#------------------------------------------------------------------------------ #$Date: 2024-07-09 05:02:26 +0300 (Tue, 09 Jul 2024) $ #$Revision: 293324 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312539.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312539 loop_ _publ_author_name 'Klein-Hessling, Christian' 'Blockhaus, Tobias' 'Sünkel, Karlheinz' _publ_section_title ; Synthesis, spectroscopic and crystallographic characterization of various cymantrenyl thioethers [Mn{C5HxBry(SMe)z}(PPh3)(CO)2]. ; _journal_coeditor_code QF3063 _journal_issue 8 _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_paper_doi 10.1107/S205322962400603X _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Mn (C10 H15 S) (C18 H15 P) (C O)2]' _chemical_formula_moiety 'C30 H30 Mn O2 P S5' _chemical_formula_sum 'C30 H30 Mn O2 P S5' _chemical_formula_weight 668.75 _chemical_name_systematic Dicarbonyl[\h^5^-1,2,3,4,5-pentakis(methylsulfanyl)cyclopentadienyl](triphenylphosphane-\kP)manganese _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 107.9340(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.5274(5) _cell_length_b 13.6748(5) _cell_length_c 17.9841(7) _cell_measurement_reflns_used 9916 _cell_measurement_temperature 107(2) _cell_measurement_theta_max 27.1047 _cell_measurement_theta_min 2.7945 _cell_volume 2931.2(2) _computing_cell_refinement ; APEX2 (Bruker, 2011) ; _computing_data_collection ; APEX2 (Bruker, 2011) ; _computing_data_reduction ; SAINT (Bruker, 2011) ; _computing_publication_material ; Mercury (Macrae et al., 2020) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 107 _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 VENTURE' _diffrn_measurement_method 'mix of omega and phi scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0558 _diffrn_reflns_av_unetI/netI 0.0344 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 46511 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.121 _diffrn_reflns_theta_min 2.979 _diffrn_source 'rotating anode generator' _exptl_absorpt_coefficient_mu 0.890 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.7143 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS2016; Krause et al., 2015) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.515 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1384 _exptl_crystal_size_max 0.030 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.412 _refine_diff_density_min -0.502 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 357 _refine_ls_number_reflns 6471 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0408 _refine_ls_R_factor_gt 0.0300 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0268P)^2^+3.0744P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0695 _refine_ls_wR_factor_ref 0.0757 _reflns_number_gt 5457 _reflns_number_total 6471 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file qf3063.cif _cod_data_source_block compd_11 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2312539 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.974 _shelx_estimated_absorpt_t_max 0.982 _shelx_hkl_file ; -2 0 0 210.88 9.94 -2 0 0 221.73 9.79 2 0 0 214.16 9.21 2 0 0 214.49 9.96 2 0 0 199.64 9.73 -2 0 0 202.55 9.17 3 0 0 55.45 3.27 -3 0 0 60.78 4.25 -3 0 0 52.00 4.09 3 0 0 59.94 4.30 -3 0 0 52.03 3.27 3 0 0 55.69 4.52 -4 0 0 5.26 1.40 4 0 0 6.87 2.47 4 0 0 3.54 2.06 4 0 0 4.66 1.25 -4 0 0 3.55 1.91 -4 0 0 4.98 2.29 -5 0 0 2.86 2.46 -5 0 0 4.86 2.24 -5 0 0 0.66 1.20 5 0 0 3.78 2.22 5 0 0 3.69 2.83 5 0 0 2.74 1.33 6 0 0 600.32 26.66 6 0 0 610.10 28.55 -6 0 0 605.51 26.63 -6 0 0 598.51 28.34 6 0 0 643.75 29.31 -6 0 0 614.16 28.98 7 0 0 345.98 18.63 7 0 0 338.86 15.88 7 0 0 321.34 17.85 -7 0 0 354.30 15.97 -7 0 0 318.67 18.15 -7 0 0 349.72 17.96 -8 0 0 191.62 13.06 -8 0 0 193.26 12.44 8 0 0 205.72 10.46 -8 0 0 198.08 10.41 8 0 0 199.33 12.72 9 0 0 4.48 1.80 9 0 0 1.14 3.01 -9 0 0 -0.67 1.42 9 0 0 2.75 3.69 -9 0 0 -2.89 2.38 10 0 0 28.30 5.72 -10 0 0 25.36 3.65 10 0 0 30.10 6.58 10 0 0 26.15 3.66 11 0 0 411.24 24.17 -11 0 0 386.46 18.90 11 0 0 384.71 22.71 -11 0 0 390.74 18.89 -12 0 0 108.23 7.17 -12 0 0 95.81 7.04 12 0 0 97.20 10.74 12 0 0 95.43 10.37 -13 0 0 -1.10 2.19 13 0 0 -0.91 3.38 13 0 0 1.69 4.25 -13 0 0 -2.34 1.80 14 0 0 105.67 11.29 14 0 0 93.65 13.21 -14 0 0 82.79 7.01 15 0 0 49.52 10.31 15 0 0 59.70 9.92 -15 0 0 53.23 5.14 1 -1 0 0.20 0.54 1 -1 0 -0.31 0.41 1 -1 0 -0.50 0.39 1 1 0 -0.52 0.21 1 1 0 0.19 0.30 -2 1 0 1489.28 60.73 -2 1 0 1442.72 60.81 3 -1 0 1621.39 67.04 3 -1 0 1662.74 67.68 3 -1 0 1719.75 67.73 -3 -1 0 1568.00 65.94 -3 -1 0 1600.71 67.14 -3 1 0 1633.87 67.61 3 1 0 1604.43 67.22 3 1 0 1661.25 65.97 -3 1 0 1603.91 66.97 3 1 0 1539.40 67.75 -3 1 0 1588.33 67.62 -4 -1 0 1193.63 49.88 4 -1 0 1244.76 51.01 4 -1 0 1248.70 52.05 4 -1 0 1222.80 51.93 -4 -1 0 1207.68 51.40 -4 -1 0 1019.19 51.74 4 1 0 1223.78 51.53 -4 1 0 1254.65 52.02 4 1 0 1251.59 49.94 -4 1 0 1223.83 51.84 4 1 0 1274.66 52.41 -4 1 0 1203.03 50.94 -5 -1 0 293.93 14.81 -5 -1 0 298.38 13.10 5 -1 0 311.22 15.50 5 -1 0 297.82 14.16 5 -1 0 310.98 15.69 -5 -1 0 323.14 15.84 5 1 0 290.71 15.73 -5 1 0 279.18 15.02 5 1 0 290.89 13.10 5 1 0 287.27 14.78 -5 1 0 292.33 15.31 -5 1 0 294.85 14.18 6 -1 0 2.76 1.67 6 -1 0 5.41 2.71 -6 -1 0 3.86 2.27 -6 -1 0 1.38 1.06 -6 -1 0 3.68 2.84 6 -1 0 4.27 3.22 -6 1 0 6.80 2.55 -6 1 0 3.08 2.16 6 1 0 6.19 3.34 -6 1 0 2.79 1.67 6 1 0 1.14 2.27 -7 -1 0 256.54 14.10 7 -1 0 264.53 13.06 7 -1 0 252.32 15.01 7 -1 0 251.00 14.67 -7 -1 0 257.99 11.88 -7 1 0 229.41 12.73 -7 1 0 242.61 14.73 7 1 0 240.12 14.92 -7 1 0 261.59 14.65 7 1 0 263.59 11.95 7 1 0 272.52 14.57 -8 -1 0 1.97 2.41 8 -1 0 0.17 2.82 -8 -1 0 1.94 1.33 8 -1 0 1.16 3.18 -8 -1 0 -2.55 2.10 8 -1 0 2.93 1.60 8 1 0 2.98 2.67 8 1 0 1.30 1.23 -8 1 0 1.36 2.09 8 1 0 0.06 3.12 -8 1 0 4.17 1.88 -8 1 0 1.98 2.81 9 -1 0 204.49 14.38 -9 -1 0 218.90 10.92 -9 -1 0 182.82 12.87 9 -1 0 213.80 13.89 9 -1 0 199.40 11.54 9 1 0 211.79 15.29 9 1 0 196.82 14.49 9 1 0 217.49 10.58 -9 1 0 244.49 15.64 -9 1 0 211.27 11.60 10 -1 0 42.74 7.47 -10 -1 0 47.64 3.93 10 -1 0 50.07 5.12 -10 -1 0 53.50 4.06 10 -1 0 38.25 6.68 10 1 0 46.24 6.92 10 1 0 46.92 8.12 -10 1 0 49.16 4.90 11 -1 0 167.44 14.27 11 -1 0 191.81 14.35 -11 -1 0 196.64 9.94 -11 -1 0 183.61 9.87 11 -1 0 181.79 11.21 11 1 0 201.16 15.00 -11 1 0 194.53 11.26 11 1 0 193.73 14.06 12 -1 0 124.79 12.13 -12 -1 0 94.40 6.18 -12 -1 0 101.54 6.31 12 -1 0 104.73 10.53 12 1 0 110.70 10.61 -12 1 0 97.09 7.55 -12 1 0 90.75 7.56 12 1 0 106.05 11.16 -13 -1 0 2.09 1.68 13 -1 0 5.03 4.01 -13 -1 0 2.92 2.03 13 1 0 8.99 4.98 13 1 0 6.72 5.14 -13 1 0 6.01 2.81 -13 1 0 0.47 2.98 -14 -1 0 -0.56 1.34 14 -1 0 -0.67 3.59 14 -1 0 1.62 4.49 14 1 0 5.14 5.66 14 1 0 3.06 5.37 -14 1 0 -2.19 2.45 15 -1 0 22.71 7.13 15 -1 0 31.75 7.95 15 1 0 31.56 8.12 15 1 0 27.98 8.15 -15 1 0 13.59 3.77 0 2 0 279.76 12.39 0 2 0 290.30 12.50 0 2 0 283.67 12.52 -1 -2 0 111.85 5.14 -1 -2 0 109.03 5.70 1 -2 0 108.46 5.44 1 -2 0 108.43 5.79 -1 -2 0 99.74 5.24 1 -2 0 112.19 5.71 -1 2 0 109.95 5.78 1 2 0 113.61 5.74 -1 2 0 101.68 5.61 -1 2 0 104.50 5.36 1 2 0 113.88 5.32 1 2 0 113.26 5.14 2 -2 0 193.98 9.20 -2 -2 0 188.03 9.41 -2 -2 0 185.23 8.68 2 -2 0 191.30 9.02 2 -2 0 195.20 9.35 2 2 0 185.00 9.43 2 2 0 178.06 8.63 -2 2 0 195.13 9.02 2 2 0 188.38 7.83 2 2 0 159.25 7.78 -2 2 0 181.31 9.03 -2 2 0 177.49 9.20 -3 -2 0 24.86 2.64 3 -2 0 21.36 3.16 3 -2 0 32.63 3.14 3 -2 0 26.94 3.23 -3 -2 0 27.15 3.09 -3 2 0 27.70 2.82 3 2 0 26.75 2.63 3 2 0 29.85 3.24 -3 2 0 26.50 3.46 -3 2 0 27.50 2.99 -4 -2 0 215.92 11.06 4 -2 0 225.26 11.23 -4 -2 0 238.49 12.27 4 -2 0 221.69 11.80 4 -2 0 216.77 11.53 -4 2 0 210.58 11.51 -4 2 0 215.74 11.12 4 2 0 216.25 12.06 4 2 0 217.96 11.06 -4 2 0 223.05 11.83 -5 -2 0 19.76 3.70 -5 -2 0 19.76 3.19 -5 -2 0 18.46 1.31 5 -2 0 20.10 3.56 5 -2 0 16.37 2.94 5 -2 0 23.43 3.75 -5 2 0 17.62 2.94 5 2 0 22.05 3.58 -5 2 0 14.81 3.53 -5 2 0 28.01 4.21 5 2 0 22.31 3.96 6 -2 0 0.37 1.86 6 -2 0 2.57 2.68 -6 -2 0 2.98 0.81 -6 -2 0 1.65 1.96 6 -2 0 -0.23 2.55 -6 -2 0 3.86 2.18 -6 2 0 4.66 2.80 -6 2 0 1.17 1.86 6 2 0 6.75 3.34 6 2 0 6.35 2.60 -6 2 0 6.14 3.06 -7 -2 0 7.47 1.17 -7 -2 0 7.79 3.01 7 -2 0 11.82 3.10 7 -2 0 8.32 2.33 7 -2 0 7.31 2.67 -7 -2 0 8.09 1.22 -7 -2 0 9.32 2.76 -7 2 0 10.17 3.11 -7 2 0 12.13 2.63 7 2 0 9.54 3.18 7 2 0 6.35 3.61 -7 2 0 8.66 3.42 -8 -2 0 210.28 9.47 8 -2 0 217.95 11.89 -8 -2 0 195.97 9.38 -8 -2 0 199.67 13.70 8 -2 0 232.07 14.01 -8 -2 0 209.61 12.76 -8 2 0 219.95 11.89 -8 2 0 196.36 13.19 8 2 0 196.01 13.90 8 2 0 194.41 12.59 -8 2 0 208.06 13.16 9 -2 0 33.36 6.09 9 -2 0 36.22 4.75 -9 -2 0 41.79 5.89 9 -2 0 43.88 6.81 -9 -2 0 31.23 2.54 -9 -2 0 39.51 2.76 9 2 0 43.90 6.95 9 2 0 37.01 5.88 -9 2 0 37.19 4.91 10 -2 0 186.12 11.06 10 -2 0 163.03 13.23 10 -2 0 167.29 12.71 -10 -2 0 169.63 8.15 10 2 0 166.99 12.39 -10 2 0 162.54 10.48 10 2 0 183.97 14.30 -11 -2 0 72.37 4.09 11 -2 0 77.44 6.71 11 -2 0 66.09 9.65 11 -2 0 78.83 10.25 11 2 0 83.09 10.75 11 2 0 58.15 8.23 12 -2 0 38.53 7.62 12 -2 0 44.40 5.64 -12 -2 0 36.42 2.24 12 -2 0 38.98 8.05 -12 -2 0 35.30 2.17 -12 2 0 35.74 5.29 12 2 0 40.25 7.23 12 2 0 37.72 8.43 13 -2 0 -0.44 4.23 13 -2 0 -0.49 3.66 13 2 0 2.92 4.67 -13 2 0 2.53 3.01 -13 2 0 -0.43 2.86 13 2 0 2.52 3.29 14 -2 0 107.57 13.92 14 -2 0 106.01 11.73 14 2 0 87.47 13.01 14 2 0 111.25 14.62 -14 2 0 88.11 7.85 15 -2 0 2.61 4.38 15 -2 0 -6.76 3.96 15 2 0 -4.07 3.40 -15 2 0 -2.53 3.23 15 2 0 1.42 4.65 0 -3 0 0.47 1.06 0 -3 0 -0.69 1.16 0 -3 0 -0.52 1.29 0 3 0 -0.38 0.90 0 3 0 0.28 1.00 0 3 0 1.89 1.18 1 -3 0 347.67 15.85 1 -3 0 340.71 15.82 -1 -3 0 347.84 15.25 1 -3 0 351.41 15.42 -1 3 0 352.08 15.41 1 3 0 343.95 15.21 -1 3 0 350.70 15.91 1 3 0 324.94 15.23 -1 3 0 341.67 15.80 1 3 0 352.71 15.68 1 3 0 358.87 15.38 1 3 0 348.96 15.81 -2 -3 0 45.00 4.03 -2 -3 0 52.38 3.03 2 -3 0 52.00 4.20 -2 -3 0 45.17 3.46 2 -3 0 51.50 4.36 2 -3 0 54.58 3.78 -2 3 0 50.05 3.81 -2 3 0 48.54 3.84 2 3 0 53.05 3.02 2 3 0 52.56 3.58 2 3 0 52.97 4.23 -2 3 0 49.36 4.03 -3 -3 0 451.18 20.00 3 -3 0 455.77 20.51 3 -3 0 446.93 21.00 -3 -3 0 418.07 20.84 3 -3 0 451.31 20.67 3 3 0 465.59 18.71 -3 3 0 442.08 20.92 3 3 0 430.15 19.90 -3 3 0 447.57 20.47 -3 3 0 457.13 20.69 3 3 0 472.65 21.20 3 3 0 453.75 18.70 -4 -3 0 164.29 8.44 -4 -3 0 151.50 9.39 4 -3 0 158.93 8.98 4 -3 0 154.69 8.93 4 -3 0 142.54 9.27 -4 3 0 143.62 9.16 -4 3 0 150.38 8.78 4 3 0 144.39 8.26 4 3 0 167.87 9.80 -4 3 0 145.81 8.74 5 -3 0 39.96 4.96 5 -3 0 36.98 4.51 -5 -3 0 34.48 4.79 5 -3 0 35.22 5.06 -5 -3 0 34.76 3.76 5 3 0 33.79 4.12 -5 3 0 40.45 4.19 -5 3 0 43.31 5.09 -5 3 0 40.92 5.27 5 3 0 37.84 5.41 6 -3 0 116.33 8.89 -6 -3 0 111.03 7.52 6 -3 0 113.26 8.48 6 -3 0 126.72 8.09 -6 -3 0 130.53 8.95 -6 3 0 108.76 8.23 6 3 0 138.35 8.38 6 3 0 119.67 9.26 -6 3 0 106.04 7.58 -6 3 0 100.25 8.04 -7 -3 0 141.05 10.43 7 -3 0 155.49 9.50 7 -3 0 153.67 10.48 7 -3 0 143.84 10.53 -7 -3 0 151.48 9.39 -7 3 0 130.39 9.61 -7 3 0 148.44 10.36 7 3 0 141.47 9.44 -7 3 0 129.05 8.91 7 3 0 155.84 10.85 8 -3 0 12.66 4.19 8 -3 0 14.57 3.58 8 -3 0 16.74 4.40 -8 -3 0 12.57 4.02 -8 -3 0 7.85 2.91 -8 3 0 13.99 4.14 8 3 0 13.22 4.29 8 3 0 11.89 3.44 -8 3 0 12.80 3.64 -8 3 0 18.57 3.50 9 -3 0 176.54 12.47 9 -3 0 151.64 12.04 -9 -3 0 133.68 10.40 9 -3 0 159.26 10.50 9 3 0 171.62 12.64 -9 3 0 151.13 10.27 9 3 0 159.56 11.18 10 -3 0 418.40 24.05 10 -3 0 397.44 21.33 10 -3 0 418.71 23.83 10 3 0 452.12 23.00 -10 3 0 403.93 21.26 10 3 0 394.74 24.34 11 -3 0 126.32 11.63 11 -3 0 102.39 10.88 11 -3 0 116.88 9.28 11 3 0 125.17 10.64 11 3 0 124.63 12.48 -11 3 0 120.96 9.35 12 -3 0 186.24 15.14 12 -3 0 170.71 14.56 12 -3 0 175.74 11.91 12 3 0 177.75 13.89 12 3 0 190.22 15.48 13 -3 0 34.62 8.10 13 -3 0 44.88 8.80 13 -3 0 45.94 6.53 13 3 0 43.92 7.60 13 3 0 43.94 9.47 -13 3 0 44.18 6.53 14 -3 0 22.51 6.59 14 -3 0 35.53 7.91 14 3 0 16.62 6.98 14 3 0 16.38 5.66 -14 3 0 21.67 4.71 15 -3 0 135.99 13.71 15 -3 0 149.96 14.63 15 3 0 156.93 13.78 -15 3 0 131.69 11.00 15 3 0 134.92 14.67 0 -4 0 31.34 2.99 0 -4 0 35.34 3.21 0 -4 0 35.72 3.04 0 4 0 34.73 3.17 0 4 0 32.86 2.96 0 4 0 35.29 3.69 -1 -4 0 25.05 2.80 1 -4 0 25.12 2.83 1 -4 0 28.82 3.04 -1 -4 0 28.11 2.74 1 -4 0 28.84 3.49 -1 4 0 32.07 4.01 -1 4 0 30.81 2.70 -1 4 0 27.80 3.49 1 4 0 29.90 2.71 1 4 0 23.92 3.05 1 4 0 26.58 2.58 1 4 0 30.49 3.00 2 -4 0 3260.58 175.21 -2 4 0 3310.80 176.24 2 4 0 3415.96 163.69 3 -4 0 15.31 3.20 3 -4 0 11.95 2.63 3 -4 0 12.72 3.00 -3 -4 0 19.31 2.51 -3 -4 0 16.57 2.95 -3 4 0 13.13 2.47 -3 4 0 12.23 2.94 3 4 0 18.36 3.33 3 4 0 16.42 2.53 3 4 0 15.02 1.70 -3 4 0 14.57 2.92 3 4 0 16.35 1.68 -4 -4 0 120.73 8.12 4 -4 0 116.54 8.41 4 -4 0 115.73 7.97 4 -4 0 121.42 7.91 -4 -4 0 116.31 7.07 4 4 0 116.59 7.19 4 4 0 126.84 5.51 -4 4 0 130.90 7.77 -4 4 0 117.66 8.27 -4 4 0 117.27 7.94 4 4 0 121.80 5.47 -5 -4 0 8.19 2.91 5 -4 0 3.64 2.43 -5 -4 0 6.36 2.40 5 -4 0 4.00 2.04 5 -4 0 1.58 2.10 5 4 0 6.44 2.11 -5 4 0 4.66 2.50 -5 4 0 3.89 2.41 5 4 0 3.82 2.84 -5 4 0 2.88 2.22 6 -4 0 45.20 5.51 6 -4 0 45.30 4.86 6 -4 0 45.72 6.11 -6 -4 0 44.72 4.30 -6 -4 0 50.37 5.43 6 4 0 44.57 4.78 -6 4 0 37.73 5.03 -6 4 0 42.35 5.84 -6 4 0 44.77 5.72 6 4 0 44.30 6.07 -7 -4 0 1.76 2.77 7 -4 0 2.09 2.25 7 -4 0 -1.74 1.41 -7 -4 0 0.42 1.62 7 4 0 3.78 2.49 -7 4 0 0.38 2.32 -7 4 0 -1.48 1.57 -7 4 0 -2.87 2.49 8 -4 0 12.48 4.09 -8 -4 0 12.85 3.35 8 -4 0 12.84 3.57 8 -4 0 13.58 3.87 8 4 0 12.35 4.46 8 4 0 12.57 