#------------------------------------------------------------------------------ #$Date: 2024-08-07 01:03:20 +0300 (Wed, 07 Aug 2024) $ #$Revision: 293986 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312532.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312532 loop_ _publ_author_name 'Shit, Pradip' 'Tetrault, Timothy' 'Zhang, Wenhui' 'Yoon, Mi Kyung' 'Oliver, Allen G.' 'Serianni, Anthony S.' _publ_section_title ; Conformational disorder in the crystal structure of methyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1→4)-2-acetamido-2-deoxy-β-D-glucopyranoside (methyl β-chitobioside) methanol monosolvate. ; _journal_coeditor_code DG3055 _journal_issue 'Pt 7' _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_page_first 331 _journal_page_last 336 _journal_paper_doi 10.1107/S2053229624005199 _journal_volume 80 _journal_year 2024 _chemical_absolute_configuration rm _chemical_formula_iupac 'C17 H30 N2 O11, C H4 O' _chemical_formula_moiety 'C17 H30 N2 O11, C H4 O' _chemical_formula_sum 'C18 H34 N2 O12' _chemical_formula_weight 470.47 _chemical_name_common ; Methyl \b-chitobioside methanol monosolvate ; _chemical_name_systematic ;Methyl 2-acetamido-2-deoxy-\b-D-glucopyranosyl-(1\\rightarrow4)-2-acetamido-2-deoxy-\b-D-glucopyranoside methanol monosolvate ; _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method ; FinalCif V123 by Daniel Kratzert, Freiburg 2023, https://dkratzert.de/finalcif.html ; _cell_angle_alpha 90 _cell_angle_beta 90.022(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 4.75990(10) _cell_length_b 14.3223(5) _cell_length_c 16.6515(5) _cell_measurement_reflns_used 9983 _cell_measurement_temperature 260(2) _cell_measurement_theta_max 71.9395 _cell_measurement_theta_min 2.6535 _cell_volume 1135.18(6) _computing_cell_refinement ; SAINT (Bruker, 2023) ; _computing_data_collection ; APEX-4 (Bruker, 2023) ; _computing_data_reduction ; SAINT (Bruker, 2023) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2020) ; _computing_publication_material ; FinalCIF (Kratzert, 2023) ; _computing_structure_refinement ; SHELXL2019 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2018 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 260(2) _diffrn_detector 'CMOS Area Detector' _diffrn_detector_area_resol_mean 7.41 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker Venture' _diffrn_measurement_method 'combination of \w and \f-scans' _diffrn_radiation_monochromator 'HELIOS Multi-layer' _diffrn_radiation_probe x-ray _diffrn_radiation_source 'Incoatec Diamond micro-focus' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0475 _diffrn_reflns_av_unetI/netI 0.0400 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 20006 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 72.661 _diffrn_reflns_theta_min 2.653 _diffrn_source_current 1.2 _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 0.993 _exptl_absorpt_correction_T_max 1.0 _exptl_absorpt_correction_T_min 0.8252 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (SADABS2016; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.376 _exptl_crystal_description needle _exptl_crystal_F_000 504 _exptl_crystal_size_max 0.258 _exptl_crystal_size_mid 0.039 _exptl_crystal_size_min 0.022 _refine_diff_density_max 0.194 _refine_diff_density_min -0.137 _refine_ls_abs_structure_details ; Twinning involves inversion, so Flack parameter cannot be determined ; _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.044 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 330 _refine_ls_number_reflns 4462 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.044 _refine_ls_R_factor_all 0.0316 _refine_ls_R_factor_gt 0.0312 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0524P)^2^+0.0431P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0796 _refine_ls_wR_factor_ref 0.0801 _reflns_number_gt 4410 _reflns_number_total 4462 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dg3055sup1.cif _cod_data_source_block I _cod_depositor_comments 'Adding full bibliography for 2312532.cif.' _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 2312532 _cod_database_fobs_code 2312532 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.784 _shelx_estimated_absorpt_t_max 0.978 _shelx_hkl_file ; -1 0 0 152.68 6.70 1 0 0 158.18 7.50 2 0 0 3955.00 160.48 3 0 0 26.00 4.50 4 0 0 25.00 2.10 4 0 0 26.10 5.80 4 0 0 29.00 2.10 4 0 0 25.90 2.00 4 0 0 25.20 2.00 4 0 0 28.40 2.20 4 0 0 26.40 2.20 4 0 0 27.30 2.30 4 0 0 26.60 2.00 4 0 0 24.50 1.90 -5 0 0 17.50 1.90 5 0 0 15.80 1.70 5 0 0 16.50 1.50 5 0 0 17.70 1.60 5 0 0 15.20 1.40 5 0 0 14.20 1.40 5 -1 0 17.30 1.50 5 -1 0 17.30 1.50 5 -1 0 15.40 1.40 5 -1 0 14.50 1.40 5 -1 0 15.40 1.60 4 -1 0 55.59 3.30 4 -1 0 55.99 3.60 4 -1 0 63.59 3.40 4 -1 0 55.59 3.20 4 -1 0 58.29 3.30 4 -1 0 55.49 3.10 4 -1 0 61.69 3.40 4 -1 0 56.89 6.20 4 -1 0 56.89 3.40 3 -1 0 159.58 10.30 2 -1 0 64.19 4.80 0 -1 0 0.40 0.20 0 -1 0 0.10 0.20 1 1 0 9999.00 394.86 -2 -1 0 61.09 4.00 2 1 0 67.19 5.00 3 1 0 164.08 10.70 4 1 0 55.59 3.20 4 1 0 63.59 3.60 4 1 0 60.49 3.40 4 1 0 57.39 3.40 4 1 0 59.59 3.40 4 1 0 59.29 3.50 4 1 0 56.69 3.40 4 1 0 59.49 6.60 4 1 0 58.19 3.70 4 1 0 56.79 3.00 -5 -1 0 15.60 1.50 5 1 0 17.00 1.50 5 1 0 16.00 1.60 5 1 0 16.80 1.70 5 1 0 18.70 1.80 5 1 0 16.50 1.60 5 1 0 16.50 1.70 5 -2 0 20.30 1.80 5 -2 0 17.10 1.40 5 -2 0 19.20 1.50 5 -2 0 18.70 1.50 5 -2 0 18.00 1.70 5 -2 0 16.90 1.40 4 -2 0 1.10 0.60 4 -2 0 1.70 0.90 4 -2 0 1.60 0.80 4 -2 0 1.20 0.70 4 -2 0 2.20 1.70 4 -2 0 1.30 0.70 4 -2 0 1.80 0.80 4 -2 0 0.50 0.60 4 -2 0 1.20 0.70 3 -2 0 40.60 5.70 2 -2 0 487.45 20.20 2 -2 0 453.85 21.10 1 -2 0 240.68 11.10 1 -2 0 263.67 11.00 0 -2 0 205.88 9.20 0 -2 0 208.28 9.20 0 2 0 242.08 9.00 -1 -2 0 251.87 10.80 1 2 0 226.48 10.90 1 2 0 238.08 10.30 1 2 0 255.67 11.20 -2 -2 0 453.25 19.80 2 2 0 452.25 20.90 -3 -2 0 35.70 3.50 3 2 0 45.70 6.50 4 2 0 0.90 0.80 4 2 0 0.70 0.80 4 2 0 0.30 0.70 4 2 0 1.00 0.80 4 2 0 2.10 2.10 4 2 0 1.50 0.80 4 2 0 2.00 0.60 4 2 0 2.40 0.90 4 2 0 1.70 0.90 4 2 0 2.00 0.80 -5 -2 0 18.20 1.50 5 2 0 19.60 1.70 5 2 0 17.40 1.70 5 2 0 15.90 1.40 5 2 0 17.90 1.80 5 2 0 18.20 1.60 5 2 0 16.30 1.60 5 2 0 17.90 1.60 5 -3 0 8.20 1.00 5 -3 0 9.60 1.30 5 -3 0 9.40 1.70 5 -3 0 8.80 1.00 -5 3 0 9.00 1.00 4 -3 0 37.60 2.80 4 -3 0 42.70 6.40 4 -3 0 34.80 2.30 4 -3 0 39.80 2.40 4 -3 0 36.50 2.30 4 -3 0 37.80 2.70 4 -3 0 38.00 2.50 -4 3 0 37.90 2.30 3 -3 0 24.40 2.00 3 -3 0 31.60 1.90 3 -3 0 28.70 2.10 3 -3 0 22.70 2.50 3 -3 0 27.90 1.90 3 -3 0 31.40 4.80 2 -3 0 546.85 23.40 2 -3 0 544.05 24.00 -1 3 0 1040.20 46.60 0 -3 0 -0.10 0.50 0 -3 0 -0.30 0.70 0 3 0 0.40 0.60 1 3 0 1038.50 41.40 -2 -3 0 543.15 23.40 2 3 0 523.75 24.20 -3 -3 0 30.40 4.30 3 3 0 29.60 2.10 3 3 0 30.50 2.20 3 3 0 35.50 5.80 3 3 0 28.00 2.00 3 3 0 28.30 2.20 3 3 0 27.90 1.80 3 3 0 28.10 2.30 3 3 0 26.10 2.10 3 3 0 29.90 2.30 4 3 0 34.60 2.50 4 3 0 31.60 2.40 4 3 0 36.80 2.70 4 3 0 33.50 2.60 4 3 0 34.90 2.10 4 3 0 37.40 2.70 4 3 0 36.60 2.50 4 3 0 28.80 5.30 4 3 0 32.90 2.40 4 3 0 40.00 2.60 -5 -3 0 7.10 1.00 5 3 0 7.80 1.20 5 3 0 9.10 1.40 5 3 0 7.20 1.10 5 3 0 11.40 1.40 5 3 0 9.20 1.10 5 3 0 9.40 1.30 5 3 0 8.70 1.30 5 -4 0 88.69 4.10 5 -4 0 88.19 4.20 5 -4 0 85.89 3.90 5 -4 0 86.99 4.30 -5 4 0 83.69 3.90 4 -4 0 18.50 1.60 4 -4 0 19.20 1.50 4 -4 0 19.80 1.70 4 -4 0 18.90 2.20 4 -4 0 16.80 1.50 4 -4 0 21.00 4.40 4 -4 0 15.80 1.70 -4 4 0 15.70 1.60 -4 4 0 18.50 4.40 -4 4 0 17.30 1.40 3 -4 0 22.80 1.60 3 -4 0 18.40 1.40 3 -4 0 28.10 4.50 3 -4 0 22.90 1.50 3 -4 0 19.00 1.70 3 -4 0 23.20 2.30 2 -4 0 27.10 2.90 2 -4 0 25.80 2.90 1 -4 0 152.28 7.40 1 -4 0 151.18 6.90 -1 4 0 135.19 7.10 0 -4 0 75.39 4.50 0 -4 0 77.29 4.40 0 4 0 92.89 4.20 -1 -4 0 131.39 6.20 -1 -4 0 135.99 7.10 1 4 0 133.79 6.00 1 4 0 136.69 7.10 -2 -4 0 27.60 3.70 2 4 0 24.00 3.60 3 4 0 21.10 2.60 3 4 0 19.10 4.10 3 4 0 27.40 2.80 3 4 0 21.10 1.80 3 4 0 21.30 1.80 3 4 0 18.90 1.90 3 4 0 22.50 2.10 3 4 0 20.60 1.80 4 4 0 16.60 1.80 4 4 0 19.30 5.00 4 4 0 15.20 2.00 4 4 0 17.50 1.90 4 4 0 20.60 2.40 4 4 0 18.80 1.50 4 4 0 19.30 2.00 4 4 0 16.90 2.00 4 4 0 18.00 2.00 4 4 0 15.40 1.70 -5 -4 0 78.39 4.00 5 4 0 81.89 4.20 5 4 0 83.59 4.10 5 4 0 82.99 4.10 5 4 0 86.69 4.30 5 4 0 80.39 4.20 5 4 0 84.09 3.90 5 4 0 82.39 4.10 5 -5 0 0.50 0.70 5 -5 0 1.00 0.60 -5 5 0 1.00 0.40 4 -5 0 178.28 7.70 4 -5 0 173.08 8.00 4 -5 0 185.58 13.00 4 -5 0 166.38 7.20 4 -5 0 165.78 7.40 4 -5 0 158.38 7.30 -4 5 0 151.98 7.20 -4 5 0 163.58 7.20 -4 5 0 178.18 16.20 3 -5 0 112.39 5.10 3 -5 0 108.69 5.70 3 -5 0 110.59 5.00 3 -5 0 114.69 4.90 3 -5 0 108.19 7.40 3 -5 0 112.79 5.70 -3 5 0 100.59 4.90 -3 5 0 100.49 5.10 -3 5 0 104.29 7.80 2 -5 0 133.59 7.20 2 -5 0 138.99 7.90 -2 5 0 116.99 7.50 1 -5 0 1196.68 46.60 -1 5 0 1127.09 47.20 0 -5 0 0.10 0.80 0 -5 0 0.50 1.00 0 5 0 -0.10 0.80 0 5 0 0.80 0.70 -1 -5 0 1033.80 41.50 -1 -5 0 997.30 40.30 1 5 0 965.10 41.10 -2 -5 0 124.49 7.80 2 5 0 119.99 7.90 -3 -5 0 104.79 8.00 3 5 0 109.69 5.10 3 5 0 117.29 5.50 3 5 0 114.99 5.40 3 5 0 114.49 5.70 3 5 0 109.19 5.30 3 5 0 111.89 5.80 3 5 0 107.19 5.40 3 5 0 109.89 8.70 3 5 0 107.59 5.40 3 5 0 110.19 5.40 3 5 0 110.99 5.70 -4 -5 0 153.88 7.30 4 5 0 164.48 7.80 4 5 0 155.58 7.70 4 5 0 161.18 7.10 4 5 0 164.28 7.70 4 5 0 152.38 7.40 4 5 0 155.08 7.40 4 5 0 177.98 7.60 4 5 0 158.38 7.30 4 5 0 138.19 13.20 4 5 0 164.68 7.40 -5 -5 0 0.80 0.60 5 5 0 2.80 0.70 5 5 0 1.50 0.70 5 5 0 2.60 1.30 5 5 0 0.80 0.70 5 5 0 1.50 0.90 5 5 0 1.20 0.70 5 -6 0 24.00 1.50 5 -6 0 23.40 1.80 4 -6 0 25.10 2.40 4 -6 0 24.30 1.90 4 -6 0 26.60 1.80 4 -6 0 20.80 1.50 4 -6 0 30.60 5.50 -4 6 0 22.40 1.60 -4 6 0 33.90 5.20 3 -6 0 84.29 4.00 3 -6 0 85.79 4.10 3 -6 0 88.19 5.00 3 -6 0 88.89 6.30 3 -6 0 84.79 4.30 -3 6 0 83.49 4.00 -3 6 0 89.09 7.00 -3 6 0 91.19 4.00 2 -6 0 91.79 5.50 2 -6 0 94.09 6.50 -2 6 0 82.59 6.00 1 -6 0 488.35 22.00 -1 6 0 500.05 21.20 0 -6 0 2255.07 90.39 -1 -6 0 419.26 18.20 -1 -6 0 451.65 19.50 1 6 0 402.56 18.90 -2 -6 0 97.49 6.80 2 6 0 85.99 6.60 2 6 0 83.69 6.50 -3 -6 0 76.29 6.90 3 6 0 78.59 4.50 3 6 0 84.49 4.60 3 6 0 80.49 4.00 3 6 0 83.29 4.30 3 6 0 85.29 4.40 3 6 0 80.59 7.30 3 6 0 80.99 4.30 3 6 0 81.29 4.30 3 6 0 75.19 4.20 3 6 0 86.99 4.60 -4 -6 0 24.50 2.00 4 6 0 22.80 2.20 4 6 0 24.60 1.80 4 6 0 21.10 2.00 4 6 0 22.90 2.00 4 6 0 24.10 2.20 4 6 0 21.60 2.10 4 6 0 23.30 1.90 4 6 0 22.30 2.40 4 6 0 22.60 2.10 4 6 0 17.30 4.40 -5 -6 0 21.40 1.60 5 6 0 23.00 1.60 5 6 0 22.10 1.70 5 6 0 24.40 1.70 5 6 0 24.60 1.90 5 6 0 22.80 1.70 5 6 0 25.80 1.70 5 6 0 22.50 1.80 5 -7 0 2.80 0.70 5 -7 0 3.30 0.70 4 -7 0 1.10 0.60 4 -7 0 1.10 1.70 -4 7 0 2.10 0.60 3 -7 0 33.30 2.00 3 -7 0 33.50 2.10 3 -7 0 36.30 3.70 3 -7 0 33.40 2.90 3 -7 0 34.30 2.20 -3 7 0 43.80 8.20 -3 7 0 33.70 1.90 2 -7 0 151.38 9.80 2 -7 0 163.58 8.40 -2 7 0 168.78 9.30 1 -7 0 427.36 19.90 -1 7 0 425.76 18.70 0 -7 0 0.10 0.90 0 -7 0 2.00 1.30 0 7 0 1.10 1.10 0 7 0 0.10 0.70 -1 -7 0 375.76 16.70 -1 -7 0 370.56 17.80 1 7 0 362.56 17.20 -2 -7 0 146.79 9.50 2 7 0 148.49 9.30 2 7 0 140.39 9.30 -3 -7 0 28.40 2.20 -3 -7 0 31.20 2.40 -3 -7 0 30.00 5.40 3 7 0 31.90 2.10 3 7 0 34.00 2.50 3 7 0 33.60 2.40 3 7 0 31.10 2.60 3 7 0 35.10 2.40 3 7 0 36.40 2.50 3 7 0 28.10 2.40 3 7 0 32.80 2.40 3 7 0 34.70 5.80 3 7 0 34.20 2.70 -4 -7 0 1.40 0.80 4 7 0 0.30 0.70 4 7 0 2.00 0.90 4 7 0 0.80 1.30 4 7 0 1.90 0.90 4 7 0 0.60 0.70 4 7 0 2.60 1.00 5 7 0 2.20 0.60 5 7 0 3.60 1.40 5 7 0 3.70 0.70 5 7 0 3.00 0.80 5 7 0 2.00 0.60 5 7 0 2.60 0.70 5 7 0 3.10 0.80 5 -8 0 44.10 2.40 4 -8 0 15.30 1.40 4 -8 0 15.80 2.10 3 -8 0 408.66 18.00 3 -8 0 416.76 17.10 3 -8 0 417.16 17.00 -3 8 0 409.26 16.80 -3 8 0 434.56 20.80 2 -8 0 319.07 13.60 2 -8 0 325.87 17.30 -2 8 0 345.27 16.20 1 -8 0 151.38 9.40 -1 8 0 157.18 8.20 0 -8 0 344.47 16.70 0 -8 0 350.06 16.90 0 8 0 339.07 15.20 0 8 0 365.96 16.00 -1 -8 0 141.39 8.90 -1 -8 0 144.69 7.90 1 8 0 131.59 8.40 -2 -8 0 314.07 16.60 -2 -8 0 293.77 12.50 -2 -8 0 276.17 12.60 2 8 0 295.77 12.70 2 8 0 331.07 13.30 2 8 0 286.57 12.40 2 8 0 292.87 15.70 2 8 0 320.07 13.10 2 8 0 265.27 15.70 2 8 0 315.87 13.30 -3 -8 0 347.27 19.90 -3 -8 0 361.86 17.00 3 8 0 362.26 15.40 3 8 0 329.27 19.30 3 8 0 372.16 15.20 3 8 0 367.76 16.30 3 8 0 375.76 15.90 3 8 0 350.76 15.40 3 8 0 378.56 15.60 3 8 0 376.16 15.50 3 8 0 383.76 16.00 3 8 0 372.66 15.50 -4 -8 0 12.10 1.60 -4 -8 0 12.20 1.50 4 8 0 14.40 1.60 4 8 0 14.50 1.60 4 8 0 17.30 2.20 4 8 0 17.50 1.70 4 8 0 14.20 1.70 4 8 0 17.20 1.80 4 8 0 13.50 1.70 4 8 0 16.00 1.40 4 8 0 16.20 1.60 -5 -8 0 40.40 2.20 5 8 0 44.10 2.20 5 8 0 43.80 2.40 5 8 0 41.20 2.40 5 -9 0 14.10 1.20 4 -9 0 53.19 3.10 4 -9 0 64.29 3.70 3 -9 0 100.89 4.60 3 -9 0 86.79 4.50 3 -9 0 96.19 5.40 -3 9 0 104.69 7.50 2 -9 0 42.80 6.00 2 -9 0 40.10 2.40 -2 9 0 44.60 4.20 1 -9 0 104.29 5.00 1 -9 0 106.09 7.90 -1 9 0 109.59 6.60 0 -9 0 -0.70 0.90 0 -9 0 -0.90 1.00 0 9 0 0.80 0.70 0 9 0 1.10 1.60 -1 -9 0 98.09 4.70 -1 -9 0 100.19 6.60 -1 -9 0 95.29 5.00 -1 -9 0 113.59 7.90 1 9 0 94.89 6.40 1 9 0 111.99 7.50 -2 -9 0 32.70 2.30 -2 -9 0 41.00 2.60 -2 -9 0 37.10 5.80 2 9 0 35.80 2.60 2 9 0 38.80 2.80 2 9 0 37.00 4.30 2 9 0 41.60 2.80 2 9 0 41.40 2.90 2 9 0 35.50 2.40 2 9 0 35.20 2.60 2 9 0 38.60 2.30 2 9 0 34.50 5.40 -3 -9 0 87.39 4.50 -3 -9 0 91.99 4.80 -3 -9 0 77.89 7.90 3 9 0 93.29 4.80 3 9 0 93.09 4.70 3 9 0 98.69 5.20 3 9 0 92.59 4.60 3 9 0 92.99 4.70 3 9 0 93.69 5.00 3 9 0 88.19 4.30 3 9 0 80.39 4.60 3 9 0 81.39 4.50 -4 -9 0 50.89 3.00 4 9 0 54.99 3.10 4 9 0 56.69 3.40 4 9 0 55.49 3.10 4 9 0 52.79 3.40 4 9 0 54.89 3.00 4 9 0 53.29 3.10 -5 -9 0 13.60 1.10 5 9 0 14.70 1.20 5 9 0 15.10 1.20 5 9 0 13.40 1.10 4 -10 0 22.70 2.20 3 -10 0 20.00 1.60 3 -10 0 19.10 2.40 -3 10 0 17.70 3.60 2 -10 0 27.30 5.40 2 -10 0 25.90 2.60 -2 10 0 22.60 3.60 1 -10 0 52.39 5.60 1 -10 0 51.09 3.10 1 -10 0 51.29 3.00 -1 10 0 58.99 4.80 -1 10 0 58.49 4.20 0 -10 0 328.47 14.30 0 -10 0 358.26 17.70 0 -10 0 337.37 14.40 0 -10 0 337.87 17.50 0 10 0 346.57 16.70 -1 -10 0 49.80 3.00 -1 -10 0 51.79 4.70 -1 -10 0 49.70 2.90 -1 -10 0 51.39 5.40 1 10 0 53.09 5.30 1 10 0 49.70 2.90 -2 -10 0 20.20 1.80 -2 -10 0 21.10 2.00 -2 -10 0 22.60 4.90 2 10 0 21.60 4.30 2 10 0 22.90 2.30 2 10 0 21.50 1.60 2 10 0 22.90 1.90 2 10 0 19.70 1.90 2 10 0 21.30 2.40 -3 -10 0 14.00 4.20 -3 -10 0 18.90 2.00 -3 -10 0 19.50 1.90 3 10 0 16.70 2.10 3 10 0 18.80 2.00 3 10 0 18.30 1.90 3 10 0 17.00 2.20 3 10 0 19.60 1.60 3 10 0 18.30 1.80 3 10 0 17.50 1.70 -4 -10 0 19.30 1.70 4 10 0 21.10 1.70 4 10 0 20.70 1.60 4 10 0 20.50 1.70 4 10 0 19.80 1.50 4 10 0 20.10 2.10 4 10 0 15.90 1.80 4 -11 0 82.79 4.30 3 -11 0 -0.60 0.90 3 -11 0 0.30 0.60 2 -11 0 64.79 3.60 2 -11 0 67.89 7.30 2 -11 0 62.79 4.10 -2 11 0 70.79 5.90 -2 11 0 72.99 5.50 1 -11 0 290.47 12.60 1 -11 0 287.37 