#------------------------------------------------------------------------------ #$Date: 2024-08-07 01:02:34 +0300 (Wed, 07 Aug 2024) $ #$Revision: 293980 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312529.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312529 loop_ _publ_author_name 'Wysocki, Waldemar' 'Kamecka, Anna' 'Karczmarzyk, Zbigniew' _publ_section_title ; Synthesis and structural characterizations of three carbonyl(α-diimine)hydrido(triphenylphosphine)ruthenium(II) complexes with derivatives of 1,10-phenanthroline. ; _journal_coeditor_code YD3043 _journal_issue 'Pt 7' _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_page_first 319 _journal_page_last 330 _journal_paper_doi 10.1107/S2053229624005898 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Ru H (C14 H12 N2) (C18 H15 P)2 (C O)] P F6' _chemical_formula_moiety 'C51 H43 N2 O P2 Ru +, F6 P -' _chemical_formula_sum 'C51 H43 F6 N2 O P3 Ru' _chemical_formula_weight 1007.85 _chemical_name_systematic 'Carbonylhydrido(4,7-dimethyl-1,10-phenanthroline-\k^2^N,N)bis(triphenylphosphane-\kP)ruthenium(II) hexafluoridophosphate' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary difmap _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 109.266(6) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.9624(8) _cell_length_b 21.9572(7) _cell_length_c 17.1148(9) _cell_measurement_reflns_used 6785 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 27.7630 _cell_measurement_theta_min 2.2900 _cell_volume 5307.9(5) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) ; _computing_publication_material ; SHELXL2014 (Sheldrick, 2015) and WinGX (Farrugia, 2012) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS2013 (Sheldrick, 2008) ; _diffrn_ambient_temperature 298(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.861 _diffrn_measurement_device_type 'KM4 CCD four-circle' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0343 _diffrn_reflns_av_unetI/netI 0.0558 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 25375 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.792 _diffrn_reflns_theta_min 2.393 _exptl_absorpt_coefficient_mu 0.442 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.69833 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlis PRO (Rigaku OD, 2022) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.261 _exptl_crystal_description needle _exptl_crystal_F_000 2056 _exptl_crystal_size_max 0.40 _exptl_crystal_size_mid 0.10 _exptl_crystal_size_min 0.10 _refine_diff_density_max 0.463 _refine_diff_density_min -0.702 _refine_ls_extinction_coef 0.00095(16) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method ; SHELXL2014 (Sheldrick, 2015) ; _refine_ls_goodness_of_fit_ref 1.036 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 638 _refine_ls_number_reflns 11913 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.036 _refine_ls_R_factor_all 0.0709 _refine_ls_R_factor_gt 0.0473 _refine_ls_shift/su_max 0.005 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0530P)^2^+3.0506P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1105 _refine_ls_wR_factor_ref 0.1253 _reflns_number_gt 8859 _reflns_number_total 11913 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yd3043sup1.cif _cod_data_source_block 3_Ru47dmphen _cod_depositor_comments 'Adding full bibliography for 2312527--2312529.cif.' _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2312529 _cod_database_fobs_code 2312529 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 0 0 2 2007.47 51.5151 2 0 0 -2 2019.13 51.8896 2 0 0 3 9.42081 9.54239 2 0 0 -3 5.75807 10.4941 2 0 0 4 2194.32 77.0245 2 0 0 -4 2086.14 76.0208 2 0 0 -5 2.55570 18.4550 2 0 0 5-4.27029 14.7803 2 0 0 6 8453.64 185.174 2 0 0 -6 7692.53 178.195 2 0 0 -7-16.8854 28.2138 2 0 0 -8 23423.5 361.870 2 0 0 -9-4.26656 33.2589 2 0 0 -10 19803.5 383.879 2 0 0 -11 37.4873 31.0507 2 0 0 -12 7126.51 260.089 2 0 0 -13-11.9041 38.0026 2 0 0 -14 3248.76 193.826 2 0 0 -15-43.1431 49.4717 2 0 0 -16 3395.20 220.020 2 0 0 -17 5.51471 42.0407 2 0 0 -18 2109.89 192.531 2 0 0 -19-27.2068 48.0801 2 0 0 -20 1264.91 160.352 2 0 -1 -2 31.0023 9.77624 2 0 1 -2 23.6552 7.52608 2 0 1 2 27.4890 8.83494 2 0 -1 2 33.5669 9.20728 2 0 -1 -3 14122.2 174.779 2 0 1 3 13475.9 175.464 2 0 1 -3 14122.6 161.681 2 0 -1 3 14048.3 161.495 2 0 1 4 39.2287 15.6687 2 0 -1 4 54.9384 16.4684 2 0 -1 -4 46.9342 17.6961 2 0 1 -4 43.2113 18.0289 2 0 1 5 1459.67 72.0840 2 0 -1 -5 1337.68 70.8631 2 0 1 -5 1382.69 68.8732 2 0 -1 5 1487.85 69.0093 2 0 -1 -6 589.890 53.2210 2 0 1 6 712.622 55.7423 2 0 1 -6 673.213 52.8692 2 0 -1 6 696.266 53.6215 2 0 -1 -7 1041.29 74.3641 2 0 1 -7 1021.11 72.2072 2 0 -1 -8 205.589 42.9373 2 0 1 -8 268.750 44.1436 2 0 -1 -9 250.289 45.5533 2 0 1 -9 207.968 40.8598 2 0 -1 -10 165.862 47.6035 2 0 1 -10 165.527 42.3378 2 0 1 -11-15.1736 33.5884 2 0 -1 -11 9.35837 35.7855 2 0 1 -12 35.3605 33.0722 2 0 -1 -12 47.1333 35.6039 2 0 1 -13 17.4507 41.9399 2 0 -1 -13-27.2922 44.1240 2 0 -1 -14 1632.51 140.274 2 0 1 -14 1579.11 135.756 2 0 -1 -15 1143.28 125.533 2 0 1 -15 1181.16 126.592 2 0 -1 -16 63.1146 47.4544 2 0 1 -16-81.5354 62.3167 2 0 -1 -17 497.503 101.603 2 0 1 -17 350.747 88.8500 2 0 1 -18 33.7307 50.3881 2 0 -1 -18 60.8500 46.1238 2 0 1 -19 392.166 95.9712 2 0 -1 -19 252.067 88.8637 2 0 -1 -20 11.7460 63.3305 2 0 1 -20-36.4856 70.8481 2 0 1 -21 5.55049 61.7100 2 0 -2 0 11.4835 37.3825 3 0 -2 -1 16.2286 56.8071 2 0 2 1-0.02543 30.3894 2 0 2 -1 291.125 21.7702 3 0 -2 1 417.246 55.5676 3 0 2 -2 6054.44 99.8903 1 0 2 -2 892.779 64.0640 3 0 -2 2 5976.44 99.4493 3 0 2 -2 3113.58 91.2903 2 0 2 -3 1379.99 43.4427 3 0 -2 -3 1402.17 58.3428 2 0 2 3 1289.04 55.8567 2 0 2 -3 1364.99 49.1797 2 0 -2 3 1315.48 49.2540 2 0 2 4 19740.0 241.963 2 0 2 -4 19463.0 218.513 2 0 -2 4 19458.2 216.198 2 0 2 -4 19667.6 180.756 3 0 -2 -4 19089.2 242.760 2 0 -2 5 33802.1 325.151 2 0 -2 -5 33765.3 355.566 2 0 2 -5 33446.2 323.944 2 0 2 5 33776.8 354.375 2 0 -2 6 1353.53 72.5240 2 0 -2 -6 1357.01 78.8569 2 0 2 -6 1350.38 73.4027 2 0 2 -7 16427.6 275.604 2 0 -2 -7 15737.8 290.341 2 0 -2 -8 3289.33 143.763 2 0 2 -8 3542.42 138.941 2 0 2 -9 14106.3 298.113 2 0 -2 -9 13990.9 309.932 2 0 2 -10 3899.02 165.787 2 0 -2 -10 3784.55 173.512 2 0 -2 -11 9104.35 279.497 2 0 2 -11 9390.72 273.688 2 0 2 -12 539.505 70.4551 2 0 -2 -12 536.341 75.3924 2 0 2 -13 3408.19 185.640 2 0 -2 -13 3375.78 193.067 2 0 2 -14 1239.78 120.485 2 0 -2 -14 1362.79 128.711 2 0 2 -15 2718.37 187.056 2 0 -2 -15 2675.25 189.659 2 0 -2 -16-9.92687 44.3520 2 0 2 -16-6.48575 53.7900 2 0 2 -17 2854.62 209.883 2 0 -2 -17 2851.95 213.355 2 0 -2 -18 472.319 96.9689 2 0 2 -18 429.421 104.415 2 0 2 -19 1997.26 199.212 2 0 -2 -19 1827.90 183.809 2 0 2 -20 188.747 90.9658 2 0 -2 -20 129.691 72.5698 2 0 2 -21 552.858 118.291 2 0 -3 0 29.3621 9.17999 3 0 -3 -1 6038.86 92.8204 2 0 -3 1 6352.37 92.8619 3 0 3 -1 6054.94 92.6599 3 0 -3 2 1616.83 45.5816 2 0 3 -2 1723.22 45.5037 2 0 -3 2 1663.17 49.9168 3 0 3 -2 1664.21 49.6588 3 0 3 -2 1561.07 43.6591 1 0 3 2 1581.45 55.8192 2 0 -3 2 1616.65 43.5564 1 0 -3 -2 1504.75 55.1894 2 0 3 -3 3667.47 78.5516 3 0 -3 3 3720.52 81.6356 2 0 -3 -3 3731.08 99.5313 2 0 3 -3 3804.97 82.3120 2 0 3 3 3563.28 94.3527 2 0 -3 3 3715.99 79.4177 3 0 3 -3 3572.99 78.6877 1 0 3 -4 5575.41 102.606 3 0 3 4 5314.95 128.900 2 0 -3 -4 5576.48 136.371 2 0 -3 4 5495.09 113.913 2 0 3 -4 5547.27 116.948 2 0 3 -4 5298.37 108.600 1 0 3 -5 26.8473 12.3038 3 0 -3 5 35.6458 16.1912 2 0 3 -5-2.92078 15.8955 2 0 3 5 14.4610 14.5240 2 0 -3 -5-3.89596 19.5624 2 0 3 -6 275.820 35.8367 2 0 3 -6 281.157 28.1474 3 0 -3 -6 218.538 36.9265 2 0 -3 6 271.326 31.9602 2 0 3 -7 1015.58 53.8683 3 0 3 -7 1047.17 70.7067 2 0 -3 7 1048.77 68.0681 2 0 -3 -7 924.477 73.9719 2 0 3 -8 4411.66 118.519 3 0 3 -8 4364.64 153.750 2 0 -3 -8 4301.52 165.970 2 0 3 -9 10.2357 17.5854 3 0 3 -9 7.24996 27.2748 2 0 -3 -9-38.5500 44.9896 2 0 -3 -10 4679.99 194.203 2 0 3 -10 4732.99 184.331 2 0 3 -10 4770.21 137.791 3 0 -3 -11 442.075 70.7687 2 0 3 -11 446.694 67.5129 2 0 3 -12 88.8187 38.0930 2 0 -3 -12 159.164 41.0335 2 0 3 -13 79.1433 36.6899 2 0 -3 -13 32.8764 37.8380 2 0 -3 -14 166.534 54.0174 2 0 3 -14 213.179 61.2902 2 0 3 -15 490.701 88.0130 2 0 -3 -15 529.795 91.8285 2 0 3 -16 53.5175 49.0394 2 0 -3 -16 42.6347 44.5112 2 0 -3 -17 110.603 55.0132 2 0 3 -17 224.776 73.8891 2 0 -3 -18 1321.46 159.221 2 0 3 -18 1276.82 150.791 2 0 -3 -19 43.0031 46.7077 2 0 3 -19-74.8063 74.5809 2 0 -3 -20 19.3257 50.8986 2 0 3 -20 80.9737 72.0486 2 0 3 -21-28.0828 48.3942 2 0 -4 0 11334.3 143.845 3 0 4 -1 146.671 12.6969 1 0 -4 1 138.565 12.1080 1 0 4 -1 151.512 18.5690 3 0 -4 -1 161.240 17.2434 2 0 -4 1 165.016 19.9317 3 0 -4 2 47553.8 302.254 3 0 -4 2 48142.6 247.121 1 0 4 2 48703.4 325.423 2 0 -4 2 46435.8 256.258 2 0 4 -2 48062.3 246.474 1 0 4 -2 48716.2 299.523 3 0 -4 -2 46960.9 324.573 2 0 -4 3 28.2629 10.8701 1 0 -4 3 19.3949 13.1125 3 0 -4 -3 33.0483 16.4683 2 0 4 -3 61.3192 15.5454 2 0 -4 3 46.8026 13.4842 2 0 4 -3 41.8193 11.2563 1 0 4 3 61.2614 15.6542 2 0 4 -3 33.4961 14.4168 3 0 4 -4 8984.11 141.355 1 0 4 -4 8914.71 144.922 2 0 -4 -4 8785.28 179.489 2 0 -4 4 8593.85 140.617 3 0 4 4 8805.91 174.568 2 0 4 -4 8560.61 139.995 3 0 -4 4 8969.47 145.841 2 0 4 5 7167.39 167.996 2 0 4 -5 6796.22 139.084 1 0 -4 5 7024.21 144.067 2 0 4 -5 6987.50 130.542 3 0 -4 -5 6791.97 172.521 2 0 4 -5 7139.25 151.604 2 0 -4 6 8187.28 171.340 2 0 4 -6 8152.98 148.782 3 0 4 -6 8002.41 173.937 2 0 4 -6 7798.57 163.689 1 0 -4 -6 7597.02 195.982 2 0 -4 -7 3642.46 145.272 2 0 4 -7 3708.74 128.566 2 0 -4 7 3755.34 127.417 2 0 4 -7 3680.71 106.037 3 0 4 -8 8666.28 214.045 2 0 4 -8 8835.17 172.204 3 0 -4 -8 8632.17 238.693 2 0 4 -9 9044.42 181.965 3 0 4 -9 8938.11 232.915 2 0 -4 -9 8266.32 249.530 2 0 4 -10 5508.66 195.866 2 0 -4 -10 5055.53 206.816 2 0 4 -10 5553.33 150.336 3 0 4 -11 7646.60 244.945 2 0 -4 -11 7142.99 257.773 2 0 4 -12-18.5066 40.4517 2 0 -4 -12 19.6871 37.4874 2 0 -4 -13 2097.30 153.798 2 0 4 -13 2130.98 150.183 2 0 -4 -14 5215.71 253.618 2 0 4 -14 5089.96 238.697 2 0 -4 -15 305.649 73.3521 2 0 4 -15 373.856 74.4352 2 0 -4 -16 1383.50 148.740 2 0 4 -16 1317.27 136.066 2 0 4 -17 1302.58 151.186 2 0 -4 -17 1199.63 142.944 2 0 -4 -18 711.761 119.088 2 0 4 -18 865.869 126.114 2 0 4 -19 961.345 137.534 2 0 -4 -19 810.138 127.493 2 0 4 -20 168.899 70.3852 2 0 -4 -20 129.466 75.0912 2 0 4 -21 547.191 112.832 2 0 -5 0 29.5193 16.0387 3 0 -5 1 40315.3 303.764 3 0 -5 1 38794.7 209.763 1 0 5 -1 40324.5 299.783 3 0 -5 2 7022.62 105.114 2 0 -5 2 6817.24 97.5039 1 0 5 -2 6921.29 95.9032 1 0 -5 -2 7069.54 135.469 2 0 -5 2 6847.94 128.857 3 0 5 -2 7208.48 127.874 3 0 5 -3 578.712 33.9075 2 0 -5 -3 527.215 42.6172 2 0 -5 3 567.145 38.7666 3 0 5 3 615.090 44.3158 2 0 -5 3 512.568 31.6729 1 0 5 -3 560.535 33.3536 1 0 -5 3 606.589 35.2667 2 0 5 -3 598.314 38.4412 3 0 5 -4 1352.65 56.3473 1 0 5 -4 1352.01 59.1397 3 0 -5 -4 1347.51 74.1683 2 0 5 4 1420.43 71.7321 2 0 -5 4 1365.05 60.5804 3 0 5 -4 1442.86 59.5882 2 0 -5 4 1419.41 57.9166 2 0 5 -5 36.3641 14.1307 3 0 5 -5 35.5146 15.8733 2 0 -5 5 21.8267 12.0884 3 0 -5 -5 48.6354 26.5442 2 0 5 -5 28.7382 12.8150 1 0 -5 5 44.9397 13.8349 2 0 -5 6 1008.86 59.7074 2 0 5 -6 1172.00 64.3815 1 0 -5 -6 1039.55 77.3483 2 0 5 -6 1042.36 64.2771 2 0 5 -6 1071.43 58.5580 3 0 5 -7 1521.52 83.3302 2 0 -5 -7 1379.29 94.6394 2 0 5 -7 1545.52 71.8682 3 0 -5 7 1505.83 80.5720 2 0 5 -8 1648.43 94.2898 2 0 -5 -8 1515.80 103.620 2 0 5 -8 1633.90 77.0847 3 0 5 -9 92.2416 20.6008 3 0 -5 -9 94.6886 32.8040 2 0 5 -9 106.041 35.5518 2 0 5 -10 1721.55 113.515 2 0 -5 -10 1767.97 124.787 2 0 -5 -11 2127.10 142.596 2 0 5 -11 2017.22 129.921 2 0 5 -12 848.047 91.3963 2 0 -5 -12 788.814 96.9746 2 0 -5 -13 177.540 64.9393 2 0 5 -13 197.695 59.9920 2 0 5 -14 492.692 81.0196 2 0 -5 -14 489.239 84.8772 2 0 -5 -15 210.891 62.9625 2 0 5 -15 186.225 50.9602 2 0 5 -16 7.67810 40.7760 2 0 -5 -16-23.3103 45.9510 2 0 -5 -17 84.8586 57.6962 2 0 5 -17 194.563 66.0601 2 0 -5 -18 47.3815 45.2615 2 0 5 -18 137.836 47.2670 2 0 5 -19 353.597 80.0083 2 0 -5 -19 99.5068 84.5790 2 0 5 -20-46.8368 55.5465 2 0 -5 -20-25.3000 54.2490 2 0 5 -21 129.314 51.4666 2 0 -6 0 37979.0 253.222 1 0 -6 0 39278.6 329.802 3 0 6 -1 4452.90 109.276 3 0 -6 1 4336.79 111.245 3 0 6 -1 4185.79 77.3371 1 0 -6 1 4242.81 76.2073 1 0 6 -2 7790.51 144.629 3 0 -6 -2 7247.15 146.688 2 0 -6 2 7225.75 104.941 1 0 -6 2 7218.40 114.858 2 0 6 -2 7128.03 102.679 1 0 -6 2 7401.63 145.383 3 0 -6 3 1594.50 55.8900 1 0 6 -3 1707.84 69.4307 3 0 -6 -3 1544.64 73.8644 2 0 -6 3 1595.44 57.6896 2 0 6 -3 1656.72 55.6744 1 0 -6 3 1647.09 70.1639 3 0 -6 -4 5656.93 156.274 2 0 6 -4 5619.05 117.855 2 0 6 -4 5993.44 130.184 3 0 -6 4 5757.20 118.104 1 0 -6 4 5641.33 133.485 3 0 -6 4 6043.81 122.364 2 0 6 -4 5840.78 119.246 1 0 6 4 5862.04 151.554 2 0 -6 -5 1297.88 82.3067 2 0 6 -5 1355.79 62.6293 1 0 6 -5 1242.83 61.7739 2 0 -6 5 1225.80 65.0066 3 0 6 -5 1334.57 65.6745 3 0 -6 5 1396.15 64.6946 2 0 -6 6 2215.42 88.2372 2 0 -6 -6 2151.98 112.880 2 0 6 -6 2182.61 84.5737 3 0 6 -6 2104.48 87.8005 2 0 -6 6 2037.11 86.7407 3 0 6 -6 1962.79 82.8285 1 0 6 -7 4938.05 132.207 3 0 -6 -7 4644.48 175.137 2 0 -6 7 4854.56 142.432 2 0 6 -7 4848.16 145.657 2 0 6 -8 11817.9 246.218 2 0 6 -8 12227.4 216.729 3 0 -6 -8 11667.4 289.395 2 0 6 -9 1212.33 87.2395 2 0 -6 -9 1111.25 98.0070 2 0 -6 -10 2119.48 139.681 2 0 6 -10 2319.46 128.213 2 0 -6 -11 226.283 55.7979 2 0 6 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0 -7 4 5500.46 120.561 2 0 -7 -5 2928.76 126.519 2 0 -7 5 2916.87 105.832 3 0 7 -5 3053.28 98.6123 2 0 7 -5 3165.24 97.8243 1 0 7 -5 3156.35 105.350 3 0 -7 5 2979.96 95.4584 2 0 -7 6 2191.72 95.4102 3 0 7 -6 2142.48 88.9291 2 0 7 -6 2256.39 90.8690 1 0 -7 6 2327.62 91.3428 2 0 -7 -6 2276.45 119.811 2 0 7 -6 2353.98 94.4230 3 0 -7 7 58.5241 21.2981 2 0 7 -7 74.6281 26.3904 3 0 7 -7 62.1773 20.6797 2 0 -7 -7 64.0339 32.4372 2 0 7 -8 134.535 34.1641 2 0 -7 -8 114.882 34.3106 2 0 7 -9 117.545 33.3799 2 0 -7 -9 76.6874 39.5279 2 0 -7 -10 602.813 77.8560 2 0 7 -10 716.268 73.2907 2 0 7 -11 480.975 66.0654 2 0 -7 -11 406.732 69.9570 2 0 7 -12-18.6610 40.6345 2 0 -7 -12-62.9383 53.3714 2 0 7 -13 191.343 52.7398 2 0 -7 -13 113.304 47.7262 2 0 7 -14-14.0675 42.6918 2 0 -7 -14 14.3161 34.9334 2 0 -7 -15 229.483 70.8760 2 0 7 -15 432.265 75.6047 2 0 -7 -16 8.10162 49.7228 2 0 7 -16 104.004 54.6441 2 0 -7 -17 147.228 56.3072 2 0 7 -17 212.511 59.3148 2 0 7 -18 387.762 84.9171 2 0 -7 -18 373.661 91.3338 2 0 7 -19 57.0582 40.3046 2 0 -7 -19 98.1545 60.5452 2 0 7 -20-43.9957 39.6102 2 0 -8 0 340.790 39.2968 3 0 -8 0 363.608 30.3414 1 0 -8 1 20936.6 282.019 3 0 -8 1 20172.8 196.835 1 0 -8 -1 21132.1 283.101 3 0 -8 2 209.480 32.3645 3 0 -8 -2 164.247 28.1160 2 0 8 -2 225.412 29.2923 3 0 8 -2 185.019 20.0332 1 0 -8 2 212.468 20.3387 1 0 -8 3 18241.8 267.158 3 0 -8 -3 17935.2 269.939 2 0 -8 3 17521.1 210.600 2 0 8 -3 19660.5 264.433 3 0 8 -3 17714.6 192.145 1 0 -8 3 17948.9 200.015 1 0 -8 -4 2643.19 113.342 2 0 -8 4 2552.41 104.787 3 0 -8 4 2691.86 85.4848 2 0 -8 4 2598.81 82.6424 1 0 8 -4 2828.39 101.745 3 0 8 -4 2731.37 83.9683 1 0 -8 5 1804.72 88.0701 3 0 -8 5 1882.31 76.8715 2 0 -8 -5 1956.31 107.456 2 0 8 -5 1826.95 75.2915 2 0 8 -5 1896.66 75.7289 1 0 -8 6 56.6436 16.4775 2 0 8 -6 6.65924 19.0307 2 0 -8 6-14.2865 20.7444 3 0 -8 -6 22.1778 22.7931 2 0 8 -6 17.5547 15.4517 1 0 -8 -7 9983.39 266.365 2 0 -8 7 10140.3 205.078 2 0 8 -7 9677.36 204.577 2 0 -8 7 9106.67 209.293 3 0 -8 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40.3945 2 0 -9 4 490.019 37.4453 1 0 -9 -4 507.323 55.1346 2 0 9 -4 533.932 36.5964 1 0 -9 4 511.428 50.8670 3 0 9 -5 11.5949 12.8336 1 0 -9 5 10.2006 14.5662 1 0 -9 -5 47.3033 28.9596 2 0 -9 5 14.8513 15.0827 2 0 -9 5-4.37649 24.1243 3 0 -9 6 1467.84 73.2338 2 0 9 -6 1540.51 73.3143 1 0 -9 6 1318.33 82.2874 3 0 9 -6 1310.38 71.7318 2 0 -9 -6 1371.04 100.423 2 0 -9 7 1262.58 82.6297 3 0 -9 7 1293.91 73.2876 2 0 -9 -7 1240.94 99.3001 2 0 9 -7 1342.48 78.3637 2 0 9 -8 702.199 61.9319 2 0 -9 -8 775.516 84.0059 2 0 -9 -9 432.213 65.8334 2 0 9 -9 441.367 52.0131 2 0 -9 -10 35.6799 35.9606 2 0 9 -10 98.3597 32.3175 2 0 -9 -11 36.8084 38.7579 2 0 9 -11 65.3092 29.4974 2 0 -9 -12 109.363 49.9500 2 0 9 -12 103.115 48.3047 2 0 9 -13 497.211 70.5757 2 0 -9 -13 496.284 85.0167 2 0 9 -14 29.3582 31.2023 2 0 -9 -14-30.3693 56.8759 2 0 9 -15 51.8575 40.3332 2 0 -9 -15 5.82355 59.4803 2 0 -9 -16 97.4302 55.3387 2 0 9 -16 254.048 63.9316 2 0 -9 -17 28.3978 43.9761 2 0 9 -17-3.61056 44.1240 2 0 -9 -18 244.592 76.0224 2 0 9 -18 391.716 92.2800 2 0 -9 -19 59.9617 61.2234 2 0 -10 0 6401.19 176.858 3 0 -10 0 6635.14 134.967 1 0 -10 -1 6449.22 176.590 3 0 -10 1 6014.60 121.013 1 0 -10 1 6545.86 177.778 3 0 -10 2 28530.8 259.707 1 0 -10 -2 28535.9 350.804 2 0 -10 -2 29115.8 377.897 3 0 -10 2 28689.8 375.658 3 0 -10 3 5696.10 170.814 3 0 -10 3 5830.82 122.576 1 0 -10 3 5844.71 132.623 2 0 10 -3 5434.17 112.557 1 0 -10 -3 5581.03 164.344 2 0 -10 4 1909.48 77.9768 2 0 -10 4 1806.31 99.7624 3 0 10 -4 1739.78 67.9504 1 0 -10 4 1810.28 72.6780 1 0 -10 -4 1794.69 101.464 2 0 -10 5 1941.00 82.8562 1 0 -10 -5 1970.23 112.271 2 0 -10 5 2098.69 86.0289 2 0 10 -5 1992.53 78.9115 1 0 -10 5 1892.78 102.772 3 0 10 -6 11084.8 202.831 1 0 -10 6 10336.6 240.176 3 0 -10 6 10523.6 199.669 2 0 -10 -6 10671.0 276.237 2 0 -10 7 425.126 43.1331 2 0 -10 -7 372.245 59.6593 2 0 -10 7 359.385 48.4117 3 0 10 -7 410.461 45.9861 2 0 -10 8 3444.34 145.195 3 0 -10 -8 3413.49 174.745 2 0 10 -8 3590.72 133.987 2 0 10 -9 1957.77 108.960 2 0 -10 -9 2028.19 140.827 2 0 10 -10 2000.71 114.741 2 0 -10 -10 1975.82 145.896 2 0 -10 -11 4815.11 236.218 2 0 10 -11 4625.28 183.783 2 0 10 -12 1285.37 102.539 2 0 -10 -12 1296.89 130.809 2 0 -10 -13 916.592 114.795 2 0 10 -13 881.922 91.0665 2 0 -10 -14 1874.51 167.937 2 0 10 -14 2050.75 148.409 2 0 10 -15 206.652 51.0989 2 0 -10 -15 156.368 65.1513 2 0 10 -16 1717.34 145.268 2 0 -10 -16 1683.25 174.352 2 0 10 -17 365.902 77.2914 2 0 -10 -17 114.012 67.4905 2 0 -10 -18 586.817 117.607 2 0 -11 0 4.48058 11.3068 1 0 -11 0-5.97745 29.9504 3 0 -11 -1 15.8729 24.7440 3 0 -11 1-18.4967 31.1444 3 0 -11 1-0.54133 12.8573 1 0 -11 -1-18.6073 17.3330 2 0 -11 2 694.366 66.1063 3 0 -11 2 698.390 43.4502 1 0 -11 -2 683.090 64.6635 3 0 -11 -2 664.947 58.2748 2 0 -11 3 280.857 29.4498 1 0 -11 3 287.083 30.5486 2 0 11 -3 295.345 28.8202 1 0 -11 -3 287.555 40.5203 2 0 -11 3 322.175 48.6731 3 0 11 -4 1288.35 59.2409 1 0 -11 4 1374.77 69.0834 2 0 -11 4 1324.84 89.8841 3 0 -11 -4 1339.67 91.5757 2 0 -11 4 1333.92 63.8346 1 0 11 -5 454.336 38.4862 1 0 -11 5 535.742 44.7053 1 0 -11 -5 513.913 61.0732 2 0 -11 5 500.696 57.7747 3 0 -11 5 523.798 44.2620 2 0 11 -6 227.128 30.8077 1 0 -11 6 222.070 32.7417 2 0 -11 -6 207.077 50.7003 2 0 -11 6 208.383 38.5135 3 0 -11 -7 31.6533 30.5141 2 0 -11 7 1.13617 24.1957 3 0 -11 7-4.90193 19.5894 2 0 -11 8 1645.23 105.627 3 0 -11 -8 1680.55 126.682 2 0 11 -9 529.095 57.2200 2 0 -11 -9 511.488 74.6081 2 0 -11 -10 179.313 60.6697 2 0 11 -10 241.139 46.7485 2 0 -11 -11 214.723 60.4188 2 0 11 -11 292.032 54.1138 2 0 -11 -12 354.607 75.1382 2 0 11 -12 374.009 64.0072 2 0 11 -13-14.1797 34.9362 