#------------------------------------------------------------------------------ #$Date: 2024-05-23 04:50:14 +0300 (Thu, 23 May 2024) $ #$Revision: 292001 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312510.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312510 loop_ _publ_author_name 'Abrahams, Brendan F.' 'Commons, Christopher J.' 'Hudson, Timothy A.' 'Sanchez-Arlt, Robin' _publ_section_title ; Supramolecular hydrogen-bonded networks formed from copper(II) carboxylate dimers. ; _journal_coeditor_code JX3083 _journal_issue 6 _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_paper_doi 10.1107/S2053229624004534 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '(C8 H20 N) [Cu2 (C7 H5 O3)2 (C7 H4.5 O3)2 (C H4 O) (H2 O)], 2C4 H8 O2' _chemical_formula_moiety 'C8 H20 N +, C29 H25 Cu2 O14 -, 2(C4 H8 O2)' _chemical_formula_sum 'C45 H61 Cu2 N O18' _chemical_formula_weight 1031.02 _chemical_name_systematic ; Tetraethylammonium aquatris(\m-4-hydroxybenzoato)methanol(\m-4-oxidobenzoato)dicopper(II) dioxane disolvate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 76.132(4) _cell_angle_beta 69.646(3) _cell_angle_gamma 75.304(4) _cell_formula_units_Z 1 _cell_length_a 10.1659(4) _cell_length_b 10.7383(6) _cell_length_c 12.9878(4) _cell_measurement_reflns_used 7244 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 77.7690 _cell_measurement_theta_min 3.6790 _cell_volume 1267.74(10) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2018) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2018) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2018) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _diffrn_ambient_temperature 100.00(10) _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.973 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Rigaku XtaLAB Synergy Dualflex diffractometer with a HyPix detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0467 _diffrn_reflns_av_unetI/netI 0.0414 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 17988 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.953 _diffrn_reflns_theta_min 5.776 _exptl_absorpt_coefficient_mu 1.630 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.88532 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2018) ; _exptl_crystal_colour 'clear blue' _exptl_crystal_density_diffrn 1.350 _exptl_crystal_description irregular _exptl_crystal_F_000 540 _exptl_crystal_size_max 0.165 _exptl_crystal_size_mid 0.115 _exptl_crystal_size_min 0.054 _refine_diff_density_max 0.725 _refine_diff_density_min -0.998 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 459 _refine_ls_number_reflns 5262 _refine_ls_number_restraints 419 _refine_ls_restrained_S_all 1.036 _refine_ls_R_factor_all 0.0727 _refine_ls_R_factor_gt 0.0679 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1206P)^2^+1.2732P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1951 _refine_ls_wR_factor_ref 0.1999 _reflns_number_gt 4672 _reflns_number_total 5262 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jx3083.cif _cod_data_source_block compound_2 _cod_database_code 2312510 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.775 _shelx_estimated_absorpt_t_max 0.917 _shelx_hkl_file ; 0 0 1 157653. 6978.46 10 0 0 1 159498. 6976.50 9 0 0 2 144617. 6470.82 10 0 0 2 144511. 6467.25 9 0 0 2 157676. 6545.32 8 0 0 3 18937.2 925.344 10 0 0 3 21535.5 1038.67 8 0 0 4 2307.81 280.833 11 0 0 4 2379.63 287.811 8 0 0 5 22842.3 1331.84 11 0 0 5 24445.5 1322.71 8 0 0 6 1883.29 333.842 8 0 0 7 4019.50 486.810 8 0 0 8 21597.8 1053.60 30 0 0 8 20179.4 1341.00 8 0 0 8 20068.5 1038.66 44 0 0 8 21214.8 1089.61 49 0 0 8 20557.4 1053.42 18 0 0 9 24225.0 1188.72 19 0 0 9 22512.1 1161.99 40 0 0 9 22842.5 1154.03 20 0 0 9 25628.7 1257.36 49 0 0 9 26026.4 1225.33 36 0 0 9 24263.8 1196.85 42 0 0 9 22840.1 1189.58 44 0 0 9 25016.3 1206.01 30 0 0 9 23120.0 1168.43 28 0 0 9 22635.3 1182.00 46 0 0 9 25297.4 1216.36 18 0 0 9 21311.4 1498.02 8 0 0 9 22272.6 1174.36 16 0 0 10 22576.9 1150.85 42 0 0 10 22380.4 1144.72 46 0 0 10 22111.8 1119.72 40 0 0 10 21276.3 1134.42 19 0 0 10 23959.6 1181.23 18 0 0 10 24231.2 1219.62 49 0 0 10 24299.2 1170.05 30 0 0 10 21710.0 1124.30 28 0 0 10 21920.9 1157.54 44 0 0 10 19644.4 1093.70 20 0 0 10 23622.2 1174.30 36 0 0 11 56604.6 2516.64 49 0 0 11 54504.8 2473.58 18 0 0 11 50375.7 2445.22 44 0 0 11 51936.2 2424.00 46 0 0 11 47288.8 2401.45 32 0 0 11 51603.5 2418.16 19 0 0 11 46150.7 2389.77 40 0 0 11 43326.4 3071.95 12 0 0 11 56480.3 2466.93 36 0 0 11 50994.8 2429.25 42 0 0 11 55806.8 2458.31 30 0 0 11 51711.8 2414.41 28 0 0 12 563.706 148.311 25 0 0 12 986.378 228.835 49 0 0 12 680.771 161.883 36 0 0 12 673.430 182.826 18 0 0 12 723.354 154.271 19 0 0 12 611.180 152.113 42 0 0 13 47.3101 101.099 42 0 0 13 189.813 117.576 25 0 0 13 77.6429 139.780 18 0 0 13 252.131 170.690 49 0 0 14 180.427 114.133 18 0 0 14 203.391 135.252 49 0 -1 14 47.3375 116.502 49 0 -1 13 4225.69 329.175 29 0 -1 13 4097.86 337.304 49 0 -1 13 2894.85 255.277 25 0 -1 13 3174.51 277.622 36 0 -1 13 2856.34 262.333 42 0 -1 12 2697.02 311.772 49 0 -1 12 2373.85 285.456 29 0 -1 12 2107.08 252.988 36 0 -1 12 2027.82 213.538 19 0 -1 12 2167.18 239.269 25 0 -1 12 2189.38 250.287 42 0 -1 11 6466.47 998.846 12 0 -1 11 8154.22 549.153 20 0 -1 11 11358.9 656.903 29 0 -1 11 10163.4 621.074 36 0 -1 11 10013.5 612.150 42 0 -1 11 8567.59 564.026 19 0 -1 11 10464.0 673.579 49 0 -1 10 7435.21 1011.67 12 0 -1 10 11029.4 624.941 42 0 -1 10 9247.29 612.305 44 0 -1 10 8864.64 565.802 20 0 -1 10 10508.3 633.023 36 0 -1 10 9468.11 585.632 28 0 -1 10 8668.50 559.940 40 0 -1 10 11195.1 651.085 29 0 -1 10 9274.39 589.588 46 0 -1 10 11057.3 685.390 49 0 -1 10 9506.22 581.091 19 0 -1 9 43805.3 2023.37 44 0 -1 9 46485.3 2039.65 42 0 -1 9 38702.5 1970.00 40 0 -1 9 43597.8 2017.44 30 0 -1 9 40733.6 1993.54 46 0 -1 9 39957.9 1994.70 17 0 -1 9 44395.7 2083.87 49 0 -1 9 40874.4 2006.32 16 0 -1 9 47237.5 2065.59 29 0 -1 9 41470.2 1990.13 28 0 -1 9 41840.2 2002.85 19 0 -1 9 41489.6 1990.79 20 0 -1 8 42986.8 2078.58 49 0 -1 8 40970.9 2328.35 8 0 -1 8 42149.9 2018.78 44 0 -1 8 44670.7 2019.97 30 0 -1 8 42580.4 2004.75 17 0 -1 8 40110.0 2002.95 16 0 -1 8 39965.9 1995.95 46 0 -1 8 41701.3 1997.10 20 0 -1 8 42768.4 1995.85 28 0 -1 8 47019.9 2050.52 29 0 -1 8 45658.9 2036.34 42 0 -1 7 13743.9 697.898 14 0 -1 7 14494.4 1002.90 8 0 -1 6 1157.71 136.666 14 0 -1 6 1336.35 293.708 8 0 -1 5 337.623 221.457 11 0 -1 5 345.205 218.876 8 0 -1 5 332.571 142.623 9 0 -1 5 299.078 139.016 10 0 -1 4 91896.7 3962.80 8 0 -1 4 82552.7 3961.84 11 0 -1 4 83440.1 3863.14 10 0 -1 4 83067.5 3849.70 9 0 -1 3 1586.89 196.400 9 0 -1 3 1612.07 191.161 10 0 -1 3 1720.35 231.634 11 0 -1 3 1787.62 246.114 8 0 -1 2 92811.7 4146.04 11 0 -1 2 92686.0 4136.16 10 0 1 -2 90892.1 4088.59 2 0 -1 1 68758.8 3105.46 11 0 1 -1 70249.0 3110.42 2 0 -1 0 170439. 7573.07 10 0 1 0 171956. 7572.34 2 0 1 1 277861. 12202.1 11 0 1 1 275566. 12234.2 8 0 -1 -1 277016. 12188.7 10 0 1 2 70607.3 3160.26 2 0 1 3 1171.06 105.322 7 0 1 3 1249.63 211.002 8 0 1 4 289.049 180.114 12 0 -1 -4 136.597 52.5735 4 0 1 4 340.909 172.171 8 0 1 5 1428.58 262.972 8 0 1 6 2908.47 377.111 8 0 1 7 1959.03 341.046 8 0 1 8 3064.47 440.937 8 0 1 8 2971.64 264.091 30 0 1 8 3141.07 269.339 29 0 1 8 3158.20 279.605 49 0 1 8 2739.05 250.511 46 0 1 9 7640.84 498.637 30 0 1 9 7173.92 479.014 46 0 1 9 8680.64 535.305 49 0 1 9 7608.47 468.997 42 0 1 9 8203.80 487.627 19 0 1 9 8149.53 517.937 29 0 1 9 7890.98 487.569 36 0 1 9 7511.50 487.373 18 0 1 9 7559.68 477.313 44 0 1 9 7121.71 457.433 16 0 1 10 29068.6 1409.33 49 0 1 10 26953.2 1339.20 19 0 1 10 25886.0 1319.11 28 0 1 10 27881.2 1348.23 25 0 1 10 23053.2 1306.53 16 0 1 10 26639.8 1343.51 44 0 1 10 28737.5 1370.57 30 0 1 10 25124.8 1316.11 40 0 1 10 28369.5 1360.90 36 0 1 10 27095.4 1343.23 46 0 1 10 26145.3 1323.82 42 0 1 10 29215.7 1395.18 29 0 1 10 28103.8 1365.00 18 0 1 11 2267.44 278.804 30 0 1 11 2271.11 262.013 44 0 1 11 2263.16 250.092 19 0 1 11 2190.90 284.696 29 0 1 11 2069.72 298.309 49 0 1 11 2346.36 262.354 32 0 1 11 1945.61 240.004 40 0 1 11 2189.65 266.592 18 0 1 11 2573.77 276.278 46 0 1 11 2018.85 228.193 42 0 1 11 2447.49 254.340 28 0 1 11 2028.78 238.436 25 0 1 11 2829.45 265.109 36 0 1 12 2878.34 279.331 40 0 1 12 3601.01 323.030 30 0 1 12 3459.66 332.101 29 0 1 12 2659.86 276.983 32 0 1 12 2567.92 288.640 44 0 1 12 3555.22 319.204 18 0 1 12 3284.40 342.598 49 0 1 12 3303.90 284.883 19 0 1 12 3324.61 304.110 46 0 1 12 2929.31 282.562 28 0 1 12 3465.13 292.745 36 0 1 12 2804.52 279.441 25 0 1 12 2796.35 258.533 42 0 1 13 7513.47 472.298 19 0 1 13 8678.43 549.313 29 0 1 13 7399.68 477.277 25 0 1 13 9860.75 574.453 49 0 1 13 8638.39 529.756 18 0 1 14 3433.10 282.753 49 0 1 14 3197.52 270.384 29 0 -2 14 2677.09 228.937 49 0 -2 13 172.707 130.137 18 0 -2 13 159.958 148.389 49 0 -2 13 110.049 101.624 25 0 -2 13 200.139 127.070 29 0 -2 13 153.376 104.357 42 0 -2 13 132.749 106.067 36 0 -2 12 481.639 164.227 29 0 -2 12 66.4034 126.103 36 0 -2 12 178.716 176.660 49 0 -2 12 173.374 155.228 18 0 -2 12 198.304 135.925 42 0 -2 11 833.760 185.728 36 0 -2 11 1060.10 211.239 29 0 -2 11 642.591 395.394 12 0 -2 11 795.764 199.921 18 0 -2 11 906.282 191.947 42 0 -2 11 764.408 161.285 20 0 -2 11 590.619 145.950 19 0 -2 10 930.272 171.199 19 0 -2 10 1030.75 204.063 42 0 -2 10 1134.95 214.923 29 0 -2 10 640.415 172.900 20 0 -2 10 938.797 209.446 18 0 -2 9 11956.9 686.388 18 0 -2 9 12171.3 693.712 29 0 -2 9 11234.8 652.431 20 0 -2 9 9975.38 632.129 19 0 -2 9 9930.17 1151.48 12 0 -2 9 10216.9 672.060 44 0 -2 9 11930.2 687.099 42 0 -2 9 10757.3 654.170 17 0 -2 8 7342.69 487.192 16 0 -2 8 7276.07 497.267 44 0 -2 8 7494.30 487.353 17 0 -2 8 7393.51 501.429 42 0 -2 8 7956.18 504.297 18 0 -2 8 7927.63 479.796 28 0 -2 8 8307.99 469.618 14 0 -2 8 6528.26 461.593 46 0 -2 8 8883.47 524.606 29 0 -2 7 9808.33 579.392 18 0 -2 7 8848.47 803.599 8 0 -2 7 10560.4 556.189 14 0 -2 6 1605.39 255.845 9 0 -2 6 1475.84 304.506 8 0 -2 6 1823.81 170.764 14 0 -2 6 1622.58 252.944 10 0 -2 5 3883.36 257.013 14 0 -2 5 4154.96 374.212 9 0 -2 5 4060.50 424.720 8 0 -2 5 4530.77 388.861 10 0 -2 4 3991.75 381.786 11 0 -2 4 4846.13 384.391 9 0 -2 4 4134.31 374.875 10 0 -2 4 4210.93 410.948 8 0 -2 3 218314. 9822.28 11 0 -2 3 224147. 9831.98 10 0 -2 3 216878. 9815.63 9 0 -2 2 45657.4 2136.39 11 0 2 -2 44912.8 2144.54 2 0 -2 2 47909.4 2192.41 10 0 2 -1 21640.1 1061.63 2 0 -2 1 20907.3 986.789 11 0 -2 0 36208.3 1682.88 10 0 2 0 34580.4 1682.27 2 0 -2 -1 165710. 7374.14 10 0 -2 -2 741425. 32462.0 10 0 2 2 733201. 32515.8 2 0 -2 -3 711.736 81.9334 10 0 2 3 824.183 158.348 2 0 2 4 1728.74 176.782 7 0 2 4 1992.66 298.631 8 0 2 4 1374.18 265.621 12 0 2 5 77010.8 3741.51 12 0 2 5 78465.2 3745.64 8 0 2 6 108578. 5159.29 8 0 2 7 797.529 284.820 8 0 2 8 634.842 149.847 35 0 2 8 793.656 146.340 29 0 2 8 782.873 161.602 49 0 2 8 738.363 158.558 46 0 2 9 4315.41 343.141 46 0 2 9 4516.79 318.780 43 0 2 9 4478.02 335.729 19 0 2 9 4206.72 322.426 44 0 2 9 4391.46 325.147 27 0 2 9 4398.96 333.206 18 0 2 9 4515.00 328.811 36 0 2 9 4940.83 362.919 29 0 2 9 4614.49 372.103 49 0 2 9 4499.52 331.014 25 0 2 10 2414.15 273.039 29 0 2 10 2033.92 228.238 36 0 2 10 2544.71 259.995 19 0 2 10 2427.24 271.613 46 0 2 10 2237.84 245.039 18 0 2 10 2080.20 209.688 42 0 2 10 2032.58 237.408 25 0 2 10 2493.66 298.053 49 0 2 10 2360.41 245.760 44 0 2 11 108.381 134.800 25 0 2 11 194.013 153.298 28 0 2 11 206.956 149.064 19 0 2 11 130.264 144.172 18 0 2 11 342.737 195.747 49 0 2 11 182.435 153.917 29 0 2 11 133.918 157.937 32 0 2 11 228.244 180.278 46 0 2 11 69.2632 143.841 44 0 2 11 358.166 163.769 40 0 2 12 3826.42 325.682 18 0 2 12 3894.61 316.351 40 0 2 12 4045.35 349.778 29 0 2 12 3479.73 325.345 32 0 2 12 3604.57 312.836 19 0 2 12 3104.58 310.709 44 0 2 12 4187.18 342.042 46 0 2 12 3696.68 309.506 28 0 2 12 4506.83 383.862 49 0 2 12 3592.58 303.940 25 0 2 13 5383.70 386.075 25 0 2 13 6478.01 399.481 40 0 2 13 7387.82 442.083 46 0 2 13 7126.19 459.626 29 0 2 13 5420.12 400.951 32 0 2 13 6191.50 405.288 19 0 2 13 5252.93 411.101 44 0 2 13 5850.14 416.250 18 0 2 13 8535.46 495.239 49 0 2 13 5945.19 396.128 28 0 2 14 6217.00 422.337 29 0 2 14 6963.86 442.543 49 0 -3 13 1301.04 162.070 42 0 -3 13 1210.78 143.446 25 0 -3 13 1447.17 178.000 18 0 -3 13 1382.13 163.011 36 0 -3 12 462.667 151.788 29 0 -3 12 470.674 162.845 18 0 -3 12 403.321 141.435 42 0 -3 12 489.888 124.039 20 0 -3 11 1431.03 224.086 42 0 -3 11 1228.25 214.776 29 0 -3 11 1328.92 189.680 20 0 -3 11 1501.93 226.335 18 0 -3 10 5270.37 890.430 12 0 -3 10 7433.89 488.524 20 0 -3 10 7337.19 509.077 29 0 -3 10 7734.92 522.236 18 0 -3 10 5712.89 441.386 19 0 -3 10 7930.29 535.265 42 0 -3 9 9.49704 150.883 17 0 -3 9-27.0510 133.697 20 0 -3 9 60.9455 146.650 18 0 -3 9 100.490 373.848 12 0 -3 9 99.8257 132.999 29 0 -3 8 1460.18 214.829 17 0 -3 8 1560.12 214.076 18 0 -3 8 1460.84 466.760 12 0 -3 8 1323.86 192.834 14 0 -3 8 1513.99 207.592 29 0 -3 7 374.260 134.504 18 0 -3 7 628.782 149.753 17 0 -3 7 360.472 217.690 8 0 -3 7 471.126 136.054 14 0 -3 7 396.192 138.705 29 0 -3 7 388.441 146.463 16 0 -3 6 16344.4 1040.14 9 0 -3 6 15474.2 1043.36 10 0 -3 6 17481.3 834.187 14 0 -3 5 11957.2 590.120 14 0 -3 5 10687.8 805.049 8 0 -3 5 12132.4 786.993 9 0 -3 5 12943.1 809.172 10 0 -3 4 142.834 164.636 10 0 -3 4 136.151 181.187 9 0 -3 3 196997. 8260.67 10 0 -3 3 175793. 8036.59 14 0 -3 3 192051. 8241.70 9 0 3 -2 66209.5 3102.20 2 0 -3 1 3063.82 310.914 10 0 3 -1 2905.31 296.778 2 0 3 0 33179.9 1625.37 2 0 -3 0 31833.8 1609.08 10 0 -3 -1 10505.6 622.967 10 0 -3 -2 139866. 6326.97 10 0 3 2 142376. 6388.90 2 0 -3 -3 73473.1 3394.07 10 0 3 3 77352.2 3494.48 2 0 3 5 135424. 6094.10 13 0 3 5 140830. 6194.35 7 0 3 6 150356. 6687.39 13 0 3 7 3521.50 248.462 13 0 3 8 33246.4 1620.36 43 0 3 8 34798.6 1636.65 19 0 3 8 33794.9 1653.48 49 0 3 8 34236.4 1625.60 27 0 3 8 33323.7 1617.60 25 0 3 8 35100.3 1640.74 35 0 3 9 50.4631 122.935 29 0 3 9 109.297 112.839 25 0 3 9 160.348 143.313 35 0 3 9 84.1399 105.602 18 0 3 9 56.8895 136.885 19 0 3 9 109.271 129.567 43 0 3 9 143.625 116.738 44 0 3 9 220.540 160.077 49 0 3 9 148.644 135.546 27 0 3 10 180.884 169.860 32 0 3 10 254.901 186.031 49 0 3 10 237.917 148.580 19 0 3 10 362.647 186.038 30 0 3 10 198.613 129.725 44 0 3 10 56.7360 140.989 29 0 3 10 197.667 131.454 25 0 3 10 176.176 144.778 27 0 3 10 211.729 122.051 18 0 3 10 224.427 168.978 46 0 3 11 223.776 136.900 44 0 3 11 154.858 182.573 49 0 3 11 232.536 150.750 19 0 3 11-10.2681 177.424 30 0 3 11 202.733 169.823 32 0 3 11 224.547 135.219 25 0 3 11 199.608 179.257 46 0 3 11 168.796 139.020 29 0 3 11 171.863 124.258 18 0 3 12 50.9416 140.053 28 0 3 12 115.030 145.792 19 0 3 12 124.105 135.250 29 0 3 12 221.527 159.892 32 0 3 12 262.805 185.492 49 0 3 12 130.071 117.330 18 0 3 12 210.283 132.741 44 0 3 12 124.662 123.238 25 0 3 12 78.9467 149.892 40 0 3 12 374.537 179.670 46 0 3 12 9.61462 182.082 30 0 3 13 3622.99 283.319 28 0 3 13 3719.06 287.524 40 0 3 13 3935.68 303.783 19 0 3 13 4029.12 348.052 49 0 3 13 3911.62 316.376 29 0 3 13 3055.03 267.996 25 0 3 13 3472.30 301.595 32 0 3 13 4329.75 324.122 46 0 3 13 2783.14 269.901 44 0 3 14 2549.43 230.034 46 0 -4 13 3269.20 236.028 42 0 -4 12 2066.88 201.919 20 0 -4 12 2445.58 239.162 18 0 -4 11 5620.01 434.693 36 0 -4 11 5609.85 402.195 20 0 -4 11 5556.31 413.408 29 0 -4 11 6192.51 436.543 18 0 -4 10 4147.28 370.052 29 0 -4 10 4839.01 376.498 20 0 -4 10 4832.31 386.252 18 0 -4 9 6616.56 459.207 20 0 -4 9 6339.29 458.594 17 0 -4 9 5128.65 427.382 29 0 -4 9 6999.61 482.952 42 0 -4 9 5485.69 853.782 12 0 -4 9 5713.39 444.993 18 0 -4 8 13875.7 1334.09 12 0 -4 8 12552.9 765.687 29 0 -4 8 14269.3 775.694 14 0 -4 8 13656.8 783.603 18 0 -4 8 14403.0 809.891 42 0 -4 7 219.252 119.319 29 0 -4 7 154.928 133.941 14 0 -4 7 258.736 316.193 12 0 -4 7 140.181 117.895 18 0 -4 6 339.732 139.058 14 0 -4 6 418.148 220.070 10 0 -4 6 224.558 119.133 18 0 -4 6 390.889 217.963 9 0 -4 6 259.315 129.903 17 0 -4 6 255.680 197.147 8 0 -4 5 349.290 240.425 8 0 -4 5 362.237 218.980 10 0 -4 5 672.141 257.313 9 0 -4 4 4132.66 279.700 14 0 -4 4 4020.56 446.501 9 0 -4 4 4045.58 448.952 10 0 -4 3 59920.8 2790.53 14 0 -4 3 64567.8 3064.49 10 0 -4 3 65935.8 3064.86 9 0 -4 2 137101. 6089.28 14 0 -4 1 111585. 5054.67 10 0 4 -1 105652. 5033.33 2 0 -4 0 64778.1 3068.51 10 0 4 0 63128.5 3080.93 2 0 -4 -1 7234.84 526.533 10 0 4 1 7335.27 563.302 2 0 -4 -2 17438.6 967.838 10 0 4 3 12850.3 807.442 2 0 -4 -3 12260.9 715.726 10 0 -4 -4 7052.24 445.762 10 0 4 4 7263.91 408.224 13 0 4 5 2103.03 195.889 13 0 4 5 2468.55 315.512 7 0 4 6 2895.25 291.806 7 0 4 6 2755.77 228.035 13 0 4 7 42381.1 1956.82 46 0 4 7 40253.4 1929.91 13 0 4 8 9567.30 576.695 49 0 4 8 9295.99 536.124 25 0 4 8 10178.0 563.709 38 0 4 8 9332.20 528.827 41 0 4 8 9519.05 572.126 46 0 4 8 10190.0 560.922 27 0 4 8 8822.69 546.399 43 0 4 8 9455.69 531.335 44 0 4 8 8891.68 530.149 29 0 4 8 9275.98 567.794 35 0 4 8 9096.65 557.075 19 0 4 8 9470.87 545.078 22 0 4 9 29.7590 169.863 32 0 4 9 131.260 113.685 29 0 4 9 61.5597 150.183 35 0 4 9 103.745 147.643 19 0 4 9-14.7248 121.099 25 0 4 9 179.336 118.702 44 0 4 9 28.8903 163.065 49 0 4 9 104.405 141.680 27 0 4 10 1338.50 233.037 32 0 4 10 1816.61 255.813 49 0 4 10 1478.27 199.373 25 0 4 10 1610.40 203.732 29 0 4 10 1163.83 187.528 44 0 4 10 1705.22 245.440 30 0 4 10 1546.78 213.257 27 0 4 10 1469.61 230.712 35 0 4 10 1757.94 242.956 19 0 4 11 1047.28 223.525 32 0 4 11 665.391 161.746 25 0 4 11 718.111 160.653 29 0 4 11 757.130 209.336 30 0 4 11 781.780 167.862 44 0 4 11 937.327 225.613 49 0 4 11 848.153 201.959 19 0 4 12 2550.98 251.907 28 0 4 12 2415.02 273.090 19 0 4 12 2838.74 294.533 30 0 4 12 2274.61 233.918 44 0 4 12 2730.84 265.404 40 0 4 12 2355.35 280.655 32 0 4 12 2159.90 245.688 29 0 4 12 2730.68 286.379 46 0 4 13-54.5464 160.662 30 0 4 13 37.9406 150.652 32 0 4 13 39.2456 117.804 28 0 4 13 163.092 108.891 29 0 4 13 22.2818 151.664 46 0 4 13 90.0417 129.532 40 0 4 14 1017.17 140.197 40 0 4 14 1063.07 161.633 46 0 -5 13 44.7569 62.3607 49 0 -5 12 6513.90 406.189 36 0 -5 11 2034.03 223.539 18 0 -5 11 2096.31 220.586 20 0 -5 11 2383.18 242.225 42 0 -5 11 1775.17 227.183 36 0 -5 10 2627.66 287.486 42 0 -5 10 2606.20 264.487 18 0 -5 10 2238.15 262.659 20 0 -5 9 9739.92 613.033 42 0 -5 9 8424.76 567.842 29 0 -5 9 10359.2 607.953 20 0 -5 9 9163.82 587.422 18 0 -5 8 12842.2 796.584 18 0 -5 8 15948.5 836.343 17 0 -5 8 12252.0 781.454 29 0 -5 8 11458.5 1323.07 12 0 -5 8 16074.8 823.346 14 0 -5 8 15572.3 849.992 42 0 -5 7 922.196 185.903 17 0 -5 7 759.605 184.788 14 0 -5 7 781.502 161.983 18 0 -5 7 661.060 392.081 12 0 -5 6 13911.6 735.868 17 0 -5 6 12358.5 705.074 18 0 -5 6 11987.5 1015.94 9 0 -5 6 11845.6 1019.73 10 0 -5 5 1361.14 340.520 9 0 -5 5 1016.13 261.594 4 0 -5 5 830.564 269.234 8 0 -5 5 1437.70 348.670 10 0 -5 5 1271.70 180.614 14 0 -5 5 1099.57 171.154 17 0 -5 4 2514.59 398.166 9 0 -5 4 2287.04 214.099 14 0 -5 4 2311.17 394.153 10 0 -5 3 3096.71 428.503 9 0 -5 3 2743.58 227.337 14 0 -5 2 620.074 117.701 14 0 -5 2 502.067 224.362 10 0 -5 1 234516. 