12.60 -1 11 0 301.67 13.90 -1 11 0 304.27 15.20 0 -11 0 0.50 0.60 0 -11 0 0.90 0.80 0 -11 0 1.60 1.50 0 -11 0 0.80 1.60 0 -11 0 1.60 0.80 0 11 0 2.80 2.00 -1 -11 0 274.77 11.80 -1 -11 0 280.17 11.70 -1 -11 0 282.07 14.90 -1 -11 0 251.07 12.30 -1 -11 0 297.87 18.80 1 11 0 267.27 11.60 1 11 0 268.97 15.20 -2 -11 0 53.89 7.80 -2 -11 0 60.09 3.60 -2 -11 0 58.89 3.40 2 11 0 58.99 3.10 2 11 0 60.39 3.80 2 11 0 58.69 3.50 2 11 0 61.99 3.70 2 11 0 58.69 3.40 -3 -11 0 0.40 0.80 -3 -11 0 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7 -2 130.39 6.40 3 7 -2 121.49 5.90 3 7 -2 124.49 6.40 3 7 -2 131.39 5.70 3 7 -2 122.09 6.30 3 7 -2 123.69 10.70 3 7 -2 128.39 6.00 3 7 -2 128.49 6.00 3 7 -2 131.39 6.20 -3 -7 2 120.99 6.10 -3 -7 2 119.29 5.90 2 7 -2 82.49 5.20 2 7 -2 82.59 7.00 2 7 -2 87.59 7.30 -2 -7 2 92.09 7.10 1 7 -2 123.39 6.90 1 7 -2 145.09 8.80 -1 -7 2 149.99 8.80 -1 -7 2 153.18 7.80 0 7 -2 1032.40 41.90 0 7 -2 1111.49 42.90 0 -7 2 981.90 43.40 0 -7 2 1024.00 43.40 -1 7 -2 162.68 8.30 1 -7 2 155.18 9.20 -2 7 -2 96.69 6.50 2 -7 2 101.09 7.50 -3 7 -2 127.69 5.80 -3 7 -2 139.29 9.20 3 -7 2 137.89 6.90 3 -7 2 148.59 6.20 3 -7 2 139.89 6.00 3 -7 2 136.49 6.20 3 -7 2 146.69 8.90 3 -7 2 130.59 5.90 -4 7 -2 52.39 2.40 4 -7 2 51.79 2.80 4 -7 2 47.60 3.40 4 -7 2 44.30 2.50 5 -7 2 25.50 1.60 5 -7 2 24.30 1.70 5 6 -2 10.30 1.00 5 6 -2 10.30 1.30 5 6 -2 8.50 1.10 5 6 -2 9.30 1.20 5 6 -2 12.50 1.30 -5 -6 2 9.50 1.10 4 6 -2 17.40 1.70 4 6 -2 24.70 2.20 4 6 -2 22.20 1.90 4 6 -2 20.80 2.00 4 6 -2 22.60 1.90 4 6 -2 20.20 1.90 4 6 -2 23.90 2.20 4 6 -2 23.30 2.00 -4 -6 2 21.50 1.90 -4 -6 2 22.30 2.40 3 6 -2 16.40 2.00 3 6 -2 18.40 4.40 3 6 -2 17.90 1.90 3 6 -2 17.50 1.50 3 6 -2 20.90 1.80 3 6 -2 20.90 2.00 3 6 -2 20.00 1.90 3 6 -2 20.00 1.80 3 6 -2 24.10 2.30 -3 -6 2 19.80 1.80 -3 -6 2 17.60 3.80 -3 -6 2 19.70 1.90 2 6 -2 87.69 7.00 2 6 -2 90.89 5.50 2 6 -2 94.69 7.20 -2 -6 2 93.29 6.90 1 6 -2 66.69 4.10 1 6 -2 71.89 5.50 -1 -6 2 68.49 5.20 -1 -6 2 65.69 4.30 0 6 -2 14.60 2.10 0 6 -2 12.50 1.60 0 -6 2 10.80 2.10 -1 6 -2 85.59 5.10 1 -6 2 85.09 5.80 -2 6 -2 112.39 7.30 2 -6 2 108.99 6.30 2 -6 2 94.69 7.10 -3 6 -2 23.60 4.00 -3 6 -2 20.40 1.40 3 -6 2 23.90 3.90 3 -6 2 18.60 1.30 3 -6 2 20.60 1.60 3 -6 2 18.30 1.60 3 -6 2 15.80 1.30 3 -6 2 19.70 2.20 -4 6 -2 24.90 7.10 -4 6 -2 20.20 1.50 4 -6 2 22.00 1.80 4 -6 2 22.60 1.60 4 -6 2 26.10 1.80 4 -6 2 22.10 2.30 5 -6 2 11.30 1.20 5 -6 2 10.40 1.10 5 5 -2 11.10 1.40 5 5 -2 13.90 1.60 5 5 -2 12.40 1.40 5 5 -2 11.60 1.50 5 5 -2 11.90 1.20 -5 -5 2 10.50 1.20 4 5 -2 42.60 3.00 4 5 -2 41.00 2.70 4 5 -2 45.00 3.00 4 5 -2 45.10 3.10 4 5 -2 44.70 2.70 4 5 -2 41.30 2.60 4 5 -2 42.20 2.80 4 5 -2 39.40 8.00 4 5 -2 43.10 2.70 -4 -5 2 38.10 2.70 -4 -5 2 40.30 2.80 3 5 -2 31.20 5.40 3 5 -2 33.90 2.50 3 5 -2 34.30 2.60 3 5 -2 34.00 2.00 3 5 -2 33.00 2.30 3 5 -2 32.70 2.30 3 5 -2 31.80 2.50 3 5 -2 32.40 2.30 3 5 -2 29.60 2.20 3 5 -2 33.90 2.40 -3 -5 2 30.80 2.20 -3 -5 2 28.90 4.60 -3 -5 2 30.90 2.40 2 5 -2 49.70 4.90 2 5 -2 46.70 4.80 2 5 -2 52.49 3.90 -2 -5 2 48.30 4.50 1 5 -2 26.50 3.30 1 5 -2 28.80 2.40 -1 -5 2 30.00 3.10 -1 -5 2 31.60 2.50 0 5 -2 75.39 3.90 0 5 -2 82.89 4.40 0 -5 2 69.69 4.60 0 -5 2 69.19 4.50 -1 5 -2 32.50 2.70 1 -5 2 32.90 3.20 1 -5 2 36.40 2.60 -2 5 -2 49.00 4.20 2 -5 2 47.20 3.70 -3 5 -2 35.40 4.30 3 -5 2 36.90 2.20 3 -5 2 38.00 2.20 3 -5 2 35.40 2.70 3 -5 2 34.20 1.90 3 -5 2 31.40 3.70 3 -5 2 37.80 2.60 3 -5 2 35.60 2.30 3 -5 2 34.90 2.10 -4 5 -2 50.39 6.10 -4 5 -2 41.20 2.40 4 -5 2 50.49 2.80 4 -5 2 46.60 2.50 4 -5 2 46.70 2.70 4 -5 2 44.50 2.80 4 -5 2 44.00 3.10 4 -5 2 48.10 5.50 -5 5 -2 9.70 0.90 5 -5 2 14.60 1.60 5 -5 2 11.70 1.20 5 -5 2 11.50 1.30 5 -5 2 10.80 1.00 5 4 -2 38.30 2.60 5 4 -2 43.50 2.70 5 4 -2 43.30 2.80 5 4 -2 45.00 2.60 5 4 -2 43.00 2.40 -5 -4 2 40.80 2.40 4 4 -2 82.59 4.30 4 4 -2 87.29 4.90 4 4 -2 81.79 8.30 4 4 -2 80.39 4.30 4 4 -2 90.79 4.70 4 4 -2 87.79 4.10 4 4 -2 88.39 4.60 4 4 -2 88.59 4.50 4 4 -2 83.69 4.70 4 4 -2 88.09 4.50 -4 -4 2 80.69 4.40 -4 -4 2 80.69 4.30 3 4 -2 40.70 6.30 3 4 -2 42.60 2.40 3 4 -2 44.00 2.70 3 4 -2 49.50 3.30 3 4 -2 45.10 3.00 3 4 -2 44.30 2.80 -3 -4 2 47.50 4.70 2 4 -2 29.90 3.50 2 4 -2 21.20 4.00 2 4 -2 21.30 3.70 -2 -4 2 21.00 3.40 1 4 -2 269.17 12.70 1 4 -2 268.77 11.70 -1 -4 2 271.87 12.70 0 4 -2 210.48 9.00 0 4 -2 218.18 9.40 0 -4 2 206.78 9.70 0 -4 2 202.68 9.80 -1 4 -2 285.67 13.40 1 -4 2 313.77 13.30 1 -4 2 322.57 14.10 -2 4 -2 22.10 3.20 2 -4 2 22.30 2.90 -3 4 -2 44.20 4.70 3 -4 2 40.20 2.50 3 -4 2 45.20 4.40 3 -4 2 41.00 3.00 3 -4 2 42.50 2.40 3 -4 2 43.60 2.40 3 -4 2 46.80 2.60 3 -4 2 42.30 2.40 -4 4 -2 92.39 7.70 4 -4 2 90.39 4.50 4 -4 2 91.99 4.80 4 -4 2 85.69 4.30 4 -4 2 91.29 4.50 4 -4 2 96.19 4.70 4 -4 2 85.69 7.10 4 -4 2 90.49 4.30 -5 4 -2 41.20 2.20 5 -4 2 47.30 2.60 5 -4 2 45.60 2.30 5 -4 2 51.39 2.50 5 -4 2 42.40 3.20 5 3 -2 12.50 1.80 5 3 -2 12.70 1.30 5 3 -2 9.70 1.20 5 3 -2 8.90 1.40 5 3 -2 11.10 1.40 -5 -3 2 11.60 1.50 4 3 -2 20.30 2.20 4 3 -2 18.80 1.80 4 3 -2 17.00 1.70 4 3 -2 19.30 1.80 4 3 -2 21.70 2.40 4 3 -2 16.90 2.20 4 3 -2 15.30 1.80 4 3 -2 13.20 3.80 4 3 -2 19.00 2.10 -4 -3 2 16.10 1.70 -4 -3 2 15.40 1.70 3 3 -2 93.39 7.80 3 3 -2 82.09 4.40 3 3 -2 82.79 4.20 3 3 -2 85.09 4.30 3 3 -2 78.69 3.90 3 3 -2 82.29 4.50 3 3 -2 85.49 4.40 3 3 -2 81.59 4.20 -3 -3 2 75.29 5.90 2 3 -2 108.29 6.20 2 3 -2 105.09 7.30 -2 -3 2 100.89 6.40 1 3 -2 752.72 30.70 -1 -3 2 762.22 31.50 0 -3 2 488.85 20.40 0 -3 2 496.05 20.50 1 -3 2 852.71 35.10 2 -3 2 107.19 6.40 3 -3 2 87.89 4.20 3 -3 2 85.89 4.20 3 -3 2 83.69 4.10 3 -3 2 78.29 6.30 3 -3 2 84.29 4.10 3 -3 2 78.39 4.00 3 -3 2 81.89 4.40 3 -3 2 84.69 4.30 3 -3 2 87.29 4.20 -4 3 -2 18.70 4.10 4 -3 2 14.90 1.80 4 -3 2 18.40 1.70 4 -3 2 16.70 1.60 4 -3 2 16.90 1.50 4 -3 2 18.80 1.80 4 -3 2 18.10 1.50 4 -3 2 15.00 1.50 4 -3 2 16.40 1.60 4 -3 2 21.60 4.50 -5 3 -2 12.50 1.10 5 -3 2 12.40 1.30 5 -3 2 12.80 1.30 5 -3 2 10.20 1.20 5 -3 2 11.70 1.10 5 2 -2 3.00 0.90 5 2 -2 2.10 0.70 5 2 -2 2.80 0.80 5 2 -2 3.50 0.80 5 2 -2 2.90 0.80 -5 -2 2 0.70 0.70 4 2 -2 70.99 3.90 4 2 -2 65.99 3.70 4 2 -2 68.99 3.90 4 2 -2 67.79 3.70 4 2 -2 65.09 4.10 4 2 -2 69.99 3.70 4 2 -2 67.49 7.30 4 2 -2 68.39 3.50 4 2 -2 68.69 3.90 -4 -2 2 65.69 3.70 3 2 -2 128.79 6.60 3 2 -2 132.89 6.40 3 2 -2 141.19 6.30 3 2 -2 140.69 10.00 -3 -2 2 146.39 8.30 2 2 -2 108.79 6.10 2 2 -2 110.09 7.10 -2 -2 2 85.29 6.00 1 2 -2 183.48 8.90 1 2 -2 184.78 8.20 -1 -2 2 176.48 8.60 0 2 -2 103.19 4.50 0 2 -2 96.89 4.70 0 -2 2 83.19 4.60 1 -2 2 177.38 8.20 2 -2 2 92.79 5.90 3 -2 2 151.48 6.80 3 -2 2 141.89 6.50 3 -2 2 154.38 9.50 3 -2 2 140.39 6.70 3 -2 2 146.89 6.70 -4 2 -2 70.39 6.60 4 -2 2 70.89 4.00 4 -2 2 70.99 3.80 4 -2 2 68.29 4.00 4 -2 2 75.39 3.90 4 -2 2 76.99 3.90 4 -2 2 63.19 6.40 4 -2 2 68.79 3.90 4 -2 2 71.89 3.70 4 -2 2 69.89 3.70 4 -2 2 69.49 3.70 5 -2 2 4.00 0.80 5 -2 2 2.30 0.80 5 -2 2 2.40 0.70 5 -2 2 3.50 0.80 5 -2 2 3.30 0.80 5 1 -2 20.60 1.60 5 1 -2 19.10 1.60 5 1 -2 18.20 1.80 5 1 -2 19.90 1.70 5 1 -2 20.80 1.70 -5 -1 2 21.70 1.60 4 1 -2 40.80 2.70 4 1 -2 41.50 2.80 4 1 -2 51.59 7.80 4 1 -2 41.30 2.50 4 1 -2 40.20 2.60 4 1 -2 45.60 3.10 4 1 -2 39.90 2.60 4 1 -2 40.20 2.70 3 1 -2 145.39 10.20 2 1 -2 566.34 25.20 2 1 -2 572.04 26.30 -2 -1 2 620.04 25.00 1 1 -2 435.06 19.40 -1 -1 2 474.15 19.10 0 1 -2 814.82 35.60 1 -1 2 484.95 20.20 2 -1 2 613.54 26.60 3 -1 2 140.89 7.60 3 -1 2 151.08 9.50 4 -1 2 44.20 2.90 4 -1 2 45.20 2.90 4 -1 2 58.39 7.90 4 -1 2 42.30 2.90 4 -1 2 43.90 2.70 4 -1 2 40.80 2.60 4 -1 2 41.30 2.80 4 -1 2 45.30 2.80 4 -1 2 45.00 2.80 4 -1 2 42.50 2.70 5 -1 2 22.20 1.80 5 -1 2 21.60 1.70 5 -1 2 20.60 1.70 5 -1 2 21.00 1.60 5 -1 2 21.10 1.70 5 0 -2 7.10 1.10 5 0 -2 6.80 1.30 5 0 -2 5.70 1.00 5 0 -2 5.30 0.80 -5 0 2 6.10 0.90 4 0 -2 38.60 2.80 4 0 -2 34.80 2.20 4 0 -2 35.40 2.40 4 0 -2 32.10 6.40 4 0 -2 35.50 2.50 4 0 -2 34.40 2.40 4 0 -2 34.30 2.40 4 0 -2 33.70 2.40 -4 0 2 32.80 2.40 3 0 -2 246.68 14.40 2 0 -2 189.48 10.40 2 0 -2 190.48 9.60 -2 0 2 182.38 8.80 1 0 -2 418.76 22.60 0 0 2 517.25 20.90 1 0 2 407.86 17.20 2 0 2 183.18 9.70 3 0 2 258.37 14.20 4 0 2 36.10 2.30 4 0 2 30.50 2.20 4 0 2 31.10 2.30 4 0 2 28.00 2.70 4 0 2 33.30 2.50 4 0 2 33.70 2.30 4 0 2 32.80 2.40 4 0 2 32.70 2.40 4 0 2 35.00 2.50 4 0 2 35.20 2.50 4 0 2 34.40 5.70 4 0 2 34.00 2.40 5 0 2 5.40 0.90 5 0 2 6.30 1.10 5 0 2 5.00 1.00 5 0 2 4.60 1.00 5 0 2 7.00 1.20 5 0 2 5.80 1.00 5 0 2 7.20 1.00 5 -1 -2 20.40 1.50 5 -1 -2 21.90 1.60 5 -1 -2 22.20 1.60 5 -1 -2 21.80 1.60 5 -1 -2 22.50 1.90 -5 1 2 17.70 1.50 4 -1 -2 41.00 3.00 4 -1 -2 44.00 2.60 4 -1 -2 49.00 7.70 4 -1 -2 43.80 2.70 4 -1 -2 41.00 2.40 4 -1 -2 42.50 2.50 4 -1 -2 42.00 2.70 4 -1 -2 40.80 2.60 -4 1 2 40.40 3.10 3 -1 -2 150.68 10.20 2 -1 -2 558.64 25.00 1 -1 -2 473.65 20.60 1 -1 -2 509.85 20.20 1 -1 -2 489.25 20.90 -1 1 2 504.85 20.20 0 -1 -2 792.12 34.50 1 1 2 463.05 19.40 -2 -1 -2 573.94 24.80 2 1 2 604.54 25.90 3 1 2 147.09 9.60 3 1 2 140.79 7.10 4 1 2 46.40 7.30 4 1 2 44.30 2.80 4 1 2 45.00 2.90 4 1 2 44.40 2.80 4 1 2 43.40 2.80 4 1 2 41.90 2.70 4 1 2 42.60 2.50 4 1 2 40.30 2.90 4 1 2 41.40 2.70 4 1 2 42.60 3.00 4 1 2 45.20 2.90 5 1 2 21.50 1.70 5 1 2 19.20 1.70 5 1 2 20.50 1.60 5 1 2 22.00 1.80 5 1 2 19.90 1.80 5 1 2 19.00 1.60 5 1 2 21.50 1.70 5 -2 -2 3.20 0.90 5 -2 -2 3.20 0.70 5 -2 -2 3.30 0.70 -5 2 2 3.20 0.70 4 -2 -2 70.99 3.70 4 -2 -2 63.49 6.70 4 -2 -2 71.69 4.10 4 -2 -2 67.69 3.60 4 -2 -2 69.79 3.60 4 -2 -2 71.59 4.00 4 -2 -2 70.59 3.70 -4 2 2 65.39 3.60 -4 2 2 67.59 3.60 3 -2 -2 143.09 6.30 3 -2 -2 140.49 9.60 2 -2 -2 112.89 6.90 2 -2 -2 105.29 5.70 1 -2 -2 188.88 8.60 1 -2 -2 191.48 8.60 1 -2 -2 172.38 8.20 0 -2 -2 87.19 4.10 0 -2 -2 74.59 3.60 1 2 2 165.38 7.80 -2 -2 -2 116.59 6.30 2 2 2 98.59 6.60 -3 -2 -2 129.19 8.10 3 2 2 136.39 6.60 3 2 2 149.19 6.60 3 2 2 140.99 6.60 3 2 2 140.19 6.60 3 2 2 144.99 6.50 3 2 2 141.09 6.70 3 2 2 149.49 9.70 3 2 2 152.68 6.80 4 2 2 62.39 6.50 4 2 2 71.89 4.10 4 2 2 70.19 3.90 4 2 2 62.69 3.90 4 2 2 69.59 3.90 4 2 2 72.19 3.80 4 2 2 71.69 4.00 4 2 2 70.39 4.00 4 2 2 65.29 3.90 4 2 2 66.29 3.70 4 2 2 69.09 3.50 5 2 2 4.10 0.80 5 2 2 3.20 0.90 5 2 2 1.90 0.70 5 2 2 2.70 0.80 5 2 2 1.80 0.80 5 2 2 3.90 0.90 5 2 2 2.60 0.80 5 -3 -2 13.50 1.20 5 -3 -2 10.20 1.20 5 -3 -2 12.80 1.20 5 -3 -2 15.00 1.60 -5 3 2 8.90 1.00 -5 3 2 10.10 1.10 4 -3 -2 22.20 4.80 4 -3 -2 16.80 2.00 4 -3 -2 15.30 1.40 4 -3 -2 15.20 1.90 4 -3 -2 16.60 1.60 4 -3 -2 18.40 1.50 4 -3 -2 16.80 1.50 -4 3 2 16.00 1.50 -4 3 2 17.20 1.50 3 -3 -2 84.29 6.80 3 -3 -2 80.59 4.10 3 -3 -2 87.69 4.00 3 -3 -2 82.09 4.40 2 -3 -2 113.19 6.90 2 -3 -2 109.19 6.20 1 -3 -2 757.22 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4.40 0.90 1 16 -3 10.20 1.30 1 16 -3 11.10 1.40 1 16 -3 8.10 1.10 -1 -16 3 8.90 1.10 0 16 -3 16.40 1.50 0 -16 3 16.20 1.50 0 -16 3 20.30 1.90 1 -16 3 8.80 1.20 3 15 -3 5.30 0.80 -3 -15 3 3.70 0.70 2 15 -3 4.70 1.10 2 15 -3 4.90 1.10 2 15 -3 4.00 0.90 -2 -15 3 2.90 0.90 -2 -15 3 4.60 0.70 1 15 -3 22.00 2.00 1 15 -3 23.30 1.90 1 15 -3 25.90 2.00 -1 -15 3 24.60 2.20 -1 -15 3 19.90 1.90 0 -15 3 7.00 1.20 0 -15 3 4.40 1.10 1 -15 3 27.00 2.20 2 -15 3 4.40 0.90 2 -15 3 3.70 1.50 3 14 -3 11.90 1.30 3 14 -3 11.10 1.30 -3 -14 3 14.30 1.40 -3 -14 3 12.60 1.00 2 14 -3 10.90 1.60 2 14 -3 10.60 1.50 2 14 -3 12.50 1.60 -2 -14 3 12.90 1.20 -2 -14 3 12.70 1.50 1 14 -3 12.30 1.50 -1 -14 3 11.50 1.20 -1 -14 3 9.70 1.60 -1 -14 3 13.20 1.60 0 -14 3 18.00 1.70 0 -14 3 17.90 2.10 1 -14 3 11.80 1.40 1 -14 3 11.90 1.60 2 -14 3 14.90 1.60 3 13 -3 9.00 2.20 3 13 -3 10.20 1.40 -3 -13 3 9.30 1.60 -3 -13 3 8.80 1.20 2 13 -3 29.00 2.20 2 13 -3 30.40 2.50 2 13 -3 27.10 2.40 -2 -13 3 32.30 2.40 -2 -13 3 27.50 2.00 1 13 -3 22.20 2.00 -1 -13 3 21.80 2.40 -1 -13 3 24.40 2.20 -1 -13 3 21.50 1.70 0 13 -3 34.10 5.90 0 -13 3 29.90 2.50 0 -13 3 29.10 2.20 1 -13 3 23.30 2.10 1 -13 3 21.70 2.00 2 -13 3 31.10 2.30 2 -13 3 30.30 2.30 3 -13 3 9.40 1.00 3 -13 3 9.20 1.20 4 12 -3 6.80 1.00 4 12 -3 6.00 0.80 -4 -12 3 5.90 0.80 -4 -12 3 6.50 0.80 3 12 -3 4.30 0.90 3 12 -3 3.90 1.10 3 12 -3 6.10 1.30 3 12 -3 2.90 0.90 -3 -12 3 4.80 1.00 -3 -12 3 4.20 1.00 2 12 -3 -0.20 0.70 2 12 -3 1.30 1.00 2 12 -3 0.50 0.90 2 12 -3 0.00 0.80 -2 -12 3 0.40 0.70 -2 -12 3 -0.10 0.70 1 12 -3 63.09 6.90 -1 -12 3 59.29 3.20 -1 -12 3 57.29 6.50 -1 -12 3 60.89 3.80 -1 -12 3 56.89 3.60 0 12 -3 9.90 3.50 0 -12 3 5.50 0.90 0 -12 3 5.50 2.70 0 -12 3 6.10 1.20 0 -12 3 4.10 1.20 -1 12 -3 56.99 6.10 -1 12 -3 66.99 5.00 1 -12 3 62.69 3.50 1 -12 3 61.59 3.60 2 -12 3 1.10 1.30 2 -12 3 1.10 0.80 3 -12 3 4.80 1.20 3 -12 3 5.70 0.90 4 -12 3 4.60 0.90 4 11 -3 3.20 0.80 4 11 -3 3.00 0.80 4 11 -3 4.30 0.80 -4 -11 3 2.70 0.70 -4 -11 3 3.00 0.80 3 11 -3 3.40 1.00 3 11 -3 4.20 1.10 3 11 -3 2.10 1.00 3 11 -3 5.60 1.10 -3 -11 3 4.40 1.10 -3 -11 3 2.50 0.90 2 11 -3 20.60 2.00 2 11 -3 24.30 2.10 2 11 -3 34.20 6.20 2 11 -3 25.50 2.30 2 11 -3 23.20 2.30 -2 -11 3 25.10 2.00 -2 -11 3 23.60 2.20 -2 -11 3 22.00 5.10 1 11 -3 13.40 4.10 -1 -11 3 11.00 2.10 -1 -11 3 12.10 1.70 -1 -11 3 9.30 3.00 0 11 -3 113.59 8.50 0 11 -3 99.89 6.40 0 -11 3 109.69 5.50 0 -11 3 117.09 5.20 0 -11 3 109.69 8.30 0 -11 3 112.79 5.50 -1 11 -3 13.60 3.10 -1 11 -3 13.10 2.70 1 -11 3 12.30 1.60 -2 11 -3 31.20 4.10 -2 11 -3 29.20 4.30 2 -11 3 21.50 1.90 2 -11 3 21.00 2.20 3 -11 3 5.40 1.00 3 -11 3 3.30 1.20 4 -11 3 2.20 0.80 4 10 -3 19.90 1.90 4 10 -3 22.20 1.70 4 10 -3 22.10 1.90 4 10 -3 22.60 1.70 -4 -10 3 21.80 1.80 -4 -10 3 20.40 2.10 3 10 -3 12.60 1.40 3 10 -3 13.20 1.80 3 10 -3 9.20 1.40 3 10 -3 12.30 1.80 3 10 -3 12.10 1.70 -3 -10 3 10.30 1.60 -3 -10 3 12.70 1.50 2 10 -3 14.30 4.10 2 10 -3 7.00 1.40 2 10 -3 8.10 1.40 -2 -10 3 7.50 3.00 -2 -10 3 7.60 1.20 -2 -10 3 4.70 1.30 1 10 -3 8.30 3.10 -1 -10 3 9.30 2.90 -1 -10 3 10.90 1.30 -1 -10 3 10.40 1.60 -1 -10 3 10.30 1.50 0 10 -3 39.60 3.40 0 10 -3 47.70 4.80 0 -10 3 44.40 4.70 0 -10 3 37.70 2.60 0 -10 3 40.70 2.60 -1 10 -3 14.40 2.50 -1 10 -3 9.80 2.80 1 -10 3 8.10 1.20 1 -10 3 9.00 1.30 -2 10 -3 9.50 2.60 -2 10 -3 8.10 2.50 2 -10 3 5.50 1.10 2 -10 3 8.50 1.20 3 -10 3 13.40 1.90 3 -10 3 15.20 1.60 4 -10 3 24.30 2.20 4 -10 3 22.20 1.60 4 9 -3 11.30 1.20 4 9 -3 10.90 1.20 4 9 -3 12.40 1.60 4 9 -3 10.30 1.60 4 9 -3 11.00 1.30 4 9 -3 12.60 1.50 -4 -9 3 13.30 1.50 -4 -9 3 12.30 1.40 3 9 -3 32.90 2.60 3 9 -3 31.30 6.20 3 9 -3 31.80 2.20 3 9 -3 31.90 2.60 3 9 -3 34.00 2.30 3 9 -3 29.00 2.70 3 9 -3 31.60 2.40 3 9 -3 31.60 2.20 -3 -9 3 29.00 2.40 -3 -9 3 32.20 7.40 -3 -9 3 34.90 2.40 2 9 -3 25.30 4.90 2 9 -3 30.00 5.60 2 9 -3 22.20 2.10 2 9 -3 20.60 1.90 2 9 -3 22.10 2.10 -2 -9 3 20.40 2.10 -2 -9 3 18.50 4.20 -2 -9 3 17.40 1.80 1 9 -3 24.90 2.70 1 9 -3 26.70 4.50 -1 -9 3 27.50 3.00 -1 -9 3 26.60 4.70 -1 -9 3 25.40 3.20 0 9 -3 69.49 4.40 0 9 -3 68.49 5.60 0 -9 3 63.49 