2 0 -11 -13-24.0584 51.5819 2 0 -11 -14-54.0089 61.4598 2 0 11 -14 38.6865 35.7629 2 0 -11 -15 203.643 65.4727 2 0 11 -15 259.823 62.3489 2 0 -11 -16 77.8162 51.4109 2 0 11 -16 141.590 52.1717 2 0 -11 -17-65.0846 49.9159 2 0 -11 -18 101.680 70.9378 2 0 -12 0 3812.01 111.257 1 0 -12 0 3619.86 147.965 3 0 -12 -1 30.8804 30.1169 3 0 -12 -1 49.3188 21.3608 2 0 -12 1 56.1056 13.9107 1 0 -12 1 35.3778 27.9654 3 0 -12 -2 3310.00 143.100 3 0 -12 2 3356.31 97.8852 1 0 -12 2 3220.58 142.014 3 0 -12 -2 3303.39 129.025 2 0 -12 -3 1327.83 92.9275 3 0 -12 3 1480.53 73.3551 2 0 -12 3 1489.37 67.6247 1 0 -12 -3 1388.53 90.5537 2 0 12 -3 1471.89 63.5971 1 0 -12 3 1315.91 94.2465 3 0 -12 4 15807.7 241.776 2 0 -12 4 16298.5 230.057 1 0 -12 4 15922.5 319.306 3 0 -12 -4 15645.0 313.128 2 0 12 -4 15160.8 208.225 1 0 -12 5 1265.88 70.0764 2 0 -12 5 1358.62 71.4182 1 0 -12 5 1270.13 93.0420 3 0 12 -5 1292.25 65.1145 1 0 -12 -5 1283.72 97.9890 2 0 12 -6 1640.14 79.0504 1 0 -12 6 1612.68 81.2331 2 0 -12 6 1579.63 106.108 3 0 -12 -6 1526.12 113.402 2 0 -12 -7 2588.60 151.959 2 0 -12 7 2413.21 131.171 3 0 -12 7 2425.79 102.411 2 0 -12 8 4903.48 186.809 3 0 -12 -8 5304.36 226.700 2 0 -12 9 251.199 50.1431 3 0 -12 -9 351.583 68.4922 2 0 -12 -10 5381.57 247.356 2 0 12 -10 5135.76 181.805 2 0 -12 -11 11.9156 35.4486 2 0 12 -11 50.6712 26.6819 2 0 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223.257 3 0 -14 -4 200.015 42.4242 2 0 14 -4 188.704 27.4751 1 0 -14 4 211.554 32.0671 2 0 -14 4 173.906 44.5777 3 0 -14 -4 185.806 46.2309 3 0 -14 4 212.199 29.6555 1 0 -14 5 7650.86 173.088 1 0 14 -5 7215.51 156.140 1 0 -14 5 7153.09 237.379 3 0 -14 -5 7222.78 239.723 2 0 -14 5 7361.24 176.663 2 0 -14 6 136.552 36.9556 3 0 -14 -6 163.221 50.7662 2 0 14 -6 174.694 28.8060 1 0 -14 6 186.192 32.6156 2 0 -14 -7 3691.24 189.304 2 0 -14 7 3651.07 174.665 3 0 -14 -8 33.2517 29.3589 2 0 -14 8 44.1391 33.7522 3 0 -14 -9 3789.46 208.388 2 0 -14 9 3640.59 178.188 3 0 -14 -10 783.775 100.389 2 0 -14 -11 1865.44 157.431 2 0 -14 -12 363.374 83.2990 2 0 -14 -13 3515.81 234.115 2 0 -14 -14 189.864 68.6105 2 0 -14 -15 3234.76 242.671 2 0 -14 -16 493.636 108.125 2 0 -14 -17 763.965 132.817 2 0 -15 0-24.2629 21.7371 2 0 -15 0 11.6621 15.7194 1 0 -15 0 14.9979 32.9246 3 0 -15 -1 2420.87 105.051 1 0 -15 -1 2431.17 141.271 3 0 -15 1 2473.12 96.5967 1 0 -15 1 2319.09 137.533 3 0 -15 -1 2427.79 117.072 2 0 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85.7031 64.8234 2 0 -15 -17 128.874 73.6213 2 0 -16 0 851.580 61.1431 1 0 -16 0 755.839 84.5613 3 0 -16 0 798.674 66.7034 2 0 -16 1 689.489 81.6656 3 0 -16 -1 657.970 57.9749 1 0 -16 -1 678.756 82.2009 3 0 -16 1 673.705 51.9550 1 0 -16 -1 678.227 64.8040 2 0 -16 -2 7196.96 198.675 1 0 -16 -2 7281.02 251.459 3 0 -16 2 7530.96 171.157 1 0 -16 -2 7271.09 216.716 2 0 -16 2 7226.68 250.605 3 0 -16 3 1269.03 109.848 3 0 -16 3 1338.68 80.7937 2 0 -16 -3 1375.20 98.7612 2 0 -16 3 1495.30 76.9014 1 0 -16 -3 1313.70 109.440 3 0 -16 -4 5856.51 215.660 2 0 -16 4 5919.69 153.775 1 0 -16 -4 5429.40 218.696 3 0 -16 4 5824.09 230.051 3 0 -16 5 381.314 41.2573 1 0 -16 -5 374.527 63.1753 3 0 -16 5 331.143 61.0909 3 0 -16 -5 333.381 58.2956 2 0 -16 6 3386.58 181.403 3 0 -16 -6 3649.70 188.153 2 0 -16 -6 3657.33 182.933 3 0 -16 6 3888.69 132.139 1 0 -16 7 857.560 96.5828 3 0 -16 -7 808.237 97.9203 2 0 -16 -7 837.202 95.4559 3 0 -16 8 187.934 49.9095 3 0 -16 -8 220.913 58.9520 2 0 -16 9 73.0555 40.1533 3 0 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0 27161.6 207.322 1 -1 4 -1 2104.62 66.6470 3 1 -4 1 2097.63 67.7931 3 -1 4 -1 1996.60 57.3756 1 1 -4 1 2006.67 58.1466 1 1 -4 2 21803.0 208.419 1 1 -4 2 21808.3 226.541 3 -1 4 -2 22099.2 138.452 2 -1 4 -2 22348.5 209.675 1 -1 4 -2 23392.8 229.506 3 -1 -4 -3 10.5999 15.2100 2 -1 4 -3 29.3589 11.6412 2 -1 4 -3 22.4348 12.0658 1 1 -4 3 21.7189 8.06068 2 1 -4 3 27.3953 14.3022 3 1 -4 3 24.1535 12.5466 1 -1 4 -3 30.8932 13.4624 3 1 -4 4 5227.80 125.336 1 -1 4 -4 5420.27 109.247 2 -1 4 -4 5865.87 127.625 3 -1 -4 -4 5291.78 144.741 2 -1 4 -4 5485.32 125.572 1 1 -4 4 5490.41 108.842 2 -1 -4 -5 2775.03 116.268 2 -1 4 -5 2740.11 89.6791 2 -1 4 -5 3047.66 96.9946 3 -1 4 -5 2836.76 97.6991 1 1 -4 5 2862.08 91.1310 2 -1 4 -6 526.609 47.3167 2 1 -4 6 468.337 41.9097 2 -1 -4 -6 520.845 58.9337 2 -1 4 -6 582.977 48.6582 3 -1 -4 -7 3662.63 151.460 2 -1 4 -7 3854.92 122.432 3 1 -4 7 3610.69 126.989 2 -1 4 -7 3664.94 126.917 2 -1 4 -8 4039.03 130.531 3 -1 4 -8 3911.56 142.972 2 -1 -4 -8 3860.55 165.810 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108.989 1 -1 -5 -4 3672.58 123.971 2 1 -5 4 3985.07 90.1646 2 -1 5 -4 4049.98 112.611 3 1 -5 4 3815.36 109.466 1 1 -5 4 3865.80 112.496 3 -1 5 -5 252.243 27.5384 2 -1 5 -5 272.289 30.4300 1 -1 5 -5 319.760 34.4722 3 -1 -5 -5 303.251 42.0629 2 1 -5 5 272.592 27.4307 2 -1 5 -6 248.868 33.7579 2 1 -5 6 192.463 27.1105 2 -1 5 -6 224.080 28.9369 3 -1 -5 -6 270.416 47.4166 2 -1 5 -7 518.565 47.8286 3 1 -5 7 434.209 43.0730 2 -1 5 -7 487.329 51.8668 2 -1 -5 -7 377.209 54.6831 2 -1 5 -8 101.066 29.9488 2 -1 -5 -8 89.6903 30.9533 2 -1 -5 -9 5269.21 208.432 2 -1 5 -9 5465.26 181.404 2 -1 5 -10 1719.44 111.878 2 -1 -5 -10 1594.31 120.600 2 -1 -5 -11 1669.78 131.827 2 -1 5 -11 1837.79 122.874 2 -1 5 -12 7466.34 256.672 2 -1 -5 -12 6632.41 273.745 2 -1 5 -13 1862.38 139.217 2 -1 -5 -13 1679.05 145.686 2 -1 -5 -14 100.745 56.6120 2 -1 5 -14 61.9747 44.3739 2 -1 5 -15 2932.17 192.840 2 -1 -5 -15 2757.48 199.563 2 -1 -5 -16-15.6134 47.3382 2 -1 5 -16 127.849 58.8257 2 -1 5 -17 1359.36 151.412 2 -1 -5 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129.420 2 2 5 -8 2661.95 126.048 2 2 5 -8 2617.80 75.1610 3 -2 -5 7 3817.54 93.8078 3 2 -5 -7 4068.76 151.241 2 2 5 -7 4030.89 142.798 2 2 5 -7 4013.33 90.0151 3 -2 -5 6 5.64862 20.4197 2 -2 -5 6 14.0333 9.91036 3 2 5 -6 0.62651 10.9745 3 2 5 -6-2.79507 24.5348 2 2 -5 -6-25.9291 26.5015 2 2 -5 -5 1991.41 92.0258 2 -2 -5 5 2263.45 95.0944 2 2 -5 -5 2051.46 73.3124 3 -2 5 5 2297.99 95.2302 2 2 5 -5 2235.09 94.6822 2 -2 -5 5 2107.01 67.3354 3 -2 5 4 6486.50 146.951 2 2 -5 -4 5993.17 142.711 2 2 -5 -4 6075.06 124.377 3 -2 -5 4 6074.77 114.324 3 -2 -5 4 6421.02 151.493 2 -2 -5 3 1727.25 74.4812 2 2 -5 -3 1604.45 64.5547 3 2 -5 -3 1556.27 65.6526 2 -2 5 3 1651.26 65.8102 2 -2 5 2 1568.18 56.0153 2 -2 5 2 1607.82 64.7546 3 2 -5 -2 1659.23 65.9638 3 2 -5 -2 1566.25 56.1957 2 2 -5 -1 550.754 40.8829 1 2 -5 -1 609.827 41.4270 3 -2 5 1 557.075 38.2504 3 -2 5 1 511.597 26.2963 2 2 -5 -1 541.071 27.0417 2 2 -5 0 41509.6 345.074 3 -2 5 0 41060.2 333.191 3 -2 5 0 39672.5 308.736 1 2 -5 0 41273.4 319.932 1 2 -5 1 27037.3 287.245 3 -2 5 -1 28253.9 287.365 3 2 -5 1 26501.3 262.376 1 -2 5 -1 27517.2 262.016 1 2 -5 2 4677.12 114.942 1 2 -5 2 4736.85 126.231 3 -2 5 -2 4920.75 116.664 1 -2 5 -2 4943.83 125.540 3 -2 5 -3 5775.29 88.8929 2 -2 5 -3 6066.35 145.191 3 2 -5 3 5915.51 138.895 1 -2 5 -3 6208.41 139.978 1 2 -5 3 5513.43 88.0247 2 2 -5 4 1936.32 61.9717 2 -2 -5 -4 2038.31 100.536 2 -2 5 -4 2052.19 65.3774 2 -2 5 -4 2175.54 90.2199 1 2 -5 4 1994.28 88.6937 1 -2 5 -4 2222.70 91.6852 3 2 -5 5 1993.01 74.3167 2 2 -5 5 2026.79 95.9948 1 -2 5 -5 2141.88 94.1789 3 -2 -5 -5 2082.13 106.837 2 -2 5 -5 2120.76 79.2669 2 -2 5 -6 5230.39 137.280 2 -2 -5 -6 5282.71 180.644 2 2 -5 6 5281.86 135.547 2 2 -5 7 2115.41 95.2647 2 -2 5 -7 2062.09 96.2689 2 -2 -5 -7 2060.67 123.203 2 -2 -5 -8 9077.66 267.842 2 -2 5 -8 8731.11 213.798 2 -2 5 -9 4797.02 170.709 2 -2 -5 -9 4522.63 198.426 2 -2 5 -10 973.656 86.2736 2 -2 -5 -10 975.991 98.5592 2 -2 -5 -11 1715.00 135.104 2 -2 5 -11 1856.19 124.319 2 -2 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31.8684 2 -2 -7 -4 598.378 60.3878 2 -2 7 -4 584.370 33.5594 2 2 -7 4 565.418 54.9779 3 2 -7 5 2813.71 115.948 1 2 -7 5 2857.82 83.4367 2 -2 7 -5 2838.19 84.6748 2 -2 -7 -5 2868.23 134.868 2 -2 7 -6 45.7992 16.9443 2 2 -7 6 66.8453 23.6252 1 -2 -7 -6 46.6723 29.8035 2 2 -7 6 85.7185 18.2633 2 -2 -7 -7 6412.54 221.226 2 -2 7 -7 6431.48 163.023 2 2 -7 7 6427.18 159.237 2 -2 7 -8 4306.98 144.991 2 -2 -7 -8 3927.04 183.929 2 -2 -7 -9 2522.62 156.576 2 -2 7 -9 2642.57 123.328 2 -2 -7 -10 1636.25 134.571 2 -2 7 -10 1700.60 108.821 2 -2 7 -11 3243.09 158.710 2 -2 -7 -11 3279.45 191.767 2 -2 -7 -12 1423.10 133.479 2 -2 7 -12 1630.81 122.755 2 -2 -7 -13 656.252 97.7311 2 -2 7 -13 750.680 87.1439 2 -2 7 -14 641.331 92.1449 2 -2 -7 -14 702.471 109.634 2 -2 7 -15 540.240 90.0611 2 -2 -7 -15 508.829 97.0974 2 -2 -7 -16 1497.08 160.751 2 -2 7 -16 1694.67 155.276 2 -2 -7 -17 471.221 100.413 2 -2 7 -17 601.056 100.350 2 -2 7 -18 1316.61 147.057 2 -2 -7 -18 1147.91 156.193 2 2 8 -21-49.0123 54.8062 2 2 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1033.49 65.9036 3 2 -8 -6 930.382 73.3232 2 2 8 -6 1105.17 50.9834 1 2 -8 -5 1028.76 70.5602 2 2 8 -5 996.399 41.4824 1 2 -8 -5 945.010 63.1999 3 -2 -8 5 1128.27 72.8139 2 -2 -8 5 1115.16 65.5898 3 2 -8 -4 160.518 29.9251 2 2 -8 -4 188.869 35.7659 3 -2 8 4 320.164 38.0416 2 -2 -8 4 164.038 27.6100 3 2 8 -4 193.425 15.2136 1 -2 -8 4 216.914 34.4257 2 2 -8 -3 326.484 38.0222 3 -2 8 3 338.435 32.0447 2 -2 -8 3 356.606 39.4878 3 2 -8 -3 339.053 35.7938 2 -2 8 2 7563.46 138.027 2 2 -8 -2 7358.36 139.426 2 2 -8 -2 7279.33 172.479 3 2 -8 -1 233.784 32.6792 1 2 -8 -1 251.399 22.9980 2 2 -8 -1 296.285 40.1131 3 2 -8 0 40.4926 20.7741 1 2 -8 0-33.0814 22.3918 3 2 -8 0-3.82475 6.50266 2 -2 8 0-3.01231 12.5592 1 2 -8 1 1122.07 60.9248 1 2 -8 1 1145.46 74.7897 3 -2 8 -1 1249.55 63.3878 1 2 -8 2 2509.53 107.717 3 2 -8 2 2572.70 95.0120 1 -2 8 -2 2644.03 93.0607 1 -2 8 -3 0.08092 12.3246 1 2 -8 3-9.08513 17.5071 1 2 -8 3 4.90483 21.1646 3 2 -8 4 7057.99 105.844 2 2 -8 4 7349.91 177.248 1 -2 8 -4 7166.77 108.227 2 2 -8 4 7305.86 192.501 3 -2 8 -4 7839.97 174.712 1 -2 -8 -4 7045.87 204.842 2 -2 8 -5 15833.5 193.071 2 2 -8 5 16229.1 280.488 1 2 -8 5 16559.7 194.154 2 -2 -8 -5 16633.4 331.205 2 -2 8 -6 367.865 34.9318 2 2 -8 6 369.221 35.4604 2 2 -8 6 352.713 45.9695 1 -2 -8 -6 360.451 51.9994 2 -2 -8 -7 2618.83 147.106 2 2 -8 7 2479.81 97.9531 2 -2 8 -7 2517.84 100.402 2 2 -8 8 945.585 65.1830 2 -2 -8 -8 931.708 96.0496 2 -2 8 -8 1031.65 72.1566 2 -2 8 -9 353.833 51.7739 2 -2 -8 -9 276.178 63.3561 2 -2 8 -10 1266.01 95.6400 2 -2 -8 -10 1320.68 123.084 2 -2 8 -11 141.487 43.0853 2 -2 -8 -11 161.646 56.0829 2 -2 -8 -12 241.156 60.9148 2 -2 8 -12 309.047 56.6147 2 -2 8 -13 193.937 54.9049 2 -2 -8 -13 159.111 53.6295 2 -2 -8 -14 244.205 61.4570 2 -2 8 -14 350.147 73.8430 2 -2 8 -15 490.509 78.8942 2 -2 -8 -15 486.891 98.8735 2 -2 -8 -16-8.86325 61.9489 2 -2 8 -16 48.2263 40.6331 2 -2 -8 -17 429.644 99.7329 2 -2 8 -17 312.699 66.1892 2 -2 -8 -18 73.6222 65.7621 2 2 9 -20 460.328 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10 -15 652.159 93.6049 2 2 10 -14 761.925 91.9100 2 2 -10 -14 719.207 105.553 2 2 -10 -13 351.106 79.3715 2 2 10 -13 408.000 71.8112 2 2 -10 -12 400.058 79.2091 2 2 10 -12 357.145 65.6083 2 2 -10 -11 34.9067 37.1994 2 2 10 -11 61.0821 28.8818 2 2 -10 -10 2878.13 169.160 2 2 10 -10 2952.36 147.880 2 -2 -10 10 2821.28 122.951 3 2 10 -9-43.3922 34.8898 2 -2 -10 9 30.4299 21.0085 3 2 -10 -9-30.1027 41.3856 2 2 10 -8 929.434 61.6444 1 2 -10 -8 901.513 72.7430 3 -2 -10 8 796.784 65.0385 3 2 -10 -8 957.701 87.4947 2 2 10 -7 8423.60 158.029 1 2 -10 -7 8116.87 240.128 2 -2 -10 7 8361.27 204.286 3 2 -10 -7 8048.11 205.056 3 2 -10 -6 626.849 62.1613 3 -2 -10 6 713.283 63.2274 3 2 10 -6 721.110 40.3224 1 2 -10 -6 715.514 69.6661 2 -2 -10 5 5141.32 158.526 3 2 10 -5 4746.48 83.9452 1 2 -10 -5 5169.94 167.456 2 2 -10 -5 4953.24 157.881 3 -2 -10 5 5082.13 160.621 2 -2 -10 4 1344.97 82.9566 3 2 -10 -4 1303.09 80.1708 2 -2 -10 4 1441.56 84.2059 2 -2 10 4 1536.71 83.7687 2 2 10 -4 1197.71 34.1411 1 2 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3273.89 152.785 1 -2 -17 3 3117.61 171.619 3 -2 -17 3 3350.07 74.9036 1 2 -17 -2 183.514 54.7251 3 -2 -17 2 102.048 34.1558 3 2 -17 -2 177.106 36.0403 1 2 -17 -2 154.850 31.4188 2 -2 -17 2 152.260 18.6388 1 2 -17 -1 2084.52 101.175 2 -2 -17 1 2217.14 78.9401 1 2 -17 -1 2277.19 118.056 1 2 -17 -1 2108.05 143.893 3 -2 -17 1 2117.91 143.110 3 2 -17 0 177.372 28.9311 2 2 -17 0 33.5072 39.2676 3 -2 -17 0 199.321 52.1660 3 2 -17 0 132.304 31.7767 1 -2 -17 0 161.163 24.9679 1 2 -17 1-14.1209 17.5417 1 2 -17 1-14.8170 39.0378 3 2 -17 1 9.04863 11.0512 2 -2 -17 -1 26.5006 36.1823 3 -2 -17 -1-7.76544 19.6598 1 2 -17 2 1568.04 131.076 3 -2 -17 -2 1534.65 126.573 3 2 -17 2 1271.53 54.8348 2 -2 -17 -2 1508.64 114.806 2 2 -17 2 1393.83 91.4709 1 -2 -17 -3 1136.04 102.810 2 2 -17 3 1288.72 89.5468 1 2 -17 3 1288.67 117.482 3 2 -17 4 108.659 50.6028 3 -2 -17 -4 148.654 52.2985 2 2 -17 4 134.567 34.7375 1 -2 -17 -5 3562.61 189.631 2 2 -17 5 4063.54 211.690 3 2 -17 5 4549.45 173.302 1 2 -17 6 359.333 74.4389 3 2 -17 6 373.256 56.7591 1 -2 -17 -6 290.398 64.9022 2 2 -17 7 2508.28 138.144 1 2 -17 7 2035.30 153.807 3 -2 -17 -7 2016.21 156.248 2 2 -17 8 42.2097 42.4281 3 -2 -17 -8 12.4019 39.2181 2 -2 -17 -9 662.942 105.673 2 -2 -17 -10 330.468 78.1844 2 -2 -17 -11 487.329 98.8798 2 -2 -17 -12 34.6439 40.9905 2 -2 -17 -13 981.554 139.200 2 -2 -17 -14 167.077 78.1783 2 -2 -17 -15 512.967 112.180 2 2 -18 -16 97.1733 69.9626 2 2 -18 -15 317.914 71.6530 3 2 -18 -15 289.526 82.5542 2 2 -18 -14 615.604 120.296 2 2 -18 -14 603.810 89.2996 3 2 -18 -13 483.418 102.819 2 2 -18 -13 398.852 72.4091 3 2 -18 -12 1290.37 122.885 3 -2 -18 12 1302.04 121.372 3 2 -18 -12 1345.57 152.515 2 2 -18 -11 638.582 102.284 2 -2 -18 11 664.449 87.7992 3 2 -18 -11 589.063 84.9787 3 2 -18 -10-44.9377 47.5262 2 2 -18 -10 28.2544 34.4092 3 -2 -18 10-5.19619 34.4355 3 -2 -18 9 274.695 60.7084 3 2 -18 -9 248.273 66.2694 3 2 -18 -9 197.457 51.2410 2 2 -18 -8 348.402 66.5225 2 -2 -18 8 377.607 68.7976 3 2 -18 -8 469.385 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135.740 3 -2 -18 -2 1488.49 114.647 2 2 -18 2 1587.65 100.354 1 -2 -18 -2 1564.82 135.827 3 2 -18 3 228.092 62.7030 3 2 -18 3 304.110 46.5454 1 -2 -18 -3 237.236 61.5696 3 -2 -18 -3 272.625 52.9694 2 2 -18 4 718.589 73.0584 1 -2 -18 -4 592.086 78.2178 2 2 -18 4 560.930 87.2910 3 2 -18 5 923.777 110.035 3 -2 -18 -5 698.168 83.5033 2 2 -18 5 1117.59 89.8554 1 -2 -18 -6 141.506 46.9261 2 2 -18 6 211.866 67.4839 3 2 -18 6 97.5455 37.9287 1 -2 -18 -7 44.8519 42.5163 2 2 -18 7 113.957 34.8714 1 2 -18 7 118.650 59.9668 3 2 -18 8-21.9651 40.2237 3 -2 -18 -8-51.7473 42.7697 2 -2 -18 -9 493.228 90.2007 2 -2 -18 -10 282.689 73.6813 2 -2 -18 -11-21.3822 40.1715 2 -2 -18 -12 464.456 97.5688 2 -2 -18 -13 125.015 58.3566 2 -2 -18 -14-45.7521 58.1941 2 2 -19 -16 214.855 67.6956 2 2 -19 -15 52.5377 66.3183 2 2 -19 -15-3.45886 37.5516 3 2 -19 -14 687.577 122.657 2 2 -19 -14 642.058 98.6849 3 2 -19 -13 12.4869 45.6425 2 2 -19 -13 23.2517 36.7158 3 2 -19 -12 603.800 109.097 2 -2 -19 12 481.796 79.2429 3 2 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607.293 115.956 2 2 -20 -15 267.333 82.1443 2 2 -20 -15 203.968 65.6321 3 2 -20 -14-38.4632 42.6820 3 2 -20 -14 67.0581 66.2623 2 2 -20 -13 1589.31 173.483 2 2 -20 -13 1812.23 155.230 3 -2 -20 12-74.7791 53.1941 3 2 -20 -12-3.98450 37.6563 3 2 -20 -11 644.647 106.728 2 -2 -20 11 678.072 99.5077 3 2 -20 -11 861.487 111.707 3 2 -20 -10 154.471 52.3408 3 -2 -20 10 231.228 63.8605 3 2 -20 -10 144.311 51.3259 2 2 -20 -9 52.2935 32.3045 2 2 -20 -9 78.4629 37.3034 3 -2 -20 9 50.9271 45.0304 3 -2 -20 8 27.2813 41.0169 3 2 -20 -8-14.5111 33.9986 3 2 -20 -8-1.91470 31.0896 2 -2 -20 7 47.1031 41.6263 3 2 -20 -7 28.8967 38.3841 3 2 -20 -7-25.5476 31.4000 2 2 -20 -6 272.219 64.8104 3 2 -20 -6 114.479 41.1526 1 -2 -20 6 226.805 62.5817 3 2 -20 -6 275.118 57.8152 2 -2 -20 5 2217.47 164.916 3 2 -20 -5 2231.35 143.840 2 2 -20 -5 2021.86 156.818 3 2 -20 -5 1961.13 137.919 1 2 -20 -4 402.355 61.8315 1 2 -20 -4 464.226 65.1516 2 -2 -20 4 325.100 70.9361 3 2 -20 -4 274.183 62.4703 3 -2 -20 3 336.622 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52.7317 3 -2 -20 -9 256.606 68.1524 2 2 -20 9 152.205 58.9104 3 -2 -20 -10 124.721 50.9753 2 -2 -20 -11 743.604 119.149 2 -2 -20 -12-116.347 62.2588 2 -2 -20 -13 33.1297 62.0084 2 2 -21 -15 22.2746 67.0404 2 2 -21 -15 146.276 46.6229 3 2 -21 -14 486.257 90.4999 3 2 -21 -14 532.548 111.849 2 2 -21 -13 484.927 105.401 2 2 -21 -13 369.878 81.9471 3 2 -21 -12 463.753 93.8861 2 2 -21 -12 567.396 95.3956 3 2 -21 -11 334.268 78.3972 2 2 -21 -11 439.869 82.8495 3 -2 -21 11 386.320 80.3527 3 2 -21 -10 897.230 111.011 3 2 -21 -10 866.661 113.654 2 -2 -21 10 840.316 111.800 3 2 -21 -9 131.109 50.8120 3 2 -21 -9 108.991 54.3016 2 -2 -21 9-25.4512 46.9958 3 -2 -21 8 268.082 64.7276 3 2 -21 -8 298.320 68.5852 2 2 -21 -8 309.730 69.4000 3 2 -21 -7 169.941 59.4361 3 -2 -21 7 201.920 64.9691 3 2 -21 -7 194.742 49.7998 2 -2 -21 6 999.678 116.836 3 2 -21 -6 893.532 109.237 3 2 -21 -6 929.963 100.538 2 2 -21 -6 985.227 103.591 1 2 -21 -5 939.132 95.5140 1 2 -21 -5 988.247 114.456 3 2 -21 -5 897.453 93.1990 2 -2 -21 5 896.944 113.541 3 2 -21 -4 2034.88 134.882 1 -2 -21 4 1829.27 154.322 3 2 -21 -4 1868.94 154.963 3 2 -21 -4 1398.50 106.481 2 2 -21 -3 557.685 68.8886 1 -2 -21 3 679.395 99.7598 3 2 -21 -3 724.606 102.018 3 2 -21 -2 4250.17 233.023 3 -2 -21 2 3830.34 220.185 3 2 -21 -2 4270.12 180.752 1 -2 -21 1 114.364 55.5172 3 2 -21 -1 21.7608 12.2148 1 2 -21 -1 32.3056 48.5468 3 2 -21 0 546.258 88.9167 3 2 -21 0 529.281 62.6780 1 -2 -21 0 381.885 64.3048 2 -2 -21 0 389.687 74.7714 3 -2 -21 -1 874.794 91.7033 2 2 -21 1 852.835 110.666 3 -2 -21 -1 1000.01 118.730 3 -2 -21 -2 590.111 98.4178 3 2 -21 2 664.021 99.0509 3 -2 -21 -2 527.236 75.2882 2 2 -21 3 1597.11 150.078 3 -2 -21 -3 1445.65 138.531 3 -2 -21 -3 1355.44 121.365 2 -2 -21 -4 1628.53 136.688 2 2 -21 4 1885.75 165.465 3 -2 -21 -4 2073.54 172.554 3 -2 -21 -5 2171.31 176.718 3 -2 -21 -5 1600.02 142.011 2 2 -21 5 1754.69 163.112 3 2 -21 6 2972.05 211.532 3 -2 -21 -6 2766.70 194.637 2 -2 -21 -6 3386.18 221.466 3 2 -21 7 837.579 121.365 3 -2 -21 -7 1052.88 127.929 3 -2 -21 -7 780.643 107.601 2 -2 -21 -8 781.267 116.610 3 2 -21 8 704.461 106.504 3 -2 -21 -8 610.668 102.802 2 -2 -21 -9 321.165 79.3488 2 -2 -21 -9 268.051 76.1763 3 2 -21 9 304.273 79.9439 3 -2 -21 -10 269.834 82.3247 2 -2 -21 -11 115.396 49.8742 2 -2 -21 -12 543.736 103.323 2 -2 -21 -13 522.000 105.965 2 2 -22 -15-31.3321 25.6652 3 2 -22 -14 538.246 95.3721 3 2 -22 -14 621.204 118.762 2 2 -22 -13 70.7040 67.7292 2 2 -22 -13 85.7632 45.4042 3 2 -22 -12 1027.69 142.783 2 2 -22 -12 856.220 116.075 3 2 -22 -11 5.15669 47.0009 2 2 -22 -11 3.45416 46.8413 3 -2 -22 11 20.8711 50.3663 3 2 -22 -10 160.174 56.1089 2 -2 -22 10 487.648 91.7298 3 2 -22 -10 402.765 84.7163 3 2 -22 -9 209.778 62.0682 2 -2 -22 9 219.153 70.3652 3 2 -22 -9 208.780 62.9189 3 2 -22 -8 121.577 49.8368 3 2 -22 -8 75.0360 44.3243 2 -2 -22 8 21.9929 41.3969 3 2 -22 -7-76.3871 39.2914 2 2 -22 -7-16.7099 33.7992 1 -2 -22 7-40.2692 42.6531 3 2 -22 -7-41.3168 52.5872 3 2 -22 -6 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411.220 71.8689 2 -3 -5 -13 357.357 74.6122 2 -3 5 -14 14.0810 35.4252 2 -3 -5 -14 29.1575 41.4160 2 -3 5 -15 317.892 72.9630 2 -3 -5 -15 317.254 79.8399 2 -3 -5 -16 47.4274 55.0310 2 -3 