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0 5 11 2207.19 269.479 30 0 5 11 2176.30 285.823 32 0 5 11 2208.49 250.057 27 0 5 11 1962.57 211.487 44 0 5 12 6531.33 460.737 32 0 5 12 7214.71 455.991 30 0 5 13 1926.23 222.343 40 0 5 13 2684.61 249.812 30 0 5 13 2145.15 208.799 28 0 5 13 2351.54 249.629 32 0 5 14 34.3920 115.145 46 0 5 14 114.450 96.0138 40 0 -6 12-80.4664 65.3845 36 0 -6 12-127.138 88.9566 49 0 -6 12-17.0043 66.3184 42 0 -6 11 392.749 143.205 49 0 -6 11 271.158 113.510 36 0 -6 11 471.733 123.321 20 0 -6 11 552.398 126.568 42 0 -6 10-18.9909 150.939 49 0 -6 10 168.686 129.445 20 0 -6 10 183.330 131.936 42 0 -6 9 1312.89 193.498 18 0 -6 9 1982.26 280.205 49 0 -6 9 1708.19 234.661 42 0 -6 8 14814.7 801.241 42 0 -6 8 11207.5 1309.80 12 0 -6 8 14288.9 854.414 49 0 -6 8 12114.5 747.051 18 0 -6 7 9952.41 589.518 17 0 -6 7 7910.08 533.937 18 0 -6 7 9390.22 587.278 42 0 -6 6 9023.22 565.122 17 0 -6 6 10128.9 578.939 14 0 -6 6 6823.34 831.084 10 0 -6 6 7018.74 822.843 9 0 -6 5 14340.8 1163.09 9 0 -6 5 14654.6 815.355 17 0 -6 5 16077.2 830.177 14 0 -6 5 13776.7 1170.13 10 0 -6 4 2323.06 443.688 10 0 -6 4 3283.75 493.046 9 0 -6 4 2420.11 230.219 17 0 -6 4 2618.06 249.836 14 0 6 -4 2442.11 232.632 15 0 -6 3 11962.3 649.376 14 0 -6 3 11593.7 959.233 9 0 -6 2 4285.07 535.036 10 0 -6 2 4399.11 304.825 14 0 -6 1 660.088 264.455 10 0 6 -1 711.099 113.205 13 0 -6 1 433.570 111.754 14 0 -6 1 769.195 284.519 9 0 6 0 8639.71 475.850 13 0 -6 0 8283.53 456.322 14 0 -6 0 8528.43 719.977 10 0 -6 -1 27350.8 1549.42 10 0 6 1 26117.0 1270.04 13 0 6 2 46042.4 2143.48 13 0 -6 -2 46224.2 2385.81 10 0 -6 -3 82759.7 4015.68 10 0 6 3 84341.2 3812.81 13 0 6 4 35735.6 1656.24 13 0 -6 -4 32959.7 1828.66 9 0 -6 -4 33152.7 1790.99 10 0 6 5 13880.7 760.089 32 0 6 5 14103.9 761.661 48 0 6 5 15026.1 774.304 38 0 6 5 13481.3 751.878 22 0 6 6 26001.3 1275.08 48 0 6 6 27254.8 1293.53 38 0 6 6 23409.2 1531.94 7 0 6 6 26013.7 1286.90 32 0 6 6 26005.3 1287.99 13 0 6 6 23974.6 1248.30 37 0 6 7 710.963 173.332 37 0 6 7 703.562 190.941 35 0 6 7 741.435 189.355 46 0 6 7 645.303 166.832 13 0 6 7 968.833 194.073 32 0 6 8 242.297 158.011 38 0 6 8 166.985 170.129 46 0 6 8 238.026 168.003 35 0 6 8 152.840 171.615 32 0 6 8 112.056 147.031 13 0 6 8 55.9721 105.434 44 0 6 9 952.423 221.592 32 0 6 9 651.933 208.033 46 0 6 9 773.482 164.068 41 0 6 9 870.824 196.545 27 0 6 9 689.423 212.369 19 0 6 9 611.094 142.223 44 0 6 10 575.119 149.124 41 0 6 10 840.474 218.410 32 0 6 10 687.770 209.119 46 0 6 10 479.749 139.855 44 0 6 10 797.089 193.536 27 0 6 11 4924.23 353.369 44 0 6 11 6248.06 408.610 27 0 6 11 6080.67 428.482 35 0 6 11 6019.82 435.812 46 0 6 11 5560.74 419.116 30 0 6 12 15089.6 820.613 46 0 6 12 14866.9 809.313 30 0 6 13 8508.15 476.585 30 0 6 13 7927.41 468.898 40 0 6 13 7441.86 438.664 28 0 6 14 1426.85 142.440 40 0 -7 11 846.549 132.698 49 0 -7 11 965.322 112.917 20 0 -7 11 959.615 114.482 42 0 -7 11 621.669 102.803 36 0 -7 10 30.3779 91.0829 36 0 -7 10 33.9619 96.3729 42 0 -7 10 28.2102 125.029 49 0 -7 9-59.8642 118.512 42 0 -7 9-74.4337 132.648 20 0 -7 9 9.51144 152.572 49 0 -7 8 4859.43 434.153 49 0 -7 8 5423.49 401.842 20 0 -7 8 4918.84 387.832 42 0 7 -7 15434.6 900.887 24 0 -7 7 14231.5 1493.92 12 0 -7 6 54339.0 2473.46 17 0 -7 6 59343.2 2491.50 14 0 -7 5 20342.5 1074.42 17 0 -7 5 17387.3 1486.18 10 0 -7 5 17897.9 1491.67 9 0 -7 4 4748.84 656.300 9 0 -7 4 4409.00 647.913 10 0 -7 4 4874.48 363.566 14 0 7 -4 4450.68 352.591 15 0 -7 4 4429.14 341.885 17 0 -7 3 6465.24 710.977 9 0 -7 3 5728.29 376.906 14 0 -7 3 4513.80 338.132 17 0 7 -3 4566.56 368.497 15 0 -7 2 9373.17 905.862 10 0 -7 2 10553.9 587.488 14 0 7 -2 10173.4 611.193 15 0 -7 1 28414.5 1667.25 9 0 7 -1 25221.1 1231.29 15 0 7 -1 24416.5 1189.79 13 0 -7 1 26611.8 1626.36 10 0 -7 1 24577.9 1189.49 14 0 7 -1 22265.5 1199.08 48 0 -7 0 350.815 241.843 10 0 7 0 124.764 129.921 48 0 -7 0 108.403 99.7135 14 0 -7 0 240.435 257.341 9 0 7 0 216.343 134.245 15 0 7 0 101.313 110.220 13 0 -7 -1 36496.4 2126.46 10 0 7 1 36410.5 1793.26 48 0 7 1 38022.8 1805.97 15 0 7 1 38652.5 1794.22 13 0 -7 -1 38145.0 2160.76 9 0 -7 -2 23928.3 1468.01 10 0 7 2 22331.3 1175.21 48 0 -7 -2 24766.4 1505.13 9 0 7 2 24212.4 1183.66 13 0 7 3 62787.7 2846.99 38 0 -7 -3 59469.8 3112.89 10 0 7 3 65265.0 2867.45 13 0 7 3 58762.0 2835.37 24 0 7 3 60244.5 2852.68 48 0 -7 -3 63120.5 3171.62 9 0 7 3 61359.2 2852.44 15 0 -7 -4 52862.0 2814.44 9 0 7 4 54602.1 2552.52 15 0 7 4 57920.7 2574.45 13 0 7 4 52283.7 2527.79 24 0 7 4 55482.5 2560.32 38 0 7 5 68704.9 3242.96 48 0 7 5 68522.2 3222.92 15 0 7 5 72409.1 3236.82 32 0 7 5 70605.8 3247.95 38 0 7 6 2121.52 230.058 15 0 7 6 1978.79 414.026 7 0 7 6 2180.68 257.978 32 0 7 6 2006.46 257.231 38 0 7 6 2470.43 268.129 48 0 7 6 1999.10 251.679 13 0 7 6 2024.91 260.708 46 0 7 7 1785.33 251.092 46 0 7 7 2086.96 256.990 13 0 7 7 1760.64 258.188 32 0 7 7 1857.44 271.086 35 0 7 7 1631.02 221.847 37 0 7 7 1849.24 258.875 38 0 7 8 5934.09 446.304 46 0 7 8 5793.30 448.110 32 0 7 8 5540.17 433.079 13 0 7 8 5773.90 458.797 35 0 7 9 1301.29 238.769 46 0 7 9 1203.65 238.775 32 0 7 9 1358.47 246.891 35 0 7 9 1038.45 164.676 44 0 7 10 789.282 160.718 41 0 7 10 1112.12 227.136 32 0 7 10 1082.33 199.328 30 0 7 10 686.043 133.339 44 0 7 10 747.138 188.076 27 0 7 10 1114.59 218.419 46 0 7 11 1050.60 181.939 27 0 7 11 710.960 171.593 30 0 7 11 882.401 198.970 46 0 7 12 3999.55 313.281 30 0 7 12 4752.52 341.382 46 0 7 13 2898.99 240.474 46 0 7 13 2861.69 230.806 40 0 7 14 1757.53 138.718 46 0 7 14 1176.34 118.487 40 0 -8 10 1272.93 122.831 42 0 -8 10 1204.61 154.792 49 0 -8 10 945.960 120.526 36 0 -8 9 877.646 172.184 49 0 -8 9 751.547 130.922 36 0 -8 9 950.438 136.141 42 0 -8 9 1205.28 157.578 20 0 -8 8 893.629 153.308 42 0 -8 8 941.879 208.143 49 0 -8 8 1075.46 174.744 20 0 -8 7 17142.6 821.659 20 0 -8 7 14452.4 786.709 42 0 -8 7 15712.3 863.487 49 0 -8 6 28906.6 1517.70 42 0 8 -6 33244.3 1546.50 24 0 -8 5 5868.71 450.898 42 0 8 -5 7491.53 506.953 24 0 -8 5 5428.82 796.447 9 0 -8 5 8690.70 512.356 14 0 -8 4 14634.5 1253.96 10 0 -8 4 16692.0 806.593 14 0 -8 4 14510.0 1252.52 9 0 8 -4 14454.7 790.104 15 0 -8 3 3391.49 302.471 14 0 -8 3 2609.59 538.905 10 0 8 -3 3240.16 308.566 15 0 -8 2 5392.35 380.789 14 0 -8 2 4674.71 676.121 10 0 8 -2 5303.30 408.693 15 0 -8 2 5354.90 699.315 9 0 -8 1 2350.46 486.787 10 0 -8 1 3207.01 558.310 9 0 8 -1 2983.74 280.019 48 0 -8 1 3029.03 265.052 14 0 8 -1 3165.56 308.181 15 0 8 0 16816.3 902.889 15 0 -8 0 17487.5 1299.53 9 0 8 0 16997.7 868.675 13 0 -8 0 16608.4 1268.97 10 0 8 0 15992.6 880.062 48 0 -8 0 15327.9 829.934 14 0 8 1 1588.69 228.408 48 0 8 1 1346.76 198.767 13 0 8 1 1635.95 239.228 24 0 8 1 1537.33 231.679 15 0 -8 -1 1540.15 405.915 9 0 -8 -1 1948.24 403.105 10 0 8 2 549.613 183.022 24 0 8 2 468.934 163.006 13 0 8 2 442.997 146.228 38 0 8 2 676.031 189.615 48 0 -8 -2 452.979 292.771 9 0 -8 -2 391.024 266.825 10 0 8 3 6833.66 461.364 15 0 -8 -3 5526.53 626.812 10 0 8 3 6679.01 461.879 48 0 8 3 6530.53 443.163 38 0 -8 -3 6395.90 691.107 9 0 8 3 6382.91 451.692 13 0 8 3 6191.90 440.367 24 0 8 4 44513.2 2080.11 13 0 8 4 44359.1 2067.71 15 0 -8 -4 38452.5 2348.31 9 0 8 4 40994.9 2036.44 24 0 8 4 43398.7 2075.92 48 0 8 4 43298.0 2063.44 38 0 8 5 14456.5 1317.11 7 0 8 5 17665.7 916.232 15 0 8 5 18201.3 946.686 13 0 8 5 16730.6 925.858 38 0 8 5 15639.1 873.296 24 0 8 6 122.022 171.175 48 0 8 6 94.3359 163.748 46 0 8 6-34.4276 136.757 15 0 8 6 123.444 160.250 38 0 8 7 20889.8 1064.48 38 0 8 7 18580.5 1044.53 46 0 8 7 19659.5 1065.22 35 0 8 7 21075.9 1073.24 13 0 8 7 17761.9 995.035 15 0 8 8 2814.83 250.486 44 0 8 8 3342.11 325.295 46 0 8 8 3447.68 344.793 35 0 8 9 882.353 213.071 35 0 8 9 594.077 163.398 30 0 8 9 919.946 207.381 46 0 8 10 1274.31 185.886 30 0 8 10 1444.37 209.068 27 0 8 10 1437.81 226.247 46 0 8 10 1347.33 182.680 41 0 8 10 1038.23 226.031 35 0 8 11 1896.09 231.966 35 0 8 11 1749.64 199.896 27 0 8 11 1533.79 186.193 30 0 8 11 1398.84 209.281 46 0 8 12 378.016 132.625 46 0 8 12 264.558 101.122 30 0 8 13 760.856 118.086 40 0 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1 9 9 16282.2 922.086 46 1 9 10 14369.3 714.301 27 1 9 10 15563.3 755.299 35 1 9 10 10897.3 660.901 41 1 9 10 14657.2 739.571 46 1 9 10 10071.7 669.326 30 1 9 11 3695.38 265.824 27 1 9 11 3642.01 292.670 46 1 9 12 589.021 132.775 46 1 9 12 394.774 102.288 30 1 9 13 364.114 94.3385 40 1 9 13 493.433 101.624 46 -1 -10 7 45.2790 54.6648 36 -1 -10 7 13.4449 68.5055 20 -1 -10 6 1506.51 161.205 20 -1 -10 6 1108.52 169.280 49 1 10 -6 1210.80 156.574 24 -1 -10 5 988.928 176.152 49 1 10 -5 957.927 175.351 24 -1 -10 5 929.552 154.254 20 1 10 -4 1973.44 220.123 15 1 10 -4 2378.75 261.059 24 1 10 -3 3008.10 296.789 15 1 10 -3 3752.91 337.282 24 1 10 -2 166.705 149.615 15 1 10 -2 109.290 174.864 24 1 10 -1 792.546 181.121 48 1 10 -1 892.338 211.327 15 1 10 -1 1165.43 237.726 24 -1 -10 0 7960.27 971.145 9 1 10 0 8912.39 598.760 48 1 10 1 18732.7 983.575 15 1 10 1 18295.7 981.827 24 1 10 1 16352.6 943.858 48 1 10 2 5896.01 450.454 24 1 10 2 6076.81 453.549 48 -1 -10 -2 5414.21 721.264 9 1 10 3 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2318.62 219.488 15 1 12 6 1611.11 184.563 35 1 12 7 3546.76 262.200 35 1 12 8 1561.06 156.453 35 1 12 8 1488.73 151.483 41 1 12 8 1751.24 156.438 27 -1 -12 -8 1117.61 129.394 21 1 12 9 12.0587 63.8173 35 1 13 0 868.365 111.898 15 1 13 0 989.048 110.682 24 1 13 1 1122.71 129.530 15 1 13 1 1118.87 120.769 24 -1 -13 -1 883.979 110.667 21 1 13 2 1152.62 120.775 24 -1 -13 -2 1409.53 138.368 21 1 13 3 564.584 111.490 15 -1 -13 -4 483.729 103.021 21 -1 -13 -5 248.023 84.1641 21 -1 -13 -6 199.955 67.6250 21 -2 12 5 555.284 84.9076 41 -2 12 5 283.898 82.5733 27 2 -12 -4 730.646 99.9235 21 -2 12 4 582.243 99.8322 41 -2 12 3 280.276 90.5981 41 2 -12 -3 577.237 100.158 21 -2 12 2 4381.16 245.442 24 2 -12 -2 4751.78 267.366 21 -2 12 1 4465.98 225.009 24 -2 12 1 1768.69 170.841 41 2 -12 0 2310.68 177.828 21 -2 12 0 2348.02 183.611 24 2 -12 1 62.6674 64.0624 21 -2 12 -2 57.2386 62.0718 24 -2 11 8 859.797 99.1726 41 -2 11 8 828.645 105.857 27 -2 11 7 4153.38 273.270 27 -2 11 6 361.835 114.866 41 2 -11 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10 -2 8 -3 4187.65 356.128 15 2 -8 3 4413.06 340.773 14 2 -8 3 4475.90 689.055 4 -2 8 -3 4655.94 384.190 24 2 -8 3 3687.07 359.531 21 -2 8 -4 1675.48 221.974 15 2 -8 4 1549.12 212.329 14 2 -8 4 1483.71 424.858 4 2 -8 4 1309.06 180.701 20 2 -8 4 1431.53 432.159 9 2 -8 4 1469.32 216.974 21 -2 8 -4 1584.99 254.090 24 2 -8 5 2121.10 251.237 21 2 -8 5 2402.95 247.280 20 2 -8 5 2821.15 276.996 14 -2 8 -5 2861.57 298.788 24 2 -8 6 8766.00 551.468 20 -2 8 -6 8936.77 567.610 24 2 -8 6 10278.0 586.725 14 2 -8 7 3226.56 283.022 14 2 -8 7 3282.01 268.604 20 2 -8 8 1689.57 254.058 49 2 -8 8 1900.19 200.998 20 2 -8 9 4324.86 282.889 20 2 -8 9 3420.97 320.171 49 2 -8 10 87.3491 93.5720 49 -2 7 12 3594.47 237.278 46 -2 7 12 3428.08 240.703 40 -2 7 12 3308.09 235.174 28 -2 7 11 552.331 151.150 40 -2 7 11 598.513 140.374 46 -2 7 10 10599.2 621.218 44 -2 7 10 12643.4 647.343 46 -2 7 10 11362.6 623.148 41 -2 7 9 22390.1 1147.22 41 -2 7 9 23375.8 1153.07 46 -2 7 9 22462.4 1142.66 44 -2 7 8 2501.95 270.599 41 -2 7 8 2225.40 241.632 44 -2 7 8 2301.04 261.243 13 -2 7 8 2439.89 253.741 46 -2 7 8 2152.60 265.634 35 -2 7 7 1936.85 252.204 35 -2 7 7 1928.33 257.115 13 -2 7 7 1672.70 221.398 46 -2 7 6 538.750 189.717 35 -2 7 6 680.227 193.402 13 -2 7 6 440.077 163.407 46 -2 7 5 3109.32 263.781 24 -2 7 5 2920.91 286.215 15 2 -7 -5 2273.43 486.544 4 -2 7 5 3248.52 316.821 13 -2 7 5 3082.01 297.694 35 -2 7 5 2928.19 264.833 46 2 -7 -4 2910.42 525.541 4 -2 7 4 2538.46 275.034 15 -2 7 4 2825.10 262.785 24 -2 7 4 2613.15 271.264 35 -2 7 3 27014.0 1417.55 35 -2 7 3 29349.7 1435.99 24 -2 7 3 30764.3 1478.75 13 2 -7 -3 31024.2 1957.61 4 -2 7 3 29527.0 1453.70 15 -2 7 2 13160.4 1107.95 2 2 -7 -2 14237.1 1175.11 4 2 -7 -2 11335.1 961.537 10 -2 7 2 13200.2 743.645 13 -2 7 2 12455.4 717.716 24 2 -7 -1 42594.3 2389.99 10 2 -7 -1 44516.5 2573.21 4 -2 7 1 42759.9 2012.47 24 -2 7 1 42742.6 2013.14 13 -2 7 1 40316.0 1996.04 48 -2 7 1 43316.0 2015.05 15 -2 7 1 40182.2 1950.98 39 2 -7 0 17134.5 877.139 14 2 -7 0 18564.7 1305.15 10 -2 7 0 15795.1 914.832 48 -2 7 0 18129.7 935.091 13 -2 7 0 18169.8 942.774 15 -2 7 0 19324.5 1379.94 2 2 -7 1 13730.0 731.681 14 -2 7 -1 13519.9 754.542 13 -2 7 -1 16075.9 1224.72 2 -2 7 -1 14519.4 790.234 24 -2 7 -1 12081.8 744.258 48 2 -7 1 13974.8 1208.73 4 -2 7 -1 14499.5 783.762 15 2 -7 1 14574.0 1161.29 10 2 -7 2 36.7537 239.166 10 2 -7 2 161.897 273.311 4 -2 7 -2 72.2515 136.407 15 2 -7 2 7.55064 122.307 14 -2 7 -2 135.818 117.977 13 -2 7 -2 122.760 156.687 24 2 -7 3 6863.61 485.212 21 -2 7 -3 6765.91 477.418 15 2 -7 3 8033.20 481.970 14 2 -7 3 6786.95 834.182 4 -2 7 -3 7524.60 504.624 24 2 -7 3 8072.34 846.104 10 2 -7 4 3861.10 614.340 9 2 -7 4 4309.21 340.115 14 -2 7 -4 4262.75 337.311 15 2 -7 4 4073.79 637.062 4 -2 7 -4 4351.59 367.598 24 2 -7 4 3477.00 331.188 21 2 -7 4 3751.29 313.710 20 2 -7 5 18.4628 154.595 14 2 -7 5 155.494 135.478 20 -2 7 -5 208.389 164.943 24 2 -7 5 38.9506 253.497 9 2 -7 5 241.844 262.323 10 2 -7 5 139.620 144.567 21 2 -7 6 1903.25 233.678 20 2 -7 6 1345.93 195.147 21 2 -7 6 1275.90 193.365 42 2 -7 6 1341.98 442.011 10 2 -7 6 2274.19 258.641 14 2 -7 6 2215.85 470.123 9 -2 7 -6 1817.30 244.946 24 2 -7 7 6972.66 470.667 42 2 -7 7 8786.34 524.976 14 -2 7 -7 6415.28 470.278 24 2 -7 7 8173.71 506.938 20 2 -7 8 18982.5 902.030 20 2 -7 8 14433.6 852.147 42 2 -7 9 1144.80 178.068 20 2 -7 9 1122.17 224.427 49 2 -7 9 774.544 137.449 36 2 -7 9 588.295 143.163 42 2 -7 10 154.287 88.6614 36 2 -7 10 444.882 105.553 42 2 -7 10 519.206 126.871 20 2 -7 10 617.436 162.594 49 2 -7 11 89.6794 58.7582 42 2 -7 11 144.280 104.798 49 -2 6 13 139.401 74.1652 28 -2 6 12 1409.08 172.332 46 -2 6 12 1103.96 156.224 28 -2 6 11 5240.66 356.978 40 -2 6 11 4009.10 311.630 44 -2 6 11 4953.14 345.904 46 -2 6 10 12893.0 740.285 41 -2 6 10 14323.8 749.196 30 -2 6 10 13976.6 759.835 44 -2 6 10 15115.6 783.804 46 -2 6 9 39941.2 1877.50 44 -2 6 9 39697.8 1872.81 41 -2 6 9 40517.7 1901.20 35 -2 6 9 36713.2 1849.69 30 -2 6 9 39113.5 1883.78 46 -2 6 8 40278.1 1892.68 44 -2 6 8 40661.2 1914.66 35 -2 6 8 41075.5 1903.09 41 -2 6 8 39173.1 1893.23 46 -2 6 8 39190.9 1906.13 13 -2 6 8 36312.8 1856.14 30 -2 6 7 10324.0 637.588 35 -2 6 7 11370.2 655.369 13 -2 6 7 9912.15 613.934 46 -2 6 6 142.397 157.862 35 -2 6 6 112.292 140.810 46 -2 6 6 121.001 146.804 13 -2 6 5 1170.08 166.505 24 -2 6 5 1162.44 183.646 46 -2 6 5 1248.85 203.631 35 -2 6 5 1350.72 190.449 15 -2 6 5 1571.48 216.598 13 2 -6 -5 1130.00 339.277 4 -2 6 4 10105.0 578.357 24 -2 6 4 10424.7 600.769 35 -2 6 4 10576.3 905.468 2 2 -6 -4 10426.0 925.213 4 -2 6 4 10399.2 602.095 15 -2 6 3 22492.9 1444.29 2 -2 6 3 20262.5 1027.13 24 2 -6 -3 20501.6 1433.14 4 -2 6 3 19790.8 1039.13 15 2 -6 -3 20417.3 1266.22 10 -2 6 2 9446.98 561.834 24 2 -6 -2 9557.35 783.445 10 -2 6 2 9976.11 883.443 2 -2 6 2 9812.74 573.451 15 2 -6 -2 11085.4 937.994 4 -2 6 2 9500.58 569.341 48 2 -6 -1 8741.50 742.976 10 -2 6 1 6924.63 463.778 48 -2 6 1 7630.98 475.622 24 -2 6 1 7888.79 477.635 15 -2 6 0 37112.0 1805.62 15 2 -6 0 40320.1 2186.80 10 -2 6 0 38852.4 2218.20 2 -2 6 -1 22223.5 1131.31 24 2 -6 1 23978.5 1496.99 10 -2 6 -1 22310.7 1124.56 15 2 -6 1 22737.1 1530.64 4 -2 6 -1 20866.1 1471.67 2 2 -6 2 7314.23 744.157 10 -2 6 -2 6818.08 466.956 24 2 -6 2 8606.28 813.102 4 -2 6 -2 8265.41 782.058 2 -2 6 -2 7038.61 453.453 15 2 -6 3 513.527 315.169 4 -2 6 -3 198.218 131.963 15 -2 6 -3 575.128 276.013 2 2 -6 3-100.915 231.358 10 -2 6 -3 231.355 145.660 24 2 -6 4 3180.83 286.521 14 2 -6 4 2855.87 513.440 4 2 -6 4 3228.16 293.905 21 -2 6 -4 3057.16 271.486 15 -2 6 -4 3188.17 300.451 24 2 -6 5 563.816 325.040 9 2 -6 5 1148.21 186.044 21 2 -6 5 733.924 331.622 10 2 -6 5 1309.08 351.723 4 -2 6 -5 1446.65 212.495 24 2 -6 5 1186.66 197.533 14 2 -6 6 1158.26 190.210 20 2 -6 6 938.817 163.584 42 2 -6 6 1012.30 198.346 14 2 -6 6 713.636 167.357 21 -2 6 -6 1029.18 193.672 24 2 -6 6 779.163 328.491 9 2 -6 6 937.018 340.694 10 2 -6 7 9147.89 547.275 20 2 -6 7 7496.75 848.850 10 2 -6 7 8069.54 521.707 42 2 -6 8 6656.87 446.539 20 2 -6 8 5812.67 424.317 42 2 -6 9 1988.49 244.579 36 2 -6 9 2745.71 279.663 14 2 -6 9 2240.17 328.289 49 2 -6 9 2583.42 269.857 42 2 -6 10 1139.51 179.943 42 2 -6 10 1416.89 197.014 20 2 -6 10 891.440 226.006 49 2 -6 10 978.963 166.174 36 2 -6 11 718.485 139.780 20 2 -6 11 602.620 128.192 42 2 -6 11 657.418 174.532 49 2 -6 11 464.008 109.593 36 2 -6 12 244.672 79.7297 42 2 -6 12 313.567 105.909 49 2 -6 12 214.861 68.4986 36 -2 5 13 467.666 119.673 40 -2 5 13 448.158 108.045 28 -2 5 12 352.927 144.073 46 -2 5 12 112.079 105.579 44 -2 5 12 144.089 129.101 28 -2 5 11 771.329 162.850 44 -2 5 11 945.459 200.419 46 -2 5 10 6608.74 441.502 41 -2 5 10 7178.35 480.605 27 -2 5 10 7155.30 464.180 44 -2 5 10 6973.23 466.712 30 -2 5 10 7571.10 487.685 46 -2 5 9 184.592 157.744 30 -2 5 9 102.186 170.983 46 -2 5 9 61.4073 139.841 44 -2 5 9-47.9140 143.414 41 -2 5 8 95154.9 4482.64 30 -2 5 8 102816. 4502.88 44 -2 5 8 99620.4 4506.21 46 -2 5 8 100267. 4496.42 41 -2 5 8 95725.2 4487.55 13 -2 5 8 99283.7 4513.82 35 -2 5 7 67039.4 3118.19 46 -2 5 7 69158.4 3124.50 41 -2 5 7 68584.9 3135.10 35 -2 5 7 64824.8 3096.02 30 -2 5 7 67897.1 3129.78 13 -2 5 6 3862.78 316.868 46 -2 5 6 3867.92 330.692 35 -2 5 6 4584.44 344.305 13 -2 5 6 4658.22 358.870 32 -2 5 5 1221.13 315.256 2 -2 5 5 1298.46 207.501 32 2 -5 -5 1514.01 353.917 4 -2 5 5 1468.01 201.236 13 -2 5 5 1408.69 182.067 46 -2 5 5 1209.22 191.550 35 2 -5 -4 2844.13 440.324 4 -2 5 4 3555.35 461.435 2 2 -5 -3 21953.0 1320.99 10 -2 5 3 23166.8 1444.89 2 2 -5 -3 24119.6 1475.62 4 -2 5 2 917.026 296.564 2 2 -5 -2 771.660 234.820 10 2 -5 -1-22.3908 202.032 10 2 -5 0 23.8981 209.072 10 -2 5 0 100.534 224.508 2 2 -5 1 44682.3 2332.52 10 -2 5 -1 40449.9 2300.37 2 -2 5 -2 899.533 294.611 2 2 -5 2 1211.41 313.044 10 2 -5 2 1291.37 321.269 4 2 -5 3 137391. 6467.89 4 -2 5 -3 133035. 