5.60 0 -9 3 68.49 5.70 -1 9 -3 27.90 3.00 -1 9 -3 28.50 3.40 1 -9 3 31.20 5.30 1 -9 3 29.90 2.70 -2 9 -3 24.80 3.70 -2 9 -3 22.50 3.50 2 -9 3 21.90 1.80 2 -9 3 19.90 1.70 2 -9 3 21.40 2.20 -3 9 -3 38.70 5.80 -3 9 -3 33.40 5.40 3 -9 3 36.30 2.90 3 -9 3 33.00 2.30 3 -9 3 31.90 2.10 4 -9 3 12.60 1.60 4 -9 3 13.70 1.40 5 8 -3 11.20 1.10 5 8 -3 10.00 1.30 5 8 -3 10.90 1.10 5 8 -3 9.80 1.30 -5 -8 3 10.30 1.00 4 8 -3 24.10 1.90 4 8 -3 20.90 1.70 4 8 -3 24.80 2.30 4 8 -3 23.00 2.10 4 8 -3 24.90 1.80 4 8 -3 22.20 2.00 4 8 -3 22.10 1.80 -4 -8 3 20.80 1.90 -4 -8 3 21.30 1.80 3 8 -3 6.20 1.30 3 8 -3 5.80 1.10 3 8 -3 7.60 1.40 3 8 -3 6.80 1.40 3 8 -3 5.40 1.10 3 8 -3 5.10 2.70 3 8 -3 6.40 1.10 3 8 -3 7.10 1.10 -3 -8 3 5.50 1.20 -3 -8 3 7.90 3.00 -3 -8 3 9.40 1.50 2 8 -3 30.70 2.40 2 8 -3 30.80 1.90 2 8 -3 30.90 2.20 2 8 -3 34.60 5.80 2 8 -3 29.40 5.10 -2 -8 3 28.80 5.00 -2 -8 3 26.90 2.20 -2 -8 3 28.40 2.10 1 8 -3 48.40 3.70 1 8 -3 53.39 6.00 -1 -8 3 51.99 7.60 0 8 -3 13.70 2.70 0 8 -3 17.80 2.40 0 -8 3 13.60 2.80 0 -8 3 17.30 3.30 -1 8 -3 57.49 4.50 -1 8 -3 51.89 3.90 1 -8 3 58.19 5.40 -2 8 -3 35.10 3.70 2 -8 3 28.40 2.50 2 -8 3 33.00 2.00 2 -8 3 32.10 2.00 -3 8 -3 7.30 2.50 3 -8 3 7.20 2.20 3 -8 3 9.60 1.10 3 -8 3 8.00 1.50 3 -8 3 7.30 1.10 4 -8 3 27.70 1.90 4 -8 3 27.20 2.40 5 -8 3 11.50 1.00 5 -8 3 12.80 1.50 5 7 -3 1.30 0.70 5 7 -3 0.50 0.50 5 7 -3 1.20 0.50 5 7 -3 1.20 0.70 5 7 -3 2.40 0.70 -5 -7 3 1.20 0.60 4 7 -3 8.70 1.20 4 7 -3 9.40 1.40 4 7 -3 9.70 1.50 4 7 -3 11.40 1.80 4 7 -3 7.70 1.10 4 7 -3 7.70 1.40 4 7 -3 8.20 1.20 -4 -7 3 11.10 1.50 -4 -7 3 10.90 1.40 3 7 -3 24.40 1.90 3 7 -3 25.00 2.20 3 7 -3 25.20 2.00 3 7 -3 25.00 2.30 3 7 -3 24.00 2.50 3 7 -3 22.90 1.90 3 7 -3 19.40 4.60 -3 -7 3 21.60 1.90 -3 -7 3 20.30 4.30 -3 -7 3 21.00 2.00 2 7 -3 38.90 5.90 2 7 -3 39.80 2.30 2 7 -3 40.20 5.90 2 7 -3 38.00 3.40 -2 -7 3 37.80 5.50 -2 -7 3 35.40 2.50 1 7 -3 54.49 4.60 1 7 -3 66.99 5.70 -1 -7 3 64.99 5.40 0 7 -3 392.66 17.00 0 7 -3 374.46 15.90 0 -7 3 337.37 17.20 0 -7 3 376.26 17.50 -1 7 -3 71.49 4.50 -1 7 -3 68.89 4.60 1 -7 3 57.99 5.30 -2 7 -3 42.90 4.00 2 -7 3 40.40 2.80 2 -7 3 39.90 2.20 -3 7 -3 21.50 1.50 -3 7 -3 27.90 4.30 3 -7 3 28.00 3.90 3 -7 3 27.50 1.70 3 -7 3 27.90 1.90 3 -7 3 26.20 1.70 4 -7 3 10.70 1.20 4 -7 3 8.00 1.50 4 -7 3 8.00 1.00 5 -7 3 1.50 0.70 5 -7 3 1.40 0.60 5 6 -3 11.00 1.20 5 6 -3 10.70 1.20 5 6 -3 10.70 1.00 5 6 -3 10.60 1.20 5 6 -3 11.40 1.30 -5 -6 3 10.50 1.10 4 6 -3 19.90 1.90 4 6 -3 19.00 1.70 4 6 -3 19.20 2.20 4 6 -3 17.00 1.80 4 6 -3 20.80 2.20 4 6 -3 16.00 1.90 4 6 -3 16.60 2.10 -4 -6 3 15.80 1.80 3 6 -3 113.99 9.60 3 6 -3 119.59 5.70 3 6 -3 118.29 5.70 3 6 -3 115.29 5.80 3 6 -3 114.19 5.60 3 6 -3 113.59 6.00 3 6 -3 118.39 5.40 3 6 -3 117.69 6.00 -3 -6 3 127.09 5.80 -3 -6 3 127.59 9.10 -3 -6 3 129.49 5.90 2 6 -3 23.20 4.50 2 6 -3 29.10 3.10 1 6 -3 1053.39 45.30 1 6 -3 1044.70 43.90 -1 -6 3 1136.99 45.60 0 6 -3 67.39 3.90 0 6 -3 73.69 4.60 0 -6 3 66.69 4.80 0 -6 3 73.49 4.90 -1 6 -3 1238.38 47.70 1 -6 3 1091.39 48.80 -2 6 -3 29.10 3.30 2 -6 3 30.50 3.00 -3 6 -3 124.29 5.40 -3 6 -3 124.79 8.40 3 -6 3 125.49 5.70 3 -6 3 133.29 8.10 3 -6 3 132.79 5.80 3 -6 3 121.69 5.50 3 -6 3 129.29 6.30 3 -6 3 110.59 5.40 4 -6 3 18.70 2.10 4 -6 3 19.20 1.70 4 -6 3 20.00 1.70 5 -6 3 12.80 1.20 5 -6 3 12.30 1.20 5 5 -3 3.80 0.80 5 5 -3 4.60 0.90 5 5 -3 4.00 0.90 5 5 -3 4.30 1.00 5 5 -3 4.00 0.70 -5 -5 3 3.60 0.80 4 5 -3 45.90 7.10 4 5 -3 55.19 3.40 4 5 -3 56.69 3.70 4 5 -3 55.09 3.20 4 5 -3 52.79 3.40 4 5 -3 59.79 3.60 4 5 -3 59.29 3.20 4 5 -3 53.59 3.10 -4 -5 3 57.49 3.40 -4 -5 3 57.99 3.30 3 5 -3 28.90 2.30 3 5 -3 28.60 5.30 3 5 -3 29.00 2.10 3 5 -3 31.80 1.90 3 5 -3 31.10 2.30 3 5 -3 28.60 2.10 3 5 -3 28.50 2.40 3 5 -3 30.90 2.20 -3 -5 3 33.60 2.20 -3 -5 3 32.20 3.30 -3 -5 3 37.10 5.40 2 5 -3 158.48 10.20 2 5 -3 160.58 8.70 -2 -5 3 171.48 9.80 1 5 -3 124.29 7.40 1 5 -3 120.29 6.30 -1 -5 3 121.49 7.20 0 5 -3 3192.28 135.29 -1 5 -3 139.99 7.00 1 -5 3 134.89 7.90 -2 5 -3 177.88 9.80 2 -5 3 197.18 9.70 -3 5 -3 31.30 4.00 3 -5 3 34.70 2.60 3 -5 3 29.80 1.90 3 -5 3 29.60 1.90 3 -5 3 30.60 2.00 3 -5 3 35.80 2.20 3 -5 3 34.00 2.10 3 -5 3 34.70 4.60 -4 5 -3 55.39 3.00 -4 5 -3 61.59 6.10 4 -5 3 65.09 3.20 4 -5 3 64.39 5.80 4 -5 3 58.69 3.70 4 -5 3 66.89 3.50 4 -5 3 64.39 3.30 4 -5 3 62.99 3.40 5 -5 3 4.40 0.80 5 -5 3 4.90 0.70 5 -5 3 4.00 0.90 5 4 -3 3.70 0.90 5 4 -3 3.90 0.80 5 4 -3 3.70 0.90 5 4 -3 3.30 1.00 5 4 -3 2.80 0.80 -5 -4 3 3.10 0.70 4 4 -3 39.90 7.50 4 4 -3 35.20 2.60 4 4 -3 33.20 2.60 4 4 -3 33.00 2.80 4 4 -3 37.90 2.50 4 4 -3 37.50 2.30 4 4 -3 36.60 2.40 4 4 -3 34.10 2.60 -4 -4 3 36.40 2.40 -4 -4 3 33.60 2.50 3 4 -3 121.19 5.80 3 4 -3 111.89 5.30 3 4 -3 114.79 5.50 3 4 -3 115.39 9.30 3 4 -3 111.99 5.80 3 4 -3 108.69 5.00 3 4 -3 116.39 5.40 -3 -4 3 104.29 5.40 -3 -4 3 116.09 8.00 -3 -4 3 105.29 5.30 2 4 -3 35.40 5.40 2 4 -3 28.10 3.10 2 4 -3 36.00 5.20 -2 -4 3 34.00 4.40 1 4 -3 274.27 13.80 1 4 -3 266.67 12.40 -1 -4 3 306.67 13.50 0 4 -3 7.00 1.50 0 4 -3 6.20 1.10 0 -4 3 5.50 1.40 0 -4 3 4.90 1.40 -1 4 -3 306.87 14.80 1 -4 3 331.57 14.00 -2 4 -3 25.10 3.00 2 -4 3 33.30 3.00 -3 4 -3 110.79 7.90 3 -4 3 121.39 5.60 3 -4 3 117.49 5.40 3 -4 3 107.69 7.50 3 -4 3 117.39 5.50 3 -4 3 117.79 5.90 3 -4 3 116.69 5.50 3 -4 3 123.19 5.40 3 -4 3 118.99 5.50 -4 4 -3 40.10 5.00 4 -4 3 41.40 4.70 4 -4 3 39.90 2.60 4 -4 3 37.50 2.70 4 -4 3 41.30 2.60 4 -4 3 42.80 2.40 4 -4 3 39.80 2.60 4 -4 3 39.00 2.40 -5 4 -3 3.00 0.50 5 -4 3 3.60 0.90 5 -4 3 4.80 0.80 5 -4 3 3.20 0.70 5 -4 3 4.20 0.70 5 3 -3 7.40 1.00 5 3 -3 7.40 1.00 5 3 -3 7.80 1.30 5 3 -3 5.80 1.10 5 3 -3 9.70 1.60 -5 -3 3 6.90 1.40 4 3 -3 27.00 2.30 4 3 -3 28.40 6.20 4 3 -3 27.10 2.30 4 3 -3 26.60 2.20 4 3 -3 25.00 2.50 4 3 -3 25.60 2.10 4 3 -3 29.60 2.10 4 3 -3 25.40 1.90 -4 -3 3 27.00 2.10 -4 -3 3 28.00 2.10 3 3 -3 148.89 6.70 3 3 -3 146.19 10.60 3 3 -3 138.39 6.70 3 3 -3 133.49 6.80 3 3 -3 137.99 7.80 3 3 -3 146.39 6.60 3 3 -3 148.99 6.40 -3 -3 3 153.28 9.20 2 3 -3 192.78 11.10 2 3 -3 177.98 9.70 -2 -3 3 203.68 10.20 1 3 -3 73.99 4.20 1 3 -3 67.49 4.80 -1 -3 3 80.19 4.80 0 3 -3 292.17 12.10 0 3 -3 304.27 12.40 0 -3 3 267.17 12.70 -1 3 -3 78.49 4.40 1 -3 3 81.79 4.40 -2 3 -3 185.98 9.90 2 -3 3 210.38 10.10 -3 3 -3 134.29 9.10 3 -3 3 140.99 6.70 3 -3 3 172.08 8.10 3 -3 3 165.78 7.30 3 -3 3 144.09 6.60 3 -3 3 157.28 7.00 3 -3 3 146.29 6.80 3 -3 3 156.88 9.40 -4 3 -3 34.80 5.40 4 -3 3 28.20 1.90 4 -3 3 36.00 5.90 4 -3 3 31.00 2.30 4 -3 3 30.20 2.20 4 -3 3 30.20 2.00 4 -3 3 24.90 1.90 4 -3 3 26.80 2.00 4 -3 3 29.50 2.20 4 -3 3 29.50 2.10 5 -3 3 9.20 1.50 5 -3 3 9.30 1.10 5 -3 3 8.80 1.10 5 -3 3 8.10 0.90 5 -3 3 10.00 1.30 5 2 -3 21.60 1.60 5 2 -3 22.70 2.00 5 2 -3 20.40 1.70 5 2 -3 21.90 1.70 5 2 -3 23.80 1.70 -5 -2 3 18.90 1.60 -5 -2 3 22.50 1.70 4 2 -3 101.99 5.80 4 2 -3 113.09 5.50 4 2 -3 115.09 5.60 4 2 -3 108.69 5.50 4 2 -3 96.69 9.30 4 2 -3 106.79 5.10 4 2 -3 115.99 5.40 4 2 -3 115.59 5.40 -4 -2 3 108.79 5.30 -4 -2 3 107.59 5.30 3 2 -3 50.89 2.90 3 2 -3 52.59 3.00 3 2 -3 53.69 3.10 3 2 -3 50.39 2.60 3 2 -3 54.29 6.00 3 2 -3 51.29 3.30 -3 -2 3 49.70 4.50 2 2 -3 171.78 10.00 2 2 -3 159.58 8.80 -2 -2 3 171.08 8.90 1 2 -3 703.83 30.40 -1 -2 3 752.72 30.30 0 2 -3 93.39 4.40 0 2 -3 86.99 4.20 0 -2 3 86.49 4.70 2 -2 3 173.28 9.10 3 -2 3 50.79 3.00 3 -2 3 53.59 3.10 3 -2 3 53.49 3.10 3 -2 3 56.29 3.10 3 -2 3 55.29 2.90 3 -2 3 52.39 4.90 3 -2 3 55.39 3.00 3 -2 3 51.79 2.80 3 -2 3 51.79 3.20 -4 2 -3 100.99 8.20 4 -2 3 111.99 5.30 4 -2 3 109.59 5.40 4 -2 3 114.99 5.60 4 -2 3 111.19 5.50 4 -2 3 112.49 5.40 4 -2 3 122.89 5.50 4 -2 3 117.49 8.60 4 -2 3 111.19 5.60 4 -2 3 119.29 5.60 4 -2 3 114.89 5.60 4 -2 3 108.69 5.30 5 -2 3 24.20 1.60 5 -2 3 25.20 1.60 5 -2 3 20.90 1.70 5 -2 3 25.00 2.40 5 -2 3 25.50 1.80 5 -2 3 23.90 1.80 5 1 -3 50.69 2.70 5 1 -3 51.39 2.90 5 1 -3 50.09 2.80 5 1 -3 50.69 2.70 5 1 -3 53.79 3.20 -5 -1 3 49.10 2.80 -5 -1 3 52.79 2.70 4 1 -3 22.40 1.90 4 1 -3 22.90 2.50 4 1 -3 21.10 1.70 4 1 -3 23.30 4.90 4 1 -3 22.20 2.00 4 1 -3 24.80 1.90 4 1 -3 19.00 1.80 4 1 -3 20.50 1.90 -4 -1 3 20.10 1.80 -4 -1 3 21.00 1.80 3 1 -3 37.50 2.80 3 1 -3 43.20 2.50 3 1 -3 46.70 6.30 3 1 -3 42.60 2.90 -3 -1 3 43.10 3.80 2 1 -3 308.57 15.20 2 1 -3 303.37 14.10 -2 -1 3 280.67 13.60 1 1 -3 284.57 13.40 1 1 -3 297.37 12.90 -1 -1 3 307.27 13.10 0 1 -3 213.88 8.80 0 1 -3 209.78 8.90 0 -1 3 201.58 9.30 -1 1 -3 261.47 12.10 1 -1 3 309.77 12.50 2 -1 3 286.17 13.60 3 -1 3 44.90 2.50 3 -1 3 45.50 2.70 3 -1 3 44.00 2.60 3 -1 3 46.00 4.60 3 -1 3 44.60 2.70 3 -1 3 44.00 2.70 3 -1 3 41.60 2.70 -4 1 -3 23.80 4.60 4 -1 3 23.20 1.80 4 -1 3 19.80 1.50 4 -1 3 22.10 1.80 4 -1 3 23.10 2.00 4 -1 3 21.90 2.00 4 -1 3 19.90 1.90 4 -1 3 20.70 1.90 4 -1 3 23.80 4.70 4 -1 3 22.90 1.90 4 -1 3 20.60 2.00 4 -1 3 22.10 2.00 4 -1 3 25.20 1.90 5 -1 3 55.19 3.10 5 -1 3 56.69 3.10 5 -1 3 57.99 3.10 5 -1 3 55.89 2.90 5 -1 3 54.19 2.90 5 -1 3 54.09 3.00 5 0 -3 5.10 0.90 5 0 -3 6.90 1.30 5 0 -3 5.70 0.90 5 0 -3 3.90 0.80 5 0 -3 2.80 0.80 -5 0 3 4.30 0.80 -5 0 3 5.90 0.90 4 0 -3 64.49 4.10 4 0 -3 60.79 6.90 4 0 -3 67.79 3.70 4 0 -3 64.09 3.70 4 0 -3 70.49 3.60 4 0 -3 65.29 3.30 4 0 -3 68.39 3.70 4 0 -3 71.29 3.60 -4 0 3 71.59 3.60 -4 0 3 63.09 3.60 3 0 -3 90.79 7.60 3 0 -3 89.69 4.80 3 0 -3 94.49 4.40 3 0 -3 86.09 4.80 2 0 -3 97.39 6.20 2 0 -3 97.19 6.70 -2 0 3 99.69 5.50 -1 0 3 856.31 34.80 0 0 -3 28.50 1.90 0 0 -3 31.20 1.80 0 0 3 37.00 2.60 2 0 3 101.99 6.30 3 0 3 93.89 4.80 3 0 3 99.29 5.20 3 0 3 96.79 4.90 3 0 3 99.29 4.70 3 0 3 95.89 4.80 3 0 3 94.89 4.60 3 0 3 103.79 7.40 3 0 3 94.19 4.80 4 0 3 76.99 6.90 4 0 3 71.19 3.90 4 0 3 68.89 3.70 4 0 3 67.29 3.90 4 0 3 77.49 4.10 4 0 3 65.89 3.80 4 0 3 69.59 3.70 4 0 3 66.69 3.90 4 0 3 68.29 3.80 4 0 3 71.89 4.00 4 0 3 73.29 3.80 4 0 3 64.79 3.40 5 0 3 4.80 1.00 5 0 3 3.70 0.90 5 0 3 5.50 0.90 5 0 3 4.20 0.90 5 0 3 4.60 0.80 5 0 3 5.60 1.00 5 0 3 5.40 0.90 5 -1 -3 55.29 2.90 5 -1 -3 51.79 2.80 5 -1 -3 54.19 3.20 -5 1 3 55.19 2.80 -5 1 3 51.99 2.80 4 -1 -3 20.50 1.90 4 -1 -3 20.80 2.10 4 -1 -3 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109.79 5.30 4 -2 -3 104.59 5.20 4 -2 -3 108.69 5.60 4 -2 -3 114.99 5.20 4 -2 -3 114.49 5.30 4 -2 -3 102.49 8.90 -4 2 3 112.29 5.20 -4 2 3 109.89 5.30 3 -2 -3 55.69 5.60 3 -2 -3 50.69 2.80 3 -2 -3 54.09 3.30 3 -2 -3 49.90 2.70 2 -2 -3 178.38 8.30 2 -2 -3 162.18 9.50 1 -2 -3 699.23 29.70 1 -2 -3 752.42 29.50 1 -2 -3 709.53 29.80 0 -2 -3 76.69 3.90 0 -2 -3 89.59 4.40 -1 -2 -3 731.03 29.30 1 2 3 705.63 29.30 2 2 3 169.78 9.20 -3 -2 -3 57.59 4.70 3 2 3 52.29 3.20 3 2 3 49.60 5.00 3 2 3 53.89 3.10 3 2 3 57.29 3.20 3 2 3 54.39 3.20 3 2 3 52.99 3.20 3 2 3 50.89 3.10 3 2 3 52.59 2.90 3 2 3 52.79 3.20 3 2 3 54.19 3.00 3 2 3 51.29 3.10 4 2 3 112.79 5.80 4 2 3 112.09 5.30 4 2 3 112.29 5.50 4 2 3 107.69 5.60 4 2 3 111.39 8.80 4 2 3 119.09 5.70 4 2 3 115.09 5.70 4 2 3 113.79 5.60 4 2 3 108.99 5.60 4 2 3 119.19 5.80 4 2 3 113.99 5.70 5 2 3 23.60 1.70 5 2 3 23.80 1.70 5 2 3 26.50 1.80 5 2 3 21.60 1.90 5 2 3 24.10 1.90 5 2 3 21.80 1.80 5 2 3 23.40 1.80 5 -3 -3 10.10 1.30 5 -3 -3 10.40 1.00 5 -3 -3 9.20 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3.20 0.90 3 -11 -3 2.80 1.30 2 -11 -3 26.80 2.00 2 -11 -3 22.90 2.00 2 -11 -3 24.10 4.80 -2 11 3 21.80 3.60 1 -11 -3 11.30 1.50 1 -11 -3 12.20 2.00 1 -11 -3 12.90 1.40 1 -11 -3 18.10 4.30 -1 11 3 14.10 2.90 0 -11 -3 106.79 8.50 0 -11 -3 118.79 8.70 0 -11 -3 118.49 5.50 0 -11 -3 116.19 5.70 0 -11 -3 114.69 5.60 -1 -11 -3 10.20 2.90 -1 -11 -3 9.50 1.50 -1 -11 -3 6.10 2.60 1 11 3 11.70 1.50 1 11 3 9.80 1.50 1 11 3 5.60 1.70 1 11 3 10.40 1.40 -2 -11 -3 22.00 2.20 -2 -11 -3 20.30 1.90 -2 -11 -3 21.60 4.90 2 11 3 20.70 2.00 2 11 3 25.30 2.60 2 11 3 20.70 2.10 2 11 3 23.00 1.80 2 11 3 23.50 2.30 2 11 3 20.50 2.30 2 11 3 22.00 2.10 -3 -11 -3 4.00 1.10 -3 -11 -3 2.10 0.90 3 11 3 2.90 1.00 3 11 3 2.20 0.90 3 11 3 3.60 1.10 3 11 3 3.50 1.10 3 11 3 3.40 0.80 3 11 3 3.40 1.00 3 11 3 2.40 0.90 -4 -11 -3 2.70 0.70 4 11 3 2.80 0.80 4 11 3 4.00 0.80 4 11 3 4.20 0.90 4 11 3 3.00 0.80 4 11 3 4.40 0.90 4 -12 -3 8.10 1.10 3 -12 -3 2.60 1.10 3 -12 -3 6.70 1.10 2 -12 -3 0.90 0.80 1 -12 -3 48.40 7.30 1 -12 -3 66.99 3.50 1 -12 -3 51.69 3.20 1 -12 -3 53.89 2.90 0 -12 -3 3.40 0.90 0 -12 -3 3.20 1.00 0 -12 -3 6.20 2.70 0 -12 -3 3.00 1.10 0 -12 -3 4.60 2.50 0 12 3 6.70 1.20 -1 -12 -3 64.09 3.80 -1 -12 -3 71.99 3.70 -1 -12 -3 68.49 7.20 -1 -12 -3 58.19 6.10 1 12 3 61.19 3.60 1 12 3 66.69 3.70 1 12 3 60.29 3.60 1 12 3 63.79 3.80 -2 -12 -3 2.60 0.90 -2 -12 -3 1.10 0.90 2 12 3 -1.20 0.70 2 12 3 1.00 0.90 2 12 3 0.60 0.90 2 12 3 0.20 1.10 2 12 3 2.00 1.10 -3 -12 -3 4.30 1.30 -3 -12 -3 3.80 1.00 3 12 3 4.60 1.00 3 12 3 5.30 1.20 3 12 3 3.90 1.00 3 12 3 5.00 1.20 3 12 3 4.90 1.10 3 12 3 4.10 0.80 -4 -12 -3 6.60 0.80 4 12 3 5.90 1.00 4 12 3 5.50 0.80 4 12 3 6.30 1.00 4 12 3 4.90 0.80 4 12 3 6.30 0.90 3 -13 -3 9.40 1.40 3 -13 -3 6.20 1.50 2 -13 -3 26.40 2.50 2 -13 -3 32.90 2.10 2 -13 -3 30.70 2.30 1 -13 -3 25.80 2.20 1 -13 -3 25.50 2.00 0 -13 -3 30.00 2.00 0 -13 -3 31.40 2.50 0 -13 -3 30.00 2.40 0 -13 -3 25.80 5.60 0 -13 -3 29.70 5.40 0 13 3 28.80 2.20 -1 -13 -3 20.20 2.10 -1 -13 -3 21.70 1.90 1 13 3 23.90 2.20 1 13 3 23.90 2.00 1 13 3 24.60 2.10 1 13 3 21.90 2.10 -2 -13 -3 28.40 2.30 -2 -13 -3 27.30 2.10 2 13 3 30.70 2.30 2 13 3 26.70 2.30 2 13 3 27.30 2.50 2 13 3 28.40 2.20 2 13 3 29.90 2.30 -3 -13 -3 9.10 1.20 -3 -13 -3 11.80 1.40 3 13 3 8.00 1.80 3 13 3 12.10 1.50 3 13 3 10.80 1.30 3 13 3 7.70 1.20 3 -14 -3 17.40 1.40 2 -14 -3 13.30 1.50 2 -14 -3 13.00 1.60 1 -14 -3 11.90 1.50 1 -14 -3 14.30 1.70 0 -14 -3 17.90 2.00 0 -14 -3 17.40 1.60 0 -14 -3 18.30 1.90 0 14 3 15.80 1.60 0 14 3 16.30 1.60 -1 -14 -3 13.30 1.50 -1 -14 -3 12.40 1.60 1 14 3 14.30 1.60 1 14 3 12.80 1.60 1 14 3 10.10 1.40 1 14 3 11.20 1.40 -2 -14 -3 12.20 1.40 -2 -14 -3 12.20 1.50 2 14 3 10.90 1.60 2 14 3 12.50 1.60 2 14 3 15.20 1.80 2 14 3 13.80 1.80 -3 -14 -3 14.00 1.30 -3 -14 -3 12.70 1.30 3 14 3 12.60 1.40 3 14 3 13.30 1.30 3 14 3 15.90 1.40 3 14 3 16.00 1.30 3 -15 -3 5.80 0.70 2 -15 -3 4.90 1.00 -2 15 3 2.40 0.70 1 -15 -3 22.70 1.90 1 -15 -3 21.90 1.90 -1 15 3 23.80 1.70 -1 15 3 25.30 1.80 0 -15 -3 4.80 1.20 0 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4 4.30 0.80 1 16 -4 9.00 1.00 1 16 -4 11.30 1.30 1 16 -4 13.20 1.50 -1 -16 4 12.90 2.10 -1 -16 4 10.70 1.10 0 16 -4 7.90 1.00 0 -16 4 5.70 1.10 0 -16 4 8.40 1.30 1 -16 4 12.90 1.50 2 -16 4 4.40 0.70 2 15 -4 0.50 0.70 2 15 -4 3.20 0.90 2 15 -4 0.70 0.80 -2 -15 4 2.10 0.80 1 15 -4 5.70 1.40 1 15 -4 4.10 1.00 1 15 -4 3.00 0.90 -1 -15 4 3.00 0.90 -1 -15 4 4.80 1.20 0 -15 4 18.60 1.60 0 -15 4 17.40 2.00 1 -15 4 3.50 1.00 2 -15 4 3.10 0.80 2 -15 4 2.50 1.10 3 14 -4 2.60 0.70 3 14 -4 2.50 0.80 -3 -14 4 4.00 0.80 -3 -14 4 2.40 0.70 2 14 -4 