#------------------------------------------------------------------------------ #$Date: 2024-06-28 04:46:00 +0300 (Fri, 28 Jun 2024) $ #$Revision: 292633 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/25/2312528.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312528 _cell_angle_alpha 94.141 _cell_angle_beta 97.381 _cell_angle_gamma 111.957 _cell_length_a 11.7657 _cell_length_b 14.1033 _cell_length_c 14.9728 _exptl_crystal_F_000 1028.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file yd30432_Ru29dmphensup3.hkl _cod_data_source_block 2_Ru29dmphen _shelx_title ' SIR92 run in space group P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 264.42 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 23804.89 17160.57 5405.90 o 2 0 0 5345.89 4260.37 93.41 o 3 0 0 16799.16 16254.01 864.61 o 4 0 0 879.59 891.37 38.72 o 5 0 0 619.56 530.75 41.65 o 6 0 0 1162.73 1061.54 90.76 o 7 0 0 9.18 13.14 5.37 o 8 0 0 41.26 57.47 25.70 o 9 0 0 172.70 199.26 48.30 o 10 0 0 51.35 72.15 24.47 o 11 0 0 7.65 10.04 31.83 o 12 0 0 1.01 18.83 34.06 o -13 1 0 4.85 -35.27 38.15 o -12 1 0 1.51 -28.83 28.83 o -11 1 0 69.64 31.82 14.58 o -10 1 0 373.54 357.60 70.28 o -9 1 0 531.87 497.43 82.82 o -8 1 0 220.14 285.36 53.39 o -7 1 0 444.84 402.42 92.53 o -6 1 0 741.01 758.99 60.20 o -5 1 0 923.06 1047.28 56.48 o -4 1 0 6591.30 6431.27 122.81 o -3 1 0 69916.29 62733.88 840.05 o -2 1 0 1734.77 2093.97 68.86 o -1 1 0 2932.13 3374.29 177.21 o 1 1 0 15554.70 16205.44 315.96 o 2 1 0 89.46 77.50 11.35 o 3 1 0 3724.71 3866.24 144.22 o 4 1 0 2423.26 2778.77 204.46 o 5 1 0 3186.15 3377.91 160.01 o 6 1 0 1331.65 1108.90 102.87 o 7 1 0 25.70 47.22 25.31 o 8 1 0 97.33 141.34 41.86 o 9 1 0 0.08 -13.85 22.34 o 10 1 0 224.80 304.56 103.32 o 11 1 0 179.01 168.97 80.84 o 12 1 0 8.24 -59.03 59.03 o -13 2 0 0.87 -49.25 49.25 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