5 -16-2.87256 45.0269 2 -3 -5 -17 197.659 66.8280 2 -3 5 -17 190.716 61.7887 2 -3 5 -18 119.187 63.0463 2 -3 -5 -18 30.1934 51.6425 2 -3 5 -19 409.570 101.190 2 3 6 -21 211.144 75.1499 2 3 -6 -20 1231.33 160.045 2 3 6 -20 1479.96 168.500 2 3 -6 -19-76.8941 67.3687 2 3 6 -19 63.2414 62.8156 2 3 -6 -18 3109.05 230.372 2 3 6 -18 2818.94 209.031 2 3 -6 -17 131.544 62.4873 2 3 6 -17 175.540 61.9127 2 3 6 -16 2569.57 187.597 2 3 -6 -16 2509.16 191.190 2 3 -6 -15 2487.38 180.776 2 3 6 -15 2598.12 177.753 2 3 -6 -14 4594.31 237.540 2 3 6 -14 4434.65 224.412 2 3 -6 -13 1212.28 117.026 2 3 6 -13 1321.80 114.862 2 3 -6 -12 155.642 53.4256 2 3 6 -12 261.603 56.2343 2 3 -6 -11 60.7001 38.2976 2 3 6 -11 108.473 37.6972 2 3 -6 -10 7873.00 256.266 2 3 -6 -10 8160.91 170.689 3 3 6 -10 8309.21 248.823 2 3 -6 -9 1133.45 90.8747 2 3 -6 -9 1141.16 63.8979 3 3 6 -9 1140.35 91.6096 2 3 -6 -8 6304.04 205.407 2 -3 -6 8 6266.35 124.287 3 3 -6 -8 6224.02 143.198 3 3 6 -8 6338.15 197.137 2 3 6 -7 537.302 58.3687 2 3 -6 -7 585.942 60.4230 2 3 -6 -7 552.029 45.9710 3 -3 -6 7 679.525 42.2178 3 -3 -6 6 21396.5 232.439 3 3 6 -6 21071.7 324.579 2 3 -6 -6 20809.6 257.099 3 3 -6 -6 20419.9 321.715 2 -3 6 5 224.499 31.7384 2 3 -6 -5 212.439 32.4759 2 3 -6 -5 222.642 29.1568 3 -3 -6 5 227.755 25.7868 3 -3 -6 5 250.963 38.7966 2 -3 6 4 875.287 54.5361 2 -3 -6 4 940.827 65.4780 2 3 -6 -4 838.602 54.4029 3 -3 6 4 861.201 51.2563 3 3 -6 -4 839.928 55.6726 2 3 -6 -3 1670.13 69.6941 2 3 -6 -3 1633.88 75.6327 3 -3 6 3 1656.77 67.5424 2 -3 6 3 1743.19 74.6739 3 -3 6 2 14928.7 173.586 2 3 -6 -2 14854.9 181.843 2 3 -6 -2 14929.3 240.747 1 -3 6 2 15476.5 223.691 3 3 -6 -2 15928.6 232.096 3 -3 6 1 843.226 53.1219 3 -3 -6 1 733.846 28.9256 1 -3 6 1 699.789 31.0214 2 3 -6 -1 829.530 56.8872 3 3 -6 -1 833.283 35.6469 2 3 -6 -1 758.229 53.8590 1 -3 6 1 836.483 55.4248 1 3 -6 0 20418.0 264.510 1 3 -6 0 20376.8 281.945 3 -3 6 0 21162.4 273.670 3 -3 -6 0 19729.6 186.237 1 -3 6 0 21208.0 261.712 1 3 -6 1 1603.00 75.8127 1 -3 6 -1 1826.45 79.2444 1 3 -6 1 1633.56 83.6624 3 -3 6 -1 1734.92 81.9105 3 -3 -6 -1 1637.99 62.5100 1 3 -6 2 8702.79 193.811 3 3 -6 2 8513.84 180.475 1 -3 6 -2 9109.10 182.811 1 3 -6 3 207.053 33.4516 1 -3 6 -3 248.143 18.5189 2 -3 6 -3 328.825 37.9972 1 -3 -6 -4 418.164 55.0831 2 -3 6 -4 390.510 29.0632 2 3 -6 4 384.342 45.4033 1 -3 6 -5 130.734 25.1385 2 -3 -6 -5 117.207 38.6692 2 3 -6 5 74.3463 25.1814 1 3 -6 6 5168.62 137.749 2 3 -6 6 5356.31 177.141 1 -3 -6 -6 5125.69 189.407 2 -3 6 -6 5093.99 135.049 2 -3 6 -7 223.404 34.3883 2 3 -6 7 249.148 35.4194 2 -3 -6 -7 200.757 45.7947 2 -3 -6 -8 3370.06 175.868 2 -3 6 -8 3377.43 132.932 2 -3 6 -9 949.663 80.6413 2 -3 -6 -9 894.630 98.2354 2 -3 6 -10 6414.31 212.604 2 -3 -6 -10 6618.76 265.259 2 -3 6 -11 271.115 51.7095 2 -3 -6 -11 309.008 69.1417 2 -3 6 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20.9529 1 -4 6 -3-5.96875 13.2034 2 -4 6 -4 3165.37 88.8091 2 4 -6 4 2981.18 129.080 1 4 -6 5 13.4313 22.0487 1 -4 6 -5 0.21761 12.8933 2 -4 -6 -5 7.27572 30.2632 2 -4 6 -6 1279.53 72.5602 2 -4 -6 -6 1219.36 97.1813 2 4 -6 6 1153.20 90.1114 1 -4 6 -7 1466.37 83.7995 2 -4 -6 -7 1314.80 102.792 2 -4 6 -8 1982.30 106.124 2 -4 -6 -8 1839.36 133.363 2 -4 6 -9 481.934 58.6704 2 -4 -6 -9 430.199 72.2570 2 -4 -6 -10 2589.19 172.338 2 -4 6 -10 2876.38 148.213 2 -4 -6 -11 23.8351 40.9199 2 -4 6 -11 106.574 34.4638 2 -4 -6 -12 1624.33 147.370 2 -4 6 -12 1741.84 129.920 2 -4 6 -13 80.4781 38.5544 2 -4 -6 -13 122.806 53.1735 2 -4 6 -14 301.066 64.7887 2 -4 -6 -14 328.672 76.7872 2 -4 6 -15 14.1866 48.1723 2 -4 -6 -15 11.1182 39.4899 2 -4 -6 -16 37.4767 47.3228 2 -4 6 -16 120.963 59.8976 2 -4 -6 -17 407.265 109.571 2 -4 6 -17 203.689 66.9856 2 -4 -6 -18 515.259 116.547 2 4 7 -21 304.227 99.6054 2 4 -7 -20 485.451 107.825 2 4 7 -20 348.324 79.0743 2 4 -7 -19 1091.75 142.550 2 4 7 -19 1151.83 146.311 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2 -4 -7 -6 659.138 77.4569 2 -4 7 -7 1105.04 71.6481 2 -4 -7 -7 1020.01 96.5582 2 4 -7 7 1013.40 89.4839 1 -4 7 -8 6892.76 192.090 2 -4 -7 -8 6636.38 251.300 2 -4 7 -9 47.4367 21.8265 2 -4 -7 -9 98.0241 41.2556 2 -4 -7 -10 2779.65 179.489 2 -4 7 -10 3118.02 149.302 2 -4 7 -11 2863.03 152.268 2 -4 -7 -11 2748.82 188.476 2 -4 7 -12 331.219 55.6969 2 -4 -7 -12 406.837 86.1948 2 -4 7 -13 1019.24 105.953 2 -4 -7 -13 829.270 112.133 2 -4 -7 -14-15.0625 43.2809 2 -4 7 -14 23.6059 37.5096 2 -4 -7 -15 594.048 104.141 2 -4 7 -15 730.130 103.128 2 -4 -7 -16 802.839 127.468 2 -4 -7 -17 241.730 81.3796 2 4 8 -21 191.710 79.8795 2 4 -8 -20 97.0148 68.9336 2 4 8 -20-56.2846 61.0527 2 4 -8 -19 280.002 88.0529 2 4 8 -19 74.6917 51.1243 2 4 -8 -18 975.208 134.823 2 4 8 -18 1145.19 139.831 2 4 -8 -17 576.455 109.733 2 4 8 -17 570.238 103.359 2 4 -8 -16 35.0094 44.3762 2 4 8 -16-48.2096 56.8058 2 4 -8 -15 995.645 120.885 2 4 8 -15 1043.45 117.754 2 4 -8 -14 716.914 99.1945 2 4 -8 -14 828.763 68.1369 3 4 8 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129.107 34.2793 3 4 -8 -2 107.335 27.6576 1 -4 8 2 70.0409 14.4014 2 -4 -8 2 61.6940 7.64488 1 4 -8 -2 80.8976 12.7031 2 -4 -8 1 657.735 33.4467 1 -4 8 1 599.496 30.8273 2 4 -8 -1 759.970 61.6537 1 4 -8 -1 681.577 63.0069 3 4 -8 -1 654.623 35.0117 2 4 -8 0 1750.37 96.5030 3 4 -8 0 1656.70 90.7140 1 -4 -8 0 1699.56 63.2737 1 4 -8 1 1320.06 85.5369 3 4 -8 1 1441.31 85.5640 1 -4 -8 -1 1359.25 64.3944 1 4 -8 2 312.105 39.8612 1 4 -8 2 368.316 49.6899 3 -4 -8 -2 352.013 37.0650 1 4 -8 3 10513.2 241.645 1 -4 8 -4 150.503 16.4400 2 4 -8 4 166.895 40.6708 1 -4 8 -5 5243.04 111.345 2 -4 -8 -5 4901.94 193.962 2 4 -8 5 5104.50 180.994 1 4 -8 6 12.1625 26.8533 1 -4 8 -6-5.87842 17.3272 2 -4 8 -7 310.748 36.9481 2 -4 -8 -7 338.063 63.4120 2 4 -8 7 291.503 49.2337 1 -4 8 -8 41.0585 22.1423 2 -4 -8 -8 29.0940 35.4565 2 -4 8 -9 3074.36 132.883 2 -4 -8 -9 3047.51 184.205 2 -4 8 -10 68.8602 36.6254 2 -4 -8 -10 80.0520 57.6235 2 -4 -8 -11 2403.87 178.483 2 -4 8 -11 2276.07 133.115 2 -4 8 -12 10.9362 37.2057 2 -4 -8 -12 94.7036 47.0505 2 -4 -8 -13 1136.98 129.224 2 -4 8 -13 1305.44 117.719 2 -4 8 -14 429.394 80.4309 2 -4 -8 -14 432.423 85.9189 2 -4 -8 -15 99.0538 48.5358 2 -4 -8 -16 39.8600 51.3480 2 -4 -8 -17 986.518 140.432 2 4 9 -21 128.392 79.1468 2 4 -9 -20 242.569 75.1488 2 4 9 -20 380.568 88.5577 2 4 -9 -19 122.081 76.0023 2 4 9 -19-39.2492 45.5280 2 4 9 -18 1143.64 137.670 2 4 -9 -18 1091.90 144.776 2 4 -9 -17 132.609 48.7765 2 4 9 -17 165.117 67.3047 2 4 -9 -16 1822.11 172.401 2 4 9 -16 2157.71 173.305 2 4 -9 -15 124.616 45.6570 2 4 9 -15 234.695 67.8963 2 4 -9 -14 3252.55 209.100 2 4 -9 -14 3570.48 144.130 3 4 9 -14 3393.36 199.854 2 4 -9 -13 505.045 87.7238 2 4 9 -13 581.506 82.3473 2 4 -9 -13 575.669 59.7231 3 4 -9 -12 1393.04 123.622 2 4 9 -12 1420.65 117.798 2 4 -9 -12 1465.02 89.8941 3 4 -9 -11 229.126 40.1751 3 4 -9 -11 189.834 52.5551 2 4 9 -11 182.593 50.8251 2 -4 -9 11 171.823 30.3262 3 4 -9 -10 3506.10 178.767 2 4 9 -10 3471.60 172.287 2 -4 -9 10 3400.39 116.302 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264.701 1 4 -9 2 4750.09 160.676 1 4 -9 2 4813.53 175.040 3 -4 -9 -2 4615.91 131.987 1 4 -9 3 8.05610 20.3173 1 4 -9 4 1832.03 106.651 1 -4 9 -4 1593.46 40.7508 2 -4 9 -5-5.33982 9.02600 2 4 -9 5-29.3982 27.3843 1 -4 -9 -5 42.8189 36.5735 2 -4 -9 -6 8591.29 274.242 2 4 -9 6 8803.30 252.543 1 -4 9 -6 9197.00 161.834 2 -4 -9 -7 1023.73 100.564 2 4 -9 7 1010.94 91.3182 1 -4 9 -7 1132.37 67.6468 2 -4 -9 -8 913.590 101.365 2 -4 9 -8 1196.42 73.9271 2 -4 -9 -9 3221.95 191.780 2 -4 9 -9 3253.30 132.787 2 -4 -9 -10 3231.44 202.099 2 -4 9 -10 3126.90 141.185 2 -4 9 -11 61.9767 31.6694 2 -4 -9 -11 84.5937 41.3438 2 -4 -9 -12 1162.15 130.762 2 -4 9 -12 1295.82 103.797 2 -4 9 -13 79.9510 44.3087 2 -4 -9 -13 96.6746 51.5203 2 -4 -9 -14 2339.08 196.541 2 -4 -9 -15 90.7512 62.9137 2 -4 -9 -16 558.952 119.096 2 -4 -9 -17 130.578 71.9091 2 4 10 -21-3.02470 54.6140 2 4 10 -20 41.0082 56.2649 2 4 -10 -19 688.293 126.611 2 4 10 -19 467.846 102.936 2 4 -10 -18 135.789 70.1903 2 4 10 -18 10.0413 42.9991 2 4 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1 -4 11 2 30.9653 13.4397 2 -4 -11 1 9190.78 124.430 1 4 -11 -1 9466.73 232.704 1 4 -11 -1 9228.89 246.901 3 4 -11 -1 9046.37 129.992 2 -4 -11 0 3779.42 97.5703 1 4 -11 0 3770.37 145.815 1 4 -11 0 3632.75 157.208 3 4 -11 1 5357.65 175.975 1 -4 -11 -1 5483.66 134.996 1 4 -11 1 5339.70 195.407 3 4 -11 2-50.6247 42.5749 3 4 -11 2-25.0899 21.9107 1 4 -11 3 5296.39 181.936 1 4 -11 3 5340.13 202.333 3 4 -11 4 2542.14 131.014 1 4 -11 4 2289.34 135.642 3 4 -11 5 1870.89 115.813 1 -4 -11 -5 1740.33 126.417 2 4 -11 6 345.793 52.9320 1 -4 -11 -6 290.078 58.0889 2 -4 11 -6 322.212 24.9409 2 -4 -11 -7 3509.17 189.527 2 -4 11 -7 3612.72 99.8518 2 4 -11 7 3865.17 178.555 1 -4 -11 -8 679.145 90.4015 2 -4 11 -8 749.590 52.6688 2 4 -11 8 683.807 79.5739 1 -4 11 -9 4781.74 144.815 2 -4 -11 -9 4403.68 233.866 2 -4 -11 -10 402.906 79.2669 2 -4 11 -10 330.048 39.4485 2 -4 -11 -11 1033.41 125.263 2 -4 -11 -12 596.847 98.6741 2 -4 -11 -13 930.889 127.704 2 -4 -11 -14 1120.72 145.643 2 -4 -11 -15 800.754 124.186 2 -4 -11 -16-93.2112 69.8593 2 4 -12 -19 298.369 94.6171 2 4 12 -19 268.862 76.1768 2 4 -12 -18 100.957 63.7514 2 4 12 -18 110.243 38.7407 2 4 -12 -17-64.7673 64.9666 2 4 12 -17 46.2253 51.0740 2 4 -12 -16 63.6718 48.3992 2 4 12 -16 77.2918 43.5278 2 4 -12 -15 331.535 75.7331 2 4 -12 -15 415.394 61.1366 3 4 12 -15 585.966 89.5642 2 4 -12 -14 9.68395 39.9794 2 4 -12 -14-11.7231 25.1039 3 4 -12 -13 1490.51 141.799 2 4 -12 -13 1669.15 111.520 3 -4 -12 12 567.584 60.4327 3 4 -12 -12 585.971 89.2685 2 4 -12 -12 686.505 76.6022 3 4 -12 -11 472.079 73.9830 2 4 -12 -11 530.638 67.2427 3 -4 -12 11 463.036 55.0194 3 4 -12 -10 1805.76 138.200 2 4 -12 -10 1815.55 114.286 3 -4 -12 10 1762.37 103.974 3 4 -12 -9 144.674 42.5761 2 4 -12 -9 130.794 36.0546 3 -4 -12 9 135.322 34.6260 3 4 12 -9 116.613 21.0423 1 4 -12 -8 2335.63 139.663 2 4 12 -8 2305.82 64.8749 1 4 -12 -8 2482.48 129.083 3 -4 -12 8 2322.21 121.305 3 4 -12 -7 246.593 45.4387 2 -4 -12 7 218.159 38.4529 3 4 -12 -7 155.732 38.4860 3 4 -12 -6 58.0506 29.2989 3 4 -12 -6 13.7466 22.6211 2 -4 -12 6 35.2633 24.9614 3 4 -12 -5 3099.55 131.720 2 -4 -12 5 3184.47 139.704 3 4 -12 -5 3191.48 146.860 3 4 -12 -4 2913.88 115.676 2 4 -12 -4 2912.53 140.853 3 -4 12 4 3047.19 116.285 2 4 -12 -4 2978.05 147.848 1 4 -12 -3 2970.15 104.835 2 4 -12 -3 2994.29 141.588 1 4 -12 -3 2879.73 141.348 3 -4 12 3 2926.57 104.485 2 4 -12 -2 4814.46 183.682 3 4 -12 -2 4874.81 175.803 1 4 -12 -2 4834.02 118.132 2 4 -12 -1 41.6988 10.5274 2 -4 -12 1 37.1649 9.00125 1 4 -12 -1 65.1276 30.8605 3 4 -12 -1 27.8107 18.8037 1 -4 -12 0 1966.08 71.9645 1 4 -12 0 1821.20 115.365 3 4 -12 0 1833.28 105.206 1 4 -12 1 182.210 37.4745 1 4 -12 1 212.976 46.9797 3 4 -12 2 1082.70 93.5057 3 4 -12 2 1274.71 89.2795 1 4 -12 3 1041.14 81.8462 1 4 -12 3 1032.40 95.3902 3 4 -12 4 8413.60 241.038 1 4 -12 4 7888.22 260.511 3 4 -12 5 454.908 60.4226 1 -4 -12 -5 311.286 60.4832 2 4 -12 6 505.919 65.5957 1 -4 -12 -6 449.288 71.2036 2 4 -12 7 111.672 39.7366 1 -4 -12 -7 83.3577 44.4936 2 -4 12 -7 87.3390 16.6659 2 -4 -12 -8 2591.80 173.194 2 4 -12 8 2863.86 162.293 1 -4 12 -8 2362.01 87.0955 2 -4 -12 -9 183.795 59.2488 2 -4 -12 -10 1512.44 147.155 2 -4 -12 -11-54.2842 43.5138 2 -4 -12 -12 1077.66 133.634 2 -4 -12 -13-15.4946 34.8417 2 -4 -12 -14 874.640 126.864 2 -4 -12 -15 189.383 70.0141 2 -4 -12 -16 604.644 121.037 2 4 -13 -18 488.185 106.701 2 4 13 -18 332.080 77.0318 2 4 -13 -17 347.313 93.6749 2 4 -13 -16 367.081 87.9972 2 4 -13 -15 389.050 90.3740 2 4 -13 -15 328.248 55.3048 3 4 -13 -14 425.980 82.8958 2 4 -13 -14 490.766 62.9698 3 4 -13 -13 148.549 36.8238 3 4 -13 -13 146.892 46.0477 2 4 -13 -12 2657.92 184.541 2 4 -13 -12 2764.40 148.711 3 -4 -13 12 2556.43 129.351 3 4 -13 -11 1020.88 111.428 2 -4 -13 11 1158.46 87.5394 3 4 -13 -11 1334.80 103.935 3 4 -13 -10 1496.75 127.716 2 -4 -13 10 1530.37 101.601 3 4 -13 -10 1622.38 111.331 3 4 -13 -9 1027.34 101.504 2 4 -13 -9 1082.72 89.1320 3 -4 -13 9 1094.72 88.8593 3 4 13 -8 5013.81 75.1477 1 4 -13 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35.2194 1 4 -13 5 6379.76 221.162 1 -4 -13 -5 5756.54 235.999 2 -4 -13 -6 2891.47 174.935 2 4 -13 6 2812.38 153.321 1 4 -13 7 375.066 58.2362 1 -4 -13 -7 361.452 73.1945 2 -4 -13 -8 6774.10 285.335 2 4 -13 8 7493.44 267.447 1 -4 -13 -9 209.804 55.7682 2 -4 -13 -10 1688.31 158.099 2 -4 -13 -11 139.980 61.8403 2 -4 -13 -12 328.021 77.3893 2 -4 -13 -13 888.194 127.050 2 -4 -13 -14 173.514 74.2570 2 -4 -13 -15 202.344 85.8634 2 4 -14 -18 254.227 71.9189 2 4 -14 -17 286.384 78.8708 2 4 -14 -16 75.7214 48.3268 2 4 -14 -15 685.831 79.8850 3 4 -14 -15 887.866 126.915 2 4 -14 -14 1407.14 150.643 2 4 -14 -14 1273.38 111.883 3 4 -14 -13 1221.23 134.992 2 4 -14 -13 1192.69 101.629 3 4 -14 -12 24.7209 39.9173 2 4 -14 -12 80.5163 27.7518 3 -4 -14 11 3099.44 151.561 3 4 -14 -11 3308.17 163.621 3 4 -14 -11 3352.84 199.380 2 4 -14 -10 3288.88 192.352 2 4 -14 -10 3206.70 160.572 3 -4 -14 10 3162.57 154.318 3 4 -14 -9 780.890 88.3617 2 4 -14 -9 766.807 81.4894 3 -4 -14 9 669.413 73.8106 3 4 -14 -8 94.1883 41.7636 2 -4 -14 8 125.631 35.2424 3 4 -14 -8 100.101 39.3183 3 4 -14 -7 1064.92 95.4848 3 -4 -14 7 1029.57 90.3371 3 4 -14 -7 1058.04 95.2230 2 4 -14 -6 124.985 40.0188 2 4 -14 -6 172.840 43.5503 3 -4 -14 6 103.401 35.8030 3 4 -14 -5 1033.73 95.0410 1 4 -14 -5 1094.22 81.9752 2 4 -14 -5 1166.81 99.5568 3 -4 -14 5 1054.20 90.6928 3 4 -14 -4 4837.96 156.279 2 -4 -14 4 4681.11 187.306 3 4 -14 -4 4814.54 195.037 1 4 -14 -4 4682.10 191.994 3 4 -14 -3 4480.34 188.971 3 4 -14 -3 4599.44 138.141 2 4 -14 -3 4264.43 178.167 1 4 -14 -2 429.086 37.5043 2 4 -14 -2 441.615 57.1361 1 4 -14 -2 483.491 69.4539 3 4 -14 -1 3067.52 144.325 1 4 -14 -1 2895.86 157.411 3 4 -14 -1 2907.74 81.5697 2 -4 -14 1 2854.03 71.8430 1 4 -14 0 99.7710 29.4772 1 4 -14 0 31.3934 35.0090 3 -4 -14 0 54.4657 14.3488 1 4 -14 1 839.266 87.3425 3 4 -14 1 842.742 75.1273 1 4 -14 2 519.176 60.6852 1 4 -14 2 516.209 75.0692 3 4 -14 3 504.745 74.6857 3 4 -14 3 520.905 63.7374 1 4 -14 4 5.16877 38.9138 3 4 -14 4-5.24343 27.8173 1 -4 -14 -4-15.2850 40.1340 2 4 -14 5 8085.39 251.838 1 4 -14 5 7781.71 277.587 3 -4 -14 -5 7093.80 267.458 2 4 -14 6 899.904 89.9069 1 -4 -14 -6 785.389 96.3051 2 4 -14 7 1790.61 130.441 1 -4 -14 -7 1616.40 139.841 2 -4 -14 -8 11.9590 47.9093 2 4 -14 8-12.6103 33.0751 1 -4 -14 -9 772.578 110.307 2 -4 -14 -10 7.57653 39.9066 2 -4 -14 -11-48.1113 62.1494 2 -4 -14 -12 83.8932 50.9615 2 -4 -14 -13 465.531 104.523 2 -4 -14 -14 1.69647 47.8468 2 -4 -14 -15 751.944 124.378 2 4 -15 -18 311.824 92.5663 2 4 -15 -17 233.109 74.7660 2 4 -15 -16 0.41348 56.1810 2 4 -15 -15 283.021 72.0293 2 4 -15 -15 201.934 49.7965 3 4 -15 -14 180.726 60.2933 2 4 -15 -14 319.511 61.1788 3 4 -15 -13 629.439 79.8399 3 4 -15 -13 645.325 106.862 2 4 -15 -12 447.963 83.5708 2 -4 -15 12 342.081 54.8162 3 4 -15 -12 419.670 63.8118 3 4 -15 -11 1398.46 135.651 2 -4 -15 11 1248.39 102.444 3 4 -15 -11 1324.78 112.519 3 -4 -15 10 1467.22 111.250 3 4 -15 -10 1578.74 134.666 2 4 -15 -10 1480.84 117.399 3 4 -15 -9 445.653 70.3577 2 -4 -15 9 424.455 65.3049 3 4 -15 -9 534.225 71.1059 3 4 -15 -8 171.135 46.7917 3 4 -15 -8 198.284 48.3282 2 -4 -15 8 122.121 37.3419 3 4 -15 -7-8.35424 28.1331 2 -4 -15 7 54.7261 34.1561 3 4 -15 -7-29.8856 34.7425 3 4 -15 -6 2264.01 128.078 2 4 -15 -6 2249.35 139.087 3 -4 -15 6 2124.51 131.506 3 -4 -15 5 788.947 84.5521 3 4 -15 -5 744.890 81.4034 3 4 -15 -5 743.310 83.5556 1 4 -15 -5 735.897 69.9589 2 4 -15 -4 2621.46 118.219 2 4 -15 -4 2655.75 148.599 1 4 -15 -4 2523.09 148.616 3 -4 -15 4 2494.21 143.248 3 4 -15 -3 132.933 26.6751 2 4 -15 -3 147.264 50.8526 3 -4 -15 3 160.495 46.0929 3 4 -15 -3 142.885 42.4535 1 4 -15 -2 4647.24 124.863 2 4 -15 -2 4718.36 186.818 1 4 -15 -2 4626.73 204.483 3 4 -15 -1 9454.20 258.555 1 4 -15 -1 9392.01 288.495 3 -4 -15 1 8826.18 123.987 1 -4 -15 1 9249.92 130.767 1 4 -15 -1 8611.33 142.654 2 -4 -15 0 822.484 49.2022 1 4 -15 0 767.218 91.4025 3 4 -15 0 758.933 74.6054 1 4 -15 1 1744.92 130.842 3 4 -15 1 1892.11 115.152 1 4 -15 2 2218.45 148.431 3 4 -15 2 2417.94 131.676 1 4 -15 3 15.4602 36.5250 3 4 -15 3 47.1630 21.7512 1 4 -15 4 1706.52 119.358 1 4 -15 4 1662.73 133.428 3 -4 -15 -4 1664.53 131.328 2 4 -15 5 539.262 69.3238 1 4 -15 5 465.108 80.1878 3 -4 -15 -5 451.858 80.4543 2 4 -15 6 2429.65 144.843 1 -4 -15 -6 2198.52 159.607 2 4 -15 7 862.013 91.0401 1 -4 -15 -7 795.949 98.5145 2 -4 -15 -8 1297.96 133.001 2 4 -15 8 1575.20 127.461 1 -4 -15 -9 496.562 85.5841 2 -4 -15 -10 843.452 120.477 2 -4 -15 -11 86.3134 61.4036 2 -4 -15 -12 371.004 93.0778 2 -4 -15 -13 54.6075 61.2568 2 -4 -15 -14 1014.11 142.437 2 4 -16 -17 100.201 64.7660 2 4 -16 -16 429.008 101.148 2 4 -16 -15 43.5409 28.3074 3 4 -16 -15 16.6710 48.6749 2 4 -16 -14 876.995 124.152 2 4 -16 -14 889.795 97.2456 3 4 -16 -13 87.1008 49.9909 2 4 -16 -13 100.551 39.2927 3 4 -16 -12 308.297 69.6634 2 4 -16 -12 469.466 72.1664 3 -4 -16 12 348.992 56.5165 3 4 -16 -11 679.131 96.3651 2 4 -16 -11 751.161 86.6122 3 -4 -16 11 692.702 80.9549 3 4 -16 -10 984.444 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43.5495 2 -5 -9 11 20.5340 13.1284 3 5 -9 -11 2.02263 23.5565 3 5 -9 -10 127.826 47.0698 2 -5 -9 10 140.469 24.6656 3 5 -9 -10 227.224 44.5779 3 -5 -9 9-1.86562 16.2024 3 5 -9 -9 7.86136 38.5856 2 5 -9 -9 7.52393 24.7698 3 5 -9 -8 14217.1 269.481 3 -5 -9 8 13738.1 238.466 3 5 -9 -8 14366.4 323.036 2 5 -9 -7 102.819 26.4023 2 5 -9 -7 145.210 34.5661 3 -5 -9 7 142.063 27.2357 3 5 9 -6 2292.16 48.9720 1 5 -9 -6 2677.78 119.164 3 5 -9 -6 2633.50 122.872 2 5 -9 -5 1106.90 92.5940 1 5 -9 -5 983.953 75.4033 3 5 -9 -5 1248.05 80.8897 2 -5 9 4 13880.8 228.731 2 5 -9 -4 13380.9 274.571 3 5 -9 -4 14057.8 307.418 1 5 -9 -4 13109.0 234.393 2 -5 9 3 765.760 49.4007 2 5 -9 -3 753.859 68.9907 3 5 -9 -3 735.359 51.0427 2 5 -9 -3 794.217 73.9830 1 -5 9 2 1604.10 61.3111 2 5 -9 -2 1760.87 102.992 3 5 -9 -2 1789.20 106.910 1 5 -9 -2 1792.98 70.9671 2 -5 -9 2 1649.83 49.0136 1 -5 9 1 411.264 26.5981 2 -5 -9 1 467.016 32.3188 1 5 -9 -1 506.616 57.7205 3 5 -9 -1 466.587 54.4749 1 -5 -9 0 1823.63 74.2514 1 5 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96.1704 2 5 -10 -17-15.5048 56.5731 2 5 10 -17 101.119 39.6354 2 5 -10 -16 959.041 129.131 2 5 10 -16 1161.45 133.003 2 5 -10 -15 209.316 67.6107 2 5 10 -15 196.765 57.6216 2 5 -10 -14 39.3967 51.6447 2 5 -10 -14 4.59767 29.7157 3 5 10 -14 1.32929 36.6170 2 5 10 -13 1495.30 134.728 2 5 -10 -13 1665.85 103.041 3 5 -10 -13 1514.64 142.091 2 -5 -10 12-6.28559 19.6087 3 5 -10 -12 45.7288 35.1708 3 5 -10 -11 613.969 87.0031 2 -5 -10 11 653.087 52.0216 3 5 -10 -11 687.755 66.1189 3 5 -10 -10 2582.40 155.962 2 5 -10 -10 2696.21 125.861 3 -5 -10 10 2524.10 107.435 3 5 -10 -9 130.263 42.3388 2 5 -10 -9 181.768 42.4239 3 -5 -10 9 185.342 33.8532 3 5 -10 -8 6675.79 196.909 3 -5 -10 8 6226.09 171.862 3 5 10 -8 6357.30 116.268 1 5 -10 -8 6351.51 221.932 2 5 10 -7 48.4529 9.49601 1 5 -10 -7 64.4514 30.4751 3 5 -10 -7 31.3102 25.7159 2 5 10 -7 46.0395 8.87791 1 -5 -10 7 71.0615 22.8538 3 5 -10 -6 116.411 32.8238 3 5 -10 -6 180.768 37.6377 2 5 -10 -5 16287.7 309.147 