3.90 1.10 2 14 -4 4.90 1.00 2 14 -4 4.10 1.20 -2 -14 4 5.10 1.40 -2 -14 4 5.40 1.10 1 14 -4 17.70 1.70 1 14 -4 13.60 1.80 -1 -14 4 15.20 1.70 -1 -14 4 12.90 1.20 -1 -14 4 13.90 1.80 0 -14 4 25.00 2.00 0 -14 4 22.00 2.20 1 -14 4 14.10 1.70 2 -14 4 4.90 1.00 2 -14 4 4.30 1.20 3 13 -4 9.70 1.40 3 13 -4 9.50 1.20 -3 -13 4 8.50 1.00 -3 -13 4 10.80 1.40 2 13 -4 37.00 2.80 2 13 -4 37.80 2.50 2 13 -4 43.60 2.90 -2 -13 4 39.70 2.30 -2 -13 4 39.70 2.70 -1 -13 4 15.50 1.90 0 13 -4 65.79 7.10 0 -13 4 59.39 3.50 0 -13 4 63.39 3.80 1 -13 4 14.30 1.80 1 -13 4 16.00 1.60 2 -13 4 47.80 2.90 2 -13 4 46.10 2.90 3 -13 4 8.20 1.10 4 12 -4 1.10 0.70 -4 -12 4 1.80 0.60 3 12 -4 18.50 2.00 3 12 -4 20.60 1.90 3 12 -4 18.10 1.60 -3 -12 4 16.90 1.80 -3 -12 4 16.40 1.50 2 12 -4 29.50 3.50 2 12 -4 18.20 2.20 2 12 -4 23.50 2.00 2 12 -4 21.30 1.90 -2 -12 4 22.50 2.00 -2 -12 4 22.50 2.50 1 12 -4 34.30 6.20 1 12 -4 26.90 2.10 -1 -12 4 30.30 2.40 -1 -12 4 27.60 1.90 -1 -12 4 23.20 2.40 -1 -12 4 26.00 5.40 0 12 -4 49.30 6.20 0 -12 4 56.49 7.60 0 -12 4 49.50 3.30 0 -12 4 53.89 3.10 -1 12 -4 31.00 5.40 -1 12 -4 27.70 3.60 1 -12 4 24.70 2.20 1 -12 4 24.20 2.00 2 -12 4 21.90 2.10 2 -12 4 27.00 2.40 3 -12 4 21.60 1.70 3 -12 4 19.80 1.90 4 -12 4 2.00 0.70 4 11 -4 28.00 1.80 4 11 -4 29.20 2.00 4 11 -4 27.90 1.90 -4 -11 4 30.10 1.80 -4 -11 4 27.90 1.90 3 11 -4 30.90 2.40 3 11 -4 27.30 2.10 3 11 -4 30.70 2.10 3 11 -4 24.90 2.10 3 11 -4 29.50 2.50 -3 -11 4 28.90 2.10 -3 -11 4 28.20 2.30 2 11 -4 33.70 2.50 2 11 -4 32.30 2.40 2 11 -4 37.30 2.80 2 11 -4 44.40 7.50 2 11 -4 35.20 2.70 -2 -11 4 35.20 6.50 -2 -11 4 32.50 2.30 -2 -11 4 36.00 2.60 1 11 -4 34.60 6.00 -1 -11 4 24.90 1.90 -1 -11 4 26.90 5.00 -1 -11 4 24.50 2.20 -1 -11 4 29.70 2.80 0 11 -4 136.59 10.70 0 11 -4 142.69 8.10 0 -11 4 136.59 6.10 0 -11 4 138.19 9.70 0 -11 4 138.59 6.70 0 -11 4 142.49 6.60 -1 11 -4 30.80 3.40 -1 11 -4 30.90 4.70 1 -11 4 31.30 2.30 1 -11 4 31.70 2.30 -2 11 -4 38.00 5.50 -2 11 -4 34.70 4.80 2 -11 4 36.00 2.70 2 -11 4 35.80 2.50 3 -11 4 31.50 2.00 3 -11 4 31.10 2.50 4 -11 4 29.50 2.00 4 10 -4 41.70 2.40 4 10 -4 40.70 2.40 4 10 -4 38.00 2.40 4 10 -4 38.40 2.60 -4 -10 4 36.80 2.40 -4 -10 4 42.30 2.90 3 10 -4 57.89 3.50 3 10 -4 52.59 3.40 3 10 -4 50.89 3.00 3 10 -4 50.49 3.30 2 10 -4 32.20 3.60 2 10 -4 41.00 6.80 2 10 -4 36.50 2.70 2 10 -4 39.20 2.90 2 10 -4 53.79 6.60 -2 -10 4 41.30 6.40 -2 -10 4 39.10 2.80 -2 -10 4 40.30 2.60 1 10 -4 54.19 4.40 1 10 -4 59.59 6.10 -1 -10 4 55.99 3.40 -1 -10 4 50.39 3.30 -1 -10 4 52.79 3.10 -1 -10 4 60.39 5.90 0 10 -4 11.10 2.20 0 10 -4 9.40 3.10 0 -10 4 4.50 1.10 0 -10 4 5.40 1.10 0 -10 4 8.30 2.70 -1 10 -4 61.79 4.70 -1 10 -4 69.79 5.80 1 -10 4 62.39 3.50 1 -10 4 61.79 3.50 -2 10 -4 44.10 4.30 -2 10 -4 45.00 4.90 2 -10 4 44.60 3.00 2 -10 4 41.60 3.00 2 -10 4 41.60 2.60 3 -10 4 43.80 4.40 3 -10 4 62.79 3.10 3 -10 4 53.19 3.00 3 -10 4 47.90 3.40 4 -10 4 47.40 2.80 4 -10 4 38.60 2.30 4 9 -4 1.80 1.00 4 9 -4 1.20 0.80 4 9 -4 1.40 0.60 -4 -9 4 1.80 0.70 -4 -9 4 2.40 0.80 3 9 -4 29.90 2.50 3 9 -4 28.50 2.20 3 9 -4 29.00 2.50 3 9 -4 36.00 2.80 3 9 -4 24.00 5.50 3 9 -4 31.10 2.20 3 9 -4 27.80 2.00 -3 -9 4 29.70 5.70 -3 -9 4 33.10 2.30 -3 -9 4 32.40 2.50 2 9 -4 14.10 3.90 2 9 -4 13.20 1.70 2 9 -4 11.40 1.50 2 9 -4 13.60 3.70 -2 -9 4 12.10 1.50 -2 -9 4 11.70 1.60 1 9 -4 67.29 6.30 1 9 -4 54.89 4.40 -1 -9 4 60.79 3.50 -1 -9 4 64.59 6.00 -1 -9 4 55.99 3.60 -1 -9 4 66.79 3.30 0 9 -4 89.99 6.70 0 -9 4 96.19 8.40 0 -9 4 84.69 4.40 0 -9 4 88.79 4.50 -1 9 -4 63.79 4.40 -1 9 -4 66.59 5.20 1 -9 4 50.99 3.10 -2 9 -4 14.20 3.00 2 -9 4 14.40 1.50 2 -9 4 13.10 1.70 2 -9 4 11.60 1.30 -3 9 -4 37.70 4.50 -3 9 -4 34.30 4.90 3 -9 4 36.20 2.80 3 -9 4 34.70 2.30 3 -9 4 29.70 2.70 3 -9 4 31.40 2.10 4 -9 4 1.00 0.90 4 -9 4 3.30 0.90 5 8 -4 1.50 0.60 5 8 -4 2.80 0.60 5 8 -4 3.30 0.70 -5 -8 4 2.10 0.50 4 8 -4 8.80 1.10 4 8 -4 8.30 1.30 4 8 -4 10.60 1.60 4 8 -4 10.40 1.50 4 8 -4 10.60 1.60 -4 -8 4 9.40 1.40 -4 -8 4 12.30 1.50 3 8 -4 21.70 1.80 3 8 -4 23.20 1.80 3 8 -4 25.20 2.40 3 8 -4 23.40 2.20 3 8 -4 19.40 4.80 3 8 -4 22.60 2.00 3 8 -4 24.40 2.00 -3 -8 4 24.60 5.00 -3 -8 4 20.70 2.10 -3 -8 4 23.80 2.00 2 8 -4 16.30 1.60 2 8 -4 16.80 4.30 2 8 -4 25.40 5.30 2 8 -4 15.20 1.70 -2 -8 4 16.80 1.70 -2 -8 4 12.90 3.30 -2 -8 4 17.10 1.90 1 8 -4 127.29 7.50 1 8 -4 138.09 9.30 -1 -8 4 147.89 9.30 0 8 -4 31.30 2.80 0 8 -4 31.30 3.90 0 -8 4 34.50 3.90 -1 8 -4 150.48 8.00 -1 8 -4 164.28 8.70 1 -8 4 140.49 8.30 -2 8 -4 23.40 3.50 -2 8 -4 19.50 3.10 2 -8 4 20.20 1.70 2 -8 4 20.30 1.60 2 -8 4 20.40 2.10 -3 8 -4 36.00 5.10 -3 8 -4 20.10 3.60 3 -8 4 27.50 2.50 3 -8 4 32.70 2.10 3 -8 4 24.00 2.50 3 -8 4 28.80 1.80 4 -8 4 14.10 1.50 4 -8 4 10.60 1.60 5 -8 4 2.50 0.70 5 -8 4 3.40 0.70 5 7 -4 6.70 0.90 5 7 -4 6.60 0.90 5 7 -4 6.30 0.80 -5 -7 4 5.30 0.80 -5 -7 4 6.00 0.90 4 7 -4 21.00 2.30 4 7 -4 23.20 2.10 4 7 -4 22.40 1.70 4 7 -4 23.10 1.80 4 7 -4 22.00 2.00 4 7 -4 20.80 2.00 -4 -7 4 25.90 2.00 -4 -7 4 22.30 2.00 3 7 -4 28.30 2.80 3 7 -4 37.00 2.80 3 7 -4 27.90 2.10 3 7 -4 37.30 3.30 3 7 -4 32.10 2.40 3 7 -4 28.40 2.30 3 7 -4 30.40 5.80 -3 -7 4 30.40 2.40 -3 -7 4 32.90 5.50 2 7 -4 100.79 6.50 2 7 -4 103.39 8.60 -2 -7 4 97.99 7.70 -2 -7 4 103.69 5.00 -2 -7 4 97.19 4.80 1 7 -4 58.19 4.40 1 7 -4 58.29 5.50 -1 -7 4 66.79 5.50 0 7 -4 52.49 4.40 0 7 -4 55.69 3.60 0 -7 4 59.39 4.70 -1 7 -4 67.09 4.40 -1 7 -4 69.39 4.70 1 -7 4 52.39 5.90 -2 7 -4 119.29 7.20 2 -7 4 108.99 5.10 2 -7 4 104.29 5.50 2 -7 4 117.29 5.10 -3 7 -4 40.60 4.40 3 -7 4 35.20 2.90 3 -7 4 38.90 2.30 3 -7 4 36.50 2.10 3 -7 4 32.80 2.10 3 -7 4 33.50 2.80 3 -7 4 40.00 2.40 4 -7 4 24.70 1.90 4 -7 4 28.00 2.30 4 -7 4 23.10 1.60 5 -7 4 7.70 1.00 5 -7 4 8.10 1.00 5 6 -4 7.60 1.00 5 6 -4 6.60 1.00 5 6 -4 6.00 0.70 5 6 -4 8.00 0.90 -5 -6 4 7.30 0.90 -5 -6 4 7.50 0.90 4 6 -4 8.40 1.90 4 6 -4 6.50 1.10 4 6 -4 6.60 1.30 -4 -6 4 5.90 1.20 -4 -6 4 6.40 1.90 3 6 -4 63.39 3.50 3 6 -4 56.39 6.80 3 6 -4 61.79 3.90 3 6 -4 64.99 3.80 3 6 -4 59.09 3.70 3 6 -4 64.19 3.50 -3 -6 4 64.89 6.30 -3 -6 4 69.69 3.60 -3 -6 4 70.29 3.80 2 6 -4 101.59 8.20 2 6 -4 105.49 6.70 -2 -6 4 97.19 7.30 1 6 -4 477.55 22.20 1 6 -4 463.05 20.90 -1 -6 4 507.05 22.30 0 6 -4 276.97 12.40 0 6 -4 257.57 11.50 0 -6 4 240.98 12.60 -1 6 -4 533.55 22.30 -1 6 -4 545.45 22.50 1 -6 4 480.85 22.30 -2 6 -4 125.99 7.30 2 -6 4 116.89 7.10 -3 6 -4 82.69 7.40 -3 6 -4 65.49 3.30 3 -6 4 73.19 4.20 3 -6 4 63.59 4.10 3 -6 4 69.49 3.40 3 -6 4 72.39 5.80 3 -6 4 77.19 3.60 3 -6 4 65.69 3.50 4 -6 4 5.10 0.90 4 -6 4 6.40 1.50 4 -6 4 6.80 2.00 5 -6 4 7.90 1.00 5 -6 4 8.80 1.00 5 5 -4 22.80 1.90 5 5 -4 19.70 1.60 5 5 -4 22.60 1.50 5 5 -4 22.10 1.60 5 5 -4 21.00 1.40 -5 -5 4 21.90 2.20 -5 -5 4 21.20 1.50 4 5 -4 10.50 4.00 4 5 -4 16.40 1.60 4 5 -4 15.60 2.20 4 5 -4 14.90 1.80 4 5 -4 16.40 1.60 4 5 -4 18.70 2.10 4 5 -4 18.40 2.10 -4 -5 4 16.70 1.80 -4 -5 4 15.60 1.70 3 5 -4 44.30 2.60 3 5 -4 44.20 2.90 3 5 -4 44.90 4.60 3 5 -4 42.00 2.90 3 5 -4 43.40 2.90 3 5 -4 41.50 7.00 3 5 -4 41.90 2.60 -3 -5 4 42.70 2.70 -3 -5 4 41.00 5.90 -3 -5 4 42.90 2.80 2 5 -4 23.60 4.20 2 5 -4 31.40 3.30 -2 -5 4 25.60 4.00 1 5 -4 503.35 22.20 1 5 -4 513.75 23.40 -1 -5 4 549.15 23.50 0 -5 4 1135.69 49.80 -1 5 -4 553.64 23.60 -1 5 -4 591.04 23.70 1 -5 4 534.45 23.60 -2 5 -4 30.60 3.10 2 -5 4 33.20 3.10 -3 5 -4 51.29 4.90 3 -5 4 49.70 2.80 3 -5 4 47.30 3.20 3 -5 4 46.10 2.50 3 -5 4 49.50 4.50 3 -5 4 48.60 2.70 3 -5 4 48.60 2.70 3 -5 4 43.80 2.50 -4 5 -4 17.20 3.90 4 -5 4 19.90 1.60 4 -5 4 15.90 1.40 4 -5 4 15.30 3.30 4 -5 4 18.20 2.00 4 -5 4 15.10 1.60 4 -5 4 17.60 1.70 5 -5 4 22.00 1.70 5 -5 4 25.20 1.70 5 -5 4 24.50 1.50 5 4 -4 15.90 1.30 5 4 -4 15.30 1.20 5 4 -4 15.20 1.40 5 4 -4 15.40 2.00 5 4 -4 17.10 2.00 -5 -4 4 16.10 1.40 -5 -4 4 12.90 1.30 4 4 -4 35.60 2.60 4 4 -4 35.50 2.40 4 4 -4 29.30 6.40 4 4 -4 38.40 2.70 4 4 -4 38.00 2.70 4 4 -4 37.30 2.40 4 4 -4 35.70 2.90 -4 -4 4 34.80 2.40 -4 -4 4 38.50 2.60 3 4 -4 9.30 1.20 3 4 -4 5.90 2.70 3 4 -4 9.50 1.40 3 4 -4 10.30 1.50 3 4 -4 14.10 3.20 -3 -4 4 13.30 3.30 -3 -4 4 7.00 1.30 2 4 -4 34.00 3.50 2 4 -4 33.10 4.20 -2 -4 4 32.70 3.60 1 4 -4 33.20 3.60 -1 -4 4 41.30 3.50 0 4 -4 517.85 21.20 0 4 -4 500.55 20.70 0 -4 4 484.85 21.60 -1 4 -4 39.50 2.90 1 -4 4 41.20 2.90 -2 4 -4 31.80 3.20 2 -4 4 35.90 3.20 -3 4 -4 10.10 2.60 3 -4 4 9.20 1.50 3 -4 4 9.90 2.30 3 -4 4 6.90 1.00 3 -4 4 8.00 1.20 3 -4 4 7.50 1.00 3 -4 4 7.20 1.40 3 -4 4 7.40 0.90 3 -4 4 9.00 1.20 3 -4 4 9.00 1.30 -4 4 -4 36.30 6.00 4 -4 4 42.10 2.50 4 -4 4 41.70 2.60 4 -4 4 39.20 2.60 4 -4 4 44.10 2.70 4 -4 4 52.69 5.70 4 -4 4 40.20 2.80 4 -4 4 41.10 2.40 5 -4 4 18.10 2.20 5 -4 4 16.60 1.20 5 -4 4 21.10 2.10 5 -4 4 15.40 1.60 5 3 -4 11.20 1.10 5 3 -4 11.90 1.20 5 3 -4 10.00 1.50 5 3 -4 10.40 1.20 5 3 -4 11.00 1.40 -5 -3 4 10.90 1.20 -5 -3 4 9.70 1.40 4 3 -4 35.60 2.30 4 3 -4 30.50 2.80 4 3 -4 33.10 2.20 4 3 -4 32.10 2.50 4 3 -4 33.00 2.50 4 3 -4 32.90 2.40 4 3 -4 26.20 5.30 -4 -3 4 32.90 2.30 -4 -3 4 31.60 2.30 3 3 -4 87.49 4.60 3 3 -4 92.29 6.90 3 3 -4 88.09 4.60 3 3 -4 104.99 8.60 3 3 -4 88.09 4.30 3 3 -4 90.99 4.40 3 3 -4 99.59 4.70 -3 -3 4 80.79 4.30 -3 -3 4 76.39 6.40 -3 -3 4 87.89 4.50 2 3 -4 30.20 4.60 2 3 -4 27.80 3.70 -2 -3 4 28.80 3.80 1 3 -4 177.78 10.10 1 3 -4 178.08 8.40 -1 -3 4 161.58 9.00 0 3 -4 1543.55 69.09 -1 3 -4 182.08 8.30 1 -3 4 166.78 8.20 1 -3 4 187.88 8.80 -2 3 -4 23.90 2.70 2 -3 4 26.70 2.70 -3 3 -4 91.39 6.80 3 -3 4 93.89 4.70 3 -3 4 101.89 4.80 3 -3 4 96.59 4.60 3 -3 4 89.19 6.70 3 -3 4 98.29 5.00 3 -3 4 91.59 4.70 3 -3 4 98.79 4.60 3 -3 4 105.89 5.00 3 -3 4 103.49 4.80 -4 3 -4 39.70 4.80 4 -3 4 38.30 2.40 4 -3 4 31.30 4.40 4 -3 4 39.80 2.50 4 -3 4 36.10 2.50 4 -3 4 37.10 2.30 4 -3 4 33.20 2.30 4 -3 4 31.00 2.20 4 -3 4 33.20 2.40 4 -3 4 36.20 2.20 4 -3 4 35.10 2.40 5 -3 4 12.70 1.50 5 -3 4 12.70 1.50 5 -3 4 10.90 1.20 5 -3 4 12.30 1.40 5 -3 4 10.80 1.20 5 2 -4 18.90 1.40 5 2 -4 19.30 1.40 5 2 -4 18.40 1.40 5 2 -4 16.60 1.80 5 2 -4 19.90 1.60 -5 -2 4 17.50 1.50 -5 -2 4 18.30 1.50 4 2 -4 15.60 1.60 4 2 -4 13.80 1.50 4 2 -4 13.50 1.70 4 2 -4 14.80 1.80 4 2 -4 13.60 1.70 4 2 -4 14.60 2.10 4 2 -4 9.10 3.50 -4 -2 4 13.20 1.60 -4 -2 4 10.60 1.50 3 2 -4 55.79 3.00 3 2 -4 53.99 3.40 3 2 -4 58.99 6.30 3 2 -4 55.49 3.30 -3 -2 4 57.09 4.90 2 2 -4 129.59 7.70 2 2 -4 130.59 8.60 -2 -2 4 137.09 7.70 1 2 -4 235.08 10.40 1 2 -4 217.38 10.90 -1 -2 4 222.78 10.70 0 2 -4 1397.06 62.49 -1 2 -4 246.08 11.00 1 -2 4 259.97 11.20 -2 2 -4 126.29 7.10 2 -2 4 137.29 7.40 -3 2 -4 55.09 5.00 3 -2 4 64.29 3.30 3 -2 4 49.30 4.00 3 -2 4 61.39 5.20 3 -2 4 57.69 3.20 3 -2 4 59.89 3.40 3 -2 4 60.69 3.30 3 -2 4 62.49 3.40 -4 2 -4 12.70 3.20 4 -2 4 16.80 1.80 4 -2 4 15.50 1.60 4 -2 4 12.20 1.60 4 -2 4 13.30 1.60 4 -2 4 16.10 3.70 4 -2 4 13.20 1.50 4 -2 4 16.40 1.80 4 -2 4 15.60 1.90 4 -2 4 11.10 1.30 4 -2 4 14.20 1.60 4 -2 4 12.60 1.50 5 -2 4 19.40 1.60 5 -2 4 20.80 1.50 5 -2 4 21.20 1.60 5 -2 4 19.50 1.40 5 -2 4 18.00 1.70 5 -2 4 21.60 1.60 5 1 -4 11.20 1.70 5 1 -4 11.40 1.10 5 1 -4 11.60 1.60 5 1 -4 12.50 1.40 -5 -1 4 11.00 1.20 -5 -1 4 11.40 1.20 4 1 -4 42.90 2.70 4 1 -4 36.00 2.50 4 1 -4 38.90 2.60 4 1 -4 37.70 3.00 4 1 -4 36.60 2.40 4 1 -4 29.90 5.50 -4 -1 4 40.90 2.60 -4 -1 4 40.20 2.60 3 1 -4 44.70 3.10 3 1 -4 43.90 2.80 3 1 -4 48.30 2.70 3 1 -4 46.50 5.50 3 1 -4 50.69 2.70 -3 -1 4 49.99 4.40 2 1 -4 310.87 16.00 2 1 -4 305.17 15.00 -2 -1 4 327.27 14.80 1 1 -4 456.65 20.80 1 1 -4 495.45 20.40 1 1 -4 480.75 19.80 -1 -1 4 493.45 20.70 0 1 -4 604.84 24.30 0 -1 4 588.94 24.80 -1 1 -4 490.45 20.50 1 -1 4 506.25 20.70 2 -1 4 324.17 15.00 3 -1 4 46.80 2.80 3 -1 4 47.60 2.80 3 -1 4 44.40 4.60 3 -1 4 51.39 3.00 3 -1 4 42.60 3.10 3 -1 4 51.79 2.80 3 -1 4 47.40 2.60 3 -1 4 45.90 2.80 3 -1 4 49.20 2.90 3 -1 4 49.60 2.90 -4 1 -4 39.20 4.70 4 -1 4 40.90 2.50 4 -1 4 39.10 6.00 4 -1 4 43.20 2.80 4 -1 4 41.40 2.70 4 -1 4 38.90 2.60 4 -1 4 38.80 2.60 4 -1 4 41.30 2.70 4 -1 4 41.70 2.50 4 -1 4 42.40 2.80 4 -1 4 38.80 2.50 4 -1 4 39.80 2.70 4 -1 4 34.30 2.20 5 -1 4 12.50 1.20 5 -1 4 13.90 1.50 5 -1 4 11.10 1.30 5 -1 4 14.20 1.30 5 -1 4 13.80 1.50 5 -1 4 13.00 1.40 5 0 -4 17.80 1.50 5 0 -4 19.10 1.80 5 0 -4 19.40 1.80 -5 0 4 17.80 1.50 -5 0 4 19.10 1.50 4 0 -4 61.89 6.80 4 0 -4 49.30 2.90 4 0 -4 50.29 2.90 4 0 -4 49.90 3.50 4 0 -4 50.39 3.10 4 0 -4 48.70 3.00 -4 0 4 49.50 2.90 -4 0 4 52.19 3.00 3 0 -4 71.39 3.60 3 0 -4 70.19 3.60 3 0 -4 73.59 4.00 3 0 -4 78.89 7.10 3 0 -4 71.69 4.10 2 0 -4 6.60 2.00 2 0 -4 6.70 2.10 -2 0 4 6.70 1.60 1 0 -4 20.00 1.80 1 0 -4 21.30 2.50 -1 0 4 18.70 2.10 0 0 -4 14.20 1.50 0 0 -4 13.40 1.40 0 0 4 17.20 2.10 -1 0 -4 16.40 1.40 -1 0 -4 16.60 1.60 1 0 4 17.90 1.70 2 0 4 6.70 1.80 3 0 4 71.89 5.90 3 0 4 71.19 3.80 3 0 4 68.99 3.90 3 0 4 69.79 3.80 3 0 4 74.99 4.00 3 0 4 69.09 3.90 3 0 4 77.69 3.90 3 0 4 71.89 3.70 3 0 4 73.89 3.60 -4 0 -4 50.49 5.30 4 0 4 53.49 3.20 4 0 4 53.29 3.30 4 0 4 57.39 3.30 4 0 4 56.09 3.10 4 0 4 56.79 3.30 4 0 4 52.19 3.10 4 0 4 52.89 2.90 4 0 4 49.10 5.40 4 0 4 50.79 3.10 4 0 4 53.79 3.20 4 0 4 53.49 3.10 4 0 4 54.49 3.40 5 0 4 20.20 1.70 5 0 4 19.90 1.60 5 0 4 20.70 1.60 5 0 4 20.90 1.50 5 0 4 18.50 1.70 5 0 4 21.30 1.60 5 0 4 18.90 1.70 5 -1 -4 11.90 1.50 5 -1 -4 12.60 1.80 5 -1 -4 11.70 1.90 -5 1 4 12.60 1.20 -5 1 4 11.20 1.20 4 -1 -4 35.80 6.30 4 -1 -4 43.10 2.60 4 -1 -4 38.90 2.50 4 -1 -4 37.40 2.90 4 -1 -4 41.10 2.40 4 -1 -4 40.70 2.70 -4 1 4 37.50 2.50 -4 1 4 39.50 2.50 3 -1 -4 48.90 5.40 3 -1 -4 47.40 2.60 3 -1 -4 49.70 2.70 3 -1 -4 47.60 3.10 2 -1 -4 311.67 15.80 2 -1 -4 319.67 15.40 -2 1 4 327.57 14.40 1 -1 -4 487.35 20.60 1 -1 -4 491.85 21.00 -1 1 4 500.45 20.80 0 -1 -4 619.84 24.80 0 -1 -4 582.94 24.30 -1 -1 -4 518.85 20.00 1 1 4 471.55 20.50 2 1 4 317.37 14.90 3 1 4 45.30 2.70 3 1 4 45.40 3.20 3 1 4 46.30 2.90 3 1 4 47.90 2.90 3 1 4 48.40 2.90 3 1 4 44.90 2.80 3 1 4 43.10 2.80 3 1 4 45.70 2.60 3 1 4 47.80 4.70 3 1 4 44.80 2.90 3 1 4 46.00 2.80 -4 -1 -4 41.10 4.50 4 1 4 39.50 2.40 4 1 4 37.80 2.50 4 1 4 39.60 2.70 4 1 4 42.60 2.90 4 1 4 38.80 2.60 4 1 4 37.40 2.80 4 1 4 37.50 2.60 4 1 4 40.90 2.70 4 1 4 43.80 6.50 4 1 4 41.30 2.80 4 1 4 37.80 2.60 4 1 4 44.30 2.60 5 1 4 13.00 1.30 5 1 4 12.30 1.40 5 1 4 13.30 1.30 5 1 4 13.30 1.40 5 1 4 11.60 1.20 5 1 4 11.00 1.30 5 1 4 13.60 1.40 5 -2 -4 17.80 1.40 5 -2 -4 19.80 1.80 5 -2 -4 19.70 1.40 -5 2 4 18.50 1.40 -5 2 4 18.60 1.50 4 -2 -4 13.70 1.90 4 -2 -4 12.40 3.70 4 -2 -4 14.60 1.40 4 -2 -4 14.70 1.80 4 -2 -4 15.40 1.60 4 -2 -4 11.90 1.50 -4 2 4 14.40 1.60 -4 2 4 13.90 1.50 3 -2 -4 61.89 3.10 3 -2 -4 63.69 6.10 3 -2 -4 60.19 3.60 -3 2 4 60.19 3.20 -3 2 4 60.09 3.70 2 -2 -4 137.29 8.00 2 -2 -4 128.99 8.10 2 -2 -4 134.79 6.90 1 -2 -4 232.18 11.00 1 -2 -4 234.98 11.10 1 -2 -4 247.28 10.80 0 -2 -4 1312.67 58.29 -1 -2 -4 236.68 10.50 1 2 4 223.98 10.10 -2 -2 -4 123.89 6.50 2 2 4 126.99 7.20 -3 -2 -4 64.59 5.10 3 2 4 62.49 3.50 3 2 4 55.99 3.30 3 2 4 59.29 3.70 3 2 4 61.79 3.20 3 2 4 63.09 5.40 3 2 4 64.09 3.50 3 2 4 61.49 3.50 4 2 4 12.20 1.40 4 2 4 14.40 1.80 4 2 4 12.70 1.60 4 2 4 12.80 3.20 4 2 4 15.90 1.90 4 2 4 12.50 1.70 4 2 4 14.80 1.60 4 2 4 14.50 1.90 4 2 4 12.10 1.50 4 2 4 14.70 1.70 4 2 4 13.60 1.80 4 2 4 14.10 1.60 5 2 4 20.10 1.50 5 2 4 20.70 1.70 5 2 4 19.60 1.60 5 2 4 17.30 1.70 5 2 4 21.10 1.60 5 2 4 19.70 1.60 5 2 4 20.90 1.70 5 2 4 21.60 1.90 5 -3 -4 11.10 1.80 5 -3 -4 9.70 1.00 -5 3 4 11.20 1.10 -5 3 4 11.50 1.20 4 -3 -4 31.30 2.10 4 -3 -4 34.50 2.70 4 -3 -4 33.40 2.10 4 -3 -4 32.00 2.50 4 -3 -4 30.30 5.30 -4 3 4 35.70 2.20 -4 3 4 38.20 2.30 3 -3 -4 95.59 4.40 3 -3 -4 97.89 7.60 3 -3 -4 90.09 4.40 3 -3 -4 91.89 4.90 -3 3 4 100.19 4.60 -3 3 4 90.29 4.40 2 -3 -4 30.70 4.20 2 -3 -4 29.20 2.80 1 -3 -4 159.68 8.20 1 -3 -4 169.78 8.10 1 -3 -4 173.28 8.40 0 -3 -4 1609.24 64.09 -1 -3 -4 170.38 8.00 1 3 4 159.38 7.50 -2 -3 -4 28.10 2.40 2 3 4 26.70 2.90 3 3 4 88.79 4.50 3 3 4 94.89 4.80 3 3 4 94.59 4.90 3 3 4 95.79 4.50 3 3 4 87.79 6.80 3 3 4 86.79 4.60 3 3 4 100.19 4.80 3 3 4 95.29 4.80 3 3 4 93.49 4.70 3 3 4 97.29 4.80 3 3 4 84.59 5.00 3 3 4 92.09 4.80 4 3 4 36.80 2.60 4 3 4 33.10 2.60 4 3 4 31.40 2.30 4 3 4 34.00 2.60 4 3 4 33.80 2.50 4 3 4 33.90 2.60 4 3 4 33.70 2.60 4 3 4 30.50 2.40 4 3 4 30.90 5.30 4 3 4 34.60 2.20 4 3 4 36.00 2.60 5 3 4 10.50 1.30 5 3 4 12.00 1.40 5 3 4 12.90 1.40 5 3 4 10.80 1.20 5 3 4 11.80 1.40 5 3 4 11.80 1.40 5 3 4 11.90 1.10 5 3 4 11.00 1.30 5 -4 -4 16.00 1.40 -5 4 4 16.00 1.20 -5 4 4 16.00 1.20 4 -4 -4 38.40 3.00 4 -4 -4 40.20 2.40 4 -4 -4 39.90 2.20 4 -4 -4 47.40 7.90 4 -4 -4 39.90 2.70 -4 4 4 40.90 2.50 -4 4 4 40.60 2.40 3 -4 -4 9.40 1.40 3 -4 -4 10.10 3.00 3 -4 -4 9.30 1.10 -3 4 4 10.20 1.10 -3 4 4 10.90 1.30 2 -4 -4 35.40 3.40 2 -4 -4 31.50 3.20 1 -4 -4 39.00 3.20 1 -4 -4 42.70 2.70 0 -4 -4 471.55 20.30 -1 -4 -4 37.10 2.90 1 4 4 38.30 2.40 -2 -4 -4 33.30 2.60 -2 -4 -4 35.00 3.60 2 4 4 31.60 3.20 -3 -4 -4 9.50 2.60 3 4 4 9.80 1.30 3 4 4 9.20 1.40 3 4 4 6.80 1.20 3 4 4 8.80 1.50 3 4 4 7.90 1.40 3 4 4 9.40 1.50 3 4 4 6.60 1.80 3 4 4 7.70 1.10 3 4 4 10.40 1.50 3 4 4 6.70 2.30 3 4 4 8.00 1.50 3 4 4 9.30 1.50 4 4 4 34.70 2.70 4 4 4 39.40 2.80 4 4 4 40.30 6.30 4 4 4 30.20 2.90 4 4 4 36.60 2.40 4 4 4 34.90 2.50 4 4 4 39.40 2.40 4 4 4 37.70 2.80 4 4 4 36.80 2.70 4 4 4 38.70 2.80 4 4 4 35.50 2.70 4 4 4 38.70 2.60 5 4 4 22.40 2.30 5 4 4 18.20 2.20 5 4 4 18.00 2.20 5 4 4 17.20 1.40 5 4 4 16.20 1.70 5 4 4 18.40 1.70 5 4 4 15.30 1.30 5 -5 -4 21.40 1.70 5 -5 -4 21.20 1.40 -5 5 4 23.10 1.40 4 -5 -4 18.40 1.50 4 -5 -4 14.90 1.30 4 -5 -4 16.60 2.20 4 -5 -4 16.20 1.60 -4 5 4 20.80 4.60 -4 5 4 15.40 1.40 -4 5 4 18.60 1.60 3 -5 -4 40.10 4.10 3 -5 -4 42.30 2.70 3 -5 -4 44.90 4.50 3 -5 -4 43.30 2.40 -3 5 4 44.10 2.40 -3 5 4 47.60 2.60 2 -5 -4 31.00 3.30 2 -5 -4 25.00 2.80 1 -5 -4 551.94 22.10 -1 5 4 451.55 21.10 0 5 4 1453.55 65.99 -1 -5 -4 461.15 20.00 -2 -5 -4 27.20 3.10 -2 -5 -4 28.40 4.40 2 5 4 27.70 2.90 -3 -5 -4 45.00 5.00 3 5 4 43.90 4.50 3 5 4 44.20 3.40 3 5 4 44.70 3.00 3 5 4 45.70 2.90 3 5 4 42.80 2.60 3 5 4 46.30 3.00 3 5 4 42.60 2.60 3 5 4 44.40 3.00 3 5 4 45.10 2.90 3 5 4 46.10 3.10 3 5 4 44.30 2.70 4 5 4 17.30 1.70 4 5 4 14.90 1.90 4 5 4 17.20 2.10 4 5 4 16.50 1.90 4 5 4 17.30 2.20 4 5 4 16.40 1.70 4 5 4 18.00 1.50 4 5 4 15.40 1.90 4 5 4 18.90 2.10 4 5 4 16.70 1.90 4 5 4 12.80 2.10 5 5 4 23.10 1.80 5 5 4 22.00 1.70 5 5 4 23.50 1.50 5 5 4 24.30 1.50 5 5 4 24.40 1.80 5 5 4 22.50 1.80 5 5 4 22.60 1.50 5 5 4 22.10 1.70 5 5 4 25.60 1.90 5 -6 -4 6.90 1.00 -5 6 4 9.10 0.80 4 -6 -4 4.70 1.90 4 -6 -4 5.70 1.00 -4 6 4 5.60 1.10 3 -6 -4 66.09 5.30 3 -6 -4 70.69 5.80 -3 6 4 57.59 5.70 -3 6 4 59.99 3.30 -3 6 4 66.09 3.20 2 -6 -4 99.19 6.90 2 -6 -4 110.99 5.90 -2 6 4 95.49 6.60 1 -6 -4 514.65 22.50 -1 6 4 486.35 21.30 0 -6 -4 252.77 12.30 -1 -6 -4 416.46 18.60 -2 -6 -4 102.79 5.90 -2 -6 -4 111.19 7.70 2 6 4 97.79 6.00 -3 -6 -4 68.19 6.60 3 6 4 64.99 3.90 3 6 4 62.89 3.60 3 6 4 68.29 4.00 3 6 4 69.59 3.90 3 6 4 68.09 3.60 3 6 4 62.99 3.50 3 6 4 72.59 4.60 3 6 4 62.19 5.40 3 6 4 65.69 3.90 3 6 4 64.19 3.90 3 6 4 69.49 3.80 3 6 4 64.49 3.80 4 6 4 4.80 1.60 4 6 4 4.10 1.50 4 6 4 4.50 1.60 4 6 4 4.80 1.40 4 6 4 5.60 1.60 4 6 4 5.90 1.70 4 6 4 4.50 1.00 4 6 4 5.50 1.70 4 6 4 5.10 1.70 5 6 4 8.50 1.10 5 6 4 7.40 0.80 5 6 4 6.10 1.00 5 6 4 8.50 0.90 5 6 4 6.70 0.80 5 6 4 6.20 1.00 5 6 4 8.50 1.10 5 6 4 8.50 1.20 5 6 4 7.10 1.00 5 -7 -4 6.80 1.30 4 -7 -4 23.80 1.50 4 -7 -4 20.20 2.30 -4 7 4 25.00 1.70 -4 7 4 21.60 1.50 3 -7 -4 37.80 2.30 -3 7 4 36.60 2.10 -3 7 4 33.00 2.20 -3 7 4 36.80 5.50 2 -7 -4 110.19 7.50 2 -7 -4 98.19 5.10 -2 7 4 102.49 6.80 -2 7 4 101.29 5.30 1 -7 -4 68.39 5.40 -1 7 4 69.19 4.40 0 -7 -4 50.79 4.20 0 7 4 45.60 3.10 -1 -7 -4 56.29 4.90 -1 -7 -4 52.49 4.20 -2 -7 -4 109.69 8.20 -2 -7 -4 95.89 6.60 2 7 4 107.09 5.20 2 7 4 110.79 6.70 2 7 4 108.29 5.40 2 7 4 103.69 5.20 2 7 4 107.19 5.00 2 7 4 102.89 5.30 -3 -7 -4 37.60 6.00 3 7 4 29.80 2.20 3 7 4 37.50 2.70 3 7 4 31.60 2.50 3 7 4 34.30 2.60 3 7 4 34.40 2.60 3 7 4 35.00 2.30 3 7 4 32.60 2.60 3 7 4 33.10 2.60 3 7 4 36.00 2.80 4 7 4 22.40 2.00 4 7 4 21.60 2.20 4 7 4 26.60 2.20 4 7 4 19.80 2.10 4 7 4 24.70 1.80 4 7 4 23.70 1.80 4 7 4 22.40 2.10 4 7 4 24.40 2.10 5 7 4 6.90 1.00 5 7 4 7.50 0.80 5 7 4 9.10 1.10 5 7 4 6.20 0.90 5 7 4 6.50 0.90 5 7 4 8.00 1.00 5 7 4 6.30 0.90 5 -8 -4 2.50 0.60 4 -8 -4 15.20 2.10 4 -8 -4 11.60 1.10 -4 8 4 12.10 1.00 3 -8 -4 27.50 1.90 3 -8 -4 20.90 4.30 -3 8 4 25.90 4.30 -3 8 4 29.20 1.70 -3 8 4 26.40 1.90 2 -8 -4 18.10 1.50 2 -8 -4 19.10 4.10 2 -8 -4 15.40 1.60 -2 8 4 17.10 3.10 -2 8 4 20.90 1.50 -2 8 4 20.30 1.20 1 -8 -4 139.19 9.00 1 -8 -4 142.19 8.20 -1 8 4 144.79 7.50 0 -8 -4 26.40 3.80 0 -8 -4 29.10 4.20 -1 -8 -4 141.09 9.30 -1 -8 -4 146.39 8.50 -2 -8 -4 16.20 1.80 -2 -8 -4 17.70 4.20 -2 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2.60 2 -7 9 40.00 3.30 2 -7 9 40.40 2.60 3 -7 9 67.09 3.90 3 -7 9 63.19 3.60 4 -7 9 9.50 1.70 4 -7 9 7.00 1.20 4 -7 9 9.90 1.80 4 6 -9 8.40 1.30 4 6 -9 5.50 1.30 -4 -6 9 7.40 1.20 -4 -6 9 6.60 0.90 3 6 -9 9.80 1.60 3 6 -9 19.00 4.60 3 6 -9 9.20 3.70 3 6 -9 11.80 1.60 -3 -6 9 9.20 3.30 -3 -6 9 14.90 1.80 -3 -6 9 11.20 1.90 -3 -6 9 10.70 1.30 2 6 -9 66.39 7.60 -2 -6 9 67.09 4.10 -2 -6 9 67.79 3.50 -2 -6 9 66.09 3.70 -2 -6 9 68.09 7.10 1 6 -9 50.29 6.00 1 6 -9 52.09 5.10 -1 -6 9 58.09 3.20 -1 -6 9 56.49 2.90 -1 -6 9 66.29 6.30 -1 -6 9 57.69 3.50 0 6 -9 49.30 4.40 0 6 -9 59.39 5.60 0 -6 9 54.09 3.30 0 -6 9 56.59 5.40 -1 6 -9 59.19 4.60 -1 6 -9 61.99 5.20 1 -6 9 58.19 3.20 1 -6 9 55.19 5.00 1 -6 9 55.39 3.20 1 -6 9 56.99 3.20 1 -6 9 58.89 3.80 -2 6 -9 72.79 5.60 -2 6 -9 65.89 5.40 2 -6 9 64.59 3.40 2 -6 9 74.69 3.70 2 -6 9 70.19 3.80 2 -6 9 67.79 4.30 -3 6 -9 13.20 3.00 -3 6 -9 16.20 3.00 3 -6 9 14.00 2.10 3 -6 9 12.80 1.70 3 -6 9 12.40 1.50 4 -6 9 8.10 1.40 4 -6 9 9.30 1.30 4 -6 9 8.50 1.40 5 5 -9 4.30 0.80 5 5 -9 3.80 0.60 -5 -5 9 3.00 0.50 4 5 -9 7.60 1.50 4 5 -9 8.50 1.40 -4 -5 9 9.00 1.10 -4 -5 9 9.90 1.30 3 5 -9 17.20 4.80 3 5 -9 17.00 2.00 3 5 -9 22.70 4.90 3 5 -9 19.30 2.10 -3 -5 9 21.50 2.50 -3 -5 9 22.40 4.90 -3 -5 9 23.10 2.00 -3 -5 9 19.50 1.70 2 5 -9 23.10 5.00 2 5 -9 27.90 5.00 -2 -5 9 27.60 5.10 -2 -5 9 23.20 2.00 -2 -5 9 21.30 1.80 -2 -5 9 22.40 2.20 1 5 -9 9.00 3.00 1 5 -9 7.80 3.00 -1 -5 9 7.00 1.30 -1 -5 9 6.80 1.20 -1 -5 9 9.20 2.90 0 5 -9 139.99 7.90 0 5 -9 142.39 12.30 0 -5 9 131.29 9.00 -1 5 -9 6.40 2.20 -1 5 -9 11.00 2.30 1 -5 9 8.50 1.50 1 -5 9 5.90 2.10 1 -5 9 6.80 1.10 1 -5 9 8.20 1.20 -2 5 -9 22.10 3.20 -2 5 -9 28.60 3.70 2 -5 9 25.70 2.10 2 -5 9 23.90 2.40 2 -5 9 25.90 1.90 2 -5 9 22.70 2.10 -3 5 -9 19.40 3.40 -3 5 -9 18.90 3.10 3 -5 9 23.10 1.80 3 -5 9 21.10 2.30 3 -5 9 22.60 2.00 3 -5 9 21.80 2.10 4 -5 9 11.20 1.50 4 -5 9 8.50 1.70 4 -5 9 10.90 1.30 5 -5 9 4.30 0.80 5 -5 9 3.10 0.90 5 4 -9 7.10 0.80 5 4 -9 8.10 1.10 -5 -4 9 6.70 0.80 -5 -4 9 8.00 0.70 4 4 -9 35.00 2.80 4 4 -9 30.40 2.40 -4 -4 9 34.40 2.40 -4 -4 9 35.80 2.20 3 4 -9 50.49 3.40 3 4 -9 42.60 7.20 3 4 -9 57.09 6.30 -3 -4 9 48.70 3.60 -3 -4 9 54.59 3.00 -3 -4 9 55.69 3.30 -3 -4 9 46.10 6.60 2 4 -9 51.09 7.70 2 4 -9 59.29 5.70 -2 -4 9 47.70 2.70 -2 -4 9 44.90 6.50 -2 -4 9 49.99 3.30 -2 -4 9 43.90 2.90 1 4 -9 50.49 8.80 1 4 -9 53.49 4.90 -1 -4 9 50.09 5.20 0 4 -9 95.99 6.80 0 4 -9 107.09 7.10 0 -4 9 95.99 7.10 -1 4 -9 57.49 4.20 -1 4 -9 57.49 4.60 -2 4 -9 46.30 4.00 -2 4 -9 47.60 4.00 2 -4 9 49.99 2.60 2 -4 9 49.00 2.90 2 -4 9 49.90 3.50 2 -4 9 50.29 2.80 -3 4 -9 51.59 4.50 -3 4 -9 58.29 5.00 3 -4 9 54.39 3.10 3 -4 9 53.69 2.90 3 -4 9 50.69 2.80 3 -4 9 55.69 3.70 3 -4 9 49.99 3.30 3 -4 9 47.30 3.00 3 -4 9 59.09 3.40 4 -4 9 37.40 2.10 4 -4 9 34.40 2.90 4 -4 9 36.80 2.20 4 -4 9 37.70 2.70 4 -4 9 38.60 2.50 5 -4 9 8.50 1.10 5 -4 9 9.30 1.10 5 3 -9 4.70 0.70 5 3 -9 6.50 1.00 -5 -3 9 3.50 0.50 -5 -3 9 5.00 0.70 4 3 -9 19.30 2.00 4 3 -9 18.50 2.20 -4 -3 9 20.30 1.60 -4 -3 9 22.20 1.80 3 3 -9 42.50 7.70 3 3 -9 42.40 3.00 3 3 -9 52.79 7.60 -3 -3 9 45.50 2.60 -3 -3 9 40.30 2.80 -3 -3 9 42.10 6.10 2 3 -9 47.90 5.30 -2 -3 9 45.60 2.60 -2 -3 9 45.70 5.00 -2 -3 9 47.50 2.80 -2 -3 9 42.70 3.10 1 3 -9 130.89 8.80 1 3 -9 133.79 9.00 -1 -3 9 134.69 12.30 0 3 -9 423.26 18.80 0 3 -9 413.56 19.30 0 -3 9 420.16 19.90 -1 3 -9 143.09 7.60 -1 3 -9 143.49 7.80 -2 3 -9 43.60 3.70 -2 3 -9 46.10 4.80 2 -3 9 39.20 2.50 2 -3 9 46.20 2.80 2 -3 9 45.30 3.10 2 -3 9 43.50 2.30 2 -3 9 44.20 3.20 2 -3 9 44.20 2.50 -3 3 -9 49.00 4.20 3 -3 9 47.40 3.00 3 -3 9 47.30 3.40 3 -3 9 41.50 2.50 3 -3 9 43.30 2.90 3 -3 9 41.00 3.10 3 -3 9 49.70 2.60 3 -3 9 51.79 2.90 3 -3 9 47.70 2.70 3 -3 9 48.10 2.70 4 -3 9 23.10 2.20 4 -3 9 22.50 1.70 4 -3 9 20.90 2.30 4 -3 9 23.90 1.70 4 -3 9 25.10 1.90 4 -3 9 19.90 2.00 4 -3 9 22.30 2.00 5 -3 9 4.80 0.80 5 -3 9 5.70 1.10 5 2 -9 3.40 0.60 5 2 -9 4.70 0.90 -5 -2 9 2.80 0.80 -5 -2 9 3.30 0.60 4 2 -9 2.70 0.90 4 2 -9 1.60 1.10 -4 -2 9 1.60 0.70 -4 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2.00 4 1 -9 23.90 2.40 -4 -1 9 23.40 1.80 -4 -1 9 24.30 2.00 3 1 -9 22.80 4.90 3 1 -9 20.10 5.00 -3 -1 9 20.30 1.70 -3 -1 9 22.20 2.40 -3 -1 9 22.30 1.90 2 1 -9 60.19 5.90 -2 -1 9 56.39 5.40 -2 -1 9 77.49 3.70 1 1 -9 244.38 12.50 1 1 -9 250.77 12.20 1 1 -9 222.28 12.50 -1 -1 9 244.68 12.80 0 1 -9 334.17 14.90 0 1 -9 302.77 15.10 0 -1 9 325.87 15.80 -1 1 -9 228.38 10.90 -1 1 -9 246.28 11.10 -2 1 -9 57.29 3.70 -2 1 -9 50.19 4.60 2 -1 9 58.49 2.90 2 -1 9 53.29 3.30 2 -1 9 65.99 3.00 2 -1 9 52.89 3.00 -3 1 -9 16.20 3.70 -3 1 -9 31.30 6.60 3 -1 9 26.70 1.80 3 -1 9 26.00 2.20 3 -1 9 19.80 1.80 3 -1 9 21.60 2.30 3 -1 9 21.70 2.10 3 -1 9 23.30 1.90 3 -1 9 23.30 1.70 3 -1 9 28.00 2.30 3 -1 9 23.10 1.90 3 -1 9 22.20 1.90 3 -1 9 27.40 2.50 4 -1 9 28.60 1.90 4 -1 9 30.20 2.00 4 -1 9 25.80 2.10 4 -1 9 33.10 2.90 4 -1 9 26.10 1.90 4 -1 9 24.80 1.90 4 -1 9 27.90 2.30 4 -1 9 27.30 2.40 4 -1 9 30.20 2.20 4 -1 9 25.80 1.80 5 -1 9 5.10 0.70 5 -1 9 7.10 1.20 5 -1 9 7.00 0.90 5 -1 9 7.40 0.90 5 0 -9 16.20 1.50 -5 0 9 19.60 1.30 4 0 -9 3.90 1.20 4 0 -9 1.90 0.90 -4 0 9 1.50 0.80 -4 0 9 2.40 0.80 3 0 -9 26.80 2.10 3 0 -9 27.90 4.10 3 0 -9 30.80 5.40 3 0 -9 23.60 5.20 -3 0 9 22.40 2.00 -3 0 9 26.50 2.50 -3 0 9 25.10 1.80 2 0 -9 10.70 2.20 2 0 -9 7.70 2.80 2 0 -9 9.50 3.10 -2 0 9 8.30 1.50 -2 0 9 8.90 1.00 -2 0 9 6.60 2.00 1 0 -9 346.17 16.30 1 0 -9 327.47 15.90 -1 0 9 326.87 16.40 0 0 -9 34.30 3.30 -1 0 -9 320.37 14.30 -2 0 -9 9.00 1.60 2 0 9 7.90 1.10 2 0 9 8.40 2.10 2 0 9 9.10 1.40 2 0 9 7.30 1.10 2 0 9 6.10 0.80 2 0 9 9.10 1.40 -3 0 -9 24.90 4.70 3 0 9 28.20 2.30 3 0 9 22.50 1.90 3 0 9 25.30 3.60 3 0 9 25.00 2.30 3 0 9 24.20 2.00 3 0 9 31.30 2.80 3 0 9 26.40 1.70 3 0 9 25.00 2.00 3 0 9 27.30 3.10 3 0 9 20.70 2.10 4 0 9 2.10 0.80 4 0 9 3.00 1.40 4 0 9 2.40 0.90 4 0 9 2.70 0.80 4 0 9 2.20 0.80 4 0 9 2.70 0.80 4 0 9 3.80 1.10 4 0 9 3.90 0.90 4 0 9 1.40 0.80 4 0 9 2.30 0.90 4 0 9 3.50 0.90 4 0 9 2.30 1.10 5 0 9 24.80 1.50 5 0 9 20.20 1.30 5 0 9 20.50 1.90 5 -1 -9 6.50 0.90 -5 1 9 5.10 0.60 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0.90 -5 2 9 3.60 0.50 -5 2 9 4.40 0.70 4 -2 -9 3.20 1.00 -4 2 9 1.00 0.80 -4 2 9 2.00 0.60 3 -2 -9 41.70 4.10 3 -2 -9 42.40 6.70 -3 2 9 39.60 3.00 -3 2 9 41.40 2.60 -3 2 9 40.50 2.40 2 -2 -9 106.09 6.80 2 -2 -9 116.19 9.50 2 -2 -9 105.59 8.00 -2 2 9 99.69 5.30 -2 2 9 105.89 5.00 1 -2 -9 83.19 5.90 1 -2 -9 81.09 6.00 0 -2 -9 262.77 13.10 0 -2 -9 246.28 12.10 -1 -2 -9 85.09 4.80 -1 -2 -9 81.79 6.00 -2 -2 -9 104.09 7.10 2 2 9 92.09 4.80 2 2 9 100.39 4.90 2 2 9 107.59 5.60 2 2 9 96.39 5.00 3 2 9 43.70 2.90 3 2 9 42.50 3.10 3 2 9 43.30 2.70 3 2 9 41.80 2.60 3 2 9 49.80 3.50 3 2 9 34.30 2.80 3 2 9 40.90 2.60 3 2 9 37.90 2.80 3 2 9 41.30 2.30 3 2 9 42.70 3.00 4 2 9 4.40 0.90 4 2 9 3.30 1.10 4 2 9 1.90 1.10 4 2 9 3.70 1.00 4 2 9 3.00 0.90 4 2 9 2.50 0.90 4 2 9 4.00 1.40 4 2 9 3.10 1.00 4 2 9 3.80 1.00 4 2 9 2.50 1.30 4 2 9 1.90 0.70 4 2 9 2.80 0.90 5 2 9 3.30 0.60 5 2 9 2.80 0.60 5 2 9 4.70 0.80 5 2 9 4.60 0.60 5 2 9 3.10 0.60 5 2 9 3.90 0.90 5 2 9 2.90 1.00 -5 3 9 4.60 0.50 4 -3 -9 19.80 1.90 4 -3 -9 15.30 1.80 -4 3 9 22.30 1.50 -4 3 9 21.30 1.70 3 -3 -9 31.00 5.40 -3 3 9 52.09 3.70 -3 3 9 46.20 2.80 -3 3 9 46.80 2.50 2 -3 -9 44.40 4.60 2 -3 -9 54.29 6.90 2 -3 -9 47.40 4.40 -2 3 9 45.80 3.60 -2 3 9 43.40 2.30 -2 3 9 47.60 2.70 1 -3 -9 135.69 8.40 1 -3 -9 126.49 8.20 1 -3 -9 156.78 9.00 0 -3 -9 435.86 19.60 0 -3 -9 395.76 18.40 -1 -3 -9 136.29 8.50 -2 -3 -9 44.70 4.30 2 3 9 45.10 3.00 2 3 9 40.20 2.70 2 3 9 42.60 2.50 2 3 9 37.30 2.40 2 3 9 38.90 2.50 2 3 9 37.30 2.50 2 3 9 42.80 2.80 2 3 9 42.80 3.20 2 3 9 39.90 2.70 -3 -3 -9 43.80 6.10 3 3 9 42.90 2.80 3 3 9 46.70 2.60 3 3 9 42.70 3.40 3 3 9 43.40 2.90 3 3 9 42.90 3.00 3 3 9 37.20 2.70 3 3 9 43.20 2.70 3 3 9 43.60 2.70 3 3 9 43.00 2.70 3 3 9 44.70 3.10 3 3 9 42.30 2.40 3 3 9 41.10 3.10 4 3 9 20.20 2.30 4 3 9 21.00 1.90 4 3 9 20.20 2.00 4 3 9 20.40 1.70 4 3 9 22.30 2.10 4 3 9 21.30 2.50 4 3 9 18.50 2.00 4 3 9 20.50 1.60 4 3 9 23.50 1.60 4 3 9 20.50 1.80 4 3 9 24.70 1.90 4 3 9 24.20 1.80 5 3 9 3.30 0.60 5 3 9 4.20 0.60 5 3 9 3.70 0.70 5 3 9 4.30 0.70 5 3 9 5.00 0.90 5 3 9 5.30 0.70 5 3 9 5.20 0.90 5 3 9 5.60 0.70 -5 4 9 10.00 0.90 4 -4 -9 35.40 2.70 -4 4 9 37.20 2.30 -4 4 9 37.30 2.10 -3 4 9 48.60 2.90 -3 4 9 49.20 3.30 -3 4 9 50.99 2.60 2 -4 -9 49.50 4.60 -2 4 9 50.19 2.80 -2 4 9 50.29 3.10 -2 4 9 47.80 2.40 1 -4 -9 56.79 4.90 1 -4 -9 57.29 4.90 0 -4 -9 108.69 8.20 0 -4 -9 96.19 5.90 -1 -4 -9 58.59 5.10 -2 -4 -9 44.20 4.40 2 4 9 47.60 2.80 2 4 9 44.80 2.90 2 4 9 37.60 2.50 2 4 9 45.40 2.90 2 4 9 37.30 2.20 2 4 9 44.10 3.40 2 4 9 46.00 2.60 2 4 9 41.00 2.60 2 4 9 41.20 3.10 2 4 9 45.60 2.90 2 4 9 40.80 2.70 -3 -4 -9 56.39 6.30 3 4 9 59.69 4.10 3 4 9 48.80 3.10 3 4 