6389.47 2 2 -5 4 31338.4 1873.59 10 2 -5 4 31746.9 1851.09 4 -2 5 -4 29115.9 1766.54 2 2 -5 5 15702.9 855.705 21 2 -5 5 16529.5 858.752 42 2 -5 5 17852.0 1261.28 10 -2 5 -5 16933.4 873.658 24 2 -5 5 16099.4 1169.43 4 2 -5 6 5334.41 380.084 42 2 -5 6 5250.47 660.798 10 -2 5 -6 5123.34 377.614 24 2 -5 6 5510.85 650.798 9 2 -5 7 606.919 175.059 20 2 -5 7 586.437 160.560 42 2 -5 7 153.835 261.536 9 2 -5 7 803.968 309.185 10 2 -5 8 3389.53 314.827 20 2 -5 8 3420.69 311.465 14 2 -5 8 2987.49 298.012 42 2 -5 8 2468.52 468.641 10 2 -5 8 2332.32 617.802 12 2 -5 9 744.960 183.485 20 2 -5 9 714.055 178.619 42 2 -5 9 444.211 221.602 49 2 -5 9 784.353 187.118 14 2 -5 10 481.152 154.835 14 2 -5 10 301.565 201.333 49 2 -5 10 227.431 133.981 36 2 -5 10 478.508 163.497 42 2 -5 10 378.640 163.884 20 2 -5 11 1403.51 188.215 19 2 -5 11 1365.36 190.399 36 2 -5 11 1656.50 208.071 42 2 -5 11 1347.96 236.875 49 2 -5 12 1136.47 195.228 49 2 -5 12 1281.24 159.694 36 2 -5 12 1358.18 165.480 42 2 -5 13 682.593 102.552 42 2 -5 13 508.872 114.949 49 2 -5 13 597.979 102.776 25 -2 4 13 327.613 120.528 40 -2 4 13 355.499 114.714 28 -2 4 12 2579.89 252.097 40 -2 4 12 2029.32 219.595 44 -2 4 12 2544.19 240.282 28 -2 4 12 2993.63 264.666 46 -2 4 11 159.655 134.383 44 -2 4 11 7.46916 114.788 29 -2 4 11-25.6836 179.186 46 -2 4 10 206.187 179.983 46 -2 4 10 85.1105 132.044 41 -2 4 10 146.025 176.317 32 -2 4 10 154.171 163.873 27 -2 4 10 295.821 125.131 29 -2 4 10 250.205 172.380 30 -2 4 10 194.649 139.447 44 -2 4 9 142.824 139.391 44 -2 4 9 339.599 148.061 41 -2 4 9 387.632 188.708 46 -2 4 9 120.243 136.805 29 -2 4 9 189.692 169.692 30 -2 4 9 283.886 190.398 32 -2 4 8 28993.4 1399.68 32 -2 4 8 27990.4 1373.67 46 -2 4 8 27923.6 1351.01 41 -2 4 8 26984.0 1372.29 35 -2 4 8 28336.6 1365.06 44 -2 4 8 27537.6 1361.37 30 -2 4 8 26455.6 1345.49 29 -2 4 8 24787.7 1323.48 13 -2 4 7 59493.7 2894.50 35 -2 4 7 61205.2 2882.27 13 -2 4 7 63331.5 2886.54 41 -2 4 7 62762.3 2894.27 46 -2 4 7 62006.3 2884.50 30 -2 4 7 66209.1 2924.37 32 -2 4 6 114509. 5235.43 30 -2 4 6 119062. 5258.85 13 -2 4 6 117030. 5258.87 35 -2 4 6 115846. 5249.32 46 2 -4 -5 44827.1 2417.04 4 -2 4 5 46696.3 2184.06 13 -2 4 5 48143.0 2429.30 2 2 -4 -4 15151.7 931.070 10 -2 4 4 16794.5 1070.57 2 -2 4 4 16179.7 1003.29 11 2 -4 -4 17200.3 1089.90 4 2 -4 -3 54317.6 2640.60 4 -2 4 3 47513.4 2445.69 11 -2 4 3 53878.6 2627.22 2 2 -4 -3 49989.3 2499.67 10 -2 4 2 620.149 247.002 2 2 -4 -2 508.515 248.686 4 -2 4 2 936.151 153.339 11 2 -4 0 8665.47 668.784 10 -2 4 0 8192.32 685.561 2 2 -4 1 3510.24 437.128 10 -2 4 -1 4568.39 478.065 2 2 -4 2 19698.3 1213.28 4 -2 4 -2 18961.4 1178.51 2 2 -4 2 17976.2 1181.38 10 -2 4 -3 59796.3 3041.52 2 2 -4 3 62251.8 3091.40 4 2 -4 4 65030.6 3183.39 10 -2 4 -4 58723.9 3063.94 2 2 -4 4 62615.7 3134.13 4 2 -4 5 99680.4 4684.20 10 2 -4 5 94950.1 4590.76 4 -2 4 -5 92228.4 4529.47 2 2 -4 6 46283.3 2177.62 18 2 -4 6 48773.3 2192.71 42 2 -4 6 52644.6 2599.06 10 2 -4 7 13555.0 756.003 20 2 -4 7 13231.0 750.877 42 2 -4 7 13400.6 747.491 18 2 -4 7 14236.5 751.496 14 2 -4 7 11859.1 984.844 9 2 -4 7 12900.4 1036.09 10 2 -4 8 200.992 227.356 10 2 -4 8 689.710 383.271 12 2 -4 8 763.484 170.869 18 2 -4 8 714.575 173.899 42 2 -4 8 587.235 164.408 14 2 -4 8 516.168 177.950 20 2 -4 9 619.694 175.170 14 2 -4 9 805.895 194.762 42 2 -4 9 693.224 436.639 12 2 -4 9 327.466 226.692 49 2 -4 9 774.396 191.857 18 2 -4 10 1608.73 215.755 14 2 -4 10 1471.46 227.497 42 2 -4 10 1633.16 287.852 49 2 -4 10 1968.02 243.908 36 2 -4 10 1634.09 236.298 18 2 -4 10 1284.40 497.659 12 2 -4 11 1669.71 219.748 36 2 -4 11 1792.37 270.941 49 2 -4 11 1145.79 162.114 45 2 -4 11 2012.82 240.496 42 2 -4 11 1739.18 226.001 20 2 -4 12 2221.83 238.945 42 2 -4 12 2409.21 226.115 20 2 -4 12 1693.03 211.466 36 2 -4 12 2139.07 266.431 49 2 -4 12 1651.40 195.664 19 2 -4 13 3576.56 257.796 42 2 -4 13 2991.72 243.264 36 2 -4 13 3485.73 283.924 49 2 -4 14 1275.90 131.403 49 2 -4 14 1237.82 113.785 25 -2 3 13 2150.56 208.326 44 -2 3 13 2725.20 220.164 28 -2 3 13 1827.71 199.551 29 -2 3 13 3014.38 227.781 40 -2 3 12 2243.40 236.706 44 -2 3 12 2476.96 245.801 28 -2 3 12 2317.46 249.838 40 -2 3 12 2137.67 235.396 29 -2 3 11 11827.2 645.388 28 -2 3 11 10792.1 640.309 44 -2 3 11 11858.4 654.475 40 -2 3 11 10459.4 642.678 29 -2 3 11 12491.4 672.298 46 -2 3 10 3751.44 328.320 29 -2 3 10 2952.82 283.230 18 -2 3 10 3567.24 327.980 32 -2 3 10 3348.30 312.698 44 -2 3 10 3109.98 324.801 30 -2 3 10 4097.43 347.276 46 -2 3 9 1961.74 220.541 41 -2 3 9 2214.33 246.598 44 -2 3 9 1862.64 242.256 29 -2 3 9 1950.11 257.788 32 -2 3 9 1922.78 251.604 30 -2 3 9 1949.39 234.135 19 -2 3 9 1953.00 216.370 18 -2 3 9 2448.51 272.848 46 -2 3 8 1044.19 174.069 44 -2 3 8 820.455 173.725 19 -2 3 8 662.833 185.919 46 -2 3 8 699.747 191.055 32 -2 3 8 782.625 184.393 30 -2 3 8 563.628 132.895 18 -2 3 8 620.635 161.302 41 -2 3 7 1096.21 169.683 44 -2 3 7 1145.62 187.863 46 -2 3 7 992.245 175.270 30 -2 3 7 1047.30 191.463 35 -2 3 7 1131.21 194.575 32 -2 3 7 1017.58 148.441 13 -2 3 7 1139.07 171.189 41 -2 3 7 1062.23 180.375 19 -2 3 7 1552.00 398.924 8 -2 3 6 148207. 6867.24 35 -2 3 6 152615. 6858.20 13 -2 3 6 166128. 7309.90 11 -2 3 6 158132. 6889.76 49 -2 3 5 101327. 4668.38 11 -2 3 5 101208. 4785.58 8 2 -3 -5 93334.3 4508.31 4 -2 3 5 93463.4 4508.78 2 -2 3 4 13006.2 931.560 8 -2 3 4 10959.0 793.854 11 -2 3 4 11349.2 782.300 2 2 -3 -4 11963.9 786.739 4 -2 3 3 204673. 9355.96 11 -2 3 3 208686. 9493.52 8 -2 3 3 208982. 9408.71 2 2 -3 -3 207322. 9405.45 4 -2 3 2 30854.7 1668.08 8 -2 3 2 31542.1 1652.97 2 2 -3 -2 31682.4 1652.69 4 -2 3 2 29682.0 1534.82 11 2 -3 -1 10132.2 718.363 4 -2 3 0 2855.73 357.768 2 -2 3 -1 6282.70 526.308 2 2 -3 2 149.537 202.320 4 -2 3 -2 97.1512 197.169 2 -2 3 -3 12501.6 807.407 2 2 -3 3 11662.4 807.325 4 2 -3 4 5176.47 506.058 10 2 -3 4 4745.77 463.101 4 -2 3 -4 4877.02 453.294 2 2 -3 5 90211.1 4274.41 4 2 -3 5 95508.5 4386.18 10 -2 3 -5 87187.2 4238.79 2 2 -3 6 67656.7 3414.98 4 2 -3 6 80173.3 3619.90 10 2 -3 7 38906.2 1884.55 18 2 -3 7 38705.2 1879.84 20 2 -3 7 39872.3 2123.34 9 2 -3 7 38504.9 1886.04 42 2 -3 7 42990.1 2460.30 12 2 -3 7 42102.1 1881.89 14 2 -3 7 39749.4 1884.78 29 2 -3 7 37778.9 2151.11 10 2 -3 8 36885.2 1695.49 42 2 -3 8 31392.7 1651.59 47 2 -3 8 35759.4 1687.62 18 2 -3 8 34686.6 1682.61 29 2 -3 8 37176.2 1667.53 14 2 -3 8 35143.1 2300.40 12 2 -3 9 56.4354 128.907 14 2 -3 9 255.970 363.715 12 2 -3 9 48.4864 137.795 29 2 -3 9 60.0247 146.668 42 2 -3 9 50.3016 169.824 49 2 -3 9-83.2941 154.757 47 2 -3 9-29.6301 134.566 18 2 -3 10-81.5784 151.213 29 2 -3 10 125.965 147.975 42 2 -3 10 215.470 357.176 12 2 -3 10 125.950 161.298 18 2 -3 10 153.324 149.888 36 2 -3 10 16.0049 133.170 14 2 -3 10 133.638 162.988 20 2 -3 10-13.0349 194.704 49 2 -3 11 195.105 111.673 45 2 -3 11 370.794 157.777 20 2 -3 11 275.376 166.017 42 2 -3 11 361.252 151.987 36 2 -3 11 124.485 184.897 49 2 -3 11 206.703 167.184 18 2 -3 12 2148.65 250.186 36 2 -3 12 2523.32 268.277 42 2 -3 12 1950.32 287.841 49 2 -3 12 1933.97 230.657 19 2 -3 12 2331.81 243.256 20 2 -3 13 2659.56 273.620 49 2 -3 13 2531.16 243.292 36 2 -3 14 689.803 136.200 49 2 -3 14 788.005 121.030 25 -2 2 13 5955.47 360.684 28 -2 2 13 5151.53 362.909 44 -2 2 13 5353.84 368.846 29 -2 2 12 1797.93 214.692 44 -2 2 12 1942.95 225.594 29 -2 2 12 1404.07 212.692 28 -2 2 12 1282.81 182.963 18 -2 2 12 1391.04 213.139 40 -2 2 11 5636.54 399.758 18 -2 2 11 5684.18 413.208 44 -2 2 11 6058.46 418.421 40 -2 2 11 6829.93 446.720 29 -2 2 11 6387.42 419.489 28 -2 2 10 9958.61 608.520 44 -2 2 10 9165.21 563.389 19 -2 2 10 10280.8 604.179 18 -2 2 10 11330.3 645.926 29 -2 2 10 8205.63 553.688 16 -2 2 10 9741.21 596.631 32 -2 2 10 10243.0 607.427 28 -2 2 10 10739.0 631.705 30 -2 2 10 9792.23 605.296 40 -2 2 9 988.414 213.925 46 -2 2 9 746.169 175.442 44 -2 2 9 678.096 178.275 29 -2 2 9 874.626 164.785 16 -2 2 9 869.043 173.306 18 -2 2 9 941.665 381.258 8 -2 2 9 830.405 188.125 32 -2 2 9 915.945 172.964 19 -2 2 9 657.159 197.233 30 -2 2 8 5183.96 365.918 44 -2 2 8 4396.19 338.502 41 -2 2 8 4368.78 331.361 16 -2 2 8 4982.22 345.696 19 -2 2 8 4612.97 661.653 8 -2 2 8 4897.72 369.511 32 -2 2 8 4903.03 325.795 23 -2 2 8 4854.16 391.197 49 -2 2 8 4874.22 356.374 18 -2 2 8 5424.22 384.021 30 -2 2 8 5212.19 380.454 46 -2 2 7 26485.5 1278.86 44 -2 2 7 26436.2 1306.61 49 -2 2 7 28143.4 1298.52 32 -2 2 7 25333.7 1281.99 30 -2 2 7 28610.5 1749.07 11 -2 2 7 25048.2 1259.27 41 -2 2 7 29967.3 1816.11 8 -2 2 7 25013.2 1278.64 46 -2 2 7 25409.3 1270.67 18 -2 2 6 36600.5 2112.08 8 -2 2 6 33948.5 2030.64 11 -2 2 5 90178.2 4131.36 2 2 -2 -5 84671.8 4097.76 4 -2 2 4 208960. 9497.78 2 -2 2 4 221448. 9720.82 8 2 -2 -4 202017. 9479.90 4 -2 2 4 221214. 9630.58 11 -2 2 3 61465.9 3011.91 2 -2 2 3 65098.0 3139.50 8 -2 2 3 65966.4 3055.45 11 2 -2 -3 61134.5 3000.09 4 -2 2 2 104434. 4943.24 2 2 -2 -2 107567. 4937.95 4 -2 2 2 109849. 5006.49 8 -2 2 1 7905.68 567.446 2 -2 2 1 7882.41 560.211 8 2 -2 -1 7740.42 554.453 4 -2 2 0 1374.35 223.067 8 2 -2 0 1901.20 261.685 4 -2 2 -1 2335.59 297.977 2 -2 2 -2 41593.3 2044.93 2 2 -2 2 40764.7 2044.00 4 -2 2 -3 31963.2 1627.25 2 2 -2 3 31548.2 1634.26 4 -2 2 -4 21077.3 1139.61 2 2 -2 4 20528.9 1149.30 4 2 -2 4 21064.9 1196.13 10 -2 2 -5 35126.2 1802.32 2 2 -2 5 38105.3 1913.70 10 2 -2 5 36207.7 1816.18 4 2 -2 6 30176.7 1474.01 10 2 -2 6 23111.6 1259.34 4 2 -2 7 57291.6 2868.32 10 2 -2 7 55752.2 2807.46 9 2 -2 7 61804.3 3174.76 12 2 -2 8 17704.4 909.530 20 2 -2 8 18260.2 923.731 42 2 -2 8 16399.6 958.454 49 2 -2 8 18290.1 925.944 18 2 -2 8 18465.7 896.529 14 2 -2 8 17464.0 924.768 29 2 -2 8 19248.8 1427.30 12 2 -2 8 15837.1 902.558 47 2 -2 8 14684.4 1050.82 10 2 -2 9 22002.3 1107.31 42 2 -2 9 18906.5 1079.08 47 2 -2 9 21374.9 1109.08 18 2 -2 9 22137.0 1113.27 29 2 -2 9 21934.6 1063.68 14 2 -2 9 19169.7 1053.11 31 2 -2 9 19919.7 1144.23 49 2 -2 9 20174.2 1656.16 12 2 -2 9 21824.1 1091.61 20 2 -2 10 6510.86 437.394 20 2 -2 10 4821.37 379.801 31 2 -2 10 5539.53 439.157 36 2 -2 10 5414.55 476.727 49 2 -2 10 5988.39 458.696 29 2 -2 10 5803.89 431.750 47 2 -2 10 6239.03 457.033 18 2 -2 10 6123.73 900.496 12 2 -2 10 5491.69 393.049 14 2 -2 11 13298.6 773.387 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1690.61 211.246 24 -3 9 -6 1238.05 165.873 24 3 -9 6 1404.31 178.902 14 -3 9 -7 99.3403 104.812 39 3 -9 8 383.998 120.553 49 -3 8 10 418.762 94.5254 41 -3 8 10 406.897 105.280 40 -3 8 9 21.1689 108.689 41 -3 8 9 106.306 110.767 40 -3 8 9 19.5332 91.1663 44 -3 8 9-11.7344 126.841 27 -3 8 8 126.237 113.220 44 -3 8 8 144.683 139.221 27 -3 8 8 169.331 140.305 41 -3 8 7 3057.32 296.121 27 -3 8 7 2889.15 285.185 13 -3 8 6 3600.58 297.555 35 -3 8 6 3712.81 340.048 13 -3 8 5 3749.34 298.002 35 3 -8 -5 3240.04 289.225 21 -3 8 5 3745.49 296.448 24 3 -8 -4 5871.37 412.492 21 -3 8 4 6010.13 409.423 24 3 -8 -3 4779.79 389.746 21 3 -8 -3 5122.60 720.922 4 -3 8 3 5331.06 427.453 13 -3 8 3 5414.30 400.009 24 -3 8 3 5606.17 424.870 15 -3 8 2 198.208 165.715 13 3 -8 -2-18.7356 169.104 21 -3 8 2 112.667 157.637 24 3 -8 -2 91.9139 248.836 4 3 -8 -1 50570.0 2361.03 21 -3 8 1 51749.3 2377.98 15 -3 8 1 50119.3 2371.74 13 3 -8 -1 46599.2 2948.00 4 -3 8 1 51689.2 2366.45 24 -3 8 1 47635.3 2293.12 39 3 -8 0 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336.724 4 3 -7 4 1576.71 231.136 21 -3 7 -4 1316.38 228.260 24 -3 7 -4 1347.78 206.850 15 3 -7 4 1329.69 213.041 14 3 -7 5 3088.15 580.832 10 3 -7 5 3738.04 604.558 9 3 -7 5 4326.30 345.755 14 3 -7 5 3611.13 329.234 21 3 -7 5 3771.94 301.409 20 -3 7 -5 4070.22 350.233 24 3 -7 5 3398.47 550.213 4 3 -7 6 38.5398 129.591 20 3 -7 6 264.600 285.457 9 3 -7 6 204.776 159.974 14 3 -7 6 215.359 138.827 21 -3 7 -6 293.911 151.730 24 3 -7 6 79.4903 238.001 10 3 -7 7 3071.99 275.710 20 3 -7 7 3334.63 299.542 14 -3 7 -7 2373.48 253.969 24 3 -7 8 1766.88 214.749 20 3 -7 8 1794.06 234.393 14 3 -7 9 8554.94 526.319 42 3 -7 9 9953.97 639.741 49 3 -7 10 2469.93 186.740 42 3 -7 10 2934.46 277.935 49 3 -7 11 917.701 137.319 49 -3 7 -11 953.454 121.702 39 -3 6 12 170.702 92.2574 40 -3 6 12 101.564 84.5420 28 -3 6 11 5777.78 356.909 40 -3 6 11 6042.57 352.157 46 -3 6 10 35925.7 1835.52 41 -3 6 10 40443.7 1859.80 44 -3 6 10 41018.5 1866.99 40 -3 6 10 40820.1 1855.43 46 -3 6 9 21427.3 1130.60 41 -3 6 9 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1 4 8 8 3299.67 320.344 32 4 8 8 3385.39 620.966 7 4 8 8 3850.26 346.508 48 4 8 9 22886.4 1166.26 43 4 8 9 23899.8 1223.34 37 4 8 9 21027.1 1151.83 32 4 8 9 21206.9 1150.79 48 4 8 9 23462.7 1191.15 22 4 8 10 73.9276 159.079 43 4 8 10-64.6429 178.191 38 4 8 10 129.995 211.453 37 4 8 10-103.816 183.559 35 4 8 10 9.06328 149.453 32 4 8 11 6393.62 481.680 46 4 8 11 5597.48 442.161 38 4 8 11 6297.14 471.207 37 4 8 11 5587.56 444.821 35 4 8 11 5845.19 436.020 32 4 8 12 3665.92 324.886 38 4 8 12 3868.62 333.601 22 4 8 12 3816.80 325.118 35 4 8 12 3889.25 333.481 32 4 8 12 4050.87 355.848 46 4 8 13 1733.46 192.426 35 4 8 13 1906.28 223.090 32 4 8 13 1849.27 221.083 46 4 8 14 379.114 113.074 46 4 8 14 190.196 116.355 32 4 8 14 150.071 118.939 30 4 8 15 797.553 106.986 30 -4 -9 7 30.5738 80.1719 20 -4 -9 7 83.5259 76.1572 42 -4 -9 6 7798.25 466.153 17 -4 -9 5 5717.37 388.111 17 -4 -9 4 1936.59 216.787 17 4 9 -4 1562.31 214.766 15 -4 -9 3 53.2834 124.388 17 4 9 -3-43.3421 144.220 15 4 9 -2 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295.004 7 4 9 6 262.174 160.551 22 4 9 7 723.145 186.200 22 -4 -9 -7 160.679 271.933 1 4 9 7 463.057 161.619 15 4 9 7 281.405 281.386 7 4 9 7 390.662 187.926 48 4 9 8 2800.16 308.819 48 4 9 8 3351.08 340.969 38 4 9 8 2697.04 332.832 37 4 9 8 2835.70 303.307 22 -4 -9 -8 2660.99 503.333 1 4 9 8 2271.24 522.148 7 4 9 9 614.153 194.748 22 4 9 9 391.354 187.917 38 4 9 9 381.950 218.314 37 4 9 9 238.300 142.583 32 4 9 9 441.928 166.000 48 4 9 10 1537.67 250.202 37 4 9 10 1259.83 247.915 35 4 9 10 1312.10 197.506 32 4 9 10 1824.12 244.810 22 4 9 11 4978.05 383.088 38 4 9 11 4779.62 380.704 37 4 9 11 4444.27 374.061 35 4 9 11 3632.84 326.584 32 4 9 12 4511.78 345.816 38 4 9 12 4614.66 339.190 35 4 9 12 4069.80 318.441 32 4 9 13 4714.29 322.986 35 4 9 13 5660.18 359.366 46 4 9 14 1151.70 140.926 30 4 9 14 1434.47 144.069 46 -4 -10 6 321.722 75.0329 42 -4 -10 6 110.698 81.2533 20 -4 -10 5 2336.94 214.983 42 4 10 -5 2906.36 233.118 24 -4 -10 4 2294.91 206.156 17 4 10 -4 2094.00 209.292 15 -4 -10 3 1005.04 149.935 17 4 10 -3 959.990 175.079 15 -4 -10 2 3609.20 284.777 17 4 10 -2 4195.29 349.084 15 4 10 -2 3529.26 296.200 48 4 10 -1 147.337 140.820 48 4 10 -1 188.113 167.322 15 4 10 0 4408.06 378.254 15 4 10 0 3932.18 353.835 48 4 10 1 1850.80 263.897 15 4 10 1 1435.03 241.140 48 -4 -10 -2 929.085 398.098 1 4 10 2 867.517 216.064 34 4 10 2 1003.12 428.034 7 4 10 2 979.703 218.453 48 4 10 3 3311.60 355.273 15 4 10 3 4385.60 381.492 48 4 10 4 17545.5 1050.08 38 4 10 4 23091.3 1117.22 15 4 10 4 17633.9 1683.11 7 -4 -10 -4 17418.2 1559.64 1 4 10 4 22563.3 1119.37 48 4 10 5 1067.54 213.520 38 4 10 5 1356.71 224.787 15 4 10 5 1331.22 455.415 7 -4 -10 -5 644.889 379.428 1 4 10 6 2357.54 289.686 38 4 10 6 2494.87 280.985 15 4 10 7 1854.33 259.970 38 4 10 7 1304.71 254.784 37 4 10 7 1547.21 222.343 15 4 10 7 1887.78 275.756 48 4 10 8 2019.92 272.231 38 4 10 8 1578.39 260.979 37 4 10 8 1430.28 247.659 48 4 10 9 1920.70 265.129 38 4 10 9 1713.03 241.506 48 4 10 9 1866.09 259.525 37 4 10 10 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559.772 13 -5 9 1 10648.1 562.225 24 5 -9 -1 10542.8 554.195 21 -5 9 0 2455.33 216.023 41 -5 9 0 3068.46 266.108 13 5 -9 0 3167.30 267.422 21 5 -9 1 456.402 149.023 21 -5 9 -1 372.851 106.682 39 -5 9 -1 112.988 118.375 13 -5 9 -1 449.057 151.824 24 -5 9 -2 224.570 110.562 39 -5 9 -2 280.926 141.175 24 -5 9 -3 1853.23 185.767 39 -5 9 -3 2064.45 214.698 24 5 -9 3 1930.17 211.170 21 -5 9 -4 1278.33 162.400 39 -5 9 -4 1359.79 165.116 24 5 -9 4 1250.35 168.332 21 -5 9 -5 2844.74 217.797 39 -5 9 -5 2456.18 205.913 24 5 -9 5 2762.09 208.599 21 -5 9 -6 3970.86 257.973 39 -5 9 -7 61.1120 64.0579 39 5 -9 7 93.4775 69.7448 49 -5 8 8 222.907 67.7511 44 -5 8 7 95.2788 86.6082 44 -5 8 7 93.5463 97.0611 41 -5 8 7 106.481 89.9754 27 -5 8 6 99.6518 97.6763 44 -5 8 6 66.1340 111.232 41 -5 8 6 52.8285 102.037 27 -5 8 6 49.6232 100.786 13 -5 8 5 544.788 146.626 41 -5 8 5 555.261 130.365 27 -5 8 5 658.106 146.110 13 -5 8 4 325.599 147.089 41 -5 8 4 228.296 123.762 27 5 -8 -4 100.152 100.783 21 -5 8 4 185.446 138.712 13 -5 8 3 5687.29 391.450 41 -5 8 3 6068.24 390.897 24 5 -8 -3 5306.35 365.005 21 -5 8 2 6812.81 446.149 41 -5 8 2 6573.88 475.156 13 -5 8 2 7359.82 460.258 24 5 -8 -2 6891.63 446.241 21 -5 8 1 6734.44 431.612 41 -5 8 1 6173.81 400.056 39 -5 8 1 6448.37 462.760 13 -5 8 1 6857.50 453.698 24 5 -8 -1 7015.28 445.865 21 5 -8 0 115.958 158.916 21 -5 8 0 13.3135 128.577 41 -5 8 0 94.5176 123.296 39 -5 8 0 68.1837 136.755 13 -5 8 -1 34486.9 1659.56 39 -5 8 -1 31833.7 1690.43 13 -5 8 -1 36648.7 1704.44 24 5 -8 1 36282.0 1698.52 21 -5 8 -2 5184.86 364.989 39 -5 8 -2 4593.11 366.686 13 -5 8 -2 5482.50 396.054 24 5 -8 2 5254.80 390.711 21 -5 8 -3 1917.83 215.115 39 5 -8 3 1677.79 193.811 14 -5 8 -3 1248.71 183.222 13 -5 8 -3 2322.51 243.896 24 -5 8 -4 3335.80 288.414 39 5 -8 4 2875.82 267.430 14 -5 8 -4 3580.09 298.565 24 5 -8 4 3982.34 308.495 21 5 -8 5 1116.47 170.976 21 -5 8 -5 1043.86 175.422 39 5 -8 5 751.082 151.884 14 -5 8 -5 965.895 163.884 24 5 -8 6 2932.18 246.520 21 5 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599.493 342.501 4 5 -7 -1 735.002 184.678 21 -5 7 0 25421.3 1241.13 39 5 -7 0 23165.9 1774.36 4 5 -7 0 25706.3 1271.70 21 5 -7 1 52298.3 3330.09 10 -5 7 -1 61007.6 2825.14 39 -5 7 -1 62671.7 2860.50 24 -5 7 -1 55913.9 3415.04 2 5 -7 1 62223.6 2857.11 21 5 -7 2 46644.0 3090.64 10 -5 7 -2 55562.5 2589.32 39 5 -7 2 48449.5 3150.97 4 -5 7 -2 57437.5 2618.08 24 -5 7 -2 52554.9 3177.98 2 5 -7 2 57482.0 2618.45 21 5 -7 3 11771.1 1126.84 10 -5 7 -3 12604.1 706.074 39 5 -7 3 9270.58 1046.22 4 -5 7 -3 13303.1 722.608 24 -5 7 -3 9642.19 1045.81 2 -5 7 -4 2505.52 266.425 39 -5 7 -4 1658.34 217.002 13 -5 7 -4 2499.42 266.485 24 5 -7 4 2673.79 276.294 21 5 -7 5 946.464 192.665 21 5 -7 5 712.757 174.584 14 -5 7 -5 1060.46 188.377 24 5 -7 6 525.261 155.467 21 5 -7 6 418.803 150.341 14 -5 7 -6 300.144 135.446 24 -5 7 -7 5266.86 371.199 39 5 -7 7 5278.86 360.986 14 -5 7 -8 187.016 136.132 39 5 -7 8 132.740 110.629 14 -5 7 -9-5.10938 107.562 39 5 -7 9 80.8784 99.5048 14 5 -7 9 120.807 112.524 49 -5 7 -10 1380.28 136.463 39 5 -7 10 614.311 119.671 49 -5 6 10 199.444 71.9090 44 -5 6 10 45.8745 74.6151 28 -5 6 9 744.059 120.163 40 -5 6 9 848.722 132.280 28 -5 6 9 686.271 128.917 44 -5 6 8 6340.97 397.967 41 -5 6 8 5897.95 367.334 40 -5 6 7 10340.6 555.949 40 -5 6 7 11542.0 589.262 27 -5 6 6 21313.5 1092.83 40 -5 6 6 24438.8 1151.53 41 -5 6 6 22391.6 1127.34 27 -5 6 6 21117.4 1145.97 13 -5 6 5 564.412 180.323 41 -5 6 5 413.188 134.744 40 -5 6 5 352.004 152.886 27 -5 6 5 423.793 163.156 13 -5 6 4 6056.71 415.098 41 -5 6 4 4003.43 640.807 2 -5 6 4 4719.68 346.796 39 -5 6 4 5280.72 386.404 27 -5 6 4 5817.19 440.566 13 5 -6 -3 7.10010 121.890 21 -5 6 3 90.7324 149.618 41 -5 6 3 196.979 246.274 2 -5 6 3 61.0585 121.507 39 -5 6 3 34.2747 147.101 24 5 -6 -3-336.700 305.670 4 -5 6 2 5278.69 389.051 41 -5 6 2 5394.20 364.878 39 -5 6 2 4947.82 692.809 2 -5 6 2 5291.62 391.094 24 5 -6 -2 3784.04 633.474 4 5 -6 -2 4492.64 358.521 21 5 -6 -1 1102.66 203.052 21 5 -6 -1 767.861 313.801 10 -5 6 1 1700.76 456.883 2 -5 6 1 1113.76 184.741 39 -5 6 1 1380.15 226.078 24 5 -6 -1 1532.31 420.392 4 5 -6 0 