3 5 -10 -5 16309.1 288.606 2 5 -10 -5 16238.5 350.334 1 5 -10 -4 388.662 56.5206 1 5 -10 -4 459.746 46.7719 2 5 -10 -4 418.961 56.4396 3 -5 10 4 414.444 43.0771 2 5 -10 -3 6246.31 195.247 3 -5 10 3 5961.71 138.087 2 5 -10 -3 6185.55 203.403 1 5 -10 -3 5868.18 144.766 2 -5 10 2 1016.45 50.7024 2 5 -10 -2 1086.21 84.1330 1 5 -10 -2 1125.78 56.4241 2 5 -10 -2 1131.71 86.0299 3 -5 -10 2 993.061 36.1263 1 5 -10 -1 879.235 76.0771 1 -5 -10 1 859.732 43.2420 1 5 -10 -1 878.264 79.1519 3 -5 10 1 821.082 36.5113 2 -5 -10 0 2540.36 87.3835 1 5 -10 0 2465.22 130.234 3 5 -10 0 2417.69 122.967 1 -5 -10 -1-16.4943 16.4089 1 5 -10 1 22.0952 28.0567 3 5 -10 1 3.68990 19.6657 1 5 -10 2 2519.33 128.967 1 5 -10 3 906.009 82.0107 1 5 -10 4 201.767 43.9486 1 5 -10 5 1814.99 121.146 1 -5 -10 -5 1793.49 127.558 2 -5 10 -5 1807.75 53.1051 2 5 -10 6-16.6524 28.8879 1 -5 10 -6 11.7423 12.5729 2 -5 -10 -6 54.3506 40.1795 2 5 -10 7 214.211 49.5840 1 -5 10 -7 227.530 29.1512 2 -5 -10 -7 249.066 65.3153 2 -5 -10 -8 1265.71 121.747 2 5 -10 8 1295.28 113.247 1 -5 10 -8 1341.77 77.4505 2 -5 10 -9 28.1876 22.5562 2 -5 -10 -9 24.5934 37.6374 2 -5 10 -10 657.544 65.5520 2 -5 -10 -10 676.418 98.3666 2 -5 -10 -11 32.3764 39.2497 2 -5 -10 -12-39.0425 55.8815 2 -5 -10 -13 461.148 96.5112 2 -5 -10 -14-23.7660 54.2466 2 -5 -10 -15-26.5083 57.4642 2 -5 -10 -16 91.8424 69.5200 2 5 11 -21 499.444 106.904 2 5 11 -20 13.8500 49.4291 2 5 -11 -19 508.399 108.761 2 5 11 -19 479.069 101.567 2 5 -11 -18 993.132 143.186 2 5 11 -18 867.299 119.846 2 5 -11 -17 263.477 73.6581 2 5 11 -17 384.736 87.7967 2 5 -11 -16 197.357 72.7383 2 5 11 -16 188.439 51.1579 2 5 11 -15 1579.61 145.977 2 5 -11 -15 1496.15 153.591 2 5 -11 -14 64.2185 45.4624 2 5 -11 -14 138.653 39.6829 3 5 -11 -13 3969.75 227.543 2 5 -11 -13 4223.79 170.570 3 5 -11 -12 195.640 54.4079 2 -5 -11 12 117.793 23.1432 3 5 -11 -12 167.782 46.2969 3 5 -11 -11 2063.54 149.371 2 -5 -11 11 1877.70 96.2235 3 5 -11 -11 2159.76 122.427 3 5 -11 -10 1172.57 107.521 2 -5 -11 10 1133.55 75.6134 3 5 -11 -10 1193.70 89.5435 3 5 11 -10 1283.83 66.6693 1 5 -11 -9 5618.04 222.175 2 5 11 -9 5621.35 119.708 1 5 -11 -9 5813.50 193.387 3 -5 -11 9 5342.25 168.682 3 5 -11 -8 167.971 41.1659 3 5 -11 -8 151.877 38.3122 2 5 11 -8 213.242 20.1571 1 -5 -11 8 239.422 39.8924 3 5 -11 -7 4410.86 174.791 2 5 -11 -7 4391.88 167.978 3 -5 -11 7 4334.97 153.680 3 -5 -11 6 1951.55 104.785 3 5 -11 -6 2044.44 113.806 3 5 -11 -6 2029.43 111.207 2 5 -11 -5 3176.72 144.069 3 5 -11 -5 3354.37 164.685 1 5 -11 -5 3254.49 130.725 2 5 -11 -4 1950.29 113.282 3 5 -11 -4 1861.52 120.027 1 -5 11 4 1992.98 91.5475 2 5 -11 -4 2046.47 97.4990 2 -5 11 3 10223.7 183.813 2 5 -11 -3 10539.4 267.668 3 5 -11 -3 10497.1 272.698 1 5 -11 -3 10621.3 194.367 2 5 -11 -2 116.373 35.5576 1 -5 -11 2 79.8053 8.48479 1 5 -11 -2 75.5247 27.6011 3 -5 11 2 131.307 19.8758 2 5 -11 -2 95.5242 16.6779 2 5 -11 -1 6012.95 199.801 1 -5 -11 1 6118.62 113.774 1 5 -11 -1 6084.40 208.352 3 5 -11 0-8.05467 21.8645 1 -5 -11 0 1.36844 11.5193 1 5 -11 0 10.6463 27.8962 3 5 -11 1 8665.63 258.821 3 5 -11 1 8965.34 242.306 1 -5 -11 -1 9088.10 186.477 1 5 -11 2 13.6093 31.9559 3 5 -11 2-24.8575 24.3875 1 5 -11 3 8173.14 241.909 1 5 -11 4 131.423 35.6217 1 5 -11 5 8851.43 266.770 1 -5 -11 -5 8289.14 280.928 2 -5 11 -6 979.732 41.7159 2 -5 -11 -6 1005.88 105.444 2 5 -11 6 1031.08 97.1067 1 -5 -11 -7 1468.73 128.346 2 -5 11 -7 1344.79 60.3990 2 5 -11 7 1352.89 113.166 1 -5 -11 -8 1276.85 122.292 2 -5 11 -8 1248.76 66.3266 2 5 -11 8 1425.39 121.808 1 -5 -11 -9 3992.82 226.734 2 -5 -11 -10 75.3129 41.7516 2 -5 -11 -11 2684.11 202.734 2 -5 -11 -12 26.2086 43.5462 2 -5 -11 -13 1158.70 145.470 2 -5 -11 -14 874.031 130.354 2 -5 -11 -15 1573.58 177.630 2 5 12 -20 317.242 71.0805 2 5 -12 -19 22.6491 63.9649 2 5 12 -19 36.3982 53.3627 2 5 -12 -18 456.430 96.8289 2 5 12 -18 420.184 89.6022 2 5 -12 -17-76.5721 67.3377 2 5 12 -17 13.7382 35.2457 2 5 -12 -16 362.790 89.5539 2 5 -12 -15 88.8484 41.7451 2 5 -12 -14 611.393 97.5327 2 5 -12 -14 684.504 73.3894 3 5 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73.6780 1 5 -12 -2 842.284 49.4261 2 -5 12 2 856.172 47.8757 2 5 -12 -2 839.818 83.8063 3 5 -12 -1 1553.02 104.013 1 -5 -12 1 1625.63 59.1110 1 5 -12 -1 1837.80 120.485 3 5 -12 -1 1605.22 52.9730 2 -5 -12 0 417.124 36.3669 1 5 -12 0 373.109 51.6229 1 5 -12 0 385.264 59.8901 3 5 -12 1 3927.89 165.147 1 -5 -12 -1 4112.38 125.325 1 5 -12 1 4133.74 184.791 3 5 -12 2 2040.84 132.659 3 5 -12 2 1894.83 116.882 1 5 -12 3 122.023 47.3915 3 5 -12 3 102.607 29.1450 1 5 -12 4 609.806 73.3053 1 5 -12 5 1942.98 131.018 1 -5 -12 -5 1882.69 142.315 2 -5 -12 -6 1660.71 135.716 2 5 -12 6 1926.78 132.785 1 -5 -12 -7 998.786 112.455 2 5 -12 7 1217.68 109.457 1 -5 -12 -8 220.376 64.2399 2 5 -12 8 236.687 55.4512 1 -5 -12 -9 151.536 54.4367 2 -5 -12 -10 16.0216 42.0525 2 -5 -12 -11 279.269 73.6653 2 -5 -12 -12 50.6788 57.6267 2 -5 -12 -13 250.879 83.0639 2 -5 -12 -14 227.941 70.5717 2 -5 -12 -15 98.9278 67.2422 2 5 -13 -19 61.1366 41.9686 2 5 -13 -18 244.607 71.2402 2 5 -13 -17 219.872 69.0106 2 5 -13 -16 299.803 84.3224 2 5 -13 -15 52.3233 52.0307 2 5 -13 -14 4235.00 252.962 2 5 -13 -14 4500.54 193.858 3 5 -13 -13-113.469 54.9423 2 5 -13 -13-11.5026 31.5717 3 5 -13 -12 4277.74 230.330 2 -5 -13 12 3743.69 151.021 3 5 -13 -12 4123.43 180.833 3 5 -13 -11 1953.08 152.498 2 5 -13 -11 2136.19 132.168 3 -5 -13 11 2071.88 114.372 3 5 -13 -10 2390.92 159.956 2 -5 -13 10 2389.48 125.332 3 5 -13 -10 2534.31 144.120 3 5 -13 -9 3181.05 174.353 2 5 -13 -9 3447.26 162.449 3 -5 -13 9 3163.49 146.133 3 5 -13 -8 1027.31 92.3265 2 5 -13 -8 1119.59 94.7249 3 -5 -13 8 1102.59 86.3090 3 5 -13 -7 971.606 85.8699 2 5 -13 -7 1082.16 94.1180 3 -5 -13 7 909.653 79.9447 3 5 -13 -6 7293.88 218.061 2 5 -13 -6 7332.69 259.231 1 5 -13 -6 7349.25 233.738 3 -5 -13 6 6906.70 215.119 3 5 -13 -5 825.724 89.1244 1 5 -13 -5 801.802 82.2899 3 5 -13 -5 829.529 68.8546 2 5 -13 -4 457.905 49.0233 2 5 -13 -4 382.803 58.5917 1 5 -13 -4 428.446 60.5499 3 -5 13 4 526.142 51.3968 2 5 -13 -3 669.984 76.4695 3 5 -13 -3 809.539 80.9198 1 -5 13 3 690.313 50.7316 2 5 -13 -3 754.965 55.8025 2 5 -13 -2 8096.83 254.309 3 5 -13 -2 8157.21 244.862 1 5 -13 -2 7970.25 149.905 2 5 -13 -1 1273.85 95.9743 1 -5 -13 1 1165.90 49.3250 1 5 -13 -1 1280.21 105.338 3 5 -13 -1 1141.10 44.0565 2 5 -13 0 4263.47 190.518 3 5 -13 0 3984.29 169.543 1 -5 -13 0 4362.21 114.480 1 5 -13 1 362.635 64.6964 3 -5 -13 -1 491.744 44.4574 1 5 -13 1 416.137 56.3363 1 5 -13 2 3244.99 156.037 1 5 -13 2 3080.86 170.223 3 5 -13 3 1642.61 113.026 1 5 -13 3 1579.26 122.773 3 5 -13 4 1426.45 110.387 1 -5 -13 -5 9946.44 322.316 2 5 -13 5 10967.2 308.419 1 5 -13 6 1638.14 122.896 1 -5 -13 -6 1638.49 137.161 2 -5 -13 -7 867.575 104.474 2 5 -13 7 1151.86 107.203 1 5 -13 8 2075.13 150.973 1 -5 -13 -8 1709.57 147.991 2 -5 -13 -9 519.146 93.6114 2 -5 -13 -10 1738.91 160.708 2 -5 -13 -11 411.112 87.0238 2 -5 -13 -12 431.996 95.0443 2 -5 -13 -13 1038.78 143.596 2 -5 -13 -14 362.025 100.432 2 -5 -13 -15 377.851 93.6295 2 5 -14 -18-75.7357 76.8461 2 5 -14 -17-19.4562 58.9151 2 5 -14 -16 81.7132 56.9678 2 5 -14 -15 119.888 54.1784 2 5 -14 -14 426.696 84.0764 2 5 -14 -14 545.036 78.7855 3 5 -14 -13 682.855 103.709 2 5 -14 -13 496.249 68.8838 3 5 -14 -12 274.097 69.3978 2 -5 -14 12 242.975 43.4214 3 5 -14 -12 393.642 65.2852 3 5 -14 -11 1209.35 120.439 2 -5 -14 11 1167.77 92.4272 3 5 -14 -11 1251.23 105.412 3 5 -14 -10 811.567 95.7833 2 -5 -14 10 825.841 77.2947 3 5 -14 -10 906.965 89.1010 3 5 -14 -9 317.638 60.2102 2 5 -14 -9 332.555 62.3262 3 -5 -14 9 221.518 44.5504 3 5 -14 -8 379.662 60.6878 2 5 -14 -8 375.731 60.0130 3 -5 -14 8 353.406 52.1051 3 5 -14 -7 494.365 64.1409 2 5 -14 -7 526.057 70.8828 3 -5 -14 7 498.330 63.8297 3 5 -14 -6 4.31250 28.9093 1 5 -14 -6 9.21330 26.6816 2 5 -14 -6 5.05778 33.9695 3 -5 -14 6-12.8552 33.8362 3 5 -14 -5 241.281 42.2403 2 5 -14 -5 169.262 42.6443 3 -5 -14 5 230.270 46.9747 3 5 -14 -5 285.341 56.5755 1 5 -14 -4 4098.03 187.562 1 5 -14 -4 4308.44 189.704 3 5 -14 -4 4207.12 142.990 2 5 -14 -3 1314.86 107.415 3 5 -14 -3 1142.54 96.9168 1 5 -14 -3 1265.21 72.1440 2 5 -14 -2 32.3705 32.8818 3 5 -14 -2 27.3333 12.0211 2 5 -14 -2 20.0872 25.3445 1 5 -14 -1 5.12157 40.3723 3 -5 -14 1-3.71181 9.42095 1 5 -14 -1-23.4767 30.7397 1 5 -14 -1 5.64232 5.75969 2 5 -14 0 2021.29 135.896 3 5 -14 0 2004.34 122.940 1 -5 -14 0 2046.57 79.4853 1 5 -14 1 2150.57 127.499 1 5 -14 1 2111.02 143.201 3 -5 -14 -1 2154.04 93.3274 1 5 -14 2 730.999 75.1867 1 5 -14 2 669.683 86.7543 3 5 -14 3 3830.31 176.196 1 5 -14 3 3689.23 193.159 3 5 -14 4 4954.53 205.996 1 5 -14 5 254.520 53.7765 1 -5 -14 -5 308.731 67.4013 2 5 -14 6 381.477 66.3328 1 -5 -14 -6 401.791 72.1124 2 5 -14 7 304.607 60.6539 1 -5 -14 -7 196.294 60.0210 2 -5 -14 -8 436.744 84.5865 2 5 -14 8 394.131 69.1228 1 -5 -14 -9 645.587 101.971 2 -5 -14 -10 381.394 78.5336 2 -5 -14 -11 143.342 56.5244 2 -5 -14 -12-94.7411 72.9727 2 -5 -14 -13 259.536 83.7682 2 -5 -14 -14 15.8728 43.4044 2 5 -15 -18 474.908 107.903 2 5 -15 -17 92.6268 64.0983 2 5 -15 -16 977.805 139.390 2 5 -15 -15 1028.05 136.051 2 5 -15 -14 787.841 114.609 2 5 -15 -14 957.080 98.4756 3 5 -15 -13 950.460 122.342 2 5 -15 -13 1058.59 102.673 3 5 -15 -12 2701.57 187.732 2 -5 -15 12 1971.40 123.447 3 5 -15 -12 2714.98 159.906 3 -5 -15 11 1227.52 99.1862 3 5 -15 -11 1345.45 128.461 2 5 -15 -11 1467.33 118.905 3 5 -15 -10 2565.78 170.117 2 -5 -15 10 2532.06 144.065 3 5 -15 -10 2930.90 162.311 3 5 -15 -9 325.408 63.5437 2 5 -15 -9 232.833 53.6131 3 -5 -15 9 217.432 43.9116 3 5 -15 -8 1897.35 129.967 2 5 -15 -8 1761.44 129.647 3 -5 -15 8 1734.28 119.796 3 5 -15 -7 14.5923 24.4077 2 5 -15 -7-5.68660 37.9635 1 5 -15 -7-15.1172 39.9106 3 -5 -15 7 34.9611 29.1520 3 5 -15 -6 752.888 75.5817 2 5 -15 -6 743.258 83.8679 3 5 -15 -6 687.910 87.9024 1 -5 -15 6 692.956 77.4684 3 5 -15 -5 2876.86 165.979 1 -5 -15 5 2717.83 149.865 3 5 -15 -5 2656.20 154.681 3 5 -15 -5 2624.42 125.030 2 5 -15 -4 2838.09 157.303 1 5 -15 -4 2847.93 160.498 3 5 -15 -4 2681.46 116.036 2 5 -15 -3 1909.92 132.366 3 5 -15 -3 1984.92 131.065 1 5 -15 -3 1835.14 88.5622 2 5 -15 -2 5260.29 206.420 1 5 -15 -2 5331.54 223.992 3 5 -15 -2 5237.07 124.631 2 5 -15 -1 4387.03 185.393 1 5 -15 -1 4511.13 208.915 3 5 -15 -1 3774.44 77.8350 2 5 -15 0 7099.04 262.428 3 5 -15 0 6975.52 233.600 1 5 -15 1 1954.02 140.913 3 5 -15 1 1993.39 126.430 1 5 -15 2 17.8522 33.8167 3 5 -15 2 30.6062 26.1198 1 5 -15 3 1057.39 97.6251 1 5 -15 3 1040.93 111.352 3 5 -15 4 2786.75 175.608 3 5 -15 4 2985.82 163.824 1 5 -15 5 19.1271 32.4954 1 -5 -15 -5 19.7157 37.6709 2 5 -15 6 314.180 57.4988 1 -5 -15 -6 320.371 66.2012 2 -5 -15 -7 1461.37 138.951 2 5 -15 7 1754.04 137.257 1 -5 -15 -8 1398.37 140.194 2 5 -15 8 1577.76 134.339 1 -5 -15 -9 1775.31 166.648 2 -5 -15 -10 55.6418 50.7107 2 -5 -15 -11 661.988 116.523 2 -5 -15 -12 665.677 117.267 2 -5 -15 -13 120.547 65.3170 2 -5 -15 -14 1032.33 148.768 2 5 -16 -18 690.650 130.732 2 5 -16 -17 34.3841 76.4914 2 5 -16 -16 97.4907 64.3143 2 5 -16 -15 53.6005 52.3882 2 5 -16 -14 33.9690 46.1709 2 5 -16 -14 36.2166 41.2082 3 5 -16 -13 926.689 121.120 2 5 -16 -13 989.292 105.257 3 5 -16 -12 1112.13 128.235 2 -5 -16 12 967.153 90.2743 3 5 -16 -12 1147.71 111.100 3 5 -16 -11 36.3327 45.0226 2 5 -16 -11 59.1775 44.6994 3 -5 -16 11 103.915 39.8761 3 5 -16 -10 1121.38 116.423 2 -5 -16 10 1019.62 96.0478 3 5 -16 -10 1086.06 108.500 3 5 -16 -9 65.4852 34.3436 2 5 -16 -9 72.7423 41.4447 3 -5 -16 9 70.2691 27.3230 3 5 -16 -8 754.969 86.2094 2 5 -16 -8 793.273 91.1171 3 -5 -16 8 697.130 81.4840 3 5 -16 -7 71.0079 34.2553 2 5 -16 -7 61.0536 36.1957 3 5 -16 -7 28.4246 31.4733 1 -5 -16 7 80.7441 34.5865 3 5 -16 -6-37.2425 27.9810 2 5 -16 -6 19.5654 33.9622 1 5 -16 -6-28.5609 35.9093 3 -5 -16 6 16.7269 32.9274 3 5 -16 -5 3069.02 137.317 2 5 -16 -5 3108.59 173.672 1 5 -16 -5 3062.43 172.120 3 -5 -16 5 2984.29 161.984 3 5 -16 -4 146.498 31.2354 2 5 -16 -4 137.491 44.3809 3 -5 -16 4 183.337 48.9943 3 5 -16 -4 194.130 43.7113 1 5 -16 -3 540.687 67.2676 1 5 -16 -3 489.637 76.0220 3 5 -16 -3 588.054 51.5915 2 5 -16 -2 283.005 57.8885 3 5 -16 -2 325.426 53.0974 1 5 -16 -2 265.717 28.4126 2 5 -16 -1-13.7984 29.2904 1 5 -16 -1 2.92732 38.8130 3 5 -16 0 1193.45 113.797 3 5 -16 0 1227.50 101.408 1 5 -16 1 159.337 55.1113 3 5 -16 1 69.4759 25.8320 1 5 -16 2 1030.92 115.065 3 5 -16 2 1016.89 95.2414 1 5 -16 3 1543.38 116.775 1 5 -16 3 1374.36 130.653 3 5 -16 4 92.4816 34.4393 1 5 -16 4 124.213 54.8725 3 -5 -16 -4 146.398 53.5634 2 5 -16 5 625.999 81.7101 1 -5 -16 -5 624.847 90.7268 2 5 -16 6-9.54605 36.4293 1 -5 -16 -6 31.3652 36.5857 2 5 -16 7 65.0469 35.8610 1 -5 -16 -7 60.3435 50.9429 2 -5 -16 -8-14.2857 44.7742 2 5 -16 8 19.0034 34.0957 1 -5 -16 -9 285.578 76.9160 2 -5 -16 -10 69.9796 52.7483 2 -5 -16 -11 96.0503 70.2806 2 -5 -16 -12 148.440 67.8150 2 -5 -16 -13 35.3484 43.4902 2 5 -17 -17 416.793 101.045 2 5 -17 -16-50.3777 66.7409 2 5 -17 -15 319.716 87.7287 2 5 -17 -14 123.378 62.0442 2 5 -17 -14 178.261 56.4060 3 5 -17 -13 1205.09 138.499 2 5 -17 -13 1340.94 124.279 3 5 -17 -12 68.8236 44.8627 2 5 -17 -12 103.337 46.2909 3 5 -17 -11 2965.57 197.326 2 5 -17 -11 3330.84 189.918 3 -5 -17 11 3134.20 171.183 3 5 -17 -10-16.6369 39.4391 2 5 -17 -10-5.51616 43.9481 3 -5 -17 10 17.9255 32.1782 3 5 -17 -9 1326.63 118.447 2 5 -17 -9 1523.11 130.677 3 -5 -17 9 1343.85 115.882 3 5 -17 -8 6.25706 35.2803 3 5 -17 -8 3.20458 27.3717 2 -5 -17 8 57.5973 38.1391 3 5 -17 -8-7.88551 34.6621 1 5 -17 -7 194.164 41.2290 2 5 -17 -7 250.808 59.3574 3 -5 -17 7 224.311 52.9337 3 5 -17 -7 231.959 59.5106 1 5 -17 -6 8.11452 20.5805 2 5 -17 -6-47.0866 49.2703 3 -5 -17 6-8.71908 30.2155 3 5 -17 -6-19.0289 39.7701 1 5 -17 -5 1995.56 112.363 2 5 -17 -5 1999.23 144.213 1 5 -17 -5 2131.84 147.033 3 -5 -17 5 2006.96 138.508 3 5 -17 -4 281.999 41.4683 2 5 -17 -4 404.949 80.2858 3 5 -17 -4 295.213 50.7139 1 -5 -17 4 239.111 53.8834 3 5 -17 -3 2524.03 105.366 2 5 -17 -3 3226.08 182.615 3 5 -17 -3 3283.35 173.193 1 -5 -17 3 3451.40 184.849 3 5 -17 -2 1134.32 102.280 1 5 -17 -2 1098.77 112.604 3 5 -17 -1 7314.84 280.907 3 5 -17 -1 7457.76 250.715 1 5 -17 0-35.5140 20.0732 1 5 -17 0-27.0548 38.6929 3 5 -17 1 487.948 80.2029 3 5 -17 1 531.753 70.1213 1 5 -17 2 189.400 62.5233 3 5 -17 2 166.825 40.5480 1 5 -17 3 156.753 60.2275 3 5 -17 3 136.490 41.2213 1 5 -17 4 196.345 56.1603 3 -5 -17 -4 195.238 58.4569 2 5 -17 4 296.094 60.5251 1 5 -17 5 2811.81 167.466 1 -5 -17 -5 2333.83 171.638 2 5 -17 6-27.2886 32.4498 1 -5 -17 -6 12.7869 38.8756 2 -5 -17 -7 1917.75 163.447 2 5 -17 7 2479.10 165.342 1 -5 -17 -8 1135.53 134.110 2 5 -17 8 1452.69 134.465 1 -5 -17 -9 1525.72 157.369 2 -5 -17 -10 300.532 80.8194 2 -5 -17 -11 819.321 124.305 2 -5 -17 -12-166.483 80.6366 2 -5 -17 -13 540.724 103.291 2 5 -18 -17 231.453 79.8770 2 5 -18 -16-57.6145 54.3383 2 5 -18 -15 77.1542 52.0080 2 5 -18 -14 732.527 118.899 2 5 -18 -14 427.294 78.8182 3 5 -18 -13 312.327 84.8878 2 5 -18 -13 412.774 79.1879 3 5 -18 -12 758.175 108.596 2 5 -18 -12 872.232 104.225 3 5 -18 -11 1072.31 122.485 2 -5 -18 11 1491.80 125.197 3 5 -18 -11 1244.20 122.975 3 5 -18 -10 787.963 101.498 2 5 -18 -10 820.426 100.628 3 -5 -18 10 732.085 89.3449 3 5 -18 -9 115.380 34.1549 2 5 -18 -9 110.531 45.7815 3 -5 -18 9 182.316 52.7852 3 -5 -18 8 44.2342 37.0461 3 5 -18 -8 8.57527 24.2780 2 5 -18 -8 24.8933 36.8484 1 5 -18 -8-15.7632 41.6234 3 5 -18 -7 81.8172 30.9143 2 5 -18 -7 178.845 53.7878 1 5 -18 -7 113.270 48.5048 3 -5 -18 7 103.824 40.2874 3 5 -18 -6 466.794 60.8978 2 5 -18 -6 543.793 78.7041 3 5 -18 -6 550.282 81.5516 1 -5 -18 6 526.772 77.4019 3 5 -18 -5 586.440 78.8192 1 5 -18 -5 459.868 55.6162 2 -5 -18 5 555.055 83.8427 3 5 -18 -5 607.873 83.9348 3 -5 -18 4 123.483 40.1158 3 5 -18 -4 225.036 39.9368 2 5 -18 -4 131.817 48.9256 1 5 -18 -4 142.531 44.4291 3 5 -18 -3 28.6079 24.5693 1 5 -18 -3 23.3851 39.5305 3 -5 -18 3-16.0003 43.5330 3 5 -18 -2 327.317 67.8740 3 5 -18 -2 318.864 50.9874 1 5 -18 -1 734.833 93.6251 3 5 -18 -1 697.122 80.1912 1 5 -18 0-26.8355 32.9678 1 5 -18 0 97.0991 56.2767 3 5 -18 1 400.191 77.9503 3 5 -18 1 447.037 63.0266 1 5 -18 2 30.9551 43.7193 3 5 -18 2 32.0755 20.2495 1 5 -18 3 582.293 87.7967 3 5 -18 3 594.434 79.1263 1 5 -18 4 387.708 70.3985 1 5 -18 4 277.997 70.7486 3 -5 -18 -4 418.990 81.9345 2 5 -18 5-36.9855 46.0767 3 5 -18 5 29.0326 38.2162 1 -5 -18 -5-55.5569 49.5288 2 5 -18 6 718.020 90.6908 1 -5 -18 -6 532.281 88.7797 2 5 -18 7-46.6489 49.3355 1 -5 -18 -7 74.3364 50.7130 2 -5 -18 -8 87.5689 47.8744 2 5 -18 8 175.033 60.0317 1 -5 -18 -9 180.335 65.1124 2 -5 -18 -10 89.8024 58.4843 2 -5 -18 -11 219.827 73.6706 2 -5 -18 -12 196.635 69.9526 2 5 -19 -16 25.8537 55.5306 2 5 -19 -15 169.879 73.9187 2 5 -19 -14 962.551 132.146 2 5 -19 -14 1030.92 121.640 3 5 -19 -13 37.5668 41.8411 2 5 -19 -13 59.9345 40.0920 3 5 -19 -12 926.711 119.834 2 5 -19 -12 814.116 104.613 3 5 -19 -11 444.852 83.7462 2 -5 -19 11 433.548 72.8289 3 5 -19 -11 511.581 83.0060 3 5 -19 -10 2036.63 159.694 2 -5 -19 10 2108.32 156.004 3 5 -19 -10 2319.96 166.985 3 5 -19 -9 1414.21 128.018 2 5 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177.983 68.2061 3 5 -19 4 187.233 51.7176 1 -5 -19 -4 74.1211 51.2946 2 5 -19 5 426.041 73.0914 1 5 -19 5 433.217 86.2448 3 -5 -19 -5 281.933 71.2264 2 -5 -19 -6 2236.06 180.401 2 5 -19 6 2838.20 177.031 1 -5 -19 -7 660.964 101.935 2 5 -19 7 902.436 107.940 1 -5 -19 -8 1597.89 165.163 2 5 -19 8 1671.89 145.068 1 -5 -19 -9-33.6590 56.4191 2 -5 -19 -10 212.265 65.3791 2 -5 -19 -11 13.4292 49.9587 2 5 -20 -16 424.369 110.230 2 5 -20 -15 82.2812 68.3561 2 5 -20 -14 6.09757 42.1245 2 5 -20 -14 28.4222 45.6521 3 5 -20 -13 567.841 99.6674 2 5 -20 -13 558.748 91.2676 3 5 -20 -12 116.182 53.8906 2 5 -20 -12 61.8579 42.6658 3 5 -20 -11 1236.51 131.242 2 -5 -20 11 990.494 107.768 3 5 -20 -11 1214.81 127.101 3 5 -20 -10 633.663 93.7777 2 -5 -20 10 613.092 91.1674 3 5 -20 -10 637.134 97.1086 3 5 -20 -9 307.596 59.2304 2 5 -20 -9 296.387 67.7678 1 5 -20 -9 287.426 62.1995 3 -5 -20 9 375.142 75.7914 3 5 -20 -8 40.2549 24.9218 2 5 -20 -8 113.545 45.7079 1 5 -20 -8 70.6769 39.4174 3 -5 -20 8 43.1801 44.4520 3 5 -20 -7 437.992 77.9456 3 -5 -20 7 513.966 79.8746 3 5 -20 -7 449.397 78.0647 1 5 -20 -6 21.6612 44.6604 3 5 -20 -6 60.3054 34.0807 1 -5 -20 6 32.9539 37.8094 3 5 -20 -5 1223.28 122.443 3 -5 -20 5 1328.27 128.085 3 5 -20 -5 1197.36 115.264 1 5 -20 -4 252.003 55.3352 1 5 -20 -4 233.777 67.7690 3 -5 -20 4 195.872 61.0126 3 5 -20 -3 2145.93 147.432 1 5 -20 -3 2183.70 166.251 3 -5 -20 3 2272.40 167.005 3 5 -20 -2 799.301 87.7726 1 5 -20 -2 929.479 113.520 3 -5 -20 2 1031.20 118.698 3 5 -20 -1 95.0985 23.7760 1 5 -20 -1 96.7676 54.5241 3 -5 -20 1 39.8283 44.8372 3 5 -20 0 399.203 62.5123 1 5 -20 0 334.653 70.4948 3 5 -20 1 1333.07 136.919 3 5 -20 1 1553.49 125.788 1 5 -20 2 280.405 75.7010 3 5 -20 2 108.575 35.1758 1 5 -20 3 243.392 70.7411 3 5 -20 3 216.875 52.7347 1 -5 -20 -3 195.801 56.9791 2 -5 -20 -4 15.4034 36.7521 2 5 -20 4 77.5097 45.7017 1 5 -20 4 5.91963 45.8220 3 5 -20 5 580.792 84.9957 1 5 -20 5 566.944 99.7255 3 -5 -20 -5 572.754 95.0233 2 5 -20 6 64.1664 30.1687 1 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1 -6 