#------------------------------------------------------------------------------ #$Date: 2024-06-28 04:46:00 +0300 (Fri, 28 Jun 2024) $ #$Revision: 292633 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/25/2312529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312529 _cell_angle_alpha 90.000 _cell_angle_beta 109.266 _cell_angle_gamma 90.000 _cell_length_a 14.9624 _cell_length_b 21.9572 _cell_length_c 17.1148 _exptl_crystal_F_000 2056.00 _reflns_d_resolution_high 0.7378 _cod_data_source_file yd30433_Ru47dmphensup4.hkl _cod_data_source_block 3_Ru47dmphen _shelx_title ' SIR92 run in space group P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50475.42 50589.99 28184.80 o 3 0 0 17548.50 14772.18 132.34 o 4 0 0 27205.25 29393.91 265.61 o 5 0 0 266.08 193.79 21.57 o 6 0 0 41148.58 43256.66 465.63 o 7 0 0 1793.22 1693.07 101.29 o 8 0 0 3199.74 3097.97 148.12 o 9 0 0 2015.37 2212.11 135.56 o 10 0 0 3154.27 3050.97 169.68 o 11 0 0 3338.89 3534.31 192.11 o 12 0 0 1590.76 1531.65 135.32 o 13 0 0 198.34 181.13 68.26 o 14 0 0 1.31 35.42 44.00 o 15 0 0 619.85 766.76 111.28 o 16 0 0 1405.11 1447.68 159.33 o 17 0 0 252.27 249.96 84.12 o 18 0 0 139.24 207.44 84.13 o 2 1 0 26667.41 30594.64 256.84 o 3 1 0 1244.51 1692.15 31.37 o 4 1 0 15459.21 14674.66 188.54 o 5 1 0 2230.57 2468.50 49.48 o 6 1 0 4165.44 4908.27 110.82 o 7 1 0 826.23 932.05 54.03 o 8 1 0 1348.61 1055.98 62.41 o 9 1 0 708.44 640.75 54.57 o 10 1 0 1223.36 1233.19 77.69 o 11 1 0 3.10 10.55 27.93 o 12 1 0 0.24 24.03 29.56 o 13 1 0 56.10 116.17 42.25 o 14 1 0 671.66 703.52 73.53 o 15 1 0 1.01 -17.76 37.70 o 16 1 0 91.25 137.56 47.74 o 17 1 0 84.38 88.36 44.26 o 18 1 0 295.16 392.63 77.68 o 3 2 0 52066.21 51253.45 175.82 o 4 2 0 952.82 1052.82 29.04 o 5 2 0 0.30 14.34 7.13 o 6 2 0 34.05 21.87 29.58 o 7 2 0 2349.48 2012.45 77.85 o 8 2 0 2229.23 2354.44 90.96 o 9 2 0 7407.85 7517.04 187.79 o 10 2 0 1946.28 2092.26 99.88 o 11 2 0 946.90 1154.96 90.75 o 12 2 0 133.54 108.53 47.39 o 13 2 0 288.69 309.00 48.40 o 14 2 0 7.55 31.17 31.38 o 15 2 0 371.82 364.99 59.82 o 16 2 0 157.37 127.77 46.35 o 17 2 0 50.22 33.22 64.63 o 18 2 0 170.27 207.16 57.38 o 1 3 0 106028.69 106788.00 531.79 o 2 3 0 1620.43 1784.22 29.50 o 3 3 0 6364.15 5850.61 53.37 o 4 3 0 5472.28 5702.37 129.06 o 5 3 0 11028.12 10612.25 151.04 o 6 3 0 2330.33 2582.06 64.16 o 7 3 0 13190.42 13672.00 202.38 o 8 3 0 9.72 24.27 18.25 o 9 3 0 2.11 7.52 20.02 o 10 3 0 3040.89 2904.22 117.46 o 11 3 0 3542.67 3485.11 134.99 o 12 3 0 1199.84 1203.29 87.00 o 13 3 0 2205.16 2487.25 128.45 o 14 3 0 3866.28 3857.56 167.35 o 15 3 0 175.67 216.12 51.42 o 16 3 0 389.19 441.68 68.45 o 17 3 0 1227.65 1223.50 111.00 o 18 3 0 424.51 502.06 114.34 o 0 4 0 15793.82 12471.72 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197.09 243.55 58.66 o 17 5 0 309.25 277.85 59.11 o 18 5 0 96.99 105.32 65.91 o 0 6 0 43214.86 43025.12 726.72 o 1 6 0 7337.69 7805.12 142.81 o 2 6 0 20.93 10.45 7.90 o 3 