3.65 -8 4 0 12.43 3.94 -9 -4 0 681.56 32.88 9 -4 0 694.26 34.25 9 -4 0 712.49 32.98 9 -4 0 656.83 34.39 9 4 0 704.15 33.08 9 4 0 679.15 35.24 -9 4 0 672.66 32.66 10 -4 0 47.43 7.60 -10 -4 0 47.32 6.59 10 -4 0 49.22 6.58 10 -4 0 32.85 6.95 10 4 0 52.45 7.22 10 4 0 35.83 7.47 -10 4 0 51.51 6.55 11 -4 0 173.94 13.67 11 -4 0 183.80 12.63 11 -4 0 191.24 14.76 11 4 0 173.66 14.64 11 4 0 178.51 13.14 12 -4 0 32.46 6.67 12 -4 0 31.51 7.08 12 -4 0 34.76 5.82 12 4 0 19.28 7.10 12 4 0 34.87 6.75 13 -4 0 232.61 18.01 13 -4 0 245.64 15.25 13 -4 0 249.13 18.58 13 4 0 232.50 16.48 -13 4 0 211.96 14.78 13 4 0 241.49 19.51 14 -4 0 132.70 13.19 14 -4 0 96.10 13.12 -14 4 0 114.85 10.14 14 4 0 98.08 14.16 14 4 0 128.03 12.38 0 -5 0 -0.03 1.46 0 -5 0 -0.23 1.30 0 -5 0 0.92 1.55 0 5 0 3.16 1.58 0 5 0 2.25 1.74 0 5 0 0.24 1.23 1 -5 0 1053.00 45.42 1 -5 0 1037.02 45.21 -1 -5 0 1053.90 44.74 -1 -5 0 1037.55 44.66 1 -5 0 1058.37 44.69 -1 5 0 1031.76 45.16 1 5 0 1021.98 44.63 1 5 0 1090.34 45.08 -1 5 0 1049.88 44.65 1 5 0 1074.15 45.14 -1 5 0 1045.21 45.31 2 -5 0 398.28 18.68 2 -5 0 401.34 19.52 2 -5 0 418.93 19.64 -2 -5 0 397.35 18.25 2 5 0 417.79 18.57 -2 5 0 407.63 19.46 2 5 0 395.71 18.22 -2 5 0 384.37 19.37 2 5 0 415.06 19.24 2 5 0 422.27 19.45 3 -5 0 3.55 1.94 3 -5 0 6.53 2.43 -3 -5 0 1.28 1.25 -3 -5 0 5.58 1.94 -3 -5 0 5.31 2.43 3 -5 0 6.75 2.55 -3 5 0 6.46 2.11 -3 5 0 2.79 2.22 3 5 0 1.45 1.26 -3 5 0 2.99 1.89 3 5 0 4.90 2.02 3 5 0 1.21 1.63 4 -5 0 439.61 20.66 -4 -5 0 393.46 19.81 -4 -5 0 436.85 21.46 4 -5 0 415.36 21.48 4 -5 0 459.77 21.48 4 5 0 422.81 19.97 -4 5 0 439.62 21.47 4 5 0 419.08 18.55 4 5 0 441.09 21.56 -4 5 0 425.99 20.56 -4 5 0 419.53 21.03 4 5 0 470.32 18.67 5 -5 0 152.19 10.06 -5 -5 0 163.62 10.78 5 -5 0 167.09 10.08 -5 -5 0 162.53 9.24 5 -5 0 148.47 10.34 -5 5 0 163.56 10.47 -5 5 0 161.94 9.84 5 5 0 160.68 6.89 5 5 0 161.21 10.93 -5 5 0 173.72 10.39 5 5 0 154.10 9.13 5 5 0 155.85 6.88 6 -5 0 56.30 5.79 -6 -5 0 50.26 5.64 6 -5 0 52.24 5.76 6 -5 0 55.30 5.59 -6 -5 0 53.38 4.99 6 5 0 41.81 6.02 -6 5 0 47.72 6.30 6 5 0 50.86 4.84 -6 5 0 50.88 5.57 -6 5 0 50.36 5.45 7 -5 0 4.71 2.68 -7 -5 0 -0.06 1.90 7 -5 0 2.02 2.18 -7 -5 0 -1.04 2.37 7 -5 0 -0.08 2.36 -7 5 0 -1.16 2.74 -7 5 0 1.98 2.26 -7 5 0 -1.46 2.33 7 5 0 -0.74 2.80 7 5 0 1.69 1.91 8 -5 0 -2.99 2.15 8 -5 0 0.13 2.66 -8 -5 0 -2.50 1.76 8 -5 0 -3.22 1.75 -8 5 0 0.52 2.24 8 5 0 -1.31 2.25 -8 5 0 -0.61 2.66 8 5 0 0.46 2.55 -9 -5 0 75.46 7.38 9 -5 0 80.76 8.02 9 -5 0 81.01 7.74 9 -5 0 87.73 9.08 9 5 0 77.33 7.43 9 5 0 75.87 8.69 -9 5 0 83.20 8.57 10 -5 0 0.30 3.66 10 -5 0 2.72 3.67 10 -5 0 6.92 3.95 -10 -5 0 4.27 3.04 10 5 0 3.03 3.55 10 5 0 3.07 3.19 11 -5 0 -0.04 3.00 11 -5 0 0.69 2.92 11 -5 0 -1.26 3.26 11 5 0 -1.65 3.03 11 5 0 -5.51 2.13 12 -5 0 3.72 2.67 12 -5 0 -4.79 1.83 12 -5 0 -1.01 3.23 12 5 0 0.84 3.50 12 5 0 8.99 5.95 13 -5 0 22.82 6.02 13 -5 0 28.49 8.48 13 -5 0 25.93 5.31 13 5 0 29.42 8.67 13 5 0 41.68 7.68 14 -5 0 18.53 5.75 14 -5 0 29.42 7.52 14 5 0 8.01 5.22 -14 5 0 11.03 4.79 14 5 0 14.02 5.42 0 -6 0 195.50 10.53 0 -6 0 194.60 10.31 0 -6 0 179.42 10.59 0 6 0 199.01 10.42 0 6 0 183.28 10.38 0 6 0 195.89 10.65 1 -6 0 14.25 3.19 1 -6 0 16.07 2.72 -1 -6 0 16.62 2.85 1 -6 0 16.66 3.42 -1 -6 0 12.98 2.60 1 6 0 10.56 2.43 1 6 0 14.26 2.70 -1 6 0 11.30 2.49 -1 6 0 10.76 2.83 1 6 0 16.08 2.90 1 6 0 9.82 2.58 -1 6 0 12.40 2.81 2 -6 0 3.16 2.19 2 -6 0 2.14 2.31 -2 -6 0 6.04 1.95 2 -6 0 4.04 1.90 -2 6 0 3.49 1.72 -2 6 0 5.58 2.66 2 6 0 5.13 1.97 -2 6 0 8.08 2.75 2 6 0 5.73 2.01 2 6 0 7.46 2.33 2 6 0 6.32 2.29 2 6 0 5.95 1.95 -3 -6 0 1543.53 65.47 3 -6 0 1521.17 65.63 -3 -6 0 1580.23 63.55 3 -6 0 1502.28 64.44 3 -6 0 1486.71 65.47 3 6 0 1533.55 64.11 -3 6 0 1495.83 65.37 3 6 0 1570.47 65.56 -3 6 0 1503.71 65.51 3 6 0 1411.11 63.90 3 6 0 1542.64 65.26 -3 6 0 1526.08 64.43 -4 -6 0 6.38 2.77 4 -6 0 1.15 2.36 -4 -6 0 0.65 1.66 4 -6 0 3.61 1.92 4 -6 0 8.05 2.96 4 6 0 3.72 2.71 -4 6 0 2.34 1.94 -4 6 0 9.50 2.90 4 6 0 6.02 1.49 -4 6 0 2.31 2.51 4 6 0 3.89 1.42 4 6 0 2.30 1.80 5 -6 0 273.90 15.00 -5 -6 0 234.85 14.52 -5 -6 0 232.34 12.98 5 -6 0 253.93 13.92 5 -6 0 242.52 14.87 -5 6 0 237.15 15.85 5 6 0 258.04 13.31 -5 6 0 244.63 13.64 -5 6 0 272.30 16.01 5 6 0 255.15 15.05 5 6 0 258.76 11.33 5 6 0 256.27 11.27 -6 -6 0 227.51 14.08 -6 -6 0 200.18 11.86 6 -6 0 216.00 13.97 6 -6 0 215.83 13.50 6 -6 0 240.46 13.31 -6 6 0 217.73 12.82 -6 6 0 217.74 13.37 6 6 0 218.54 13.92 -6 6 0 200.40 13.54 6 6 0 221.38 12.19 7 -6 0 227.21 14.02 7 -6 0 243.20 14.18 -7 -6 0 220.52 12.80 7 -6 0 213.42 14.61 7 6 0 243.82 13.24 -7 6 0 220.61 13.75 7 6 0 217.40 14.66 -7 6 0 220.70 13.72 -8 -6 0 1.23 2.25 8 -6 0 1.18 2.48 8 -6 0 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7.60 2 -7 0 105.07 6.76 -2 -7 0 102.04 6.68 2 -7 0 93.73 7.46 -2 7 0 96.44 7.52 2 7 0 99.46 6.46 2 7 0 92.25 7.08 -2 7 0 95.41 7.34 2 7 0 95.25 6.56 2 7 0 92.75 6.56 2 7 0 101.56 7.16 -2 7 0 89.06 6.38 3 -7 0 28.93 3.91 3 -7 0 25.37 4.42 -3 -7 0 34.18 3.46 3 -7 0 23.31 4.46 -3 7 0 28.27 4.46 -3 7 0 27.74 4.48 3 7 0 32.66 3.58 3 7 0 27.68 4.44 3 7 0 32.96 3.36 -3 7 0 26.11 3.88 3 7 0 23.23 3.94 3 7 0 24.42 3.54 4 -7 0 728.00 35.34 4 -7 0 779.53 34.30 4 -7 0 744.44 35.40 -4 -7 0 765.27 35.37 -4 7 0 712.26 35.04 4 7 0 745.02 33.57 4 7 0 759.91 35.07 4 7 0 795.39 33.78 4 7 0 726.21 32.56 -4 7 0 751.50 36.94 4 7 0 774.71 35.47 -4 7 0 755.25 33.99 4 7 0 749.18 32.60 -5 -7 0 145.05 9.15 5 -7 0 157.63 12.62 -5 -7 0 149.57 10.78 5 -7 0 157.44 9.99 5 7 0 151.70 7.75 -5 7 0 143.10 10.68 -5 7 0 146.92 10.34 -5 7 0 147.34 9.68 5 7 0 161.94 7.83 5 7 0 156.12 9.31 5 7 0 159.18 11.15 6 -7 0 178.39 12.38 6 -7 0 168.55 12.40 -6 -7 0 161.04 12.15 -6 -7 0 192.69 10.99 6 -7 0 181.36 11.65 6 7 0 200.55 11.18 -6 7 0 194.86 11.76 6 7 0 189.39 8.31 6 7 0 187.40 12.94 6 7 0 187.69 8.31 -6 7 0 173.50 11.98 7 -7 0 65.94 6.71 7 -7 0 74.16 8.22 -7 -7 0 74.84 6.24 7 -7 0 71.73 7.22 7 7 0 71.55 6.34 7 7 0 61.87 8.49 8 -7 0 8.71 3.59 8 -7 0 5.88 3.82 -8 -7 0 7.75 3.08 8 -7 0 12.87 3.85 8 7 0 16.72 3.85 -8 7 0 12.46 4.32 8 7 0 4.39 3.45 9 -7 0 56.52 7.99 -9 -7 0 46.02 6.28 9 -7 0 49.59 7.57 9 -7 0 44.94 7.62 9 7 0 49.85 8.42 9 7 0 72.49 7.30 10 -7 0 39.57 7.10 10 -7 0 32.04 6.30 -10 -7 0 31.76 6.20 10 -7 0 44.83 8.10 10 7 0 31.61 7.66 10 7 0 27.20 5.40 11 -7 0 5.05 4.21 11 -7 0 4.77 3.58 11 -7 0 4.44 4.36 11 7 0 -1.59 3.52 11 7 0 0.76 3.82 12 -7 0 -4.71 3.83 12 -7 0 3.15 4.27 12 -7 0 7.28 4.54 12 7 0 3.85 5.30 12 7 0 2.61 3.72 13 -7 0 12.07 5.43 13 -7 0 12.07 7.06 13 -7 0 16.73 5.32 13 7 0 4.79 7.10 13 7 0 11.20 4.56 14 -7 0 33.71 7.95 14 -7 0 56.14 9.71 14 -7 0 30.77 6.53 14 7 0 26.71 9.60 -14 7 0 33.57 6.82 14 7 0 36.90 7.24 0 -8 0 38.25 4.02 0 -8 0 34.35 4.68 0 -8 0 31.53 4.46 0 8 0 30.95 4.37 0 8 0 34.05 4.78 0 8 0 28.98 4.09 -1 -8 0 93.90 7.00 1 -8 0 111.40 7.26 -1 -8 0 90.38 7.11 1 -8 0 95.40 7.82 1 -8 0 97.33 7.56 1 8 0 113.01 7.54 1 8 0 103.88 7.23 1 8 0 98.40 7.15 -1 8 0 97.05 7.46 -1 8 0 100.78 7.71 1 8 0 99.51 7.31 -1 8 0 100.06 6.94 2 -8 0 43.25 5.79 2 -8 0 47.21 5.95 -2 -8 0 46.43 4.60 2 -8 0 49.16 4.81 2 8 0 43.17 4.83 2 8 0 47.31 5.14 2 8 0 47.42 4.48 2 8 0 43.33 4.59 -2 8 0 53.37 4.70 2 8 0 52.03 4.77 -2 8 0 46.23 5.81 -3 -8 0 26.81 3.65 3 -8 0 26.54 4.05 3 -8 0 35.80 5.17 3 -8 0 27.85 4.85 -3 8 0 30.13 5.08 3 8 0 25.57 3.78 -3 8 0 27.76 4.64 3 8 0 29.90 3.71 3 8 0 33.32 4.98 -3 8 0 34.24 4.47 3 8 0 33.08 4.28 3 8 0 29.99 4.78 4 -8 0 47.00 6.55 4 -8 0 37.21 4.90 4 -8 0 43.20 6.18 4 8 0 43.25 5.69 4 8 0 46.77 4.10 -4 8 0 39.48 5.90 -4 8 0 42.32 4.58 4 8 0 43.33 5.87 4 8 0 45.52 4.60 4 8 0 42.26 3.95 -4 8 0 39.47 5.88 4 8 0 45.07 4.52 5 -8 0 159.35 11.83 -5 -8 0 160.23 11.44 5 -8 0 155.27 10.61 5 -8 0 175.93 11.87 -5 8 0 163.40 11.86 5 8 0 157.82 10.02 5 8 0 180.17 9.02 5 8 0 175.67 8.90 5 8 0 165.87 11.30 5 8 0 182.27 10.41 5 8 0 157.37 13.11 -5 8 0 169.49 10.64 6 -8 0 6.92 3.09 6 -8 0 7.65 3.03 -6 -8 0 6.14 2.32 6 -8 0 5.93 2.81 6 8 0 10.01 1.63 6 8 0 4.78 2.49 6 8 0 4.43 3.06 -6 8 0 5.27 2.70 6 8 0 8.06 2.52 7 -8 0 85.28 8.58 7 -8 0 72.78 7.69 7 -8 0 82.05 7.63 -7 -8 0 85.93 6.80 -7 8 0 73.75 7.41 7 8 0 73.60 6.60 7 8 0 88.98 8.72 8 -8 0 50.40 8.02 8 -8 0 68.78 8.86 -8 -8 0 60.36 7.84 8 -8 0 62.45 7.91 -8 8 0 67.18 8.25 8 8 0 71.27 6.84 8 8 0 61.65 9.15 -9 -8 0 25.05 5.04 9 -8 0 30.29 6.70 9 -8 0 39.35 6.82 9 -8 0 48.18 7.35 9 8 0 37.29 7.77 10 -8 0 -2.59 2.85 10 -8 0 1.43 3.54 10 -8 0 -0.72 2.72 10 8 0 0.15 4.79 10 8 0 -1.83 2.79 11 -8 0 244.10 17.36 11 -8 0 240.41 18.74 11 -8 0 263.51 17.74 11 8 0 259.36 19.66 11 8 0 243.66 15.91 12 -8 0 31.46 6.87 12 -8 0 27.17 6.31 12 -8 0 20.53 6.25 12 8 0 21.68 5.72 12 8 0 23.79 7.90 13 -8 0 10.88 5.29 13 -8 0 7.55 4.99 13 -8 0 -0.24 3.94 13 8 0 3.46 4.51 13 8 0 -1.72 5.98 0 -9 0 -1.72 1.46 0 -9 0 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133.06 17.38 0 -10 0 59.04 5.89 0 -10 0 41.94 6.06 0 10 0 45.10 6.25 0 10 0 49.81 5.27 0 10 0 45.48 6.02 0 10 0 60.41 5.76 1 -10 0 366.51 19.78 -1 -10 0 377.38 19.34 1 -10 0 387.11 18.89 -1 -10 0 365.64 18.91 1 -10 0 361.67 19.45 1 10 0 360.47 19.13 1 10 0 334.50 18.55 -1 10 0 343.66 19.27 1 10 0 347.52 19.05 -1 10 0 348.69 18.49 1 10 0 367.85 19.09 -1 10 0 357.64 19.55 -2 -10 0 105.22 7.89 2 -10 0 104.07 7.60 2 -10 0 95.03 8.40 2 10 0 105.52 8.39 2 10 0 102.81 7.76 -2 10 0 86.26 7.97 2 10 0 98.10 7.98 2 10 0 99.46 7.64 -2 10 0 84.94 7.11 2 10 0 100.85 7.79 3 -10 0 145.81 11.40 -3 -10 0 143.01 9.66 3 -10 0 156.48 11.15 3 -10 0 158.08 10.15 -3 10 0 155.83 10.04 3 10 0 145.96 10.75 3 10 0 154.14 9.97 3 10 0 156.46 10.79 3 10 0 147.14 9.92 -3 10 0 158.99 11.16 3 10 0 147.64 9.60 4 -10 0 9.39 3.76 4 -10 0 5.70 3.52 4 -10 0 9.96 3.30 4 10 0 5.17 2.50 4 10 0 8.87 3.49 4 10 0 9.91 3.04 4 10 0 8.07 3.26 4 10 0 14.51 3.28 4 10 0 12.71 2.84 -4 10 0 9.24 2.89 5 -10 0 5.18 3.13 5 -10 0 4.33 3.45 5 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9.36 -6 11 -5 45.75 5.18 6 11 5 62.21 5.46 6 11 5 41.73 7.32 6 11 5 50.92 4.99 7 -11 5 5.06 4.76 7 -11 5 1.52 2.24 7 -11 5 0.24 2.89 7 11 5 -2.54 4.24 7 11 5 0.75 1.53 7 11 5 4.98 2.02 -7 11 -5 -5.21 2.51 7 11 5 2.62 3.51 8 -11 5 90.10 7.54 8 -11 5 80.04 11.24 8 -11 5 108.32 11.54 8 11 5 56.05 10.10 8 11 5 78.83 5.84 8 11 5 98.04 10.18 9 -11 5 0.80 4.45 9 -11 5 7.04 5.28 9 -11 5 -0.67 2.43 -9 11 -5 -0.43 3.44 9 11 5 -1.43 3.60 9 11 5 4.29 5.96 10 -11 5 22.51 6.61 10 -11 5 27.07 8.11 10 -11 5 14.13 4.48 10 11 5 11.67 5.38 10 11 5 10.90 5.76 11 -12 -5 16.87 5.34 11 -12 -5 33.05 7.50 11 12 -5 16.18 7.55 -11 12 5 27.95 8.10 10 -12 -5 38.98 7.38 10 -12 -5 24.69 7.33 -10 12 5 28.86 6.76 10 12 -5 31.73 2.52 10 12 -5 14.54 6.72 9 -12 -5 61.33 9.30 9 -12 -5 45.43 8.60 9 12 -5 45.34 3.66 9 12 -5 53.31 3.32 -9 12 5 42.67 8.30 9 12 -5 35.61 7.46 8 -12 -5 129.70 12.54 8 -12 -5 130.60 12.06 8 12 -5 107.83 7.37 -8 12 5 129.38 12.27 8 12 -5 110.08 10.97 8 12 -5 112.61 7.62 8 12 -5 121.39 6.30 -7 -12 5 29.80 4.43 7 -12 -5 36.13 7.59 7 -12 -5 37.58 7.12 -7 12 5 25.99 7.27 7 12 -5 25.32 2.85 7 12 -5 22.85 4.05 7 12 -5 30.86 6.63 6 -12 -5 -1.80 2.57 -6 -12 5 1.06 2.19 6 -12 -5 -0.01 3.67 6 12 -5 -3.36 3.18 -6 12 5 -2.34 3.20 6 12 -5 -1.30 1.31 5 -12 -5 19.70 5.21 5 -12 -5 14.44 5.31 5 12 -5 18.82 2.96 5 12 -5 14.66 3.80 5 12 -5 20.59 4.29 -5 12 5 21.82 5.93 5 12 -5 11.18 2.35 -4 -12 5 195.74 12.66 4 -12 -5 204.87 14.95 4 -12 -5 194.18 14.13 4 12 -5 187.42 10.57 4 12 -5 181.47 12.12 4 12 -5 180.75 12.10 -4 12 5 188.68 14.03 4 12 -5 194.55 13.93 4 12 -5 190.79 10.56 3 -12 -5 43.29 7.50 3 -12 -5 43.72 7.33 -3 -12 5 47.27 6.78 3 12 -5 48.24 4.84 3 12 -5 44.13 4.77 -3 12 5 46.20 7.76 3 12 -5 44.48 5.03 3 12 -5 45.86 5.68 2 -12 -5 90.15 9.50 2 -12 -5 116.91 10.49 -2 -12 5 95.41 9.17 -2 -12 5 96.67 7.56 2 12 -5 113.63 7.87 -2 12 5 109.50 9.65 2 12 -5 110.15 7.60 2 12 -5 105.29 7.55 -1 -12 5 42.56 5.66 1 -12 -5 38.32 6.76 -1 -12 5 41.42 6.47 -1 12 5 46.48 7.04 1 12 -5 55.33 5.82 1 12 -5 40.18 4.20 -1 12 5 50.45 7.67 1 12 -5 38.13 4.23 0 -12 5 208.89 14.93 0 -12 5 248.02 14.25 0 -12 -5 253.97 16.10 0 12 5 229.04 15.34 0 12 5 219.40 14.70 0 12 -5 207.93 11.26 0 12 -5 216.25 11.37 0 12 -5 202.30 13.44 0 12 5 226.14 15.71 1 -12 5 5.76 3.97 1 -12 5 5.23 3.43 1 12 5 6.08 3.68 1 12 5 2.41 2.86 1 12 5 5.81 3.85 -1 12 -5 3.21 2.97 -1 12 -5 6.70 1.77 2 -12 5 32.18 6.62 2 -12 5 26.74 5.65 -2 12 -5 27.75 2.88 2 12 5 20.02 5.56 -2 12 -5 22.62 2.60 2 12 5 28.33 5.17 2 12 5 25.38 5.52 3 -12 5 4.85 3.40 3 -12 5 5.18 3.74 3 12 5 6.37 3.51 3 12 5 0.13 2.64 3 12 5 4.70 3.18 3 12 5 1.63 3.78 -3 12 -5 2.57 1.40 4 -12 5 80.32 9.05 4 -12 5 78.44 10.09 4 -12 5 82.16 5.32 4 12 5 97.43 9.13 -4 12 -5 74.83 5.56 4 12 5 83.12 7.58 4 12 5 83.60 7.55 4 12 5 94.93 10.10 5 -12 5 -2.54 2.39 5 -12 5 6.47 4.03 5 -12 5 4.33 1.90 5 12 5 -3.31 3.02 5 12 5 3.38 2.64 5 12 5 -0.73 3.06 5 12 5 1.63 2.53 -5 12 -5 0.06 2.10 6 -12 5 58.59 9.17 6 -12 5 69.81 10.17 6 -12 5 73.35 5.58 -6 12 -5 54.84 5.49 6 12 5 64.78 6.18 6 12 5 53.04 5.65 6 12 5 52.37 8.04 7 -12 5 28.21 6.38 7 -12 5 40.03 8.29 7 -12 5 30.96 4.51 7 12 5 22.75 3.76 7 12 5 32.52 6.29 -7 12 -5 21.40 4.63 7 12 5 34.71 8.38 7 12 5 32.96 4.24 8 -12 5 48.75 9.09 8 -12 5 36.86 8.27 8 -12 5 33.70 5.23 8 12 5 32.10 6.88 8 12 5 25.07 8.20 8 12 5 31.53 3.04 9 -12 5 19.47 6.69 9 -12 5 6.21 3.18 9 -12 5 26.32 7.10 9 12 5 -6.82 4.56 9 12 5 10.22 5.16 10 -13 -5 40.91 8.84 10 -13 -5 26.24 7.46 -10 13 5 19.32 7.31 10 13 -5 20.55 6.96 9 -13 -5 3.05 2.88 9 -13 -5 7.53 4.35 9 13 -5 1.80 