3 -5 684.373 62.7715 2 -6 -3 -6 197.115 48.1729 2 -6 3 -6 203.759 39.4908 2 6 -3 6 201.776 43.0503 1 -6 3 -7 3.93251 28.2216 2 -6 -3 -7-18.3941 27.4211 2 -6 3 -8 760.756 80.8601 2 -6 -3 -8 579.827 73.0467 2 -6 3 -9 28.4156 30.6038 2 -6 -3 -9 47.4227 31.0097 2 -6 3 -10 2583.21 161.354 2 -6 -3 -10 2368.18 169.033 2 -6 3 -11 74.6995 45.0006 2 -6 -3 -11 21.4014 41.1631 2 -6 3 -12 3799.12 209.462 2 -6 -3 -12 3729.54 226.804 2 -6 -3 -13-5.54719 38.2979 2 -6 3 -13 9.63880 45.0506 2 -6 -3 -14 211.860 75.2010 2 -6 3 -14 256.475 71.2819 2 -6 3 -15-26.1022 46.1428 2 -6 -3 -15-23.5762 46.3183 2 -6 3 -16 394.170 97.1035 2 -6 -3 -16 267.882 74.8431 2 -6 3 -17-10.5938 56.6114 2 -6 -3 -17 50.9701 70.5567 2 6 4 -21 271.034 77.6021 2 6 -4 -21 79.2063 42.6793 2 6 4 -20 299.505 78.7869 2 6 -4 -20 259.309 78.2747 2 6 4 -19 168.830 69.2947 2 6 -4 -19 60.9925 54.6165 2 6 -4 -18 959.848 126.777 2 6 4 -18 1261.10 150.483 2 6 4 -17 2343.51 192.389 2 6 -4 -17 2016.53 177.506 2 6 -4 -16 947.959 118.415 2 6 4 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6.84999 41.0939 2 -6 4 -13 1359.07 134.116 2 -6 -4 -13 1315.79 143.516 2 -6 4 -14 518.302 90.2051 2 -6 -4 -14 462.475 93.9381 2 -6 4 -15 1300.40 139.492 2 -6 -4 -15 1134.00 144.074 2 -6 4 -16 287.455 64.7058 2 -6 -4 -16 183.520 61.9355 2 -6 -4 -17 307.060 82.3193 2 6 5 -21-8.10374 54.6886 2 6 -5 -21 47.0730 29.7258 2 6 5 -20-107.019 61.9653 2 6 -5 -20 8.69128 48.3173 2 6 -5 -19-19.8256 42.2137 2 6 5 -19 38.8505 54.0756 2 6 -5 -18 116.594 56.7740 2 6 5 -18 117.291 60.3706 2 6 -5 -17 91.8700 50.3955 2 6 5 -17 61.7529 44.5864 2 6 -5 -16 76.0787 39.7793 2 6 5 -16-9.96965 49.4687 2 6 -5 -15-11.1358 44.2641 2 6 5 -15-103.923 58.8026 2 6 -5 -14 251.372 72.8991 2 6 5 -14 289.431 77.3259 2 6 -5 -13 716.900 96.2792 2 6 -5 -13 807.476 46.1178 3 6 5 -13 854.273 101.113 2 6 -5 -12 88.3521 46.7976 2 6 -5 -12 81.5236 16.8284 3 6 5 -12 56.7078 40.5652 2 6 -5 -11 1813.54 73.3210 3 6 5 -11 1787.28 130.449 2 6 -5 -11 1603.37 127.064 2 -6 -5 10 240.301 16.3107 3 6 -5 -10 319.063 33.1429 3 6 5 -10 330.223 62.1717 2 6 -5 -10 254.421 52.5395 2 -6 -5 9 495.735 29.2755 3 6 -5 -9 528.539 43.2859 3 6 5 -9 569.544 73.3283 2 6 -5 -9 521.370 66.1661 2 6 -5 -8 7859.96 162.294 3 -6 5 8 7461.95 154.469 3 6 -5 -8 7714.36 233.142 2 6 -5 -7 3256.03 108.472 3 -6 5 7 3123.27 103.755 3 6 -5 -7 3249.84 144.026 2 6 -5 -6 80.2026 28.9219 3 6 5 -6 53.3247 20.4790 1 6 -5 -6 113.186 44.7888 1 -6 5 6 59.6890 15.8746 3 6 -5 -6 51.4482 27.3896 2 6 5 -5 1271.96 59.1030 1 -6 5 5 1319.37 71.9714 3 6 -5 -5 1352.00 94.3320 1 6 -5 -5 1382.10 86.4628 2 -6 5 4 51.1658 20.6347 2 6 -5 -4 37.9571 28.4155 1 6 5 -4 3.20195 17.5028 1 6 -5 -4 24.3056 18.4395 2 -6 -5 3 242.701 27.2520 1 6 -5 -3 243.363 47.6094 1 6 5 -3 214.472 25.9621 1 -6 5 3 193.864 25.6491 2 6 -5 -2 1418.10 91.0846 1 6 5 -2 1426.61 68.1111 1 -6 -5 2 1415.57 63.9142 1 -6 5 2 1453.06 70.7007 2 -6 -5 1 60.0046 15.5041 1 6 5 -1 17.9336 15.2163 1 6 -5 -1 28.4873 26.2738 1 -6 5 1-6.48629 17.3566 2 -6 -5 0 142.899 23.4543 1 6 5 0 132.128 23.2870 1 6 -5 0 109.576 27.6765 1 6 5 1 13.5731 18.6733 1 6 -5 1 33.3905 18.3152 1 6 -5 2 90.8730 31.5693 1 6 -5 3 948.019 82.0985 1 6 -5 4-16.0380 29.3022 1 -6 5 -4 24.4894 17.1264 2 6 -5 5 212.379 46.4850 1 -6 5 -5 210.809 35.2843 2 -6 5 -6 700.620 64.5290 2 -6 -5 -6 662.558 79.6153 2 6 -5 6 668.973 80.5596 1 -6 5 -7 556.726 63.5461 2 -6 -5 -7 541.690 77.8640 2 6 -5 7 492.553 73.1964 1 -6 5 -8-25.8766 30.1531 2 -6 -5 -8-33.0787 34.4552 2 -6 5 -9 51.7601 30.8246 2 -6 -5 -9 52.1955 45.8542 2 -6 5 -10 182.337 45.2358 2 -6 -5 -10 143.453 48.0932 2 -6 5 -11 540.727 79.4978 2 -6 -5 -11 519.397 86.8085 2 -6 5 -12 234.061 58.0863 2 -6 -5 -12 241.252 66.2420 2 -6 5 -13 601.534 89.6309 2 -6 -5 -13 590.745 99.1532 2 -6 5 -14-8.43605 35.8232 2 -6 -5 -14 6.21773 43.5315 2 -6 5 -15 21.5034 40.3728 2 -6 -5 -15-98.5453 60.3339 2 -6 -5 -16-80.8948 76.8538 2 -6 -5 -17 38.0659 48.8486 2 6 6 -21 103.042 55.0636 2 6 -6 -20 494.481 104.085 2 6 6 -20 728.586 126.271 2 6 -6 -19 72.6534 59.5373 2 6 6 -19 31.9795 54.1245 2 6 6 -18 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69.3121 18.2392 1 6 -6 -5 59.8203 23.4558 2 6 -6 -5 86.0048 30.8420 3 6 -6 -4 12647.8 243.127 3 6 6 -4 12484.5 174.177 1 6 -6 -4 12763.7 243.996 2 6 -6 -4 12788.1 282.103 1 -6 6 4 12915.0 232.246 2 -6 -6 3 1053.76 51.4186 1 6 6 -3 1057.31 53.8388 1 6 -6 -3 1038.23 81.2838 1 6 -6 -3 1071.99 68.0929 2 -6 6 3 1215.83 67.9995 2 -6 -6 2 391.594 33.2336 1 6 6 -2 391.189 35.2342 1 6 -6 -2 354.146 44.2212 1 -6 6 2 388.212 34.2882 2 6 -6 -1 471.914 54.6061 1 -6 -6 1 472.783 38.7240 1 -6 6 1 496.224 39.0350 2 6 6 -1 417.290 39.1054 1 -6 -6 0 8844.66 182.201 1 6 -6 0 8568.33 223.953 1 -6 6 0 8533.52 154.125 2 6 6 0 8948.42 186.315 1 6 -6 1 3861.55 153.142 1 6 -6 2 14037.2 302.057 1 6 -6 3 871.678 79.6700 1 -6 6 -3 907.172 54.5948 2 6 -6 4 10226.4 273.929 1 -6 6 -4 10145.0 191.570 2 6 -6 5 38.4911 31.6814 1 -6 6 -5 13.8948 17.0449 2 -6 6 -6 1166.42 77.4337 2 -6 -6 -6 1055.42 102.837 2 6 -6 6 1081.21 98.5240 1 -6 6 -7-6.70492 23.3938 2 -6 -6 -7-31.6520 37.0190 2 6 -6 7 14.0139 29.4564 1 -6 6 -8 3347.42 148.718 2 -6 -6 -8 3181.14 181.920 2 -6 6 -9 4635.53 188.181 2 -6 -6 -9 4253.92 221.621 2 -6 6 -10 1502.41 115.860 2 -6 -6 -10 1529.35 141.301 2 -6 6 -11 95.0934 36.6816 2 -6 -6 -11 28.4739 42.0562 2 -6 6 -12 1724.45 137.106 2 -6 -6 -12 1568.23 155.710 2 -6 6 -13-36.7747 34.7359 2 -6 -6 -13 22.8708 39.6249 2 -6 6 -14 1409.67 134.720 2 -6 -6 -14 1452.35 155.618 2 -6 -6 -15 18.4428 40.4496 2 -6 -6 -16 1246.41 163.536 2 6 7 -21 270.930 97.3511 2 6 -7 -20 102.878 66.5327 2 6 7 -20 102.668 70.3806 2 6 -7 -19 87.0307 68.5380 2 6 7 -19 183.959 62.3827 2 6 -7 -18 270.128 77.7421 2 6 7 -18 313.135 88.4426 2 6 -7 -17-39.9497 56.9967 2 6 7 -17-23.1523 47.3414 2 6 -7 -16 313.641 80.5651 2 6 7 -16 312.042 80.5471 2 6 -7 -15-7.94301 57.5766 2 6 7 -15-3.52175 44.7952 2 6 -7 -14 123.984 62.9708 2 6 -7 -14 40.6473 15.4733 3 6 7 -14 158.381 56.2192 2 6 -7 -13 34.4866 43.5073 2 6 -7 -13 11.7604 24.0085 3 6 7 -13 42.2250 39.2267 2 6 -7 -12 232.390 61.5005 2 6 -7 -12 230.948 35.8399 3 6 7 -12 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814.011 42.5171 1 -6 9 2 809.381 46.6366 2 6 -9 -2 826.781 78.6180 1 6 -9 -2 799.811 75.2317 3 6 -9 -1 917.045 82.5898 3 -6 9 1 916.801 42.8840 2 -6 -9 1 1001.71 53.5136 1 6 -9 -1 994.756 82.2032 1 -6 9 0 677.615 31.3731 2 -6 -9 0 744.914 52.4634 1 6 -9 0 756.413 74.7315 1 6 -9 1 275.984 48.3155 1 -6 9 -1 206.509 15.5220 2 -6 9 -2 341.909 20.2263 2 6 -9 2 386.571 56.3099 1 -6 9 -2 300.215 18.2889 2 -6 9 -3 243.980 19.1680 2 6 -9 3 294.663 53.9719 1 -6 9 -4 188.258 20.5580 2 6 -9 4 157.005 39.2907 1 6 -9 5 990.950 95.4953 1 -6 9 -5 1062.86 54.0117 2 6 -9 6 38.5233 30.4258 1 -6 9 -6-0.46555 16.7871 2 -6 -9 -6-28.9381 40.1418 2 6 -9 7 30.7972 29.6917 1 -6 9 -7 8.78544 20.9606 2 -6 -9 -7-38.1104 41.9927 2 -6 9 -8-10.4533 25.3208 2 -6 -9 -8 5.97650 37.6262 2 6 -9 8-12.2927 33.0391 1 -6 9 -9 13.0850 19.6848 2 -6 -9 -9 65.3964 53.2129 2 -6 9 -10 155.684 34.6917 2 -6 -9 -10 199.103 60.0783 2 -6 -9 -11 72.9364 40.5362 2 -6 -9 -12 410.108 89.7760 2 -6 -9 -13 54.8394 56.2432 2 -6 -9 -14 298.019 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182.319 76.3817 2 7 -19 9-0.35123 40.7545 1 -7 -19 -10 375.924 103.886 2 7 -20 -16 45.1782 64.2585 2 7 -20 -15 255.547 83.4370 2 7 -20 -14 29.6285 48.0596 2 7 -20 -13 170.723 65.4595 2 7 -20 -13 201.389 59.8222 3 7 -20 -13 363.754 88.3889 1 7 -20 -12 3.33002 43.1666 3 7 -20 -12 3.18697 46.2477 1 7 -20 -11 306.935 76.4030 3 7 -20 -11 404.745 87.6073 1 7 -20 -10 19.5146 46.6118 1 7 -20 -10 81.6013 44.7627 3 -7 -20 10 54.0445 37.0313 3 7 -20 -9 1527.85 156.750 1 7 -20 -9 1251.56 130.810 3 -7 -20 9 1365.46 127.273 3 7 -20 -8 85.1335 48.6015 1 7 -20 -8 69.8079 49.7791 3 -7 -20 8 33.2480 31.2513 3 7 -20 -7 11.8017 37.6585 3 -7 -20 7 38.2825 36.4200 3 7 -20 -7 12.3228 40.0604 1 7 -20 -6 104.817 48.5917 1 7 -20 -6 149.234 55.1548 3 -7 -20 6 41.0409 34.0881 3 7 -20 -5 15.8707 27.9482 1 7 -20 -5 61.3696 57.8631 3 -7 -20 5-13.9196 39.6646 3 -7 -20 4 386.108 82.4870 3 7 -20 -4 182.881 55.9882 3 7 -20 -4 249.184 51.0025 1 7 -20 -3 923.224 104.070 1 7 -20 -3 1050.10 126.501 3 7 -20 -2 11.1024 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42.2700 1 -8 6 -6 64.4388 25.9021 2 -8 -6 -6 53.9738 37.8585 2 -8 6 -7 98.3905 40.4834 2 -8 -6 -7 4.94466 43.0912 2 8 -6 7 57.2450 41.8680 1 -8 6 -8 235.488 46.2853 2 -8 -6 -8 104.612 48.2471 2 8 -6 8 162.480 48.2814 1 -8 -6 -9 554.609 89.6149 2 -8 6 -9 500.327 68.6711 2 -8 6 -10 157.587 48.4375 2 -8 -6 -10 56.5114 41.4086 2 -8 6 -11 87.3578 43.4668 2 -8 -6 -11 177.372 64.7812 2 -8 -6 -12 38.7528 55.2403 2 -8 -6 -13-17.3207 60.4644 2 -8 -6 -14-124.065 55.6268 2 -8 -6 -15-9.93683 39.7278 2 8 7 -21 146.613 74.2526 2 8 7 -20 669.596 94.9679 2 8 -7 -20 732.681 134.317 2 8 7 -19 277.755 83.7735 2 8 -7 -19 158.315 60.7888 2 8 7 -18 34.6921 42.9315 2 8 -7 -18 59.2250 49.6401 2 8 7 -17 907.609 122.429 2 8 -7 -17 865.651 123.899 2 8 7 -16 292.868 78.3434 2 8 -7 -16 245.468 68.9056 2 8 7 -15 3825.17 235.162 2 8 -7 -15 3614.27 230.305 2 8 7 -14 1414.90 137.565 2 8 -7 -14 1460.74 138.539 2 8 -7 -13 1445.67 138.603 2 8 -7 -12 1466.17 132.900 2 -8 -7 11 592.209 39.6611 3 8 -7 -11 582.844 82.2204 2 8 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5664.49 171.422 2 8 -7 5 5172.53 228.400 1 8 -7 6 463.253 78.2160 1 -8 -7 -6 460.657 75.7861 2 -8 7 -6 621.813 71.4803 2 -8 7 -7 3201.92 146.156 2 -8 -7 -7 2840.27 181.734 2 8 -7 7 2786.61 179.733 1 -8 7 -8 664.249 71.2584 2 -8 -7 -8 609.424 93.5994 2 8 -7 8 641.239 97.0794 1 -8 7 -9 1069.56 96.3095 2 -8 -7 -9 736.913 102.124 2 -8 7 -10 1799.39 126.181 2 -8 -7 -10 2187.38 177.667 2 -8 -7 -11 238.778 78.4390 2 -8 -7 -12 1501.37 163.403 2 -8 -7 -13 1253.34 154.991 2 -8 -7 -14-20.5135 44.9160 2 -8 -7 -15 913.986 134.931 2 8 8 -21 532.666 121.972 2 8 8 -20 98.7167 55.2568 2 8 -8 -20 4.62835 40.1741 2 8 8 -19 47.5015 39.5284 2 8 -8 -19 23.3755 55.3645 2 8 8 -18 121.580 53.4245 2 8 -8 -18 77.6207 61.5841 2 8 8 -17 254.399 70.9377 2 8 -8 -17 205.068 74.1788 2 8 8 -16 239.964 68.7839 2 8 -8 -16 270.530 75.1138 2 8 -8 -15 635.311 100.771 2 8 -8 -14-27.7997 37.7606 2 8 -8 -13 727.606 61.9011 3 8 -8 -13 878.885 113.774 2 8 -8 -12 3392.83 132.462 3 8 -8 -12 3167.78 190.457 2 8 -8 -11-24.8860 29.9236 3 -8 -8 11 5.51534 13.0017 3 8 -8 -11-18.1652 41.6198 2 8 -8 -10 79.2212 28.2741 3 -8 -8 10 53.4979 19.5312 3 8 -8 -10 29.9046 35.5047 2 8 8 -10 76.4098 27.7410 1 8 -8 -9 1257.35 85.8651 3 8 -8 -9 1275.15 115.744 1 8 -8 -9 1211.74 107.049 2 8 8 -9 1142.63 67.3822 1 8 8 -8 3083.01 103.500 1 8 -8 -8 3005.56 156.409 2 8 -8 -8 3391.31 182.204 1 8 -8 -7 824.236 88.5669 1 8 -8 -7 864.221 81.8681 2 8 8 -7 808.057 50.7380 1 8 -8 -6 127.994 42.9729 1 8 -8 -6 83.1365 26.9820 2 8 8 -6 84.8194 17.8412 1 8 -8 -5 403.283 67.8136 1 8 8 -5 379.353 37.6500 1 8 -8 -5 344.442 49.5693 2 8 -8 -4 859.665 87.8121 1 8 8 -4 930.108 59.7312 1 -8 -8 4 938.812 56.5240 1 -8 8 3 32.1784 22.9060 2 8 8 -3 15.4989 14.7377 1 -8 -8 3-3.53391 10.7219 1 8 -8 -3-3.53209 36.2370 1 8 8 -2-7.92567 21.1747 1 8 -8 -2 31.6244 26.0854 1 -8 -8 2 7.29443 9.32804 1 -8 8 2 22.8786 16.3716 2 8 -8 -1 737.502 80.2105 1 -8 8 1 782.358 53.8721 2 8 8 -1 851.468 66.8240 1 -8 8 0 267.781 32.3726 2 8 -8 0 329.172 56.7949 1 8 -8 1 799.406 83.6996 1 -8 8 -1 913.427 58.4522 2 8 -8 2 458.322 69.2336 1 8 -8 3-41.1384 43.6107 1 -8 8 -3-19.2519 21.6040 2 8 -8 4-6.17928 34.5889 1 -8 8 -4-14.6477 22.8877 2 8 -8 5 465.911 71.8734 1 -8 8 -5 525.450 52.3442 2 8 -8 6 26.8762 30.8419 1 -8 8 -6-4.24447 29.1352 2 -8 -8 -6 36.3160 39.6938 2 8 -8 7 218.671 57.7751 1 -8 8 -7 212.944 39.5674 2 -8 -8 -7 181.162 57.5185 2 -8 8 -8 183.156 37.4593 2 -8 -8 -8 206.380 57.2862 2 8 -8 8 205.569 62.2842 1 -8 -8 -9 330.295 74.2770 2 -8 -8 -10 159.643 58.6809 2 -8 -8 -11 67.5227 48.1615 2 -8 -8 -12 119.140 63.1529 2 -8 -8 -13-50.7251 42.5962 2 -8 -8 -14 130.511 72.4215 2 8 9 -21 305.044 88.4605 2 8 9 -20 156.745 79.0146 2 8 -9 -20 54.7729 31.4381 2 8 9 -19 194.059 61.8126 2 8 -9 -19 37.9944 40.6415 2 8 9 -18 593.478 105.034 2 8 -9 -18 476.527 100.889 2 8 -9 -17-54.2295 56.8182 2 8 -9 -16 1104.26 137.896 2 8 -9 -15 56.1403 46.6660 2 8 -9 -14 2222.77 174.132 2 8 -9 -13 1110.13 80.0441 3 8 -9 -13 1033.29 122.595 2 8 -9 -12 1668.70 99.1471 3 8 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74.2137 1 -8 9 1 569.704 44.5007 2 8 -9 0 2512.45 149.220 1 -8 9 0 2598.48 87.3507 2 8 -9 1 1122.75 102.928 1 -8 9 -1 1025.56 54.4667 2 8 -9 2 2069.52 140.414 1 -8 9 -2 2151.08 77.3998 2 -8 9 -2 2189.73 80.2982 2 8 -9 3 1706.90 131.560 1 -8 9 -3 1862.96 73.6777 2 8 -9 4 3822.48 196.653 1 -8 9 -4 4123.54 120.460 2 8 -9 5 832.427 97.8776 1 -8 9 -5 985.811 65.6193 2 -8 9 -6 8142.05 192.437 2 -8 -9 -6 7740.34 296.389 2 8 -9 6 7905.01 299.857 1 8 -9 7 98.5417 55.2288 1 -8 -9 -7 189.463 67.7040 2 -8 -9 -8 1546.77 145.264 2 8 -9 8 1517.72 141.340 1 -8 -9 -9 698.150 102.486 2 -8 -9 -10 2891.09 210.643 2 -8 -9 -11 1245.83 147.068 2 -8 -9 -12 778.893 118.122 2 -8 -9 -13 42.8859 68.6405 2 -8 -9 -14 1607.22 174.671 2 8 -10 -19 296.170 85.0959 2 8 -10 -18 238.989 80.7528 2 8 -10 -17 20.8197 41.8012 2 8 -10 -16 779.929 112.234 2 8 -10 -15 96.2480 51.3349 2 8 -10 -14 1037.93 125.688 2 8 -10 -13 1965.53 111.100 3 8 -10 -13 1720.08 150.472 2 8 -10 -12 34.6260 30.6208 3 8 -10 -12 30.0699 38.2045 2 8 -10 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412.471 68.1657 1 8 -10 0 3265.27 175.010 1 -8 10 0 3087.59 85.7885 2 8 -10 1-12.1242 35.4811 1 -8 10 -1 43.6468 12.3063 2 -8 10 -2 565.918 34.7791 2 8 -10 2 566.588 81.9277 1 -8 10 -2 571.157 34.6512 2 8 -10 3 112.586 40.5499 1 -8 10 -3 133.022 19.8956 2 8 -10 4 130.007 39.0585 1 -8 10 -4 265.615 30.1788 2 8 -10 5 324.062 67.3396 1 8 -10 6 602.690 87.3458 1 -8 -10 -6 587.432 86.9851 2 8 -10 7 266.983 62.0548 1 -8 -10 -7 333.208 75.3997 2 -8 -10 -8 21.4957 31.7228 2 8 -10 8 77.1495 51.5464 1 -8 -10 -9 182.812 60.4524 2 -8 -10 -10 361.583 81.7205 2 -8 -10 -11-60.9497 63.2208 2 -8 -10 -12 65.8014 52.8486 2 -8 -10 -13 224.156 85.3129 2 8 -11 -19 822.044 142.888 2 8 -11 -18 123.336 62.7210 2 8 -11 -17 1003.01 136.437 2 8 -11 -16 712.512 114.673 2 8 -11 -15 1026.55 128.951 2 8 -11 -14 122.918 51.2705 2 8 -11 -13 2503.73 132.544 3 8 -11 -13 2198.24 170.510 2 8 -11 -12 183.828 43.6332 3 8 -11 -12 205.424 58.6215 2 8 -11 -11 3860.19 165.108 3 -8 -11 11 3269.96 128.215 3 8 -11 -11 3469.51 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9-4.45062 16.9058 3 10 0 -8 764.629 79.2185 1 10 0 -7 11.2028 30.0981 1 10 0 -6 2444.54 135.059 1 10 0 -5 25.1636 27.0048 1 10 0 -4 13447.5 313.315 1 10 0 -3 0.50226 28.1826 1 10 0 -2 1372.72 103.192 1 10 0 -1-46.5592 34.6605 1 10 0 0 2826.55 157.198 1 10 0 1 58.2594 40.2837 1 10 0 2 141.145 48.0136 1 10 0 3-31.1799 36.6944 1 10 0 4 2941.41 177.049 1 10 0 5-53.8122 49.8766 1 -10 0 -6 3415.93 183.332 2 -10 0 -7-9.99607 34.8901 2 -10 0 -8 1421.37 124.242 2 -10 0 -9 10.0140 47.5350 2 -10 0 -10 211.928 59.1612 2 -10 0 -11-39.4187 38.0328 2 -10 0 -12 550.804 94.3157 2 -10 0 -13-11.1505 36.4222 2 -10 0 -14 1360.06 157.162 2 10 1 -20 106.941 51.2892 2 10 -1 -20 33.6662 58.1975 2 10 1 -19 385.752 90.6936 2 10 -1 -19 426.655 95.1341 2 10 1 -18 36.7220 53.2060 2 10 -1 -18 6.35925 48.8416 2 10 1 -17 39.5010 46.0471 2 10 -1 -17 30.4374 42.2030 2 10 1 -16 176.089 65.8401 2 10 -1 -16 204.293 73.7525 2 10 1 -15 1095.51 132.576 2 10 -1 -15 989.296 129.566 2 10 1 -14 172.872 52.6204 2 10 -1 -14 211.539 59.3060 2 10 1 -13 2589.49 188.683 2 10 -1 -13 2814.28 194.653 2 10 1 -12 1369.59 116.310 1 10 -1 -12 1372.83 117.789 1 10 -1 -12 1080.11 124.901 2 10 1 -12 1199.84 125.928 2 10 1 -11 1557.74 115.101 1 10 -1 -11 1525.36 136.398 2 10 -1 -11 1636.93 124.852 1 10 1 -10 357.606 57.4729 1 10 -1 -10 358.265 60.3003 1 10 -1 -9 593.198 73.6476 1 10 1 -9 629.350 70.3238 1 10 1 -8 842.098 82.6403 1 10 -1 -8 783.928 82.7540 1 10 1 -7 3925.19 165.534 1 10 -1 -7 3686.89 169.298 1 10 1 -6 585.486 66.7345 1 10 -1 -6 560.012 69.8272 1 10 1 -5 5043.58 187.239 1 10 -1 -5 5065.69 198.465 1 10 1 -4 8.63627 23.7109 1 10 -1 -4 42.1145 31.5459 1 10 1 -3 1750.29 112.200 1 10 -1 -3 1786.34 118.070 1 10 1 -2-15.1139 28.5419 1 10 -1 -2 18.1196 21.3435 1 10 1 -1 1739.91 119.563 1 10 -1 -1 1653.67 118.824 1 10 1 0 1099.86 97.7678 1 10 -1 0 1190.81 106.512 1 10 1 1 5372.39 217.587 1 10 -1 1 5147.33 216.017 1 10 1 2 42.0011 26.2050 1 10 -1 2 8.12593 26.7618 1 10 1 3 336.013 65.5446 1 10 -1 3 291.877 56.9376 1 10 1 4 106.619 41.2671 1 10 -1 4 24.1573 45.5046 1 10 -1 5-57.8069 41.2529 1 10 1 5 339.377 73.2965 1 -10 1 -6 23.6955 36.7146 2 -10 -1 -6 10.8579 32.6456 2 10 -1 6 7.30812 40.0622 1 -10 1 -7 512.105 75.7089 2 -10 -1 -7 625.302 87.7990 2 -10 1 -8 365.870 62.7652 2 -10 -1 -8 320.363 64.6875 2 -10 1 -9 2066.79 161.047 2 -10 -1 -9 2011.21 160.009 2 -10 1 -10 444.503 89.3711 2 -10 -1 -10 425.579 84.5083 2 -10 1 -11 1179.72 129.952 2 -10 -1 -11 1184.65 134.706 2 -10 1 -12 116.043 48.1954 2 -10 -1 -12 192.160 59.2971 2 -10 1 -13 5.93466 38.9080 2 -10 -1 -13-63.4779 43.4985 2 -10 -1 -14-284.197 78.3825 2 -10 -1 -15 154.385 79.0129 2 10 2 -20-115.518 70.0346 2 10 -2 -20 81.2479 64.7559 2 10 2 -19 249.899 80.1060 2 10 -2 -19 214.779 69.5318 2 10 2 -18 184.944 69.1593 2 10 -2 -18 118.885 64.6033 2 10 2 -17 34.3478 40.5037 2 10 -2 -17 76.6298 49.9139 2 10 2 -16-51.6087 51.6413 2 10 -2 -16 4.22623 47.1787 2 10 2 -15 383.616 75.8879 2 10 -2 -15 349.927 74.3772 2 10 2 -14 2076.86 173.722 2 10 -2 -14 2116.32 176.240 2 10 2 -13 1872.11 162.743 2 10 -2 -13 1805.96 156.905 2 10 2 -12 76.8110 42.9345 1 10 -2 -12 68.5908 47.4637 1 10 -2 -12 29.3730 48.7792 2 10 2 -11 3424.91 167.632 1 10 -2 -11 3004.33 187.293 2 10 -2 -11 3607.65 188.283 1 10 2 -10 704.977 74.7619 1 10 -2 -10 647.571 87.7690 2 10 -2 -10 833.017 89.9329 1 10 -2 -9 287.001 54.1828 1 10 2 -9 296.454 47.9816 1 10 2 -8 495.724 62.7673 1 10 -2 -8 522.979 70.6279 1 10 2 -7 2368.03 126.601 1 10 -2 -7 2408.09 141.334 1 10 2 -6 135.659 34.4232 1 10 -2 -6 144.979 37.2681 1 10 -2 -5 9331.02 272.391 1 10 2 -5 8969.48 243.655 1 10 -2 -4 282.976 52.4745 1 10 2 -4 241.177 46.8418 1 10 2 -3 4127.79 169.521 1 10 -2 -3 4025.29 181.772 1 10 2 -2 2874.26 146.590 1 10 -2 -2 2746.08 152.190 1 10 2 -1 1312.59 101.937 1 10 -2 -1 1359.88 107.409 1 10 2 0 1923.44 126.928 1 10 -2 0 1956.77 135.318 1 10 2 1 96.9895 33.3034 1 10 -2 1 92.3182 41.5887 1 10 -2 2 1302.39 115.913 1 10 2 2 1168.28 105.426 1 10 2 3 4329.41 207.477 1 10 -2 3 4308.54 210.307 1 10 -2 4 609.164 83.4699 1 10 2 4 637.617 84.6518 1 -10 2 -5 4708.22 196.419 2 10 -2 5 5283.20 249.856 1 -10 2 -6 900.737 91.5494 2 -10 -2 -6 850.048 94.8244 2 10 -2 6 881.852 110.802 1 -10 2 -7 2521.67 157.017 2 -10 -2 -7 2606.81 170.362 2 -10 2 -8 194.126 55.1088 2 -10 -2 -8 282.140 70.1413 2 -10 2 -9 84.5824 36.0472 2 -10 -2 -9 153.554 57.4257 2 -10 2 -10 34.3840 42.8303 2 -10 -2 -10 19.0795 45.6729 2 -10 2 -11 410.886 83.8267 2 -10 -2 -11 315.477 73.6624 2 -10 2 -12-54.9926 54.1191 2 -10 -2 -12 56.1636 60.3210 2 -10 -2 -13 857.415 122.192 2 -10 -2 -14 243.972 66.2699 2 10 3 -20 580.082 114.454 2 10 -3 -20 563.458 124.725 2 10 3 -19-41.3795 56.1309 2 10 -3 -19-8.47803 54.5767 2 10 3 -18 181.401 57.0707 2 10 -3 -18 314.430 81.8564 