6 0 21495.87 22375.32 251.11 o 4 6 0 1715.27 1424.29 28.28 o 5 6 0 4826.23 4973.08 106.96 o 6 6 0 9439.91 9443.75 108.06 o 7 6 0 1706.05 1865.86 56.50 o 8 6 0 2252.49 2306.95 68.81 o 9 6 0 2829.25 2971.68 111.62 o 10 6 0 1155.56 1071.89 103.54 o 11 6 0 191.34 162.06 33.62 o 12 6 0 7261.32 7373.76 442.90 o 13 6 0 2587.94 2780.49 136.26 o 14 6 0 293.50 263.76 50.74 o 15 6 0 1710.55 1997.31 127.53 o 16 6 0 1675.78 1619.06 121.67 o 17 6 0 16.22 29.89 47.76 o 18 6 0 178.88 97.55 62.24 o 1 7 0 1684.53 1736.91 34.19 o 2 7 0 503.94 370.48 15.81 o 3 7 0 2799.55 2590.59 45.92 o 4 7 0 8624.56 8126.56 270.30 o 5 7 0 6847.90 6176.84 207.33 o 6 7 0 25.99 5.96 7.07 o 7 7 0 1114.21 1063.69 41.96 o 8 7 0 3860.01 3897.26 118.79 o 9 7 0 553.64 477.40 33.96 o 10 7 0 6938.95 7325.13 186.07 o 11 7 0 14.31 62.89 31.18 o 12 7 0 268.82 208.22 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13 9 0 1753.43 1919.42 175.11 o 14 9 0 1781.41 2205.00 203.23 o 15 9 0 398.93 419.58 99.96 o 16 9 0 246.37 272.88 83.85 o 0 10 0 7033.60 7089.71 126.59 o 1 10 0 1056.25 1116.16 34.05 o 2 10 0 2007.91 2089.37 48.02 o 3 10 0 768.01 588.91 22.74 o 4 10 0 1929.89 2066.10 54.78 o 5 10 0 2701.59 2690.51 67.46 o 6 10 0 5518.87 5314.44 236.44 o 7 10 0 1904.66 1724.39 79.10 o 8 10 0 3599.59 3372.02 95.91 o 9 10 0 5762.75 5783.93 147.56 o 10 10 0 1389.44 1391.81 133.52 o 11 10 0 77.49 98.98 42.04 o 12 10 0 678.90 615.28 102.33 o 13 10 0 240.92 268.84 83.54 o 14 10 0 0.12 -24.21 60.86 o 15 10 0 441.25 462.70 108.88 o 16 10 0 212.23 179.17 81.74 o 1 11 0 675.25 929.46 32.51 o 2 11 0 5345.64 5645.10 83.74 o 3 11 0 717.41 549.52 34.36 o 4 11 0 3615.77 4046.59 77.82 o 5 11 0 12.26 0.85 10.32 o 6 11 0 2592.75 2464.50 70.75 o 7 11 0 2363.02 2530.16 87.84 o 8 11 0 1933.81 1802.75 53.24 o 9 11 0 321.34 327.66 68.96 o 10 11 0 89.76 50.77 33.32 o 11 11 0 161.69 135.36 48.97 o 12 11 0 324.30 330.32 84.46 o 13 11 0 401.73 436.22 98.41 o 14 11 0 1333.38 1248.21 157.49 o 15 11 0 10.05 -34.88 78.96 o 16 11 0 59.96 -96.08 96.08 o 0 12 0 4058.14 4045.08 103.78 o 1 12 0 626.47 593.25 23.30 o 2 12 0 1881.67 2110.46 54.09 o 3 12 0 3988.91 3462.02 61.57 o 4 12 0 1795.34 2055.21 56.98 o 5 12 0 366.33 431.45 28.72 o 6 12 0 5325.27 5796.63 170.28 o 7 12 0 4028.11 3837.36 107.69 o 8 12 0 2413.70 2563.95 166.43 o 9 12 0 929.62 813.14 100.85 o 10 12 0 2523.18 2191.82 170.46 o 11 12 0 60.36 68.57 34.13 o 12 12 0 3097.14 2994.76 217.52 o 13 12 0 1036.51 1037.00 139.08 o 14 12 0 118.61 -23.85 67.34 o 15 12 0 1330.89 1511.54 180.39 o 1 13 0 4807.35 4495.50 65.39 o 2 13 0 9773.91 9782.49 121.56 o 3 13 0 377.81 355.56 21.66 o 4 13 0 10099.72 10469.57 132.29 o 5 13 0 4769.55 4594.06 98.73 o 6 13 0 295.80 305.94 27.24 o 7 13 0 3331.58 3366.84 132.28 o 8 13 0 6736.97 6802.20 274.39 o 9 13 0 1651.62 1618.28 142.82 o 10 13 0 354.20 407.58 81.18 o 11 13 0 956.52 819.66 113.53 o 12 13 0 250.77 202.84 63.73 o 13 13 0 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