2546.86 506.902 10 -5 6 0 2953.47 277.423 39 5 -6 0 3645.79 608.029 4 5 -6 0 2980.66 295.659 21 5 -6 1 7416.50 853.178 10 -5 6 -1 8804.64 536.804 39 -5 6 -1 9395.90 964.321 2 -5 6 -1 8911.22 561.628 24 5 -6 1 8502.43 551.395 21 5 -6 2 25857.0 1837.27 10 -5 6 -2 26449.6 1319.58 39 5 -6 2 26759.9 1852.68 4 -5 6 -2 25070.7 1816.93 2 -5 6 -2 26168.6 1335.49 24 5 -6 2 26373.6 1336.17 21 5 -6 3 52113.2 3060.19 4 -5 6 -3 51012.8 3032.22 2 -5 6 -3 52888.4 2496.28 24 -5 6 -3 53699.9 2489.07 39 5 -6 3 49850.3 3039.69 10 5 -6 4 4238.49 643.213 10 -5 6 -4 3919.20 617.195 2 -5 6 -4 4399.50 353.079 24 5 -6 4 2881.14 571.199 4 5 -6 4 4028.52 354.067 21 -5 6 -5 1991.28 444.135 2 -5 6 -5 2041.92 250.685 24 5 -6 5 1736.25 419.179 4 5 -6 5 2585.36 277.577 21 5 -6 6 1343.83 213.837 21 5 -6 6 1689.60 415.166 10 -5 6 -6 1354.78 194.280 24 5 -6 7 1072.41 188.320 21 5 -6 7 1816.96 229.239 14 5 -6 8 863.256 175.925 14 5 -6 8 625.451 136.875 21 5 -6 9-8.59939 152.837 49 -5 6 -10 573.025 136.012 39 5 -6 10 602.790 133.972 14 5 -6 10 500.736 141.071 49 -5 6 -11 1784.08 158.001 39 5 -6 11 1754.09 153.215 45 -5 5 10 8.71809 83.4366 44 -5 5 10 56.7281 95.7912 40 -5 5 10-15.6810 98.7908 28 -5 5 9 31.6965 122.034 40 -5 5 9 257.925 130.006 28 -5 5 8 302.123 155.133 41 -5 5 8 486.745 147.690 40 -5 5 7 9364.29 513.320 40 -5 5 7 8013.35 476.822 46 -5 5 7 9154.42 520.745 27 -5 5 6 2698.85 259.412 40 -5 5 6 3005.91 284.435 27 -5 5 6 2743.27 276.644 13 -5 5 5 12508.8 670.221 41 -5 5 5 10881.7 616.878 40 -5 5 5 9681.79 595.947 39 -5 5 5 11357.7 647.339 27 -5 5 5 10680.8 672.227 13 -5 5 4 15022.1 794.273 41 -5 5 4 13602.6 744.556 39 5 -5 -4 11621.3 1034.71 4 -5 5 4 14015.2 771.045 27 -5 5 4 13605.9 1143.91 2 -5 5 3 5311.26 386.296 41 -5 5 3 4956.39 350.898 39 5 -5 -3 4745.40 628.952 4 -5 5 3 4753.69 657.955 2 -5 5 3 4842.46 369.111 24 5 -5 -3 4359.16 331.119 21 -5 5 2 9653.00 582.118 41 5 -5 -2 10380.0 961.186 4 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1613.72 218.606 24 5 -5 5 1770.00 240.898 21 5 -5 6 234.219 159.617 21 5 -5 6 169.174 285.984 10 -5 5 -6 503.874 300.441 2 5 -5 6 551.034 277.884 4 -5 5 -6 419.380 158.687 24 5 -5 7 7444.21 849.933 10 5 -5 7 6378.05 453.793 47 5 -5 7 7688.26 476.140 21 5 -5 8 2410.38 253.359 47 5 -5 8 2679.68 250.610 21 5 -5 9 90.9661 94.4586 42 5 -5 9-87.2127 141.644 14 5 -5 9-113.544 160.237 49 5 -5 10 36.9803 120.873 14 5 -5 10 43.9126 139.083 49 -5 5 -11 237.838 117.747 39 5 -5 11 402.338 120.113 14 5 -5 11 203.027 122.592 49 5 -5 12 774.507 126.457 49 -5 5 -12 1070.13 116.462 39 5 -5 12 1124.26 125.785 45 -5 4 11 127.556 86.2633 44 -5 4 11 248.498 90.0609 28 -5 4 10 2094.80 210.137 40 -5 4 10 2194.11 204.878 28 -5 4 9 3120.62 272.961 40 -5 4 9 2896.69 262.515 28 -5 4 8 883.898 188.069 41 -5 4 8 695.111 178.521 40 -5 4 8 802.843 144.467 29 -5 4 8 981.866 144.476 23 -5 4 7 4479.23 345.436 44 -5 4 7 4108.05 324.925 40 -5 4 7 2904.15 263.168 39 -5 4 7 4007.15 338.760 41 -5 4 7 3406.65 314.797 27 -5 4 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1376.36 4 -5 4 -1 18165.4 962.591 24 5 -4 1 17695.8 955.612 21 -5 4 -2 145.537 279.132 2 5 -4 2 434.339 147.893 21 -5 4 -2 446.372 145.422 24 -5 4 -3 975.310 364.622 2 5 -4 3 768.713 171.976 21 -5 4 -3 751.810 157.166 24 5 -4 3 978.862 329.670 4 -5 4 -4 12317.3 1014.65 2 5 -4 4 10306.7 942.029 4 -5 4 -4 10052.9 607.263 24 5 -4 4 11072.3 626.370 21 -5 4 -5 18833.7 1365.63 2 5 -4 5 16909.0 1312.66 4 -5 4 -5 18159.1 960.197 24 5 -4 5 19274.6 984.915 21 5 -4 5 20471.1 1470.06 10 5 -4 6 113.725 114.522 20 5 -4 6 324.211 283.306 10 -5 4 -6 32.7170 260.783 2 5 -4 6 153.356 199.652 4 -5 4 -6 121.259 124.940 24 5 -4 6 198.662 154.270 21 5 -4 7 1121.64 193.546 21 5 -4 7 1110.11 164.707 42 5 -4 7 1004.29 176.890 20 5 -4 7 671.804 325.691 10 5 -4 8 16445.0 1362.82 10 5 -4 8 19242.3 961.378 20 5 -4 8 18074.3 937.071 42 5 -4 8 17100.4 971.386 47 5 -4 8 18804.4 944.487 21 5 -4 9 14056.1 716.564 42 5 -4 9 15830.6 772.280 14 5 -4 9 12071.1 727.562 47 5 -4 9 11831.7 761.848 49 5 -4 9 10577.9 666.320 21 5 -4 10 148.386 120.271 42 5 -4 10 215.305 168.927 49 5 -4 10 403.146 150.837 14 5 -4 10 308.409 156.944 47 5 -4 11 740.210 153.232 42 5 -4 11 742.942 157.812 14 5 -4 12 457.609 117.658 45 -5 4 -12 268.056 102.256 39 5 -4 12 267.145 105.642 14 5 -4 12 142.988 122.980 49 5 -4 13 1061.96 132.641 19 5 -4 13 599.587 110.306 25 -5 3 11 7678.04 422.095 28 -5 3 10 11040.0 586.432 40 -5 3 10 12376.5 590.913 28 -5 3 9 7783.44 471.260 44 -5 3 9 7204.47 460.543 40 -5 3 9 6134.41 446.116 29 -5 3 9 7354.37 457.612 28 -5 3 8 4536.49 347.355 44 -5 3 8 4429.29 339.034 40 -5 3 8 2915.63 272.307 18 -5 3 8 3483.14 286.711 16 -5 3 8 4275.59 343.544 46 -5 3 8 3895.18 299.966 23 -5 3 7 10720.0 599.762 44 -5 3 7 9817.95 588.468 41 -5 3 7 9577.25 570.498 40 -5 3 7 8419.92 533.579 39 -5 3 7 7537.25 527.064 18 -5 3 7 8931.93 563.150 46 -5 3 7 9962.36 579.333 27 -5 3 7 9391.04 550.321 23 -5 3 6 501.865 159.749 44 -5 3 6 512.818 177.570 40 -5 3 6 378.489 139.007 39 -5 3 6 455.635 169.543 27 -5 3 6 411.332 134.158 13 -5 3 6 271.492 267.160 11 -5 3 6 375.841 168.512 46 -5 3 5 149.517 154.529 41 -5 3 5 337.778 162.862 40 -5 3 5 431.514 144.067 39 -5 3 5 321.523 336.988 8 -5 3 5 393.058 153.510 27 -5 3 5 216.281 252.332 11 -5 3 5 324.070 151.938 46 -5 3 4 1430.48 352.461 2 -5 3 4 1380.88 190.116 40 -5 3 4 1412.74 187.918 39 -5 3 4 1091.13 387.059 8 -5 3 4 1320.64 191.754 27 -5 3 4 1316.99 199.117 41 -5 3 4 1542.47 355.397 11 -5 3 3 2644.08 472.582 2 -5 3 3 3424.97 286.268 41 -5 3 3 3147.09 265.602 39 -5 3 3 3657.33 555.663 8 5 -3 -3 3562.15 482.815 4 -5 3 3 2924.87 262.100 27 -5 3 3 2402.30 427.037 11 -5 3 2 49554.7 2306.04 41 -5 3 2 50542.7 2296.50 39 -5 3 2 51167.1 2761.67 8 -5 3 2 52720.9 2791.97 2 5 -3 -2 46577.4 2657.00 4 -5 3 2 47714.9 2302.61 24 -5 3 1 43357.8 2041.06 41 -5 3 1 43401.8 2038.60 39 -5 3 1 46939.6 2442.91 8 -5 3 1 46593.4 2535.27 2 5 -3 -1 44325.9 2448.56 4 -5 3 1 42961.9 2054.44 24 -5 3 0 335865. 14728.6 39 -5 3 0 363009. 15295.9 2 5 -3 0 339925. 15191.4 4 -5 3 0 323286. 14738.1 24 5 -3 1 94709.1 4524.88 4 -5 3 -1 88881.0 4071.52 24 5 -3 2 3605.23 284.394 21 -5 3 -2 4723.48 587.491 2 -5 3 -3 4902.77 331.988 39 -5 3 -3 5410.60 629.795 2 5 -3 3 4995.45 590.596 4 -5 3 -3 4411.30 324.486 24 5 -3 3 4687.91 329.338 21 -5 3 -4 1837.94 203.332 24 5 -3 4 2196.00 397.468 4 -5 3 -4 2387.61 434.501 2 -5 3 -5 22544.2 1472.57 2 5 -3 5 21158.4 1396.56 4 -5 3 -5 20438.9 1049.03 24 5 -3 5 21754.1 1074.83 21 5 -3 6 150.616 135.792 21 -5 3 -6 153.178 228.082 2 5 -3 6 115.823 112.964 20 5 -3 6 587.850 303.934 10 5 -3 6 326.056 216.669 4 5 -3 7-30.1691 144.692 21 5 -3 7-61.3386 122.991 20 5 -3 7 369.816 302.165 10 5 -3 7 36.9842 279.202 12 5 -3 7 142.788 107.805 42 5 -3 8 182.540 137.311 21 5 -3 8 326.676 143.762 20 5 -3 8 175.401 125.429 42 5 -3 8 283.876 252.310 10 5 -3 8 328.289 314.344 12 5 -3 9 25012.0 1744.66 10 5 -3 9 30877.4 1383.62 42 5 -3 9 26253.8 1329.78 21 5 -3 9 22121.5 1873.60 12 5 -3 9 25798.8 1403.85 49 5 -3 9 28943.8 1420.17 47 5 -3 10 3885.51 315.176 42 5 -3 10 3548.34 285.103 36 5 -3 10 3919.83 325.714 14 5 -3 10 2952.87 333.787 49 5 -3 10 3148.36 334.150 47 5 -3 11 7523.44 451.618 42 5 -3 11 5162.35 412.209 31 5 -3 11 6593.92 434.031 14 5 -3 11 6512.84 453.529 47 5 -3 11 6057.66 462.789 49 5 -3 12 654.655 150.299 45 5 -3 12 732.907 146.902 42 5 -3 12 380.041 118.014 14 5 -3 12 179.315 137.297 49 5 -3 12 460.264 146.827 47 5 -3 13-17.3475 86.6352 45 5 -3 13-30.7958 120.491 19 5 -3 13-61.7185 102.284 49 5 -3 14 107.721 77.2287 19 5 -3 14 23.4451 68.8318 25 -5 2 11 2312.75 211.544 29 -5 2 11 3455.71 233.365 28 -5 2 10 14840.8 766.185 44 -5 2 10 12564.0 751.318 29 -5 2 10 14990.4 754.426 28 -5 2 9 18607.3 895.816 44 -5 2 9 18266.7 891.583 40 -5 2 9 13374.1 834.425 18 -5 2 9 14614.3 829.718 16 -5 2 9 16393.0 892.742 29 -5 2 9 19769.2 888.303 28 -5 2 9 14976.5 827.050 23 -5 2 8 7870.39 499.922 44 -5 2 8 7791.45 493.120 40 -5 2 8 6321.04 456.709 18 -5 2 8 6613.44 454.814 16 -5 2 8 8170.98 490.832 28 -5 2 8 6422.29 448.310 23 -5 2 7 16655.7 834.818 44 -5 2 7 15675.7 817.040 40 -5 2 7 13215.3 781.951 39 -5 2 7 13577.9 794.675 18 -5 2 7 13095.9 1325.91 8 -5 2 7 10974.7 1210.39 11 -5 2 7 14299.2 788.666 23 -5 2 7 14586.8 815.994 46 -5 2 6 15311.6 819.466 44 -5 2 6 14790.0 810.664 40 -5 2 6 14499.6 796.619 39 -5 2 6 15525.9 1380.78 8 -5 2 6 14361.6 808.553 27 -5 2 6 14600.2 1274.64 11 -5 2 6 14107.1 812.085 46 -5 2 5 2006.21 235.377 44 -5 2 5 1729.92 226.807 40 -5 2 5 2261.07 224.372 39 -5 2 5 1996.88 520.679 8 -5 2 5 1990.63 231.412 27 -5 2 5 2186.43 237.817 46 -5 2 5 1562.02 399.011 11 -5 2 4 10218.7 579.627 41 -5 2 4 10313.6 566.247 40 -5 2 4 9649.99 559.282 39 -5 2 4 10351.9 988.202 8 -5 2 4 8316.53 804.174 2 -5 2 4 9538.71 559.003 27 -5 2 4 9345.96 905.585 11 -5 2 4 9056.99 553.802 46 -5 2 3 1356.10 182.861 41 -5 2 3 1212.64 166.803 40 -5 2 3 1272.11 169.175 39 -5 2 3 1401.94 392.555 8 -5 2 3 1439.21 173.269 27 -5 2 3 1518.76 354.438 2 -5 2 2 715.412 147.722 41 -5 2 2 896.020 145.319 39 -5 2 2 447.086 278.405 8 5 -2 -2 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32 5 9 13 5281.40 356.246 46 5 9 14 2849.60 236.219 30 5 9 14 2800.78 211.591 46 -5 -10 5 335.196 91.0750 42 5 10 -5 505.067 100.426 24 -5 -10 4 1983.55 178.810 17 5 10 -4 1696.63 169.055 15 -5 -10 3 1000.47 142.185 17 5 10 -3 846.768 163.583 15 -5 -10 2 845.314 144.413 17 5 10 -2 961.847 185.813 15 5 10 -2 803.691 150.510 48 -5 -10 1 1056.15 157.908 17 5 10 -1 1600.41 230.793 15 5 10 -1 1376.24 198.027 48 5 10 0 4207.27 358.762 34 5 10 0 4081.32 365.172 15 5 10 0 4321.12 352.991 48 5 10 1 2444.21 288.784 34 5 10 1 2340.65 282.472 15 5 10 1 2266.89 276.212 48 5 10 2-19.4437 169.641 48 5 10 2 20.3787 161.349 34 5 10 3 124.062 165.651 34 5 10 3 514.246 187.674 15 5 10 3 635.575 200.573 48 5 10 4 6166.00 478.785 15 5 10 4 6778.84 497.913 48 5 10 5 9877.33 632.129 34 5 10 5 9569.83 620.689 15 5 10 6 3353.25 331.072 15 5 10 6 2944.33 296.105 22 5 10 6 3879.26 366.602 48 5 10 7 1578.76 234.655 15 5 10 7 2459.70 299.102 48 5 10 7 1936.32 248.979 22 5 10 8 862.722 191.710 22 5 10 8 983.464 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451.959 6 -6 -8 -6 6038.09 807.718 1 6 8 6 6716.18 478.247 48 6 8 6 5830.07 434.054 22 6 8 6 5108.81 762.572 3 -6 -8 -7 207.298 313.132 1 6 8 7 121.960 134.267 43 6 8 7 344.100 308.707 3 6 8 7 329.779 152.046 34 6 8 7 257.315 138.944 15 6 8 7 351.624 351.210 7 6 8 7 132.907 167.696 48 6 8 7 217.708 158.160 22 6 8 8-15.7483 127.145 43 -6 -8 -8 119.557 269.110 1 6 8 8 148.927 142.474 34 6 8 8 244.767 272.307 7 6 8 8 98.8567 163.428 48 6 8 8 66.6835 165.375 22 6 8 9 4880.11 387.026 43 6 8 9 5987.60 430.575 22 6 8 9 4332.13 734.562 7 6 8 9 4607.45 388.491 48 6 8 10 3390.70 318.253 43 6 8 10 4117.79 409.591 37 6 8 10 4341.97 358.336 22 6 8 11 24433.4 1117.22 43 6 8 11 16118.1 1082.06 35 6 8 11 19319.3 1079.39 32 6 8 11 26056.4 1154.39 22 6 8 11 23004.6 1163.10 46 6 8 12 520.155 165.064 46 6 8 12 436.157 161.387 43 6 8 12 314.548 158.559 38 6 8 12 453.686 146.322 32 6 8 13 247.604 125.115 46 6 8 13 69.9102 116.474 38 6 8 13 371.284 130.902 32 6 8 13 163.449 140.140 22 6 8 14 33.3814 89.8989 32 6 8 15 424.766 93.5401 30 -6 -9 6 295.684 84.3670 42 -6 -9 6 557.884 89.7430 17 -6 -9 5 924.206 132.132 17 -6 -9 4 4286.30 295.476 17 6 9 -4 3276.02 269.637 15 -6 -9 3 4905.77 340.108 17 6 9 -3 4428.44 347.465 15 6 9 -2 1150.61 184.557 34 6 9 -2 1498.80 216.721 15 6 9 -2 1457.64 196.847 48 6 9 -1 176.211 140.861 34 6 9 -1 127.177 162.308 15 6 9 -1-72.6157 156.167 48 6 9 0 120.714 145.213 34 6 9 0 125.416 171.986 15 6 9 0 116.278 161.092 48 6 9 1 127.170 163.921 34 6 9 1 257.745 169.448 15 6 9 1 46.5178 302.784 7 6 9 1 256.951 172.369 48 6 9 2 171.312 166.350 34 6 9 2 147.291 265.908 7 6 9 2 177.819 175.292 48 -6 -9 -2 209.203 272.343 1 6 9 3 1272.95 233.772 48 6 9 3 1341.48 222.977 34 6 9 3 927.832 210.602 15 6 9 3 1421.35 451.691 7 -6 -9 -3 993.765 408.382 1 6 9 4 1903.69 259.555 15 6 9 4 1708.29 482.842 7 -6 -9 -4 1534.46 474.681 1 6 9 5 7147.91 494.723 34 6 9 5 5555.24 431.927 22 6 9 5 7191.86 496.248 15 -6 -9 -5 5837.67 822.659 1 6 9 5 7469.76 513.263 48 6 9 6 2012.63 266.893 34 6 9 6 2007.63 242.440 22 6 9 6 1885.56 258.010 15 6 9 6 2118.25 550.498 7 6 9 6 1937.05 282.136 48 -6 -9 -6 2074.63 518.746 1 6 9 7 15235.5 797.167 34 6 9 7 10581.1 755.476 15 6 9 7 12142.2 1322.39 7 6 9 7 15963.4 823.380 48 6 9 7 13544.3 770.185 22 -6 -9 -7 11508.3 1204.98 1 6 9 8 176.456 130.382 43 6 9 8 119.044 165.401 48 6 9 8 82.6140 141.610 34 6 9 8 282.537 161.072 22 6 9 9-71.4770 129.633 43 6 9 9 111.234 200.229 37 6 9 9 32.2092 137.857 48 6 9 9-97.8504 150.590 22 6 9 10 915.903 173.659 43 6 9 10 1256.78 205.795 22 6 9 10 696.228 235.753 37 6 9 11 113.039 164.950 46 6 9 11 26.1584 149.280 38 6 9 11-44.9873 181.171 37 6 9 11-34.6230 142.481 35 6 9 11 79.3741 145.726 22 6 9 12 863.937 180.819 46 6 9 12 1008.85 184.587 22 6 9 12 868.627 177.494 38 6 9 12 834.684 196.053 37 6 9 13 680.275 144.089 46 6 9 13 649.208 138.714 38 6 9 14 111.717 95.6970 30 -6 -10 4 2337.33 180.219 17 -6 -10 3 1642.62 163.511 17 6 10 -3 1441.72 172.582 15 -6 -10 2 2046.63 188.175 17 6 10 -2 1610.68 207.833 15 6 10 -2 1462.80 173.050 48 -6 -10 1 1352.37 163.498 17 6 10 -1 1293.42 204.988 15 6 10 -1 1172.10 183.863 48 6 10 0 2782.29 281.900 34 6 10 0 3095.69 302.893 15 6 10 0 2906.85 282.469 48 6 10 1 6317.65 457.031 34 6 10 1 6713.93 473.957 15 6 10 1 6173.49 455.309 48 6 10 2 1471.78 238.318 34 6 10 2 1888.75 253.687 48 6 10 3 706.369 201.744 34 6 10 3 554.714 190.243 15 6 10 3 807.389 207.035 48 6 10 4 648.373 192.669 15 6 10 4 844.774 219.113 48 6 10 5 2181.38 270.244 34 6 10 5 2265.35 264.411 15 6 10 6 11895.5 685.613 34 6 10 6 10509.1 665.039 15 6 10 6 9277.27 614.663 22 6 10 6 13562.7 719.142 48 6 10 7 3884.69 330.003 34 6 10 7 2678.87 293.158 15 6 10 7 4251.26 355.283 48 6 10 7 3237.01 297.654 22 6 10 8 3890.20 348.569 48 6 10 8 3391.66 311.160 22 6 10 9 1410.11 229.569 38 6 10 9 1430.36 251.876 37 6 10 9 953.379 204.177 48 6 10 9 1469.63 211.738 22 6 10 10 238.825 152.571 38 6 10 10 220.973 179.005 37 6 10 10 189.279 135.692 22 6 10 11 276.139 160.960 46 6 10 11 525.572 173.290 37 6 10 11 664.866 151.818 35 6 10 11 436.453 144.079 22 6 10 12 57.9901 114.766 46 6 10 12 21.8941 106.854 38 6 10 13 334.471 96.0668 46 6 11 -3 2041.93 179.115 24 6 11 -2 1698.08 173.603 15 6 11 -1 433.941 110.178 48 6 11 -1 397.413 134.344 15 6 11 0 738.235 158.538 15 6 11 0 566.095 141.151 48 6 11 1 7960.44 485.315 15 6 11 1 6522.07 455.106 48 6 11 2 3865.15 329.537 48 6 11 3 3176.77 295.608 15 6 11 3 2827.31 292.191 48 6 11 4 1033.84 198.408 15 6 11 4 1020.27 212.629 48 6 11 5 140.805 129.382 38 6 11 5 630.541 167.654 15 6 11 6 1518.77 216.015 38 6 11 6 1627.90 223.201 15 6 11 7 1167.19 193.757 38 6 11 7 1141.46 221.921 37 6 11 7 1566.09 222.410 48 6 11 8 3631.27 318.890 38 6 11 8 3100.33 328.580 37 6 11 8 4254.36 332.278 48 6 11 9 2538.02 257.401 38 6 11 9 2464.25 266.951 37 6 11 9 2359.80 238.795 48 6 11 10 657.527 145.454 38 6 11 10 631.449 153.309 37 6 11 10 304.716 146.727 35 6 11 11 255.508 108.044 38 6 11 11 154.298 98.1008 35 6 11 12 406.469 100.106 46 6 12 -1 691.310 100.453 15 6 12 0 1449.35 154.205 15 6 12 0 1087.95 142.278 24 6 12 1 335.581 111.534 15 6 12 1 100.882 94.9637 24 6 12 1 3.95534 95.7750 48 6 12 2 2603.94 216.658 24 6 12 2 2195.32 221.484 48 6 12 3 2336.98 226.871 15 6 12 3 2202.41 227.968 48 6 12 4 523.747 137.250 15 6 12 4 551.870 151.752 48 6 12 5-28.6719 106.366 37 6 12 5 149.925 108.482 15 6 12 6-26.4816 83.3324 38 6 12 6 37.6865 97.9428 37 6 12 7 81.2156 90.2647 38 6 12 7 52.1749 101.006 37 6 12 7 280.540 123.490 48 6 12 8 129.929 103.685 38 6 12 8 214.750 103.125 37 6 12 8 478.337 122.842 48 6 12 9 648.978 155.104 46 6 12 9 1012.68 136.518 38 6 12 9 834.556 119.665 37 6 12 9 1039.98 159.783 35 6 12 10 796.479 141.835 46 6 12 10 736.868 129.283 35 6 13 3 1538.74 132.341 15 6 13 3 948.052 120.796 48 6 13 4 698.924 97.0626 15 6 13 4 779.771 110.418 48 6 13 5 226.267 89.2399 48 7 -9 0 1989.33 145.683 6 7 -9 1 2016.99 154.312 21 7 -9 1 2850.49 171.879 6 7 -9 2 226.040 63.4631 21 7 -9 2 188.055 62.3355 6 7 -9 3 1238.06 109.324 21 -7 8 4 48.9601 58.8383 44 -7 8 3 487.594 99.9537 44 7 -8 -2 977.312 114.566 6 7 -8 -1 466.241 92.9492 21 -7 8 1 528.929 119.776 13 7 -8 0 232.341 95.9872 21 -7 8 0 147.483 94.0842 13 -7 8 -1 3839.82 253.578 39 -7 8 -1 3590.43 286.154 13 7 -8 2 217.356 110.506 21 -7 8 -2 172.209 90.0040 39 -7 8 -3 3480.91 236.453 39 7 -8 3 3290.46 248.815 21 -7 8 -4 2239.34 179.661 39 7 -8 4 2195.17 181.922 6 -7 8 -5 2012.53 169.224 39 7 -8 5 2064.52 169.639 21 7 -8 6 38.9244 61.7982 21 -7 7 6 4796.40 276.308 44 -7 7 5 1865.71 167.416 44 -7 7 4 1744.23 181.267 44 -7 7 4 2051.16 176.453 41 -7 7 3 2126.71 192.490 41 -7 7 3 2146.37 216.774 13 7 -7 -3 2257.87 178.483 6 7 -7 -2 810.652 118.980 21 -7 7 2 1054.61 146.338 41 7 -7 -1 366.326 116.060 21 -7 7 1 321.566 110.991 41 -7 7 1 330.491 108.631 39 -7 7 1 354.974 144.440 13 7 -7 0 695.285 150.287 21 -7 7 0 799.384 145.189 39 -7 7 0 713.090 161.742 13 -7 7 -1 2506.78 225.391 39 -7 7 -1 2193.05 242.586 13 7 -7 1 2648.60 237.347 21 -7 7 -2 5738.02 375.231 39 -7 7 -2 4905.83 391.989 13 -7 7 -3 13419.1 642.243 39 7 -7 3 9106.56 598.537 14 -7 7 -3 9673.26 632.022 13 -7 7 -3 13276.5 650.455 24 7 -7 3 13561.1 656.281 21 -7 7 -4 7720.40 416.990 39 7 -7 4 6461.15 390.572 14 7 -7 5 4966.65 348.926 14 7 -7 5 6054.02 371.456 21 7 -7 6 2425.83 209.323 14 7 -7 6 2531.03 217.520 21 7 -7 7 663.086 109.361 21 -7 7 -7 465.649 117.198 39 -7 7 -8 6.66029 75.2994 39 -7 6 7 1364.51 129.651 44 -7 6 6 9236.00 496.247 44 -7 6 5 12924.4 676.559 44 -7 6 4 14478.8 732.499 44 -7 6 4 14617.0 731.185 41 -7 6 3 915.449 160.207 41 7 -6 -3 803.825 134.889 6 -7 6 3 602.675 128.046 39 -7 6 3 722.167 164.511 13 -7 6 2 5107.44 351.725 41 -7 6 2 4943.10 339.140 39 7 -6 -2 4695.18 313.293 21 7 -6 -1 153.095 122.334 21 -7 6 1-18.7692 124.470 41 -7 6 1 26.4385 129.588 39 7 -6 0 140.689 135.893 21 -7 6 0 145.074 114.784 41 -7 6 0-21.0832 127.831 39 7 -6 1 22.9002 146.108 21 -7 6 -1-22.0678 131.746 39 -7 6 -1 58.2917 143.747 24 7 -6 2-7.99230 141.350 21 -7 6 -2 166.375 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951.702 383.087 3 -7 -7 -8 1192.89 436.018 1 7 7 8 821.101 407.089 7 7 7 8 1101.71 211.955 48 7 7 9 6751.50 466.669 43 7 7 9 6383.54 437.791 34 7 7 9 6511.38 467.988 6 7 7 9 5538.17 762.883 3 7 7 10 791.999 195.570 43 7 7 10 839.864 242.254 37 7 7 10 973.463 223.491 22 7 7 11 298.472 162.660 46 7 7 11 240.809 164.722 43 7 7 11 330.748 204.703 37 7 7 12 2971.47 285.191 43 7 7 12 2183.35 232.888 19 7 7 12 3345.86 326.938 37 7 7 12 1754.76 243.338 46 7 7 13 7900.95 465.166 43 7 7 13 7450.31 461.968 22 7 7 14 1157.17 166.996 43 7 7 14 906.758 153.588 32 7 7 14 878.375 150.786 22 7 7 15 129.524 78.0471 32 7 7 15 197.283 74.4171 30 -7 -8 6 1053.79 123.296 42 -7 -8 5 881.533 137.474 17 7 8 -4 1327.46 171.820 15 7 8 -3 5263.21 365.577 