2 10 3 -17 101.708 65.2917 2 10 -3 -17 127.085 58.8279 2 10 3 -16 509.347 97.2676 2 10 -3 -16 358.463 77.7042 2 10 3 -15 34.8002 38.5245 2 10 -3 -15 19.5703 47.3114 2 10 3 -14 4926.41 263.419 2 10 -3 -14 4582.79 255.223 2 10 -3 -13 249.913 76.0943 2 10 -3 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2 10 -3 5 1046.09 115.665 1 -10 3 -6 1667.70 123.018 2 -10 -3 -6 1482.05 128.168 2 10 -3 6 1569.97 142.863 1 -10 3 -7 274.893 57.3405 2 -10 -3 -7 223.319 63.0828 2 10 -3 7 160.836 53.6535 1 -10 3 -8 2001.04 144.654 2 -10 -3 -8 1877.09 153.445 2 -10 3 -9 14.2532 45.0531 2 -10 -3 -9 28.8934 40.5151 2 -10 3 -10 1740.78 147.246 2 -10 -3 -10 1620.62 152.728 2 -10 3 -11-46.1612 53.5957 2 -10 -3 -11 26.9071 62.8202 2 -10 -3 -12 68.3334 44.9757 2 -10 -3 -13-20.2194 48.2826 2 -10 -3 -14-17.6988 53.3410 2 10 4 -20 558.198 117.507 2 10 -4 -20 629.896 126.186 2 10 4 -19 17.1605 46.5686 2 10 -4 -19 220.550 82.1022 2 10 4 -18 122.245 53.2148 2 10 -4 -18-5.21487 49.0783 2 10 4 -17 34.3459 46.2220 2 10 -4 -17 64.7744 48.6809 2 10 4 -16-123.102 75.5025 2 10 -4 -16 20.1695 54.8264 2 10 4 -15 1264.03 135.285 2 10 -4 -15 1366.80 151.494 2 10 -4 -14 1221.03 133.740 2 10 4 -13 2445.89 145.071 1 10 -4 -13 2393.58 180.713 2 10 4 -12 1342.63 103.484 1 10 -4 -12 1213.76 115.898 1 10 -4 -12 1225.98 125.708 2 10 4 -11 433.708 62.6395 1 10 -4 -11 403.476 76.3081 2 10 -4 -11 464.855 75.0729 1 10 -4 -10 579.735 84.6069 2 10 4 -10 810.578 77.2443 1 10 -4 -10 745.316 91.3935 1 10 -4 -9 992.051 97.6222 1 10 4 -9 924.817 78.6504 1 10 -4 -9 898.710 99.3510 2 10 -4 -8 453.481 69.8457 1 10 4 -8 440.725 54.3253 1 10 -4 -7 184.918 49.6796 1 10 4 -7 201.261 36.3758 1 10 -4 -6 9155.70 287.072 1 10 4 -6 9582.08 238.895 1 10 -4 -5 3018.04 164.143 1 10 4 -5 2874.36 131.862 1 10 -4 -4 221.151 46.5273 1 10 4 -4 224.678 41.9053 1 10 4 -3 3209.44 144.904 1 10 -4 -3 3306.84 170.244 1 10 4 -2 2351.02 129.156 1 10 -4 -2 2344.65 145.317 1 10 4 -1 0.99080 26.6207 1 10 -4 -1-36.6684 35.0396 1 10 4 0 149.518 41.3495 1 10 -4 0 90.9471 41.0040 1 10 4 1 51.9415 27.0839 1 10 -4 1 17.0931 30.5972 1 10 -4 2 1201.79 112.827 1 10 4 2 1370.96 115.720 1 10 -4 3 4035.60 210.060 1 10 4 3 4138.61 200.826 1 10 -4 4 2282.94 160.984 1 -10 4 -5 2343.61 135.681 2 10 -4 5 2336.56 168.446 1 -10 4 -6 2904.55 157.198 2 -10 -4 -6 3052.20 183.721 2 10 -4 6 2990.63 196.347 1 -10 4 -7 1211.07 109.425 2 -10 -4 -7 1197.63 118.992 2 10 -4 7 1178.27 133.882 1 -10 4 -8 283.284 59.0833 2 -10 -4 -8 243.901 60.8614 2 -10 4 -9 367.690 75.2288 2 -10 -4 -9 321.160 72.4727 2 -10 4 -10 516.213 85.9335 2 -10 -4 -10 296.339 75.5074 2 -10 -4 -11 196.917 65.0501 2 -10 -4 -12 496.741 100.988 2 -10 -4 -13 187.438 73.9921 2 -10 -4 -14 307.726 82.7477 2 10 5 -20 346.021 103.315 2 10 -5 -20 261.157 94.7859 2 10 5 -19 909.339 137.440 2 10 -5 -19 771.952 130.174 2 10 5 -18 265.968 80.4623 2 10 -5 -18 251.464 86.9199 2 10 5 -17 1052.39 139.301 2 10 -5 -17 816.882 120.401 2 10 5 -16-15.5291 58.9903 2 10 -5 -16-100.341 66.6784 2 10 -5 -15 3022.49 213.610 2 10 -5 -14-6.87411 49.6446 2 10 5 -13 4665.17 191.524 1 10 -5 -13 4308.04 237.751 2 10 -5 -12 1566.86 135.904 1 10 5 -12 1692.26 110.430 1 10 -5 -12 1668.63 146.608 2 10 5 -11 2631.98 135.815 1 10 -5 -11 2481.66 171.749 2 10 -5 -11 2675.07 171.188 1 10 -5 -10 2031.61 145.459 1 10 -5 -10 1773.90 141.339 2 10 5 -10 2080.27 115.129 1 10 5 -9 53.4245 29.9279 1 10 -5 -9 79.7695 48.4604 1 10 -5 -9 40.6966 30.8360 2 10 5 -8 339.018 44.3956 1 10 -5 -8 415.302 67.7800 1 10 -5 -7 2661.58 160.682 1 10 5 -7 2550.71 121.402 1 10 -5 -6 1241.02 110.450 1 10 5 -6 1131.40 81.0255 1 10 -5 -5 6104.55 237.849 1 10 5 -5 6142.38 188.215 1 10 5 -4 3135.30 136.645 1 10 -5 -4 2880.06 165.429 1 10 5 -3 3264.37 144.900 1 10 -5 -3 3012.42 166.278 1 10 5 -2 936.049 84.5740 1 10 -5 -2 969.554 94.5763 1 10 5 -1 1408.25 107.173 1 10 -5 -1 1518.36 121.304 1 10 -5 0 838.280 93.1898 1 10 5 0 857.144 82.4300 1 10 -5 1 3984.78 201.439 1 10 5 1 4150.68 188.077 1 10 -5 2 306.178 65.7332 1 10 5 2 493.088 73.0879 1 10 -5 3 176.436 57.7048 1 10 -5 4 655.086 88.2737 1 10 -5 5 18.4399 44.1783 1 -10 5 -5 102.290 34.5693 2 -10 5 -6 1221.74 99.1429 2 10 -5 6 1262.29 132.643 1 -10 5 -7 561.369 70.0394 2 -10 -5 -7 409.939 77.9303 2 10 -5 7 490.104 86.4518 1 -10 5 -8 270.051 54.1778 2 -10 -5 -8 274.097 70.5662 2 -10 5 -9 1969.52 144.660 2 -10 -5 -9 1886.16 161.507 2 -10 -5 -10 150.603 58.2881 2 -10 -5 -11 783.838 121.151 2 -10 -5 -12 23.6445 53.9016 2 -10 -5 -13-66.0064 67.2073 2 10 6 -20 522.613 102.488 2 10 -6 -20 305.909 79.9900 2 10 6 -19 192.498 76.9457 2 10 -6 -19 192.704 83.2031 2 10 6 -18 2.03910 54.1128 2 10 -6 -18 126.871 71.0179 2 10 6 -17-50.0161 43.2241 2 10 -6 -17-46.4136 50.2626 2 10 -6 -16 391.125 89.6009 2 10 -6 -15 183.178 64.2397 2 10 -6 -14 1981.84 170.334 2 10 6 -13 453.396 59.5439 1 10 -6 -13 361.188 82.4311 2 10 -6 -12 1917.24 151.037 1 10 6 -12 1841.42 111.758 1 10 -6 -12 1546.11 140.998 2 10 6 -11 261.408 50.3925 1 10 -6 -11 274.728 65.3940 1 10 -6 -11 238.525 60.0480 2 10 6 -10 42.3288 22.3121 1 10 -6 -10-15.7998 40.5614 2 10 -6 -10 51.6612 31.1917 1 10 -6 -9 54.4886 46.6666 1 10 -6 -9-1.60335 41.7737 2 10 6 -9-1.13148 19.1530 1 10 6 -8 1851.52 100.860 1 10 -6 -8 1943.84 137.944 2 10 -6 -8 1928.93 139.009 1 10 6 -7-2.99355 18.1996 1 10 -6 -7-1.54951 28.2584 1 10 -6 -6 1275.63 115.529 1 10 6 -6 1254.95 82.8438 1 10 -6 -5 275.867 58.9934 1 10 6 -5 317.120 45.8400 1 10 6 -4 8742.20 225.672 1 10 -6 -4 8853.48 291.294 1 10 -6 -3 379.017 63.5792 1 10 6 -3 422.689 56.1995 1 10 -6 -2 720.919 87.0853 1 10 6 -2 789.703 75.1971 1 10 6 -1 240.799 47.7631 1 10 -6 -1 241.298 55.6912 1 10 -6 0 885.634 96.2719 1 10 6 0 1077.62 93.5219 1 10 -6 1 117.108 44.9473 1 10 6 1 206.034 45.8720 1 10 -6 2 350.482 72.1423 1 10 6 2 324.882 59.1593 1 10 -6 3 574.046 88.0643 1 10 -6 4 4930.63 240.257 1 -10 6 -4 4845.54 175.057 2 10 -6 5 402.688 75.0196 1 -10 6 -5 521.493 62.7296 2 -10 6 -6 1998.00 124.300 2 10 -6 6 2098.61 165.693 1 -10 6 -7 40.5648 44.0910 2 -10 -6 -7 65.7304 44.9428 2 10 -6 7 9.54258 37.7603 1 -10 6 -8 623.136 75.6677 2 -10 -6 -8 669.780 97.3689 2 10 -6 8 850.581 114.642 1 -10 -6 -9-1.24097 43.9720 2 -10 -6 -10 260.607 76.1396 2 -10 -6 -11 230.712 68.0390 2 -10 -6 -12 490.330 96.8485 2 -10 -6 -13 222.194 69.1621 2 10 7 -20 378.157 105.183 2 10 -7 -20 51.5357 58.3865 2 10 -7 -19 202.389 73.0119 2 10 -7 -18 69.4939 44.9245 2 10 -7 -17 81.4423 52.9510 2 10 -7 -16 1062.88 133.996 2 10 -7 -15 689.802 109.882 2 10 7 -14 984.724 87.8317 1 10 -7 -14 775.647 105.651 2 10 7 -13 1389.71 98.7793 1 10 -7 -13 1216.53 130.302 2 10 -7 -12 1489.46 138.511 1 10 7 -12 1451.64 97.1531 1 10 -7 -12 1352.46 132.691 2 10 -7 -11 3623.37 208.137 2 10 -7 -11 3740.74 210.612 1 10 7 -11 3889.14 151.324 1 10 7 -10 142.289 37.2910 1 10 -7 -10-5.57901 37.3503 2 10 -7 -10 113.689 49.4191 1 10 -7 -9 3690.63 197.677 1 10 7 -9 3551.56 135.923 1 10 -7 -9 3296.66 182.255 2 10 -7 -8 1580.56 126.095 2 10 -7 -8 1676.44 135.505 1 10 7 -8 1881.73 98.2503 1 10 7 -7 41.1115 23.4291 1 10 -7 -7 18.2429 32.9365 1 10 -7 -6 3527.88 190.213 1 10 7 -6 3660.29 136.567 1 10 -7 -5 999.455 103.838 1 10 7 -5 893.297 70.9450 1 10 -7 -4 2254.90 152.669 1 10 7 -4 2070.19 108.816 1 10 7 -3 4471.25 164.893 1 10 -7 -3 4608.05 214.948 1 10 -7 -2 435.974 64.8211 1 10 7 -2 440.981 54.6510 1 10 -7 -1 3493.24 189.042 1 10 7 -1 3684.61 161.550 1 10 -7 0 6748.76 263.732 1 10 7 0 6800.83 227.339 1 10 -7 1 153.054 49.2763 1 10 7 1 143.290 42.4894 1 10 -7 2 2845.89 179.470 1 10 -7 3-16.7869 42.0548 1 10 -7 4 303.798 68.0107 1 -10 7 -4 357.232 49.1771 2 10 -7 5 171.829 54.4901 1 -10 7 -5 255.573 44.4463 2 10 -7 6 175.553 60.4940 1 -10 7 -6 92.4198 32.6537 2 -10 -7 -7 1371.83 135.873 2 10 -7 7 1368.36 143.612 1 -10 -7 -8 625.856 101.637 2 10 -7 8 610.406 100.012 1 -10 -7 -9 1714.93 163.215 2 -10 -7 -10 914.710 121.862 2 -10 -7 -11 199.054 66.8835 2 -10 -7 -12 81.3022 52.5369 2 -10 -7 -13 191.813 80.3929 2 10 -8 -20 173.227 60.8351 2 10 -8 -19 569.313 112.216 2 10 -8 -18-78.2428 61.0096 2 10 -8 -17 12.5937 49.7053 2 10 -8 -16 366.384 80.0684 2 10 -8 -15 507.062 96.2733 2 10 8 -14 869.562 79.6014 1 10 -8 -14 786.633 111.838 2 10 8 -13 551.473 60.8771 1 10 -8 -13 543.040 91.7713 2 10 8 -12 378.974 51.7208 1 10 -8 -12 412.113 81.3652 1 10 -8 -12 305.484 62.2294 2 10 -8 -11 1976.07 159.086 1 10 8 -11 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360.398 82.8834 1 11 -14 -2 289.915 72.2075 1 11 -14 -1-15.2305 49.3489 1 11 -14 0 149.456 54.0702 1 11 -14 1 32.0990 41.8527 1 11 -14 2 26.7956 40.8163 1 11 -14 3-58.8093 58.2289 1 11 -14 4-15.4109 49.3958 1 11 -14 5 495.511 99.6627 1 11 -14 6-32.8899 58.1950 1 -11 -14 -6-35.0286 54.5203 2 11 -14 7-37.4417 52.5293 1 -11 -14 -7-130.852 81.8493 2 -11 -14 -8 65.4587 64.4831 2 11 -14 8 43.1880 62.1024 1 11 -14 9-28.9865 58.4107 1 11 -15 -18 121.778 61.5938 2 11 -15 -17 42.3233 60.4651 2 11 -15 -16 687.971 116.365 2 11 -15 -16 1021.47 138.999 1 11 -15 -15 219.040 67.9494 1 11 -15 -15 341.334 79.4563 2 11 -15 -14 435.594 93.8957 1 11 -15 -14 393.801 91.6814 2 11 -15 -13 671.459 108.064 1 11 -15 -13 487.913 85.0979 2 11 -15 -12 530.510 100.358 1 11 -15 -12 452.407 83.7280 2 11 -15 -11 202.206 63.8277 1 11 -15 -11 258.988 62.4743 2 11 -15 -10 881.251 124.495 1 11 -15 -10 736.109 99.8088 2 11 -15 -9 650.816 104.278 1 11 -15 -8 1476.22 155.302 1 11 -15 -7 1012.82 125.924 1 11 -15 -6 1071.38 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48.8388 1 17 -9 -12 5.14879 26.1542 1 17 -9 -11 237.067 65.5794 1 17 -9 -10 938.757 135.552 1 17 -9 -9-96.7464 46.8133 1 17 -9 -8 1226.88 152.401 1 17 -9 -7-9.23278 23.3941 1 17 -9 -6 963.572 137.354 1 17 -9 -5 131.358 50.7560 1 17 -9 -4 661.811 116.886 1 17 -9 -3 608.705 116.041 1 17 -9 -2 225.071 69.6930 1 17 -10 -11 24.4468 48.1409 1 17 -10 -10 63.2834 35.8980 1 17 -10 -9 412.141 88.5569 1 17 -10 -8 39.8156 48.5406 1 17 -10 -7-10.8879 51.4129 1 17 -10 -6 234.335 70.7073 1 17 -10 -5 83.6758 47.5400 1 17 -10 -3 12.7084 48.5915 1 17 -11 -9 687.116 117.202 1 17 -11 -8 247.379 69.6170 1 17 -11 -7 547.053 104.622 1 17 -11 -6-263.844 72.5398 1 17 -11 -5 945.949 141.719 1 18 0 -16 488.976 93.9440 1 18 0 -15 2.15723 35.8435 1 18 0 -14 393.383 78.1045 1 18 0 -13 158.886 48.8119 1 18 0 -12 522.658 89.4636 1 18 0 -11 53.5468 48.6340 1 18 0 -10 362.936 82.1589 1 18 0 -9 9.59290 26.8242 1 18 0 -8 515.789 88.7326 1 18 0 -7-0.71829 57.3098 1 18 0 -6 1489.96 160.642 1 18 0 -5-61.1778 61.5559 1 18 0 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81.6463 1 18 1 1 82.0824 68.7939 1 18 -2 -15 214.005 62.9879 1 18 -2 -14 76.2708 38.7852 1 18 2 -13 669.732 96.5225 1 18 -2 -13 540.409 96.7244 1 18 2 -12 3.93952 31.3272 1 18 -2 -12 20.1793 41.7254 1 18 -2 -11 418.092 88.5048 1 18 2 -11 259.445 59.5603 1 18 2 -10-48.0697 36.4496 1 18 -2 -10 32.5531 45.0439 1 18 2 -9 473.789 79.9917 1 18 -2 -9 481.673 96.4755 1 18 2 -8 202.149 63.2876 1 18 -2 -8 212.318 51.5642 1 18 2 -7 587.856 108.230 1 18 -2 -7 722.300 108.025 1 18 2 -6 436.782 99.3883 1 18 -2 -6 313.184 85.2673 1 18 2 -5 1089.49 139.587 1 18 -2 -5 1120.81 148.882 1 18 2 -4 210.830 74.0921 1 18 -2 -4 82.0521 50.9745 1 18 2 -3 953.346 128.921 1 18 -2 -3 1065.40 150.615 1 18 2 -2 6.12657 45.9959 1 18 -2 -2-43.4864 44.5203 1 18 2 -1 124.477 54.4424 1 18 -2 -1 134.086 70.2363 1 18 2 0 190.335 70.4605 1 18 -2 0 194.186 81.1916 1 18 2 1 166.415 70.6820 1 18 -3 -15 51.8209 32.4223 1 18 -3 -14 12.4498 39.3393 1 18 -3 -13 111.115 44.1075 1 18 -3 -12-48.9957 31.0883 1 18 -3 -11 8.42814 23.2474 1 18 3 -11 5.42254 15.5806 1 18 3 -10 1165.44 125.914 1 18 -3 -10 1175.47 150.884 1 18 3 -9 42.4836 50.0479 1 18 -3 -9 97.5773 30.4627 1 18 3 -8 297.267 78.5294 1 18 -3 -8 151.365 57.3971 1 18 3 -7 54.6665 52.5567 1 18 -3 -7 98.7818 31.6261 1 18 3 -6-88.2666 66.0523 1 18 -3 -6-59.8934 58.0248 1 18 3 -5 102.689 63.5853 1 18 -3 -5 129.398 80.3094 1 18 3 -4 237.268 81.6741 1 18 -3 -4 148.072 61.7946 1 18 3 -3 99.8463 51.8472 1 18 -3 -3 80.0676 65.5519 1 18 3 -2 653.199 108.425 1 18 -3 -2 651.035 119.880 1 18 3 -1 33.7715 55.7278 1 18 -3 -1-3.95428 50.8414 1 18 3 0 465.596 106.032 1 18 3 1-41.1028 65.6168 1 18 -4 -14 79.1592 42.1141 1 18 -4 -13 82.5785 40.9055 1 18 -4 -12-1.59040 12.0142 1 18 -4 -11 105.653 43.9821 1 18 -4 -10 622.260 111.254 1 18 4 -9 541.538 95.3690 1 18 -4 -9 570.744 104.067 1 18 4 -8 30.5445 43.9359 1 18 -4 -8 42.4818 46.1852 1 18 4 -7 1304.96 141.920 1 18 -4 -7 374.846 74.9505 1 18 4 -6 208.424 63.0356 1 18 -4 -6 118.566 56.2081 1 18 4 -5 633.678 104.811 1 18 -4 -5 546.416 109.678 1 18 4 -4 724.716 110.179 1 18 -4 -4 763.415 132.780 1 18 4 -3 228.468 64.3619 1 18 -4 -3 218.458 87.8970 1 18 4 -2 418.500 86.5091 1 18 -4 -2 334.444 90.8457 1 18 4 -1 263.276 81.9647 1 18 -4 -1 123.691 48.8310 1 18 4 0 27.7179 53.9574 1 18 4 1 219.399 79.2102 1 18 -5 -13 30.8147 51.4375 1 18 -5 -12 112.269 43.9700 1 18 -5 -11 119.906 43.8042 1 18 -5 -10-4.08296 45.9388 1 18 -5 -9 716.172 112.978 1 18 -5 -8 69.1382 48.0028 1 18 5 -7 18.1237 52.0000 1 18 -5 -7 141.713 54.5587 1 18 5 -6-49.6134 52.4681 1 18 -5 -6 67.4581 37.7453 1 18 5 -5 102.179 61.4671 1 18 -5 -5-19.6964 77.2435 1 18 5 -4-39.7037 43.7665 1 18 -5 -4-18.8842 68.7691 1 18 5 -3 23.6449 35.2397 1 18 -5 -3 12.1380 73.9456 1 18 5 -2-5.13779 45.4095 1 18 -5 -2 55.4932 59.9402 1 18 5 -1 376.094 90.4667 1 18 5 0 97.6793 61.1231 1 18 5 1 313.840 92.0334 1 18 -6 -12 407.802 87.5427 1 18 -6 -11 304.985 73.7657 1 18 -6 -10 752.784 119.358 1 18 -6 -9-8.51597 35.3292 1 18 -6 -8 1169.08 148.010 1 18 -6 -7-23.5145 24.8934 1 18 -6 -6 1240.82 151.069 1 18 -6 -5 125.352 65.2945 1 18 6 -4 962.961 125.451 1 18 -6 -4 936.011 143.292 1 18 6 -3 188.788 58.9314 1 18 -6 -3 258.651 97.2063 1 18 6 -2 257.117 71.9933 1 18 6 -1 19.5893 51.2871 1 18 6 0 90.4746 57.7236 1 18 -7 -11 100.951 48.4596 1 18 -7 -10 82.0413 41.1074 1 18 -7 -9 7.01312 38.4989 1 18 -7 -8 279.760 75.3526 1 18 -7 -7 177.874 58.3620 1 18 -7 -6-65.7711 51.9219 1 18 -7 -5-16.7770 53.7501 1 18 -7 -4 139.892 79.3433 1 18 -8 -9 669.835 114.466 1 18 -8 -8-13.2605 23.7055 1 18 -8 -7 581.708 108.504 1 18 -8 -6 509.368 103.450 1 19 0 -14 264.203 70.7935 1 19 0 -13-117.200 44.6293 1 19 0 -12 22.6978 22.5779 1 19 0 -11 2.27650 12.4780 1 19 0 -10 1372.64 152.910 1 19 0 -9-154.691 62.4906 1 19 0 -8 657.249 108.841 1 19 0 -7-91.6276 80.6462 1 19 0 -6 394.015 97.9521 1 19 0 -5-13.7678 54.4401 1 19 0 -4 119.518 62.1544 1 19 0 -3 70.8293 68.1197 1 19 -1 -14 247.353 69.1127 1 19 1 -13 327.886 73.3939 1 19 -1 -13 311.293 72.3646 1 19 -1 -12 361.800 83.9581 1 19 1 -12 557.141 89.2413 1 19 1 -11-77.3921 37.9561 1 19 -1 -11 56.7609 27.4989 1 19 1 -10 99.8014 48.2970 1 19 -1 -10 94.0713 40.7422 1 19 1 -9-28.8084 31.8394 1 19 -1 -9 40.9032 30.8896 1 19 1 -8 5.25377 44.6006 1 19 -1 -8 135.860 55.2938 1 19 1 -7 206.762 77.2428 1 19 -1 -7-8.86195 52.7123 1 19 1 -6-60.1208 74.0924 1 19 -1 -6 58.6165 59.6079 1 19 1 -5 505.032 109.679 1 19 -1 -5 646.292 117.717 1 19 1 -4 417.137 101.822 1 19 -1 -4 223.576 74.2219 1 19 1 -3 288.274 78.7556 1 19 -1 -3 468.139 113.298 1 19 1 -2 129.937 62.6495 1 19 -2 -13 85.8408 52.3829 1 19 -2 -12 117.506 46.3275 1 19 2 -11 212.606 63.8419 1 19 -2 -11 330.853 75.0514 1 19 2 -10 144.046 41.9254 1 19 -2 -10 108.113 45.3261 1 19 2 -9 650.404 109.136 1 19 -2 -9 825.834 114.907 1 19 2 -8 379.204 89.2844 1 19 -2 -8 313.848 78.2696 1 19 2 -7 221.557 80.8982 1 19 -2 -7 384.549 97.6343 1 19 2 -6 18.4694 51.1091 1 19 -2 -6 92.4739 55.9642 1 19 2 -5 11.1678 52.5623 1 19 -2 -5 75.5171 71.8977 1 19 2 -4 213.812 78.6583 1 19 -2 -4 346.622 104.865 1 19 2 -3 225.870 69.6980 1 19 2 -2-77.3221 68.0373 1 19 -3 -12 744.180 114.562 1 19 -3 -11 382.963 82.7965 1 19 -3 -10-85.5945 41.8293 1 19 3 -9 107.293 68.9042 1 19 -3 -9-75.9625 39.9934 1 19 3 -8 246.073 79.4480 1 19 -3 -8 54.9883 50.2940 1 19 3 -7 83.5442 44.6192 1 19 -3 -7 95.2075 57.9963 1 19 3 -6 400.663 92.8435 1 19 -3 -6 538.353 118.727 1 19 3 -5-55.3545 68.3585 1 19 -3 -5 15.1144 55.1964 1 19 3 -4 733.456 120.172 1 19 3 -3-109.295 57.0523 1 19 3 -2 242.461 71.0363 1 19 -4 -10 241.416 66.2362 1 19 -4 -9 392.209 87.0002 1 19 -4 -8 294.302 77.9471 1 19 -4 -7 637.591 110.869 1 19 4 -6 10.7644 52.6404 1 19 -4 -6-43.6769 52.0784 1 19 4 -5 444.680 103.005 1 19 4 -4 52.4802 45.5267 1 19 4 -3 59.1009 57.1966 1 19 4 -2 196.435 77.8371 1 19 4 -1 167.069 75.0405 1 19 5 -3 297.561 78.5665 1 19 5 -2 164.974 71.9884 1 19 5 -1-9.12247 45.8919 1 20 1 -11 591.288 131.758 1 20 1 -10 199.705 68.1459 1 20 1 -9 373.338 87.5593 1 20 1 -8 136.389 68.3222 1 20 1 -7 266.114 93.2197 1 20 2 -8 9.99711 62.5388 1 20 2 -7 9.24159 62.6971 1 20 2 -6-117.114 68.4427 1 20 3 -6 471.986 106.609 1 20 3 -5 73.0606 55.9410 1 0 0 0 0.00 0.00 0 TITL AK_Ru_47dmphen_20220919 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 14.962416 21.957208 17.114808 90.0000 109.2662 90.0000 ZERR 5.00 0.000776 0.000744 0.000870 0.0000 0.0058 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O F P Ru UNIT 255.00 265.00 10.00 5.00 30.00 15.00 5.00 TREF HKLF 4 END ; _shelx_hkl_checksum 64665 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL SIR92 run in space group P 21/c CELL 0.71073 14.9624 21.9572 17.1148 90.000 109.266 90.000 ZERR 4.00 0.0008 0.0007 0.0009 0.000 0.006 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O F P RU UNIT 204 172 8 4 24 12 4 MERG 2 MORE -1 FMAP 2 PLAN -10 ACTA BOND $H CONF ABIN omit 1 3 1 omit 0 2 0 omit -1 1 1 omit 0 2 1 omit 1 1 0 omit 1 2 0 omit -1 2 1 omit 0 1 2 omit 0 2 2 omit -1 2 3 omit -2 2 1 omit -6 0 2 omit -2 1 1 omit -6 5 3 omit 2 2 0 omit -6 6 2 omit 1 0 2 omit -2 0 4 omit -1 0 2 omit -1 2 2 omit -2 0 2 omit 0 3 2 omit -2 3 1 omit -2 1 3 omit 1 5 6 omit -1 3 3 omit 0 3 3 omit 1 2 1 L.S. 100 TEMP 25.00 WGHT 0.053000 3.050600 EXTI 0.000945 FVAR 0.96304 0.41698 MOLE 1 C2 1 0.630606 0.953556 0.693246 11.00000 0.05000 0.03929 = 0.03723 -0.00308 0.00938 -0.00933 AFIX 43 H2 2 0.568873 0.965755 0.664845 11.00000 -1.50000 AFIX 0 C3 1 0.654872 0.892723 0.687969 11.00000 0.07375 0.03931 = 0.04801 -0.00683 0.01687 -0.01103 AFIX 43 H3 2 0.609473 0.865606 0.656470 11.00000 -1.50000 AFIX 0 C4 1 0.744878 0.872492 0.728696 11.00000 0.08091 0.03420 = 0.05085 -0.00018 0.02561 0.00278 C5 1 0.910021 0.902160 0.817960 11.00000 0.06576 0.05359 = 0.08001 0.00668 0.02245 0.02424 AFIX 43 H5 2 0.931452 0.862489 0.817107 11.00000 -1.50000 AFIX 0 C6 1 0.971565 0.944910 0.859640 11.00000 0.04379 0.07364 = 0.08807 0.01056 0.01407 0.02642 AFIX 43 H6 2 1.034558 0.934174 0.885581 11.00000 -1.50000 AFIX 0 C7 1 1.003607 1.053559 0.910173 11.00000 0.03403 0.08260 = 0.06394 0.00705 0.00382 -0.00647 C8 1 0.964557 1.109077 0.913933 11.00000 0.03911 0.06701 = 0.07241 -0.00623 -0.00425 -0.01400 AFIX 43 H7 2 1.002429 1.140054 0.944770 11.00000 -1.50000 AFIX 0 C9 1 0.869850 1.120203 0.872834 11.00000 0.04687 0.04649 = 0.05310 -0.00768 0.00221 -0.01039 AFIX 43 H8 2 0.846327 1.158814 0.877097 11.00000 -1.50000 AFIX 0 C11 1 0.781928 0.976227 0.777642 11.00000 0.03694 0.03419 = 0.03288 0.00299 0.01126 0.00554 C12 1 0.812318 0.915664 0.774709 11.00000 0.05864 0.04045 = 0.04336 0.00516 0.01943 0.00757 C13 1 0.846761 1.021263 0.824649 11.00000 0.03371 0.04065 = 0.03707 0.00492 0.00922 0.00343 C14 1 0.942994 1.006489 0.865276 11.00000 0.03519 0.06187 = 0.05674 0.00569 0.00854 0.00551 C15 1 