9 47.10 3.10 3 4 9 51.59 3.40 3 4 9 50.79 3.10 3 4 9 50.89 3.40 3 4 9 52.39 3.60 3 4 9 49.10 3.20 3 4 9 51.49 3.00 3 4 9 51.29 3.40 3 4 9 52.19 2.70 4 4 9 37.10 2.40 4 4 9 35.80 2.70 4 4 9 40.40 2.10 4 4 9 35.00 2.30 4 4 9 35.30 2.40 4 4 9 35.80 2.50 4 4 9 37.80 2.60 4 4 9 33.70 3.20 4 4 9 39.50 2.30 4 4 9 40.00 2.70 5 4 9 9.10 0.80 5 4 9 6.40 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10 11.00 1.30 4 -7 10 11.00 1.50 4 6 -10 0.10 1.10 -4 -6 10 0.10 0.40 3 6 -10 46.20 3.20 -3 -6 10 46.90 3.30 2 6 -10 37.80 6.60 2 6 -10 41.70 6.30 2 6 -10 51.69 4.30 -2 -6 10 35.70 3.00 -2 -6 10 39.50 6.30 -2 -6 10 44.10 2.80 -2 -6 10 42.90 2.50 1 6 -10 150.08 11.20 1 6 -10 163.58 10.20 -1 -6 10 164.18 7.70 -1 -6 10 173.28 11.50 -1 -6 10 161.38 7.30 0 6 -10 31.80 5.00 0 6 -10 24.10 3.70 0 -6 10 21.60 4.40 0 -6 10 21.20 1.90 0 -6 10 18.70 2.00 -1 6 -10 170.28 9.40 -1 6 -10 169.28 10.20 1 -6 10 164.08 7.50 1 -6 10 164.98 8.10 1 -6 10 161.68 7.40 -2 6 -10 42.80 4.60 -2 6 -10 47.20 4.30 2 -6 10 41.00 2.70 2 -6 10 42.60 3.40 2 -6 10 39.50 2.70 3 -6 10 56.49 3.40 3 -6 10 56.89 3.80 4 -6 10 0.90 0.90 4 -6 10 1.70 1.20 4 -6 10 1.10 1.40 4 5 -10 5.80 1.30 4 5 -10 5.00 1.10 -4 -5 10 7.60 1.10 -4 -5 10 7.10 0.90 3 5 -10 34.10 6.20 3 5 -10 26.20 2.50 3 5 -10 23.70 5.70 -3 -5 10 30.60 6.00 -3 -5 10 29.90 2.30 -3 -5 10 30.90 2.70 -3 -5 10 29.50 2.00 2 5 -10 71.69 7.60 2 5 -10 81.39 7.00 -2 -5 10 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-10 152.78 8.50 0 -4 10 140.59 9.20 0 -4 10 145.09 6.70 -1 4 -10 51.09 7.70 -1 4 -10 47.60 4.00 1 -4 10 40.40 2.60 1 -4 10 46.30 2.80 1 -4 10 46.90 2.70 -2 4 -10 72.29 5.40 -2 4 -10 84.79 5.90 2 -4 10 84.69 4.20 2 -4 10 69.79 4.10 2 -4 10 78.79 4.00 2 -4 10 74.79 4.70 3 -4 10 32.40 2.40 3 -4 10 28.50 2.50 3 -4 10 32.00 2.10 3 -4 10 31.50 2.70 3 -4 10 33.70 2.60 4 -4 10 10.90 1.60 4 -4 10 7.90 1.70 4 -4 10 12.10 1.40 5 3 -10 3.30 0.70 -5 -3 10 3.00 0.40 -5 -3 10 3.40 0.60 4 3 -10 6.70 1.20 4 3 -10 7.10 1.40 -4 -3 10 9.70 1.10 -4 -3 10 8.60 1.20 3 3 -10 29.60 2.50 3 3 -10 26.90 5.70 3 3 -10 31.50 5.40 -3 -3 10 31.10 2.30 -3 -3 10 30.50 2.10 -3 -3 10 28.80 5.00 -3 -3 10 31.30 2.70 2 3 -10 26.00 4.60 -2 -3 10 24.70 1.70 -2 -3 10 21.70 2.20 -2 -3 10 24.10 4.60 -2 -3 10 22.30 1.90 1 3 -10 71.69 5.80 1 3 -10 62.59 6.30 1 3 -10 74.59 5.40 -1 -3 10 77.59 6.40 -1 -3 10 61.69 3.70 -1 -3 10 71.19 3.90 0 3 -10 47.00 4.10 0 3 -10 43.90 4.40 0 -3 10 49.50 4.80 -1 3 -10 74.09 5.00 -1 3 -10 67.39 5.10 1 -3 10 67.89 4.10 1 -3 10 69.89 3.50 -2 3 -10 26.80 3.40 -2 3 -10 27.40 3.10 2 -3 10 22.40 2.20 2 -3 10 19.90 1.70 2 -3 10 25.10 1.70 2 -3 10 27.30 1.90 2 -3 10 26.10 2.10 2 -3 10 23.80 2.50 2 -3 10 22.50 1.80 -3 3 -10 31.70 3.60 3 -3 10 36.50 2.40 3 -3 10 30.90 2.70 3 -3 10 33.50 2.90 3 -3 10 34.10 2.40 3 -3 10 33.60 2.20 3 -3 10 36.50 2.70 3 -3 10 38.00 2.30 3 -3 10 34.70 2.40 4 -3 10 9.90 1.20 4 -3 10 11.00 1.70 4 -3 10 11.80 1.60 4 -3 10 5.90 1.20 4 -3 10 9.80 1.30 4 -3 10 9.00 1.30 5 -3 10 3.40 0.90 5 -3 10 3.90 0.70 5 2 -10 3.50 0.70 -5 -2 10 2.30 0.60 -5 -2 10 2.80 0.40 4 2 -10 10.70 1.70 4 2 -10 6.00 1.10 -4 -2 10 7.60 1.00 -4 -2 10 7.90 1.20 3 2 -10 11.30 3.60 3 2 -10 8.80 3.30 3 2 -10 12.20 1.70 -3 -2 10 10.70 1.70 -3 -2 10 11.00 1.30 -3 -2 10 10.70 1.50 -3 -2 10 14.70 3.70 2 2 -10 19.20 4.50 -2 -2 10 19.60 2.20 -2 -2 10 17.20 3.60 -2 -2 10 21.10 1.50 -2 -2 10 18.90 1.70 1 2 -10 215.98 11.60 1 2 -10 201.18 11.00 1 2 -10 193.08 11.70 -1 -2 10 213.18 12.00 0 2 -10 51.39 4.60 0 2 -10 59.89 4.60 -1 2 -10 223.88 10.80 -1 2 -10 197.58 10.40 -2 2 -10 17.20 2.60 2 -2 10 19.70 2.20 2 -2 10 17.20 1.60 2 -2 10 14.30 1.70 2 -2 10 18.10 1.40 2 -2 10 22.90 2.20 2 -2 10 18.40 1.60 2 -2 10 19.50 1.60 2 -2 10 22.90 2.00 -3 2 -10 12.50 2.50 3 -2 10 10.70 1.40 3 -2 10 12.80 1.40 3 -2 10 14.40 1.40 3 -2 10 10.30 1.20 3 -2 10 12.90 1.80 3 -2 10 16.10 1.40 3 -2 10 13.30 2.00 3 -2 10 14.50 2.00 3 -2 10 13.40 1.70 3 -2 10 15.10 1.40 4 -2 10 10.30 1.20 4 -2 10 10.30 1.30 4 -2 10 7.70 1.00 4 -2 10 7.40 1.50 4 -2 10 9.50 1.50 4 -2 10 9.10 1.10 4 -2 10 8.60 1.30 4 -2 10 8.10 1.30 5 -2 10 2.60 0.90 5 -2 10 2.70 0.70 5 1 -10 6.40 0.80 -5 -1 10 7.00 0.60 -5 -1 10 6.90 0.80 4 1 -10 33.80 2.70 4 1 -10 27.00 2.10 -4 -1 10 32.50 2.20 -4 -1 10 32.30 2.00 3 1 -10 5.40 2.70 3 1 -10 7.20 1.40 3 1 -10 6.80 3.00 -3 -1 10 7.80 1.50 -3 -1 10 5.10 1.10 -3 -1 10 5.60 2.30 -3 -1 10 5.90 1.00 2 1 -10 13.10 2.70 2 1 -10 21.60 4.30 -2 -1 10 23.50 1.60 -2 -1 10 25.50 4.30 -2 -1 10 23.20 1.80 -2 -1 10 20.40 2.00 1 1 -10 23.00 3.80 1 1 -10 32.20 4.20 -1 -1 10 22.00 3.80 0 1 -10 101.39 6.60 0 1 -10 123.99 7.10 0 -1 10 115.79 7.60 -1 1 -10 21.30 2.80 -2 1 -10 26.20 2.80 2 -1 10 23.50 1.70 2 -1 10 21.60 1.70 2 -1 10 26.80 2.20 2 -1 10 22.90 1.70 2 -1 10 26.00 2.40 2 -1 10 22.40 2.20 2 -1 10 24.50 2.10 2 -1 10 22.30 1.80 2 -1 10 21.90 1.60 -3 1 -10 8.20 2.50 3 -1 10 5.10 1.00 3 -1 10 7.90 1.10 3 -1 10 7.30 1.10 3 -1 10 5.80 1.10 3 -1 10 6.50 1.30 3 -1 10 6.20 1.40 3 -1 10 7.50 1.20 3 -1 10 7.30 1.50 3 -1 10 8.10 1.50 3 -1 10 6.80 1.10 3 -1 10 10.60 1.60 4 -1 10 34.70 2.10 4 -1 10 36.50 2.30 4 -1 10 31.90 2.60 4 -1 10 32.00 2.30 4 -1 10 32.50 2.00 4 -1 10 36.60 3.00 4 -1 10 34.50 2.10 4 -1 10 34.90 2.30 4 -1 10 35.20 2.60 5 -1 10 10.00 1.00 5 -1 10 6.20 1.50 5 0 -10 18.30 1.50 -5 0 10 17.10 1.00 -5 0 10 15.30 1.20 4 0 -10 5.90 1.10 4 0 -10 4.60 1.20 -4 0 10 5.70 0.90 -4 0 10 6.10 1.10 3 0 -10 43.20 6.50 3 0 -10 39.40 2.70 3 0 -10 27.20 5.50 3 0 -10 44.30 3.10 -3 0 10 42.60 3.10 -3 0 10 42.30 2.70 -3 0 10 40.60 2.40 2 0 -10 16.20 3.90 2 0 -10 11.40 3.30 2 0 -10 14.80 2.90 -2 0 10 13.20 1.20 -2 0 10 14.90 3.20 -2 0 10 10.80 1.60 -2 0 10 11.50 1.40 1 0 -10 2.20 1.70 1 0 -10 0.50 1.00 -1 0 10 -0.10 0.80 0 0 -10 183.08 9.60 0 0 -10 175.88 10.10 -1 0 -10 0.90 1.00 -2 0 -10 10.60 2.00 2 0 10 9.00 1.50 2 0 10 15.20 1.90 2 0 10 8.50 1.20 2 0 10 9.30 1.50 2 0 10 13.30 2.00 2 0 10 12.90 1.60 2 0 10 13.40 1.70 2 0 10 13.20 1.10 2 0 10 12.50 1.50 2 0 10 12.70 1.30 -3 0 -10 40.20 5.50 3 0 10 42.60 2.60 3 0 10 46.30 2.60 3 0 10 43.60 3.00 3 0 10 38.00 2.80 3 0 10 46.80 3.40 3 0 10 46.50 2.70 3 0 10 45.50 3.10 3 0 10 44.70 2.80 3 0 10 41.90 2.90 3 0 10 37.90 2.50 3 0 10 37.90 2.60 3 0 10 43.40 2.40 4 0 10 5.10 1.00 4 0 10 6.30 1.30 4 0 10 5.20 0.90 4 0 10 6.50 0.90 4 0 10 5.20 0.90 4 0 10 3.70 1.10 4 0 10 7.20 1.40 4 0 10 5.80 1.00 4 0 10 3.60 1.40 4 0 10 5.80 0.90 4 0 10 4.00 0.90 4 0 10 3.40 1.00 5 0 10 15.70 1.30 -5 1 10 7.40 0.80 -5 1 10 6.00 0.60 4 -1 -10 33.00 2.50 -4 1 10 31.60 2.20 -4 1 10 29.30 1.90 3 -1 -10 8.00 1.30 3 -1 -10 9.10 1.50 -3 1 10 7.00 1.50 -3 1 10 7.50 1.30 -3 1 10 8.20 1.10 2 -1 -10 26.30 4.90 2 -1 -10 29.60 4.10 2 -1 -10 29.90 5.10 -2 1 10 24.50 2.10 -2 1 10 21.60 1.80 -2 1 10 24.60 1.60 1 -1 -10 37.60 7.00 1 -1 -10 20.60 3.40 0 -1 -10 106.69 6.70 0 -1 -10 115.19 7.40 -1 -1 -10 25.30 2.70 -1 -1 -10 24.20 3.70 -2 -1 -10 22.30 2.50 -2 -1 -10 24.60 3.90 2 1 10 26.10 2.50 2 1 10 24.40 1.80 2 1 10 24.50 2.20 2 1 10 28.20 2.40 2 1 10 25.00 2.10 2 1 10 23.70 1.60 2 1 10 26.00 2.10 2 1 10 20.50 1.80 -3 -1 -10 8.30 2.70 3 1 10 6.30 1.10 3 1 10 7.50 1.00 3 1 10 7.90 1.30 3 1 10 7.00 1.70 3 1 10 7.10 1.40 3 1 10 6.80 1.20 3 1 10 7.50 1.00 3 1 10 7.40 1.50 3 1 10 5.60 1.10 3 1 10 8.20 1.40 3 1 10 7.40 1.20 3 1 10 6.40 1.10 4 1 10 33.70 2.10 4 1 10 30.50 2.10 4 1 10 34.90 2.40 4 1 10 36.80 3.10 4 1 10 31.40 2.60 4 1 10 37.40 2.10 4 1 10 33.20 2.40 4 1 10 34.90 2.30 4 1 10 35.70 2.20 4 1 10 34.90 2.80 4 1 10 34.50 2.20 -5 2 10 3.20 0.60 -5 2 10 3.80 0.40 4 -2 -10 7.00 1.20 -4 2 10 8.30 1.20 -4 2 10 6.40 0.80 3 -2 -10 9.60 3.20 3 -2 -10 11.90 1.70 -3 2 10 10.60 1.40 -3 2 10 11.30 1.20 -3 2 10 13.40 1.80 2 -2 -10 25.80 3.90 2 -2 -10 20.30 4.40 2 -2 -10 14.30 3.40 -2 2 10 18.60 2.10 -2 2 10 18.00 1.30 -2 2 10 15.70 1.50 -1 2 10 283.47 13.10 0 -2 -10 55.39 4.40 -1 -2 -10 187.18 9.90 -1 -2 -10 207.48 11.70 1 2 10 213.08 8.90 1 2 10 222.48 9.40 1 2 10 213.78 9.60 -2 -2 -10 19.10 3.70 2 2 10 14.40 1.70 2 2 10 19.40 2.20 2 2 10 15.20 2.00 2 2 10 16.10 1.30 2 2 10 20.80 2.00 2 2 10 23.30 2.20 2 2 10 20.10 1.80 2 2 10 17.90 1.70 2 2 10 19.30 2.10 3 2 10 9.20 1.20 3 2 10 11.90 1.50 3 2 10 13.40 1.50 3 2 10 11.90 1.50 3 2 10 17.10 2.10 3 2 10 12.40 1.50 3 2 10 14.10 1.70 3 2 10 13.60 2.30 3 2 10 10.30 1.10 3 2 10 13.10 1.80 3 2 10 11.50 1.60 3 2 10 12.70 1.50 4 2 10 8.90 1.30 4 2 10 8.80 1.20 4 2 10 8.30 1.00 4 2 10 9.00 1.20 4 2 10 8.00 1.40 4 2 10 8.70 1.20 4 2 10 9.60 1.20 4 2 10 6.90 1.60 4 2 10 9.40 1.50 4 2 10 8.80 1.20 4 2 10 8.40 1.60 4 2 10 8.80 1.10 -5 3 10 4.30 0.60 4 -3 -10 9.80 1.30 -4 3 10 9.60 0.90 -4 3 10 8.10 1.10 -3 3 10 31.90 2.60 -3 3 10 34.60 1.90 -3 3 10 32.00 2.20 2 -3 -10 26.30 4.10 2 -3 -10 29.50 5.20 2 -3 -10 20.50 4.10 -2 3 10 25.40 2.20 -2 3 10 26.50 1.60 -2 3 10 27.10 1.90 1 -3 -10 63.79 5.40 1 -3 -10 63.89 4.90 1 -3 -10 61.09 6.10 -1 3 10 72.49 3.70 0 -3 -10 40.70 3.70 0 -3 -10 51.49 4.60 -1 -3 -10 68.79 5.60 1 3 10 67.19 3.50 1 3 10 71.59 4.20 1 3 10 65.39 3.30 1 3 10 66.89 4.10 1 3 10 66.29 3.60 -2 -3 -10 20.30 3.60 2 3 10 25.30 2.10 2 3 10 21.40 2.20 2 3 10 21.80 1.90 2 3 10 20.40 2.30 2 3 10 23.10 1.90 2 3 10 28.10 2.20 2 3 10 22.60 1.80 2 3 10 22.00 1.90 2 3 10 23.50 2.50 2 3 10 20.70 1.50 -3 -3 -10 17.20 4.60 3 3 10 30.60 2.40 3 3 10 30.30 2.30 3 3 10 32.60 2.00 3 3 10 31.20 2.70 3 3 10 30.50 2.20 3 3 10 33.00 2.50 3 3 10 29.40 3.00 3 3 10 29.80 2.20 3 3 10 33.10 2.40 3 3 10 30.80 2.80 3 3 10 34.10 2.30 4 3 10 9.70 1.60 4 3 10 10.30 1.40 4 3 10 9.60 1.20 4 3 10 9.30 1.20 4 3 10 8.60 1.70 4 3 10 9.40 1.20 4 3 10 9.40 1.30 4 3 10 10.10 1.10 4 3 10 10.70 1.50 4 3 10 9.50 1.80 4 3 10 10.80 1.30 4 -4 -10 8.90 1.30 -4 4 10 9.80 1.20 -4 4 10 10.60 0.90 -3 4 10 29.00 2.10 -3 4 10 30.60 1.70 -3 4 10 29.90 2.50 2 -4 -10 69.59 6.00 -2 4 10 77.49 3.90 -2 4 10 78.69 3.50 -2 4 10 76.59 4.30 1 -4 -10 48.10 4.70 1 -4 -10 47.80 4.60 -1 4 10 46.10 2.50 0 -4 -10 143.29 7.90 0 -4 -10 143.99 9.10 0 4 10 146.69 6.80 0 4 10 141.89 6.50 -1 -4 -10 43.50 4.50 1 4 10 46.50 2.90 1 4 10 42.50 2.70 1 4 10 48.10 3.40 1 4 10 42.10 3.30 1 4 10 47.80 2.80 -2 -4 -10 72.89 6.20 2 4 10 73.59 3.90 2 4 10 70.99 4.70 2 4 10 76.09 4.20 2 4 10 75.49 4.10 2 4 10 75.19 3.80 2 4 10 71.49 3.90 2 4 10 64.09 3.60 2 4 10 70.29 4.40 2 4 10 76.99 4.10 3 4 10 25.10 2.70 3 4 10 29.20 1.90 3 4 10 26.90 2.50 3 4 10 28.70 2.30 3 4 10 31.90 2.30 3 4 10 32.50 2.50 3 4 10 25.60 2.20 3 4 10 32.90 3.10 3 4 10 27.90 2.10 3 4 10 27.70 2.20 3 4 10 30.90 2.30 4 4 10 11.10 1.30 4 4 10 10.20 1.00 4 4 10 10.90 1.40 4 4 10 11.10 1.60 4 4 10 9.40 1.80 4 4 10 10.20 1.20 4 4 10 10.50 1.70 4 4 10 11.90 1.40 4 4 10 10.40 1.40 4 4 10 9.10 1.40 4 4 10 9.40 1.20 4 -5 -10 6.50 1.20 -4 5 10 7.00 0.70 -4 5 10 7.50 1.00 3 -5 -10 28.00 1.90 -3 5 10 29.00 2.00 -3 5 10 29.00 1.60 -3 5 10 29.40 2.40 2 -5 -10 74.39 3.60 2 -5 -10 66.49 6.30 -2 5 10 86.29 3.50 -2 5 10 75.19 3.90 -2 5 10 79.59 4.30 1 -5 -10 52.99 5.10 -1 5 10 54.79 3.20 0 -5 -10 42.50 4.60 0 5 10 40.10 2.30 0 5 10 43.10 2.50 -1 -5 -10 50.19 4.90 1 5 10 48.10 3.50 1 5 10 50.89 3.00 1 5 10 50.79 3.00 1 5 10 47.00 3.20 1 5 10 50.49 2.80 1 5 10 51.19 2.90 1 5 10 40.70 3.40 -2 -5 -10 72.39 6.20 2 5 10 74.29 4.20 2 5 10 80.79 4.30 2 5 10 73.39 4.00 2 5 10 77.79 4.20 2 5 10 63.99 4.40 2 5 10 71.79 3.90 2 5 10 73.89 4.30 3 5 10 29.10 2.60 3 5 10 27.00 2.20 3 5 10 28.90 2.20 3 5 10 27.70 2.30 3 5 10 27.60 1.80 3 5 10 31.90 2.30 3 5 10 30.10 2.20 3 5 10 28.40 3.00 3 5 10 32.90 2.60 3 5 10 32.90 2.60 3 5 10 30.90 2.90 4 5 10 8.70 1.90 4 5 10 7.20 1.00 4 5 10 8.80 1.50 4 5 10 7.40 0.90 4 5 10 6.40 1.00 4 5 10 5.50 1.20 4 5 10 6.10 1.00 4 5 10 8.20 1.10 4 5 10 5.10 1.10 4 -6 -10 0.40 0.80 -4 6 10 0.50 0.90 3 -6 -10 57.79 3.10 -3 6 10 59.59 3.60 -3 6 10 46.20 3.20 2 -6 -10 37.70 5.60 -2 6 10 39.00 2.30 -2 6 10 40.00 2.70 1 -6 -10 155.68 10.30 -1 6 10 154.38 6.90 -1 6 10 166.68 7.00 -1 6 10 171.58 7.50 0 -6 -10 20.00 3.80 0 6 10 18.50 1.50 0 6 10 20.00 1.70 0 6 10 23.90 2.60 0 6 10 17.50 1.60 0 6 10 18.60 1.80 -1 -6 -10 162.48 10.30 1 6 10 161.98 7.30 1 6 10 171.68 7.40 1 6 10 170.58 7.50 1 6 10 172.28 7.30 1 6 10 157.38 7.50 1 6 10 155.78 7.40 1 6 10 154.48 8.10 -2 -6 -10 41.90 5.50 2 6 10 41.10 2.90 2 6 10 43.40 2.80 2 6 10 45.30 3.60 2 6 10 39.20 2.70 2 6 10 35.00 2.70 2 6 10 41.20 2.90 2 6 10 41.40 2.90 2 6 10 35.70 3.10 2 6 10 40.20 2.60 3 6 10 43.10 4.30 3 6 10 51.59 3.10 3 6 10 56.79 3.00 3 6 10 50.69 3.70 3 6 10 51.79 3.40 3 6 10 46.50 3.40 4 6 10 0.10 1.10 4 6 10 2.10 1.10 4 6 10 0.90 0.70 4 6 10 0.80 1.00 4 6 10 0.50 0.50 4 6 10 0.60 0.60 4 6 10 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3 -1 13 19.40 1.80 3 -1 13 16.90 1.70 3 -1 13 23.30 2.50 4 -1 13 6.40 1.30 4 -1 13 7.60 1.10 4 -1 13 7.40 1.40 4 0 -13 25.30 1.80 -4 0 13 22.40 2.00 -4 0 13 27.10 1.70 3 0 -13 37.00 2.50 3 0 -13 40.30 2.80 -3 0 13 43.50 3.00 -3 0 13 40.30 2.00 -3 0 13 41.50 2.60 2 0 -13 42.90 6.40 -2 0 13 38.60 2.90 -2 0 13 43.30 2.50 1 0 -13 213.58 14.80 1 0 -13 209.88 14.60 -1 0 13 225.38 9.40 -1 0 13 223.58 10.00 0 0 -13 136.09 8.90 0 0 -13 132.19 9.50 0 0 13 142.79 6.40 0 0 13 138.49 6.20 0 0 13 133.09 6.70 0 0 13 128.49 7.00 -1 0 -13 216.08 11.90 -1 0 -13 210.48 13.10 1 0 13 214.88 9.50 1 0 13 224.38 9.30 1 0 13 220.28 9.70 1 0 13 219.98 10.30 1 0 13 220.88 9.20 1 0 13 215.98 10.20 -2 0 -13 33.20 5.40 2 0 13 39.50 2.70 2 0 13 44.60 3.10 2 0 13 42.30 3.30 2 0 13 40.90 3.30 2 0 13 39.90 2.50 3 0 13 40.20 3.20 3 0 13 39.80 2.60 3 0 13 39.00 2.20 3 0 13 39.10 3.30 3 0 13 42.10 2.90 3 0 13 33.70 2.30 3 0 13 39.70 2.50 4 0 13 31.30 2.30 4 0 13 29.60 2.10 4 0 13 28.70 2.30 -4 1 13 6.60 1.10 -4 1 13 5.40 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42.40 2.90 3 -6 14 5.80 1.30 3 -6 14 5.40 1.30 3 5 -14 12.00 1.40 -3 -5 14 10.20 1.40 -2 -5 14 22.00 1.80 -2 -5 14 22.00 2.20 1 5 -14 38.40 5.70 -1 -5 14 36.50 6.00 -1 -5 14 37.60 2.30 -1 -5 14 39.10 2.80 0 5 -14 47.00 8.30 0 5 -14 74.19 11.40 0 -5 14 56.29 3.80 0 -5 14 60.09 3.20 0 -5 14 56.19 3.40 -1 5 -14 31.60 4.90 1 -5 14 44.50 3.30 1 -5 14 35.40 2.70 1 -5 14 36.20 2.30 1 -5 14 43.80 2.50 1 -5 14 36.70 3.00 2 -5 14 22.00 2.40 2 -5 14 23.30 2.50 2 -5 14 20.60 2.10 3 -5 14 12.10 2.20 3 -5 14 15.50 2.10 4 4 -14 1.80 0.70 -4 -4 14 1.40 0.50 3 4 -14 16.00 1.70 -3 -4 14 16.20 1.40 -3 -4 14 22.10 2.60 -2 -4 14 6.40 1.10 -2 -4 14 5.80 1.30 1 4 -14 29.90 6.60 -1 -4 14 41.60 2.90 -1 -4 14 42.70 2.40 0 4 -14 8.00 2.80 0 4 -14 12.30 3.40 0 -4 14 7.00 1.20 0 -4 14 7.40 1.50 0 -4 14 9.80 1.70 0 -4 14 5.80 1.20 1 -4 14 40.10 3.20 1 -4 14 40.50 2.70 1 -4 14 41.80 2.40 1 -4 14 44.00 2.50 1 -4 14 35.50 3.10 2 -4 14 10.20 1.70 2 -4 14 7.10 1.50 2 -4 14 8.50 1.70 3 -4 14 20.50 2.30 3 -4 14 21.70 2.00 3 -4 14 22.60 2.30 4 -4 14 2.50 1.00 4 -4 14 1.60 0.80 4 3 -14 17.10 1.40 3 3 -14 18.40 