15 7 8 -3 4201.32 332.437 48 7 8 -2 5809.71 417.642 34 7 8 -2 6624.07 435.600 48 -7 -8 1 1357.65 192.942 5 7 8 -1 1519.87 209.228 34 7 8 -1 1392.15 220.200 48 7 8 0 208.017 160.782 34 7 8 0 359.624 179.974 48 -7 -8 -1 10626.3 1246.03 1 7 8 1 12029.0 1297.99 7 7 8 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337.893 3 7 8 8 768.161 188.926 34 7 8 8 1369.51 450.309 7 7 8 8 1050.98 217.104 48 7 8 8 977.450 207.933 22 7 8 9 535.535 156.866 43 7 8 9 345.288 137.880 34 7 8 9 456.662 166.401 48 7 8 9 858.229 189.897 22 7 8 10 2912.28 290.165 43 7 8 10 3545.95 328.507 22 7 8 11 124.035 157.035 46 7 8 11 141.584 141.552 43 7 8 11 263.497 169.238 22 7 8 12 789.946 176.300 46 7 8 12 1087.94 184.036 43 7 8 12 1113.01 197.991 38 7 8 12 841.370 148.541 32 7 8 13 266.852 129.157 43 7 8 13 100.107 107.558 38 7 8 13 279.643 102.713 32 7 8 13-78.8404 131.720 22 7 8 14 508.563 90.9095 32 7 8 14 458.103 116.294 22 -7 -9 5 1023.77 115.338 17 -7 -9 4-4.21149 85.3191 17 7 9 -4 50.1993 67.6269 15 -7 -9 3 6584.43 380.937 17 7 9 -3 5202.10 373.712 15 7 9 -2 4528.21 335.882 15 7 9 -2 3679.20 300.107 48 7 9 -1 6859.40 471.901 34 7 9 -1 6841.08 472.607 48 7 9 0 140.833 141.433 34 7 9 0-105.701 160.932 15 7 9 0 32.8407 151.821 48 7 9 1 188.069 163.770 48 7 9 1 54.4732 154.287 34 7 9 1 259.953 171.000 15 7 9 2-122.795 163.524 48 7 9 2-19.1289 159.623 34 7 9 3 2577.16 295.326 34 7 9 3 2379.66 284.512 15 7 9 3 2552.57 295.956 48 7 9 4 2617.11 292.226 15 7 9 5 10160.9 655.317 34 7 9 5 9903.91 648.687 15 7 9 6 6168.69 442.861 34 7 9 6 5365.57 428.632 15 7 9 6 6562.83 460.427 48 7 9 6 4832.33 392.497 22 7 9 7 3464.54 314.097 34 7 9 7 2348.71 277.265 15 7 9 7 3215.20 326.904 48 7 9 7 2802.68 282.988 22 7 9 8 2272.81 255.214 34 7 9 8 2182.84 254.533 22 7 9 8 1699.68 252.679 48 7 9 9 491.250 139.292 43 7 9 9 397.842 136.355 34 7 9 9 333.366 153.798 48 7 9 9 351.327 165.118 22 7 9 10-49.4563 119.402 43 7 9 10 156.074 199.560 37 7 9 10 173.503 137.639 22 7 9 11 127.610 151.848 46 7 9 11 140.328 121.577 43 7 9 11 137.413 148.137 38 7 9 11 110.224 178.844 37 7 9 11 93.8828 143.457 22 7 9 12 2099.68 242.098 38 7 9 12 2615.31 239.625 22 7 9 13 240.634 104.137 38 -7 -10 3 480.161 87.9330 17 7 10 -3 236.409 84.5052 15 -7 -10 2 1464.64 145.016 17 7 10 -2 1206.24 171.117 15 -7 -10 1 4710.03 308.741 17 7 10 -1 3947.38 325.196 48 7 10 0 1418.59 193.479 34 7 10 0 1659.47 214.994 15 7 10 0 1398.44 200.391 48 7 10 1 2154.38 250.137 34 7 10 1 2532.80 271.004 15 7 10 1 2099.48 251.623 48 7 10 2 3053.21 300.464 34 7 10 2 3210.59 312.096 48 7 10 3 2620.87 288.007 34 7 10 3 2424.10 286.767 15 7 10 3 2793.10 307.104 48 7 10 4 8.59825 144.726 15 7 10 5 712.720 185.186 34 7 10 5 558.595 174.128 15 7 10 6 9404.86 581.386 34 7 10 6 8066.92 558.915 15 7 10 6 10039.8 604.825 48 7 10 7 10906.8 617.055 34 7 10 7 11425.5 637.219 48 7 10 8 1420.07 208.645 48 7 10 8 1171.73 187.171 22 7 10 9 43.5938 180.139 37 7 10 9 188.327 128.499 48 7 10 9 52.1384 129.986 22 7 10 10 957.728 184.066 38 7 10 10 958.226 207.808 37 7 10 10 766.337 159.028 22 7 10 11 41.8938 120.024 46 7 10 11-135.623 153.512 37 7 10 11 98.9723 108.470 22 7 10 12 391.444 127.880 46 7 10 12 630.436 137.832 38 7 10 12 603.869 148.332 37 7 11 -1 2755.47 225.100 15 7 11 0 2081.91 197.079 15 7 11 0 1120.34 169.447 48 7 11 1 1164.25 184.609 15 7 11 1 1174.41 171.769 48 7 11 2 2423.78 246.927 48 7 11 3 1090.09 181.120 34 7 11 3 903.392 182.121 15 7 11 3 1154.37 190.339 48 7 11 4 1435.98 210.757 15 7 11 4 2007.02 232.155 48 7 11 5 129.912 104.094 38 7 11 5 29.8593 130.279 34 7 11 5-26.3689 129.794 15 7 11 6 918.672 174.979 38 7 11 6 1060.14 180.574 15 7 11 7 5106.33 399.378 38 7 11 7 6968.34 438.209 48 7 11 8 959.756 173.101 38 7 11 8 968.893 206.935 37 7 11 8 1299.72 185.679 48 7 11 9 523.155 145.828 38 7 11 9 674.385 173.866 37 7 11 10 290.722 138.219 46 7 11 10 402.957 125.839 38 7 11 10 486.441 139.572 37 7 11 10 231.370 117.077 35 7 11 11 179.725 102.643 46 7 11 11 361.385 103.642 38 7 11 11 289.660 109.755 37 7 12 1 2534.40 187.483 15 7 12 1 2172.09 171.856 24 7 12 2 114.518 76.4610 24 7 12 2 46.2548 84.8447 48 7 12 3 340.802 106.534 15 7 12 3 167.702 108.073 48 7 12 4 567.682 126.887 15 7 12 4 854.987 148.297 48 7 12 5 345.645 116.293 37 7 12 5 606.330 116.399 15 7 12 6-27.8884 98.9753 37 7 12 6-15.3736 107.053 48 7 12 7 22.8074 77.2464 38 7 12 7 130.424 98.4031 37 7 12 7-13.8821 103.306 48 7 12 8 650.987 117.967 38 7 12 8 567.554 121.868 37 7 12 9 215.812 78.9814 38 7 12 9 5.44193 78.4472 37 7 12 9-49.8269 85.0775 35 8 -8 0 2888.16 175.746 6 8 -8 1 1596.11 126.823 6 8 -8 2 1953.75 140.274 21 8 -8 3 218.575 65.6413 21 8 -8 3 471.929 69.9056 6 -8 7 3 32.9948 56.3931 44 -8 7 2 1732.80 165.392 44 8 -7 -2 2557.27 156.361 6 8 -7 -1 157.527 78.2470 6 8 -7 0 63.8228 75.0145 21 8 -7 0 17.6048 85.3709 6 -8 7 0 23.7007 80.7264 39 -8 7 0 28.8344 86.1454 13 8 -7 1 276.745 98.0369 21 8 -7 1 259.603 96.7815 6 -8 7 -1 247.249 89.3474 39 -8 7 -1 163.851 101.552 13 8 -7 2-12.8615 93.6418 21 -8 7 -2 32.8179 88.9885 39 -8 7 -2-44.9316 89.8000 13 -8 7 -3 2120.86 187.267 39 8 -7 3 2366.03 196.188 21 8 -7 3 2318.63 196.603 6 -8 7 -4 7099.48 402.640 39 8 -7 4 7215.96 407.173 21 8 -7 4 7312.81 407.826 6 8 -7 5 8130.36 427.546 6 8 -7 6 4899.95 286.044 21 -8 7 -7 2331.60 160.529 39 -8 6 5 1133.75 112.887 44 -8 6 4 6172.67 359.854 44 -8 6 4 6623.76 345.171 23 -8 6 3 8138.23 449.619 44 -8 6 2 1776.46 163.509 39 -8 6 2 2031.59 206.502 13 8 -6 -2 2010.76 171.533 6 8 -6 -1 574.436 122.888 6 -8 6 1 544.379 118.866 39 8 -6 0 804.885 130.626 21 8 -6 0 844.281 147.308 6 -8 6 0 868.829 148.385 39 8 -6 1-21.8614 109.611 21 -8 6 -1 92.2112 113.459 39 8 -6 2 41.6930 119.697 21 -8 6 -2 23.8282 114.282 39 8 -6 3 1431.87 188.942 21 8 -6 4 5235.06 354.214 21 8 -6 4 5171.84 349.585 6 -8 6 -5 10415.0 562.441 39 8 -6 5 9795.49 555.470 6 -8 6 -6 9104.08 477.031 39 8 -6 6 7652.09 470.795 14 8 -6 6 7720.43 453.149 6 8 -6 6 8662.66 476.478 21 -8 6 -7 9686.36 494.287 39 8 -6 7 8082.50 492.745 14 8 -6 7 9038.49 487.191 21 8 -6 8 3215.85 225.330 45 -8 6 -8 4204.69 249.812 39 -8 6 -9 388.760 70.4014 39 -8 5 6 7.74179 55.9806 44 -8 5 5-19.1291 78.7237 44 -8 5 5 61.8800 73.4443 23 -8 5 4 4205.99 285.568 44 -8 5 3 6521.67 396.992 44 -8 5 3 6606.89 386.116 39 -8 5 3 6153.89 416.848 13 8 -5 -3 6533.08 367.982 6 -8 5 2 7025.74 433.722 39 8 -5 -2 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736.101 156.819 6 -8 4 1 551.667 161.816 39 -8 4 0 5980.36 404.702 41 8 -4 0 6122.01 408.526 21 8 -4 1 2667.39 258.804 21 8 -4 2 7911.66 497.978 21 8 -4 3 895.717 190.117 21 -8 4 -3 1126.50 197.049 39 -8 4 -4 8977.91 559.282 39 8 -4 4 9395.58 570.365 21 8 -4 5 874.487 192.786 21 8 -4 5 1129.13 187.069 6 -8 4 -5 822.355 181.506 39 8 -4 6 748.359 155.170 6 -8 4 -6 764.804 171.974 39 8 -4 7 1316.29 179.692 6 -8 4 -7 1864.53 215.167 39 8 -4 7 1805.67 218.962 21 -8 4 -8 3058.49 260.539 39 8 -4 8 3090.09 265.059 21 8 -4 9 8289.50 475.609 45 -8 4 -9 7994.94 463.538 39 8 -4 9 7742.91 488.984 47 -8 4 -10 5156.50 329.034 39 8 -4 10 5606.04 362.104 14 8 -4 11 4588.20 268.452 45 8 -4 11 3332.63 266.825 19 -8 3 7 3253.18 227.960 44 -8 3 6 5105.19 324.090 44 -8 3 6 5186.37 322.515 23 -8 3 5 2632.91 236.990 44 -8 3 5 2905.78 236.642 39 -8 3 5 3029.40 246.545 23 -8 3 4 2023.45 212.143 44 -8 3 4 2296.32 228.153 39 -8 3 3 1433.74 191.022 44 -8 3 3 1611.47 210.261 39 8 -3 -3 1542.19 173.944 6 8 -3 -2 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1543.63 190.729 47 8 -3 12 2977.72 209.440 45 8 -3 12 2509.15 213.673 19 -8 2 7 7315.53 408.602 44 -8 2 7 8186.46 406.997 23 -8 2 6 10826.3 598.927 44 -8 2 6 10296.4 593.947 16 -8 2 5 9485.35 538.809 39 -8 2 5 10273.6 548.599 23 -8 2 4 3062.49 266.319 44 -8 2 4 3350.47 290.060 39 -8 2 3 8546.85 538.713 44 -8 2 3 10167.6 572.038 39 -8 2 2 1979.43 214.594 44 -8 2 2 2170.51 251.275 39 8 -2 -2 2040.47 218.728 6 -8 2 1 1366.87 439.545 2 8 -2 -1 1870.62 224.191 6 8 -2 0 3245.83 284.684 21 8 -2 0 4129.13 327.223 6 -8 2 0 3128.64 629.261 2 8 -2 1 644.213 162.199 21 8 -2 1 534.387 167.754 6 -8 2 -1 578.497 177.829 39 -8 2 -1 544.094 138.723 26 -8 2 -1 561.634 414.525 2 -8 2 -2 17177.9 892.669 39 8 -2 2 16050.4 879.757 21 8 -2 2 16423.7 897.337 6 -8 2 -3 10438.4 622.094 39 -8 2 -3 11673.9 1139.83 2 8 -2 3 10905.3 626.423 21 8 -2 3 9983.23 626.862 6 -8 2 -4 25890.5 1335.63 39 -8 2 -4 26917.2 1954.31 2 8 -2 4 27845.1 1355.94 21 8 -2 4 27093.1 1356.07 6 -8 2 -5 7104.20 466.918 39 -8 2 -5 7810.41 920.795 2 8 -2 5 7651.71 490.450 21 8 -2 5 6520.84 470.924 6 -8 2 -6 5276.87 381.733 39 8 -2 6 5374.50 394.901 6 -8 2 -6 4159.95 690.636 2 -8 2 -7 1470.27 399.727 2 -8 2 -7 1540.07 204.738 39 8 -2 7 1765.72 214.781 6 8 -2 7 1901.51 239.636 21 -8 2 -8 3781.24 302.257 39 8 -2 8 3604.28 297.045 6 8 -2 8 4235.74 339.187 21 8 -2 9 270.497 142.776 45 -8 2 -9 296.364 128.841 39 8 -2 10 108.595 137.179 45 -8 2 -10 126.293 108.255 39 8 -2 10 301.037 189.664 47 8 -2 11 114.613 122.776 45 8 -2 11 131.561 112.508 14 8 -2 11 56.0403 158.331 47 8 -2 12 3744.57 256.927 45 8 -2 12 2857.96 252.242 19 8 -2 12 2836.62 265.154 47 8 -2 12 3037.55 254.286 31 8 -2 13 1109.58 126.622 19 8 -2 13 685.259 101.636 31 -8 1 8-21.0389 56.3729 29 -8 1 7 427.255 102.445 44 -8 1 7 385.724 103.403 16 -8 1 7 436.105 116.895 23 -8 1 6 2938.75 248.147 44 -8 1 6 2534.25 241.710 18 -8 1 6 3621.04 266.844 16 -8 1 6 3695.44 275.515 23 -8 1 5 7153.63 469.288 44 -8 1 5 8263.44 501.118 39 -8 1 5 8537.48 502.476 23 -8 1 4 13552.2 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1 -7 7183.96 890.365 2 8 -1 7 8488.66 502.984 6 8 -1 8 697.746 186.548 21 8 -1 8 393.001 147.421 45 8 -1 8 372.948 132.106 6 -8 1 -8 405.039 135.078 39 -8 1 -9 9667.99 572.090 39 8 -1 9 9689.97 569.341 6 8 -1 10 10403.5 612.667 45 8 -1 11 1244.50 189.484 45 8 -1 11 1455.36 253.212 47 8 -1 12 274.867 123.714 45 8 -1 12 345.532 130.665 19 8 -1 12 156.397 130.060 31 8 -1 12 181.383 174.635 47 8 -1 13 1678.38 169.777 45 8 -1 13 1559.50 169.870 19 8 -1 13 1159.58 166.308 31 8 -1 13 1536.26 196.679 47 8 -1 14 73.3585 65.6792 19 -8 0 8 1896.37 152.351 16 -8 0 8 1798.93 168.036 29 -8 0 7 327.466 96.0140 44 -8 0 7 365.864 104.319 18 -8 0 7 309.856 110.639 16 -8 0 6 444.376 119.323 44 -8 0 6 254.295 121.895 18 -8 0 6 509.056 136.876 16 -8 0 6 312.468 140.504 23 -8 0 5 12.6532 115.869 44 -8 0 4 47.6339 108.827 44 -8 0 4 73.8780 158.872 23 -8 0 3 1064.61 160.082 44 -8 0 3 938.800 390.308 8 -8 0 3 346.475 324.808 11 -8 0 2 36040.4 1824.98 44 -8 0 2 47435.3 1909.64 39 -8 0 2 33849.8 2444.92 8 -8 0 2 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483.562 26 8 8 4 6837.77 508.027 6 8 8 4 7990.43 522.154 48 8 8 5 474.115 193.279 6 -8 -8 -5 555.682 158.971 26 8 8 5 606.270 197.119 48 8 8 6 2146.64 263.695 15 -8 -8 -6 2353.73 249.019 26 8 8 6 2432.41 295.005 6 8 8 6 2687.69 295.350 48 8 8 6 1965.55 245.469 22 8 8 7 809.061 169.282 15 -8 -8 -7 772.111 161.356 26 8 8 7 917.966 203.288 48 8 8 7 989.085 189.916 22 8 8 7 572.490 190.682 6 8 8 8 845.463 162.307 43 8 8 8 938.041 180.366 34 8 8 8 945.456 201.938 48 8 8 8 1072.29 199.085 22 8 8 8 895.416 198.625 6 8 8 9 1855.01 221.037 43 -8 -8 -9 1395.09 225.113 5 8 8 9 1709.63 214.901 34 8 8 9 2147.06 259.531 22 8 8 10 5052.77 433.512 37 8 8 10 4907.86 375.356 22 8 8 11 860.224 163.592 43 8 8 11 892.682 222.716 37 8 8 11 1009.50 186.613 22 8 8 12 1191.29 169.239 43 8 8 12 822.286 181.158 38 8 8 12 1114.24 217.872 37 8 8 12 1327.83 188.086 22 8 8 13 2627.88 223.821 43 8 8 14 218.095 83.8981 22 -8 -9 3 937.582 121.010 17 8 9 -3 667.805 109.472 15 8 9 -2 1587.21 184.540 15 8 9 -2 1330.41 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99.7845 45 -9 4 -9 618.702 97.7761 39 9 -4 10 349.412 74.7918 45 -9 3 5 3681.53 249.022 44 -9 3 5 6322.43 292.235 23 -9 3 4 2437.59 188.653 39 -9 3 4 2448.12 197.454 23 -9 3 3 4109.62 294.797 44 -9 3 3 5856.38 338.166 39 -9 3 2 695.247 123.365 44 9 -3 -2 956.983 133.535 6 -9 3 2 992.826 165.181 39 -9 3 1 175.247 99.3848 44 9 -3 -1 305.529 118.860 6 -9 3 1 439.333 143.098 39 9 -3 0 6224.41 411.237 6 9 -3 1-5.88119 111.057 21 9 -3 1 7.76691 124.970 6 -9 3 -2 11035.8 631.319 39 9 -3 2 10381.2 609.011 21 9 -3 2 11191.2 638.446 6 -9 3 -3 9490.61 526.473 39 9 -3 3 8679.38 510.270 21 9 -3 3 9015.56 528.651 6 -9 3 -4 8618.44 541.132 39 9 -3 4 9661.70 558.772 21 -9 3 -5 13998.5 779.473 39 9 -3 5 14696.5 797.926 6 9 -3 5 15164.6 800.125 21 -9 3 -6 9274.62 562.957 39 9 -3 6 9921.23 573.861 6 9 -3 6 10395.6 590.112 21 9 -3 7 556.877 123.291 45 9 -3 7 643.228 139.081 6 -9 3 -7 658.092 147.886 39 9 -3 8 55.6433 92.9269 45 -9 3 -8 101.811 106.638 39 9 -3 9 301.897 105.421 45 -9 3 -9 371.823 103.062 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1 -2 491.554 159.780 26 -9 1 -2 578.286 359.588 2 9 -1 3 333.997 156.855 21 9 -1 3 297.046 151.111 6 -9 1 -3 244.677 150.569 39 -9 1 -3 225.241 142.748 26 -9 1 -4 2445.00 258.672 39 -9 1 -4 2284.83 576.068 2 9 -1 4 2713.83 272.406 21 -9 1 -5 2485.04 253.648 39 9 -1 5 2891.32 276.537 6 9 -1 5 2953.73 287.332 21 -9 1 -5 2185.45 520.928 2 -9 1 -6 2352.99 240.205 39 9 -1 6 2463.42 254.053 6 9 -1 6 2582.96 273.550 21 9 -1 7 8302.36 507.315 45 -9 1 -7 8087.90 515.299 39 9 -1 8 16169.3 836.127 45 -9 1 -8 14820.7 818.587 39 9 -1 8 17294.6 850.826 6 9 -1 9 1229.61 179.532 45 9 -1 10 5719.37 353.242 45 9 -1 10 4130.88 322.011 19 9 -1 11 3030.70 232.974 45 9 -1 11 2101.65 205.602 19 9 -1 12 87.0508 85.5561 45 9 -1 12 59.9483 79.4857 19 9 -1 12 53.5800 130.512 47 9 -1 13 107.334 73.2656 31 9 -1 13 199.698 93.5627 47 -9 0 6 151.643 74.0804 18 -9 0 6 291.418 92.8810 16 -9 0 5 408.064 116.541 18 -9 0 4 346.698 145.275 23 9 0 -3 768.461 134.429 33 -9 0 3 1254.31 189.184 23 9 0 -2 231.979 116.334 6 -9 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1 8 102.374 114.602 33 9 1 9 10476.0 599.570 45 9 1 9 10129.3 587.235 6 9 1 10 12404.6 705.766 45 9 1 10 13843.1 816.855 47 9 1 11 4735.90 329.891 45 9 1 11 5369.11 427.520 47 9 1 12 3989.04 281.589 45 9 1 12 3666.21 316.435 31 9 1 12 4390.60 352.199 47 9 1 13 594.901 105.522 19 9 1 13 822.176 148.972 31 -9 -1 -13 567.773 114.512 26 9 1 13 934.663 171.931 47 9 1 14 169.283 104.177 47 -9 -2 6 3548.71 242.664 16 -9 -2 6 2904.51 242.852 29 -9 -2 5 2312.81 217.802 16 -9 -2 4 8784.76 517.431 16 -9 -2 4 8452.63 517.866 23 -9 -2 3 4352.99 339.580 23 -9 -2 2 1203.05 204.026 39 9 2 -2 1182.95 178.806 33 -9 -2 2 912.287 151.134 26 -9 -2 2 1189.38 192.242 23 -9 -2 1 3005.47 290.432 39 9 2 -1 3151.51 287.354 33 -9 -2 1 2642.69 254.419 26 9 2 -1 2819.13 254.651 6 -9 -2 1 3282.49 290.226 23 9 2 0 622.216 162.332 6 -9 -2 0 1075.94 190.518 39 9 2 0 865.745 181.696 33 -9 -2 0 775.458 171.803 26 -9 -2 -1 28367.8 1461.69 39 -9 -2 -1 32798.0 1517.01 5 -9 -2 -1 31067.8 1476.44 26 9 2 1 27872.5 1461.66 6 -9 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348.415 6 -9 -5 -9 4436.94 376.021 5 9 5 9 3960.64 333.799 31 -9 -5 -9 5177.71 372.856 26 9 5 9 5285.17 381.811 6 9 5 9 3779.18 361.686 47 9 5 10 1206.60 197.271 6 9 5 10 1259.03 230.669 37 9 5 10 1795.44 210.742 31 -9 -5 -10 1786.58 214.624 26 9 5 10 1659.53 224.918 47 9 5 11 1056.25 187.805 31 -9 -5 -11 1343.26 173.774 26 9 5 11 1337.27 206.054 47 9 5 12 1017.67 163.027 31 9 5 12 935.559 169.877 47 9 5 13 884.836 166.439 43 9 5 13 710.526 157.801 22 9 5 14 107.116 85.9716 22 -9 -6 5 750.114 97.0807 17 -9 -6 4 985.762 128.584 18 -9 -6 4 1145.82 114.458 16 9 6 -4 1211.70 118.558 48 -9 -6 3-30.5197 89.2355 18 -9 -6 3-45.7658 84.2949 16 9 6 -3 39.6550 100.012 48 -9 -6 2 633.126 118.650 16 9 6 -2 607.555 156.051 48 -9 -6 0 6758.58 482.453 5 9 6 0 6873.36 483.423 6 9 6 1 738.574 176.286 6 -9 -6 -1 1042.78 193.316 5 -9 -6 -2 3606.02 327.234 5 9 6 2 3471.51 329.590 33 9 6 2 3606.08 321.360 6 -9 -6 -3 2337.23 282.195 5 9 6 3 2006.88 505.190 3 9 6 3 2309.45 273.160 33 -9 -6 -3 2679.93 282.833 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96.9879 32 9 6 14 571.884 115.052 22 -9 -7 4 776.291 110.834 17 9 7 -3 1261.99 141.844 48 -9 -7 2 1097.61 127.787 18 9 7 -2 1303.03 168.305 48 -9 -7 1 101.378 88.1148 18 9 7 -1 87.7825 110.866 34 9 7 -1 160.458 132.252 48 -9 -7 0 1653.47 216.015 5 9 7 0 2028.05 229.689 6 -9 -7 -1 5030.13 385.698 5 9 7 1 5047.00 393.193 6 9 7 1 5944.50 413.372 48 -9 -7 -2 1937.76 244.201 5 -9 -7 -2 2217.62 253.086 26 9 7 2 2086.49 251.175 6 9 7 3 1481.23 228.830 6 -9 -7 -3 1332.05 231.694 5 -9 -7 -3 1703.78 230.711 26 -9 -7 -4 28560.6 1458.71 26 9 7 4 30519.6 1490.23 6 9 7 4 29698.1 1485.95 48 -9 -7 -5 2070.94 273.018 5 -9 -7 -5 2272.48 258.309 26 9 7 5 2368.04 276.518 6 9 7 5 2086.38 270.713 48 -9 -7 -6 564.421 190.854 5 -9 -7 -6 659.308 175.813 26 9 7 6 753.473 191.171 48 -9 -7 -7 2382.85 282.917 5 -9 -7 -7 2415.86 262.580 26 9 7 7 3113.32 300.316 6 9 7 7 2221.60 274.792 48 9 7 8 1639.70 231.805 6 9 7 8 1255.21 187.620 43 -9 -7 -8 1694.15 233.049 5 -9 -7 -8 1436.79 201.178 26 9 7 8 1317.99 207.319 48 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2595.11 285.698 6 9 8 5 2806.93 288.028 48 -9 -8 -6 1438.24 219.859 5 9 8 6 1006.41 185.640 15 -9 -8 -6 1227.06 183.809 26 9 8 6 1431.37 217.821 48 9 8 6 755.921 166.048 22 9 8 7 843.677 195.196 6 -9 -8 -7 914.125 182.804 5 -9 -8 -7 553.062 141.824 26 9 8 7 807.882 182.061 48 9 8 7 626.859 160.353 22 -9 -8 -8 1232.15 209.051 5 9 8 8 1768.74 212.887 34 -9 -8 -8 1178.44 167.645 26 9 8 8 1356.13 204.166 48 9 8 8 1316.31 199.441 22 9 8 8 1490.24 220.607 6 -9 -8 -9 643.489 153.553 5 9 8 9 643.677 168.243 22 9 8 10 391.041 121.798 43 9 8 10 560.316 198.773 37 -9 -8 -10 333.083 129.365 5 9 8 10 677.578 162.678 22 9 8 11 445.655 124.558 43 9 8 11 498.609 174.388 37 9 8 11 694.610 153.089 22 9 8 12 651.812 121.611 43 9 8 12 520.751 144.165 37 9 8 12 972.411 149.541 22 9 8 13 515.087 106.136 43 -9 -9 2 52.3509 62.2284 17 9 9 -2 31.3393 60.4731 15 9 9 -1 2608.39 217.907 15 9 9 -1 2215.46 196.377 48 9 9 0 2719.01 229.199 15 9 9 0 2222.03 216.606 48 9 9 1 830.549 151.815 34 -9 -9 -1 727.608 130.105 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12235.1 674.466 39 10 -3 5 13639.1 691.810 6 -10 3 -6 7742.43 463.037 39 -10 3 -6 8077.80 456.013 26 10 -3 6 9115.78 480.350 6 -10 3 -7 2145.72 192.104 39 10 -3 7 2589.71 199.018 6 -10 3 -8-42.2924 75.0246 39 10 -3 8-162.636 128.255 47 10 -3 9 59.3306 98.5668 47 10 -3 10 58.2690 61.3779 31 -10 3 -10-57.8380 59.0807 26 -10 2 4 9051.28 449.758 16 10 -2 -2 136.215 76.6961 33 -10 2 2 144.731 101.984 23 10 -2 -1 505.200 101.631 6 10 -2 0-5.34310 99.7581 6 -10 2 0 120.698 120.059 39 10 -2 1 81.2697 113.993 6 -10 2 -1 83.7198 130.500 39 10 -2 2 751.538 155.155 6 -10 2 -2 775.970 164.022 39 10 -2 3 1169.03 181.172 6 -10 2 -3 1238.78 177.928 39 -10 2 -4 3391.93 274.736 39 -10 2 -4 3169.49 256.729 26 -10 2 -5 14122.1 773.816 39 -10 2 -5 14663.3 772.720 26 10 -2 5 16045.7 801.057 6 -10 2 -6 14453.5 789.006 39 10 -2 6 16682.9 817.868 6 -10 2 -7 5076.41 340.302 39 10 -2 7 5919.37 362.184 6 -10 2 -8 3283.95 235.384 39 10 -2 9 404.766 81.9701 45 10 -2 9 344.875 149.513 47 10 -2 10 608.452 