) ? C5 C4 C8 . . 120.95(17) ? C4 C5 H5 . . 120.2 ? C4 C5 C6 . . 119.61(17) ? C6 C5 H5 . . 120.2 ? C5 C6 C9 . . 120.02(16) ? C7 C6 C5 . . 120.26(17) ? C7 C6 C9 . . 119.63(17) ? C2 C7 C6 . . 120.52(18) ? C2 C7 H7 . . 119.7 ? C6 C7 H7 . . 119.7 ? O3 C8 O4 . . 121.02(18) ? O3 C8 C4 . . 119.55(17) ? O4 C8 C4 . . 119.39(17) ? O5 C9 O6 . . 123.65(18) ? O5 C9 C6 . . 123.26(18) ? O6 C9 C6 . . 113.07(16) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 O1 . 2.0620(13) ? Co1 O1 7_445 2.0621(13) ? Co1 O7 . 2.1645(15) ? Co1 O7 7_445 2.1646(15) ? Co1 O8 7_445 2.0760(15) ? Co1 O8 . 2.0760(15) ? Ca1 O3 2 2.4641(15) ? Ca1 O3 . 2.4641(15) ? Ca1 O4 . 2.5393(15) ? Ca1 O4 2 2.5393(15) ? Ca1 O9 2 2.4526(17) ? Ca1 O9 . 2.4526(17) ? Ca1 O10 . 2.4013(16) ? Ca1 O10 2 2.4013(16) ? O1 C1 . 1.259(2) ? O2 C1 . 1.257(2) ? O3 C8 . 1.249(2) ? O4 C8 . 1.273(2) ? O5 C9 . 1.222(2) ? O6 H6 . 0.841(18) ? O6 C9 . 1.297(2) ? O7 H7A . 0.819(15) ? O7 H7B . 0.839(15) ? O8 H8A . 0.824(15) ? O8 H8B . 0.835(15) ? O9 H9A . 0.8410 ? O9 H9B . 0.8481 ? O10 H10A . 0.861(15) ? O10 H10B . 0.835(16) ? C1 C2 . 1.514(3) ? C2 C3 . 1.390(3) ? C2 C7 . 1.391(3) ? C3 H3 . 0.9300 ? C3 C4 . 1.394(3) ? C4 C5 . 1.392(3) ? C4 C8 . 1.501(3) ? C5 H5 . 0.9300 ? C5 C6 . 1.395(3) ? C6 C7 . 1.392(3) ? C6 C9 . 1.489(3) ? C7 H7 . 0.9300 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O6 H6 O2 5_455 0.841(18) 1.740(17) 2.539(2) 158(2) yes O7 H7A O4 4_444 0.819(15) 2.092(15) 2.890(2) 165(2) yes O7 H7B O5 6 0.839(15) 2.110(16) 2.904(2) 158(2) yes O8 H8A O4 6 0.824(15) 1.927(15) 2.732(2) 165(2) yes O8 H8B O2 7_445 0.835(15) 2.50(2) 3.058(2) 124.9(17) yes O8 H8B O5 4_444 0.835(15) 2.342(17) 3.027(2) 140(2) yes O9 H9A O3 5 0.84(2) 1.93(2) 2.745(2) 164.6(2) yes O10 H10A O5 7_455 0.861(15) 1.932(18) 2.768(2) 163(3) yes O10 H10B O7 3 0.835(16) 2.141(16) 2.968(2) 171(3) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Co1 O1 C1 O2 . . . . -5.3(3) ? Co1 O1 C1 C2 . . . . 174.87(12) ? Ca1 O3 C8 O4 . . . . 14.5(2) ? Ca1 O3 C8 C4 . . . . -163.08(15) ? Ca1 O4 C8 O3 . . . . -14.0(2) ? Ca1 O4 C8 C4 . . . . 163.57(16) ? O1 C1 C2 C3 . . . . -6.8(3) ? O1 C1 C2 C7 . . . . 174.80(18) ? O2 C1 C2 C3 . . . . 173.34(19) ? O2 C1 C2 C7 . . . . -5.1(3) ? C1 C2 C3 C4 . . . . -179.23(17) ? C1 C2 C7 C6 . . . . 178.93(17) ? C2 C3 C4 C5 . . . . -0.2(3) ? C2 C3 C4 C8 . . . . 176.09(18) ? C3 C2 C7 C6 . . . . 0.5(3) ? C3 C4 C5 C6 . . . . 1.5(3) ? C3 C4 C8 O3 . . . . -5.4(3) ? C3 C4 C8 O4 . . . . 177.01(18) ? C4 C5 C6 C7 . . . . -1.8(3) ? C4 C5 C6 C9 . . . . 174.90(17) ? C5 C4 C8 O3 . . . . 170.90(19) ? C5 C4 C8 O4 . . . . -6.7(3) ? C5 C6 C7 C2 . . . . 0.8(3) ? C5 C6 C9 O5 . . . . 9.4(3) ? C5 C6 C9 O6 . . . . -169.1(2) ? C7 C2 C3 C4 . . . . -0.8(3) ? C7 C6 C9 O5 . . . . -173.9(2) ? C7 C6 C9 O6 . . . . 7.6(3) ? C8 C4 C5 C6 . . . . -174.76(17) ? C9 C6 C7 C2 . . . . -175.93(18) ? _cod_database_fobs_code 2312507