1.70 3 3 -14 19.00 2.00 -3 -3 14 21.00 1.50 -3 -3 14 20.50 2.10 -2 -3 14 16.90 2.30 1 3 -14 28.20 4.70 1 3 -14 51.19 7.10 -1 -3 14 40.10 2.80 -1 -3 14 41.30 2.40 0 3 -14 39.70 5.80 0 3 -14 27.20 4.80 0 -3 14 33.90 2.80 0 -3 14 30.90 2.80 0 -3 14 34.30 2.40 0 -3 14 36.50 2.40 -1 3 -14 35.40 5.60 -1 3 -14 44.30 4.80 1 -3 14 36.00 3.10 1 -3 14 38.40 2.30 1 -3 14 39.40 2.30 1 -3 14 36.60 3.10 1 -3 14 40.90 2.60 2 -3 14 16.60 2.30 2 -3 14 14.40 1.70 2 -3 14 16.00 2.20 3 -3 14 21.40 2.40 3 -3 14 21.50 2.40 3 -3 14 21.90 2.10 4 -3 14 15.10 1.70 4 -3 14 16.90 1.70 4 2 -14 2.40 0.80 -4 -2 14 2.30 0.60 3 2 -14 8.30 1.20 3 2 -14 11.20 1.60 -3 -2 14 13.30 1.70 -3 -2 14 15.70 1.30 -2 -2 14 53.69 3.00 -2 -2 14 51.19 3.40 1 2 -14 36.30 5.40 1 2 -14 55.69 6.00 -1 -2 14 51.19 2.70 -1 -2 14 49.99 3.20 0 2 -14 21.40 4.30 0 2 -14 19.30 3.90 0 -2 14 17.80 2.30 0 -2 14 21.00 2.50 0 -2 14 17.40 1.70 0 -2 14 22.00 1.90 -1 2 -14 44.10 4.80 -1 2 -14 45.20 6.10 1 -2 14 45.90 3.00 1 -2 14 49.10 3.60 1 -2 14 45.80 3.50 1 -2 14 47.20 2.60 1 -2 14 47.10 2.60 2 -2 14 56.09 3.30 2 -2 14 54.79 3.00 2 -2 14 49.70 3.70 2 -2 14 52.99 3.80 3 -2 14 12.40 1.70 3 -2 14 14.00 2.10 3 -2 14 10.60 1.90 4 -2 14 2.40 1.20 4 -2 14 2.90 1.10 4 -2 14 4.80 1.20 -4 -1 14 1.10 0.50 3 1 -14 2.20 1.00 -3 -1 14 5.30 0.90 -3 -1 14 4.40 1.20 2 1 -14 31.50 5.90 -2 -1 14 37.80 2.40 -2 -1 14 35.20 2.70 1 1 -14 8.10 2.90 1 1 -14 6.10 2.40 -1 -1 14 4.20 1.10 -1 -1 14 4.90 0.90 0 1 -14 242.78 14.00 0 1 -14 247.68 14.80 0 -1 14 242.88 11.60 0 -1 14 258.97 10.80 0 -1 14 250.47 10.60 0 -1 14 263.27 11.00 -1 1 -14 7.10 2.30 -1 1 -14 9.20 2.90 1 -1 14 4.60 0.80 1 -1 14 4.70 0.80 1 -1 14 4.60 1.40 1 -1 14 5.60 1.50 1 -1 14 3.60 1.20 -2 1 -14 27.60 6.10 2 -1 14 39.00 2.50 2 -1 14 36.30 2.80 2 -1 14 38.00 3.20 2 -1 14 38.10 3.20 3 -1 14 4.70 1.50 3 -1 14 4.90 1.00 3 -1 14 4.20 1.10 3 -1 14 3.20 1.30 4 -1 14 1.10 0.90 4 -1 14 0.30 0.90 4 -1 14 1.80 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17 16.30 1.60 -1 -6 -17 10.00 1.10 1 6 17 13.80 1.50 1 6 17 7.90 1.60 1 6 17 7.20 1.50 1 6 17 12.40 1.30 1 6 17 10.00 1.20 -2 -6 -17 2.60 0.60 2 6 17 2.40 1.70 2 6 17 4.40 0.80 2 6 17 2.00 0.80 2 -7 -17 14.20 1.00 -2 7 17 12.60 1.20 1 -7 -17 2.30 0.70 1 -7 -17 2.90 0.60 -1 7 17 2.20 0.70 -1 7 17 2.10 0.60 0 -7 -17 8.80 1.00 0 7 17 9.00 1.30 0 7 17 9.60 1.10 -1 -7 -17 3.50 0.80 1 7 17 2.70 0.80 1 7 17 3.40 0.80 1 7 17 3.60 0.80 1 7 17 3.00 1.10 -2 -7 -17 13.30 1.00 2 7 17 13.00 1.60 2 7 17 13.00 1.20 2 7 17 15.20 1.80 1 -8 -17 4.80 0.80 -1 8 17 3.50 0.70 0 -8 -17 2.60 0.70 0 -8 -17 3.50 0.60 0 8 17 3.60 0.70 0 8 17 4.00 0.90 0 8 17 3.00 0.80 -1 -8 -17 5.30 0.70 -1 -8 -17 6.40 0.80 1 8 17 5.40 0.90 1 8 17 6.20 1.50 1 8 17 4.10 0.90 1 -9 -17 6.40 0.80 -1 9 17 6.10 0.90 0 -9 -17 4.80 1.10 0 -9 -17 5.80 0.70 0 9 17 4.10 0.80 -1 -9 -17 7.50 0.80 1 9 17 5.20 0.80 1 9 17 6.80 0.80 -1 -8 18 2.60 0.50 -1 -7 18 2.30 0.70 -1 -7 18 2.50 0.80 0 -7 18 24.40 1.90 1 -7 18 3.20 0.80 2 6 -18 2.80 0.80 -2 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2.30 1 1 18 35.90 2.70 2 1 18 5.60 1.30 2 1 18 4.90 1.10 2 1 18 7.20 0.90 -2 2 18 6.30 0.90 -2 2 18 6.90 1.00 -2 2 18 5.00 0.80 -2 2 18 6.20 0.80 -1 2 18 13.10 1.50 -1 2 18 14.20 1.50 -1 2 18 12.30 1.30 -1 2 18 13.60 1.60 0 2 18 3.90 1.10 0 2 18 2.20 0.60 0 2 18 1.90 0.80 0 2 18 1.60 0.80 1 2 18 14.40 1.50 1 2 18 15.20 1.40 1 2 18 15.60 1.90 1 2 18 15.10 2.10 2 2 18 6.20 0.90 2 2 18 7.30 1.20 2 2 18 5.70 1.30 -2 3 18 4.80 0.80 -2 3 18 6.20 1.00 -2 3 18 6.00 0.90 -2 3 18 4.20 0.70 -1 3 18 5.20 0.80 -1 3 18 3.30 0.70 -1 3 18 5.50 1.10 -1 3 18 4.30 1.00 0 3 18 13.90 1.40 0 3 18 13.90 2.20 0 3 18 12.20 1.40 1 3 18 3.50 0.90 1 3 18 3.90 1.10 1 3 18 5.50 1.30 1 3 18 2.60 1.30 2 3 18 5.40 1.10 2 3 18 6.30 0.90 2 3 18 5.00 1.30 -2 4 18 5.50 0.70 -2 4 18 3.90 0.70 -2 4 18 3.60 0.60 -1 4 18 17.80 1.40 -1 4 18 17.40 1.70 -1 4 18 18.00 1.30 -1 4 18 16.00 1.40 0 4 18 2.70 1.00 0 4 18 3.10 0.90 0 4 18 2.00 0.80 1 4 18 17.90 1.80 1 4 18 19.20 1.60 1 4 18 20.10 1.70 2 4 18 7.60 1.10 2 4 18 2.70 0.90 2 4 18 4.30 0.80 2 4 18 4.80 1.10 2 -5 -18 9.50 0.90 -2 5 18 10.20 1.00 1 -5 -18 10.00 0.90 -1 5 18 11.10 1.20 -1 5 18 8.80 1.00 -1 5 18 9.20 1.00 0 5 18 18.10 1.50 0 5 18 18.80 1.50 0 5 18 18.60 1.80 1 5 18 8.80 1.20 1 5 18 9.60 1.10 1 5 18 8.20 1.20 2 5 18 8.20 1.10 2 5 18 8.20 1.20 2 5 18 9.80 1.10 2 -6 -18 2.00 0.50 -2 6 18 1.40 0.50 1 -6 -18 5.00 0.70 -1 6 18 4.60 0.80 -1 6 18 4.20 0.70 0 6 18 3.00 0.70 0 6 18 1.80 0.60 0 6 18 4.00 0.90 -1 -6 -18 4.70 0.70 1 6 18 6.30 1.00 1 6 18 4.90 0.90 1 6 18 6.10 0.90 -2 -6 -18 1.90 0.40 2 6 18 2.40 0.80 2 6 18 2.30 0.60 2 6 18 1.70 0.70 1 -7 -18 4.00 0.70 -1 7 18 2.20 0.60 0 -7 -18 25.00 1.60 0 -7 -18 23.50 1.50 0 7 18 27.80 1.80 0 7 18 24.90 1.60 1 7 18 3.10 0.70 1 7 18 3.80 0.70 1 -8 -18 3.70 0.60 -1 8 18 2.00 0.50 0 -8 -18 1.60 0.50 0 -8 -18 1.00 0.40 0 8 18 1.00 0.50 -1 -8 -18 4.60 0.60 1 8 18 3.00 0.60 1 8 18 3.60 0.70 -1 -6 19 4.20 0.90 0 -6 19 1.90 0.80 -1 -5 19 2.60 0.70 -1 -5 19 2.20 0.50 -1 -5 19 3.40 0.60 0 -5 19 6.50 0.90 0 -5 19 6.40 1.00 -1 -4 19 0.20 0.30 -1 -4 19 0.40 0.50 -1 -4 19 0.90 0.70 0 -4 19 0.40 0.50 1 -4 19 1.90 0.80 -2 -3 19 3.50 0.70 -2 -3 19 3.10 0.50 -2 -3 19 2.60 0.50 -1 -3 19 9.20 1.20 -1 -3 19 8.50 0.90 -1 -3 19 11.50 1.00 0 -3 19 9.60 1.20 0 -3 19 11.00 1.10 1 -3 19 10.50 1.00 1 -3 19 12.00 1.30 2 -3 19 4.50 1.00 -2 -2 19 11.70 1.10 -2 -2 19 11.80 1.20 -2 -2 19 13.20 1.00 -1 -2 19 2.00 0.80 -1 -2 19 1.60 0.50 -1 -2 19 2.80 0.70 0 -2 19 4.10 1.00 0 -2 19 4.80 0.70 1 -2 19 2.00 0.80 1 -2 19 3.20 0.90 1 -2 19 2.70 0.80 2 -2 19 12.90 1.50 2 -2 19 12.90 1.30 -2 -1 19 2.70 0.70 -2 -1 19 1.50 0.70 -2 -1 19 2.60 0.50 -1 -1 19 9.00 0.90 -1 -1 19 9.10 1.00 -1 -1 19 6.80 1.10 0 -1 19 1.00 0.70 0 -1 19 2.00 0.90 1 -1 19 9.60 1.00 1 -1 19 10.90 1.30 1 -1 19 9.30 1.30 2 -1 19 3.50 0.90 2 -1 19 1.60 0.70 -2 0 19 21.90 1.50 -2 0 19 20.10 1.30 -2 0 19 16.10 1.50 -1 0 19 2.80 0.60 -1 0 19 2.50 0.90 -1 0 19 2.80 0.70 0 0 19 1.30 0.90 0 0 19 0.80 0.70 1 0 19 3.70 1.00 1 0 19 3.90 0.70 2 0 19 19.70 1.70 2 0 19 21.30 1.40 2 0 19 23.60 1.80 -2 1 19 3.10 0.60 -2 1 19 2.60 0.70 -2 1 19 1.80 0.60 -1 1 19 8.50 0.80 -1 1 19 7.30 0.90 -1 1 19 8.00 1.10 -1 1 19 8.10 1.10 0 1 19 1.20 0.90 0 1 19 3.20 0.80 1 1 19 8.60 1.30 1 1 19 9.60 1.10 2 1 19 2.60 0.60 2 1 19 1.90 0.80 2 1 19 2.90 0.90 -2 2 19 13.30 1.00 -2 2 19 12.00 1.00 -2 2 19 10.30 1.10 -1 2 19 2.50 0.50 -1 2 19 3.20 0.70 -1 2 19 1.90 0.60 -1 2 19 1.40 0.80 0 2 19 3.80 1.00 0 2 19 3.10 0.80 0 2 19 3.90 0.70 1 2 19 3.80 1.10 1 2 19 1.90 0.70 2 2 19 12.80 1.30 2 2 19 13.60 1.20 -2 3 19 2.20 0.60 -2 3 19 4.60 0.60 1 -3 -19 10.10 1.00 -1 3 19 9.90 1.00 -1 3 19 11.90 0.90 -1 3 19 7.80 0.90 0 3 19 9.00 1.10 0 3 19 10.20 1.10 0 3 19 10.50 1.30 1 3 19 9.60 1.20 1 3 19 10.30 1.10 2 3 19 3.80 0.70 2 3 19 4.40 0.90 1 -4 -19 0.60 0.40 -1 4 19 1.60 0.70 -1 4 19 1.80 0.90 -1 4 19 0.10 0.50 0 4 19 -0.50 0.80 0 4 19 0.60 0.80 0 4 19 -0.10 0.60 1 4 19 0.00 0.60 1 4 19 0.20 1.30 1 4 19 1.90 0.90 -1 5 19 2.70 0.70 -1 5 19 2.70 0.60 0 5 19 7.90 1.00 0 5 19 6.50 1.00 0 5 19 8.80 1.00 1 5 19 2.90 0.80 1 5 19 3.60 0.80 1 5 19 2.90 0.70 1 -6 -19 5.10 0.70 -1 6 19 3.40 0.60 0 -6 -19 2.80 0.50 0 -6 -19 1.60 0.50 0 6 19 1.40 0.60 0 6 19 3.20 0.60 -1 -6 -19 3.90 0.50 1 6 19 4.80 0.70 1 6 19 3.90 0.70 0 -4 20 19.50 1.40 0 -3 20 -0.20 0.50 0 -3 20 0.10 0.60 -1 -2 20 6.00 0.70 -1 -2 20 5.00 0.80 0 -2 20 -0.20 1.50 0 -2 20 1.90 0.60 1 -2 20 6.60 0.90 1 -2 20 7.10 0.90 -1 -1 20 5.10 0.70 -1 -1 20 4.40 0.80 0 -1 20 17.10 1.90 0 -1 20 16.60 1.60 1 -1 20 5.80 0.70 1 -1 20 6.90 1.00 -1 0 20 16.10 1.20 -1 0 20 18.30 1.50 0 0 20 3.60 0.90 0 0 20 3.30 0.80 1 0 20 19.60 1.60 1 0 20 19.00 1.30 -1 1 20 5.60 0.70 -1 1 20 5.90 0.90 0 1 20 15.00 1.30 0 1 20 17.20 1.70 1 1 20 5.40 0.90 1 1 20 6.10 0.80 -1 2 20 5.90 0.80 -1 2 20 5.40 0.70 0 2 20 2.20 0.80 0 2 20 3.10 0.90 1 2 20 5.50 0.80 1 2 20 7.40 1.00 0 3 20 0.10 0.50 0 3 20 0.80 0.70 0 -4 -20 18.90 1.10 0 4 20 18.40 1.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 51609 _shelx_res_file ; TITL p21_a.res in P2(1) as2301a.res created by SHELXL-2019/3 at 11:53:53 on 18-Jun-2024 REM Old TITL p21 in P2(1) REM SHELXT solution in P2(1): R1 0.354, Rweak 0.260, Alpha 0.048 REM 0.880 for 9 systematic absences, Orientation as input REM Flack x = 0.417 ( 0.063 ) from 2075 Parsons' quotients REM Formula found by SHELXT: C18 N6 O8 CELL 1.54178 4.7599 14.3223 16.6515 90.000 90.022 90.000 ZERR 2.000 0.0001 0.0005 0.0005 0.000 0.002 0.000 LATT -1 SYMM -X, 1/2+Y, -Z SFAC C H N O UNIT 36 68 4 24 TEMP -13.150 SIZE 0.022 0.039 0.258 L.S. 10 BOND $H FMAP 2 PLAN -20 TWIN -1 0 0 0 1 0 0 0 1 CONF EQIV $1 -x+1, y+1/2, -z+2 HTAB O6 O8_$1 EQIV $2 x+1, y, z HTAB N1 O8_$2 EQIV $3 -x+1, y-1/2, -z+2 HTAB C9 O5_$3 HTAB C9 O8_$2 EQIV $4 -x+1, y+1/2, -z+1 HTAB O3' O6'_$4 HTAB O3 O5' HTAB O3 O6' HTAB O4' O1S EQIV $5 -x+2, y-1/2, -z+1 HTAB O6' O3'_$5 EQIV $6 x-1, y, z HTAB N1' O7'_$6 HTAB C6' O7'_$5 HTAB C8' O7'_$6 HTAB O1S O3_$4 HTAB C1S O8_$4 ACTA WGHT 0.052400 0.043100 BASF 0.49571 FVAR 0.67929 O1 4 0.661300 0.389544 1.015529 11.00000 0.05837 0.04547 = 0.02972 0.00264 0.00591 -0.00905 O3 4 0.652788 0.373653 0.732653 11.00000 0.05941 0.03187 = 0.03239 -0.00066 -0.00361 -0.00797 O5 4 0.729936 0.521816 0.943172 11.00000 0.05826 0.03256 = 0.02803 -0.00165 0.00804 0.00488 PART 1 O6 4 0.961170 0.707052 0.945272 10.50000 0.09437 0.05211 = 0.04594 -0.01779 0.00967 -0.03203 AFIX 147 H6O 2 0.875712 0.697805 0.987275 10.50000 -1.50000 AFIX 0 PART 2 O6A 4 0.538192 0.696683 0.871522 10.50000 0.14142 0.04612 = 0.10252 0.01252 0.06146 0.04820 AFIX 147 H6AO 2 0.528968 0.753853 0.871180 10.50000 -1.50000 AFIX 0 PART 0 O8 4 0.323268 0.223971 0.906710 11.00000 0.02591 0.06187 = 0.08920 0.01879 0.00477 -0.00201 N1 3 0.758262 0.276197 0.879083 11.00000 0.02062 0.03041 = 0.03868 0.00279 0.00128 0.00111 H1N 2 0.932204 0.265589 0.875544 11.00000 0.01653 C1 1 0.793607 0.425498 0.948876 11.00000 0.03821 0.03024 = 0.03066 0.00189 0.00136 0.00108 AFIX 13 H1A 2 0.997167 0.416705 0.953441 11.00000 -1.20000 AFIX 0 C2 1 0.682164 0.373584 0.875066 11.00000 0.02434 0.02883 = 0.03477 0.00336 0.00103 0.00017 AFIX 13 H2A 2 0.476738 0.378155 0.874899 11.00000 -1.20000 AFIX 0 C3 1 0.793554 0.417936 0.797531 11.00000 0.03083 0.02976 = 0.02872 -0.00086 0.00186 0.00019 AFIX 13 H3A 2 0.995667 0.405910 0.793219 11.00000 -1.20000 AFIX 0 C4 1 0.743095 0.523810 0.799374 11.00000 0.03243 0.02715 = 0.02923 0.00138 0.00416 0.00113 AFIX 13 H4A 2 0.540824 0.536263 0.796932 11.00000 -1.20000 AFIX 0 C5 1 0.863988 0.565811 0.876431 11.00000 0.05372 0.03160 = 0.02848 -0.00129 0.00442 -0.00222 AFIX 13 H5A 2 1.066193 0.553185 0.878652 11.00000 -1.20000 AFIX 0 C6 1 0.816004 0.669262 0.883146 11.00000 0.11386 0.03191 = 0.03211 -0.00412 0.00298 -0.00188 PART 1 AFIX 23 H6A 2 0.873382 0.699202 0.833542 10.50000 -1.20000 H6B 2 0.617058 0.681054 0.890635 10.50000 -1.20000 AFIX 23 PART 2 H6C 2 0.876044 0.689708 0.935970 10.50000 -1.20000 H6D 2 0.932925 0.700711 0.843857 10.50000 -1.20000 AFIX 0 PART 0 C7 1 0.808273 0.406213 1.089382 11.00000 0.08757 0.04571 = 0.02895 0.00206 -0.00182 0.00325 AFIX 137 H7A 2 0.723974 0.370095 1.131539 11.00000 -1.50000 H7B 2 0.797678 0.471347 1.102649 11.00000 -1.50000 H7C 2 1.001519 0.388351 1.083378 11.00000 -1.50000 AFIX 0 C8 1 0.575961 0.208159 0.896811 11.00000 0.02795 0.03659 = 0.04720 0.00827 0.00075 -0.00275 C9 1 0.695005 0.111459 0.901622 11.00000 0.04602 0.03363 = 0.08104 0.00920 0.00459 -0.00408 AFIX 137 H9A 2 0.609485 0.078600 0.945515 11.00000 -1.50000 H9B 2 0.894259 0.114941 0.910051 11.00000 -1.50000 H9C 2 0.657534 0.078887 0.852381 11.00000 -1.50000 AFIX 0 O1' 4 0.880895 0.570525 0.733972 11.00000 0.03175 0.02963 = 0.02798 0.00147 -0.00087 -0.00268 O3' 4 0.719639 0.740581 0.489574 11.00000 0.03469 0.03251 = 0.04291 0.01221 -0.00123 -0.00054 H3'O 2 0.566866 0.759061 0.471004 11.00000 0.05225 H3O 2 0.714878 0.397937 0.685429 11.00000 0.04560 O4' 4 0.480286 0.562135 0.428870 11.00000 0.06241 0.04304 = 0.04417 0.00601 -0.02342 -0.01061 H4'O 2 0.551437 0.604788 0.392769 11.00000 0.05164 O5' 4 0.831803 0.497533 0.614041 11.00000 0.03452 0.02537 = 0.02910 -0.00152 -0.00377 0.00537 O6' 4 0.773414 0.321497 0.548285 11.00000 0.03690 0.02686 = 0.05469 -0.00448 -0.00155 -0.00004 H6'O 2 0.908777 0.295225 0.539557 11.00000 0.08382 O7' 4 1.151042 0.799752 0.682585 11.00000 0.02331 0.05359 = 0.09068 -0.01679 0.00008 -0.00221 N1' 3 0.713862 0.745929 0.662159 11.00000 0.01911 0.02744 = 0.03958 -0.00230 0.00118 0.00165 H1N' 2 0.521653 0.758430 0.666122 11.00000 0.01966 C1' 1 0.734006 0.573098 0.661597 11.00000 0.02877 0.02569 = 0.02939 -0.00032 0.00098 0.00034 AFIX 13 H1'A 2 0.531861 0.566904 0.671392 11.00000 -1.20000 AFIX 0 C2' 1 0.795581 0.664370 0.616884 11.00000 0.02394 0.02376 = 0.03231 0.00287 0.00288 -0.00015 AFIX 13 H2'A 2 0.997740 0.667805 0.606156 11.00000 -1.20000 AFIX 0 C3' 1 0.638663 0.662276 0.536372 11.00000 0.02289 0.02618 = 0.03889 0.00720 -0.00144 0.00088 AFIX 13 H3'A 2 0.436964 0.667216 0.547368 11.00000 -1.20000 AFIX 0 C4' 1 0.689182 0.572586 0.488919 11.00000 0.03450 0.03315 = 0.02744 0.00216 -0.00435 -0.00252 AFIX 13 H4'A 2 0.874727 0.575294 0.463538 11.00000 -1.20000 AFIX 0 C5' 1 0.670942 0.485471 0.541814 11.00000 0.03078 0.02751 = 0.03144 -0.00095 -0.00613 -0.00325 AFIX 13 H5'A 2 0.474313 0.472657 0.555322 11.00000 -1.20000 AFIX 0 C6' 1 0.795617 0.402911 0.498384 11.00000 0.04440 0.03229 = 0.03527 -0.00529 -0.00440 0.00142 AFIX 23 H6'A 2 0.696242 0.392679 0.448283 11.00000 -1.20000 H6'B 2 0.991389 0.415061 0.486059 11.00000 -1.20000 AFIX 0 C7' 1 0.898435 0.809682 0.688761 11.00000 0.03128 0.03014 = 0.03765 0.00112 -0.00371 -0.00111 C8' 1 0.773997 0.896088 0.725251 11.00000 0.04253 0.03694 = 0.05868 -0.01599 -0.00634 0.00271 AFIX 137 H8'A 2 0.846644 0.950160 0.698249 11.00000 -1.50000 H8'B 2 0.822429 0.898956 0.781168 11.00000 -1.50000 H8'C 2 0.573311 0.894426 0.719681 11.00000 -1.50000 AFIX 0 O1S 4 0.540281 0.682111 0.301927 11.00000 0.06696 0.06325 = 0.05939 0.02011 -0.00089 0.00890 AFIX 147 H1S 2 0.474933 0.734452 0.294896 11.00000 -1.50000 AFIX 0 C1S 1 0.828864 0.683895 0.287973 11.00000 0.07014 0.14080 = 0.06097 0.02209 0.00657 -0.01603 AFIX 137 H1SA 2 0.900524 0.621240 0.287904 11.00000 -1.50000 H1SB 2 0.919732 0.719208 0.329534 11.00000 -1.50000 H1SC 2 0.865150 0.712465 0.236866 11.00000 -1.50000 AFIX 0 HKLF 4 REM p21_a.res in P2(1) REM wR2 = 0.0801, GooF = S = 1.044, Restrained GooF = 1.044 for all data REM R1 = 0.0312 for 4410 Fo > 4sig(Fo) and 0.0316 for all 4462 data REM 330 parameters refined using 1 restraints END WGHT 0.0526 0.0416 REM Highest difference peak 0.194, deepest hole -0.137, 1-sigma level 0.033 Q1 1 0.7291 0.3933 