85.8841 45 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16.9083 96.7782 6 10 1 10 8110.96 557.492 47 10 1 11 1811.80 216.657 31 10 1 11 2120.84 257.160 47 10 1 12 2121.21 207.862 31 -10 -1 -12 2148.99 187.842 26 10 1 12 2152.20 229.359 47 10 1 13 225.769 79.9783 43 10 1 13 274.196 87.0209 31 -10 -2 5 4309.53 265.221 18 -10 -2 5 4861.44 266.041 16 -10 -2 4 1694.77 167.405 16 -10 -2 3 619.655 130.125 16 -10 -2 3 581.289 133.726 23 10 2 -2 1487.47 175.130 33 -10 -2 2 2301.00 208.328 23 10 2 -1 5.08722 97.1554 6 -10 -2 1 6.96050 126.858 39 10 2 -1 84.5320 106.736 33 -10 -2 1-144.718 123.343 23 -10 -2 0 1472.76 197.974 39 10 2 0 1559.50 201.986 33 -10 -2 0 1000.94 167.986 26 10 2 0 1432.40 181.211 6 -10 -2 0 1470.87 192.511 23 -10 -2 -1 1781.39 222.117 39 10 2 1 1858.78 236.307 33 -10 -2 -1 1902.01 220.608 26 10 2 1 2075.85 222.623 6 -10 -2 -1 1851.71 210.937 23 10 2 2 326.987 145.296 6 -10 -2 -2 301.900 141.878 39 10 2 2 369.926 151.240 33 -10 -2 -2 257.981 156.728 26 -10 -2 -3 4864.24 368.359 39 10 2 3 5559.37 424.340 33 -10 -2 -3 5663.17 409.313 26 10 2 3 5752.40 401.649 6 -10 -2 -4 7049.32 450.684 26 10 2 4 6499.66 439.257 6 -10 -2 -5 295.088 117.783 39 10 2 5 245.198 150.039 33 -10 -2 -5 140.394 161.833 26 10 2 6 7896.33 539.107 33 10 2 6 9116.10 545.129 6 10 2 7 2915.79 284.998 33 -10 -2 -7 3352.33 311.982 26 10 2 7 3194.34 288.045 6 10 2 8 1277.35 191.882 6 10 2 8 1047.67 176.353 33 -10 -2 -8 1160.06 214.598 26 10 2 9 216.699 117.232 6 -10 -2 -9 369.109 166.290 26 -10 -2 -10 84.1720 135.522 26 10 2 10 137.021 178.363 47 10 2 11 1178.46 185.395 31 -10 -2 -11 1437.49 180.336 26 10 2 11 1227.90 220.094 47 10 2 12 150.361 107.219 31 -10 -2 -12 35.0245 98.7069 26 10 2 12-44.7662 134.111 47 10 2 13 759.963 125.884 31 -10 -2 -13 743.632 92.4408 26 10 2 13 892.914 145.709 47 -10 -3 5 2123.93 166.977 18 -10 -3 4 4327.58 300.609 18 -10 -3 4 4595.90 288.251 16 -10 -3 3 750.131 131.685 16 -10 -3 2 3739.83 274.667 16 -10 -3 2 3561.52 272.784 23 10 3 -1 911.255 146.098 6 10 3 -1 1264.63 172.090 33 -10 -3 1 1127.57 174.706 23 10 3 0 514.340 138.073 6 -10 -3 0 646.175 160.944 39 10 3 0 614.470 153.731 33 -10 -3 0 692.752 152.093 26 -10 -3 0 537.548 146.435 23 -10 -3 -1 1489.53 207.917 39 10 3 1 1746.19 227.477 33 -10 -3 -1 1631.67 216.315 26 10 3 1 1586.43 203.905 6 -10 -3 -1 1584.54 195.117 23 -10 -3 -2 4779.54 374.128 39 -10 -3 -2 6397.50 435.723 5 10 3 2 6169.26 434.879 33 -10 -3 -2 5773.03 411.604 26 10 3 2 5924.57 403.163 6 -10 -3 -2 4663.30 351.020 23 10 3 3 1347.85 204.566 6 -10 -3 -3 992.238 167.664 39 10 3 3 1514.59 223.013 33 -10 -3 -3 1529.71 240.025 5 -10 -3 -3 1179.84 211.057 26 10 3 4 763.442 179.373 6 -10 -3 -4 430.325 127.499 39 -10 -3 -4 1053.49 206.761 26 -10 -3 -5 6487.06 470.994 5 10 3 5 5738.60 443.981 33 -10 -3 -6 5899.96 446.965 5 10 3 6 5380.58 422.941 33 -10 -3 -6 5920.03 434.365 26 10 3 6 5944.36 418.429 6 -10 -3 -7 10306.0 661.118 5 10 3 7 9990.49 626.919 33 -10 -3 -7 10991.6 643.382 26 10 3 7 10513.9 625.420 6 10 3 8 5560.94 404.849 33 -10 -3 -8 5555.14 419.234 26 10 3 8 5828.97 403.640 6 -10 -3 -9 4816.79 357.640 26 10 3 9 4110.68 329.520 6 10 3 9 4072.29 384.477 47 10 3 10 125.989 124.901 31 -10 -3 -10 409.784 150.570 26 10 3 10 311.553 166.400 47 10 3 11 457.536 142.897 31 -10 -3 -11 484.821 143.220 26 10 3 11 507.840 179.839 47 10 3 12 259.284 116.544 31 -10 -3 -12 143.502 101.696 26 10 3 12 517.157 146.372 47 10 3 13 42.8248 79.9611 31 10 3 13 59.6997 73.9270 22 10 3 13 13.2852 98.2172 47 10 3 14 105.046 62.5150 43 -10 -4 4 2127.38 191.341 18 -10 -4 4 2513.78 175.805 16 10 4 -4 2430.60 165.800 48 -10 -4 3 4758.62 303.239 16 -10 -4 2 1884.51 185.258 16 -10 -4 1 2910.56 248.538 16 10 4 -1 2904.63 261.408 33 10 4 0 12959.6 710.431 33 -10 -4 0 13656.9 695.217 26 10 4 0 11102.6 676.684 6 -10 -4 0 12229.4 666.882 23 10 4 1 1153.67 179.779 6 10 4 1 1193.02 195.645 33 -10 -4 -1 1143.22 194.841 5 -10 -4 -1 1140.68 187.124 26 -10 -4 -1 899.499 157.025 23 -10 -4 -2 1594.13 211.364 39 -10 -4 -2 2453.88 271.380 5 10 4 2 2512.02 272.717 33 -10 -4 -2 2409.99 259.989 26 10 4 2 2384.73 251.551 6 -10 -4 -3 9580.55 573.306 5 10 4 3 9394.71 563.829 33 -10 -4 -3 9484.63 556.637 26 10 4 3 9012.30 539.530 6 10 4 4 1422.46 215.534 6 10 4 5 168.042 146.109 33 -10 -4 -5 49.6977 160.521 5 -10 -4 -5 140.415 156.869 26 -10 -4 -6 1879.03 254.798 5 10 4 6 1881.77 236.640 33 -10 -4 -6 2286.35 261.229 26 10 4 6 1683.63 230.989 6 10 4 6 1458.33 205.729 48 -10 -4 -7 2201.81 275.836 5 10 4 7 2030.22 241.977 33 -10 -4 -7 1981.90 252.793 26 10 4 7 2351.94 253.404 6 -10 -4 -8 7330.60 514.886 5 10 4 8 7489.39 492.272 33 -10 -4 -8 8513.53 510.233 26 10 4 8 8362.92 498.638 6 -10 -4 -9 3302.76 309.093 5 10 4 9 2695.83 258.416 31 -10 -4 -9 3657.33 310.781 26 10 4 9 3768.43 296.514 6 10 4 9 2898.10 308.811 47 -10 -4 -10 4738.62 334.151 26 10 4 10 4229.29 347.124 47 10 4 11 2506.42 241.057 31 -10 -4 -11 2820.90 242.243 26 10 4 11 2716.21 269.296 47 10 4 12 107.206 101.605 31 -10 -4 -12 69.5234 86.0377 26 10 4 12 58.1281 119.536 47 10 4 13 50.1577 102.119 43 10 4 13 208.530 95.2513 22 -10 -5 4 211.526 63.5395 18 -10 -5 3 1988.33 188.324 18 -10 -5 3 2424.41 166.752 16 10 5 -3 2264.28 193.802 48 -10 -5 2 1008.06 130.849 16 10 5 -2 1235.99 163.786 48 -10 -5 1 5400.26 332.544 16 -10 -5 0 3687.44 321.907 5 -10 -5 0 4212.92 295.318 16 10 5 0 5183.23 356.393 33 -10 -5 0 5525.06 353.044 26 10 5 0 3934.22 319.031 6 -10 -5 -1 3828.83 334.357 5 -10 -5 -1 3570.19 274.883 16 10 5 1 4592.94 347.186 33 10 5 1 4020.60 325.005 6 10 5 2 805.960 173.153 6 10 5 2 738.445 169.346 33 -10 -5 -2 824.420 190.000 5 -10 -5 -2 621.241 178.059 26 -10 -5 -3 2021.35 250.570 5 10 5 3 1950.80 249.978 33 10 5 3 2015.32 236.850 6 -10 -5 -4 6210.72 445.987 26 10 5 4 6151.81 438.297 6 10 5 5 190.111 145.465 6 10 5 5 642.815 167.577 33 -10 -5 -5 48.0957 166.873 5 -10 -5 -5 195.146 163.503 26 10 5 5 247.233 145.991 48 10 5 6 244.477 142.629 33 -10 -5 -6 181.742 167.488 5 -10 -5 -6 25.1753 151.582 26 10 5 6 149.749 138.755 48 10 5 7 116.974 141.528 6 10 5 7 87.9474 124.053 33 -10 -5 -7 129.388 163.484 5 -10 -5 -7 89.3355 150.257 26 10 5 7 135.585 115.951 48 -10 -5 -8 2810.10 308.176 5 10 5 8 3491.99 298.720 33 -10 -5 -8 3316.06 300.681 26 10 5 8 3364.39 302.743 6 -10 -5 -9 2805.04 292.842 5 -10 -5 -9 3059.68 279.276 26 10 5 9 3188.01 285.578 6 -10 -5 -10 6771.62 416.590 26 10 5 10 5891.48 405.690 6 10 5 11 1352.36 168.681 31 -10 -5 -11 1941.33 186.329 26 10 5 12 1562.02 186.289 43 10 5 13 1145.82 151.942 43 10 5 13 992.136 147.002 22 10 5 14 294.874 75.9158 43 -10 -6 2 1361.70 145.808 18 10 6 -2 1773.24 175.474 48 10 6 -1 1168.54 165.880 48 10 6 0 773.520 167.244 48 10 6 0 558.139 132.008 6 -10 -6 -1 2561.07 267.810 5 -10 -6 -1 3523.91 288.189 26 10 6 1 2438.37 262.550 6 10 6 1 3691.09 298.197 48 -10 -6 -2 3473.05 299.109 5 10 6 2 2843.39 285.765 33 10 6 2 2914.93 278.552 6 10 6 3 1522.65 223.360 33 -10 -6 -3 1547.37 225.309 5 -10 -6 -3 1473.98 226.455 26 10 6 3 1574.60 222.227 6 10 6 3 1569.53 229.978 48 -10 -6 -4 1396.05 219.684 26 10 6 4 1506.58 214.120 6 10 6 4 1110.29 203.244 48 10 6 5 629.798 176.229 6 -10 -6 -5 336.751 173.400 5 10 6 5 490.309 170.887 33 -10 -6 -5 333.613 165.570 26 10 6 5 488.184 166.057 48 -10 -6 -6 7321.41 483.382 5 10 6 6 6248.80 460.778 33 -10 -6 -6 6523.56 446.816 26 10 6 6 5760.74 437.793 48 10 6 7 291.111 156.952 6 10 6 7 376.051 149.771 33 -10 -6 -7 166.775 160.569 5 -10 -6 -7 685.368 173.756 26 10 6 7 173.214 132.465 48 10 6 8 147.992 137.366 6 -10 -6 -8-140.101 150.938 5 -10 -6 -8 89.5947 133.667 26 10 6 9 550.220 155.337 6 10 6 9 374.508 164.364 37 -10 -6 -9 532.353 150.576 5 -10 -6 -9 753.388 157.908 26 -10 -6 -10 972.290 159.525 5 -10 -6 -10 1173.56 158.268 26 10 6 11 1428.14 178.123 43 10 6 12 2332.58 214.981 43 10 6 13 1912.04 172.543 43 10 6 13 1777.19 180.554 22 10 7 -2 127.001 81.6017 15 10 7 -2 83.8558 74.3926 48 10 7 -1 23.7740 71.5164 34 10 7 -1 177.016 103.329 48 10 7 0 681.150 138.334 34 10 7 0 999.402 163.732 48 -10 -7 -1 82.0371 100.654 5 10 7 1 111.865 128.722 48 10 7 1-90.8476 110.361 6 10 7 2 1006.47 170.628 6 -10 -7 -2 786.814 166.702 5 -10 -7 -2 1082.95 188.421 26 -10 -7 -3 2508.29 263.086 5 -10 -7 -3 2512.07 259.279 26 10 7 3 2607.46 263.723 6 10 7 4 518.961 165.593 6 -10 -7 -4 394.900 165.877 5 -10 -7 -4 483.305 160.033 26 10 7 4 518.823 163.972 48 -10 -7 -5 9369.65 573.993 26 10 7 5 9427.24 590.224 6 10 7 5 9438.21 583.787 48 -10 -7 -6 1769.66 231.281 5 -10 -7 -6 1716.57 221.145 26 10 7 6 1694.18 221.375 48 10 7 7 464.598 157.964 6 -10 -7 -7 242.472 147.233 5 -10 -7 -7 270.552 140.901 26 10 7 7 310.327 139.021 48 -10 -7 -8 1352.88 207.160 5 -10 -7 -8 1361.15 187.000 26 10 7 9 32.3974 95.8199 43 10 7 9 196.586 151.538 37 -10 -7 -9 73.3007 117.552 5 -10 -7 -9 77.6330 103.087 26 10 7 9 26.5565 121.332 6 10 7 10-55.7822 98.3728 43 10 7 10 151.250 129.005 37 10 7 10 90.0225 123.900 22 10 7 11-38.7411 100.856 43 10 7 11 200.150 121.027 22 10 7 12 631.827 112.328 43 10 7 12 820.047 135.938 22 10 7 13 1100.89 115.904 43 10 8 -1 759.603 115.447 15 10 8 -1 575.021 104.521 48 10 8 0 236.786 95.2403 34 10 8 0 429.533 121.467 48 10 8 1 2504.30 235.332 34 10 8 1 3043.30 251.263 48 10 8 2 109.696 114.428 34 -10 -8 -2 98.0626 108.957 5 10 8 2 199.371 132.196 48 -10 -8 -3 108.697 115.095 5 10 8 3-114.208 120.322 6 -10 -8 -4 2242.05 255.105 5 -10 -8 -4 3046.13 257.372 26 10 8 4 2580.14 266.322 6 10 8 4 2727.50 269.295 48 -10 -8 -5 2230.88 230.024 26 10 8 5 2339.39 254.280 6 10 8 5 2469.37 252.472 48 -10 -8 -6 271.989 133.056 5 -10 -8 -6 210.399 121.639 26 10 8 6 228.588 131.647 48 -10 -8 -7 249.090 130.665 5 -10 -8 -7 176.178 113.551 26 10 8 7 145.432 126.089 48 10 8 7 183.771 104.583 22 10 8 7 354.376 145.930 6 10 8 8 1112.19 165.928 34 -10 -8 -8 785.354 171.970 5 -10 -8 -8 885.473 141.918 26 10 8 8 1053.27 157.443 22 10 8 8 1095.65 179.328 6 10 8 9 660.929 183.044 37 -10 -8 -9 661.315 146.908 5 10 8 9 832.038 146.365 22 10 8 10 113.914 127.940 37 10 8 10 280.427 119.588 22 10 8 11 63.8481 99.5374 37 10 8 11 18.0110 93.5483 22 10 8 12 86.3890 69.7581 38 10 8 12 89.5091 77.7623 22 10 9 0 805.894 107.231 15 10 9 0 511.127 94.6545 48 10 9 1 1192.81 145.004 34 10 9 1 1540.49 164.886 48 10 9 2 633.486 128.269 34 10 9 2 750.750 138.188 48 10 9 3 65.3713 103.828 34 -10 -9 -3-4.90340 91.9831 5 10 9 3 107.787 103.993 15 10 9 4 254.026 122.263 34 -10 -9 -4 263.241 111.016 5 10 9 4 150.183 108.115 15 10 9 4 363.328 134.723 48 10 9 5 43.8367 95.3450 15 10 9 5 144.811 119.464 48 10 9 6 248.581 119.005 34 -10 -9 -6 158.051 119.221 5 10 9 6 181.895 122.933 48 10 9 7 43.6209 101.783 34 -10 -9 -7 11.7590 99.8148 5 10 9 7-14.5496 95.6745 48 10 9 8 547.315 121.123 34 -10 -9 -8 414.401 122.742 5 10 9 9 576.089 163.030 37 10 9 9 456.437 106.655 22 10 9 10 805.633 160.950 37 10 9 10 1033.75 127.020 22 10 9 11 63.6330 88.1299 37 10 9 11 63.2782 72.3484 22 10 10 2 575.053 99.5503 15 10 10 2 720.188 108.965 48 10 10 3 159.712 87.5151 34 10 10 3 405.500 91.5402 15 10 10 3 161.636 92.8659 48 10 10 4 227.574 98.1825 34 10 10 4 382.640 94.2964 15 10 10 5 530.564 127.245 48 10 10 6 938.734 133.784 34 10 10 6 853.238 136.921 48 10 10 7 121.591 80.7233 34 10 10 9 94.4364 103.239 37 10 10 10 887.857 122.820 38 10 10 10 832.903 125.073 37 10 11 6 406.334 89.4771 37 -11 3 0 25.7434 50.2967 23 -11 3 -1 2105.43 168.443 39 11 -3 1 2699.25 177.966 33 11 -3 1 2411.54 158.741 6 -11 3 -2 1799.80 160.298 39 11 -3 2 2546.80 164.775 6 -11 3 -3 712.630 107.392 39 11 -3 3 1026.73 111.935 6 -11 3 -4 2081.99 166.094 39 -11 3 -5 1696.71 158.802 39 11 -3 5 2765.58 175.889 6 -11 3 -6 3058.30 215.800 39 11 -3 6 4648.63 236.332 6 11 -3 7 1538.76 157.261 47 -11 2 1 889.329 101.103 23 -11 2 0 1403.04 140.211 39 11 -2 0 1545.46 133.496 33 11 -2 0 1327.66 111.514 6 -11 2 0 1274.78 131.156 23 11 -2 1 3.35310 69.9449 6 -11 2 -1 107.835 84.1455 39 11 -2 1 53.1955 75.9197 33 11 -2 2 16.4524 82.5068 6 -11 2 -2 74.6225 90.5700 39 11 -2 3 704.258 119.183 6 -11 2 -3 531.324 114.630 39 11 -2 4 482.316 109.424 6 -11 2 -4 316.615 102.883 39 -11 2 -5 1631.22 156.766 39 11 -2 6 6382.95 352.239 33 11 -2 6 7113.59 358.075 6 -11 2 -7 4166.21 237.391 26 11 -2 7 4204.65 241.225 6 -11 2 -8 1483.27 134.614 26 -11 2 -9 954.812 97.3904 26 11 -2 9 678.796 124.697 47 -11 1 2 45.0786 57.4758 23 -11 1 1 4801.46 286.473 39 11 -1 -1 4310.92 261.827 33 -11 1 1 4637.61 277.341 23 -11 1 0 793.690 123.886 39 11 -1 0 895.853 118.185 33 11 -1 0 779.045 100.902 6 -11 1 0 721.938 120.227 23 11 -1 1 87.0526 85.3734 6 -11 1 -1 73.7633 99.3821 39 11 -1 1 91.7597 90.6677 33 -11 1 -2 5735.41 364.612 39 11 -1 2 6233.74 368.781 6 -11 1 -3 2700.75 232.181 39 11 -1 3 3499.95 253.108 6 11 -1 4 471.098 124.788 6 -11 1 -4 401.184 116.782 39 -11 1 -5 108.236 93.3794 39 -11 1 -5 38.9206 94.3488 26 11 -1 6 746.650 129.599 6 -11 1 -6 515.496 112.259 39 11 -1 6 905.776 137.649 33 -11 1 -6 948.037 133.092 26 11 -1 7 857.000 127.639 6 -11 1 -7 658.023 102.684 39 11 -1 7 815.354 120.508 33 -11 1 -7 1017.45 141.720 26 -11 1 -8 2308.74 197.318 26 -11 1 -9 1055.52 132.074 26 11 -1 10 830.159 118.841 31 -11 0 2 1578.26 151.301 16 -11 0 2 1757.53 149.151 23 -11 0 1-78.0791 94.1047 39 11 0 -1 9.98823 62.7408 33 -11 0 1-57.9130 88.7312 23 11 0 0 271.960 88.3886 6 -11 0 0 405.565 116.294 39 11 0 0 483.827 105.487 33 -11 0 0 394.531 109.481 23 -11 0 -1 5901.00 366.774 39 11 0 1 6351.92 384.310 33 11 0 1 6093.55 358.364 6 -11 0 -1 4964.75 345.671 23 -11 0 -2 5265.71 357.819 39 11 0 2 5829.44 382.675 33 11 0 2 5927.03 366.457 6 -11 0 -3 6824.76 431.442 39 11 0 3 7702.56 463.638 33 11 0 3 7677.72 450.723 6 -11 0 -4 2300.69 212.456 39 -11 0 -4 2356.89 218.851 26 11 0 4 2900.13 239.361 6 -11 0 -5 1055.88 148.408 39 11 0 5 1188.13 179.394 33 -11 0 -5 1411.76 174.379 26 11 0 6 362.655 119.979 6 -11 0 -6 346.356 102.149 39 11 0 6 203.204 110.831 33 -11 0 -6 314.949 132.612 26 11 0 7 64.2193 100.153 6 11 0 7 61.7067 92.2513 33 -11 0 -7 11.3452 112.623 26 11 0 8 419.916 104.382 6 -11 0 -8 509.501 129.754 26 11 0 9 102.497 140.232 47 -11 0 -10 758.644 126.893 26 11 0 10 932.530 161.330 47 11 0 11 404.562 97.3721 31 -11 0 -11 720.219 100.554 26 11 0 11 642.762 121.781 47 -11 -1 3 199.955 65.0521 16 -11 -1 2 2096.05 180.740 16 -11 -1 2 2502.36 182.780 23 11 1 -1 5441.76 322.254 33 -11 -1 1 5270.94 326.512 23 11 1 0-18.9800 79.0032 6 -11 -1 0 45.1480 103.218 39 11 1 0-32.1880 90.5597 33 -11 -1 0-42.6414 97.3370 23 -11 -1 -1 2390.59 224.276 39 11 1 1 2735.36 239.340 33 11 1 1 2577.33 213.302 6 -11 -1 -1 2133.67 202.433 23 -11 -1 -2 4995.02 334.971 39 11 1 2 5950.62 370.984 33 11 1 2 5556.51 345.739 6 -11 -1 -3 3014.74 257.286 39 11 1 3 4064.50 304.313 33 -11 -1 -3 3480.21 268.930 26 11 1 3 4069.63 288.505 6 -11 -1 -3 2746.80 235.307 23 -11 -1 -4 6335.46 386.079 26 11 1 4 6646.75 400.665 6 11 1 5 3526.37 284.984 33 -11 -1 -5 3205.28 271.427 26 11 1 6 3208.08 271.038 33 -11 -1 -6 3068.38 270.342 26 11 1 6 3169.19 266.700 6 11 1 7 305.871 120.735 6 11 1 7 460.226 125.414 33 -11 -1 -7 250.169 139.725 26 11 1 8 1543.19 175.439 6 -11 -1 -9 298.870 125.875 26 11 1 9 534.084 167.405 47 11 1 10 88.1484 93.2720 31 -11 -1 -10 98.7984 102.910 26 11 1 10 252.786 133.139 47 -11 -1 -11 1554.00 145.989 26 11 1 11 1369.95 168.802 47 11 1 12 582.429 104.660 47 -11 -2 3 540.003 89.7312 18 -11 -2 3 625.013 87.8496 16 -11 -2 2 655.811 106.032 16 11 2 -1 1447.94 147.024 33 -11 -2 1 1532.47 157.434 23 11 2 0 2849.94 231.417 6 -11 -2 0 3212.97 240.166 23 11 2 1-51.6887 98.0667 6 -11 -2 -1-58.9144 107.205 39 11 2 1-6.70221 106.145 33 -11 -2 -1-39.0943 102.819 23 11 2 2 612.986 139.395 6 -11 -2 -2 630.721 140.174 39 11 2 2 633.098 146.429 33 -11 -2 -2 500.410 126.182 26 -11 -2 -2 378.816 111.869 23 11 2 3 498.535 140.253 6 -11 -2 -3 457.980 124.293 39 11 2 3 578.948 152.212 33 -11 -2 -3 601.521 141.335 26 -11 -2 -4 5294.04 346.321 26 11 2 4 5196.50 344.229 6 11 2 5 5800.70 412.955 33 -11 -2 -5 6035.12 406.088 26 11 2 6 2943.33 272.361 33 -11 -2 -6 3290.48 287.158 26 11 2 6 3026.49 272.009 6 11 2 7 7192.53 470.539 33 11 2 7 7942.93 470.396 6 11 2 8 3450.71 272.911 33 -11 -2 -8 3943.82 306.789 26 11 2 8 3639.38 280.271 6 -11 -2 -9 1394.98 177.833 26 11 2 9 1170.43 147.223 6 11 2 9 1059.64 198.872 47 11 2 10 171.842 98.2240 31 -11 -2 -10 50.9312 107.920 26 11 2 10 166.931 130.473 47 11 2 11 68.2992 85.6172 31 -11 -2 -11 190.219 93.7804 26 11 2 11 73.9238 113.475 47 11 2 12 294.158 74.3895 31 -11 -2 -12 265.076 73.2208 26 11 2 12 246.301 93.9055 47 -11 -3 3 716.531 98.2367 18 -11 -3 2 754.731 107.437 16 -11 -3 1 1427.76 153.238 16 11 3 0 1413.65 166.897 33 11 3 0 1174.48 142.935 6 -11 -3 0 1429.77 146.540 23 11 3 1 1614.61 186.151 33 -11 -3 -1 1231.33 162.858 26 11 3 1 1460.86 169.422 6 -11 -3 -1 1309.32 147.541 23 11 3 2 1701.40 202.972 33 -11 -3 -2 1262.60 182.021 26 11 3 2 1665.25 191.414 6 11 3 3 720.190 151.340 6 -11 -3 -3 511.483 123.999 39 11 3 3 784.050 163.948 33 -11 -3 -3 898.785 163.565 26 11 3 4 7.08175 125.638 6 -11 -3 -4 246.509 134.322 26 11 3 5 381.891 146.993 6 11 3 5 338.261 136.753 33 -11 -3 -5 490.926 155.319 26 11 3 6 3854.16 314.595 33 11 3 7 8535.38 539.007 33 -11 -3 -7 9351.60 556.514 26 11 3 7 9552.68 544.809 6 11 3 8 7067.56 466.109 33 -11 -3 -8 8325.45 494.522 26 11 3 8 8165.85 477.071 6 11 3 9 2302.70 230.137 31 -11 -3 -9 4562.27 304.065 26 11 3 9 3972.09 271.157 6 11 3 9 3165.20 297.182 47 11 3 10 1206.41 154.733 31 -11 -3 -10 1849.48 192.258 26 11 3 10 1594.79 198.787 47 11 3 11 187.538 81.2106 31 -11 -3 -11 212.639 98.2065 26 11 3 11 214.536 113.437 47 11 3 12-25.8122 60.4674 31 -11 -3 -12 14.2866 61.0730 26 11 3 12 94.8810 79.5636 47 -11 -4 2 1393.49 156.109 18 11 4 -2 2178.37 172.597 48 -11 -4 1 1456.03 133.880 16 -11 -4 0 947.542 122.299 16 11 4 0 952.206 141.472 33 11 4 1 4286.04 310.193 33 -11 -4 -1 3825.42 292.376 26 11 4 1 3811.16 287.085 6 11 4 2 1409.28 176.874 6 11 4 2 1695.78 201.903 33 -11 -4 -2 1222.88 178.762 26 11 4 3 2390.22 254.547 33 -11 -4 -3 2508.30 244.770 26 11 4 3 2327.09 238.015 6 -11 -4 -4 1962.39 227.060 26 11 4 4 1920.87 223.312 6 11 4 5 857.230 169.291 6 11 4 5 532.160 154.977 33 -11 -4 -5 856.680 188.014 5 11 4 5 694.422 148.896 48 11 4 6 621.864 146.520 33 -11 -4 -6 384.613 153.972 5 -11 -4 -6 482.809 159.743 26 11 4 7 1848.59 214.875 33 -11 -4 -7 1803.61 223.182 26 11 4 7 2167.62 225.991 6 11 4 8 5929.18 420.758 33 -11 -4 -8 7045.99 443.292 26 11 4 8 7172.15 436.133 6 -11 -4 -9 4024.53 288.651 26 11 4 9 3600.67 272.491 6 -11 -4 -10 3987.60 272.899 26 11 4 10 2771.36 246.159 47 -11 -4 -11 769.567 125.965 26 11 4 11 645.917 116.018 47 11 4 12 369.969 99.8184 43 11 5 -2 126.782 63.4042 48 11 5 -1 1215.79 144.886 48 11 5 0 4695.82 323.790 48 11 5 1 1540.54 176.085 6 11 5 2 1118.68 172.098 6 11 5 2 1333.26 182.396 33 -11 -5 -2 1441.52 182.290 26 11 5 3 486.717 136.020 6 11 5 3 444.897 138.464 33 -11 -5 -3 264.222 134.981 5 -11 -5 -3 165.937 128.414 26 11 5 3 240.036 140.759 48 -11 -5 -4 2267.86 251.733 5 11 5 4 2248.81 250.318 33 11 5 4 