0.770913 0.806017 0.724950 11.00000 0.11735 0.04141 = 0.09429 -0.00675 0.03010 0.01551 AFIX 137 H15A 2 0.827238 0.803202 0.710013 11.00000 -1.50000 H15B 2 0.719990 0.785280 0.684331 11.00000 -1.50000 H15C 2 0.781981 0.787516 0.778138 11.00000 -1.50000 AFIX 0 C16 1 1.109023 1.042400 0.951207 11.00000 0.03542 0.12324 = 0.10973 0.01178 -0.00223 0.00327 AFIX 137 H16A 2 1.118770 1.002466 0.975393 11.00000 -1.50000 H16B 2 1.134624 1.072327 0.993602 11.00000 -1.50000 H16C 2 1.140258 1.045357 0.910544 11.00000 -1.50000 AFIX 0 C21 1 0.640803 1.170787 0.757911 11.00000 0.04778 0.04174 = 0.03794 -0.00203 0.01955 0.00232 C31 1 0.615428 1.160040 0.550260 11.00000 0.04037 0.03295 = 0.03581 0.00179 0.01154 -0.00263 C32 1 0.532270 1.180923 0.558789 11.00000 0.05372 0.05354 = 0.04061 0.00402 0.01288 0.01057 AFIX 43 H32 2 0.516054 1.169620 0.604741 11.00000 -1.50000 AFIX 0 C33 1 0.472041 1.219085 0.498608 11.00000 0.05952 0.06113 = 0.06167 0.00132 0.00528 0.01871 AFIX 43 H33 2 0.416459 1.233473 0.505111 11.00000 -1.50000 AFIX 0 C34 1 0.494569 1.235064 0.431006 11.00000 0.07739 0.04624 = 0.05796 0.01846 -0.00307 0.00024 AFIX 43 H34 2 0.455354 1.261441 0.392121 11.00000 -1.50000 AFIX 0 C35 1 0.574570 1.212684 0.419532 11.00000 0.07839 0.08785 = 0.06385 0.03915 0.02035 -0.00429 AFIX 43 H35 2 0.588000 1.222214 0.371633 11.00000 -1.50000 AFIX 0 C36 1 0.635620 1.175828 0.479211 11.00000 0.06025 0.08307 = 0.05881 0.03051 0.02833 0.00706 AFIX 43 H36 2 0.690700 1.161487 0.471690 11.00000 -1.50000 AFIX 0 C41 1 0.700120 1.041297 0.566389 11.00000 0.03513 0.03869 = 0.03182 -0.00267 0.01495 -0.00165 C42 1 0.618932 1.023329 0.502909 11.00000 0.03957 0.04669 = 0.05016 -0.00870 0.01055 -0.00140 AFIX 43 H42 2 0.566048 1.048558 0.487063 11.00000 -1.50000 AFIX 0 C43 1 0.616631 0.968140 0.463349 11.00000 0.05722 0.05921 = 0.05638 -0.02376 0.00454 -0.00263 AFIX 43 H43 2 0.562140 0.956445 0.421074 11.00000 -1.50000 AFIX 0 C44 1 0.694670 0.930298 0.486190 11.00000 0.07643 0.04913 = 0.06561 -0.02233 0.02433 0.00071 AFIX 43 H44 2 0.692827 0.893367 0.459098 11.00000 -1.50000 AFIX 0 C45 1 0.775265 0.947291 0.549144 11.00000 0.05775 0.04692 = 0.06673 -0.00815 0.02486 0.01161 AFIX 43 H45 2 0.827847 0.921803 0.564857 11.00000 -1.50000 AFIX 0 C46 1 0.777697 1.002574 0.589018 11.00000 0.03928 0.04961 = 0.04551 -0.00764 0.01542 0.00219 AFIX 43 H46 2 0.832193 1.013848 0.631586 11.00000 -1.50000 AFIX 0 C51 1 0.812664 1.147345 0.639042 11.00000 0.03507 0.04492 = 0.04128 0.00162 0.01235 -0.00550 C52 1 0.866869 1.134330 0.588241 11.00000 0.04769 0.07009 = 0.07072 -0.01295 0.03271 -0.01797 AFIX 43 H52 2 0.846588 1.104614 0.547473 11.00000 -1.50000 AFIX 0 C53 1 0.950438 1.165390 0.598287 11.00000 0.05861 0.10189 = 0.10631 -0.01709 0.04883 -0.02981 AFIX 43 H53 2 0.985774 1.156944 0.563928 11.00000 -1.50000 AFIX 0 C54 1 0.981560 1.209567 0.660364 11.00000 0.05837 0.10405 = 0.11070 -0.01706 0.03795 -0.04327 AFIX 43 H54 2 1.038233 1.230036 0.668018 11.00000 -1.50000 AFIX 0 C55 1 0.928771 1.222460 0.709395 11.00000 0.07334 0.07856 = 0.08038 -0.01934 0.02709 -0.03873 AFIX 43 H55 2 0.949517 1.251789 0.750645 11.00000 -1.50000 AFIX 0 C56 1 0.844187 1.192182 0.698337 11.00000 0.05962 0.06037 = 0.05561 -0.00956 0.02492 -0.02057 AFIX 43 H56 2 0.808036 1.202252 0.731449 11.00000 -1.50000 AFIX 0 C61 1 0.476468 1.099821 0.837769 11.00000 0.03338 0.03939 = 0.03970 0.00054 0.01391 0.00292 C62 1 0.440583 1.099798 0.903072 11.00000 0.05011 0.05966 = 0.04661 0.01179 0.02284 0.00564 AFIX 43 H62 2 0.477279 1.084732 0.954425 11.00000 -1.50000 AFIX 0 C63 1 0.350516 1.122054 0.892299 11.00000 0.05490 0.06838 = 0.06272 0.01226 0.03553 0.01407 AFIX 43 H63 2 0.327261 1.122046 0.936428 11.00000 -1.50000 AFIX 0 C64 1 0.295645 1.144098 0.816549 11.00000 0.04259 0.06364 = 0.08377 0.00211 0.03037 0.00931 AFIX 43 H64 2 0.234684 1.157949 0.809255 11.00000 -1.50000 AFIX 0 C65 1 0.329866 1.145827 0.751993 11.00000 0.05118 0.08287 = 0.05455 0.01390 0.01176 0.02435 AFIX 43 H65 2 0.292870 1.161576 0.701168 11.00000 -1.50000 AFIX 0 C66 1 0.420553 1.123900 0.762414 11.00000 0.04701 0.07511 = 0.04290 0.00810 0.01650 0.01626 AFIX 43 H66 2 0.443895 1.125412 0.718374 11.00000 -1.50000 AFIX 0 C71 1 0.569826 0.983947 0.855771 11.00000 0.04464 0.04281 = 0.04012 0.00656 0.01717 0.00325 C72 1 0.645510 0.944070 0.888317 11.00000 0.05864 0.05460 = 0.04677 0.01551 0.02070 0.01296 AFIX 43 H72 2 0.706376 0.959531 0.911883 11.00000 -1.50000 AFIX 0 C73 1 0.631069 0.881463 0.885958 11.00000 0.10155 0.05459 = 0.06686 0.02529 0.04063 0.02371 AFIX 43 H73 2 0.682096 0.855281 0.907824 11.00000 -1.50000 AFIX 0 C74 1 0.541852 0.858436 0.851489 11.00000 0.12656 0.04182 = 0.12410 0.00904 0.07360 -0.00481 AFIX 43 H74 2 0.532434 0.816540 0.850569 11.00000 -1.50000 AFIX 0 C75 1 0.466474 0.896185 0.818428 11.00000 0.08601 0.06033 = 0.14863 -0.01002 0.05434 -0.02024 AFIX 43 H75 2 0.406181 0.880024 0.794185 11.00000 -1.50000 AFIX 0 C76 1 0.480105 0.959704 0.821064 11.00000 0.04877 0.05202 = 0.09900 -0.00070 0.02238 -0.00401 AFIX 43 H76 2 0.428513 0.985477 0.799356 11.00000 -1.50000 AFIX 0 C81 1 0.662320 1.086398 0.957827 11.00000 0.03661 0.05999 = 0.03222 -0.00042 0.01020 0.00385 C82 1 0.705528 1.143121 0.970340 11.00000 0.08381 0.07592 = 0.03581 -0.00993 0.00911 -0.01430 AFIX 43 H82 2 0.699144 1.168240 0.925066 11.00000 -1.50000 AFIX 0 C83 1 0.757642 1.163016 1.048327 11.00000 0.11460 0.11095 = 0.04913 -0.02598 0.01470 -0.02983 AFIX 43 H83 2 0.784387 1.201719 1.055701 11.00000 -1.50000 AFIX 0 C84 1 0.770024 1.125256 1.115541 11.00000 0.08045 0.13879 = 0.03820 -0.01859 0.00423 0.00033 AFIX 43 H84 2 0.807192 1.137815 1.168122 11.00000 -1.50000 AFIX 0 C85 1 0.727697 1.069596 1.104665 11.00000 0.08825 0.11460 = 0.03087 0.00944 0.01509 0.02388 AFIX 43 H85 2 0.735251 1.044585 1.150253 11.00000 -1.50000 AFIX 0 C86 1 0.672976 1.049495 1.025832 11.00000 0.05952 0.08417 = 0.03549 0.01047 0.01411 0.01167 AFIX 43 H86 2 0.643903 1.011517 1.019164 11.00000 -1.50000 AFIX 0 N1 3 0.691554 0.994850 0.736934 11.00000 0.04132 0.03194 = 0.03054 0.00042 0.01190 -0.00100 N10 3 0.810083 1.078479 0.827219 11.00000 0.03147 0.04065 = 0.03434 -0.00048 0.00429 -0.00119 O22 4 0.627183 1.222479 0.762083 11.00000 0.10575 0.03929 = 0.06529 -0.00630 0.03679 0.01391 P1 6 0.698741 1.110180 0.626582 11.00000 0.03052 0.03327 = 0.03038 -0.00126 0.01188 -0.00163 P2 6 0.592910 1.065467 0.850963 11.00000 0.03215 0.04078 = 0.02887 0.00334 0.00951 0.00173 RU1 7 0.662877 1.089113 0.748584 11.00000 0.02960 0.03031 = 0.02647 -0.00177 0.00795 -0.00028 H1 2 0.559495 1.082844 0.685266 11.00000 -1.50000 MOLE 2 PART 1 F1A 5 0.741525 0.745195 0.925125 21.00000 0.14821 0.12337 = 0.09586 -0.02500 -0.04253 0.02951 F2A 5 0.867806 0.692836 1.064266 21.00000 0.22056 0.09907 = 0.28513 0.10151 0.15544 0.02175 F3A 5 0.861489 0.680187 0.967567 21.00000 0.12851 0.05516 = 0.27361 -0.00621 0.12952 0.00605 F4A 5 0.925341 0.742302 1.074989 21.00000 0.10672 0.16103 = 0.14185 0.02054 -0.03091 0.01090 F5A 5 0.808714 0.800501 1.032337 21.00000 0.13384 0.11089 = 0.12467 -0.06688 -0.00956 0.06346 F6A 5 0.884382 0.774750 0.947675 21.00000 0.51426 0.08655 = 0.29074 -0.00628 0.34568 -0.04350 PART 2 F1B 5 0.740620 0.740185 0.978060 -21.00000 0.06047 0.12393 = 0.41789 -0.01354 0.12300 -0.01406 F2B 5 0.797550 0.699842 1.050439 -21.00000 0.32375 0.12146 = 0.20451 -0.02184 0.19142 -0.08475 F3B 5 0.851234 0.698998 0.935247 -21.00000 0.10772 0.19552 = 0.16678 -0.12150 0.05570 -0.02994 F4B 5 0.957509 0.750438 1.030145 -21.00000 0.06162 0.08613 = 0.17847 -0.02081 0.03907 -0.00510 F5B 5 0.848812 0.793881 1.072199 -21.00000 0.20026 0.12806 = 0.19636 -0.07299 0.13923 -0.04494 F6B 5 0.847586 0.802853 0.947729 -21.00000 0.12794 0.10222 = 0.15311 0.05469 0.00745 -0.02551 PART 0 P3 6 0.842644 0.744306 1.001041 11.00000 0.06939 0.05698 = 0.09075 0.00093 0.04237 0.00218 HKLF 4 REM SIR92 run in space group P 21/c REM R1 = 0.0473 for 8859 Fo > 4sig(Fo) and 0.0709 for all 11913 data REM 638 parameters refined using 0 restraints END WGHT 0.0511 3.2028 REM Highest difference peak 0.463, deepest hole -0.702, 1-sigma level 0.070 Q1 1 0.8111 0.7567 0.9179 11.00000 0.05 0.46 Q2 1 0.6830 1.0901 0.7965 11.00000 0.05 0.41 Q3 1 0.5767 1.0228 0.8523 11.00000 0.05 0.37 Q4 1 0.6257 1.0785 0.9085 11.00000 0.05 0.37 Q5 1 0.5971 1.0813 0.7746 11.00000 0.05 0.35 Q6 1 0.5171 1.0791 0.8431 11.00000 0.05 0.34 Q7 1 0.3393 1.2291 0.7534 11.00000 0.05 0.34 Q8 1 0.3520 0.8801 0.7640 11.00000 0.05 0.33 Q9 1 0.8402 0.8323 0.9437 11.00000 0.05 0.33 Q10 1 0.6577 1.0890 0.8278 11.00000 0.05 0.32 ; _shelx_res_checksum 40992 _shelx_fab_file ; 0 0 2 -49.74 0.00 0 0 4 -96.69 0.00 0 0 6 48.76 0.00 0 0 8 10.62 0.00 0 0 10 -22.32 0.00 0 0 12 5.43 0.00 0 0 14 2.76 0.00 0 0 16 -3.28 0.00 0 0 18 -2.30 0.00 0 0 20 0.09 0.00 0 1 2 101.45 0.00 0 1 3 124.21 0.00 0 1 4 -31.09 0.00 0 1 5 -1.45 0.00 0 1 6 -17.34 0.00 0 1 7 -33.74 0.00 0 1 8 15.91 0.00 0 1 9 14.89 0.00 0 1 10 3.05 0.00 0 1 11 5.07 0.00 0 1 12 -5.43 0.00 0 1 13 -5.94 0.00 0 1 14 0.52 0.00 0 1 15 1.18 0.00 0 1 16 2.39 0.00 0 1 17 3.36 0.00 0 1 18 -1.87 0.00 0 1 19 0.13 0.00 0 1 20 1.01 0.00 0 1 21 0.67 0.00 0 2 0 144.21 0.00 0 2 1 -120.16 0.00 0 2 2 -1.72 0.00 0 2 3 -38.12 0.00 0 2 4 -34.79 0.00 0 2 5 48.61 0.00 0 2 6 23.74 0.00 0 2 7 -4.37 0.00 0 2 8 -4.48 0.00 0 2 9 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-0.21 0.00 -5 1 22 -0.10 0.00 -4 1 22 -0.82 0.00 -9 2 22 -0.47 0.00 -8 2 22 0.23 0.00 -7 2 22 0.73 0.00 -6 2 22 0.08 0.00 -5 2 22 0.00 0.00 -4 2 22 0.20 0.00 -9 3 22 -0.08 0.00 -8 3 22 -1.13 0.00 -7 3 22 0.12 0.00 -6 3 22 1.01 0.00 -5 3 22 0.06 0.00 -4 3 22 -0.75 0.00 -8 4 22 -0.02 0.00 -7 4 22 -0.11 0.00 -6 4 22 0.05 0.00 -5 4 22 0.06 0.00 -7 5 22 0.38 0.00 -6 5 22 1.67 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 270319) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.500 0.000 458 180 ' ' 2 0.000 1.000 0.500 458 180 ' ' 3 0.063 0.790 -0.016 6 -1 ' ' 4 0.063 0.710 0.484 6 -1 ' ' 5 0.937 0.210 0.016 7 -1 ' ' 6 0.937 0.290 0.516 7 -1 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 0 0 1.442 0 1 1 1.565 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL SIR92 run in space group P 21/c CELL 14.9624 21.9572 17.1148 90.00 109.27 90.00 SPGR P21/c # Solvent Accessible Volume = 948 # Electrons Found in S.A.V. = 360 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.848 0.115 0.358 ! 3.65 eA-3 C102 0.785 0.056 0.359 ! 3.56 eA-3 C103 0.832 0.334 0.859 ! 3.04 eA-3 Q104 0.955 0.748 0.018 ! 2.89 eA-3 C105 0.927 0.085 0.345 ! 2.78 eA-3 Q106 0.156 0.184 0.047 ! 2.22 eA-3 Q107 0.870 0.710 0.595 ! 2.14 eA-3 C108 0.119 0.488 0.173 ! 2.06 eA-3 Q109 0.154 0.211 0.582 ! 1.94 eA-3 Q110 0.224 0.204 0.452 ! 1.81 eA-3 C111 0.075 0.534 0.128 ! 1.72 eA-3 Q112 0.246 0.254 0.079 ! 1.71 eA-3 Q113 0.301 0.890 0.373 ! 1.46 eA-3 C114 0.932 0.985 0.358 ! 1.41 eA-3 C115 0.978 1.001 0.421 ! 1.20 eA-3 Q116 0.591 0.442 0.342 ! 0.98 eA-3 C117 1.000 0.087 0.360 ! 0.97 eA-3 Q118 0.154 0.244 0.502 ! 0.94 eA-3 C119 0.029 0.508 0.026 ! 0.94 eA-3 Q120 0.805 0.747 0.920 ! 0.91 eA-3 C121 0.966 0.961 0.470 ! 0.91 eA-3 C122 0.214 0.559 0.080 ! 0.89 eA-3 C123 0.158 0.691 0.186 ! 0.85 eA-3 Q124 0.062 0.065 0.440 ! 0.82 eA-3 C125 0.993 0.958 0.670 ! 0.82 eA-3 Q126 0.362 0.873 0.702 ! 0.78 eA-3 Q127 0.030 0.946 0.458 ! 0.77 eA-3 C128 0.999 0.557 0.015 ! 0.77 eA-3 Q129 0.287 0.673 0.140 ! 0.75 eA-3 Q130 0.957 0.474 0.076 ! 0.75 eA-3 Q131 0.948 0.422 0.001 ! 0.75 eA-3 Q132 0.064 0.623 0.030 ! 0.73 eA-3 Q133 0.846 0.032 0.454 ! 0.73 eA-3 C134 0.984 0.595 0.049 ! 0.72 eA-3 Q135 0.545 0.304 0.734 ! 0.71 eA-3 C136 0.736 0.171 0.290 ! 0.71 eA-3 Q137 0.342 0.598 0.206 ! 0.70 eA-3 Q138 0.088 0.444 0.033 ! 0.69 eA-3 C139 0.106 0.427 0.210 ! 0.69 eA-3 C140 0.974 0.521 0.092 ! 0.69 eA-3 Q141 0.692 0.365 0.892 ! 0.69 eA-3 Q142 0.670 0.171 0.308 ! 0.68 eA-3 Q143 0.751 0.796 0.719 ! 0.68 eA-3 Q144 0.651 0.799 0.744 ! 0.67 eA-3 Q145 0.867 0.380 0.950 ! 0.67 eA-3 Q146 0.267 0.576 0.390 ! 0.66 eA-3 Q147 0.183 0.571 0.220 ! 0.66 eA-3 Q148 0.499 0.695 0.316 ! 0.66 eA-3 C149 1.004 0.976 0.333 ! 0.66 eA-3 Q150 0.025 0.397 0.923 ! 0.66 eA-3 Q151 0.072 0.431-0.002 ! 0.65 eA-3 Q152 0.943 0.012 0.548 ! 0.65 eA-3 Q153 0.237 0.818 0.751 ! 0.65 eA-3 Q154 0.171 0.605 0.247 ! 0.64 eA-3 Q155 0.499 0.838 0.796 ! 0.63 eA-3 Q156 0.133 0.058 0.484 ! 0.63 eA-3 Q157 0.095 0.896 0.530 ! 0.63 eA-3 Q158 0.153 0.039 0.532 ! 0.62 eA-3 C159 0.874 0.577 0.875 ! 0.61 eA-3 Q160 0.324 0.641 0.233 ! 0.61 eA-3 Q161 0.567 0.695 0.327 ! 0.61 eA-3 Q162 0.678 0.348 0.844 ! 0.61 eA-3 Q163 0.099 0.786 0.689 ! 0.61 eA-3 Q164 0.237 0.279 0.714 ! 0.61 eA-3 Q165 0.201 0.507 0.047 ! 0.61 eA-3 Q166 0.704 0.025 0.294 ! 0.60 eA-3 Q167 0.796 0.719 0.270 ! 0.60 eA-3 C168 0.076 0.507 0.004 ! 0.60 eA-3 Q169 0.425 0.678 0.156 ! 0.60 eA-3 Q170 0.444 0.688 0.297 ! 0.59 eA-3 Q171 0.891 0.907 0.437 ! 0.59 eA-3 Q172 0.828 0.693 0.222 ! 0.59 eA-3 Q173 0.405 0.260 0.655 ! 0.59 eA-3 Q174 0.966 0.614 0.159 ! 0.59 eA-3 Q175 0.050 0.101 0.516 ! 0.59 eA-3 Q176 0.312 0.229 0.307 ! 0.59 eA-3 Q177 0.310 0.803 0.781 ! 0.59 eA-3 Q178 0.373 0.727 0.735 ! 0.58 eA-3 Q179 0.718 0.239 0.252 ! 0.58 eA-3 Q180 0.261 0.702 0.238 ! 0.58 eA-3 Q181 0.898 0.530 0.031 ! 0.58 eA-3 Q182 0.059 0.874 0.756 ! 0.58 eA-3 Q183 0.247 0.306 0.220 ! 0.58 eA-3 Q184 0.093 0.550 0.924 ! 0.58 eA-3 Q185 0.090 0.556 0.980 ! 0.58 eA-3 Q186 0.534 0.196 0.281 ! 0.57 eA-3 Q187 0.405 0.837 0.747 ! 0.57 eA-3 Q188 0.392 0.672 0.280 ! 0.57 eA-3 Q189 0.834 0.224 0.323 ! 0.57 eA-3 Q190 0.498 0.623 0.282 ! 0.57 eA-3 Q191 0.327 0.766 0.735 ! 0.57 eA-3 Q192 0.987 0.121 0.281 ! 0.57 eA-3 Q193 0.504 0.764 0.250 ! 0.57 eA-3 Q194 0.014 0.573 0.893 ! 0.56 eA-3 Q195 0.146 0.491 0.004 ! 0.56 eA-3 Q196 0.029 0.743 0.706 ! 0.56 eA-3 Q197 0.518 0.305 0.829 ! 0.56 eA-3 Q198 0.821 0.531 0.034 ! 0.56 eA-3 Q199 0.466 0.759 0.705 ! 0.56 eA-3 ) ; _shelx_fab_checksum 69592 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C2 0.6306(3) 0.95356(14) 0.6932(2) 0.0434(8) Uani d 1 . . H H2 0.5689 0.9658 0.6648 0.065 Uiso calc 1 . . C C3 0.6549(3) 0.89272(15) 0.6880(2) 0.0545(9) Uani d 1 . . H H3 0.6095 0.8656 0.6565 0.082 Uiso calc 1 . . C C4 0.7449(3) 0.87249(14) 0.7287(2) 0.0544(10) Uani d 1 . . C C5 0.9100(3) 0.90216(18) 0.8180(3) 0.0668(11) Uani d 1 . . H H5 0.9315 0.8625 0.8171 0.100 Uiso calc 1 . . C C6 0.9716(3) 0.9449(2) 0.8596(3) 0.0704(12) Uani d 1 . . H H6 1.0346 0.9342 0.8856 0.106 Uiso calc 1 . . C C7 1.0036(3) 1.0536(2) 0.9102(3) 0.0632(11) Uani d 1 . . C C8 0.9646(3) 1.1091(2) 0.9139(3) 0.0651(11) Uani d 1 . . H H7 1.0024 1.1401 0.9448 0.098 Uiso calc 1 . . C C9 0.8699(3) 1.12020(16) 0.8728(2) 0.0523(9) Uani d 1 . . H H8 0.8463 1.1588 0.8771 0.079 Uiso calc 1 . . C C11 0.7819(2) 0.97623(13) 0.77764(18) 0.0347(7) Uani d 1 . . C C12 0.8123(3) 0.91566(14) 0.7747(2) 0.0468(8) Uani d 1 . . C C13 0.8468(2) 1.02126(14) 0.82465(19) 0.0378(7) Uani d 1 . . C C14 0.9430(2) 1.00649(17) 0.8653(2) 0.0529(9) Uani d 1 . . C C15 0.7709(4) 0.80602(17) 0.7250(3) 0.0855(15) Uani d 1 . . H H15A 0.8272 0.8032 0.7100 0.128 Uiso calc 1 . . H H15B 0.7200 0.7853 0.6843 0.128 Uiso calc 1 . . H H15C 0.7820 0.7875 0.7781 0.128 Uiso calc 1 . . C C16 1.1090(3) 1.0424(3) 0.9512(3) 0.0959(17) Uani d 1 . . H H16A 1.1188 1.0025 0.9754 0.144 Uiso calc 1 . . H H16B 1.1346 1.0723 0.9936 0.144 Uiso calc 1 . . H H16C 1.1403 1.0454 0.9105 0.144 Uiso calc 1 . . C C21 0.6408(2) 1.17079(14) 0.7579(2) 0.0411(7) Uani d 1 . . C C31 0.6154(2) 1.16004(13) 0.55026(19) 0.0366(7) Uani d 1 . . C C32 0.5323(3) 1.18092(16) 0.5588(2) 0.0499(9) Uani d 1 . . H H32 0.5161 1.1696 0.6047 0.075 Uiso calc 1 . . C C33 0.4720(3) 1.21908(18) 0.4986(3) 0.0644(11) Uani d 1 . . H H33 0.4165 1.2335 0.5051 0.097 Uiso calc 1 . . C C34 0.4946(3) 1.23506(17) 0.4310(3) 0.0668(12) Uani d 1 . . H H34 0.4554 1.2614 0.3921 0.100 Uiso calc 1 . . C C35 0.5746(3) 1.2127(2) 0.4195(3) 0.0775(13) Uani d 1 . . H H35 0.5880 1.2222 0.3716 0.116 Uiso calc 1 . . C C36 0.6356(3) 1.17583(19) 0.4792(2) 0.0652(11) Uani d 1 . . H H36 0.6907 1.1615 0.4717 0.098 Uiso calc 1 . . C C41 0.7001(2) 1.04130(13) 0.56639(18) 0.0343(7) Uani d 1 . . C C42 0.6189(2) 1.02333(15) 0.5029(2) 0.0465(8) Uani d 1 . . H H42 0.5660 1.0486 0.4871 0.070 Uiso calc 1 . . C C43 0.6166(3) 0.96814(17) 0.4633(2) 0.0611(10) Uani d 1 . . H H43 0.5621 0.9564 0.4211 0.092 Uiso calc 1 . . C C44 0.6947(3) 0.93030(17) 0.4862(3) 0.0635(11) Uani d 1 . . H H44 0.6928 0.8934 0.4591 0.095 Uiso calc 1 . . C C45 0.7753(3) 0.94729(16) 0.5491(2) 0.0561(10) Uani d 1 . . H H45 0.8278 0.9218 0.5649 0.084 Uiso calc 1 . . C C46 0.7777(2) 1.00257(15) 0.5890(2) 0.0444(8) Uani d 1 . . H H46 0.8322 1.0138 0.6316 0.067 Uiso calc 1 . . C C51 0.8127(2) 1.14734(14) 0.6390(2) 0.0405(7) Uani d 1 . . C C52 0.8669(3) 1.13433(18) 0.5882(3) 0.0596(10) Uani d 1 . . H H52 0.8466 1.1046 0.5475 0.089 Uiso calc 1 . . C C53 0.9504(3) 1.1654(2) 0.5983(3) 0.0836(15) Uani d 1 . . H H53 0.9858 1.1569 0.5639 0.125 Uiso calc 1 . . C C54 0.9816(3) 1.2096(2) 0.6604(3) 0.0886(15) Uani d 1 . . H H54 1.0382 1.2300 0.6680 0.133 Uiso calc 1 . . C C55 0.9288(3) 1.2225(2) 0.7094(3) 0.0770(13) Uani d 1 . . H H55 0.9495 1.2518 0.7506 0.115 Uiso calc 1 . . C C56 0.8442(3) 1.19218(17) 0.6983(2) 0.0571(10) Uani d 1 . . H H56 0.8080 1.2023 0.7314 0.086 Uiso calc 1 . . C C61 0.4765(2) 1.09982(13) 0.8378(2) 0.0370(7) Uani d 1 . . C C62 0.4406(3) 1.09980(16) 0.9031(2) 0.0504(9) Uani d 1 . . H H62 0.4773 1.0847 0.9544 0.076 Uiso calc 1 . . C C63 0.3505(3) 1.12205(17) 0.8923(3) 0.0580(10) Uani d 1 . . H H63 0.3273 1.1220 0.9364 0.087 Uiso calc 1 . . C C64 0.2956(3) 1.14410(17) 0.8165(3) 0.0610(10) Uani d 1 . . H H64 0.2347 1.1579 0.8093 0.091 Uiso calc 1 . . C C65 0.3299(3) 1.1458(2) 0.7520(2) 0.0643(11) Uani d 1 . . H H65 0.2929 1.1616 0.7012 0.096 Uiso calc 1 . . C C66 0.4206(3) 1.12390(17) 0.7624(2) 0.0546(9) Uani d 1 . . H H66 0.4439 1.1254 0.7184 0.082 Uiso calc 1 . . C C71 0.5698(2) 0.98395(14) 0.8558(2) 0.0417(7) Uani d 1 . . C C72 0.6455(3) 0.94407(16) 0.8883(2) 0.0525(9) Uani d 1 . . H H72 0.7064 0.9595 0.9119 0.079 Uiso calc 1 . . C C73 0.6311(4) 0.88146(19) 0.8860(3) 0.0712(13) Uani d 1 . . H H73 0.6821 0.8553 0.9078 0.107 Uiso calc 1 . . C C74 0.5419(5) 0.85844(19) 0.8515(4) 0.0895(17) Uani d 1 . . H H74 0.5324 0.8165 0.8506 0.134 Uiso calc 1 . . C C75 0.4665(4) 0.8962(2) 0.8184(4) 0.0945(17) Uani d 1 . . H H75 0.4062 0.8800 0.7942 0.142 Uiso calc 1 . . C C76 0.4801(3) 0.95970(17) 0.8211(3) 0.0671(11) Uani d 1 . . H H76 0.4285 0.9855 0.7994 0.101 Uiso calc 1 . . C C81 0.6623(2) 1.08640(16) 0.9578(2) 0.0432(8) Uani d 1 . . C C82 0.7055(3) 1.14312(19) 0.9703(2) 0.0678(12) Uani d 1 . . H H82 0.6991 1.1682 0.9251 0.102 Uiso calc 1 . . C C83 0.7576(4) 1.1630(3) 1.0483(3) 0.0946(17) Uani d 1 . . H H83 0.7844 1.2017 1.0557 0.142 Uiso calc 1 . . C C84 0.7700(4) 1.1253(3) 1.1155(3) 0.0896(16) Uani d 1 . . H H84 0.8072 1.1378 1.1681 0.134 Uiso calc 1 . . C C85 0.7277(4) 1.0696(3) 1.1047(2) 0.0790(14) Uani d 1 . . H H85 0.7353 1.0446 1.1503 0.119 Uiso calc 1 . . C C86 0.6730(3) 1.0495(2) 1.0258(2) 0.0601(10) Uani d 1 . . H H86 0.6439 1.0115 1.0192 0.090 Uiso calc 1 . . N N1 0.69155(18) 0.99485(10) 0.73693(15) 0.0346(6) Uani d 1 . . N N10 0.81008(18) 1.07848(11) 0.82722(15) 0.0371(6) Uani d 1 . . O O22 0.6272(2) 1.22248(10) 0.76208(17) 