0.8405 11.00000 0.05 0.19 Q2 1 0.3272 0.2237 0.8464 11.00000 0.05 0.17 Q3 1 0.7821 0.6220 0.6368 11.00000 0.05 0.13 Q4 1 0.8188 0.6412 0.5764 11.00000 0.05 0.13 Q5 1 0.9305 0.9365 0.7379 11.00000 0.05 0.12 Q6 1 0.8795 0.4927 0.5853 11.00000 0.05 0.12 Q7 1 0.7273 0.4112 0.9805 11.00000 0.05 0.12 Q8 1 0.7339 0.3401 0.5999 11.00000 0.05 0.12 Q9 1 0.4867 0.4883 0.5383 11.00000 0.05 0.11 Q10 1 0.7079 0.4938 0.5027 11.00000 0.05 0.11 Q11 1 0.7957 0.5436 0.9099 11.00000 0.05 0.11 Q12 1 1.2931 0.8456 0.7399 11.00000 0.05 0.11 Q13 1 0.6857 0.4901 0.6025 11.00000 0.05 0.10 Q14 1 0.8113 0.5364 0.7695 11.00000 0.05 0.10 Q15 1 0.4230 0.6795 0.9180 11.00000 0.05 0.10 Q16 1 1.2458 0.8059 0.6784 11.00000 0.05 0.10 Q17 1 0.2310 0.0273 0.7997 11.00000 0.05 0.10 Q18 1 0.6694 0.5966 0.5227 11.00000 0.05 0.10 Q19 1 0.7393 0.5502 0.8418 11.00000 0.05 0.10 Q20 1 0.3377 0.8219 0.4411 11.00000 0.05 0.10 ; _shelx_res_checksum 48032 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.6613(6) 0.38954(17) 1.01553(14) 0.0445(6) Uani d 1 . . O O3 0.6528(6) 0.37365(16) 0.73265(14) 0.0412(5) Uani d 1 . . O O5 0.7299(6) 0.52182(15) 0.94317(12) 0.0396(5) Uani d 1 . . O O6 0.9612(16) 0.7071(5) 0.9453(4) 0.0641(17) Uani d 0.5 A 1 H H6O 0.875712 0.697805 0.987275 0.096 Uiso calc 0.5 A 1 O O6A 0.538(2) 0.6967(5) 0.8715(6) 0.097(3) Uani d 0.5 A 2 H H6AO 0.528968 0.753853 0.871180 0.145 Uiso calc 0.5 A 2 O O8 0.3233(5) 0.2240(2) 0.9067(2) 0.0590(8) Uani d 1 . . N N1 0.7583(5) 0.27620(17) 0.87908(16) 0.0299(5) Uani d 1 . . H H1N 0.932(8) 0.266(2) 0.8755(19) 0.017(7) Uiso d 1 . . C C1 0.7936(7) 0.4255(2) 0.94888(17) 0.0330(6) Uani d 1 . . H H1A 0.997167 0.416705 0.953441 0.040 Uiso calc 1 . . C C2 0.6822(6) 0.37358(19) 0.87507(18) 0.0293(5) Uani d 1 . . H H2A 0.476738 0.378155 0.874899 0.035 Uiso calc 1 . . C C3 0.7936(6) 0.4179(2) 0.79753(17) 0.0298(6) Uani d 1 . . H H3A 0.995667 0.405910 0.793219 0.036 Uiso calc 1 . . C C4 0.7431(7) 0.52381(19) 0.79937(17) 0.0296(5) Uani d 1 . . H H4A 0.540824 0.536263 0.796932 0.036 Uiso calc 1 . . C C5 0.8640(8) 0.5658(2) 0.87643(17) 0.0379(6) Uani d 1 . . H H5A 1.066193 0.553185 0.878652 0.046 Uiso calc 1 . . C C6 0.8160(12) 0.6693(3) 0.8831(2) 0.0593(11) Uani d 1 . . H H6A 0.873382 0.699202 0.833542 0.071 Uiso calc 0.5 A 1 H H6B 0.617058 0.681054 0.890635 0.071 Uiso calc 0.5 A 1 H H6C 0.876044 0.689708 0.935970 0.071 Uiso calc 0.5 A 2 H H6D 0.932925 0.700711 0.843857 0.071 Uiso calc 0.5 A 2 C C7 0.8083(12) 0.4062(3) 1.0894(2) 0.0541(10) Uani d 1 . . H H7A 0.723974 0.370095 1.131539 0.081 Uiso calc 1 . . H H7B 0.797678 0.471347 1.102649 0.081 Uiso calc 1 . . H H7C 1.001519 0.388351 1.083378 0.081 Uiso calc 1 . . C C8 0.5760(6) 0.2082(2) 0.8968(2) 0.0372(7) Uani d 1 . . C C9 0.6950(8) 0.1115(3) 0.9016(3) 0.0536(9) Uani d 1 . . H H9A 0.609485 0.078600 0.945515 0.080 Uiso calc 1 . . H H9B 0.894259 0.114941 0.910051 0.080 Uiso calc 1 . . H H9C 0.657534 0.078887 0.852381 0.080 Uiso calc 1 . . O O1' 0.8809(4) 0.57052(15) 0.73397(12) 0.0298(4) Uani d 1 . . O O3' 0.7196(5) 0.74058(15) 0.48957(14) 0.0367(5) Uani d 1 . . H H3'O 0.567(12) 0.759(4) 0.471(3) 0.052(13) Uiso d 1 . . H H3O 0.715(10) 0.398(3) 0.685(3) 0.046(11) Uiso d 1 . . O O4' 0.4803(6) 0.56213(19) 0.42887(16) 0.0499(6) Uani d 1 . . H H4'O 0.551(11) 0.605(4) 0.393(3) 0.052(12) Uiso d 1 . . O O5' 0.8318(5) 0.49753(14) 0.61404(12) 0.0297(4) Uani d 1 . . O O6' 0.7734(5) 0.32150(16) 0.54828(16) 0.0395(5) Uani d 1 . . H H6'O 0.909(16) 0.295(5) 0.540(4) 0.08(2) Uiso d 1 . . O O7' 1.1510(5) 0.7998(2) 0.6826(2) 0.0559(7) Uani d 1 . . N N1' 0.7139(5) 0.74593(17) 0.66216(15) 0.0287(5) Uani d 1 . . H H1N' 0.522(8) 0.758(2) 0.6661(18) 0.020(7) Uiso d 1 . . C C1' 0.7340(6) 0.5731(2) 0.66160(16) 0.0280(5) Uani d 1 . . H H1'A 0.531861 0.566904 0.671392 0.034 Uiso calc 1 . . C C2' 0.7956(5) 0.66437(18) 0.61688(16) 0.0267(5) Uani d 1 . . H H2'A 0.997740 0.667805 0.606156 0.032 Uiso calc 1 . . C C3' 0.6387(6) 0.6623(2) 0.53637(17) 0.0293(6) Uani d 1 . . H H3'A 0.436964 0.667216 0.547368 0.035 Uiso calc 1 . . C C4' 0.6892(6) 0.5726(2) 0.48892(16) 0.0317(6) Uani d 1 . . H H4'A 0.874727 0.575294 0.463538 0.038 Uiso calc 1 . . C C5' 0.6709(6) 0.48547(19) 0.54181(17) 0.0299(6) Uani d 1 . . H H5'A 0.474313 0.472657 0.555322 0.036 Uiso calc 1 . . C C6' 0.7956(8) 0.4029(2) 0.49838(19) 0.0373(7) Uani d 1 . . H H6'A 0.696242 0.392679 0.448283 0.045 Uiso calc 1 . . H H6'B 0.991389 0.415061 0.486059 0.045 Uiso calc 1 . . C C7' 0.8984(6) 0.8097(2) 0.6888(2) 0.0330(6) Uani d 1 . . C C8' 0.7740(8) 0.8961(2) 0.7253(2) 0.0461(8) Uani d 1 . . H H8'A 0.846644 0.950160 0.698249 0.069 Uiso calc 1 . . H H8'B 0.822429 0.898956 0.781168 0.069 Uiso calc 1 . . H H8'C 0.573311 0.894426 0.719681 0.069 Uiso calc 1 . . O O1S 0.5403(7) 0.6821(2) 0.3019(2) 0.0632(8) Uani d 1 . . H H1S 0.474933 0.734452 0.294896 0.095 Uiso calc 1 . . C C1S 0.8289(14) 0.6839(6) 0.2880(3) 0.091(2) Uani d 1 . . H H1SA 0.900524 0.621240 0.287904 0.136 Uiso calc 1 . . H H1SB 0.919732 0.719208 0.329534 0.136 Uiso calc 1 . . H H1SC 0.865150 0.712465 0.236866 0.136 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0584(14) 0.0455(13) 0.0297(11) -0.0091(12) 0.0059(10) 0.0026(10) O3 0.0594(15) 0.0319(10) 0.0324(11) -0.0080(10) -0.0036(11) -0.0007(9) O5 0.0583(14) 0.0326(11) 0.0280(9) 0.0049(10) 0.0080(10) -0.0016(8) O6 0.094(4) 0.052(3) 0.046(3) -0.032(3) 0.010(3) -0.018(3) O6A 0.141(7) 0.046(3) 0.103(6) 0.048(4) 0.061(6) 0.013(4) O8 0.0259(12) 0.0619(17) 0.089(2) -0.0020(12) 0.0048(13) 0.0188(15) N1 0.0206(11) 0.0304(12) 0.0387(12) 0.0011(9) 0.0013(10) 0.0028(10) C1 0.0382(15) 0.0302(14) 0.0307(13) 0.0011(12) 0.0014(13) 0.0019(11) C2 0.0243(11) 0.0288(13) 0.0348(14) 0.0002(10) 0.0010(12) 0.0034(11) C3 0.0308(14) 0.0298(13) 0.0287(12) 0.0002(11) 0.0019(11) -0.0009(10) C4 0.0324(13) 0.0272(12) 0.0292(12) 0.0011(11) 0.0042(12) 0.0014(11) C5 0.0537(17) 0.0316(14) 0.0285(13) -0.0022(14) 0.0044(14) -0.0013(12) C6 0.114(4) 0.0319(16) 0.0321(16) -0.002(2) 0.003(2) -0.0041(14) C7 0.088(3) 0.0457(17) 0.0290(14) 0.0033(19) -0.0018(18) 0.0021(13) C8 0.0280(15) 0.0366(15) 0.0472(17) -0.0027(12) 0.0007(13) 0.0083(13) C9 0.0460(19) 0.0336(16) 0.081(3) -0.0041(15) 0.0046(19) 0.0092(17) O1' 0.0318(9) 0.0296(9) 0.0280(9) -0.0027(9) -0.0009(8) 0.0015(8) O3' 0.0347(12) 0.0325(10) 0.0429(11) -0.0005(9) -0.0012(9) 0.0122(9) O4' 0.0624(16) 0.0430(13) 0.0442(12) -0.0106(13) -0.0234(12) 0.0060(11) O5' 0.0345(9) 0.0254(8) 0.0291(9) 0.0054(7) -0.0038(9) -0.0015(7) O6' 0.0369(11) 0.0269(10) 0.0547(14) 0.0000(9) -0.0015(10) -0.0045(10) O7' 0.0233(11) 0.0536(15) 0.091(2) -0.0022(11) 0.0001(12) -0.0168(14) N1' 0.0191(11) 0.0274(11) 0.0396(12) 0.0016(9) 0.0012(9) -0.0023(9) C1' 0.0288(12) 0.0257(11) 0.0294(12) 0.0003(12) 0.0010(10) -0.0003(11) C2' 0.0239(11) 0.0238(11) 0.0323(12) -0.0001(10) 0.0029(11) 0.0029(11) C3' 0.0229(12) 0.0262(12) 0.0389(14) 0.0009(11) -0.0014(11) 0.0072(12) C4' 0.0345(13) 0.0332(13) 0.0274(12) -0.0025(13) -0.0044(11) 0.0022(12) C5' 0.0308(14) 0.0275(13) 0.0314(13) -0.0032(11) -0.0061(12) -0.0009(10) C6' 0.0444(17) 0.0323(14) 0.0353(14) 0.0014(13) -0.0044(14) -0.0053(12) C7' 0.0313(15) 0.0301(14) 0.0376(16) -0.0011(12) -0.0037(12) 0.0011(12) C8' 0.0425(17) 0.0369(15) 0.0587(19) 0.0027(14) -0.0063(16) -0.0160(16) O1S 0.0670(18) 0.0633(19) 0.0594(16) 0.0089(16) -0.0009(15) 0.0201(15) C1S 0.070(3) 0.141(6) 0.061(3) -0.016(4) 0.007(3) 0.022(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 O1 C7 . . 113.9(3) ? C3 O3 H3O . . 109(3) ? C1 O5 C5 . . 112.7(2) ? C6 O6 H6O . . 109.5 ? C6 O6A H6AO . . 109.5 ? C8 N1 C2 . . 123.5(2) ? C8 N1 H1N . . 121(2) ? C2 N1 H1N . . 115(2) ? O1 C1 O5 . . 108.7(3) ? O1 C1 C2 . . 107.9(2) ? O5 C1 C2 . . 110.2(2) ? O1 C1 H1A . . 110.0 ? O5 C1 H1A . . 110.0 ? C2 C1 H1A . . 110.0 ? N1 C2 C1 . . 110.2(2) ? N1 C2 C3 . . 110.6(2) ? C1 C2 C3 . . 110.8(2) ? N1 C2 H2A . . 108.4 ? C1 C2 H2A . . 108.4 ? C3 C2 H2A . . 108.4 ? O3 C3 C2 . . 107.0(2) ? O3 C3 C4 . . 112.5(2) ? C2 C3 C4 . . 109.8(2) ? O3 C3 H3A . . 109.2 ? C2 C3 H3A . . 109.2 ? C4 C3 H3A . . 109.2 ? O1' C4 C5 . . 106.3(2) ? O1' C4 C3 . . 111.9(2) ? C5 C4 C3 . . 110.3(2) ? O1' C4 H4A . . 109.4 ? C5 C4 H4A . . 109.4 ? C3 C4 H4A . . 109.4 ? O5 C5 C6 . . 108.0(3) ? O5 C5 C4 . . 108.1(3) ? C6 C5 C4 . . 113.1(3) ? O5 C5 H5A . . 109.2 ? C6 C5 H5A . . 109.2 ? C4 C5 H5A . . 109.2 ? O6 C6 C5 . . 111.9(5) ? O6A C6 C5 . . 114.3(5) ? O6 C6 H6A . . 109.2 ? C5 C6 H6A . . 109.2 ? O6 C6 H6B . . 109.2 ? C5 C6 H6B . . 109.2 ? H6A C6 H6B . . 107.9 ? O6A C6 H6C . . 108.7 ? C5 C6 H6C . . 108.7 ? O6A C6 H6D . . 108.7 ? C5 C6 H6D . . 108.7 ? H6C C6 H6D . . 107.6 ? O1 C7 H7A . . 109.5 ? O1 C7 H7B . . 109.5 ? H7A C7 H7B . . 109.5 ? O1 C7 H7C . . 109.5 ? H7A C7 H7C . . 109.5 ? H7B C7 H7C . . 109.5 ? O8 C8 N1 . . 121.8(3) ? O8 C8 C9 . . 122.0(3) ? N1 C8 C9 . . 116.1(3) ? C8 C9 H9A . . 109.5 ? C8 C9 H9B . . 109.5 ? H9A C9 H9B . . 109.5 ? C8 C9 H9C . . 109.5 ? H9A C9 H9C . . 109.5 ? H9B C9 H9C . . 109.5 ? C1' O1' C4 . . 116.0(2) ? C3' O3' H3'O . . 103(3) ? C4' O4' H4'O . . 98(3) ? C1' O5' C5' . . 112.6(2) ? C6' O6' H6'O . . 103(5) ? C7' N1' C2' . . 123.1(2) ? C7' N1' H1N' . . 119(2) ? C2' N1' H1N' . . 117(2) ? O1' C1' O5' . . 107.3(2) ? O1' C1' C2' . . 110.3(2) ? O5' C1' C2' . . 108.4(2) ? O1' C1' H1'A . . 110.2 ? O5' C1' H1'A . . 110.2 ? C2' C1' H1'A . . 110.2 ? N1' C2' C1' . . 112.6(2) ? N1' C2' C3' . . 109.9(2) ? C1' C2' C3' . . 108.3(2) ? N1' C2' H2'A . . 108.6 ? C1' C2' H2'A . . 108.6 ? C3' C2' H2'A . . 108.6 ? O3' C3' C4' . . 109.7(2) ? O3' C3' C2' . . 109.4(2) ? C4' C3' C2' . . 113.1(2) ? O3' C3' H3'A . . 108.2 ? C4' C3' H3'A . . 108.2 ? C2' C3' H3'A . . 108.2 ? O4' C4' C3' . . 110.1(3) ? O4' C4' C5' . . 106.3(2) ? C3' C4' C5' . . 112.3(2) ? O4' C4' H4'A . . 109.4 ? C3' C4' H4'A . . 109.4 ? C5' C4' H4'A . . 109.4 ? O5' C5' C6' . . 106.6(2) ? O5' C5' C4' . . 110.7(2) ? C6' C5' C4' . . 109.9(3) ? O5' C5' H5'A . . 109.8 ? C6' C5' H5'A . . 109.8 ? C4' C5' H5'A . . 109.8 ? O6' C6' C5' . . 109.3(3) ? O6' C6' H6'A . . 109.8 ? C5' C6' H6'A . . 109.8 ? O6' C6' H6'B . . 109.8 ? C5' C6' H6'B . . 109.8 ? H6'A C6' H6'B . . 108.3 ? O7' C7' N1' . . 122.7(3) ? O7' C7' C8' . . 121.4(3) ? N1' C7' C8' . . 115.9(3) ? C7' C8' H8'A . . 109.5 ? C7' C8' H8'B . . 109.5 ? H8'A C8' H8'B . . 109.5 ? C7' C8' H8'C . . 109.5 ? H8'A C8' H8'C . . 109.5 ? H8'B C8' H8'C . . 109.5 ? C1S O1S H1S . . 109.5 ? O1S C1S H1SA . . 109.5 ? O1S C1S H1SB . . 109.5 ? H1SA C1S H1SB . . 109.5 ? O1S C1S H1SC . . 109.5 ? H1SA C1S H1SC . . 109.5 ? H1SB C1S H1SC . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C1 . 1.376(4) ? O1 C7 . 1.435(5) ? O3 C3 . 1.420(4) ? O3 H3O . 0.91(5) ? O5 C1 . 1.416(3) ? O5 C5 . 1.428(4) ? O6 C6 . 1.356(8) ? O6 H6O . 0.8200 ? O6A C6 . 1.393(12) ? O6A H6AO . 0.8200 ? O8 C8 . 1.235(4) ? N1 C8 . 1.338(4) ? N1 C2 . 1.443(4) ? N1 H1N . 0.84(4) ? C1 C2 . 1.531(4) ? C1 H1A . 0.9800 ? C2 C3 . 1.534(4) ? C2 H2A . 0.9800 ? C3 C4 . 1.536(3) ? C3 H3A . 0.9800 ? C4 O1' . 1.437(4) ? C4 C5 . 1.529(4) ? C4 H4A . 0.9800 ? C5 C6 . 1.503(5) ? C5 H5A . 0.9800 ? C6 H6A . 0.9700 ? C6 H6B . 0.9700 ? C6 H6C . 0.9700 ? C6 H6D . 0.9700 ? C7 H7A . 0.9600 ? C7 H7B . 0.9600 ? C7 H7C . 0.9600 ? C8 C9 . 1.499(5) ? C9 H9A . 0.9600 ? C9 H9B . 0.9600 ? C9 H9C . 0.9600 ? O1' C1' . 1.394(3) ? O3' C3' . 1.419(3) ? O3' H3'O . 0.83(6) ? O4' C4' . 1.418(4) ? O4' H4'O . 0.92(5) ? O5' C1' . 1.420(3) ? O5' C5' . 1.436(4) ? O6' C6' . 1.436(4) ? O6' H6'O . 0.76(8) ? O7' C7' . 1.215(4) ? N1' C7' . 1.342(4) ? N1' C2' . 1.444(4) ? N1' H1N' . 0.93(4) ? C1' C2' . 1.533(4) ? C1' H1'A . 0.9800 ? C2' C3' . 1.535(4) ? C2' H2'A . 0.9800 ? C3' C4' . 1.527(4) ? C3' H3'A . 0.9800 ? C4' C5' . 1.530(4) ? C4' H4'A . 0.9800 ? C5' C6' . 1.508(4) ? C5' H5'A . 0.9800 ? C6' H6'A . 0.9700 ? C6' H6'B . 0.9700 ? C7' C8' . 1.501(4) ? C8' H8'A . 0.9600 ? C8' H8'B . 0.9600 ? C8' H8'C . 0.9600 ? O1S C1S . 1.393(7) ? O1S H1S . 0.8200 ? C1S H1SA . 0.9600 ? C1S H1SB . 0.9600 ? C1S H1SC . 0.9600 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O6^a H6O^a O8 2_657 0.82 2.04 2.823(7) 160.0 yes N1 H1N O8 1_655 0.84(4) 2.02(4) 2.829(4) 160(3) yes C9 H9A O5 2_647 0.96 2.59 3.525(5) 164.5 yes C9 H9B O8 1_655 0.96 2.57 3.398(5) 144.4 yes O3' H3'O O6' 2_656 0.83(6) 1.88(6) 2.692(3) 165(5) yes O3 H3O O5' . 0.91(5) 1.94(5) 2.789(3) 155(4) yes O3 H3O O6' . 0.91(5) 2.55(5) 3.212(4) 130(4) yes O4' H4'O O1S . 0.92(5) 1.88(5) 2.739(4) 155(5) yes O6' H6'O O3' 2_746 0.76(8) 1.99(8) 2.750(4) 173(7) yes N1' H1N' O7' 1_455 0.93(4) 1.88(4) 2.808(3) 171(3) yes C6' H6'A O7' 2_746 0.97 2.66 3.366(5) 130.4 yes C8' H8'C O7' 1_455 0.96 2.50 3.347(5) 146.8 yes O1S H1S O3 2_656 0.82 2.13 2.950(4) 173.1 yes C1S H1SC O8 2_656 0.96 2.56 3.371(7) 142.4 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C7 O1 C1 O5 . . . . -81.3(3) ? C7 O1 C1 C2 . . . . 159.2(3) ? C5 O5 C1 O1 . . . . 178.7(3) ? C5 O5 C1 C2 . . . . -63.3(3) ? C8 N1 C2 C1 . . . . 105.6(3) ? C8 N1 C2 C3 . . . . -131.5(3) ? O1 C1 C2 N1 . . . . -64.1(3) ? O5 C1 C2 N1 . . . . 177.4(2) ? O1 C1 C2 C3 . . . . 173.1(2) ? O5 C1 C2 C3 . . . . 54.6(3) ? N1 C2 C3 O3 . . . . 64.8(3) ? C1 C2 C3 O3 . . . . -172.7(2) ? N1 C2 C3 C4 . . . . -172.9(2) ? C1 C2 C3 C4 . . . . -50.4(3) ? O3 C3 C4 O1' . . . . -69.8(3) ? C2 C3 C4 O1' . . . . 171.2(2) ? O3 C3 C4 C5 . . . . 172.1(2) ? C2 C3 C4 C5 . . . . 53.1(3) ? C1 O5 C5 C6 . . . . -172.0(3) ? C1 O5 C5 C4 . . . . 65.3(3) ? O1' C4 C5 O5 . . . . 179.4(2) ? C3 C4 C5 O5 . . . . -59.1(3) ? O1' C4 C5 C6 . . . . 59.8(4) ? C3 C4 C5 C6 . . . . -178.7(3) ? O5 C5 C6 O6 . . . . 69.8(5) ? C4 C5 C6 O6 . . . . -170.6(4) ? O5 C5 C6 O6A . . . . -68.4(5) ? C4 C5 C6 O6A . . . . 51.3(6) ? C2 N1 C8 O8 . . . . 4.1(5) ? C2 N1 C8 C9 . . . . -177.5(3) ? C5 C4 O1' C1' . . . . -154.8(2) ? C3 C4 O1' C1' . . . . 84.7(3) ? C4 O1' C1' O5' . . . . -95.8(3) ? C4 O1' C1' C2' . . . . 146.2(2) ? C5' O5' C1' O1' . . . . 172.6(2) ? C5' O5' C1' C2' . . . . -68.3(3) ? C7' N1' C2' C1' . . . . 115.7(3) ? C7' N1' C2' C3' . . . . -123.4(3) ? O1' C1' C2' N1' . . . . -60.3(3) ? O5' C1' C2' N1' . . . . -177.6(2) ? O1' C1' C2' C3' . . . . 177.8(2) ? O5' C1' C2' C3' . . . . 60.6(3) ? N1' C2' C3' O3' . . . . 63.7(3) ? C1' C2' C3' O3' . . . . -172.8(2) ? N1' C2' C3' C4' . . . . -173.7(2) ? C1' C2' C3' C4' . . . . -50.2(3) ? O3' C3' C4' O4' . . . . -75.0(3) ? C2' C3' C4' O4' . . . . 162.6(2) ? O3' C3' C4' C5' . . . . 166.9(2) ? C2' C3' C4' C5' . . . . 44.4(3) ? C1' O5' C5' C6' . . . . -179.4(2) ? C1' O5' C5' C4' . . . . 61.1(3) ? O4' C4' C5' O5' . . . . -167.9(2) ? C3' C4' C5' O5' . . . . -47.5(3) ? O4' C4' C5' C6' . . . . 74.5(3) ? C3' C4' C5' C6' . . . . -165.1(3) ? O5' C5' C6' O6' . . . . 60.7(3) ? C4' C5' C6' O6' . . . . -179.2(3) ? C2' N1' C7' O7' . . . . -6.3(5) ? C2' N1' C7' C8' . . . . 172.3(3) ?