2330.50 236.826 6 11 5 4 2330.14 237.333 48 -11 -5 -5 2151.05 242.427 26 11 5 5 2625.93 249.399 6 11 5 5 2349.72 228.641 48 11 5 6 30.6664 111.971 33 -11 -5 -6-55.0744 135.813 5 -11 -5 -6-27.1317 132.400 26 11 5 7 345.420 145.440 6 11 5 7 544.594 140.963 33 -11 -5 -7 385.373 145.704 5 -11 -5 -7 562.612 152.516 26 11 5 8 12.6931 116.799 6 -11 -5 -8 75.9798 125.270 5 -11 -5 -8-42.5200 123.775 26 -11 -5 -9 3771.10 290.843 26 11 5 9 3906.31 290.781 6 -11 -5 -10 2193.99 200.888 26 11 5 11 3337.76 237.512 43 -11 -5 -11 2709.35 209.637 26 11 5 12 783.875 110.354 43 11 6 -1 169.033 80.3619 48 -11 -6 0 126.181 70.4160 18 11 6 0 364.562 84.3668 34 11 6 0 394.327 113.157 48 11 6 1 331.552 122.546 48 11 6 1 239.887 93.0538 6 11 6 2 319.986 110.400 6 -11 -6 -2 201.163 107.552 5 -11 -6 -2 118.273 110.975 26 11 6 3 224.527 121.363 6 -11 -6 -3 49.6341 110.445 5 11 6 3 178.552 129.259 48 -11 -6 -4 1373.65 192.761 5 -11 -6 -4 1060.43 179.482 26 11 6 4 1399.73 191.694 6 11 6 4 1426.10 188.658 48 -11 -6 -5 4442.38 323.029 26 11 6 5 4248.60 326.035 6 11 6 5 3924.47 315.758 48 -11 -6 -6 474.066 151.094 5 -11 -6 -6 454.318 143.916 26 11 6 6 440.544 129.572 48 -11 -6 -7 1891.95 239.610 5 -11 -6 -7 2386.15 231.251 26 11 6 7 2580.38 251.031 6 11 6 8 55.3437 113.226 6 -11 -6 -8 180.744 113.598 5 -11 -6 -8 21.4093 111.240 26 11 6 9 89.3383 97.1766 6 11 6 9-35.9312 81.7617 43 -11 -6 -9-21.8776 103.987 5 -11 -6 -9 27.5383 100.762 26 11 6 10 696.835 113.621 43 -11 -6 -10 832.621 119.108 26 11 6 11 355.425 92.2108 43 11 6 11 496.859 117.791 22 11 6 12 417.572 76.4549 43 11 6 12 414.819 95.8744 22 11 7 0 214.930 84.5623 48 11 7 1 767.758 117.505 34 11 7 1 1189.01 141.026 48 -11 -7 -3 57.0447 91.5134 5 11 7 3 10.6209 108.683 48 11 7 3 158.535 103.204 6 11 7 4 558.644 137.766 6 -11 -7 -4 420.650 130.742 5 -11 -7 -4 496.961 133.896 26 11 7 4 492.392 133.279 48 11 7 5 234.261 127.908 6 -11 -7 -5 303.562 122.951 26 11 7 5 176.471 120.012 48 -11 -7 -6 7913.36 510.267 5 -11 -7 -6 9036.57 490.393 26 11 7 6 7694.25 479.771 48 11 7 7 1153.94 178.432 6 -11 -7 -7 1007.20 168.539 5 -11 -7 -7 1007.61 158.240 26 11 7 7 754.170 131.479 22 11 7 8 22.5797 106.596 6 -11 -7 -8 28.6166 107.334 5 -11 -7 -8-47.4134 97.4617 26 11 7 8-8.85612 92.1542 22 -11 -7 -9 89.1042 81.8254 26 11 7 9-40.2114 99.0871 22 11 7 9 33.0705 92.4252 6 11 7 10 66.4875 93.8560 22 11 7 11-31.6120 74.0673 22 11 7 12 12.3623 56.4395 22 11 8 1 382.921 88.4692 48 11 8 2 2238.96 199.155 34 11 8 2 2976.55 211.402 15 11 8 3 256.795 101.834 34 11 8 3 198.896 97.2180 15 11 8 4 146.649 98.5308 34 11 8 4 84.0433 86.6312 15 11 8 4 82.6672 101.435 48 11 8 5 545.223 123.521 48 11 8 5 609.277 131.654 6 -11 -8 -6 2873.58 258.879 5 11 8 6 3508.41 255.141 34 -11 -8 -6 3000.02 234.963 26 11 8 6 3339.06 266.520 6 11 8 6 2723.88 239.596 48 11 8 7 1311.66 156.193 34 -11 -8 -7 964.445 153.674 5 -11 -8 -7 1208.64 141.667 26 11 8 8 55.5754 81.8486 34 -11 -8 -8 123.942 77.5503 26 11 8 9 47.4175 68.2157 22 11 8 10 305.255 82.5240 22 11 9 3 1081.34 119.534 34 11 9 3 979.539 110.110 15 11 9 4 77.1444 77.6509 34 11 9 4 122.188 62.3781 15 11 9 4 124.435 77.7623 48 11 9 5-6.59730 79.3073 48 11 9 6 14.9589 76.0586 34 11 9 6-49.6642 73.4350 48 11 9 7 266.206 80.9657 34 11 9 8 141.121 91.0390 37 12 -1 2-17.0274 48.7875 33 12 -1 3 4732.91 279.374 33 12 -1 3 4951.14 271.974 6 12 -1 4 1527.02 130.995 6 12 -1 5 617.901 89.0690 33 12 -1 6 104.348 55.3216 6 12 -1 7 178.716 81.0823 47 -12 0 -2 3101.02 212.575 39 12 0 2 3554.08 216.709 6 12 0 3 6069.33 327.319 33 12 0 3 6211.24 312.816 6 -12 0 -4 3050.80 217.299 39 12 0 4 5272.49 262.312 6 12 0 5 1599.30 154.692 33 12 0 6 738.919 105.470 6 12 0 6 557.567 93.0845 33 12 0 7 11.4726 62.1433 6 -12 0 -7 84.9790 64.5906 26 -12 0 -8 283.142 68.5523 26 12 0 8 269.391 89.9582 47 12 1 1 58.0198 56.8036 33 12 1 2 1352.22 140.644 33 12 1 2 1177.44 124.858 6 12 1 3 5922.49 322.029 33 12 1 3 5826.79 307.404 6 -12 -1 -4 4014.75 266.585 39 12 1 4 6805.27 325.717 6 12 1 5 5966.07 356.568 33 12 1 5 7082.89 360.489 6 12 1 6 2534.42 202.075 33 -12 -1 -6 2402.79 195.087 26 12 1 7 1821.24 150.644 33 -12 -1 -7 1476.99 156.269 26 12 1 7 1834.04 159.770 6 12 1 8 180.215 72.7204 6 -12 -1 -8 325.465 90.6282 26 12 1 8 254.538 104.542 47 12 1 9 107.497 83.2667 47 -12 -2 -1 773.640 105.302 16 12 2 1 1779.98 134.298 33 12 2 2 275.965 83.5414 6 12 2 2 312.997 88.3091 33 12 2 3 449.576 103.103 6 12 2 3 561.496 113.768 33 -12 -2 -4 1509.89 156.171 26 12 2 4 1837.48 171.234 6 12 2 5 4338.53 293.840 33 -12 -2 -5 3772.01 275.814 26 12 2 5 4553.84 292.261 6 12 2 6 4802.99 311.344 33 -12 -2 -6 4471.19 304.124 26 12 2 7 1348.16 143.775 33 -12 -2 -7 1452.77 158.133 26 12 2 7 1467.09 151.139 6 12 2 7 925.849 151.369 47 12 2 8 2473.65 182.103 6 12 2 8 1586.14 183.290 47 -12 -2 -9 216.159 83.8063 26 12 2 9 26.4029 83.0102 47 -12 -2 -10-88.6625 67.2427 26 12 3 1 1424.09 134.731 33 12 3 1 1472.03 139.751 48 12 3 2 721.429 105.622 6 12 3 2 864.077 120.174 33 12 3 3 441.969 106.042 6 12 3 3 512.564 111.174 33 -12 -3 -3 340.160 94.5041 26 12 3 3 283.436 97.3838 48 12 3 4 103.094 98.4650 6 12 3 4 38.2015 105.408 33 -12 -3 -4 27.8681 90.0508 26 12 3 5 616.891 124.776 6 12 3 5 534.401 120.604 33 -12 -3 -5 605.966 121.662 26 12 3 6 663.455 125.984 33 -12 -3 -6 843.497 133.828 26 12 3 7 3252.90 244.813 33 12 3 7 3571.01 254.475 6 -12 -3 -8 2994.13 230.781 26 12 3 8 2951.57 226.948 6 -12 -3 -9 2276.82 189.049 26 -12 -3 -10 68.2600 67.2810 26 12 4 1 882.979 115.341 48 12 4 2 5562.06 318.968 33 12 4 2 5311.85 305.950 48 12 4 3 667.163 111.920 6 12 4 3 710.660 119.871 33 -12 -4 -3 539.307 108.321 26 12 4 3 496.230 111.383 48 12 4 4-65.8219 94.2912 6 12 4 4-10.7569 88.4291 33 -12 -4 -4 16.4801 88.9131 26 12 4 5 577.126 122.494 6 -12 -4 -5 398.901 120.499 26 12 4 6 10.5182 84.0867 33 12 4 7 289.022 106.912 6 12 4 7 334.755 98.3697 33 -12 -4 -7 367.467 113.618 26 -12 -4 -8 1660.99 177.128 26 12 4 8 2062.69 175.412 6 -12 -4 -9 2108.40 180.933 26 -12 -4 -10 472.665 88.2909 26 12 5 2 2036.43 186.957 6 12 5 2 4099.21 223.845 48 -12 -5 -3 1525.17 153.295 26 12 5 3 1290.01 151.541 6 12 5 3 1546.46 153.417 48 12 5 4 280.660 101.935 6 -12 -5 -4 320.891 101.417 26 12 5 4 160.468 88.2965 48 12 5 5 52.8843 95.0668 6 -12 -5 -6 1474.51 164.809 26 12 5 7 42.0934 90.3733 6 -12 -5 -7 109.629 91.6841 26 12 5 8 263.809 96.9499 6 -12 -5 -8 258.931 95.1645 26 12 5 9 31.0746 69.5897 6 -12 -5 -9-45.2424 76.5933 26 -12 -5 -10 584.393 88.3276 26 12 6 2 63.9880 58.6325 34 12 6 2 128.702 70.9484 48 12 6 3 901.072 117.627 48 12 6 3 605.648 102.437 6 12 6 4 869.143 128.149 6 12 6 4 942.052 118.659 48 12 6 5 215.367 92.2105 6 -12 -6 -5 90.8386 83.3422 26 12 6 6 603.330 121.219 6 -12 -6 -6 492.354 111.046 26 12 6 7 464.331 111.842 6 -12 -6 -7 378.130 103.492 26 -12 -6 -8 1676.54 154.731 26 12 6 8 2019.54 168.139 6 -12 -6 -9 44.6223 61.8298 26 12 6 9 40.0824 65.5027 22 12 6 9-35.5757 65.2389 6 12 7 3 34.3943 57.1398 34 12 7 4 190.031 75.8338 34 12 7 4 224.407 73.0884 48 12 7 5 490.849 97.4311 6 12 7 6-44.1920 77.2312 34 -12 -7 -6 42.3981 73.8291 26 12 7 6 30.4302 77.3560 6 12 7 7 2078.03 163.092 34 -12 -7 -7 1839.79 157.774 26 -12 -7 -8 1436.08 130.697 26 0 0 0 0.00 0.00 0 TITL CC2_36B_ABS in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 10.165939 10.738333 12.987840 76.1323 69.6461 75.3039 ZERR 1.00 0.000439 0.000584 0.000401 0.0035 0.0034 0.0042 LATT 1 SFAC C H N O Cu UNIT 45.40 60.70 1.00 18.30 2.00 TREF HKLF 4 END ; _shelx_hkl_checksum 53992 _shelx_res_file ; TITL cc2_36b_a.res in P-1 compound_2.res created by SHELXL-2018/3 at 19:57:34 on 07-May-2024 REM Old TITL CC2_36B in P-1 REM SHELXT solution in P-1 REM R1 0.171, Rweak 0.010, Alpha 0.058, Orientation as input REM Formula found by SHELXT: C38 N15 O16 Cu2 CELL 1.54184 10.1659 10.7383 12.9878 76.132 69.646 75.304 ZERR 1 0.0004 0.0006 0.0004 0.004 0.003 0.004 LATT 1 SFAC C H Cu N O UNIT 45 61 2 1 18 SADI O10 C17 O10 C18 O9 C16 O9 C19 O12 C21 O12 C22 O11 C20 O11 C23 RIGU 0.01 0.01 O11 C20 C23 C21 C22 O12 RIGU 0.01 0.01 O13 C33 C35 RIGU 0.01 0.01 O9 O10 C17 C18 C16 C19 SADI C17 C16 C19 C18 C20 C21 C22 C23 RIGU 0.01 0.01 O14 C34 C32 SADI O9 C16 O9 C19 O11 C23 O11 C20 O12 C21 O10 C17 O10 C18 O12 C22 SADI N1 C28 N1 C26 N1 C30 N1 C24 SIMU 0.01 0.02 2 C17 C16 C19 C18 C20 C23 C22 C21 O10 O9 O12 O11 SADI C28 C29 C30 C31 C24 C25 C26 C27 EADP O8 O7 SIMU N1 C28 C29 C30 C31 C24 C25 C26 C27 RIGU 0.01 0.01 N1 C24 C28 C30 C26 C25 C29 C31 C27 DFIX 0.85 O6 H6 EXYZ O8 O7 L.S. 4 PLAN 5 SIZE 0.054 0.115 0.165 TEMP -173.15(10) CONF FREE O11 C15 BOND $H list 4 MORE -1 HTAB fmap 2 53 acta OMIT 0 -1 1 OMIT 0 0 1 OMIT 0 1 0 OMIT 0 1 1 OMIT 0 1 2 OMIT 1 0 0 OMIT 1 0 1 OMIT 1 0 2 OMIT 1 0 3 OMIT 1 1 1 OMIT 1 1 2 OMIT 1 2 3 REM REM REM WGHT 0.120600 1.273200 FVAR 6.75792 CU1 3 0.555201 0.103174 0.448072 11.00000 0.03027 0.03571 = 0.03388 -0.00778 -0.00424 0.00316 O6 5 -0.108982 0.237446 0.180877 11.00000 0.03702 0.05576 = 0.03625 -0.00716 -0.00810 -0.00256 AFIX 147 H6 2 -0.083253 0.289897 0.121568 11.00000 -1.50000 AFIX 0 O3 5 -0.035170 0.400586 0.996736 11.00000 0.04503 0.04736 = 0.03483 -0.01487 -0.00364 0.00269 O5 5 0.310245 -0.032634 0.464883 11.00000 0.04549 0.04008 = 0.04137 -0.00300 -0.01592 -0.00412 PART 1 O8 5 0.642150 0.278171 0.361430 10.50000 0.03978 0.03875 = 0.04359 -0.00737 -0.00114 -0.00103 PART 0 AFIX 7 H8A 2 0.718610 0.258591 0.306740 11.00000 -1.50000 PART 1 H8B 2 0.693510 0.293540 0.397200 10.50000 -1.50000 AFIX 0 PART 0 O2 5 0.321122 0.008324 0.661284 11.00000 0.03909 0.04562 = 0.03632 -0.01341 -0.00135 -0.00561 O1 5 0.418140 0.185672 0.573073 11.00000 0.05074 0.03611 = 0.04600 -0.01104 0.00923 0.00177 O4 5 0.406406 0.144084 0.374310 11.00000 0.03927 0.04962 = 0.06003 0.01123 -0.02181 -0.00880 C12 1 -0.003819 0.200647 0.230699 11.00000 0.03297 0.04744 = 0.03390 -0.01190 -0.00553 0.00287 C1 1 0.329890 0.126135 0.651716 11.00000 0.03522 0.04107 = 0.03361 -0.00972 -0.00743 0.00430 C13 1 -0.004335 0.084824 0.307191 11.00000 0.04290 0.04837 = 0.03746 -0.00786 -0.00777 -0.00861 AFIX 43 H13 2 -0.075254 0.034120 0.322676 11.00000 -1.20000 AFIX 0 C2 1 0.230324 0.200471 0.740223 11.00000 0.03667 0.04231 = 0.03528 -0.00973 -0.00724 0.00278 C8 1 0.314820 0.073595 0.397131 11.00000 0.03227 0.04155 = 0.03693 -0.01020 -0.00403 0.00389 C9 1 0.203266 0.118250 0.339876 11.00000 0.03420 0.04067 = 0.03622 -0.00974 -0.00466 0.00153 C5 1 0.050574 0.337968 0.912222 11.00000 0.03938 0.04864 = 0.03226 -0.01343 -0.00535 0.00235 C14 1 0.099616 0.044585 0.360282 11.00000 0.04411 0.04101 = 0.03618 -0.00658 -0.00818 -0.00369 AFIX 43 H14 2 0.100262 -0.034953 0.411719 11.00000 -1.20000 AFIX 0 C3 1 0.244621 0.325812 0.741358 11.00000 0.04614 0.04098 = 0.04008 -0.01193 0.00197 0.00314 AFIX 43 H3A 2 0.316244 0.365169 0.682944 11.00000 -1.20000 AFIX 0 C6 1 0.033880 0.213170 0.909934 11.00000 0.04624 0.05631 = 0.03929 -0.01608 0.00130 -0.01124 AFIX 43 H6A 2 -0.039305 0.174616 0.967266 11.00000 -1.20000 AFIX 0 C11 1 0.098775 0.275847 0.210120 11.00000 0.03875 0.04392 = 0.04968 -0.00263 -0.01188 -0.00088 AFIX 43 H11 2 0.098196 0.355615 0.158966 11.00000 -1.20000 AFIX 0 C10 1 0.200563 0.234235 0.264006 11.00000 0.03912 0.04456 = 0.05394 -0.00008 -0.01436 -0.00484 AFIX 43 H10 2 0.270647 0.285612 0.249253 11.00000 -1.20000 AFIX 0 C7 1 0.122334 0.145625 0.825523 11.00000 0.04526 0.05137 = 0.04048 -0.01787 -0.00516 -0.00494 AFIX 43 H7 2 0.109673 0.060998 0.825413 11.00000 -1.20000 AFIX 0 C4 1 0.156459 0.393954 0.825956 11.00000 0.04838 0.03924 = 0.04396 -0.01122 -0.00198 0.00018 AFIX 43 H4 2 0.168138 0.479203 0.825243 11.00000 -1.20000 AFIX 0 PART -1 N1 4 0.500891 0.002399 1.008672 10.50000 0.05107 0.06575 = 0.05591 -0.01964 -0.02039 0.01590 C28 1 0.488388 0.114564 1.063794 10.50000 0.13977 0.08768 = 0.04939 -0.02898 -0.00176 -0.01540 AFIX 23 H28A 2 0.473903 0.196396 1.010975 10.50000 -1.20000 H28B 2 0.401301 0.116172 1.129078 10.50000 -1.20000 AFIX 0 C29 1 0.601282 0.115539 1.099223 10.50000 0.16498 0.11820 = 0.07024 0.00029 -0.06803 -0.03470 AFIX 137 H29A 2 0.661689 0.028477 1.102014 10.50000 -1.50000 H29B 2 0.564592 0.139682 1.173625 10.50000 -1.50000 H29C 2 0.657728 0.179149 1.047189 10.50000 -1.50000 AFIX 0 C30 1 0.544692 -0.128576 1.072961 10.50000 0.05489 0.06994 = 0.05142 -0.02297 -0.02057 0.01595 AFIX 23 H30A 2 0.553635 -0.196311 1.029685 10.50000 -1.20000 H30B 2 0.640639 -0.132763 1.078163 10.50000 -1.20000 AFIX 0 C31 1 0.451130 -0.161509 1.184051 10.50000 0.05517 0.06716 = 0.06466 -0.01567 -0.02152 0.01032 AFIX 137 H31A 2 0.442541 -0.096612 1.228873 10.50000 -1.50000 H31B 2 0.490697 -0.248096 1.218277 10.50000 -1.50000 H31C 2 0.356621 -0.162182 1.180436 10.50000 -1.50000 AFIX 0 C24 1 0.355841 0.015216 0.997370 10.50000 0.07701 0.09765 = 0.24127 0.05160 -0.09218 -0.01960 AFIX 23 H24A 2 0.285781 0.040750 1.067429 10.50000 -1.20000 H24B 2 0.345776 0.090811 0.937786 10.50000 -1.20000 AFIX 0 C25 1 0.307552 -0.088239 0.974457 10.50000 0.11783 0.14689 = 0.16788 0.06899 -0.10042 -0.07001 AFIX 137 H25A 2 0.302477 -0.161189 1.036869 10.50000 -1.50000 H25B 2 0.374806 -0.118281 0.906230 10.50000 -1.50000 H25C 2 0.212723 -0.055201 0.964780 10.50000 -1.50000 AFIX 0 C26 1 0.605744 0.019228 0.894483 10.50000 0.11549 0.07576 = 0.04686 -0.02808 -0.01022 0.03105 AFIX 23 H26A 2 0.701856 0.001752 0.903545 10.50000 -1.20000 H26B 2 0.603984 -0.050203 0.856995 10.50000 -1.20000 AFIX 0 C27 1 0.592046 0.142448 0.818055 10.50000 0.10547 0.08040 = 0.06101 -0.01803 -0.02353 0.02530 AFIX 137 H27A 2 0.670504 0.137026 0.748239 10.50000 -1.50000 H27B 2 0.595785 0.213382 0.851822 10.50000 -1.50000 H27C 2 0.500650 0.159704 0.802766 10.50000 -1.50000 AFIX 0 PART 0 H3 2 0.000000 0.500000 1.000000 10.50000 0.08589 PART 1 O14 5 0.524260 0.404302 0.935834 10.50000 0.06952 0.06840 = 0.08005 -0.02340 -0.02115 -0.00425 C34 1 0.398196 0.495575 0.955459 10.50000 0.07236 0.05287 = 0.12201 -0.01906 -0.04484 -0.01251 AFIX 23 H34A 2 0.319904 0.456490 0.955359 10.50000 -1.20000 H34B 2 0.408427 0.571531 0.894432 10.50000 -1.20000 AFIX 0 C32 1 0.359628 0.541310 1.064424 10.50000 0.05901 0.06520 = 0.09922 -0.01446 -0.00446 -0.01119 AFIX 23 H32A 2 0.271056 0.608322 1.074551 10.50000 -1.20000 H32B 2 0.342807 0.467156 1.126593 10.50000 -1.20000 AFIX 0 PART 2 O13 5 0.462497 0.378889 1.054101 10.50000 0.10362 0.10678 = 0.16619 0.04719 -0.05642 -0.05159 C35 1 0.437972 0.563422 0.922365 10.50000 0.17456 0.13761 = 0.19303 0.05496 -0.13958 -0.06511 AFIX 23 H35A 2 0.363689 0.635523 0.902420 10.50000 -1.20000 H35B 2 0.490819 0.522107 0.855438 10.50000 -1.20000 AFIX 0 C33 1 0.371370 0.474766 1.001373 10.50000 0.10531 0.09604 = 0.31622 0.06780 -0.11765 -0.04342 AFIX 23 H33A 2 0.326123 0.430674 0.967518 10.50000 -1.20000 H33B 2 0.294405 0.520442 1.058562 10.50000 -1.20000 AFIX 0 C15 1 0.688998 0.333512 0.430018 10.50000 0.13574 0.06869 = 0.08760 -0.02929 0.00155 -0.04861 AFIX 137 H15A 2 0.607134 0.361106 0.492573 10.50000 -1.50000 H15B 2 0.731581 0.409197 0.385658 10.50000 -1.50000 H15C 2 0.760219 0.267967 0.458586 10.50000 -1.50000 AFIX 0 O7 5 0.642150 0.278171 0.361430 10.50000 0.03978 0.03875 = 0.04359 -0.00737 -0.00114 -0.00103 PART 1 O10 5 0.820608 0.468826 0.644624 10.25000 0.06402 0.06302 = 0.08712 -0.03270 -0.02806 0.01358 O9 5 0.748011 0.385419 0.488687 10.25000 0.06710 0.06295 = 0.07354 -0.03553 -0.01103 0.00620 C17 1 0.670639 0.496433 0.650862 10.25000 0.06902 0.06275 = 0.07635 -0.02870 -0.02141 0.01026 AFIX 23 H17A 2 0.620951 0.426873 0.702692 10.25000 -1.20000 H17B 2 0.621969 0.581239 0.675776 10.25000 -1.20000 AFIX 0 C16 1 0.674306 0.500221 0.537349 10.25000 0.06951 0.06504 = 0.07801 -0.02962 -0.01807 0.01037 AFIX 23 H16A 2 0.574587 0.518662 0.535516 10.25000 -1.20000 H16B 2 0.719192 0.574521 0.489595 10.25000 -1.20000 AFIX 0 C19 1 0.885928 0.346904 0.504767 10.25000 0.06771 0.05913 = 0.07935 -0.03121 -0.00603 0.01255 AFIX 23 H19A 2 0.949676 0.397624 0.441985 10.25000 -1.20000 H19B 2 0.919569 0.254449 0.494465 10.25000 -1.20000 AFIX 0 C18 1 0.914156 0.355419 0.603305 10.25000 0.06923 0.06521 = 0.09220 -0.02600 -0.02051 0.01344 AFIX 23 H18A 2 0.896272 0.276315 0.659827 10.25000 -1.20000 H18B 2 1.014992 0.363034 0.585653 10.25000 -1.20000 AFIX 0 PART 3 O11 5 0.741104 0.402822 0.479698 10.25000 0.06881 0.06011 = 0.07300 -0.03015 -0.00854 0.00766 C20 1 0.637055 0.480325 0.556957 10.25000 0.06718 0.06599 = 0.07602 -0.02894 -0.01800 0.01082 AFIX 23 H20A 2 0.564277 0.428706 0.607319 10.25000 -1.20000 H20B 2 0.588377 0.557561 0.515925 10.25000 -1.20000 AFIX 0 C23 1 0.825383 0.305696 0.540174 10.25000 0.06803 0.05961 = 0.08018 -0.02959 -0.00976 0.00863 AFIX 23 H23A 2 0.914974 0.272411 0.484547 10.25000 -1.20000 H23B 2 0.773344 0.232200 0.574225 10.25000 -1.20000 AFIX 0 C22 1 0.866277 0.335959 0.628649 10.25000 0.06359 0.06254 = 0.08826 -0.03043 -0.01698 0.01295 AFIX 23 H22A 2 0.887819 0.253077 0.678298 10.25000 -1.20000 H22B 2 0.955753 0.371003 0.593313 10.25000 -1.20000 AFIX 0 C21 1 0.702079 0.523078 0.622363 10.25000 0.07293 0.06650 = 0.08352 -0.03232 -0.02717 0.01563 AFIX 23 H21A 2 0.777256 0.570931 0.570094 10.25000 -1.20000 H21B 2 0.628310 0.586357 0.666357 10.25000 -1.20000 AFIX 0 O12 5 0.763883 0.426769 0.696573 10.25000 0.06905 0.06770 = 0.09062 -0.02997 -0.02788 0.01693 HKLF 4 REM cc2_36b_a.res in P-1 REM wR2 = 0.1999, GooF = S = 1.064, Restrained GooF = 1.036 for all data REM R1 = 0.0679 for 4672 Fo > 4sig(Fo) and 0.0727 for all 5262 data REM 459 parameters refined using 419 restraints END WGHT 0.1206 1.2732 REM Instructions for potential hydrogen bonds EQIV $3 x, y, z-1 HTAB O6 O3_$3 EQIV $4 x+1, y, z HTAB O8 O6_$4 HTAB O8 O9 EQIV $5 -x, -y, -z+1 HTAB C13 O2_$5 EQIV $6 x, y, z+1 HTAB C29 O4_$6 EQIV $7 -x, -y+1, -z+2 HTAB O3 O3_$7 REM Highest difference peak 0.725, deepest hole -0.998, 1-sigma level 0.089 Q1 1 1.0998 0.3949 0.4955 11.00000 0.05 0.73 Q2 1 0.8647 0.5168 0.5768 11.00000 0.05 0.71 Q3 1 0.9014 0.4556 0.5010 11.00000 0.05 0.67 Q4 1 0.5356 0.3946 0.3489 11.00000 0.05 0.64 Q5 1 0.3740 -0.0613 0.4970 11.00000 0.05 0.62 ; _shelx_res_checksum 21431 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu1 0.55520(4) 0.10317(4) 0.44807(3) 0.03624(19) Uani d 1 . . O O6 -0.1090(2) 0.2374(3) 0.18088(19) 0.0451(5) Uani d 1 . . H H6 -0.083253 0.289897 0.121568 0.068 Uiso calc 1 . . O O3 -0.0352(3) 0.4006(2) 0.99674(18) 0.0455(5) Uani d 1 . . O O5 0.3102(3) -0.0326(2) 0.46488(19) 0.0430(5) Uani d 1 . . O O8 0.6421(3) 0.2782(2) 0.3614(2) 0.0450(5) Uani d 0.5 A 1 H H8A 0.718610 0.258591 0.306740 0.067 Uiso d 1 . . H H8B 0.693510 0.293540 0.397200 0.067 Uiso d 0.5 A 1 O O2 0.3211(2) 0.0083(2) 0.66128(18) 0.0424(5) Uani d 1 . . O O1 0.4181(3) 0.1857(2) 0.5731(2) 0.0520(6) Uani d 1 . . O O4 0.4064(3) 0.1441(3) 0.3743(2) 0.0514(6) Uani d 1 . . C C12 -0.0038(3) 0.2006(3) 0.2307(3) 0.0405(7) Uani d 1 . . C C1 0.3299(3) 0.1261(3) 0.6517(3) 0.0390(7) Uani d 1 . . C C13 -0.0043(4) 0.0848(4) 0.3072(3) 0.0440(7) Uani d 1 . . H H13 -0.075254 0.034120 0.322676 0.053 Uiso calc 1 . . C C2 0.2303(3) 0.2005(3) 0.7402(3) 0.0405(7) Uani