1.61 9 13 -5 3.58 4.98 -9 13 5 -8.32 3.51 8 -13 -5 52.31 8.65 8 -13 -5 68.37 10.83 8 13 -5 66.00 3.97 -8 13 5 71.92 10.78 8 13 -5 62.76 5.54 8 13 -5 48.90 8.64 8 13 -5 52.50 5.42 -7 -13 5 30.43 4.68 7 -13 -5 18.40 5.91 7 -13 -5 39.57 7.55 -7 13 5 35.63 7.73 7 13 -5 25.90 3.01 7 13 -5 31.57 6.87 -6 -13 5 297.86 18.25 6 -13 -5 284.56 19.29 6 -13 -5 310.12 23.48 -6 13 5 336.96 21.64 6 13 -5 296.45 14.48 6 13 -5 297.51 14.53 6 13 -5 305.75 16.98 6 13 -5 287.88 18.32 -5 -13 5 3.40 2.72 5 -13 -5 0.48 3.36 5 -13 -5 4.13 3.27 -5 13 5 2.51 3.17 5 13 -5 -1.23 2.87 5 13 -5 5.51 3.28 5 13 -5 3.73 1.94 5 13 -5 2.88 1.80 4 -13 -5 209.28 15.08 4 -13 -5 197.08 15.65 -4 -13 5 206.56 13.87 4 13 -5 212.91 11.65 4 13 -5 200.10 11.59 4 13 -5 212.44 13.14 -4 13 5 230.16 16.38 4 13 -5 189.05 12.99 3 -13 -5 61.10 8.68 3 -13 -5 58.78 8.98 -3 -13 5 56.74 7.72 3 13 -5 54.40 5.38 3 13 -5 52.18 5.45 3 13 -5 55.38 5.79 -3 13 5 41.18 7.39 3 13 -5 53.11 5.89 2 -13 -5 13.47 4.85 2 -13 -5 16.78 5.57 -2 -13 5 13.79 4.53 -2 -13 5 17.77 3.97 -2 13 5 5.26 4.38 2 13 -5 14.94 3.52 2 13 -5 12.90 3.43 -2 13 5 13.18 4.76 2 13 -5 18.19 3.54 -1 -13 5 134.30 9.84 -1 -13 5 128.83 11.38 1 -13 -5 134.26 11.67 1 13 -5 122.67 9.64 -1 13 5 135.52 11.82 -1 13 5 148.47 11.95 1 13 -5 141.79 8.81 1 13 -5 140.76 8.57 0 -13 5 229.52 14.59 0 -13 5 255.03 16.66 0 13 -5 238.16 12.13 0 13 5 228.78 15.95 0 13 -5 213.29 14.28 0 13 -5 228.83 12.12 0 13 5 237.26 16.53 0 13 5 228.09 15.56 1 -13 5 10.04 4.11 1 -13 5 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41.93 4.20 -9 14 5 50.87 9.82 8 -14 -5 33.39 7.73 8 -14 -5 32.58 7.15 -8 14 5 16.95 6.54 8 14 -5 20.23 6.04 8 14 -5 24.50 4.12 8 14 -5 26.19 2.39 7 -14 -5 218.48 17.10 7 -14 -5 193.01 15.10 7 14 -5 187.47 14.37 -7 14 5 201.35 16.09 7 14 -5 173.78 9.42 7 14 -5 180.32 11.91 -6 -14 5 40.60 5.92 6 -14 -5 36.25 7.55 6 -14 -5 31.10 7.45 6 14 -5 39.59 3.98 6 14 -5 41.43 3.97 6 14 -5 39.58 7.17 -6 14 5 32.52 7.20 -5 -14 5 11.58 3.89 5 -14 -5 12.43 4.65 5 -14 -5 20.61 5.71 -5 14 5 18.21 5.80 5 14 -5 15.53 3.31 5 14 -5 7.13 4.44 5 14 -5 19.30 3.44 4 -14 -5 0.40 3.51 4 -14 -5 2.85 4.16 -4 -14 5 -6.15 1.76 4 14 -5 -0.30 2.06 4 14 -5 -1.58 3.50 4 14 -5 1.46 2.88 -4 14 5 -7.68 3.69 4 14 -5 1.77 2.35 3 -14 -5 -1.13 3.24 -3 -14 5 0.05 3.27 3 -14 -5 -2.71 2.98 3 14 -5 1.73 2.53 -3 14 5 -1.58 3.58 3 14 -5 -1.58 2.79 3 14 -5 -0.80 2.06 2 -14 -5 18.78 5.39 -2 -14 5 16.80 4.94 2 -14 -5 12.24 4.66 -2 -14 5 15.14 3.64 2 14 -5 14.35 3.64 2 14 -5 14.30 3.81 -2 14 5 23.98 5.94 2 14 -5 18.07 4.04 -2 14 5 20.79 5.91 2 14 -5 22.91 3.94 -1 -14 5 119.36 11.00 -1 -14 5 123.89 9.68 1 -14 -5 112.10 11.27 1 14 -5 107.33 9.44 1 14 -5 127.06 8.27 -1 14 5 146.19 12.10 -1 14 5 122.26 11.57 -1 14 5 133.10 11.75 1 14 -5 120.32 8.32 0 -14 5 68.42 7.46 0 -14 5 70.73 9.68 0 14 5 57.03 8.36 0 14 5 69.85 9.77 0 14 -5 74.13 5.63 0 14 5 58.81 8.97 1 -14 5 12.73 4.43 1 -14 5 14.80 4.77 -1 14 -5 15.89 2.48 1 14 5 10.31 5.03 -1 14 -5 9.12 2.37 1 14 5 16.62 5.02 1 14 5 5.91 3.88 2 -14 5 7.05 3.12 2 14 5 -0.48 3.06 -2 14 -5 0.78 1.61 2 14 5 -4.15 3.23 2 14 5 -2.56 2.22 3 -14 5 41.03 8.20 3 -14 5 49.55 7.83 3 14 5 23.96 5.30 3 14 5 52.28 9.15 3 14 5 62.40 8.48 -3 14 -5 34.56 3.32 4 -14 5 14.18 5.13 4 -14 5 6.44 4.02 -4 14 -5 15.81 2.51 4 14 5 13.83 5.20 4 14 5 10.44 4.03 4 14 5 15.00 5.11 5 -14 5 0.28 2.65 -5 14 -5 0.66 2.26 5 14 5 3.00 3.08 5 14 5 8.01 5.17 5 14 5 3.54 3.59 6 -14 5 17.94 3.22 6 -14 5 34.16 7.76 6 -14 5 39.82 7.84 6 14 5 20.78 6.67 6 14 5 30.26 6.71 6 14 5 32.94 5.54 7 -14 5 69.66 10.68 7 -14 5 65.42 5.81 7 -14 5 61.10 10.79 7 14 5 60.38 11.08 7 14 5 60.03 5.91 7 14 5 71.82 9.83 8 -15 -5 10.69 4.58 8 -15 -5 2.92 3.75 8 15 -5 -8.01 4.49 -8 15 5 -2.37 3.12 8 15 -5 0.05 2.55 7 -15 -5 38.28 7.88 7 -15 -5 29.92 7.31 -7 15 5 31.75 7.62 7 15 -5 21.91 6.48 7 15 -5 23.56 2.92 7 15 -5 39.37 5.71 6 -15 -5 -3.39 3.02 -6 -15 5 -3.75 2.69 6 -15 -5 3.07 4.01 6 15 -5 5.64 2.17 -6 15 5 -2.09 3.93 6 15 -5 -0.39 1.70 6 15 -5 -8.13 3.18 5 -15 -5 1.22 3.33 5 -15 -5 7.05 4.41 -5 -15 5 4.03 3.65 -5 15 5 6.53 4.68 5 15 -5 -3.52 3.71 5 15 -5 6.15 2.58 5 15 -5 5.33 2.86 -4 -15 5 26.39 5.93 4 -15 -5 36.82 7.77 4 -15 -5 41.63 8.19 4 15 -5 31.13 4.80 -4 15 5 29.73 7.49 4 15 -5 31.35 4.63 4 15 -5 32.67 5.91 -3 -15 5 -2.03 2.98 3 -15 -5 4.31 4.09 3 -15 -5 6.78 4.17 3 15 -5 1.19 2.98 3 15 -5 2.71 2.94 3 15 -5 -0.71 2.61 -3 15 5 4.04 4.36 3 15 -5 1.67 2.65 -2 -15 5 7.58 4.38 2 -15 -5 11.56 5.06 2 15 -5 9.74 3.42 2 15 -5 -2.17 2.66 2 15 -5 4.80 3.48 2 15 -5 7.00 3.02 -2 15 5 1.28 3.64 -2 15 5 4.89 5.04 -1 -15 5 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2.40 2.25 4 5 -6 2.84 1.97 -4 5 6 3.83 2.21 4 5 -6 4.51 2.24 -4 5 6 1.37 2.10 -4 5 6 3.95 2.15 -4 5 6 1.94 1.71 3 -5 -6 39.50 5.32 -3 -5 6 42.38 4.23 3 -5 -6 31.20 4.94 3 -5 -6 33.29 4.65 3 5 -6 32.49 3.40 3 5 -6 33.76 4.28 -3 5 6 32.77 4.60 -3 5 6 33.49 5.16 -3 5 6 35.22 4.97 -3 5 6 33.73 4.77 2 -5 -6 78.79 6.55 2 -5 -6 83.48 6.95 -2 -5 6 86.92 6.43 -2 -5 6 76.76 4.65 2 -5 -6 76.33 6.95 -2 -5 6 81.15 4.62 -2 5 6 88.89 6.89 -2 5 6 77.21 6.41 2 5 -6 77.68 4.48 2 5 -6 68.39 5.87 -2 5 6 88.56 6.89 2 5 -6 79.42 4.70 1 -5 -6 112.78 8.09 1 -5 -6 122.95 8.01 -1 -5 6 106.53 6.37 -1 -5 6 104.60 7.61 1 5 -6 101.98 6.27 -1 5 6 96.59 7.48 1 5 -6 110.22 7.59 -1 5 6 116.73 8.36 1 5 -6 106.21 4.81 -1 5 6 105.76 7.76 -1 5 6 110.29 7.53 0 -5 -6 0.06 2.30 0 -5 6 -1.08 1.72 0 -5 -6 -2.51 1.60 0 -5 6 0.01 1.65 0 5 -6 2.93 1.87 0 5 -6 1.24 2.27 0 5 6 0.65 2.10 0 5 6 3.50 1.95 0 5 6 0.32 1.76 0 5 6 -1.92 2.05 1 -5 6 499.65 23.45 -1 -5 -6 529.74 24.91 -1 -5 -6 475.85 24.13 -1 -5 -6 510.28 23.50 1 -5 6 469.09 24.11 1 5 6 531.74 24.99 1 5 6 485.83 24.20 -1 5 -6 463.36 23.18 -1 5 -6 492.54 24.04 1 5 6 529.39 24.54 1 5 6 489.35 23.40 -2 -5 -6 2015.46 80.92 2 -5 6 1978.16 78.42 -2 -5 -6 1864.57 81.98 2 -5 6 1926.33 82.20 2 -5 6 1940.38 81.65 2 5 6 1861.00 82.63 2 5 6 1954.07 82.75 -2 5 -6 1855.72 81.31 2 5 6 1773.38 81.88 2 5 6 1962.31 80.81 -2 5 -6 1922.94 82.00 3 -5 6 312.55 17.07 -3 -5 -6 279.73 16.93 3 -5 6 321.80 17.50 -3 -5 -6 338.93 15.95 3 -5 6 321.78 14.59 -3 5 -6 322.61 17.11 3 5 6 314.92 17.99 3 5 6 308.45 17.61 -3 5 -6 316.74 14.54 -3 5 -6 291.47 18.13 3 5 6 330.34 17.37 3 5 6 318.25 15.78 4 -5 6 134.95 9.96 4 -5 6 123.25 9.48 -4 -5 -6 139.21 8.12 -4 -5 -6 142.02 9.92 4 -5 6 120.52 7.53 -4 5 -6 134.24 7.70 4 5 6 115.15 9.38 -4 5 -6 122.68 9.35 4 5 6 140.15 10.22 4 5 6 110.00 11.35 -4 5 -6 120.30 9.18 4 5 6 134.94 7.97 -5 -5 -6 6.04 3.04 5 -5 6 10.89 3.69 5 -5 6 9.56 2.80 5 -5 6 6.55 2.97 -5 -5 -6 8.77 2.39 5 5 6 6.11 3.39 5 5 6 11.38 2.60 -5 5 -6 8.04 2.58 5 5 6 9.18 3.31 -5 5 -6 12.99 3.51 -5 5 -6 9.75 3.20 -6 -5 -6 80.21 6.10 6 -5 6 104.45 8.87 6 -5 6 93.28 7.51 6 -5 6 86.71 8.55 -6 5 -6 104.17 7.42 6 5 6 97.32 8.96 6 5 6 106.09 9.95 6 5 6 94.33 6.35 7 -5 6 42.45 6.18 -7 -5 -6 62.06 4.80 7 -5 6 51.86 7.68 7 -5 6 43.83 6.67 7 5 6 56.14 4.65 7 5 6 64.38 7.09 -7 5 -6 58.80 6.07 7 5 6 61.78 8.76 8 -5 6 28.18 5.62 8 -5 6 19.92 5.71 -8 -5 -6 20.66 3.02 8 5 6 9.73 4.72 -8 5 -6 18.38 4.74 8 5 6 22.26 3.02 8 5 6 15.18 4.61 9 -5 6 4.58 3.36 9 -5 6 0.49 3.99 9 -5 6 3.43 3.80 -9 -5 -6 2.31 1.76 9 5 6 1.57 3.60 9 5 6 4.91 1.70 9 5 6 -2.67 3.92 10 -5 6 18.09 5.59 10 -5 6 10.35 4.16 10 -5 6 6.82 4.74 10 5 6 13.41 11.08 10 5 6 22.69 6.17 10 5 6 15.81 2.16 11 -5 6 1.86 3.19 11 -5 6 -4.00 3.96 11 -5 6 4.66 4.02 11 5 6 -6.03 3.14 12 -5 6 -5.24 3.05 12 -5 6 4.39 4.56 12 -5 6 -2.70 4.39 12 5 6 -5.66 4.38 12 5 6 -1.87 6.33 15 -6 -6 13.25 5.77 15 -6 -6 26.44 7.40 15 6 -6 4.52 3.50 15 6 -6 17.71 7.20 -15 6 6 7.55 5.03 14 -6 -6 30.42 7.58 -14 -6 6 12.30 5.66 14 -6 -6 41.98 9.02 -14 6 6 19.26 5.86 14 6 -6 20.91 7.60 14 6 -6 29.30 5.17 13 -6 -6 0.13 3.71 13 -6 -6 3.61 4.75 13 6 -6 -1.22 3.76 -13 6 6 -5.49 2.62 13 6 -6 6.59 3.00 12 -6 -6 -0.55 4.09 12 -6 -6 -1.25 3.38 -12 -6 6 -0.65 2.42 12 6 -6 6.54 5.70 -12 6 6 0.67 3.17 12 6 -6 3.70 2.48 11 -6 -6 86.15 11.16 -11 -6 6 62.11 5.87 11 -6 -6 79.42 10.49 11 6 -6 75.30 6.02 -11 6 6 86.15 8.67 11 6 -6 78.00 10.24 10 -6 -6 25.59 6.19 -10 -6 6 29.95 3.76 10 -6 -6 31.67 6.26 -10 6 6 26.26 5.60 10 6 -6 39.06 7.51 10 6 -6 33.76 3.69 9 -6 -6 19.56 4.86 -9 -6 6 25.06 1.93 9 -6 -6 26.82 5.74 9 6 -6 20.79 5.63 -9 6 6 17.72 4.67 9 6 -6 31.37 2.08 9 6 -6 24.55 3.08 -8 -6 6 446.56 19.99 8 -6 -6 444.76 25.24 -8 -6 6 446.67 24.54 8 -6 -6 456.22 25.00 -8 -6 6 470.00 20.43 -8 6 6 558.04 25.36 8 6 -6 455.47 24.72 8 6 -6 439.39 20.30 -7 -6 6 1.06 2.28 -7 -6 6 0.67 1.36 7 -6 -6 0.14 1.98 7 -6 -6 2.48 3.21 7 6 -6 0.72 0.39 7 6 -6 -0.15 1.29 -7 6 6 4.49 2.94 7 6 -6 0.24 0.45 7 6 -6 2.11 2.87 -7 6 6 4.91 2.88 -7 6 6 -5.42 1.92 -6 -6 6 60.58 4.65 -6 -6 6 58.98 6.18 6 -6 -6 57.84 8.63 6 -6 -6 61.44 6.79 6 6 -6 67.19 6.34 -6 6 6 53.96 7.14 -6 6 6 61.53 6.64 -6 6 6 69.12 7.49 -6 6 6 55.06 6.10 6 6 -6 50.21 4.41 5 -6 -6 673.47 32.98 -5 -6 6 651.82 31.45 -5 -6 6 688.65 30.65 5 -6 -6 700.16 33.33 -5 6 6 687.45 32.96 -5 6 6 701.08 32.75 5 6 -6 722.81 30.62 -5 6 6 642.75 32.27 -5 6 6 681.92 32.96 5 6 -6 698.77 31.71 4 -6 -6 354.18 19.17 -4 -6 6 351.32 17.19 -4 -6 6 346.36 17.23 4 -6 -6 330.60 18.76 4 6 -6 357.11 17.15 -4 6 6 339.29 18.53 4 6 -6 363.89 17.34 -4 6 6 348.14 18.80 -3 -6 6 898.89 39.48 3 -6 -6 872.33 40.88 -3 -6 6 889.99 36.61 3 -6 -6 889.40 40.78 -3 -6 6 896.94 38.41 -3 6 6 876.13 40.71 -3 6 6 870.27 40.35 3 6 -6 946.78 39.46 3 6 -6 864.51 38.24 3 6 -6 904.38 36.62 -3 6 6 846.84 40.65 -2 -6 6 1470.82 61.54 2 -6 -6 1382.11 62.41 -2 -6 6 1454.22 59.71 2 -6 -6 1396.61 62.22 -2 -6 6 1382.85 59.08 -2 6 6 1404.43 62.22 -2 6 6 1417.06 61.86 -2 6 6 1437.98 62.54 2 6 -6 1424.49 59.12 2 6 -6 1431.84 61.24 -2 6 6 1447.02 61.92 1 -6 -6 120.97 8.91 -1 -6 6 106.20 7.86 -1 -6 6 111.90 6.85 1 -6 -6 119.13 8.26 -1 6 6 116.99 8.48 -1 6 6 111.72 8.28 -1 6 6 123.55 8.47 -1 6 6 116.53 8.79 1 6 -6 112.44 5.10 1 6 -6 119.87 8.21 1 6 -6 113.65 6.88 -1 6 6 120.87 8.33 1 6 -6 114.99 5.12 0 -6 -6 -0.31 2.06 0 -6 -6 0.73 1.93 0 -6 6 -1.31 1.44 0 -6 6 -1.87 1.42 0 6 6 -0.53 2.18 0 6 6 1.13 1.73 0 6 6 3.00 2.24 0 6 -6 0.28 1.67 0 6 6 2.89 2.19 0 6 -6 0.76 1.54 1 -6 6 35.18 4.75 -1 -6 -6 34.18 4.67 1 -6 6 31.01 4.90 -1 -6 -6 32.38 5.22 1 6 6 29.65 4.89 -1 6 -6 38.42 5.17 1 6 6 37.26 5.30 1 6 6 27.47 4.13 1 6 6 33.81 5.22 -1 6 -6 25.44 4.01 -2 -6 -6 120.30 9.14 -2 -6 -6 132.29 8.41 2 -6 6 128.64 9.44 2 -6 6 129.49 8.94 -2 6 -6 130.69 9.13 -2 6 -6 119.24 8.65 2 6 6 126.90 8.17 2 6 6 125.95 9.57 2 6 6 118.30 9.16 2 6 6 119.71 9.70 -3 -6 -6 4.50 2.01 -3 -6 -6 6.37 2.44 3 -6 6 3.83 2.72 -3 6 -6 0.28 2.50 -3 6 -6 4.95 1.34 3 6 6 5.71 2.44 3 6 6 -0.87 2.36 -3 6 -6 2.57 2.72 3 6 6 7.37 2.80 4 -6 6 427.69 21.84 -4 -6 -6 401.09 19.22 -4 -6 -6 392.20 21.17 4 -6 6 395.67 18.41 -4 6 -6 376.79 18.76 4 6 6 390.88 22.18 -4 6 -6 401.86 21.30 4 6 6 403.73 19.18 -4 6 -6 379.67 21.11 4 6 6 411.75 23.87 5 -6 6 21.17 3.42 5 -6 6 22.94 4.72 5 -6 6 22.45 4.61 -5 -6 -6 15.63 2.87 -5 -6 -6 10.58 4.38 5 6 6 24.48 5.33 -5 6 -6 19.80 3.29 5 6 6 21.55 3.28 5 6 6 17.86 4.63 -6 -6 -6 23.67 3.40 6 -6 6 28.60 5.35 6 -6 6 29.97 6.11 6 -6 6 26.40 4.09 6 6 6 24.62 3.39 6 6 6 27.36 5.75 6 6 6 29.01 6.06 -6 6 -6 30.33 4.41 -7 -6 -6 4.06 1.81 7 -6 6 9.83 4.31 7 -6 6 3.00 2.86 7 -6 6 3.84 2.59 7 6 6 7.25 3.94 7 6 6 12.90 4.94 -7 6 -6 -0.37 2.29 7 6 6 8.51 2.12 8 -6 6 8.48 4.03 8 -6 6 5.49 3.52 -8 -6 -6 12.15 2.42 8 -6 6 14.08 4.00 -8 6 -6 9.98 3.50 8 6 6 12.91 4.54 8 6 6 7.75 2.08 8 6 6 13.19 5.54 9 -6 6 8.82 5.11 9 -6 6 4.64 3.54 9 -6 6 9.10 3.79 9 6 6 7.78 4.55 9 6 6 1.90 3.59 9 6 6 6.93 1.64 10 -6 6 198.55 14.11 10 -6 6 181.03 14.06 10 -6 6 200.75 16.55 10 6 6 177.71 16.25 10 6 6 202.61 15.62 11 -6 6 1.11 3.65 11 -6 6 4.65 4.19 11 -6 6 -5.05 3.32 11 6 6 -5.67 3.69 11 6 6 -8.01 4.31 12 -6 6 -3.58 4.48 12 -6 6 1.33 3.50 12 -6 6 5.68 4.91 12 6 6 -5.50 4.13 12 6 6 -1.40 3.46 14 -7 -6 151.10 14.39 14 -7 -6 136.99 13.82 14 7 -6 86.48 13.56 -13 -7 6 -0.08 3.33 13 -7 -6 2.93 4.30 13 -7 -6 -0.47 4.07 -13 7 6 -6.47 2.50 13 7 -6 2.22 2.54 13 7 -6 -2.44 4.86 12 -7 -6 5.37 3.40 -12 -7 6 1.77 2.56 12 7 -6 5.69 2.35 -12 7 6 0.80 3.72 12 7 -6 7.64 5.73 -11 -7 6 3.79 2.17 11 -7 -6 -0.59 3.68 11 -7 -6 1.75 3.00 -11 7 6 1.57 3.48 11 7 -6 0.70 4.00 11 7 -6 4.63 1.94 -10 -7 6 132.35 7.55 10 -7 -6 138.89 12.31 10 -7 -6 99.31 10.64 -10 7 6 137.31 10.94 10 7 -6 137.12 7.65 10 7 -6 129.74 12.06 -9 -7 6 170.58 7.78 9 -7 -6 166.15 13.05 9 -7 -6 167.11 13.54 -9 -7 6 198.04 8.80 9 7 -6 176.34 8.70 -9 7 6 159.23 12.57 9 7 -6 165.38 13.21 9 7 -6 160.07 7.72 8 -7 -6 6.45 3.06 -8 -7 6 8.96 1.80 8 -7 -6 13.32 4.37 -8 7 6 13.20 3.90 8 7 -6 7.98 1.20 8 7 -6 7.25 1.10 8 7 -6 11.25 4.27 7 -7 -6 6.75 3.16 -7 -7 6 0.46 2.63 7 -7 -6 4.01 3.30 -7 -7 6 1.77 1.52 7 7 -6 2.36 3.08 -7 7 6 0.33 2.09 7 7 -6 2.29 1.57 -6 -7 6 123.07 7.80 6 -7 -6 121.25 10.33 6 -7 -6 121.38 10.39 -6 -7 6 128.24 9.34 6 7 -6 152.47 10.07 6 7 -6 130.72 7.86 -6 7 6 132.04 10.18 -6 7 6 136.52 10.38 -5 -7 6 61.99 5.28 5 -7 -6 49.47 7.99 5 -7 -6 61.12 7.87 -5 -7 6 59.30 5.56 -5 7 6 65.07 6.89 -5 7 6 67.76 6.91 -5 7 6 71.83 7.02 -5 7 6 56.91 7.14 5 7 -6 62.67 5.17 5 7 -6 65.54 6.31 -4 -7 6 140.40 8.64 -4 -7 6 143.48 8.90 4 -7 -6 139.52 10.49 4 7 -6 160.74 9.10 -4 7 6 140.80 10.26 -4 7 6 127.42 9.74 -4 7 6 151.95 10.54 4 7 -6 133.00 8.67 -4 7 6 115.52 10.43 -3 -7 6 217.49 11.49 3 -7 -6 217.02 13.95 3 -7 -6 226.92 14.04 -3 -7 6 235.12 10.32 -3 -7 6 230.28 12.78 3 7 -6 204.03 12.32 -3 7 6 218.60 13.43 -3 7 6 231.67 14.07 3 7 -6 233.46 11.70 -3 7 6 220.65 13.37 3 7 -6 237.76 10.36 2 -7 -6 55.94 5.90 -2 -7 6 60.94 5.53 -2 -7 6 57.22 4.11 2 -7 -6 61.89 6.13 2 7 -6 56.93 4.13 2 7 -6 63.54 4.02 2 7 -6 66.90 5.88 -2 7 6 58.53 6.23 2 7 -6 57.55 4.00 -2 7 6 63.47 8.29 -2 7 6 57.77 5.73 -1 -7 6 242.63 14.23 1 -7 -6 241.12 14.99 -1 -7 6 262.00 12.91 1 7 -6 253.96 11.00 -1 7 6 267.18 14.61 -1 7 6 276.04 15.15 -1 7 6 252.84 14.34 1 7 -6 258.51 11.02 1 7 -6 250.07 14.30 1 7 -6 244.43 12.77 0 -7 -6 147.35 10.36 0 -7 6 141.74 9.74 0 -7 6 127.04 8.38 0 7 6 132.43 10.00 0 7 6 129.24 9.02 0 7 6 125.52 9.57 0 7 -6 140.16 8.44 0 7 6 144.33 11.04 0 7 6 138.28 9.29 1 -7 6 0.61 1.78 1 -7 6 -0.74 2.27 -1 -7 -6 0.26 1.64 -1 -7 -6 0.35 1.72 1 7 6 -1.89 1.12 1 7 6 0.69 1.86 1 7 6 0.12 2.04 -1 7 -6 0.05 1.93 1 7 6 0.03 2.32 -1 7 -6 0.59 1.50 1 7 6 1.03 1.53 1 7 6 3.80 2.07 -2 -7 -6 49.71 4.99 2 -7 6 48.12 6.03 2 -7 6 49.58 6.43 2 7 6 41.75 6.34 2 7 6 50.52 4.88 -2 7 -6 47.28 6.23 2 7 6 50.61 7.03 2 7 6 51.52 5.69 -2 7 -6 48.92 5.99 2 7 6 47.43 5.03 2 7 6 52.52 5.87 -3 -7 -6 88.63 7.84 -3 -7 -6 97.53 6.86 3 -7 6 88.80 4.77 3 -7 6 102.37 8.24 3 -7 6 86.60 8.09 -3 7 -6 104.33 9.41 -3 7 -6 81.25 4.71 -3 7 -6 74.02 7.36 3 7 6 91.91 6.80 3 7 6 82.32 6.44 3 7 6 93.20 8.80 3 7 6 80.09 9.08 -4 -7 -6 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4.78 6 9 7 7.66 4.11 6 9 7 8.36 2.53 6 9 7 3.78 2.37 7 -9 7 24.83 5.80 7 -9 7 23.03 6.54 7 -9 7 25.78 4.03 -7 9 -7 20.69 3.97 7 9 7 21.22 6.93 7 9 7 19.74 6.11 7 9 7 22.69 3.68 7 9 7 22.37 3.57 8 -9 7 10.09 4.40 8 -9 7 6.80 2.77 8 -9 7 10.04 6.32 -8 9 -7 8.93 3.75 8 9 7 14.31 5.71 8 9 7 1.78 4.65 8 9 7 9.29 2.25 8 9 7 10.89 2.38 9 -9 7 17.00 5.12 9 -9 7 22.56 4.80 9 -9 7 19.63 6.35 9 9 7 20.99 2.14 -9 9 -7 7.24 4.33 9 9 7 11.56 6.33 10 -9 7 34.96 7.96 10 -9 7 72.74 7.78 10 -9 7 88.74 12.02 10 9 7 45.19 10.12 10 9 7 54.50 9.53 13 -10 -7 10.42 5.62 13 -10 -7 12.12 6.37 -13 10 7 11.92 6.12 13 10 -7 10.17 5.25 12 -10 -7 5.79 3.13 12 -10 -7 14.96 5.79 12 10 -7 7.49 5.46 -12 10 7 11.30 5.55 11 -10 -7 69.11 10.44 11 -10 -7 72.61 10.73 11 10 -7 60.39 9.90 -11 10 7 51.08 9.01 10 -10 -7 17.25 6.04 10 -10 -7 18.20 6.36 10 10 -7 7.03 5.28 9 -10 -7 148.47 13.65 9 -10 -7 149.11 13.13 -9 -10 7 151.68 8.25 9 10 -7 145.14 13.04 -9 10 7 150.12 13.10 9 10 -7 142.02 8.18 8 -10 -7 370.15 23.45 -8 -10 7 381.56 18.86 8 -10 -7 395.60 24.16 -8 10 7 398.02 23.41 8 10 -7 390.57 18.86 8 10 -7 401.43 22.53 -7 -10 7 27.77 5.75 7 -10 -7 33.18 6.55 7 -10 -7 24.41 5.62 -7 -10 7 31.75 4.51 -7 10 7 13.76 5.19 7 10 -7 24.86 4.25 7 10 -7 29.99 5.80 6 -10 -7 156.61 12.57 -6 -10 7 138.11 10.41 -6 -10 7 145.70 9.79 6 -10 -7 137.08 12.18 6 10 -7 147.90 10.81 -6 10 7 159.35 12.58 6 10 -7 141.56 9.62 5 -10 -7 135.57 11.27 -5 -10 7 129.93 9.37 -5 -10 7 144.13 9.76 5 -10 -7 135.42 11.28 5 10 -7 138.84 9.61 5 10 -7 143.96 9.76 5 10 -7 136.60 9.22 -5 10 7 121.51 11.11 4 -10 -7 102.04 9.40 4 -10 -7 85.92 8.71 4 10 -7 85.32 7.00 4 10 -7 97.74 5.20 -4 10 7 105.16 9.24 4 10 -7 83.25 7.63 4 10 -7 98.51 7.01 3 -10 -7 149.20 11.87 -3 -10 7 126.46 7.56 3 -10 -7 140.37 11.56 -3 -10 7 141.91 10.54 3 10 -7 141.94 8.20 3 10 -7 134.33 8.25 3 10 -7 138.55 10.20 3 10 -7 145.12 7.91 -2 -10 7 46.87 6.64 2 -10 -7 48.22 7.26 -2 -10 7 47.60 4.42 2 -10 -7 47.31 7.25 2 10 -7 45.42 3.51 2 10 -7 38.71 3.50 -2 10 7 48.41 7.49 -2 10 7 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175.98 14.55 4 -12 7 216.28 15.33 4 12 7 205.79 16.56 4 12 7 197.84 15.02 4 12 7 187.92 12.81 5 -12 7 25.08 6.72 5 -12 7 12.00 4.55 5 12 7 11.11 4.25 5 12 7 19.10 4.41 5 12 7 17.32 4.04 5 12 7 22.44 6.43 6 -12 7 1.04 4.62 6 12 7 8.53 3.21 6 12 7 15.73 6.44 6 12 7 4.26 4.21 6 12 7 5.94 2.99 -6 12 -7 3.61 1.40 7 -12 7 91.89 11.99 7 -12 7 106.03 6.53 7 -12 7 137.44 13.09 7 12 7 95.32 13.79 7 12 7 113.15 7.98 -7 12 -7 88.93 6.44 7 12 7 109.92 7.89 8 -12 7 -4.33 3.74 8 -12 7 5.18 2.48 8 -12 7 7.83 4.29 8 12 7 -2.56 4.06 8 12 7 -7.89 4.66 8 12 7 3.06 2.00 10 -13 -7 0.90 4.83 10 -13 -7 -0.82 3.79 10 13 -7 -7.22 4.81 10 13 -7 -0.07 1.38 -10 13 7 -7.81 3.72 -9 -13 7 0.82 2.22 9 -13 -7 0.20 4.10 9 -13 -7 2.00 3.46 -9 13 7 -3.22 3.64 9 13 -7 -0.05 3.90 9 13 -7 -4.04 2.43 8 -13 -7 3.12 3.47 -8 -13 7 1.45 2.43 8 -13 -7 0.38 3.56 8 13 -7 -3.75 4.16 -8 13 7 0.53 4.47 7 -13 -7 149.81 13.32 -7 -13 7 137.23 9.90 7 -13 -7 133.08 13.26 7 13 -7 137.30 11.65 -7 13 7 142.94 13.50 7 13 -7 131.57 9.91 6 -13 -7 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5 4 -9 216.11 13.10 5 4 -9 240.12 13.52 4 -4 -9 13.15 3.18 -4 -4 9 11.48 1.59 -4 -4 9 12.71 1.60 4 -4 -9 13.63 3.63 -4 -4 9 14.49 2.95 -4 -4 9 15.06 3.33 4 -4 -9 12.52 3.63 4 4 -9 11.57 3.01 -4 4 9 16.54 4.39 4 4 -9 10.84 2.64 -4 4 9 13.10 3.50 -4 4 9 12.58 3.48 -4 4 9 11.93 3.14 3 -4 -9 284.28 15.95 3 -4 -9 279.61 16.53 -3 -4 9 293.87 13.49 -3 -4 9 283.16 14.05 -3 -4 9 310.46 15.89 -3 4 9 295.15 16.09 3 4 -9 283.30 14.09 -3 4 9 275.34 16.23 -3 4 9 292.52 16.12 -3 4 9 279.18 15.98 3 4 -9 292.83 15.53 3 4 -9 297.80 13.41 -2 -4 9 30.26 4.72 -2 -4 9 33.00 3.46 2 -4 -9 32.18 5.35 2 -4 -9 35.38 4.99 -2 -4 9 36.83 3.23 -2 4 9 33.01 4.84 -2 4 9 32.84 4.90 -2 4 9 29.78 4.84 -2 4 9 36.50 5.28 2 4 -9 28.63 4.66 2 4 -9 29.75 2.97 2 4 -9 28.74 3.21 1 -4 -9 597.73 29.28 1 -4 -9 597.91 30.01 -1 -4 9 611.46 29.57 -1 -4 9 650.96 28.23 -1 -4 9 622.91 26.52 -1 4 9 603.57 29.64 -1 4 9 647.03 29.63 -1 4 9 604.66 29.93 -1 4 9 581.78 29.70 1 4 -9 614.81 26.50 1 4 -9 612.26 29.35 1 4 -9 686.86 28.19 0 -4 9 183.82 11.34 0 -4 9 170.73 10.19 0 -4 -9 153.00 11.84 0 -4 9 160.47 8.03 0 -4 -9 166.46 10.63 0 -4 -9 163.48 11.05 0 -4 9 176.74 8.15 0 4 9 160.32 10.57 0 4 9 174.63 11.42 0 4 -9 161.53 11.81 0 4 -9 171.06 9.99 0 4 9 178.14 11.70 -1 -4 -9 1.61 2.17 1 -4 9 -0.74 1.69 -1 -4 -9 3.08 2.49 -1 -4 -9 -0.62 2.02 1 -4 9 -0.73 1.87 1 -4 9 -0.47 1.00 -1 4 -9 -0.27 2.13 -1 4 -9 1.50 1.91 1 4 9 0.82 2.12 1 4 9 2.66 2.12 1 4 9 -1.11 2.22 -2 -4 -9 106.65 7.75 -2 -4 -9 101.25 8.44 2 -4 9 90.82 8.00 2 -4 9 98.24 5.99 2 -4 9 100.28 5.98 2 4 9 99.23 8.54 -2 4 -9 116.43 8.41 -2 4 -9 99.95 7.99 2 4 9 99.72 8.47 2 4 9 97.19 7.57 2 4 9 107.41 8.94 3 -4 9 317.60 18.28 3 -4 9 286.40 17.67 -3 -4 -9 303.58 16.66 3 -4 9 333.59 15.62 3 -4 9 310.79 15.30 3 4 9 340.33 18.80 -3 4 -9 286.62 17.37 3 4 9 352.73 19.06 3 4 9 329.33 18.59 -3 4 -9 329.93 17.92 3 4 9 307.36 16.81 4 -4 9 129.66 10.10 4 -4 9 136.51 8.66 -4 -4 -9 133.12 9.23 4 -4 9 122.06 8.09 4 -4 9 142.29 11.01 4 4 9 129.12 10.51 4 4 9 137.85 11.18 4 4 9 144.27 9.52 5 -4 9 2.39 2.72 5 -4 9 1.50 2.91 -5 -4 -9 5.85 2.73 5 -4 9 3.69 4.26 5 -4 9 3.62 2.13 -5 4 -9 0.94 2.11 5 4 9 1.67 3.54 5 4 9 -2.09 1.82 5 4 9 -0.03 3.10 -6 -4 -9 97.32 8.14 6 -4 9 125.79 10.44 6 -4 9 117.47 9.17 6 -4 9 118.21 11.08 6 4 9 121.53 8.57 6 4 9 131.59 11.19 6 4 9 131.56 10.79 -6 4 -9 116.92 8.88 -7 -4 -9 2.58 2.72 7 -4 9 1.91 2.99 7 -4 9 5.29 3.52 7 -4 9 7.58 5.02 7 4 9 1.22 3.65 -7 4 -9 -3.47 2.55 7 4 9 9.17 2.87 7 4 9 4.31 3.46 8 -4 9 37.24 7.93 8 -4 9 30.01 5.97 -8 -4 -9 31.00 4.70 8 -4 9 32.24 6.10 8 4 9 25.62 4.48 8 4 9 24.56 6.21 8 4 9 30.40 7.26 -9 -4 -9 64.83 6.94 9 -4 9 60.47 8.32 9 -4 9 58.13 8.25 9 -4 9 76.18 11.04 9 4 9 43.38 8.05 9 4 9 37.55 5.31 10 -4 9 5.84 3.92 -10 -4 -9 2.92 3.51 10 -4 9 10.25 4.72 10 -4 9 14.23 6.13 10 4 9 3.96 5.30 10 4 9 11.17 3.47 10 4 9 15.25 7.01 11 -4 9 6.47 4.91 11 -4 9 3.26 4.97 11 -4 9 -3.32 3.16 11 4 9 -5.03 4.39 11 4 9 3.27 2.45 11 4 9 -0.72 5.30 15 -5 -9 4.14 5.11 15 -5 -9 5.83 4.18 15 5 -9 2.09 5.08 -15 5 9 9.13 4.46 14 -5 -9 121.24 13.25 -14 -5 9 91.88 8.94 14 -5 -9 130.71 12.77 -14 5 9 127.79 11.42 14 5 -9 128.96 8.93 14 5 -9 132.45 13.88 13 -5 -9 30.86 6.72 -13 -5 9 25.24 4.39 13 -5 -9 33.26 7.64 -13 5 9 34.32 6.62 13 5 -9 26.90 7.53 13 5 -9 31.22 4.37 12 -5 -9 17.58 5.78 -12 -5 9 18.32 2.45 -12 -5 9 14.30 3.09 12 -5 -9 30.57 6.80 -12 5 9 15.66 4.47 12 5 -9 25.01 6.39 12 5 -9 16.72 2.89 -11 -5 9 2.69 1.66 11 -5 -9 10.89 4.26 11 -5 -9 4.28 3.78 -11 -5 9 3.41 1.68 -11 -5 9 3.24 1.80 11 5 -9 4.16 1.75 -11 5 9 -3.00 2.50 11 5 -9 3.50 4.15 -10 -5 9 99.16 5.72 10 -5 -9 114.72 11.35 10 -5 -9 96.46 9.98 -10 -5 9 104.54 6.99 10 5 -9 118.70 10.87 -10 5 9 115.13 9.77 10 5 -9 101.54 6.83 10 5 -9 107.35 6.15 9 -5 -9 63.56 9.25 -9 -5 9 61.00 3.15 -9 -5 9 61.17 5.24 9 -5 -9 51.73 7.72 -9 5 9 71.24 7.22 9 5 -9 55.79 4.99 9 5 -9 62.21 8.11 -8 -5 9 349.82 19.78 -8 -5 9 364.93 17.64 8 -5 -9 365.80 21.44 8 -5 -9 342.55 20.00 8 5 -9 314.67 17.18 8 5 -9 376.36 20.19 -8 5 9 346.31 19.76 7 -5 -9 21.50 5.75 -7 -5 9 16.42 3.34 -7 -5 9 22.69 4.89 7 -5 -9 38.98 5.87 7 5 -9 20.19 4.43 -7 5 9 26.61 5.88 7 5 -9 17.91 3.45 -7 5 9 25.01 4.95 6 -5 -9 1.21 2.22 6 -5 -9 -1.75 1.25 -6 -5 9 -1.11 2.09 6 -5 -9 1.01 1.95 -6 -5 9 -0.55 1.87 -6 5 9 -3.29 2.26 -6 5 9 2.95 2.76 -6 5 9 0.81 2.61 6 5 -9 1.72 1.92 -6 5 9 0.68 1.77 6 5 -9 0.28 1.95 5 -5 -9 6.86 3.25 -5 -5 9 11.33 2.96 5 -5 -9 11.75 3.37 5 -5 -9 9.81 3.45 -5 -5 9 11.04 2.99 -5 5 9 4.53 3.02 5 5 -9 11.56 2.83 5 5 -9 8.39 2.70 -5 5 9 4.79 3.07 -5 5 9 13.55 4.08 -4 -5 9 610.04 28.84 4 -5 -9 603.43 29.82 -4 -5 9 609.84 25.21 -4 -5 9 647.00 27.86 4 -5 -9 707.58 30.44 4 -5 -9 625.96 30.72 -4 5 9 509.34 28.91 4 5 -9 604.67 27.67 -4 5 9 567.04 29.89 4 5 -9 650.18 28.88 -4 5 9 587.49 29.67 3 -5 -9 27.87 4.97 3 -5 -9 16.39 3.69 -3 -5 9 19.78 2.64 -3 -5 9 21.42 3.40 -3 -5 9 22.88 3.91 3 5 -9 19.02 2.70 -3 5 9 22.43 4.17 -3 5 9 20.57 4.65 3 5 -9 19.72 2.14 -3 5 9 17.54 4.10 3 5 -9 20.69 4.09 -3 5 9 24.78 4.54 -2 -5 9 1229.20 51.14 -2 -5 9 1260.41 52.07 2 -5 -9 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3.31 3 -5 9 36.59 7.07 3 -5 9 36.65 6.02 -3 -5 -9 41.07 5.33 3 -5 9 37.80 3.62 -3 5 -9 43.00 6.26 3 5 9 41.59 6.84 3 5 9 34.01 4.98 3 5 9 42.51 6.56 4 -5 9 778.49 37.22 -4 -5 -9 784.40 35.26 4 -5 9 789.71 33.83 4 -5 9 776.41 37.23 4 -5 9 743.40 33.56 4 5 9 707.20 37.58 4 5 9 693.48 36.95 4 5 9 819.99 35.53 5 -5 9 166.29 9.74 5 -5 9 152.96 12.02 5 -5 9 151.18 12.40 5 -5 9 156.25 9.69 -5 -5 -9 159.47 10.22 5 5 9 157.69 12.61 -5 5 -9 145.90 9.53 5 5 9 167.75 13.25 5 5 9 167.75 10.51 6 -5 9 57.72 5.93 -6 -5 -9 49.96 5.96 6 -5 9 45.79 7.46 6 -5 9 43.21 7.31 -6 5 -9 46.87 5.80 6 5 9 54.34 8.57 6 5 9 45.40 5.75 6 5 9 50.83 8.57 -7 -5 -9 62.89 6.13 7 -5 9 61.70 9.48 7 -5 9 83.94 7.71 7 -5 9 65.45 8.55 -7 5 -9 61.44 8.12 7 5 9 68.28 9.27 7 5 9 56.28 9.44 7 5 9 73.80 6.36 8 -5 9 104.53 9.22 -8 -5 -9 94.37 7.39 8 -5 9 96.31 9.90 8 -5 9 127.42 12.05 -8 5 -9 85.68 8.50 8 5 9 94.63 10.71 8 5 9 118.06 11.70 8 5 9 103.37 7.68 9 -5 9 99.55 11.28 9 -5 9 120.29 11.13 -9 -5 -9 90.96 8.02 9 -5 9 124.42 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6 -9 27.79 3.80 -8 -6 9 27.01 3.97 -8 -6 9 11.85 4.26 8 -6 -9 23.22 5.39 8 -6 -9 26.59 6.25 8 6 -9 23.64 4.95 8 6 -9 24.99 3.69 -8 6 9 19.59 4.70 7 -6 -9 44.22 6.99 -7 -6 9 32.85 4.50 7 -6 -9 28.08 5.75 -7 6 9 32.10 5.74 7 6 -9 35.33 4.62 7 6 -9 23.24 4.66 6 -6 -9 67.13 8.89 -6 -6 9 66.96 6.26 6 -6 -9 75.05 7.73 -6 -6 9 68.45 6.55 6 6 -9 76.36 6.81 -6 6 9 77.13 7.31 6 6 -9 69.98 5.93 5 -6 -9 2.94 2.73 -5 -6 9 -0.55 1.74 5 -6 -9 -0.60 2.74 -5 -6 9 0.75 1.81 -5 6 9 2.31 1.99 5 6 -9 1.56 1.76 5 6 -9 2.06 1.91 -5 6 9 -0.10 2.50 -4 -6 9 22.13 4.17 4 -6 -9 27.07 4.85 -4 -6 9 23.05 3.42 4 -6 -9 21.94 4.40 4 -6 -9 20.94 4.76 4 6 -9 15.84 3.51 -4 6 9 16.46 3.91 4 6 -9 23.55 3.33 -4 6 9 16.95 3.93 -4 6 9 14.12 3.84 -3 -6 9 850.07 36.39 -3 -6 9 850.19 39.07 3 -6 -9 899.68 39.96 3 -6 -9 808.39 40.20 -3 6 9 880.04 40.03 -3 6 9 868.29 40.51 3 6 -9 851.86 40.21 3 6 -9 855.72 36.42 -3 6 9 882.83 40.20 -3 6 9 790.38 39.61 3 6 -9 811.27 35.73 -2 -6 9 26.74 4.75 -2 -6 9 16.29 2.60 2 -6 -9 13.14 3.71 2 -6 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883.72 41.01 -6 0 12 912.00 39.50 5 0 -12 142.80 10.02 5 0 -12 89.20 8.49 -5 0 12 128.88 10.47 -5 0 12 136.21 8.72 -5 0 12 123.02 8.58 -4 0 12 2740.87 123.88 4 0 -12 3163.91 125.65 -4 0 12 2889.22 127.22 -4 0 12 2999.80 125.09 -4 0 12 2998.52 124.13 4 0 -12 2999.12 125.19 -3 0 12 343.41 17.81 -3 0 12 319.59 19.58 3 0 -12 310.63 17.57 -3 0 12 308.27 17.02 3 0 -12 317.25 17.98 -3 0 12 370.35 17.78 -2 0 12 112.19 8.22 2 0 -12 119.74 8.43 2 0 -12 106.46 8.21 2 0 -12 122.21 8.81 -2 0 12 94.34 7.84 -2 0 12 107.55 8.80 -1 0 12 125.68 9.25 -1 0 12 124.00 9.00 1 0 -12 93.83 8.29 1 0 -12 105.19 8.42 1 0 -12 125.65 8.63 -1 0 12 121.19 8.57 0 0 12 82.34 7.37 0 0 12 73.29 6.76 0 0 12 92.02 7.88 0 0 -12 64.96 7.00 0 0 -12 76.01 6.91 0 0 -12 79.56 6.71 -1 0 -12 37.57 5.69 1 0 12 37.38 5.44 -1 0 -12 40.40 6.39 1 0 12 34.78 5.68 1 0 12 31.59 5.71 1 0 12 35.82 5.44 2 0 12 132.64 9.59 2 0 12 128.60 9.79 2 0 12 142.10 10.58 2 0 12 122.96 9.99 3 0 12 862.99 41.44 3 0 12 929.82 41.42 3 0 12 860.88 40.88 3 0 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14 200.59 10.91 -7 -3 14 195.73 10.81 -7 -3 14 205.35 13.83 -7 -3 14 205.85 13.42 -7 3 14 211.29 13.85 -7 3 14 202.03 14.37 7 3 -14 217.15 13.92 -6 -3 14 188.72 10.41 6 -3 -14 177.85 13.77 -6 -3 14 201.36 12.52 -6 -3 14 196.68 13.14 -6 -3 14 179.18 10.29 -6 3 14 163.52 12.33 -6 3 14 181.71 13.33 6 3 -14 197.29 12.59 5 -3 -14 -3.11 1.68 -5 -3 14 -0.80 2.95 -5 -3 14 -1.56 1.98 -5 -3 14 1.41 2.19 -5 -3 14 1.06 1.92 5 3 -14 -2.43 2.03 -5 3 14 -1.63 2.97 -5 3 14 2.12 3.03 4 -3 -14 236.99 16.34 -4 -3 14 251.79 14.43 -4 -3 14 265.03 14.13 -4 -3 14 223.74 15.69 -4 -3 14 284.36 14.46 4 3 -14 268.50 14.89 -4 3 14 262.54 16.61 -4 3 14 281.75 16.43 -3 -3 14 66.10 6.41 3 -3 -14 72.73 8.01 -3 -3 14 65.76 6.03 -3 -3 14 86.82 8.30 3 3 -14 77.51 6.31 -3 3 14 64.17 8.33 3 3 -14 71.46 6.22 -3 3 14 79.30 8.25 -2 -3 14 11.17 3.71 2 -3 -14 10.28 3.62 -2 -3 14 7.76 2.74 -2 -3 14 14.24 3.80 2 3 -14 12.39 3.41 -2 3 14 12.58 4.32 2 3 -14 10.24 2.81 -2 3 14 11.61 4.27 -1 -3 14 27.29 4.02 1 -3 -14 32.22 5.89 -1 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6.44 7 -3 14 39.30 9.10 7 3 14 35.89 6.56 7 3 14 26.85 9.03 7 3 14 33.39 7.68 8 -3 14 35.55 8.87 8 -3 14 31.75 7.14 8 -3 14 27.88 7.13 8 3 14 33.12 5.75 8 3 14 28.62 8.35 8 3 14 27.42 8.11 -14 -4 14 -2.66 1.75 -14 -4 14 2.83 3.03 14 -4 -14 3.00 4.91 14 -4 -14 2.25 4.15 -14 4 14 -4.05 4.32 14 4 -14 -6.30 3.49 -13 -4 14 12.89 4.01 -13 -4 14 10.58 2.33 -13 -4 14 8.10 2.71 13 -4 -14 16.34 6.79 13 -4 -14 17.34 5.30 -13 4 14 18.05 5.85 13 4 -14 19.16 6.38 -12 -4 14 64.61 4.54 12 -4 -14 79.67 10.14 12 -4 -14 69.58 10.92 -12 -4 14 65.84 7.03 12 4 -14 64.51 10.05 -12 4 14 92.51 11.11 -11 -4 14 72.51 4.65 11 -4 -14 70.13 13.00 -11 -4 14 78.90 7.64 11 -4 -14 70.19 9.30 11 4 -14 88.15 9.73 -11 4 14 75.82 9.85 10 -4 -14 200.29 16.22 -10 -4 14 193.33 9.41 -10 -4 14 206.96 13.15 10 -4 -14 224.07 15.03 10 4 -14 201.85 14.98 -10 4 14 166.54 13.53 9 -4 -14 201.83 14.10 9 -4 -14 208.10 16.01 -9 -4 14 178.51 9.06 -9 -4 14 182.89 12.68 9 4 -14 204.14 14.25 -9 4 14 187.39 14.08 -8 -4 14 113.83 6.32 8 -4 -14 108.41 11.04 -8 -4 14 138.01 10.35 -8 -4 14 115.08 6.30 8 -4 -14 113.91 10.13 8 4 -14 111.52 9.85 -8 4 14 118.73 10.27 -8 4 14 106.23 10.25 7 -4 -14 144.87 12.43 -7 -4 14 136.19 10.90 -7 -4 14 133.35 7.48 -7 -4 14 144.38 10.73 -7 4 14 135.03 11.02 -7 4 14 143.14 11.33 6 -4 -14 10.99 3.91 -6 -4 14 16.69 4.60 -6 -4 14 15.94 2.65 -6 -4 14 11.62 2.50 -6 -4 14 11.98 4.93 6 4 -14 15.04 4.03 -6 4 14 10.47 4.28 -6 4 14 12.26 4.79 5 -4 -14 375.60 22.25 -5 -4 14 385.56 21.34 -5 -4 14 364.49 19.55 -5 -4 14 383.96 18.16 -5 -4 14 379.29 18.13 -5 4 14 361.33 21.24 -5 4 14 403.59 22.32 5 4 -14 379.21 19.75 -4 -4 14 108.93 8.02 -4 -4 14 109.69 9.83 4 -4 -14 112.63 10.35 -4 -4 14 119.91 7.74 -4 -4 14 111.20 7.74 4 4 -14 119.47 8.37 -4 4 14 120.33 10.01 -4 4 14 108.68 9.89 -3 -4 14 32.34 4.71 -3 -4 14 34.97 4.44 3 -4 -14 32.46 6.21 -3 -4 14 29.52 5.88 3 4 -14 39.62 4.30 -3 4 14 31.55 5.86 -3 4 14 27.07 5.47 3 4 -14 35.29 4.74 2 -4 -14 84.14 8.49 -2 -4 14 77.21 5.73 -2 -4 14 54.07 7.72 -2 -4 14 78.36 7.05 2 4 -14 64.45 6.41 -2 4 14 62.01 8.56 2 4 -14 71.82 5.65 -2 4 14 65.31 8.36 -1 -4 14 0.13 1.64 -1 -4 14 3.25 1.72 -1 -4 14 1.89 2.75 1 -4 -14 -1.26 2.76 -1 -4 14 -1.90 3.22 1 4 -14 2.43 2.55 -1 4 14 -0.45 2.62 -1 4 14 2.20 2.53 0 -4 -14 7.91 3.84 0 -4 14 9.95 2.52 0 -4 14 12.20 4.41 0 -4 14 10.71 2.41 0 4 14 5.78 3.70 0 4 14 6.16 3.76 0 4 -14 12.93 3.77 1 -4 14 97.15 9.83 1 -4 14 98.65 6.94 1 -4 14 90.06 9.02 1 -4 14 99.74 6.97 1 4 14 104.37 9.73 1 4 14 111.42 9.89 1 4 14 109.10 10.47 2 -4 14 23.83 3.83 2 -4 14 34.22 6.58 2 -4 14 18.98 5.56 2 -4 14 24.49 3.82 2 4 14 32.24 6.30 2 4 14 25.01 5.87 2 4 14 17.80 5.21 3 -4 14 4.39 3.91 3 -4 14 9.40 4.52 3 -4 14 0.37 2.45 3 -4 14 2.49 2.43 3 4 14 1.76 3.03 3 4 14 -3.56 3.01 3 4 14 0.43 3.29 4 -4 14 42.95 5.79 4 -4 14 37.42 7.63 4 -4 14 41.48 7.83 4 -4 14 44.79 5.61 4 4 14 48.32 8.32 4 4 14 41.14 7.82 4 4 14 48.02 7.13 5 -4 14 5.51 3.31 5 -4 14 4.70 4.36 5 -4 14 9.15 5.10 5 4 14 6.49 4.13 5 4 14 4.21 3.47 5 4 14 0.86 3.93 6 -4 14 132.14 10.80 6 -4 14 158.94 14.30 6 -4 14 139.84 10.93 6 4 14 130.96 11.27 6 4 14 144.88 14.05 6 4 14 185.15 15.14 7 -4 14 6.61 4.82 7 -4 14 14.71 7.40 7 -4 14 20.97 6.21 7 4 14 15.26 6.70 7 4 14 6.37 6.08 7 4 14 16.89 5.23 8 -4 14 4.66 4.10 8 -4 14 -2.72 2.99 8 -4 14 -2.72 4.15 8 4 14 -6.02 2.49 8 4 14 -3.17 2.95 8 4 14 2.65 4.74 14 -5 -14 147.09 13.16 -14 5 14 96.39 12.36 13 -5 -14 72.57 12.12 -13 -5 14 58.02 6.68 13 -5 -14 50.99 9.79 13 5 -14 58.63 7.27 -13 5 14 45.79 8.44 13 5 -14 59.86 10.19 12 -5 -14 29.85 7.41 12 -5 -14 21.58 6.33 -12 -5 14 26.97 5.00 12 5 -14 28.78 7.33 -12 5 14 35.63 7.39 11 -5 -14 56.62 8.67 11 -5 -14 66.25 10.46 -11 -5 14 59.68 7.16 11 5 -14 69.62 9.51 -11 5 14 52.37 8.39 -10 -5 14 196.51 12.78 10 -5 -14 187.65 14.45 10 -5 -14 164.11 14.93 -10 5 14 204.50 14.81 10 5 -14 180.30 14.07 9 -5 -14 37.43 7.89 9 -5 -14 29.54 6.34 -9 -5 14 22.63 5.29 -9 5 14 39.61 7.10 9 5 -14 34.55 6.51 8 -5 -14 81.27 8.61 8 -5 -14 66.31 9.77 -8 -5 14 70.37 7.52 -8 5 14 78.59 8.43 8 5 -14 65.14 7.48 -8 5 14 59.89 8.61 -7 -5 14 1.29 3.61 -7 -5 14 5.59 3.42 7 -5 -14 3.66 3.24 -7 5 14 3.34 2.95 7 5 -14 6.87 3.54 -7 5 14 -5.47 2.34 6 -5 -14 202.95 15.40 -6 -5 14 217.56 10.47 -6 -5 14 224.67 10.11 -6 -5 14 188.64 12.71 -6 -5 14 205.83 13.89 6 5 -14 215.12 13.05 -6 5 14 184.10 14.08 -6 5 14 182.27 14.23 -5 -5 14 15.69 3.90 -5 -5 14 10.21 4.13 5 -5 -14 10.35 4.06 -5 -5 14 14.59 2.67 -5 -5 14 11.23 2.37 5 5 -14 11.72 3.18 -5 5 14 10.76 3.99 -5 5 14 9.94 4.59 -4 -5 14 27.45 3.79 -4 -5 14 27.80 3.67 -4 -5 14 24.14 5.09 4 -5 -14 21.96 5.77 -4 -5 14 27.61 4.26 4 5 -14 26.59 4.02 -4 5 14 23.98 5.24 -4 5 14 18.95 5.30 -3 -5 14 154.34 11.93 -3 -5 14 156.15 9.64 3 -5 -14 166.27 12.41 -3 -5 14 127.89 8.36 -3 5 14 155.48 11.99 -3 5 14 123.24 11.24 3 5 -14 141.57 8.60 3 5 -14 140.45 9.04 -2 -5 14 32.52 5.15 2 -5 -14 34.17 7.03 -2 -5 14 31.11 5.83 -2 -5 14 32.29 3.83 2 5 -14 34.34 3.56 2 5 -14 39.20 5.47 -2 5 14 34.44 6.71 -2 5 14 38.86 6.64 -1 -5 14 96.74 8.44 -1 -5 14 82.61 8.72 1 -5 -14 95.86 9.65 -1 -5 14 93.96 5.97 -1 5 14 93.73 9.65 -1 5 14 110.57 9.82 1 5 -14 108.35 8.23 0 -5 14 82.52 8.90 0 -5 14 81.72 7.88 0 -5 14 67.17 4.91 0 -5 -14 84.13 8.98 0 5 14 80.10 8.95 0 5 -14 77.01 7.37 0 5 14 73.73 7.76 1 -5 14 9.87 4.32 1 -5 14 4.63 4.00 1 -5 14 1.17 1.56 1 5 14 7.99 3.16 1 5 14 0.71 2.83 1 5 14 3.65 4.04 2 -5 14 289.53 14.12 2 -5 14 280.59 14.10 2 -5 14 285.27 18.17 2 -5 14 304.83 18.85 2 5 14 292.86 17.84 2 5 14 266.15 18.75 2 5 14 265.17 18.59 3 -5 14 91.94 9.94 3 -5 14 102.49 6.87 3 -5 14 104.32 7.10 3 -5 14 101.88 10.05 3 5 14 108.42 9.70 3 5 14 75.36 10.79 3 5 14 110.76 11.18 4 -5 14 109.85 8.12 4 -5 14 97.46 10.30 4 -5 14 107.58 7.81 4 -5 14 119.15 11.56 4 5 14 114.68 11.64 4 5 14 114.63 10.45 4 5 14 114.75 12.04 5 -5 14 58.16 6.42 5 -5 14 64.62 11.16 5 -5 14 72.69 10.46 5 -5 14 79.11 6.91 5 5 14 76.65 11.25 5 5 14 63.74 8.16 5 5 14 71.65 10.91 6 -5 14 222.41 16.64 6 -5 14 211.88 14.42 6 -5 14 205.57 16.84 6 5 14 250.12 18.26 6 5 14 189.78 16.79 6 5 14 187.81 13.90 7 -5 14 -4.27 3.30 7 -5 14 1.42 4.63 7 -5 14 3.64 3.66 7 -5 14 -2.53 4.59 7 5 14 -5.18 4.26 7 5 14 -0.65 4.30 7 5 14 -3.78 2.79 8 -5 14 -2.91 3.45 8 -5 14 -0.78 4.18 8 -5 14 -7.82 3.82 8 5 14 1.03 3.34 8 5 14 -1.45 5.18 8 5 14 5.19 6.26 13 -6 -14 11.17 5.44 13 -6 -14 5.45 4.99 -13 6 14 1.80 4.20 13 6 -14 6.38 5.49 12 -6 -14 73.92 10.68 -12 -6 14 74.02 7.09 12 -6 -14 76.31 11.79 12 6 -14 80.83 10.97 -12 6 14 75.26 10.38 -11 -6 14 16.30 4.22 11 -6 -14 16.37 5.96 11 -6 -14 20.80 6.68 -11 6 14 10.13 5.31 11 6 -14 18.67 5.53 10 -6 -14 0.52 3.81 -10 -6 14 5.68 3.31 10 -6 -14 3.58 4.23 10 6 -14 6.69 3.61 -10 6 14 -0.60 3.35 9 -6 -14 3.01 3.28 -9 -6 14 1.68 2.48 9 -6 -14 -0.96 3.65 9 6 -14 6.50 3.48 -9 6 14 3.67 3.88 -8 -6 14 179.33 13.27 -8 -6 14 190.89 12.97 8 -6 -14 208.67 15.96 8 -6 -14 196.69 14.55 8 6 -14 176.94 12.87 -8 6 14 189.87 14.18 -8 6 14 172.96 13.95 -7 -6 14 55.52 7.03 7 -6 -14 51.19 8.75 -7 -6 14 44.78 7.08 -7 6 14 55.29 8.43 7 6 -14 49.12 6.60 -7 6 14 45.79 7.34 6 -6 -14 322.36 20.51 -6 -6 14 298.84 18.10 6 6 -14 303.90 16.74 -6 6 14 263.41 18.56 -6 6 14 320.45 19.39 -5 -6 14 273.94 12.99 5 -6 -14 296.68 19.21 -5 -6 14 284.26 17.44 -5 -6 14 275.10 13.02 -5 -6 14 274.29 14.85 5 6 -14 304.75 15.33 -5 6 14 276.08 17.80 -5 6 14 246.42 17.51 -4 -6 14 185.09 10.41 -4 -6 14 185.82 13.43 4 -6 -14 171.01 13.64 -4 -6 14 194.92 10.17 4 6 -14 151.81 9.49 4 6 -14 180.17 10.24 -4 6 14 180.65 13.87 -4 6 14 217.30 14.11 -3 -6 14 4.00 2.30 3 -6 -14 1.94 3.46 -3 -6 14 5.76 3.69 -3 -6 14 0.36 2.24 3 6 -14 6.40 1.88 -3 6 14 0.98 3.26 3 6 -14 1.29 1.81 -3 6 14 4.92 3.21 -2 -6 14 197.75 9.73 -2 -6 14 220.56 14.93 -2 -6 14 218.48 12.42 2 -6 -14 187.50 14.41 -2 6 14 164.34 13.90 2 6 -14 213.90 12.13 -2 6 14 212.02 14.58 -1 -6 14 147.97 10.88 -1 -6 14 171.99 13.16 -1 -6 14 158.40 7.15 -1 -6 14 155.43 7.12 1 -6 -14 167.28 13.40 1 6 -14 168.85 11.12 -1 6 14 157.84 13.15 -1 6 14 177.88 12.95 0 -6 14 399.64 23.40 0 -6 14 416.25 21.85 0 -6 -14 397.81 23.85 0 6 -14 363.20 21.08 0 6 14 434.69 24.48 0 6 14 405.79 22.75 1 -6 14 341.63 22.72 1 -6 14 405.34 22.25 1 6 14 415.18 23.82 1 6 14 386.99 23.80 1 6 14 427.38 22.80 2 -6 14 66.67 9.28 2 -6 14 64.60 3.54 2 -6 14 58.66 3.53 2 -6 14 70.04 8.90 2 6 14 64.94 8.53 2 6 14 60.06 9.53 2 6 14 50.15 8.68 3 -6 14 25.28 2.83 3 -6 14 28.78 2.87 3 -6 14 30.30 7.05 3 -6 14 21.61 6.23 3 6 14 27.59 5.73 3 6 14 15.05 5.82 3 6 14 19.78 5.87 4 -6 14 277.10 20.82 4 -6 14 248.91 12.44 4 -6 14 250.47 17.52 4 -6 14 233.94 12.36 4 6 14 259.00 21.34 4 6 14 214.29 15.62 4 6 14 235.33 17.69 5 -6 14 17.48 5.35 5 -6 14 11.24 5.51 5 -6 14 12.63 2.90 5 -6 14 12.36 3.09 5 6 14 16.84 6.12 5 6 14 11.23 4.40 5 6 14 21.08 6.28 6 -6 14 57.50 9.65 6 -6 14 45.94 5.72 6 -6 14 39.97 8.45 6 -6 14 58.99 6.20 6 6 14 62.99 10.56 6 6 14 44.29 8.95 6 6 14 43.60 7.08 7 -6 14 6.61 5.25 7 -6 14 10.39 5.33 7 -6 14 4.46 3.14 7 6 14 10.24 4.46 7 6 14 12.47 6.18 7 6 14 -0.10 4.37 13 -7 -14 83.45 12.93 -13 -7 14 63.30 6.63 13 -7 -14 84.12 11.79 -13 7 14 60.52 9.95 13 7 -14 65.87 10.36 -12 -7 14 2.41 2.48 12 -7 -14 -3.21 2.74 12 -7 -14 -0.83 3.59 12 7 -14 5.21 4.08 12 7 -14 1.00 3.64 -12 7 14 -2.20 4.12 11 -7 -14 4.78 3.94 -11 -7 14 7.45 3.84 11 -7 -14 -0.24 3.57 -11 7 14 0.17 3.99 11 7 -14 0.36 3.87 -10 -7 14 0.86 2.73 10 -7 -14 8.96 5.14 10 -7 -14 1.13 3.10 10 7 -14 5.69 3.25 -10 7 14 -1.34 4.13 -9 -7 14 9.33 3.74 9 -7 -14 8.36 4.50 9 7 -14 12.08 4.49 -9 7 14 8.28 3.64 8 -7 -14 43.82 7.42 -8 -7 14 31.98 6.18 -8 -7 14 41.75 6.81 8 -7 -14 50.87 9.28 -8 7 14 37.65 7.45 -8 7 14 46.41 7.67 8 7 -14 49.52 6.82 7 -7 -14 239.52 17.67 -7 -7 14 245.42 15.76 -7 7 14 242.35 17.02 -7 7 14 236.69 16.65 7 7 -14 237.19 14.56 -6 -7 14 1.45 2.82 6 -7 -14 6.84 3.73 -6 -7 14 0.71 3.07 6 7 -14 4.52 2.64 -6 7 14 -2.91 2.74 -6 7 14 3.58 3.12 -5 -7 14 0.97 0.73 5 -7 -14 0.73 3.70 -5 -7 14 -3.45 1.96 -5 -7 14 1.14 3.15 -5 -7 14 1.14 0.61 -5 7 14 1.64 2.62 -5 7 14 -0.34 2.75 5 7 -14 2.39 1.87 -4 -7 14 -0.26 1.75 4 -7 -14 2.03 3.03 -4 -7 14 5.06 1.76 -4 -7 14 5.10 3.77 -4 7 14 -0.25 3.66 -4 7 14 2.09 3.24 4 7 -14 -0.53 1.42 4 7 -14 2.69 1.48 3 -7 -14 17.19 5.04 -3 -7 14 19.37 5.43 -3 -7 14 24.32 3.75 -3 -7 14 18.21 2.08 -3 7 14 20.48 5.65 3 7 -14 18.57 3.27 -3 7 14 16.10 4.52 3 7 -14 18.26 2.27 -2 -7 14 92.89 9.63 -2 -7 14 91.47 7.49 2 -7 -14 74.90 10.21 -2 7 14 92.11 9.12 2 7 -14 89.00 7.15 -2 7 14 101.60 10.27 -1 -7 14 293.09 16.77 1 -7 -14 299.43 19.82 -1 -7 14 297.54 18.96 -1 7 14 311.97 19.06 -1 7 14 260.57 18.80 1 7 -14 341.20 17.23 0 -7 14 4.52 3.14 0 -7 14 4.01 3.10 0 -7 -14 -0.19 2.43 0 7 14 3.56 3.17 0 7 14 2.52 3.78 0 7 -14 -2.65 2.42 1 -7 14 98.63 9.01 1 -7 14 74.75 10.05 1 7 14 70.22 9.90 1 7 14 79.96 10.92 1 7 14 67.63 8.76 2 -7 14 49.20 8.43 2 -7 14 58.95 8.19 2 7 14 44.04 8.42 2 7 14 39.08 6.90 2 7 14 49.01 8.92 3 -7 14 141.17 12.20 3 -7 14 119.91 13.32 3 7 14 134.47 11.40 3 7 14 136.48 13.31 4 -7 14 79.04 10.52 4 -7 14 80.49 10.76 4 7 14 79.25 8.47 4 7 14 74.71 11.47 4 7 14 65.87 10.80 5 -7 14 81.14 5.19 5 -7 14 91.35 11.77 5 7 14 77.11 11.30 5 7 14 83.71 12.45 5 7 14 91.55 9.16 6 -7 14 1.55 1.91 6 -7 14 -2.29 2.79 6 -7 14 2.73 4.29 6 -7 14 -0.95 4.01 6 7 14 -0.80 2.76 6 7 14 -7.75 2.48 6 7 14 -1.18 4.44 7 -7 14 35.35 4.52 7 -7 14 33.13 7.89 7 -7 14 37.10 8.70 7 7 14 21.98 7.89 7 7 14 42.58 8.79 7 7 14 39.23 6.68 12 -8 -14 28.80 7.69 12 -8 -14 40.03 9.31 -12 -8 14 36.57 5.37 -12 8 14 27.50 6.94 12 8 -14 34.26 7.20 11 -8 -14 4.92 4.77 11 -8 -14 -4.43 3.52 -11 -8 14 2.04 2.99 11 8 -14 5.62 3.61 -11 8 14 10.66 5.41 10 -8 -14 79.88 11.48 -10 -8 14 84.04 8.28 10 -8 -14 83.65 12.04 10 8 -14 98.80 9.63 -10 8 14 80.24 10.89 -9 -8 14 1.17 2.27 9 -8 -14 1.50 3.42 -9 8 14 1.91 3.95 9 8 -14 1.60 3.12 -8 -8 14 116.69 10.04 -8 -8 14 131.92 10.88 8 -8 -14 145.28 12.60 8 8 -14 150.49 10.80 -8 8 14 133.37 12.10 -8 8 14 121.67 13.54 7 -8 -14 11.11 5.30 -7 -8 14 11.02 4.15 -7 -8 14 17.88 4.13 -7 8 14 17.06 5.57 -7 8 14 10.94 4.50 7 8 -14 15.77 3.92 6 -8 -14 11.70 5.18 -6 -8 14 3.14 2.83 -6 -8 14 6.01 3.51 -6 8 14 8.12 4.38 6 8 -14 10.20 2.93 -6 8 14 2.48 4.03 -5 -8 14 -3.11 1.67 5 -8 -14 0.69 3.33 -5 -8 14 1.03 3.38 5 8 -14 4.49 1.77 -5 8 14 -0.82 3.21 -5 8 14 -0.31 3.48 -4 -8 14 24.34 2.55 -4 -8 14 22.39 5.66 -4 -8 14 25.21 2.76 4 -8 -14 22.59 5.76 -4 8 14 20.59 5.64 -4 8 14 21.88 5.84 -3 -8 14 5.50 3.96 -3 -8 14 4.80 2.22 3 -8 -14 5.51 4.31 3 8 -14 5.53 2.34 -3 8 14 4.68 3.28 -3 8 14 3.76 4.40 -2 -8 14 1.01 2.05 2 -8 -14 -3.68 3.35 -2 -8 14 -2.58 2.82 -2 8 14 -1.10 3.05 2 8 -14 -1.89 2.11 -2 8 14 -0.52 3.15 -1 -8 14 -2.19 3.12 1 -8 -14 2.90 3.71 -1 -8 14 5.87 3.35 -1 8 14 -0.18 2.98 -1 8 14 3.49 3.15 1 8 -14 1.49 2.55 0 -8 -14 142.16 12.82 0 -8 14 141.28 10.41 0 -8 14 113.65 10.96 0 8 -14 102.75 8.96 0 8 14 118.72 10.83 0 8 14 123.19 11.86 1 -8 14 3.38 3.57 1 -8 14 0.17 2.56 1 8 14 0.18 3.15 1 8 14 -0.40 3.50 1 8 14 -0.16 3.07 2 -8 14 41.78 7.14 2 8 14 44.71 8.89 2 8 14 60.35 8.21 3 -8 14 33.32 6.98 3 -8 14 38.66 7.55 3 8 14 28.39 7.42 3 8 14 40.11 8.51 3 8 14 