0.0680(8) Uani d 1 . . P P1 0.69874(5) 1.11018(3) 0.62658(5) 0.03094(17) Uani d 1 . . P P2 0.59291(6) 1.06547(4) 0.85096(5) 0.03407(18) Uani d 1 . . Ru Ru1 0.66288(2) 1.08911(2) 0.74858(2) 0.02911(9) Uani d 1 . . H H1 0.559(2) 1.0828(13) 0.6853(19) 0.044 Uiso d 1 . . F F1A 0.7415(11) 0.7452(7) 0.9251(7) 0.143(7) Uani d 0.417(13) A 1 F F2A 0.8678(16) 0.6928(7) 1.0643(14) 0.184(8) Uani d 0.417(13) A 1 F F3A 0.8615(16) 0.6802(6) 0.9676(15) 0.137(8) Uani d 0.417(13) A 1 F F4A 0.9253(13) 0.7423(7) 1.0750(11) 0.154(6) Uani d 0.417(13) A 1 F F5A 0.8087(11) 0.8005(7) 1.0323(10) 0.136(7) Uani d 0.417(13) A 1 F F6A 0.884(2) 0.7747(7) 0.9477(16) 0.245(13) Uani d 0.417(13) A 1 F F1B 0.7406(6) 0.7402(5) 0.9781(14) 0.190(7) Uani d 0.583(13) A 2 F F2B 0.7976(18) 0.6998(6) 1.0504(10) 0.191(7) Uani d 0.583(13) A 2 F F3B 0.8512(11) 0.6990(7) 0.9352(10) 0.154(6) Uani d 0.583(13) A 2 F F4B 0.9575(5) 0.7504(4) 1.0301(9) 0.109(3) Uani d 0.583(13) A 2 F F5B 0.8488(12) 0.7939(5) 1.0722(10) 0.157(6) Uani d 0.583(13) A 2 F F6B 0.8476(6) 0.8029(5) 0.9477(7) 0.137(5) Uani d 0.583(13) A 2 P P3 0.84264(9) 0.74431(5) 1.00104(8) 0.0684(3) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C2 0.050(2) 0.0393(16) 0.0372(18) -0.0093(15) 0.0094(15) -0.0031(14) C3 0.074(3) 0.0393(17) 0.048(2) -0.0110(19) 0.017(2) -0.0068(16) C4 0.081(3) 0.0342(17) 0.051(2) 0.0028(18) 0.026(2) -0.0002(15) C5 0.066(3) 0.054(2) 0.080(3) 0.024(2) 0.022(2) 0.007(2) C6 0.044(2) 0.074(3) 0.088(3) 0.026(2) 0.014(2) 0.011(2) C7 0.034(2) 0.083(3) 0.064(3) -0.006(2) 0.0038(18) 0.007(2) C8 0.039(2) 0.067(2) 0.072(3) -0.014(2) -0.0042(19) -0.006(2) C9 0.047(2) 0.0465(19) 0.053(2) -0.0104(17) 0.0022(17) -0.0077(16) C11 0.0369(17) 0.0342(15) 0.0329(16) 0.0055(13) 0.0113(13) 0.0030(12) C12 0.059(2) 0.0404(17) 0.0434(19) 0.0076(16) 0.0194(17) 0.0052(15) C13 0.0337(16) 0.0407(16) 0.0371(17) 0.0034(14) 0.0092(14) 0.0049(13) C14 0.0352(19) 0.062(2) 0.057(2) 0.0055(17) 0.0085(16) 0.0057(18) C15 0.117(4) 0.041(2) 0.094(4) 0.016(2) 0.030(3) -0.007(2) C16 0.035(2) 0.123(4) 0.110(4) 0.003(3) -0.002(2) 0.012(3) C21 0.048(2) 0.0417(17) 0.0379(18) 0.0023(15) 0.0196(15) -0.0020(14) C31 0.0404(18) 0.0329(15) 0.0358(17) -0.0026(14) 0.0115(14) 0.0018(13) C32 0.054(2) 0.054(2) 0.0406(19) 0.0106(17) 0.0129(17) 0.0040(16) C33 0.060(3) 0.061(2) 0.062(3) 0.019(2) 0.005(2) 0.001(2) C34 0.077(3) 0.046(2) 0.058(3) 0.000(2) -0.003(2) 0.0185(19) C35 0.078(3) 0.088(3) 0.064(3) -0.004(3) 0.020(2) 0.039(2) C36 0.060(3) 0.083(3) 0.059(3) 0.007(2) 0.028(2) 0.031(2) C41 0.0351(16) 0.0387(15) 0.0318(16) -0.0016(13) 0.0149(13) -0.0027(13) C42 0.0396(19) 0.0467(18) 0.050(2) -0.0014(16) 0.0105(16) -0.0087(16) C43 0.057(2) 0.059(2) 0.056(2) -0.003(2) 0.0045(19) -0.0238(19) C44 0.076(3) 0.049(2) 0.066(3) 0.001(2) 0.024(2) -0.0223(19) C45 0.058(2) 0.047(2) 0.067(3) 0.0116(18) 0.025(2) -0.0082(18) C46 0.0393(18) 0.0496(18) 0.046(2) 0.0022(16) 0.0154(15) -0.0076(15) C51 0.0351(17) 0.0449(17) 0.0413(18) -0.0055(14) 0.0124(14) 0.0016(14) C52 0.048(2) 0.070(2) 0.071(3) -0.0180(19) 0.033(2) -0.013(2) C53 0.059(3) 0.102(3) 0.106(4) -0.030(3) 0.049(3) -0.017(3) C54 0.058(3) 0.104(4) 0.111(4) -0.043(3) 0.038(3) -0.017(3) C55 0.073(3) 0.079(3) 0.080(3) -0.039(3) 0.027(3) -0.019(2) C56 0.060(2) 0.060(2) 0.056(2) -0.0206(19) 0.025(2) -0.0096(18) C61 0.0334(16) 0.0394(16) 0.0397(17) 0.0029(13) 0.0139(14) 0.0005(13) C62 0.050(2) 0.060(2) 0.047(2) 0.0056(18) 0.0228(17) 0.0118(17) C63 0.055(2) 0.068(2) 0.063(3) 0.014(2) 0.036(2) 0.012(2) C64 0.043(2) 0.064(2) 0.084(3) 0.0093(19) 0.030(2) 0.002(2) C65 0.051(2) 0.083(3) 0.055(2) 0.024(2) 0.0118(19) 0.014(2) C66 0.047(2) 0.075(2) 0.043(2) 0.0163(19) 0.0165(17) 0.0081(18) C71 0.0446(19) 0.0428(17) 0.0401(18) 0.0033(15) 0.0172(15) 0.0066(14) C72 0.059(2) 0.055(2) 0.047(2) 0.0130(18) 0.0207(18) 0.0155(17) C73 0.102(4) 0.055(2) 0.067(3) 0.024(3) 0.041(3) 0.025(2) C74 0.127(5) 0.042(2) 0.124(5) -0.005(3) 0.074(4) 0.009(3) C75 0.086(4) 0.060(3) 0.149(5) -0.020(3) 0.054(4) -0.010(3) C76 0.049(2) 0.052(2) 0.099(3) -0.0040(19) 0.022(2) -0.001(2) C81 0.0366(17) 0.060(2) 0.0322(17) 0.0038(16) 0.0102(14) -0.0004(15) C82 0.084(3) 0.076(3) 0.036(2) -0.014(2) 0.009(2) -0.0099(19) C83 0.115(4) 0.111(4) 0.049(3) -0.030(3) 0.015(3) -0.026(3) C84 0.080(3) 0.139(5) 0.038(2) 0.000(3) 0.004(2) -0.019(3) C85 0.088(3) 0.115(4) 0.031(2) 0.024(3) 0.015(2) 0.009(2) C86 0.060(2) 0.084(3) 0.035(2) 0.012(2) 0.0141(18) 0.0105(19) N1 0.0413(15) 0.0319(12) 0.0305(13) -0.0010(11) 0.0119(11) 0.0004(10) N10 0.0315(14) 0.0407(14) 0.0343(14) -0.0012(11) 0.0043(11) -0.0005(11) O22 0.106(2) 0.0393(14) 0.0653(18) 0.0139(14) 0.0368(17) -0.0063(12) P1 0.0305(4) 0.0333(4) 0.0304(4) -0.0016(3) 0.0119(3) -0.0013(3) P2 0.0322(4) 0.0408(4) 0.0289(4) 0.0017(3) 0.0095(3) 0.0033(3) Ru1 0.02960(14) 0.03031(13) 0.02647(13) -0.00028(10) 0.00795(9) -0.00177(9) F1A 0.148(12) 0.123(9) 0.096(8) 0.030(8) -0.043(7) -0.025(6) F2A 0.221(18) 0.099(8) 0.29(2) 0.022(11) 0.155(16) 0.102(12) F3A 0.129(11) 0.055(5) 0.27(2) 0.006(5) 0.130(14) -0.006(8) F4A 0.107(11) 0.161(12) 0.142(12) 0.011(10) -0.031(9) 0.021(10) F5A 0.134(9) 0.111(8) 0.125(10) 0.063(7) -0.010(8) -0.067(7) F6A 0.51(4) 0.087(9) 0.29(2) -0.044(13) 0.35(3) -0.006(10) F1B 0.060(5) 0.124(7) 0.42(2) -0.014(5) 0.123(9) -0.014(13) F2B 0.32(2) 0.121(8) 0.205(11) -0.085(11) 0.191(14) -0.022(7) F3B 0.108(7) 0.196(13) 0.167(10) -0.030(9) 0.056(7) -0.122(10) F4B 0.062(4) 0.086(5) 0.178(9) -0.005(3) 0.039(5) -0.021(5) F5B 0.200(12) 0.128(8) 0.196(12) -0.045(9) 0.139(10) -0.073(8) F6B 0.128(6) 0.102(6) 0.153(9) -0.026(5) 0.007(6) 0.055(6) P3 0.0694(8) 0.0570(6) 0.0908(9) 0.0022(6) 0.0424(7) 0.0009(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 C2 C3 . . 123.0(3) ? N1 C2 H2 . . 118.5 ? C3 C2 H2 . . 118.5 ? C4 C3 C2 . . 120.7(3) ? C4 C3 H3 . . 119.6 ? C2 C3 H3 . . 119.6 ? C3 C4 C12 . . 117.7(3) ? C3 C4 C15 . . 120.9(4) ? C12 C4 C15 . . 121.4(4) ? C6 C5 C12 . . 122.2(3) ? C6 C5 H5 . . 118.9 ? C12 C5 H5 . . 118.9 ? C5 C6 C14 . . 121.9(4) ? C5 C6 H6 . . 119.1 ? C14 C6 H6 . . 119.1 ? C8 C7 C14 . . 118.0(3) ? C8 C7 C16 . . 121.2(4) ? C14 C7 C16 . . 120.8(4) ? C7 C8 C9 . . 121.2(4) ? C7 C8 H7 . . 119.4 ? C9 C8 H7 . . 119.4 ? N10 C9 C8 . . 123.6(3) ? N10 C9 H8 . . 118.2 ? C8 C9 H8 . . 118.2 ? N1 C11 C12 . . 122.8(3) ? N1 C11 C13 . . 117.0(3) ? C12 C11 C13 . . 120.3(3) ? C11 C12 C4 . . 118.1(3) ? C11 C12 C5 . . 117.5(3) ? C4 C12 C5 . . 124.4(3) ? N10 C13 C14 . . 123.0(3) ? N10 C13 C11 . . 116.4(3) ? C14 C13 C11 . . 120.6(3) ? C13 C14 C7 . . 117.6(3) ? C13 C14 C6 . . 117.5(3) ? C7 C14 C6 . . 124.9(4) ? C4 C15 H15A . . 109.5 ? C4 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? C4 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C7 C16 H16A . . 109.5 ? C7 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? C7 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? O22 C21 Ru1 . . 178.5(3) ? C32 C31 C36 . . 118.3(3) ? C32 C31 P1 . . 123.1(2) ? C36 C31 P1 . . 118.5(3) ? C31 C32 C33 . . 120.4(3) ? C31 C32 H32 . . 119.8 ? C33 C32 H32 . . 119.8 ? C34 C33 C32 . . 120.1(4) ? C34 C33 H33 . . 119.9 ? C32 C33 H33 . . 119.9 ? C33 C34 C35 . . 120.4(4) ? C33 C34 H34 . . 119.8 ? C35 C34 H34 . . 119.8 ? C34 C35 C36 . . 120.0(4) ? C34 C35 H35 . . 120.0 ? C36 C35 H35 . . 120.0 ? C35 C36 C31 . . 120.7(4) ? C35 C36 H36 . . 119.7 ? C31 C36 H36 . . 119.7 ? C46 C41 C42 . . 118.6(3) ? C46 C41 P1 . . 120.8(2) ? C42 C41 P1 . . 120.2(2) ? C43 C42 C41 . . 120.3(3) ? C43 C42 H42 . . 119.9 ? C41 C42 H42 . . 119.9 ? C44 C43 C42 . . 120.4(4) ? C44 C43 H43 . . 119.8 ? C42 C43 H43 . . 119.8 ? C45 C44 C43 . . 119.9(3) ? C45 C44 H44 . . 120.0 ? C43 C44 H44 . . 120.0 ? C44 C45 C46 . . 119.7(3) ? C44 C45 H45 . . 120.1 ? C46 C45 H45 . . 120.1 ? C41 C46 C45 . . 121.0(3) ? C41 C46 H46 . . 119.5 ? C45 C46 H46 . . 119.5 ? C56 C51 C52 . . 118.3(3) ? C56 C51 P1 . . 118.7(3) ? C52 C51 P1 . . 122.8(3) ? C53 C52 C51 . . 120.5(4) ? C53 C52 H52 . . 119.8 ? C51 C52 H52 . . 119.8 ? C52 C53 C54 . . 119.8(4) ? C52 C53 H53 . . 120.1 ? C54 C53 H53 . . 120.1 ? C55 C54 C53 . . 119.8(4) ? C55 C54 H54 . . 120.1 ? C53 C54 H54 . . 120.1 ? C54 C55 C56 . . 120.4(4) ? C54 C55 H55 . . 119.8 ? C56 C55 H55 . . 119.8 ? C51 C56 C55 . . 121.2(4) ? C51 C56 H56 . . 119.4 ? C55 C56 H56 . . 119.4 ? C66 C61 C62 . . 118.2(3) ? C66 C61 P2 . . 121.7(2) ? C62 C61 P2 . . 120.1(3) ? C63 C62 C61 . . 120.6(3) ? C63 C62 H62 . . 119.7 ? C61 C62 H62 . . 119.7 ? C64 C63 C62 . . 120.1(3) ? C64 C63 H63 . . 120.0 ? C62 C63 H63 . . 120.0 ? C65 C64 C63 . . 120.5(4) ? C65 C64 H64 . . 119.8 ? C63 C64 H64 . . 119.8 ? C64 C65 C66 . . 119.8(4) ? C64 C65 H65 . . 120.1 ? C66 C65 H65 . . 120.1 ? C61 C66 C65 . . 120.8(3) ? C61 C66 H66 . . 119.6 ? C65 C66 H66 . . 119.6 ? C76 C71 C72 . . 118.4(3) ? C76 C71 P2 . . 121.9(3) ? C72 C71 P2 . . 119.5(3) ? C73 C72 C71 . . 120.8(4) ? C73 C72 H72 . . 119.6 ? C71 C72 H72 . . 119.6 ? C74 C73 C72 . . 119.9(4) ? C74 C73 H73 . . 120.0 ? C72 C73 H73 . . 120.0 ? C75 C74 C73 . . 120.7(4) ? C75 C74 H74 . . 119.6 ? C73 C74 H74 . . 119.6 ? C74 C75 C76 . . 119.8(5) ? C74 C75 H75 . . 120.1 ? C76 C75 H75 . . 120.1 ? C71 C76 C75 . . 120.3(4) ? C71 C76 H76 . . 119.8 ? C75 C76 H76 . . 119.8 ? C86 C81 C82 . . 118.5(3) ? C86 C81 P2 . . 124.1(3) ? C82 C81 P2 . . 117.4(3) ? C83 C82 C81 . . 121.4(4) ? C83 C82 H82 . . 119.3 ? C81 C82 H82 . . 119.3 ? C82 C83 C84 . . 119.7(5) ? C82 C83 H83 . . 120.2 ? C84 C83 H83 . . 120.2 ? C85 C84 C83 . . 119.8(4) ? C85 C84 H84 . . 120.1 ? C83 C84 H84 . . 120.1 ? C84 C85 C86 . . 120.9(4) ? C84 C85 H85 . . 119.6 ? C86 C85 H85 . . 119.6 ? C81 C86 C85 . . 119.7(4) ? C81 C86 H86 . . 120.2 ? C85 C86 H86 . . 120.2 ? C2 N1 C11 . . 117.6(3) ? C2 N1 Ru1 . . 126.3(2) ? C11 N1 Ru1 . . 116.02(19) ? C9 N10 C13 . . 116.5(3) ? C9 N10 Ru1 . . 129.2(2) ? C13 N10 Ru1 . . 114.18(19) ? C41 P1 C51 . . 104.45(14) ? C41 P1 C31 . . 102.86(14) ? C51 P1 C31 . . 101.74(14) ? C41 P1 Ru1 . . 112.47(10) ? C51 P1 Ru1 . . 117.13(11) ? C31 P1 Ru1 . . 116.42(10) ? C71 P2 C81 . . 104.64(15) ? C71 P2 C61 . . 102.77(15) ? C81 P2 C61 . . 102.73(15) ? C71 P2 Ru1 . . 112.49(10) ? C81 P2 Ru1 . . 115.92(11) ? C61 P2 Ru1 . . 116.68(10) ? C21 Ru1 N1 . . 178.57(12) ? C21 Ru1 N10 . . 102.96(13) ? N1 Ru1 N10 . . 76.17(9) ? C21 Ru1 P1 . . 89.17(10) ? N1 Ru1 P1 . . 89.77(7) ? N10 Ru1 P1 . . 95.08(7) ? C21 Ru1 P2 . . 90.78(10) ? N1 Ru1 P2 . . 90.46(7) ? N10 Ru1 P2 . . 97.03(7) ? P1 Ru1 P2 . . 167.58(3) ? C21 Ru1 H1 . . 88.9(10) ? N1 Ru1 H1 . . 91.9(10) ? N10 Ru1 H1 . . 167.8(10) ? P1 Ru1 H1 . . 82.4(11) ? P2 Ru1 H1 . . 85.2(11) ? F4A F2A P3 . . 60.0(7) ? F4A F2A F3A . . 95.4(16) ? P3 F2A F3A . . 59.6(8) ? P3 F3A F2A . . 56.2(8) ? F2A F4A P3 . . 65.6(10) ? P3 F1B F2B . . 64.0(9) ? F1B F2B P3 . . 55.4(5) ? F6A P3 F4A . . 98.3(12) ? F6A P3 F5A . . 96.6(10) ? F4A P3 F5A . . 90.3(7) ? F6A P3 F2A . . 137.9(17) ? F4A P3 F2A . . 54.4(12) ? F5A P3 F2A . . 113.0(12) ? F1B P3 F3B . . 95.5(9) ? F6A P3 F3A . . 91.0(9) ? F4A P3 F3A . . 95.0(11) ? F5A P3 F3A . . 170.1(11) ? F2A P3 F3A . . 64.2(11) ? F1B P3 F2B . . 60.6(12) ? F3B P3 F2B . . 98.4(8) ? F1B P3 F6B . . 98.0(8) ? F3B P3 F6B . . 94.1(8) ? F2B P3 F6B . . 156.0(12) ? F1B P3 F5B . . 92.3(7) ? F3B P3 F5B . . 172.1(8) ? F2B P3 F5B . . 86.6(6) ? F6B P3 F5B . . 83.4(6) ? F1B P3 F4B . . 177.7(7) ? F3B P3 F4B . . 86.7(7) ? F2B P3 F4B . . 118.7(12) ? F6B P3 F4B . . 82.2(5) ? F5B P3 F4B . . 85.5(5) ? F6A P3 F1A . . 88.4(14) ? F4A P3 F1A . . 172.9(10) ? F5A P3 F1A . . 86.6(7) ? F2A P3 F1A . . 121.3(12) ? F3A P3 F1A . . 87.2(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C2 N1 . 1.328(4) ? C2 C3 . 1.395(5) ? C2 H2 . 0.9300 ? C3 C4 . 1.370(5) ? C3 H3 . 0.9300 ? C4 C12 . 1.419(5) ? C4 C15 . 1.517(5) ? C5 C6 . 1.343(6) ? C5 C12 . 1.435(5) ? C5 H5 . 0.9300 ? C6 C14 . 1.431(5) ? C6 H6 . 0.9300 ? C7 C8 . 1.362(6) ? C7 C14 . 1.422(5) ? C7 C16 . 1.520(5) ? C8 C9 . 1.380(5) ? C8 H7 . 0.9300 ? C9 N10 . 1.337(4) ? C9 H8 . 0.9300 ? C11 N1 . 1.364(4) ? C11 C12 . 1.412(4) ? C11 C13 . 1.432(4) ? C13 N10 . 1.377(4) ? C13 C14 . 1.415(4) ? C15 H15A . 0.9600 ? C15 H15B . 0.9600 ? C15 H15C . 0.9600 ? C16 H16A . 0.9600 ? C16 H16B . 0.9600 ? C16 H16C . 0.9600 ? C21 O22 . 1.160(4) ? C21 Ru1 . 1.840(3) ? C31 C32 . 1.378(4) ? C31 C36 . 1.390(5) ? C31 P1 . 1.840(3) ? C32 C33 . 1.401(5) ? C32 H32 . 0.9300 ? C33 C34 . 1.354(6) ? C33 H33 . 0.9300 ? C34 C35 . 1.367(6) ? C34 H34 . 0.9300 ? C35 C36 . 1.384(5) ? C35 H35 . 0.9300 ? C36 H36 . 0.9300 ? C41 C46 . 1.387(4) ? C41 C42 . 1.393(4) ? C41 P1 . 1.834(3) ? C42 C43 . 1.383(5) ? C42 H42 . 0.9300 ? C43 C44 . 1.380(5) ? C43 H43 . 0.9300 ? C44 C45 . 1.377(5) ? C44 H44 . 0.9300 ? C45 C46 . 1.387(4) ? C45 H45 . 0.9300 ? C46 H46 . 0.9300 ? C51 C56 . 1.380(5) ? C51 C52 . 1.400(5) ? C51 P1 . 1.838(3) ? C52 C53 . 1.384(5) ? C52 H52 . 0.9300 ? C53 C54 . 1.400(6) ? C53 H53 . 0.9300 ? C54 C55 . 1.359(6) ? C54 H54 . 0.9300 ? C55 C56 . 1.386(5) ? C55 H55 . 0.9300 ? C56 H56 . 0.9300 ? C61 C66 . 1.390(4) ? C61 C62 . 1.390(4) ? C61 P2 . 1.843(3) ? C62 C63 . 1.387(5) ? C62 H62 . 0.9300 ? C63 C64 . 1.374(5) ? C63 H63 . 0.9300 ? C64 C65 . 1.363(5) ? C64 H64 . 0.9300 ? C65 C66 . 1.395(5) ? C65 H65 . 0.9300 ? C66 H66 . 0.9300 ? C71 C76 . 1.383(5) ? C71 C72 . 1.394(5) ? C71 P2 . 1.830(3) ? C72 C73 . 1.390(5) ? C72 H72 . 0.9300 ? C73 C74 . 1.366(7) ? C73 H73 . 0.9300 ? C74 C75 . 1.363(7) ? C74 H74 . 0.9300 ? C75 C76 . 1.408(6) ? C75 H75 . 0.9300 ? C76 H76 . 0.9300 ? C81 C86 . 1.384(5) ? C81 C82 . 1.387(5) ? C81 P2 . 1.839(3) ? C82 C83 . 1.376(5) ? C82 H82 . 0.9300 ? C83 C84 . 1.380(7) ? C83 H83 . 0.9300 ? C84 C85 . 1.361(7) ? C84 H84 . 0.9300 ? C85 C86 . 1.399(6) ? C85 H85 . 0.9300 ? C86 H86 . 0.9300 ? N1 Ru1 . 2.136(2) ? N10 Ru1 . 2.182(2) ? P1 Ru1 . 2.3667(8) ? P2 Ru1 . 2.3762(8) ? Ru1 H1 . 1.57(3) ? F1A P3 . 1.637(11) ? F2A F4A . 1.36(3) ? F2A P3 . 1.523(14) ? F2A F3A . 1.65(3) ? F3A P3 . 1.580(15) ? F4A P3 . 1.450(11) ? F5A P3 . 1.499(12) ? F6A P3 . 1.431(11) ? F1B P3 . 1.448(8) ? F1B F2B . 1.53(3) ? F2B P3 . 1.581(9) ? F3B P3 . 1.539(11) ? F4B P3 . 1.629(7) ? F5B P3 . 1.613(11) ? F6B P3 . 1.592(8) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C33 H33 F1B . 0.93 2.46 3.366(13) 164 yes C8 H8 F4B 4_666 0.93 2.48 3.325(10) 151 yes C35 H35 O22 4_565 0.93 2.46 3.362(6) 163 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N1 C2 C3 C4 . . . . 0.0(5) ? C2 C3 C4 C12 . . . . -1.2(5) ? C2 C3 C4 C15 . . . . 178.4(3) ? C12 C5 C6 C14 . . . . 1.6(7) ? C14 C7 C8 C9 . . . . -2.5(6) ? C16 C7 C8 C9 . . . . 176.3(4) ? C7 C8 C9 N10 . . . . 0.1(7) ? N1 C11 C12 C4 . . . . -1.4(5) ? C13 C11 C12 C4 . . . . 178.7(3) ? N1 C11 C12 C5 . . . . 178.0(3) ? C13 C11 C12 C5 . . . . -2.0(5) ? C3 C4 C12 C11 . . . . 1.8(5) ? C15 C4 C12 C11 . . . . -177.8(3) ? C3 C4 C12 C5 . . . . -177.5(4) ? C15 C4 C12 C5 . . . . 2.9(6) ? C6 C5 C12 C11 . . . . -0.4(6) ? C6 C5 C12 C4 . . . . 178.9(4) ? N1 C11 C13 N10 . . . . 3.0(4) ? C12 C11 C13 N10 . . . . -177.1(3) ? N1 C11 C13 C14 . . . . -176.8(3) ? C12 C11 C13 C14 . . . . 3.2(5) ? N10 C13 C14 C7 . . . . -0.3(5) ? C11 C13 C14 C7 . . . . 179.4(3) ? N10 C13 C14 C6 . . . . 178.3(3) ? C11 C13 C14 C6 . . . . -2.0(5) ? C8 C7 C14 C13 . . . . 2.5(6) ? C16 C7 C14 C13 . . . . -176.3(4) ? C8 C7 C14 C6 . . . . -176.0(4) ? C16 C7 C14 C6 . . . . 5.2(7) ? C5 C6 C14 C13 . . . . -0.4(6) ? C5 C6 C14 C7 . . . . 178.1(4) ? C36 C31 C32 C33 . . . . -2.5(5) ? P1 C31 C32 C33 . . . . 179.7(3) ? C31 C32 C33 C34 . . . . 0.9(6) ? C32 C33 C34 C35 . . . . 2.0(6) ? C33 C34 C35 C36 . . . . -3.2(7) ? C34 C35 C36 C31 . . . . 1.5(7) ? C32 C31 C36 C35 . . . . 1.4(6) ? P1 C31 C36 C35 . . . . 179.3(3) ? C46 C41 C42 C43 . . . . -0.4(5) ? P1 C41 C42 C43 . . . . -173.1(3) ? C41 C42 C43 C44 . . . . -0.1(6) ? C42 C43 C44 C45 . . . . 0.4(7) ? C43 C44 C45 C46 . . . . -0.3(6) ? C42 C41 C46 C45 . . . . 0.5(5) ? P1 C41 C46 C45 . . . . 173.1(3) ? C44 C45 C46 C41 . . . . -0.2(6) ? C56 C51 C52 C53 . . . . 0.7(6) ? P1 C51 C52 C53 . . . . 177.5(3) ? C51 C52 C53 C54 . . . . 0.8(7) ? C52 C53 C54 C55 . . . . -1.2(8) ? C53 C54 C55 C56 . . . . 0.0(8) ? C52 C51 C56 C55 . . . . -2.0(6) ? P1 C51 C56 C55 . . . . -178.9(3) ? C54 C55 C56 C51 . . . . 1.6(7) ? C66 C61 C62 C63 . . . . 1.4(5) ? P2 C61 C62 C63 . . . . -175.9(3) ? C61 C62 C63 C64 . . . . 0.3(6) ? C62 C63 C64 C65 . . . . -1.7(6) ? C63 C64 C65 C66 . . . . 1.3(7) ? C62 C61 C66 C65 . . . . -1.8(6) ? P2 C61 C66 C65 . . . . 175.5(3) ? C64 C65 C66 C61 . . . . 0.5(6) ? C76 C71 C72 C73 . . . . 0.0(5) ? P2 C71 C72 C73 . . . . -174.1(3) ? C71 C72 C73 C74 . . . . 0.0(6) ? C72 C73 C74 C75 . . . . 0.7(7) ? C73 C74 C75 C76 . . . . -1.2(8) ? C72 C71 C76 C75 . . . . -0.5(6) ? P2 C71 C76 C75 . . . . 173.5(4) ? C74 C75 C76 C71 . . . . 1.1(8) ? C86 C81 C82 C83 . . . . -0.3(6) ? P2 C81 C82 C83 . . . . 179.0(4) ? C81 C82 C83 C84 . . . . 2.1(8) ? C82 C83 C84 C85 . . . . -2.5(8) ? C83 C84 C85 C86 . . . . 1.2(8) ? C82 C81 C86 C85 . . . . -1.0(6) ? P2 C81 C86 C85 . . . . 179.7(3) ? C84 C85 C86 C81 . . . . 0.6(7) ? C3 C2 N1 C11 . . . . 0.5(5) ? C3 C2 N1 Ru1 . . . . 179.4(2) ? C12 C11 N1 C2 . . . . 0.2(4) ? C13 C11 N1 C2 . . . . -179.9(3) ? C12 C11 N1 Ru1 . . . . -178.8(2) ? C13 C11 N1 Ru1 . . . . 1.1(3) ? C8 C9 N10 C13 . . . . 2.1(5) ? C8 C9 N10 Ru1 . . . . -173.5(3) ? C14 C13 N10 C9 . . . . -2.0(5) ? C11 C13 N10 C9 . . . . 178.3(3) ? C14 C13 N10 Ru1 . . . . 174.3(3) ? C11 C13 N10 Ru1 . . . . -5.4(3) ? C46 C41 P1 C51 . . . . 48.9(3) ? C42 C41 P1 C51 . . . . -138.6(3) ? C46 C41 P1 C31 . . . . 154.8(3) ? C42 C41 P1 C31 . . . . -32.7(3) ? C46 C41 P1 Ru1 . . . . -79.1(3) ? C42 C41 P1 Ru1 . . . . 93.4(3) ? C56 C51 P1 C41 . . . . -164.1(3) ? C52 C51 P1 C41 . . . . 19.1(3) ? C56 C51 P1 C31 . . . . 89.1(3) ? C52 C51 P1 C31 . . . . -87.6(3) ? C56 C51 P1 Ru1 . . . . -39.0(3) ? C52 C51 P1 Ru1 . . . . 144.3(3) ? C32 C31 P1 C41 . . . . 118.5(3) ? C36 C31 P1 C41 . . . . -59.3(3) ? C32 C31 P1 C51 . . . . -133.5(3) ? C36 C31 P1 C51 . . . . 48.7(3) ? C32 C31 P1 Ru1 . . . . -4.9(3) ? C36 C31 P1 Ru1 . . . . 177.3(3) ? C76 C71 P2 C81 . . . . 131.1(3) ? C72 C71 P2 C81 . . . . -55.1(3) ? C76 C71 P2 C61 . . . . 24.0(3) ? C72 C71 P2 C61 . . . . -162.1(3) ? C76 C71 P2 Ru1 . . . . -102.3(3) ? C72 C71 P2 Ru1 . . . . 71.6(3) ? C86 C81 P2 C71 . . . . -12.7(3) ? C82 C81 P2 C71 . . . . 168.0(3) ? C86 C81 P2 C61 . . . . 94.3(3) ? C82 C81 P2 C61 . . . . -84.9(3) ? C86 C81 P2 Ru1 . . . . -137.2(3) ? C82 C81 P2 Ru1 . . . . 43.5(3) ? C66 C61 P2 C71 . . . . -106.3(3) ? C62 C61 P2 C71 . . . . 70.9(3) ? C66 C61 P2 C81 . . . . 145.2(3) ? C62 C61 P2 C81 . . . . -37.6(3) ? C66 C61 P2 Ru1 . . . . 17.3(3) ? C62 C61 P2 Ru1 . . . . -165.5(2) ? F4A F2A F3A P3 . . . . -50.4(10) ? F3A F2A F4A P3 . . . . 50.1(11) ? F2B F1B P3 F3B . . . . 96.5(9) ? F2B F1B P3 F6B . . . . -168.5(8) ? F2B F1B P3 F5B . . . . -84.8(8) ? F2A F4A P3 F6A . . . . -144.9(17) ? F2A F4A P3 F5A . . . . 118.5(16) ? F2A F4A P3 F3A . . . . -53.2(15) ? F4A F2A P3 F6A . . . . 58(2) ? F3A F2A P3 F6A . . . . -60(2) ? F3A F2A P3 F4A . . . . -117.7(18) ? F4A F2A P3 F5A . . . . -72.7(16) ? F3A F2A P3 F5A . . . . 169.6(11) ? F4A F2A P3 F3A . . . . 117.7(18) ? F4A F2A P3 F1A . . . . -173.2(12) ? F3A F2A P3 F1A . . . . 69.1(14) ? F2A F3A P3 F6A . . . . 144.7(19) ? F2A F3A P3 F4A . . . . 46.3(15) ? F2A F3A P3 F1A . . . . -127.0(13) ? F1B F2B P3 F3B . . . . -91.6(9) ? F1B F2B P3 F6B . . . . 29.0(17) ? F1B F2B P3 F5B . . . . 94.5(9) ? F1B F2B P3 F4B . . . . 177.5(7) ?