d 1 . . C C8 0.3148(3) 0.0736(3) 0.3971(3) 0.0401(7) Uani d 1 . . C C9 0.2033(3) 0.1182(3) 0.3399(3) 0.0397(7) Uani d 1 . . C C5 0.0506(4) 0.3380(3) 0.9122(3) 0.0424(7) Uani d 1 . . C C14 0.0996(4) 0.0446(3) 0.3603(3) 0.0423(7) Uani d 1 . . H H14 0.100262 -0.034953 0.411719 0.051 Uiso calc 1 . . C C3 0.2446(4) 0.3258(3) 0.7414(3) 0.0478(8) Uani d 1 . . H H3A 0.316244 0.365169 0.682944 0.057 Uiso calc 1 . . C C6 0.0339(4) 0.2132(4) 0.9099(3) 0.0494(8) Uani d 1 . . H H6A -0.039305 0.174616 0.967266 0.059 Uiso calc 1 . . C C11 0.0988(4) 0.2758(4) 0.2101(3) 0.0468(8) Uani d 1 . . H H11 0.098196 0.355615 0.158966 0.056 Uiso calc 1 . . C C10 0.2006(4) 0.2342(4) 0.2640(3) 0.0479(8) Uani d 1 . . H H10 0.270647 0.285612 0.249253 0.057 Uiso calc 1 . . C C7 0.1223(4) 0.1456(4) 0.8255(3) 0.0468(8) Uani d 1 . . H H7 0.109673 0.060998 0.825413 0.056 Uiso calc 1 . . C C4 0.1565(4) 0.3940(3) 0.8260(3) 0.0480(8) Uani d 1 . . H H4 0.168138 0.479203 0.825243 0.058 Uiso calc 1 . . N N1 0.5009(17) 0.0024(14) 1.0087(13) 0.0599(19) Uani d 0.5 B -1 C C28 0.4884(15) 0.1146(13) 1.0638(9) 0.098(4) Uani d 0.5 B -1 H H28A 0.473903 0.196396 1.010975 0.117 Uiso calc 0.5 B -1 H H28B 0.401301 0.116172 1.129078 0.117 Uiso calc 0.5 B -1 C C29 0.601(2) 0.1155(18) 1.0992(11) 0.110(5) Uani d 0.5 B -1 H H29A 0.661689 0.028477 1.102014 0.166 Uiso calc 0.5 B -1 H H29B 0.564592 0.139682 1.173625 0.166 Uiso calc 0.5 B -1 H H29C 0.657728 0.179149 1.047189 0.166 Uiso calc 0.5 B -1 C C30 0.5447(9) -0.1286(9) 1.0730(7) 0.061(2) Uani d 0.5 B -1 H H30A 0.553635 -0.196311 1.029685 0.073 Uiso calc 0.5 B -1 H H30B 0.640639 -0.132763 1.078163 0.073 Uiso calc 0.5 B -1 C C31 0.4511(16) -0.162(2) 1.1841(15) 0.065(4) Uani d 0.5 B -1 H H31A 0.442541 -0.096612 1.228873 0.097 Uiso calc 0.5 B -1 H H31B 0.490697 -0.248096 1.218277 0.097 Uiso calc 0.5 B -1 H H31C 0.356621 -0.162182 1.180436 0.097 Uiso calc 0.5 B -1 C C24 0.3558(15) 0.0152(14) 0.9974(18) 0.141(7) Uani d 0.5 B -1 H H24A 0.285781 0.040750 1.067429 0.169 Uiso calc 0.5 B -1 H H24B 0.345776 0.090811 0.937786 0.169 Uiso calc 0.5 B -1 C C25 0.3076(19) -0.0882(17) 0.9745(17) 0.137(8) Uani d 0.5 B -1 H H25A 0.302477 -0.161189 1.036869 0.206 Uiso calc 0.5 B -1 H H25B 0.374806 -0.118281 0.906230 0.206 Uiso calc 0.5 B -1 H H25C 0.212723 -0.055201 0.964780 0.206 Uiso calc 0.5 B -1 C C26 0.6057(15) 0.0192(11) 0.8945(7) 0.090(4) Uani d 0.5 B -1 H H26A 0.701856 0.001752 0.903545 0.107 Uiso calc 0.5 B -1 H H26B 0.603984 -0.050203 0.856995 0.107 Uiso calc 0.5 B -1 C C27 0.592(2) 0.142(2) 0.8181(16) 0.090(7) Uani d 0.5 B -1 H H27A 0.670504 0.137026 0.748239 0.135 Uiso calc 0.5 B -1 H H27B 0.595785 0.213382 0.851822 0.135 Uiso calc 0.5 B -1 H H27C 0.500650 0.159704 0.802766 0.135 Uiso calc 0.5 B -1 H H3 0.000000 0.500000 1.000000 0.09(2) Uiso d 1 . . O O14 0.5243(8) 0.4043(7) 0.9358(6) 0.0728(17) Uani d 0.5 C 1 C C34 0.398(2) 0.4956(17) 0.9555(18) 0.077(4) Uani d 0.5 C 1 H H34A 0.319904 0.456490 0.955359 0.093 Uiso calc 0.5 C 1 H H34B 0.408427 0.571531 0.894432 0.093 Uiso calc 0.5 C 1 C C32 0.3596(13) 0.5413(12) 1.0644(11) 0.080(3) Uani d 0.5 C 1 H H32A 0.271056 0.608322 1.074551 0.096 Uiso calc 0.5 C 1 H H32B 0.342807 0.467156 1.126593 0.096 Uiso calc 0.5 C 1 O O13 0.4625(11) 0.3789(10) 1.0541(10) 0.128(4) Uani d 0.5 D 2 C C35 0.438(2) 0.563(2) 0.9224(19) 0.154(10) Uani d 0.5 D 2 H H35A 0.363689 0.635523 0.902420 0.184 Uiso calc 0.5 D 2 H H35B 0.490819 0.522107 0.855438 0.184 Uiso calc 0.5 D 2 C C33 0.371(4) 0.475(3) 1.001(3) 0.172(18) Uani d 0.5 D 2 H H33A 0.326123 0.430674 0.967518 0.206 Uiso calc 0.5 D 2 H H33B 0.294405 0.520442 1.058562 0.206 Uiso calc 0.5 D 2 C C15 0.6890(17) 0.3335(11) 0.4300(10) 0.098(4) Uani d 0.5 A 2 H H15A 0.607134 0.361106 0.492573 0.148 Uiso calc 0.5 A 2 H H15B 0.731581 0.409197 0.385658 0.148 Uiso calc 0.5 A 2 H H15C 0.760219 0.267967 0.458586 0.148 Uiso calc 0.5 A 2 O O7 0.6421(3) 0.2782(2) 0.3614(2) 0.0450(5) Uani d 0.5 A 2 O O10 0.8206(14) 0.4688(14) 0.6446(14) 0.071(3) Uani d 0.25 E 1 O O9 0.748(3) 0.385(3) 0.489(3) 0.070(3) Uani d 0.25 E 1 C C17 0.6706(18) 0.496(2) 0.6509(17) 0.071(3) Uani d 0.25 E 1 H H17A 0.620951 0.426873 0.702692 0.085 Uiso calc 0.25 E 1 H H17B 0.621969 0.581239 0.675776 0.085 Uiso calc 0.25 E 1 C C16 0.674(3) 0.500(3) 0.5373(18) 0.073(3) Uani d 0.25 E 1 H H16A 0.574587 0.518662 0.535516 0.088 Uiso calc 0.25 E 1 H H16B 0.719192 0.574521 0.489595 0.088 Uiso calc 0.25 E 1 C C19 0.886(2) 0.347(2) 0.5048(18) 0.074(3) Uani d 0.25 E 1 H H19A 0.949676 0.397624 0.441985 0.089 Uiso calc 0.25 E 1 H H19B 0.919569 0.254449 0.494465 0.089 Uiso calc 0.25 E 1 C C18 0.914(2) 0.355(2) 0.6033(19) 0.079(3) Uani d 0.25 E 1 H H18A 0.896272 0.276315 0.659827 0.095 Uiso calc 0.25 E 1 H H18B 1.014992 0.363034 0.585653 0.095 Uiso calc 0.25 E 1 O O11 0.741(4) 0.403(3) 0.480(3) 0.071(3) Uani d 0.25 F 3 C C20 0.637(2) 0.480(3) 0.5570(19) 0.072(3) Uani d 0.25 F 3 H H20A 0.564277 0.428706 0.607319 0.087 Uiso calc 0.25 F 3 H H20B 0.588377 0.557561 0.515925 0.087 Uiso calc 0.25 F 3 C C23 0.825(2) 0.306(2) 0.5402(18) 0.073(3) Uani d 0.25 F 3 H H23A 0.914974 0.272411 0.484547 0.088 Uiso calc 0.25 F 3 H H23B 0.773344 0.232200 0.574225 0.088 Uiso calc 0.25 F 3 C C22 0.866(2) 0.336(2) 0.6286(18) 0.075(3) Uani d 0.25 F 3 H H22A 0.887819 0.253077 0.678298 0.090 Uiso calc 0.25 F 3 H H22B 0.955753 0.371003 0.593313 0.090 Uiso calc 0.25 F 3 C C21 0.702(3) 0.523(2) 0.6224(19) 0.075(3) Uani d 0.25 F 3 H H21A 0.777256 0.570931 0.570094 0.090 Uiso calc 0.25 F 3 H H21B 0.628310 0.586357 0.666357 0.090 Uiso calc 0.25 F 3 O O12 0.7639(17) 0.4268(14) 0.6966(14) 0.078(3) Uani d 0.25 F 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu1 0.0303(3) 0.0357(3) 0.0339(3) 0.00316(18) -0.00424(19) -0.00778(18) O6 0.0370(11) 0.0558(14) 0.0363(11) -0.0026(10) -0.0081(9) -0.0072(10) O3 0.0450(12) 0.0474(13) 0.0348(11) 0.0027(10) -0.0036(9) -0.0149(9) O5 0.0455(12) 0.0401(11) 0.0414(12) -0.0041(9) -0.0159(10) -0.0030(9) O8 0.0398(12) 0.0388(11) 0.0436(12) -0.0010(9) -0.0011(9) -0.0074(9) O2 0.0391(11) 0.0456(12) 0.0363(11) -0.0056(9) -0.0014(9) -0.0134(9) O1 0.0507(14) 0.0361(12) 0.0460(13) 0.0018(10) 0.0092(11) -0.0110(10) O4 0.0393(12) 0.0496(14) 0.0600(15) -0.0088(10) -0.0218(11) 0.0112(11) C12 0.0330(14) 0.0474(17) 0.0339(14) 0.0029(12) -0.0055(12) -0.0119(12) C1 0.0352(15) 0.0411(16) 0.0336(14) 0.0043(12) -0.0074(12) -0.0097(12) C13 0.0429(17) 0.0484(18) 0.0375(16) -0.0086(14) -0.0078(13) -0.0079(13) C2 0.0367(15) 0.0423(16) 0.0353(15) 0.0028(12) -0.0072(12) -0.0097(12) C8 0.0323(14) 0.0415(16) 0.0369(15) 0.0039(12) -0.0040(12) -0.0102(12) C9 0.0342(15) 0.0407(16) 0.0362(15) 0.0015(12) -0.0047(12) -0.0097(12) C5 0.0394(16) 0.0486(17) 0.0323(14) 0.0023(13) -0.0054(12) -0.0134(13) C14 0.0441(17) 0.0410(16) 0.0362(15) -0.0037(13) -0.0082(13) -0.0066(12) C3 0.0461(18) 0.0410(17) 0.0401(17) 0.0031(14) 0.0020(14) -0.0119(13) C6 0.0462(18) 0.056(2) 0.0393(17) -0.0112(15) 0.0013(14) -0.0161(15) C11 0.0387(17) 0.0439(17) 0.0497(18) -0.0009(13) -0.0119(14) -0.0026(14) C10 0.0391(17) 0.0446(18) 0.0539(19) -0.0048(14) -0.0144(15) -0.0001(15) C7 0.0453(18) 0.0514(19) 0.0405(17) -0.0049(15) -0.0052(14) -0.0179(14) C4 0.0484(19) 0.0392(16) 0.0440(17) 0.0002(14) -0.0020(14) -0.0112(13) N1 0.051(3) 0.066(3) 0.056(5) 0.016(2) -0.020(3) -0.020(3) C28 0.140(11) 0.088(7) 0.049(5) -0.015(7) -0.002(6) -0.029(5) C29 0.165(16) 0.118(11) 0.070(7) -0.035(11) -0.068(9) 0.000(7) C30 0.055(4) 0.070(5) 0.051(4) 0.016(4) -0.021(3) -0.023(4) C31 0.055(7) 0.067(8) 0.065(6) 0.010(6) -0.022(5) -0.016(5) C24 0.077(7) 0.098(9) 0.241(18) -0.020(7) -0.092(10) 0.052(10) C25 0.118(12) 0.147(14) 0.168(16) -0.070(12) -0.100(12) 0.069(13) C26 0.115(9) 0.076(6) 0.047(4) 0.031(6) -0.010(5) -0.028(4) C27 0.105(16) 0.080(10) 0.061(7) 0.025(10) -0.024(8) -0.018(6) O14 0.070(4) 0.068(4) 0.080(4) -0.004(3) -0.021(3) -0.023(3) C34 0.072(8) 0.053(8) 0.122(12) -0.013(6) -0.045(9) -0.019(9) C32 0.059(6) 0.065(6) 0.099(8) -0.011(5) -0.004(5) -0.014(6) O13 0.104(7) 0.107(7) 0.166(11) -0.052(6) -0.056(8) 0.047(7) C35 0.17(2) 0.138(15) 0.19(2) -0.065(15) -0.140(18) 0.055(15) C33 0.105(17) 0.096(15) 0.32(5) -0.043(13) -0.12(2) 0.07(2) C15 0.136(11) 0.069(7) 0.088(8) -0.049(7) 0.002(7) -0.029(6) O7 0.0398(12) 0.0388(11) 0.0436(12) -0.0010(9) -0.0011(9) -0.0074(9) O10 0.064(5) 0.063(5) 0.087(6) 0.014(4) -0.028(4) -0.033(5) O9 0.067(5) 0.063(6) 0.074(5) 0.006(4) -0.011(4) -0.036(5) C17 0.069(5) 0.063(6) 0.076(6) 0.010(5) -0.021(5) -0.029(5) C16 0.070(6) 0.065(6) 0.078(5) 0.010(5) -0.018(5) -0.030(5) C19 0.068(5) 0.059(6) 0.079(6) 0.013(5) -0.006(5) -0.031(5) C18 0.069(6) 0.065(6) 0.092(6) 0.013(5) -0.021(5) -0.026(5) O11 0.069(5) 0.060(6) 0.073(5) 0.008(4) -0.009(4) -0.030(5) C20 0.067(6) 0.066(6) 0.076(5) 0.011(5) -0.018(5) -0.029(5) C23 0.068(6) 0.060(6) 0.080(6) 0.009(5) -0.010(5) -0.030(5) C22 0.064(6) 0.063(6) 0.088(6) 0.013(5) -0.017(5) -0.030(5) C21 0.073(5) 0.067(6) 0.084(6) 0.016(5) -0.027(5) -0.032(5) O12 0.069(5) 0.068(6) 0.091(6) 0.017(4) -0.028(5) -0.030(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O5 Cu1 Cu1 2_656 2_656 84.72(7) ? O5 Cu1 O8 2_656 . 96.44(10) ? O5 Cu1 O4 2_656 . 169.41(10) ? O5 Cu1 O7 2_656 . 96.44(10) ? O8 Cu1 Cu1 . 2_656 178.59(7) ? O2 Cu1 Cu1 2_656 2_656 84.69(7) ? O2 Cu1 O5 2_656 2_656 88.27(10) ? O2 Cu1 O8 2_656 . 96.14(9) ? O2 Cu1 O1 2_656 . 169.50(10) ? O2 Cu1 O4 2_656 . 90.21(11) ? O2 Cu1 O7 2_656 . 96.14(9) ? O1 Cu1 Cu1 . 2_656 84.85(8) ? O1 Cu1 O5 . 2_656 89.95(11) ? O1 Cu1 O8 . . 94.34(10) ? O1 Cu1 O4 . . 89.64(12) ? O1 Cu1 O7 . . 94.34(10) ? O4 Cu1 Cu1 . 2_656 84.70(8) ? O4 Cu1 O8 . . 94.14(10) ? O4 Cu1 O7 . . 94.14(10) ? C12 O6 H6 . . 109.5 ? C5 O3 H3 . . 114.8(2) ? C8 O5 Cu1 . 2_656 122.7(2) ? Cu1 O8 H8A . . 109.4 ? Cu1 O8 H8B . . 109.6 ? H8A O8 H8B . . 90.7 ? C1 O2 Cu1 . 2_656 122.8(2) ? C1 O1 Cu1 . . 122.5(2) ? C8 O4 Cu1 . . 122.7(2) ? O6 C12 C13 . . 117.3(3) ? O6 C12 C11 . . 122.6(3) ? C11 C12 C13 . . 120.1(3) ? O2 C1 C2 . . 117.8(3) ? O1 C1 O2 . . 125.1(3) ? O1 C1 C2 . . 117.1(3) ? C12 C13 H13 . . 120.4 ? C14 C13 C12 . . 119.2(3) ? C14 C13 H13 . . 120.4 ? C3 C2 C1 . . 120.6(3) ? C3 C2 C7 . . 118.4(3) ? C7 C2 C1 . . 120.9(3) ? O5 C8 C9 . . 117.2(3) ? O4 C8 O5 . . 125.1(3) ? O4 C8 C9 . . 117.7(3) ? C14 C9 C8 . . 120.8(3) ? C14 C9 C10 . . 118.4(3) ? C10 C9 C8 . . 120.8(3) ? O3 C5 C6 . . 119.6(3) ? O3 C5 C4 . . 121.7(3) ? C4 C5 C6 . . 118.7(3) ? C13 C14 C9 . . 121.3(3) ? C13 C14 H14 . . 119.3 ? C9 C14 H14 . . 119.3 ? C2 C3 H3A . . 119.4 ? C4 C3 C2 . . 121.2(3) ? C4 C3 H3A . . 119.4 ? C5 C6 H6A . . 119.6 ? C7 C6 C5 . . 120.8(3) ? C7 C6 H6A . . 119.6 ? C12 C11 H11 . . 120.1 ? C10 C11 C12 . . 119.7(3) ? C10 C11 H11 . . 120.1 ? C9 C10 H10 . . 119.3 ? C11 C10 C9 . . 121.3(3) ? C11 C10 H10 . . 119.3 ? C2 C7 H7 . . 119.7 ? C6 C7 C2 . . 120.6(3) ? C6 C7 H7 . . 119.7 ? C5 C4 H4 . . 119.9 ? C3 C4 C5 . . 120.2(3) ? C3 C4 H4 . . 119.9 ? C28 N1 C24 . . 105.1(13) ? C30 N1 C28 . . 113.5(12) ? C30 N1 C24 . . 110.9(12) ? C26 N1 C28 . . 108.9(11) ? C26 N1 C30 . . 109.8(11) ? C26 N1 C24 . . 108.4(14) ? N1 C28 H28A . . 108.0 ? N1 C28 H28B . . 108.0 ? H28A C28 H28B . . 107.2 ? C29 C28 N1 . . 117.2(13) ? C29 C28 H28A . . 108.0 ? C29 C28 H28B . . 108.0 ? C28 C29 H29A . . 109.5 ? C28 C29 H29B . . 109.5 ? C28 C29 H29C . . 109.5 ? H29A C29 H29B . . 109.5 ? H29A C29 H29C . . 109.5 ? H29B C29 H29C . . 109.5 ? N1 C30 H30A . . 108.2 ? N1 C30 H30B . . 108.2 ? H30A C30 H30B . . 107.3 ? C31 C30 N1 . . 116.6(10) ? C31 C30 H30A . . 108.2 ? C31 C30 H30B . . 108.2 ? C30 C31 H31A . . 109.5 ? C30 C31 H31B . . 109.5 ? C30 C31 H31C . . 109.5 ? H31A C31 H31B . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? N1 C24 H24A . . 106.3 ? N1 C24 H24B . . 106.3 ? H24A C24 H24B . . 106.4 ? C25 C24 N1 . . 124.1(13) ? C25 C24 H24A . . 106.3 ? C25 C24 H24B . . 106.3 ? C24 C25 H25A . . 109.5 ? C24 C25 H25B . . 109.5 ? C24 C25 H25C . . 109.5 ? H25A C25 H25B . . 109.5 ? H25A C25 H25C . . 109.5 ? H25B C25 H25C . . 109.5 ? N1 C26 H26A . . 107.2 ? N1 C26 H26B . . 107.2 ? H26A C26 H26B . . 106.9 ? C27 C26 N1 . . 120.4(12) ? C27 C26 H26A . . 107.2 ? C27 C26 H26B . . 107.2 ? C26 C27 H27A . . 109.5 ? C26 C27 H27B . . 109.5 ? C26 C27 H27C . . 109.5 ? H27A C27 H27B . . 109.5 ? H27A C27 H27C . . 109.5 ? H27B C27 H27C . . 109.5 ? C34 O14 C32 . 2_667 110.4(10) ? O14 C34 H34A . . 109.2 ? O14 C34 H34B . . 109.2 ? O14 C34 C32 . . 112.2(14) ? H34A C34 H34B . . 107.9 ? C32 C34 H34A . . 109.2 ? C32 C34 H34B . . 109.2 ? O14 C32 C34 2_667 . 108.5(11) ? O14 C32 H32A 2_667 . 110.0 ? O14 C32 H32B 2_667 . 110.0 ? C34 C32 H32A . . 110.0 ? C34 C32 H32B . . 110.0 ? H32A C32 H32B . . 108.4 ? C33 O13 C35 . 2_667 111.5(16) ? O13 C35 H35A 2_667 . 107.6 ? O13 C35 H35B 2_667 . 107.6 ? H35A C35 H35B . . 107.0 ? C33 C35 H35A . . 107.6 ? C33 C35 H35B . . 107.6 ? O13 C33 H33A . . 108.8 ? O13 C33 H33B . . 108.8 ? C35 C33 O13 . . 114(2) ? C35 C33 H33A . . 108.8 ? C35 C33 H33B . . 108.8 ? H33A C33 H33B . . 107.7 ? H15A C15 H15B . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? O7 C15 H15A . . 109.5 ? O7 C15 H15B . . 109.5 ? O7 C15 H15C . . 109.5 ? Cu1 O7 H8A . . 109.4 ? C15 O7 Cu1 . . 113.1(5) ? C15 O7 H8A . . 104.8 ? C18 O10 C17 . . 120.7(17) ? C19 O9 C16 . . 109(2) ? O10 C17 H17A . . 111.0 ? O10 C17 H17B . . 111.0 ? H17A C17 H17B . . 109.0 ? C16 C17 O10 . . 103.7(17) ? C16 C17 H17A . . 111.0 ? C16 C17 H17B . . 111.0 ? O9 C16 C17 . . 117(3) ? O9 C16 H16A . . 108.1 ? O9 C16 H16B . . 108.1 ? C17 C16 H16A . . 108.1 ? C17 C16 H16B . . 108.1 ? H16A C16 H16B . . 107.3 ? O9 C19 H19A . . 106.2 ? O9 C19 H19B . . 106.2 ? O9 C19 C18 . . 124.3(19) ? H19A C19 H19B . . 106.4 ? C18 C19 H19A . . 106.2 ? C18 C19 H19B . . 106.2 ? O10 C18 C19 . . 107.2(16) ? O10 C18 H18A . . 110.3 ? O10 C18 H18B . . 110.3 ? C19 C18 H18A . . 110.3 ? C19 C18 H18B . . 110.3 ? H18A C18 H18B . . 108.5 ? C20 O11 C23 . . 107(2) ? O11 C20 H20A . . 109.4 ? O11 C20 H20B . . 109.4 ? O11 C20 C21 . . 111(2) ? H20A C20 H20B . . 108.0 ? C21 C20 H20A . . 109.4 ? C21 C20 H20B . . 109.4 ? O11 C23 H23A . . 106.9 ? O11 C23 H23B . . 106.9 ? O11 C23 C22 . . 121.6(19) ? H23A C23 H23B . . 106.7 ? C22 C23 H23A . . 106.9 ? C22 C23 H23B . . 106.9 ? C23 C22 H22A . . 108.1 ? C23 C22 H22B . . 108.1 ? H22A C22 H22B . . 107.3 ? O12 C22 C23 . . 117.0(16) ? O12 C22 H22A . . 108.1 ? O12 C22 H22B . . 108.1 ? C20 C21 H21A . . 107.8 ? C20 C21 H21B . . 107.8 ? H21A C21 H21B . . 107.2 ? O12 C21 C20 . . 118(2) ? O12 C21 H21A . . 107.8 ? O12 C21 H21B . . 107.8 ? C21 O12 C22 . . 105.2(17) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cu1 Cu1 2_656 2.6010(9) ? Cu1 O5 2_656 1.965(2) ? Cu1 O8 . 2.172(2) ? Cu1 O2 2_656 1.960(2) ? Cu1 O1 . 1.963(2) ? Cu1 O4 . 1.967(2) ? Cu1 O7 . 2.172(2) ? O6 H6 . 0.8400 ? O6 C12 . 1.365(4) ? O3 C5 . 1.344(4) ? O3 H3 . 1.223(3) ? O5 C8 . 1.263(4) ? O8 H8A . 0.8704 ? O8 H8B . 0.8746 ? O2 C1 . 1.264(4) ? O1 C1 . 1.264(4) ? O4 C8 . 1.259(4) ? C12 C13 . 1.393(5) ? C12 C11 . 1.393(5) ? C1 C2 . 1.484(4) ? C13 H13 . 0.9500 ? C13 C14 . 1.382(5) ? C2 C3 . 1.394(5) ? C2 C7 . 1.396(5) ? C8 C9 . 1.486(5) ? C9 C14 . 1.391(5) ? C9 C10 . 1.391(5) ? C5 C6 . 1.401(5) ? C5 C4 . 1.394(5) ? C14 H14 . 0.9500 ? C3 H3A . 0.9500 ? C3 C4 . 1.383(5) ? C6 H6A . 0.9500 ? C6 C7 . 1.379(5) ? C11 H11 . 0.9500 ? C11 C10 . 1.371(5) ? C10 H10 . 0.9500 ? C7 H7 . 0.9500 ? C4 H4 . 0.9500 ? N1 C28 . 1.501(14) ? N1 C30 . 1.500(13) ? N1 C24 . 1.501(14) ? N1 C26 . 1.496(14) ? C28 H28A . 0.9900 ? C28 H28B . 0.9900 ? C28 C29 . 1.380(15) ? C29 H29A . 0.9800 ? C29 H29B . 0.9800 ? C29 H29C . 0.9800 ? C30 H30A . 0.9900 ? C30 H30B . 0.9900 ? C30 C31 . 1.443(14) ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C24 H24A . 0.9900 ? C24 H24B . 0.9900 ? C24 C25 . 1.449(15) ? C25 H25A . 0.9800 ? C25 H25B . 0.9800 ? C25 H25C . 0.9800 ? C26 H26A . 0.9900 ? C26 H26B . 0.9900 ? C26 C27 . 1.459(15) ? C27 H27A . 0.9800 ? C27 H27B . 0.9800 ? C27 H27C . 0.9800 ? O14 C34 . 1.39(2) ? O14 C32 2_667 1.442(15) ? C34 H34A . 0.9900 ? C34 H34B . 0.9900 ? C34 C32 . 1.50(2) ? C32 H32A . 0.9900 ? C32 H32B . 0.9900 ? O13 C35 2_667 1.46(2) ? O13 C33 . 1.42(3) ? C35 H35A . 0.9900 ? C35 H35B . 0.9900 ? C35 C33 . 1.34(3) ? C33 H33A . 0.9900 ? C33 H33B . 0.9900 ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C15 O7 . 1.437(13) ? O7 H8A . 0.8704 ? O10 C17 . 1.454(14) ? O10 C18 . 1.430(14) ? O9 C16 . 1.434(15) ? O9 C19 . 1.431(16) ? C17 H17A . 0.9900 ? C17 H17B . 0.9900 ? C17 C16 . 1.453(17) ? C16 H16A . 0.9900 ? C16 H16B . 0.9900 ? C19 H19A . 0.9900 ? C19 H19B . 0.9900 ? C19 C18 . 1.433(17) ? C18 H18A . 0.9900 ? C18 H18B . 0.9900 ? O11 C20 . 1.426(16) ? O11 C23 . 1.436(16) ? C20 H20A . 0.9900 ? C20 H20B . 0.9900 ? C20 C21 . 1.449(17) ? C23 H23A . 0.9900 ? C23 H23B . 0.9900 ? C23 C22 . 1.476(17) ? C22 H22A . 0.9900 ? C22 H22B . 0.9900 ? C22 O12 . 1.439(14) ? C21 H21A . 0.9900 ? C21 H21B . 0.9900 ? C21 O12 . 1.417(15) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cu1 O5 C8 O4 2_656 . . . 2.4(5) ? Cu1 O5 C8 C9 2_656 . . . -177.73(19) ? Cu1 O2 C1 O1 2_656 . . . -0.7(5) ? Cu1 O2 C1 C2 2_656 . . . -179.9(2) ? Cu1 O1 C1 O2 . . . . 1.9(5) ? Cu1 O1 C1 C2 . . . . -179.0(2) ? Cu1 O4 C8 O5 . . . . -3.2(5) ? Cu1 O4 C8 C9 . . . . 177.0(2) ? O6 C12 C13 C14 . . . . -179.4(3) ? O6 C12 C11 C10 . . . . 179.1(3) ? O3 C5 C6 C7 . . . . -178.6(3) ? O3 C5 C4 C3 . . . . 178.8(3) ? O5 C8 C9 C14 . . . . -0.5(4) ? O5 C8 C9 C10 . . . . 180.0(3) ? O2 C1 C2 C3 . . . . 172.9(3) ? O2 C1 C2 C7 . . . . -5.7(5) ? O1 C1 C2 C3 . . . . -6.4(5) ? O1 C1 C2 C7 . . . . 175.0(3) ? O4 C8 C9 C14 . . . . 179.4(3) ? O4 C8 C9 C10 . . . . -0.2(5) ? C12 C13 C14 C9 . . . . 0.8(5) ? C12 C11 C10 C9 . . . . -0.4(6) ? C1 C2 C3 C4 . . . . -177.2(3) ? C1 C2 C7 C6 . . . . 177.4(3) ? C13 C12 C11 C10 . . . . 1.1(5) ? C2 C3 C4 C5 . . . . -0.1(6) ? C8 C9 C14 C13 . . . . -179.7(3) ? C8 C9 C10 C11 . . . . 179.5(3) ? C5 C6 C7 C2 . . . . -0.2(6) ? C14 C9 C10 C11 . . . . 0.0(5) ? C3 C2 C7 C6 . . . . -1.2(5) ? C6 C5 C4 C3 . . . . -1.3(6) ? C11 C12 C13 C14 . . . . -1.3(5) ? C10 C9 C14 C13 . . . . -0.2(5) ? C7 C2 C3 C4 . . . . 1.4(6) ? C4 C5 C6 C7 . . . . 1.5(6) ? C28 N1 C30 C31 . . . . 59.9(19) ? C28 N1 C24 C25 . . . . -164.0(17) ? C28 N1 C26 C27 . . . . -51(2) ? C30 N1 C28 C29 . . . . 49.3(17) ? C30 N1 C24 C25 . . . . -41(2) ? C30 N1 C26 C27 . . . . -175.9(17) ? C24 N1 C28 C29 . . . . 170.7(13) ? C24 N1 C30 C31 . . . . -58.1(19) ? C24 N1 C26 C27 . . . . 63(2) ? C26 N1 C28 C29 . . . . -73.3(16) ? C26 N1 C30 C31 . . . . -177.9(15) ? C26 N1 C24 C25 . . . . 80(2) ? O14 C34 C32 O14 . . . 2_667 57.8(17) ? C32 O14 C34 C32 2_667 . . . -58.8(18) ? O13 C35 C33 O13 2_667 . . . -46(5) ? C35 O13 C33 C35 2_667 . . . 42(5) ? O10 C17 C16 O9 . . . . 58(4) ? O9 C19 C18 O10 . . . . -34(3) ? C17 O10 C18 C19 . . . . 45(3) ? C16 O9 C19 C18 . . . . 38(4) ? C19 O9 C16 C17 . . . . -50(4) ? C18 O10 C17 C16 . . . . -57(3) ? O11 C20 C21 O12 . . . . -66(4) ? O11 C23 C22 O12 . . . . 35(4) ? C20 O11 C23 C22 . . . . -38(4) ? C20 C21 O12 C22 . . . . 56(3) ? C23 O11 C20 C21 . . . . 49(4) ? C23 C22 O12 C21 . . . . -39(3) ?