30.87 5.98 4 -8 14 1.07 3.92 4 -8 14 1.44 4.57 4 8 14 1.71 3.84 4 8 14 4.85 3.82 4 8 14 -1.44 4.61 5 -8 14 6.17 4.88 5 -8 14 22.06 6.55 5 8 14 1.93 3.56 5 8 14 5.06 5.34 5 8 14 7.32 4.44 6 -8 14 44.58 9.01 6 -8 14 40.16 8.13 6 8 14 40.68 6.92 6 8 14 49.33 9.86 6 8 14 25.95 8.52 -12 -9 14 6.65 3.64 12 -9 -14 22.70 7.27 12 -9 -14 29.71 7.48 -12 9 14 22.73 6.39 -11 -9 14 16.52 4.56 11 -9 -14 22.20 6.71 11 -9 -14 21.65 6.21 -11 9 14 32.01 7.38 11 9 -14 23.11 5.67 10 -9 -14 94.59 12.73 -10 -9 14 117.36 9.83 10 -9 -14 114.69 12.44 -10 9 14 132.42 12.86 10 9 -14 112.35 10.63 9 -9 -14 270.74 20.10 9 -9 -14 302.25 21.73 -9 -9 14 297.72 17.83 9 9 -14 324.81 18.44 -9 9 14 251.04 19.37 8 -9 -14 21.39 6.90 8 -9 -14 24.32 6.67 -8 -9 14 23.83 5.50 -8 -9 14 28.21 5.68 -8 9 14 41.39 8.07 8 9 -14 22.47 4.82 -8 9 14 23.46 6.53 7 -9 -14 9.52 4.77 -7 -9 14 9.40 4.10 -7 -9 14 5.21 3.53 -7 9 14 13.40 5.06 7 9 -14 20.35 3.90 6 -9 -14 4.26 4.63 -6 -9 14 3.56 3.30 -6 -9 14 5.07 2.80 -6 9 14 17.19 5.93 -6 9 14 7.52 3.97 6 9 -14 7.52 2.68 -5 -9 14 9.96 4.17 -5 -9 14 15.64 2.69 5 -9 -14 20.15 6.00 -5 9 14 9.49 4.27 -5 9 14 8.45 5.32 5 9 -14 14.46 2.33 -4 -9 14 -2.81 2.44 4 -9 -14 4.94 3.20 -4 9 14 4.87 3.20 -4 9 14 0.36 3.81 -3 -9 14 31.70 3.97 -3 -9 14 33.47 6.49 3 -9 -14 32.79 7.57 -3 9 14 42.09 7.70 3 9 -14 30.28 3.83 -3 9 14 22.48 5.50 -2 -9 14 13.98 3.26 2 -9 -14 8.16 4.05 -2 -9 14 10.26 3.95 -2 9 14 9.08 4.74 2 9 -14 16.38 3.49 -2 9 14 12.94 4.68 -1 -9 14 5.17 4.26 -1 -9 14 11.93 3.72 1 -9 -14 13.24 5.08 -1 9 14 17.40 5.00 1 9 -14 11.45 3.67 -1 9 14 14.52 5.47 0 -9 -14 4.70 5.04 0 -9 14 1.49 3.04 0 -9 14 0.31 2.85 0 9 14 4.27 3.95 0 9 14 9.60 5.04 0 9 14 3.30 3.44 1 -9 14 12.31 4.45 1 -9 14 11.10 4.58 1 9 14 8.28 5.32 1 9 14 12.55 4.74 1 9 14 20.14 6.34 2 -9 14 19.86 5.15 2 -9 14 15.50 5.46 2 9 14 19.37 5.14 2 9 14 14.18 5.06 2 9 14 16.25 6.33 3 -9 14 9.94 5.40 3 -9 14 2.33 3.94 3 9 14 1.80 3.83 3 9 14 9.16 4.55 3 9 14 4.15 4.56 4 -9 14 284.35 19.99 4 -9 14 262.49 18.37 4 9 14 238.95 19.63 4 9 14 256.40 19.51 4 9 14 248.52 16.65 5 -9 14 141.81 13.99 5 -9 14 154.63 13.87 5 9 14 142.85 11.44 5 9 14 128.48 14.62 5 9 14 164.82 14.69 6 -9 14 93.88 12.51 6 -9 14 105.01 13.52 6 9 14 90.84 13.83 6 9 14 101.45 9.69 6 9 14 93.39 12.88 11 -10 -14 20.68 6.90 -11 -10 14 7.54 3.87 11 -10 -14 12.02 6.25 11 10 -14 26.71 6.35 -11 10 14 18.71 5.65 10 -10 -14 8.42 5.12 10 -10 -14 4.48 4.36 -10 -10 14 -1.02 3.06 10 10 -14 1.98 3.39 -10 10 14 1.98 4.89 -9 -10 14 0.90 3.07 9 -10 -14 3.06 3.54 9 -10 -14 -4.69 4.01 9 10 -14 1.49 2.91 -9 10 14 1.44 4.58 8 -10 -14 36.11 7.86 -8 -10 14 37.30 6.36 -8 -10 14 47.91 7.03 8 -10 -14 35.31 8.22 8 10 -14 39.36 6.82 -8 10 14 47.43 8.57 -8 10 14 31.31 7.32 -7 -10 14 3.81 3.49 -7 -10 14 13.59 4.33 7 -10 -14 12.15 4.93 -7 10 14 15.46 5.39 7 10 -14 12.90 3.52 -7 10 14 12.43 5.14 -6 -10 14 22.59 3.72 -6 -10 14 23.33 5.72 6 -10 -14 25.38 6.80 -6 10 14 29.98 7.07 6 10 -14 24.78 3.60 -6 10 14 16.25 6.03 5 -10 -14 110.56 11.37 -5 -10 14 85.93 9.47 5 10 -14 88.86 5.12 -5 10 14 88.21 11.45 -5 10 14 110.98 11.16 -4 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6.32 4.38 -2 -6 15 9.16 3.57 -2 6 15 18.06 5.67 2 6 -15 12.44 3.42 -2 6 15 18.40 5.24 -1 -6 15 101.69 5.10 1 -6 -15 104.01 10.21 -1 -6 15 97.77 5.02 -1 -6 15 94.41 10.17 -1 6 15 106.18 9.73 -1 6 15 91.59 9.75 1 6 -15 99.98 8.37 0 -6 15 0.44 3.63 0 -6 -15 0.22 3.82 0 -6 15 -0.66 3.74 0 6 15 4.44 3.91 0 6 15 0.77 3.89 1 -6 15 3.47 3.46 1 -6 15 3.44 3.79 1 6 15 0.79 3.07 1 6 15 0.87 3.13 1 6 15 4.99 4.15 2 -6 15 143.28 13.20 2 -6 15 138.23 12.66 2 -6 15 151.80 7.33 2 6 15 155.00 12.41 2 6 15 152.08 13.72 2 6 15 168.13 14.19 3 -6 15 42.27 7.78 3 -6 15 31.63 8.65 3 -6 15 28.28 3.15 3 6 15 26.42 7.05 3 6 15 31.37 6.42 3 6 15 36.14 7.92 4 -6 15 -0.05 2.83 4 -6 15 8.48 2.36 4 -6 15 4.85 2.14 4 -6 15 1.90 4.68 4 6 15 6.88 4.18 4 6 15 5.78 4.49 4 6 15 9.87 6.05 5 -6 15 31.72 4.55 5 -6 15 57.31 9.71 5 -6 15 32.55 4.37 5 -6 15 38.53 7.49 5 6 15 30.62 6.01 5 6 15 28.98 7.62 5 6 15 38.75 8.62 6 -6 15 26.96 6.75 6 -6 15 23.88 4.36 6 -6 15 42.22 8.55 6 6 15 16.19 6.78 6 6 15 25.26 6.88 6 6 15 30.54 6.23 7 -6 15 34.52 5.51 7 -6 15 13.85 6.40 7 -6 15 23.81 6.48 7 6 15 18.95 7.18 7 6 15 30.35 8.42 7 6 15 30.68 6.55 13 -7 -15 273.79 22.25 -13 7 15 267.60 19.84 13 7 -15 271.18 19.82 12 -7 -15 -2.19 3.56 12 -7 -15 6.22 4.79 -12 -7 15 5.47 3.28 12 7 -15 4.09 4.13 -12 7 15 -1.61 4.22 11 -7 -15 163.51 14.60 -11 -7 15 171.81 12.24 11 -7 -15 174.58 16.05 -11 7 15 165.48 14.61 10 -7 -15 114.89 12.76 -10 -7 15 82.38 8.71 -10 7 15 83.74 11.21 10 7 -15 89.63 9.70 9 -7 -15 194.37 17.50 9 -7 -15 226.52 17.15 -9 -7 15 231.92 15.08 -9 7 15 258.99 17.50 -9 7 15 239.30 17.27 9 7 -15 244.23 15.73 -8 -7 15 -1.23 3.66 -8 -7 15 -3.17 2.81 -8 7 15 -0.59 3.64 8 7 -15 3.17 3.12 -8 7 15 -0.80 2.73 -7 -7 15 131.89 10.99 -7 -7 15 141.71 11.52 7 -7 -15 121.83 12.24 -7 7 15 117.80 11.20 7 7 -15 126.12 9.51 -7 7 15 124.15 11.77 -6 -7 15 92.41 9.17 6 -7 -15 75.72 10.82 -6 7 15 98.59 10.16 6 7 -15 86.33 7.15 -6 7 15 78.05 10.11 -5 -7 15 31.18 2.65 5 -7 -15 28.17 7.02 -5 -7 15 23.00 3.91 -5 -7 15 26.44 5.95 -5 7 15 27.87 6.64 -5 7 15 29.07 6.45 5 7 -15 26.23 3.94 -4 -7 15 97.45 6.68 -4 -7 15 113.45 10.63 4 -7 -15 120.05 11.34 -4 -7 15 97.57 6.51 4 7 -15 104.77 6.51 4 7 -15 114.26 6.86 -4 7 15 89.42 10.36 -4 7 15 109.74 10.77 3 -7 -15 23.36 6.26 -3 -7 15 17.62 5.28 -3 -7 15 24.40 4.00 -3 -7 15 14.10 1.90 3 7 -15 21.26 3.63 -3 7 15 23.80 5.57 -3 7 15 21.39 5.51 2 -7 -15 4.33 4.54 -2 -7 15 5.30 4.35 -2 -7 15 6.30 3.28 -2 7 15 8.27 4.33 2 7 -15 5.47 2.68 -2 7 15 4.95 3.38 1 -7 -15 397.22 24.41 -1 -7 15 391.38 23.94 -1 7 15 423.98 24.97 -1 7 15 471.33 24.55 1 7 -15 353.73 20.87 0 -7 15 31.70 6.87 0 -7 -15 39.69 7.50 0 -7 15 32.46 5.92 0 7 15 32.80 7.28 0 7 15 26.38 6.49 0 7 15 38.94 7.01 1 -7 15 45.58 7.38 1 -7 15 41.67 7.99 1 7 15 41.93 7.14 1 7 15 33.30 7.22 1 7 15 32.82 7.53 2 -7 15 35.72 7.35 2 -7 15 31.78 6.89 2 7 15 30.03 7.24 2 7 15 30.73 7.26 2 7 15 54.65 8.23 3 -7 15 172.18 13.70 3 -7 15 155.34 14.19 3 7 15 128.60 13.77 3 7 15 152.24 12.70 3 7 15 173.01 14.83 4 -7 15 38.69 7.60 4 -7 15 36.82 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-1 1 21 51.94 9.52 0 -1 21 4.50 4.42 0 -1 21 7.15 5.31 0 -1 21 -0.76 3.89 0 1 21 5.03 4.43 0 1 21 3.17 3.63 0 1 21 6.20 5.16 1 -1 21 26.17 7.60 1 -1 21 29.95 6.75 1 -1 21 30.94 7.65 1 1 21 31.27 8.32 1 1 21 30.68 7.32 1 1 21 25.36 6.67 -10 -2 21 -2.02 3.19 10 -2 -21 -3.21 3.81 -10 -2 21 -1.66 3.83 -10 2 21 -1.56 4.40 10 2 -21 0.44 4.27 -10 2 21 -0.75 4.11 -9 -2 21 51.25 9.11 -9 -2 21 50.31 6.83 9 -2 -21 56.63 10.15 9 2 -21 61.05 9.50 -9 2 21 48.04 9.51 -9 2 21 48.85 8.08 8 -2 -21 106.19 11.55 -8 -2 21 128.96 12.21 -8 -2 21 111.74 9.84 -8 2 21 115.62 14.05 8 2 -21 97.86 10.90 -8 2 21 114.56 10.91 -7 -2 21 190.20 16.24 -7 -2 21 188.30 13.49 7 -2 -21 190.67 16.17 7 2 -21 219.85 15.50 -7 2 21 210.12 15.72 -7 2 21 209.12 16.95 -6 -2 21 1.70 3.99 -6 -2 21 0.18 4.44 -6 2 21 12.30 5.13 -6 2 21 1.96 5.11 6 2 -21 12.20 4.54 -5 -2 21 9.12 4.52 5 -2 -21 4.74 4.04 -5 -2 21 -3.03 3.47 -5 2 21 -1.65 3.05 5 2 -21 -0.21 2.76 -5 2 21 1.70 4.04 -4 -2 21 81.50 9.89 -4 -2 21 65.44 10.53 4 -2 -21 76.50 10.63 -4 2 21 81.07 11.21 -4 2 21 75.19 10.35 4 2 -21 90.26 8.88 -3 -2 21 -3.09 3.36 -3 -2 21 -6.69 3.62 3 -2 -21 -1.26 3.45 3 2 -21 -0.78 2.46 -3 2 21 -1.25 3.78 -3 2 21 -4.40 4.44 -2 -2 21 -4.62 4.08 -2 -2 21 -0.85 3.30 -2 -2 21 -1.84 3.20 2 -2 -21 4.48 3.79 -2 2 21 -2.90 4.09 -2 2 21 6.57 5.05 -1 -2 21 -5.06 2.85 -1 -2 21 4.38 4.71 -1 -2 21 -4.58 3.15 -1 2 21 -8.04 3.10 -1 2 21 6.37 4.78 -1 2 21 -10.50 3.28 0 -2 21 32.84 6.79 0 -2 21 45.58 8.56 0 -2 21 21.55 7.02 0 2 21 31.55 7.46 0 2 21 24.15 7.76 0 2 21 20.59 6.96 1 -2 21 65.64 9.00 1 -2 21 72.49 11.31 1 -2 21 75.30 11.23 1 2 21 66.36 10.24 1 2 21 63.52 10.50 1 2 21 60.46 10.37 10 -3 -21 82.21 12.47 -10 -3 21 56.72 9.12 -10 -3 21 51.31 6.05 -10 3 21 36.24 8.22 9 -3 -21 31.66 7.82 -9 -3 21 20.37 4.72 -9 -3 21 32.33 7.50 9 3 -21 27.11 6.49 -9 3 21 30.85 7.72 -9 3 21 19.41 6.21 -8 -3 21 -0.95 3.78 -8 -3 21 1.28 3.37 8 -3 -21 11.40 4.82 8 3 -21 -3.19 3.48 -8 3 21 8.39 5.50 -8 3 21 -0.90 4.67 -7 -3 21 -5.42 2.53 7 -3 -21 3.94 3.39 -7 -3 21 2.46 4.44 -7 3 21 2.32 4.59 7 3 -21 2.67 3.45 -7 3 21 0.27 3.48 6 -3 -21 82.40 11.71 -6 -3 21 87.75 11.54 -6 -3 21 76.63 8.27 -6 3 21 107.01 14.17 -6 3 21 62.10 10.57 6 3 -21 85.29 8.67 5 -3 -21 122.33 12.14 -5 -3 21 108.72 13.40 -5 -3 21 110.19 10.07 5 3 -21 98.27 9.56 -5 3 21 111.43 12.23 -4 -3 21 0.68 3.42 -4 -3 21 0.60 3.30 4 -3 -21 5.87 4.71 -4 3 21 -1.12 4.24 4 3 -21 -1.11 3.03 -4 3 21 -5.42 4.20 -3 -3 21 6.35 4.21 3 -3 -21 10.05 5.33 -3 -3 21 5.62 3.96 3 3 -21 11.50 3.73 -3 3 21 10.97 5.62 -3 3 21 1.47 4.76 2 -3 -21 91.31 9.92 -2 -3 21 89.62 8.55 -2 -3 21 65.20 10.13 -2 -3 21 56.49 9.02 -2 3 21 58.00 9.74 -2 3 21 68.83 10.53 -1 -3 21 17.17 6.50 -1 -3 21 8.45 4.37 -1 -3 21 14.54 5.22 -1 3 21 9.92 5.56 -1 3 21 6.74 5.30 -1 3 21 11.46 5.11 0 -3 21 12.77 5.74 0 -3 21 11.71 5.96 0 -3 21 11.17 4.58 0 3 21 4.66 5.09 0 3 21 17.99 6.26 0 3 21 8.84 5.48 1 -3 21 -10.97 4.05 1 -3 21 -4.82 3.24 1 -3 21 4.48 4.80 1 3 21 9.95 5.57 1 3 21 2.44 5.18 1 3 21 -10.94 3.59 9 -4 -21 44.29 9.25 -9 -4 21 25.79 4.38 -9 -4 21 41.13 8.35 -9 4 21 41.21 7.92 -9 4 21 41.95 8.38 9 4 -21 31.28 7.01 8 -4 -21 -5.82 3.46 -8 -4 21 -0.33 3.94 -8 -4 21 -2.80 2.79 -8 4 21 -2.86 3.80 8 4 -21 5.97 4.11 -8 4 21 3.06 3.97 -7 -4 21 14.99 4.77 -7 -4 21 18.23 5.83 7 -4 -21 29.05 7.48 -7 4 21 28.01 7.65 -7 4 21 25.31 6.80 7 4 -21 17.67 5.18 6 -4 -21 5.44 4.79 -6 -4 21 -0.37 3.19 -6 -4 21 -1.03 3.82 6 4 -21 4.21 3.79 -6 4 21 0.87 3.15 -6 4 21 -1.12 3.78 -5 -4 21 334.91 19.19 5 -4 -21 328.72 22.57 -5 -4 21 326.86 22.14 5 4 -21 340.66 19.16 -5 4 21 302.32 21.58 -5 4 21 332.69 22.76 -4 -4 21 30.25 7.64 -4 -4 21 35.95 6.58 4 -4 -21 38.97 8.27 4 4 -21 34.08 5.65 -4 4 21 24.67 7.20 -4 4 21 32.20 7.46 -3 -4 21 66.05 10.56 -3 -4 21 51.42 8.49 3 -4 -21 80.98 11.12 -3 -4 21 56.14 9.97 -3 4 21 49.17 9.01 -3 4 21 70.66 10.91 2 -4 -21 51.71 8.95 -2 -4 21 20.27 6.64 -2 -4 21 33.79 8.12 -2 4 21 28.65 7.47 -2 4 21 23.30 7.24 -1 -4 21 24.62 4.96 -1 -4 21 47.17 8.29 -1 -4 21 38.59 8.88 -1 4 21 55.48 9.86 -1 4 21 50.47 9.47 -1 4 21 40.81 8.85 0 -4 21 14.05 6.14 0 -4 21 -2.57 3.24 0 -4 21 -7.49 3.85 0 4 21 -1.08 4.62 0 4 21 2.95 5.38 0 4 21 -6.74 3.92 -9 -5 21 3.30 5.05 9 -5 -21 9.76 5.48 -9 5 21 6.21 4.92 9 5 -21 2.43 4.03 -9 5 21 7.45 5.48 -8 -5 21 181.32 10.48 8 -5 -21 166.96 16.47 -8 -5 21 188.45 15.73 8 5 -21 180.47 13.63 -8 5 21 188.43 16.57 -7 -5 21 12.94 6.00 7 -5 -21 24.59 7.81 -7 -5 21 17.31 4.22 -7 5 21 17.40 6.46 7 5 -21 21.94 5.03 -7 5 21 17.38 5.95 -6 -5 21 107.71 9.54 -6 -5 21 77.15 11.70 6 -5 -21 99.63 13.37 6 5 -21 110.07 9.33 -6 5 21 86.86 12.04 -6 5 21 81.68 11.58 -5 -5 21 31.03 5.99 5 -5 -21 26.89 7.76 -5 -5 21 45.47 8.95 -5 5 21 35.01 7.98 -5 5 21 32.96 7.46 5 5 -21 31.82 5.61 -4 -5 21 58.99 10.11 4 -5 -21 59.50 10.26 -4 -5 21 40.97 7.19 -4 5 21 73.85 10.81 -4 5 21 53.09 9.54 4 5 -21 50.61 6.37 3 -5 -21 9.22 5.22 -3 -5 21 0.93 2.72 -3 -5 21 1.81 5.16 -3 -5 21 -6.12 3.59 -3 5 21 3.58 4.69 -3 5 21 1.66 4.64 -2 -5 21 92.17 12.62 -2 -5 21 78.70 9.85 2 -5 -21 67.75 10.68 -2 -5 21 72.37 6.87 -2 5 21 92.09 12.53 -2 5 21 63.11 10.51 -1 -5 21 8.13 5.34 -1 -5 21 4.63 3.30 -1 -5 21 1.03 4.82 -1 5 21 4.50 5.54 -1 5 21 7.94 5.01 -1 5 21 16.76 6.00 0 -5 21 87.28 11.12 0 -5 21 66.75 11.36 0 -5 21 56.81 6.59 0 5 21 88.89 11.74 0 5 21 89.84 12.83 0 5 21 64.93 10.93 8 -6 -21 30.40 8.03 -8 -6 21 24.70 6.57 -8 6 21 20.19 6.74 8 6 -21 25.15 5.47 -8 6 21 21.63 6.60 7 -6 -21 129.65 13.69 -7 -6 21 99.41 7.25 -7 -6 21 121.67 12.65 -7 6 21 91.79 12.43 7 6 -21 113.20 9.55 -7 6 21 93.81 12.75 -6 -6 21 20.22 4.25 6 -6 -21 24.44 7.93 -6 -6 21 40.62 7.96 -6 6 21 18.48 6.01 -6 6 21 32.35 8.04 -5 -6 21 3.35 5.07 5 -6 -21 8.37 5.85 5 6 -21 1.06 2.36 -5 6 21 -0.97 4.95 -5 6 21 6.91 4.09 -4 -6 21 -5.22 3.44 -4 -6 21 3.10 5.26 -4 -6 21 -1.61 2.65 4 -6 -21 0.19 4.72 -4 6 21 -7.35 4.04 -4 6 21 -1.02 3.76 -3 -6 21 4.74 4.78 -3 -6 21 -7.43 3.39 -3 -6 21 -3.85 2.17 3 -6 -21 5.34 5.28 -3 6 21 -9.79 3.19 -3 6 21 4.75 5.04 -2 -6 21 61.12 5.12 -2 -6 21 56.43 8.47 -2 -6 21 69.79 10.72 2 -6 -21 82.65 11.62 -2 6 21 67.20 10.53 -2 6 21 86.08 11.59 -1 -6 21 12.80 5.54 -1 -6 21 16.89 6.36 -1 6 21 17.75 6.92 -1 6 21 8.35 5.88 -1 6 21 2.57 4.88 -6 -7 21 3.37 4.80 6 -7 -21 14.93 6.24 -6 -7 21 11.94 3.08 -6 7 21 26.29 7.74 -6 7 21 10.32 5.88 6 7 -21 15.81 3.54 -5 -7 21 1.68 4.44 5 -7 -21 4.27 4.52 -5 -7 21 3.87 3.12 -5 7 21 -5.72 3.70 -5 7 21 3.59 3.75 -4 -7 21 115.92 9.79 4 -7 -21 115.97 15.04 -4 -7 21 121.85 12.95 -4 7 21 113.52 14.28 -4 7 21 124.63 13.29 -3 -7 21 -1.64 3.87 3 -7 -21 4.63 4.84 -3 -7 21 7.82 5.37 -3 7 21 7.89 5.69 -3 7 21 3.64 5.28 -9 0 22 376.15 25.84 9 0 -22 449.67 26.98 -8 0 22 236.63 18.59 8 0 -22 215.49 17.38 -8 0 22 252.97 16.48 -7 0 22 16.28 5.58 -7 0 22 23.78 7.13 -6 0 22 15.09 5.80 -6 0 22 10.05 6.11 6 0 -22 20.64 6.18 -5 0 22 4.09 4.90 -5 0 22 7.60 4.16 5 0 -22 12.21 4.90 4 0 -22 -2.02 3.76 -4 0 22 -4.95 3.63 -4 0 22 -5.81 3.95 -3 0 22 59.14 10.31 3 0 -22 44.99 7.75 -3 0 22 54.76 10.59 -2 0 22 14.69 6.00 -2 0 22 9.20 4.86 -2 0 22 14.06 5.15 -1 0 22 42.14 9.39 -1 0 22 44.15 9.23 -1 0 22 34.19 7.49 9 -1 -22 12.31 5.37 -9 -1 22 4.67 4.45 -9 -1 22 15.48 5.78 9 1 -22 5.96 4.88 -9 1 22 1.60 4.90 -9 1 22 13.05 5.03 -8 -1 22 27.52 7.03 -8 -1 22 27.92 5.91 8 -1 -22 36.64 7.61 -8 1 22 26.46 7.41 -8 1 22 30.31 6.53 -7 -1 22 -1.92 3.72 7 -1 -22 1.27 4.02 -7 -1 22 0.36 2.96 -7 1 22 -4.77 3.28 7 1 -22 -0.78 3.89 -7 1 22 2.07 4.31 6 -1 -22 35.17 8.85 -6 -1 22 38.09 7.24 -6 -1 22 39.02 9.14 -6 1 22 53.51 8.84 6 1 -22 44.66 8.17 -6 1 22 33.37 7.77 5 -1 -22 276.47 20.63 -5 -1 22 290.04 19.39 -5 -1 22 350.92 22.37 -5 1 22 298.47 21.23 -5 1 22 308.67 20.23 5 1 -22 300.92 19.46 -4 -1 22 140.67 13.15 4 -1 -22 148.30 13.38 -4 -1 22 162.71 14.87 -4 1 22 147.82 15.44 4 1 -22 164.71 12.85 -4 1 22 150.54 14.70 -3 -1 22 -3.42 3.99 -3 -1 22 -0.34 4.00 3 -1 -22 -1.74 3.44 -3 1 22 0.11 3.82 -3 1 22 -1.52 3.33 3 1 -22 6.04 3.74 -2 -1 22 -0.97 3.98 2 -1 -22 -1.30 2.74 -2 -1 22 -3.04 2.83 -2 -1 22 -6.83 3.91 -2 1 22 4.76 4.47 -2 1 22 -0.03 4.11 -1 -1 22 45.13 8.89 -1 -1 22 31.47 6.89 -1 -1 22 35.28 8.34 -1 1 22 38.15 8.35 -1 1 22 52.27 9.57 -1 1 22 27.33 7.65 -8 -2 22 51.74 9.34 8 -2 -22 59.52 10.18 -8 -2 22 46.54 7.20 8 2 -22 49.34 8.47 -8 2 22 60.51 10.65 -8 2 22 50.78 8.72 -7 -2 22 -3.61 4.08 -7 -2 22 2.49 3.85 7 -2 -22 6.02 5.23 -7 2 22 7.32 5.38 7 2 -22 2.34 4.15 -7 2 22 13.79 6.03 -6 -2 22 58.42 8.52 -6 -2 22 61.12 10.31 6 -2 -22 76.43 11.08 -6 2 22 60.09 10.55 6 2 -22 80.32 8.74 5 -2 -22 85.82 11.25 -5 -2 22 87.92 9.75 -5 -2 22 104.80 13.30 -5 2 22 92.29 12.06 5 2 -22 90.54 9.23 -5 2 22 75.88 10.72 -4 -2 22 168.01 15.29 -4 -2 22 181.51 14.29 4 -2 -22 193.25 15.71 -4 2 22 184.85 15.80 -4 2 22 175.01 15.39 4 2 -22 166.76 13.18 3 -2 -22 13.13 5.60 -3 -2 22 33.06 7.55 -3 -2 22 15.07 5.76 -3 -2 22 20.71 5.83 3 2 -22 29.93 5.83 -3 2 22 11.93 5.68 -3 2 22 21.70 7.08 -2 -2 22 27.79 7.37 2 -2 -22 37.43 6.56 -2 -2 22 25.28 6.22 -2 2 22 17.97 6.66 -2 2 22 14.09 5.56 -2 2 22 23.77 7.05 -1 -2 22 16.69 6.47 -1 -2 22 10.35 4.84 -1 -2 22 17.50 6.73 -1 2 22 20.87 7.26 -1 2 22 9.55 6.03 -1 2 22 10.07 6.42 -8 -3 22 73.41 10.66 8 -3 -22 66.67 10.82 -8 -3 22 46.82 6.91 -8 3 22 60.91 10.34 8 3 -22 56.71 8.92 -8 3 22 72.51 10.72 -7 -3 22 2.31 3.81 7 -3 -22 3.55 4.53 -7 -3 22 -0.95 3.35 7 3 -22 3.01 3.55 -7 3 22 3.33 4.24 -7 3 22 -0.75 4.62 -6 -3 22 34.82 6.51 -6 -3 22 34.04 8.45 6 -3 -22 27.56 7.53 -6 3 22 33.91 7.60 -6 3 22 49.83 9.40 6 3 -22 43.29 6.94 -5 -3 22 28.76 7.62 -5 -3 22 17.63 5.58 5 -3 -22 30.49 7.31 5 3 -22 29.48 6.10 -5 3 22 33.40 7.69 -5 3 22 28.72 7.54 -4 -3 22 64.39 10.82 -4 -3 22 89.12 9.85 4 -3 -22 101.86 11.13 -4 3 22 80.10 11.34 4 3 -22 110.39 9.32 -4 3 22 80.89 11.83 -3 -3 22 169.14 12.84 -3 -3 22 183.01 15.71 -3 -3 22 186.39 14.51 3 -3 -22 183.45 15.66 -3 3 22 139.59 14.83 -3 3 22 167.14 15.15 -2 -3 22 -6.76 4.23 -2 -3 22 8.15 4.60 -2 -3 22 -1.02 3.63 2 -3 -22 13.12 5.92 -2 3 22 13.70 5.93 -2 3 22 -9.71 4.04 -2 3 22 6.81 4.25 -1 -3 22 13.99 6.23 -1 -3 22 16.84 6.86 -1 -3 22 8.71 4.21 -1 3 22 13.82 5.87 -1 3 22 16.87 6.62 -1 3 22 28.13 7.72 -7 -4 22 193.88 13.04 -7 -4 22 214.72 17.11 -7 4 22 174.23 16.58 -7 4 22 210.81 16.60 7 4 -22 208.41 14.57 -6 -4 22 5.85 4.20 -6 -4 22 20.88 6.39 6 -4 -22 6.63 4.72 6 4 -22 26.19 5.60 -6 4 22 16.37 6.10 -6 4 22 6.50 4.43 -5 -4 22 -4.11 3.78 5 -4 -22 6.24 4.99 -5 -4 22 2.77 4.15 -5 4 22 3.02 4.30 -5 4 22 4.81 5.00 5 4 -22 -3.30 2.43 4 -4 -22 16.66 6.18 -4 -4 22 6.23 5.87 -4 -4 22 12.20 5.19 4 4 -22 21.54 4.49 -4 4 22 11.36 6.55 -4 4 22 6.61 5.49 -3 -4 22 96.81 10.22 -3 -4 22 91.52 12.74 3 -4 -22 93.21 12.89 -3 -4 22 87.73 8.57 -3 4 22 85.81 12.14 -3 4 22 92.29 12.44 -2 -4 22 -2.52 3.55 2 -4 -22 2.17 4.13 -2 -4 22 6.92 5.85 -2 -4 22 8.69 5.90 -2 4 22 2.22 4.95 -2 4 22 4.54 4.54 -2 4 22 -5.46 3.77 -6 -5 22 13.22 6.55 -6 -5 22 8.51 4.35 6 -5 -22 29.32 7.59 -6 5 22 0.23 4.95 -6 5 22 14.33 6.73 6 5 -22 22.80 4.89 5 -5 -22 9.17 5.51 -5 -5 22 4.35 4.27 5 5 -22 8.14 3.32 -5 5 22 3.42 5.59 -5 5 22 8.84 5.19 4 -5 -22 5.35 4.61 -4 -5 22 -8.87 4.03 -4 -5 22 2.19 3.56 -4 -5 22 -4.96 3.33 -4 5 22 -6.79 4.07 -4 5 22 4.94 5.24 -6 0 23 -5.08 2.09 -6 0 23 -0.12 4.22 6 0 -23 12.33 4.99 5 0 -23 0.96 5.07 -5 0 23 -0.87 4.49 -4 0 23 -4.49 4.74 -4 0 23 8.00 5.45 4 0 -23 2.50 3.67 -5 -1 23 3.72 4.65 -5 -1 23 10.99 6.00 5 -1 -23 1.84 4.09 -5 1 23 3.00 4.75 5 1 -23 3.23 4.33 -5 1 23 2.78 5.53 0 0 0 0.00 0.00 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.7143 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71072 12.531 13.683 17.986 89.996 107.932 90.002 ) _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 41120 _shelx_res_file ; TITL shelxt_a.res in P2(1)/c shelx.res created by SHELXL-2018/3 at 16:39:54 on 15-Jan-2023 CELL 0.71073 12.5274 13.6748 17.9841 90.000 107.934 90.000 ZERR 4.00 0.0005 0.0005 0.0007 0.000 0.001 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H MN O P S UNIT 120 120 4 8 4 20 MERG 2 OMIT 0 0 2 OMIT -1 1 1 OMIT -1 0 2 OMIT 1 1 0 OMIT 0 1 2 FMAP 2 PLAN 5 ACTA SIZE 0.03 0.03 0.02 TEMP -166 BOND $H CONF LIST 4 L.S. 64 WGHT 0.026800 3.074400 FVAR 0.24461 C1 1 0.835386 0.294716 0.763841 11.00000 0.01428 0.01181 = 0.01206 0.00099 0.00487 0.00154 C2 1 0.788948 0.265170 0.683930 11.00000 0.01274 0.01239 = 0.01471 -0.00008 0.00323 0.00043 C3 1 0.871472 0.283574 0.645378 11.00000 0.01491 0.01414 = 0.01193 -0.00063 0.00415 0.00076 C4 1 0.968079 0.325356 0.700105 11.00000 0.01317 0.01235 = 0.01391 0.00041 0.00440 0.00342 C5 1 0.945897 0.330821 0.774265 11.00000 0.01081 0.01301 = 0.01153 0.00058 0.00166 0.00184 C6 1 0.781087 0.462979 0.589308 11.00000 0.01881 0.01941 = 0.01856 0.00129 0.00879 0.00740 C7 1 0.914752 0.524162 0.719796 11.00000 0.01382 0.01671 = 0.01810 0.00326 0.00607 0.00392 C11 1 0.770683 0.146523 0.843124 11.00000 0.03572 0.01839 = 0.02723 0.00364 0.01620 -0.00045 AFIX 137 H11A 2 0.707174 0.121871 0.800406 11.00000 -1.50000 H11B 2 0.762567 0.125891 0.893290 11.00000 -1.50000 H11C 2 0.840774 0.120232 0.837860 11.00000 -1.50000 AFIX 0 C12 1 0.720149 0.079177 0.640811 11.00000 0.02920 0.02032 = 0.04297 -0.00886 0.01082 -0.00307 AFIX 137 H12A 2 0.756807 0.076923 0.599926 11.00000 -1.50000 H12B 2 0.659383 0.030940 0.629301 11.00000 -1.50000 H12C 2 0.775142 0.064165 0.691476 11.00000 -1.50000 AFIX 0 C13 1 0.961084 0.158318 0.562244 11.00000 0.03096 0.02173 = 0.02097 -0.00350 0.01079 0.00550 AFIX 137 H13A 2 1.034358 0.186743 0.589965 11.00000 -1.50000 H13B 2 0.962295 0.132937 0.511550 11.00000 -1.50000 H13C 2 0.944694 0.104879 0.593374 11.00000 -1.50000 AFIX 0 C14 1 1.067455 0.421424 0.600002 11.00000 0.02614 0.02679 = 0.02025 0.00102 0.01050 -0.00649 AFIX 137 H14A 2 1.024044 0.380411 0.556497 11.00000 -1.50000 H14B 2 1.137165 0.442087 0.590701 11.00000 -1.50000 H14C 2 1.023285 0.479200 0.604037 11.00000 -1.50000 AFIX 0 C15 1 1.071969 0.253874 0.914837 11.00000 0.02196 0.02311 = 0.01410 0.00463 0.00179 0.00496 AFIX 137 H15A 2 1.003813 0.229547 0.924446 11.00000 -1.50000 H15B 2 1.130852 0.263273 0.964824 11.00000 -1.50000 H15C 2 1.097329 0.206310 0.883143 11.00000 -1.50000 AFIX 0 C21 1 0.683576 0.521496 0.809335 11.00000 0.01783 0.01103 = 0.00978 0.00126 0.00500 -0.00097 C22 1 0.785836 0.512436 0.867952 11.00000 0.01588 0.01445 = 0.01445 0.00016 0.00471 0.00069 AFIX 43 H22 2 0.850027 0.490340 0.855295 11.00000 -1.20000 AFIX 0 C23 1 0.794729 0.535531 0.945031 11.00000 0.02016 0.01868 = 0.01235 -0.00055 0.00051 0.00071 AFIX 43 H23 2 0.864998 0.529479 0.984609 11.00000 -1.20000 AFIX 0 C24 1 0.702209 0.567075 0.964130 11.00000 0.03095 0.01754 = 0.00988 -0.00171 0.00749 0.00070 AFIX 43 H24 2 0.708087 0.581327 1.016945 11.00000 -1.20000 AFIX 0 C25 1 0.599965 0.578021 0.905758 11.00000 0.02129 0.02395 = 0.01896 -0.00247 0.01074 0.00428 AFIX 43 H25 2 0.536154 0.600412 0.918756 11.00000 -1.20000 AFIX 0 C26 1 0.590828 0.556411 0.828781 11.00000 0.01717 0.02161 = 0.01534 -0.00049 0.00424 0.00303 AFIX 43 H26 2 0.521193 0.565378 0.789064 11.00000 -1.20000 AFIX 0 C31 1 0.548377 0.415567 0.672729 11.00000 0.01047 0.01298 = 0.01248 -0.00041 0.00223 0.00262 C32 1 0.505164 0.400753 0.592305 11.00000 0.01596 0.01577 = 0.01414 0.00020 0.00667 0.00136 AFIX 43 H32 2 0.544190 0.426062 0.558829 11.00000 -1.20000 AFIX 0 C33 1 0.406077 0.349619 0.560551 11.00000 0.01793 0.01807 = 0.01306 -0.00430 -0.00068 0.00361 AFIX 43 H33 2 0.376488 0.341291 0.505565 11.00000 -1.20000 AFIX 0 C34 1 0.350431 0.310747 0.609310 11.00000 0.01378 0.02089 = 0.02507 -0.00697 0.00365 -0.00342 AFIX 43 H34 2 0.281374 0.277189 0.587808 11.00000 -1.20000 AFIX 0 C35 1 0.395478 0.320827 0.689302 11.00000 0.02106 0.02410 = 0.02404 -0.00029 0.01033 -0.00598 AFIX 43 H35 2 0.358677 0.291637 0.722675 11.00000 -1.20000 AFIX 0 C36 1 0.493762 0.373035 0.721484 11.00000 0.01662 0.02015 = 0.01293 -0.00053 0.00461 -0.00270 AFIX 43 H36 2 0.523817 0.379817 0.776584 11.00000 -1.20000 AFIX 0 C51 1 0.626127 0.608235 0.660441 11.00000 0.01440 0.01375 = 0.00858 0.00043 0.00501 0.00203 C52 1 0.703795 0.683749 0.667885 11.00000 0.01563 0.01691 = 0.01238 0.00099 0.00451 0.00093 AFIX 43 H52 2 0.780817 0.672174 0.694765 11.00000 -1.20000 AFIX 0 C53 1 0.669697 0.775759 0.636391 11.00000 0.02015 0.01653 = 0.01358 -0.00016 0.00614 -0.00302 AFIX 43 H53 2 0.723525 0.826350 0.641772 11.00000 -1.20000 AFIX 0 C54 1 0.557534 0.793936 0.597198 11.00000 0.02382 0.01522 = 0.01496 0.00384 0.00793 0.00489 AFIX 43 H54 2 0.534531 0.856712 0.575546 11.00000 -1.20000 AFIX 0 C55 1 0.479295 0.720237 0.589774 11.00000 0.01475 0.02165 = 0.01906 0.00215 0.00491 0.00424 AFIX 43 H55 2 0.402407 0.732360 0.562848 11.00000 -1.20000 AFIX 0 C56 1 0.513045 0.628294 0.621706 11.00000 0.01327 0.01938 = 0.01670 0.00088 0.00522 -0.00013 AFIX 43 H56 2 0.458540 0.578477 0.617134 11.00000 -1.20000 AFIX 0 MN1 3 0.827706 0.420181 0.687868 11.00000 0.01027 0.01196 = 0.00930 0.00041 0.00335 0.00097 O1 4 0.756360 0.486433 0.524637 11.00000 0.04628 0.04108 = 0.01594 0.01216 0.01415 0.02169 O2 4 0.978977 0.587240 0.740768 11.00000 0.02018 0.01753 = 0.03390 0.00026 0.00567 -0.00397 P1 5 0.675027 0.489760 0.708388 11.00000 0.01006 0.01239 = 0.00886 0.00015 0.00284 0.00042 S1 6 0.773515 0.278813 0.839084 11.00000 0.01780 0.01596 = 0.01425 0.00203 0.00842 0.00022 S2 6 0.662708 0.201003 0.644026 11.00000 0.01591 0.01967 = 0.02358 -0.00379 0.00378 -0.00190 S3 6 0.854006 0.251206 0.547210 11.00000 0.01900 0.02108 = 0.01074 -0.00326 0.00408 0.00180 S4 6 1.100346 0.352546 0.689760 11.00000 0.01183 0.02332 = 0.01855 0.00141 0.00668 0.00075 S5 6 1.042188 0.369568 0.863185 11.00000 0.01381 0.01821 = 0.01088 -0.00120 0.00027 0.00023 HKLF 4 REM shelxt_a.res in P2(1)/c REM wR2 = 0.0757, GooF = S = 1.041, Restrained GooF = 1.041 for all data REM R1 = 0.0300 for 5457 Fo > 4sig(Fo) and 0.0408 for all 6471 data REM 357 parameters refined using 0 restraints END WGHT 0.0268 3.0740 REM Highest difference peak 0.412, deepest hole -0.502, 1-sigma level 0.079 Q1 1 0.6403 0.5410 0.8170 11.00000 0.05 0.41 Q2 1 0.8344 0.2578 0.6680 11.00000 0.05 0.41 Q3 1 0.7459 0.2340 0.6672 11.00000 0.05 0.40 Q4 1 0.6534 0.5765 0.9332 11.00000 0.05 0.39 Q5 1 0.6793 0.7223 0.6444 11.00000 0.05 0.39 ; _shelx_res_checksum 72351 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.83539(16) 0.29472(14) 0.76384(11) 0.0125(4) Uani d 1 . . C C2 0.78895(16) 0.26517(14) 0.68393(12) 0.0135(4) Uani d 1 . . C C3 0.87147(16) 0.28357(14) 0.64538(11) 0.0137(4) Uani d 1 . . C C4 0.96808(16) 0.32536(14) 0.70010(11) 0.0131(4) Uani d 1 . . C C5 0.94590(16) 0.33082(14) 0.77426(11) 0.0122(4) Uani d 1 . . C C6 0.78109(18) 0.46298(16) 0.58931(13) 0.0182(4) Uani d 1 . . C C7 0.91475(17) 0.52416(15) 0.71980(12) 0.0159(4) Uani d 1 . . C C11 0.7707(2) 0.14652(16) 0.84312(14) 0.0256(5) Uani d 1 . . H H11A 0.707174 0.121871 0.800406 0.038 Uiso calc 1 . . H H11B 0.762567 0.125891 0.893290 0.038 Uiso calc 1 . . H H11C 0.840774 0.120232 0.837860 0.038 Uiso calc 1 . . C C12 0.7201(2) 0.07918(17) 0.64081(16) 0.0309(6) Uani d 1 . . H H12A 0.756807 0.076923 0.599926 0.046 Uiso calc 1 . . H H12B 0.659383 0.030940 0.629301 0.046 Uiso calc 1 . . H H12C 0.775142 0.064165 0.691476 0.046 Uiso calc 1 . . C C13 0.9611(2) 0.15832(17) 0.56224(13) 0.0239(5) Uani d 1 . . H H13A 1.034358 0.186743 0.589965 0.036 Uiso calc 1 . . H H13B 0.962295 0.132937 0.511550 0.036 Uiso calc 1 . . H H13C 0.944694 0.104879 0.593374 0.036 Uiso calc 1 . . C C14 1.0675(2) 0.42142(17) 0.60000(13) 0.0236(5) Uani d 1 . . H H14A 1.024044 0.380411 0.556497 0.035 Uiso calc 1 . . H H14B 1.137165 0.442087 0.590701 0.035 Uiso calc 1 . . H H14C 1.023285 0.479200 0.604037 0.035 Uiso calc 1 . . C C15 1.07197(18) 0.25387(16) 0.91484(12) 0.0206(5) Uani d 1 . . H H15A 1.003813 0.229547 0.924446 0.031 Uiso calc 1 . . H H15B 1.130852 0.263273 0.964824 0.031 Uiso calc 1 . . H H15C 1.097329 0.206310 0.883143 0.031 Uiso calc 1 . . C C21 0.68358(17) 0.52150(14) 0.80934(11) 0.0127(4) Uani d 1 . . C C22 0.78584(17) 0.51244(14) 0.86795(12) 0.0149(4) Uani d 1 . . H H22 0.850027 0.490340 0.855295 0.018 Uiso calc 1 . . C C23 0.79473(18) 0.53553(15) 0.94503(12) 0.0181(4) Uani d 1 . . H H23 0.864998 0.529479 0.984609 0.022 Uiso calc 1 . . C C24 0.70221(19) 0.56707(15) 0.96413(12) 0.0192(4) Uani d 1 . . H H24 0.708087 0.581327 1.016945 0.023 Uiso calc 1 . . C C25 0.59997(18) 0.57802(16) 0.90576(13) 0.0204(5) Uani d 1 . . H H25 0.536154 0.600412 0.918756 0.024 Uiso calc 1 . . C C26 0.59083(18) 0.55641(16) 0.82878(12) 0.0182(4) Uani d 1 . . H H26 0.521193 0.565378 0.789064 0.022 Uiso calc 1 . . C C31 0.54838(16) 0.41557(14) 0.67273(11) 0.0123(4) Uani d 1 . . C C32 0.50516(17) 0.40075(14) 0.59230(12) 0.0148(4) Uani d 1 . . H H32 0.544190 0.426062 0.558829 0.018 Uiso calc 1 . . C C33 0.40608(17) 0.34962(15) 0.56055(12) 0.0176(4) Uani d 1 . . H H33 0.376488 0.341291 0.505565 0.021 Uiso calc 1 . . C C34 0.35043(18) 0.31075(16) 0.60931(13) 0.0204(5) Uani d 1 . . H H34 0.281374 0.277189 0.587808 0.025 Uiso calc 1 . . C C35 0.39548(19) 0.32083(17) 0.68930(13) 0.0223(5) Uani d 1 . . H H35 0.358677 0.291637 0.722675 0.027 Uiso calc 1 . . C C36 0.49376(17) 0.37304(15) 0.72148(12) 0.0166(4) Uani d 1 . . H H36 0.523817 0.379817 0.776584 0.020 Uiso calc 1 . . C C51 0.62613(16) 0.60824(14) 0.66044(11) 0.0119(4) Uani d 1 . . C C52 0.70379(17) 0.68375(15) 0.66788(12) 0.0149(4) Uani d 1 . . H H52 0.780817 0.672174 0.694765 0.018 Uiso calc 1 . . C C53 0.66970(18) 0.77576(15) 0.63639(12) 0.0165(4) Uani d 1 . . H H53 0.723525 0.826350 0.641772 0.020 Uiso calc 1 . . C C54 0.55753(18) 0.79394(15) 0.59720(12) 0.0176(4) Uani d 1 . . H H54 0.534531 0.856712 0.575546 0.021 Uiso calc 1 . . C C55 0.47930(18) 0.72024(16) 0.58977(12) 0.0186(4) Uani d 1 . . H H55 0.402407 0.732360 0.562848 0.022 Uiso calc 1 . . C C56 0.51305(17) 0.62829(15) 0.62171(12) 0.0163(4) Uani d 1 . . H H56 0.458540 0.578477 0.617134 0.020 Uiso calc 1 . . Mn Mn1 0.82771(2) 0.42018(2) 0.68787(2) 0.01044(8) Uani d 1 . . O O1 0.75636(16) 0.48643(13) 0.52464(9) 0.0334(4) Uani d 1 . . O O2 0.97898(13) 0.58724(11) 0.74077(10) 0.0245(4) Uani d 1 . . P P1 0.67503(4) 0.48976(4) 0.70839(3) 0.01046(10) Uani d 1 . . S S1 0.77351(4) 0.27881(4) 0.83908(3) 0.01521(11) Uani d 1 . . S S2 0.66271(4) 0.20100(4) 0.64403(3) 0.02024(12) Uani d 1 . . S S3 0.85401(4) 0.25121(4) 0.54721(3) 0.01705(11) Uani d 1 . . S S4 1.10035(4) 0.35255(4) 0.68976(3) 0.01745(11) Uani d 1 . . S S5 1.04219(4) 0.36957(4) 0.86318(3) 0.01510(11) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0143(9) 0.0118(9) 0.0121(9) 0.0015(7) 0.0049(8) 0.0010(7) C2 0.0127(9) 0.0124(9) 0.0147(10) 0.0004(7) 0.0032(8) -0.0001(8) C3 0.0149(10) 0.0141(9) 0.0119(9) 0.0008(8) 0.0041(8) -0.0006(8) C4 0.0132(9) 0.0124(9) 0.0139(10) 0.0034(7) 0.0044(8) 0.0004(8) C5 0.0108(9) 0.0130(9) 0.0115(9) 0.0018(7) 0.0017(7) 0.0006(7) C6 0.0188(10) 0.0194(10) 0.0186(11) 0.0074(8) 0.0088(9) 0.0013(9) C7 0.0138(10) 0.0167(10) 0.0181(10) 0.0039(8) 0.0061(8) 0.0033(8) C11 0.0357(13) 0.0184(11) 0.0272(12) -0.0004(10) 0.0162(11) 0.0036(9) C12 0.0292(13) 0.0203(12) 0.0430(15) -0.0031(10) 0.0108(11) -0.0089(11) C13 0.0310(13) 0.0217(11) 0.0210(11) 0.0055(10) 0.0108(10) -0.0035(9) C14 0.0261(12) 0.0268(12) 0.0203(11) -0.0065(9) 0.0105(9) 0.0010(9) C15 0.0220(11) 0.0231(11) 0.0141(10) 0.0050(9) 0.0018(9) 0.0046(9) C21 0.0178(10) 0.0110(9) 0.0098(9) -0.0010(8) 0.0050(8) 0.0013(7) C22 0.0159(10) 0.0145(9) 0.0144(10) 0.0007(8) 0.0047(8) 0.0002(8) C23 0.0202(11) 0.0187(10) 0.0124(10) 0.0007(8) 0.0005(8) -0.0005(8) C24 0.0309(12) 0.0175(10) 0.0099(10) 0.0007(9) 0.0075(9) -0.0017(8) C25 0.0213(11) 0.0239(11) 0.0190(11) 0.0043(9) 0.0107(9) -0.0025(9) C26 0.0172(10) 0.0216(11) 0.0153(10) 0.0030(8) 0.0042(8) -0.0005(8) C31 0.0105(9) 0.0130(9) 0.0125(9) 0.0026(7) 0.0022(7) -0.0004(7) C32 0.0160(10) 0.0158(10) 0.0141(10) 0.0014(8) 0.0067(8) 0.0002(8) C33 0.0179(10) 0.0181(10) 0.0131(10) 0.0036(8) -0.0007(8) -0.0043(8) C34 0.0138(10) 0.0209(11) 0.0251(12) -0.0034(8) 0.0037(9) -0.0070(9) C35 0.0211(11) 0.0241(11) 0.0240(12) -0.0060(9) 0.0103(9) -0.0003(9) C36 0.0166(10) 0.0201(10) 0.0129(10) -0.0027(8) 0.0046(8) -0.0005(8) C51 0.0144(9) 0.0137(9) 0.0086(9) 0.0020(7) 0.0050(7) 0.0004(7) C52 0.0156(10) 0.0169(10) 0.0124(9) 0.0009(8) 0.0045(8) 0.0010(8) C53 0.0202(10) 0.0165(10) 0.0136(10) -0.0030(8) 0.0061(8) -0.0002(8) C54 0.0238(11) 0.0152(10) 0.0150(10) 0.0049(8) 0.0079(9) 0.0038(8) C55 0.0148(10) 0.0216(11) 0.0191(10) 0.0042(8) 0.0049(8) 0.0022(9) C56 0.0133(10) 0.0194(10) 0.0167(10) -0.0001(8) 0.0052(8) 0.0009(8) Mn1 0.01027(14) 0.01196(14) 0.00930(14) 0.00097(11) 0.00335(11) 0.00041(11) O1 0.0463(11) 0.0411(10) 0.0159(8) 0.0217(9) 0.0141(8) 0.0122(8) O2 0.0202(8) 0.0175(8) 0.0339(9) -0.0040(6) 0.0057(7) 0.0003(7) P1 0.0101(2) 0.0124(2) 0.0089(2) 0.00042(18) 0.00284(18) 0.00015(19) S1 0.0178(2) 0.0160(2) 0.0142(2) 0.00022(19) 0.0084(2) 0.00203(19) S2 0.0159(3) 0.0197(3) 0.0236(3) -0.0019(2) 0.0038(2) -0.0038(2) S3 0.0190(3) 0.0211(3) 0.0107(2) 0.0018(2) 0.0041(2) -0.0033(2) S4 0.0118(2) 0.0233(3) 0.0186(3) 0.0008(2) 0.0067(2) 0.0014(2) S5 0.0138(2) 0.0182(2) 0.0109(2) 0.00023(19) 0.00027(18) -0.00120(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C5 C1 C2 . . 107.89(17) ? C5 C1 S1 . . 125.34(15) ? C2 C1 S1 . . 126.51(15) ? C5 C1 Mn1 . . 70.32(11) ? C2 C1 Mn1 . . 70.54(11) ? S1 C1 Mn1 . . 129.22(10) ? C1 C2 C3 . . 107.77(17) ? C1 C2 S2 . . 125.95(15) ? C3 C2 S2 . . 125.64(15) ? C1 C2 Mn1 . . 70.99(11) ? C3 C2 Mn1 . . 69.94(11) ? S2 C2 Mn1 . . 131.69(11) ? C4 C3 C2 . . 108.81(17) ? C4 C3 S3 . . 127.49(15) ? C2 C3 S3 . . 123.60(15) ? C4 C3 Mn1 . . 70.21(11) ? C2 C3 Mn1 . . 71.34(11) ? S3 C3 Mn1 . . 127.26(11) ? C3 C4 C5 . . 107.13(17) ? C3 C4 S4 . . 129.66(15) ? C5 C4 S4 . . 122.71(15) ? C3 C4 Mn1 . . 71.06(11) ? C5 C4 Mn1 . . 71.24(11) ? S4 C4 Mn1 . . 129.07(11) ? C1 C5 C4 . . 108.38(17) ? C1 C5 S5 . . 126.06(15) ? C4 C5 S5 . . 125.48(15) ? C1 C5 Mn1 . . 71.30(11) ? C4 C5 Mn1 . . 69.52(11) ? S5 C5 Mn1 . . 127.42(10) ? O1 C6 Mn1 . . 175.31(19) ? O2 C7 Mn1 . . 174.41(18) ? S1 C11 H11A . . 109.5 ? S1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? S1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? S2 C12 H12A . . 109.5 ? S2 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? S2 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? S3 C13 H13A . . 109.5 ? S3 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? S3 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? S4 C14 H14A . . 109.5 ? S4 C14 H14B . . 109.5 ? H14A C14 H14B . . 109.5 ? S4 C14 H14C . . 109.5 ? H14A C14 H14C . . 109.5 ? H14B C14 H14C . . 109.5 ? S5 C15 H15A . . 109.5 ? S5 C15 H15B . . 109.5 ? H15A C15 H15B . . 109.5 ? S5 C15 H15C . . 109.5 ? H15A C15 H15C . . 109.5 ? H15B C15 H15C . . 109.5 ? C22 C21 C26 . . 118.92(18) ? C22 C21 P1 . . 119.18(15) ? C26 C21 P1 . . 121.89(15) ? C21 C22 C23 . . 120.45(19) ? C21 C22 H22 . . 119.8 ? C23 C22 H22 . . 119.8 ? C24 C23 C22 . . 120.29(19) ? C24 C23 H23 . . 119.9 ? C22 C23 H23 . . 119.9 ? C23 C24 C25 . . 119.73(19) ? C23 C24 H24 . . 120.1 ? C25 C24 H24 . . 120.1 ? C26 C25 C24 . . 120.30(19) ? C26 C25 H25 . . 119.9 ? C24 C25 H25 . . 119.9 ? C25 C26 C21 . . 120.27(19) ? C25 C26 H26 . . 119.9 ? C21 C26 H26 . . 119.9 ? C32 C31 C36 . . 118.86(18) ? C32 C31 P1 . . 117.59(15) ? C36 C31 P1 . . 123.55(15) ? C33 C32 C31 . . 120.89(19) ? C33 C32 H32 . . 119.6 ? C31 C32 H32 . . 119.6 ? C34 C33 C32 . . 119.67(19) ? C34 C33 H33 . . 120.2 ? C32 C33 H33 . . 120.2 ? C35 C34 C33 . . 119.9(2) ? C35 C34 H34 . . 120.1 ? C33 C34 H34 . . 120.1 ? C34 C35 C36 . . 120.8(2) ? C34 C35 H35 . . 119.6 ? C36 C35 H35 . . 119.6 ? C35 C36 C31 . . 119.80(19) ? C35 C36 H36 . . 120.1 ? C31 C36 H36 . . 120.1 ? C52 C51 C56 . . 118.11(18) ? C52 C51 P1 . . 118.83(15) ? C56 C51 P1 . . 122.89(15) ? C53 C52 C51 . . 120.79(19) ? C53 C52 H52 . . 119.6 ? C51 C52 H52 . . 119.6 ? C54 C53 C52 . . 120.32(19) ? C54 C53 H53 . . 119.8 ? C52 C53 H53 . . 119.8 ? C55 C54 C53 . . 119.69(19) ? C55 C54 H54 . . 120.2 ? C53 C54 H54 . . 120.2 ? C54 C55 C56 . . 120.12(19) ? C54 C55 H55 . . 119.9 ? C56 C55 H55 . . 119.9 ? C55 C56 C51 . . 120.95(19) ? C55 C56 H56 . . 119.5 ? C51 C56 H56 . . 119.5 ? C7 Mn1 C6 . . 92.24(10) ? C7 Mn1 C4 . . 92.78(8) ? C6 Mn1 C4 . . 107.93(8) ? C7 Mn1 C3 . . 127.69(8) ? C6 Mn1 C3 . . 88.47(9) ? C4 Mn1 C3 . . 38.73(7) ? C7 Mn1 C5 . . 90.21(8) ? C6 Mn1 C5 . . 147.16(8) ? C4 Mn1 C5 . . 39.24(7) ? C3 Mn1 C5 . . 64.66(7) ? C7 Mn1 C2 . . 154.30(8) ? C6 Mn1 C2 . . 106.63(9) ? C4 Mn1 C2 . . 65.19(7) ? C3 Mn1 C2 . . 38.72(7) ? C5 Mn1 C2 . . 64.45(7) ? C7 Mn1 C1 . . 121.60(8) ? C6 Mn1 C1 . . 145.00(9) ? C4 Mn1 C1 . . 65.29(7) ? C3 Mn1 C1 . . 64.65(7) ? C5 Mn1 C1 . . 38.38(7) ? C2 Mn1 C1 . . 38.47(7) ? C7 Mn1 P1 . . 94.37(7) ? C6 Mn1 P1 . . 89.40(7) ? C4 Mn1 P1 . . 160.97(6) ? C3 Mn1 P1 . . 137.93(6) ? C5 Mn1 P1 . . 123.05(5) ? C2 Mn1 P1 . . 102.93(5) ? C1 Mn1 P1 . . 96.03(5) ? C31 P1 C21 . . 104.97(9) ? C31 P1 C51 . . 101.30(9) ? C21 P1 C51 . . 99.44(9) ? C31 P1 Mn1 . . 113.29(6) ? C21 P1 Mn1 . . 117.70(7) ? C51 P1 Mn1 . . 117.84(6) ? C1 S1 C11 . . 99.92(10) ? C2 S2 C12 . . 98.91(10) ? C3 S3 C13 . . 99.72(10) ? C4 S4 C14 . . 103.97(10) ? C5 S5 C15 . . 100.24(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 C5 . 1.427(3) ? C1 C2 . 1.433(3) ? C1 S1 . 1.768(2) ? C1 Mn1 . 2.1769(19) ? C2 C3 . 1.433(3) ? C2 S2 . 1.757(2) ? C2 Mn1 . 2.171(2) ? C3 C4 . 1.423(3) ? C3 S3 . 1.767(2) ? C3 Mn1 . 2.152(2) ? C4 C5 . 1.446(3) ? C4 S4 . 1.763(2) ? C4 Mn1 . 2.1410(19) ? C5 S5 . 1.762(2) ? C5 Mn1 . 2.1640(19) ? C6 O1 . 1.153(3) ? C6 Mn1 . 1.785(2) ? C7 O2 . 1.160(3) ? C7 Mn1 . 1.776(2) ? C11 S1 . 1.811(2) ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 S2 . 1.823(2) ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 S3 . 1.806(2) ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C14 S4 . 1.804(2) ? C14 H14A . 0.9800 ? C14 H14B . 0.9800 ? C14 H14C . 0.9800 ? C15 S5 . 1.814(2) ? C15 H15A . 0.9800 ? C15 H15B . 0.9800 ? C15 H15C . 0.9800 ? C21 C22 . 1.391(3) ? C21 C26 . 1.397(3) ? C21 P1 . 1.837(2) ? C22 C23 . 1.392(3) ? C22 H22 . 0.9500 ? C23 C24 . 1.376(3) ? C23 H23 . 0.9500 ? C24 C25 . 1.392(3) ? C24 H24 . 0.9500 ? C25 C26 . 1.385(3) ? C25 H25 . 0.9500 ? C26 H26 . 0.9500 ? C31 C32 . 1.394(3) ? C31 C36 . 1.394(3) ? C31 P1 . 1.825(2) ? C32 C33 . 1.385(3) ? C32 H32 . 0.9500 ? C33 C34 . 1.383(3) ? C33 H33 . 0.9500 ? C34 C35 . 1.381(3) ? C34 H34 . 0.9500 ? C35 C36 . 1.386(3) ? C35 H35 . 0.9500 ? C36 H36 . 0.9500 ? C51 C52 . 1.397(3) ? C51 C56 . 1.400(3) ? C51 P1 . 1.849(2) ? C52 C53 . 1.392(3) ? C52 H52 . 0.9500 ? C53 C54 . 1.387(3) ? C53 H53 . 0.9500 ? C54 C55 . 1.383(3) ? C54 H54 . 0.9500 ? C55 C56 . 1.393(3) ? C55 H55 . 0.9500 ? C56 H56 . 0.9500 ? Mn1 P1 . 2.2659(6) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C5 C1 C2 C3 . . . . -0.1(2) ? S1 C1 C2 C3 . . . . -174.49(14) ? Mn1 C1 C2 C3 . . . . 60.56(14) ? C5 C1 C2 S2 . . . . 171.05(15) ? S1 C1 C2 S2 . . . . -3.3(3) ? Mn1 C1 C2 S2 . . . . -128.25(16) ? C5 C1 C2 Mn1 . . . . -60.70(13) ? S1 C1 C2 Mn1 . . . . 124.95(16) ? C1 C2 C3 C4 . . . . -0.7(2) ? S2 C2 C3 C4 . . . . -171.96(15) ? Mn1 C2 C3 C4 . . . . 60.50(14) ? C1 C2 C3 S3 . . . . 175.89(14) ? S2 C2 C3 S3 . . . . 4.7(3) ? Mn1 C2 C3 S3 . . . . -122.88(15) ? C1 C2 C3 Mn1 . . . . -61.23(13) ? S2 C2 C3 Mn1 . . . . 127.55(16) ? C2 C3 C4 C5 . . . . 1.3(2) ? S3 C3 C4 C5 . . . . -175.15(15) ? Mn1 C3 C4 C5 . . . . 62.51(13) ? C2 C3 C4 S4 . . . . 173.26(15) ? S3 C3 C4 S4 . . . . -3.2(3) ? Mn1 C3 C4 S4 . . . . -125.53(17) ? C2 C3 C4 Mn1 . . . . -61.21(14) ? S3 C3 C4 Mn1 . . . . 122.34(17) ? C2 C1 C5 C4 . . . . 0.9(2) ? S1 C1 C5 C4 . . . . 175.38(14) ? Mn1 C1 C5 C4 . . . . -59.89(13) ? C2 C1 C5 S5 . . . . -176.00(14) ? S1 C1 C5 S5 . . . . -1.6(3) ? Mn1 C1 C5 S5 . . . . 123.17(16) ? C2 C1 C5 Mn1 . . . . 60.84(13) ? S1 C1 C5 Mn1 . . . . -124.73(15) ? C3 C4 C5 C1 . . . . -1.4(2) ? S4 C4 C5 C1 . . . . -174.03(14) ? Mn1 C4 C5 C1 . . . . 61.01(13) ? C3 C4 C5 S5 . . . . 175.57(15) ? S4 C4 C5 S5 . . . . 2.9(3) ? Mn1 C4 C5 S5 . . . . -122.03(15) ? C3 C4 C5 Mn1 . . . . -62.40(13) ? S4 C4 C5 Mn1 . . . . 124.96(15) ? C26 C21 C22 C23 . . . . 1.6(3) ? P1 C21 C22 C23 . . . . -179.71(16) ? C21 C22 C23 C24 . . . . 0.4(3) ? C22 C23 C24 C25 . . . . -1.5(3) ? C23 C24 C25 C26 . . . . 0.6(3) ? C24 C25 C26 C21 . . . . 1.3(3) ? C22 C21 C26 C25 . . . . -2.4(3) ? P1 C21 C26 C25 . . . . 178.90(16) ? C36 C31 C32 C33 . . . . 3.8(3) ? P1 C31 C32 C33 . . . . -176.58(15) ? C31 C32 C33 C34 . . . . -1.5(3) ? C32 C33 C34 C35 . . . . -1.8(3) ? C33 C34 C35 C36 . . . . 2.7(3) ? C34 C35 C36 C31 . . . . -0.3(3) ? C32 C31 C36 C35 . . . . -2.9(3) ? P1 C31 C36 C35 . . . . 177.53(16) ? C56 C51 C52 C53 . . . . -1.1(3) ? P1 C51 C52 C53 . . . . -176.48(15) ? C51 C52 C53 C54 . . . . 0.2(3) ? C52 C53 C54 C55 . . . . 0.3(3) ? C53 C54 C55 C56 . . . . 0.2(3) ? C54 C55 C56 C51 . . . . -1.1(3) ? C52 C51 C56 C55 . . . . 1.6(3) ? P1 C51 C56 C55 . . . . 176.74(16) ? C32 C31 P1 C21 . . . . 164.63(15) ? C36 C31 P1 C21 . . . . -15.75(19) ? C32 C31 P1 C51 . . . . 61.53(16) ? C36 C31 P1 C51 . . . . -118.84(17) ? C32 C31 P1 Mn1 . . . . -65.66(16) ? C36 C31 P1 Mn1 . . . . 113.96(16) ? C22 C21 P1 C31 . . . . 134.26(16) ? C26 C21 P1 C31 . . . . -47.07(19) ? C22 C21 P1 C51 . . . . -121.26(16) ? C26 C21 P1 C51 . . . . 57.41(18) ? C22 C21 P1 Mn1 . . . . 7.20(18) ? C26 C21 P1 Mn1 . . . . -174.13(15) ? C52 C51 P1 C31 . . . . -174.23(15) ? C56 C51 P1 C31 . . . . 10.64(19) ? C52 C51 P1 C21 . . . . 78.29(17) ? C56 C51 P1 C21 . . . . -96.83(18) ? C52 C51 P1 Mn1 . . . . -50.07(17) ? C56 C51 P1 Mn1 . . . . 134.80(15) ? C5 C1 S1 C11 . . . . -109.70(18) ? C2 C1 S1 C11 . . . . 63.7(2) ? Mn1 C1 S1 C11 . . . . 157.66(14) ? C1 C2 S2 C12 . . . . -101.27(19) ? C3 C2 S2 C12 . . . . 68.4(2) ? Mn1 C2 S2 C12 . . . . 162.59(15) ? C4 C3 S3 C13 . . . . 62.7(2) ? C2 C3 S3 C13 . . . . -113.22(18) ? Mn1 C3 S3 C13 . . . . 155.46(13) ? C3 C4 S4 C14 . . . . 50.6(2) ? C5 C4 S4 C14 . . . . -138.59(17) ? Mn1 C4 S4 C14 . . . . -46.93(16) ? C1 C5 S5 C15 . . . . 67.77(19) ? C4 C5 S5 C15 . . . . -108.66(18) ? Mn1 C5 S5 C15 . . . . 161.08(13) ?