#------------------------------------------------------------------------------ #$Date: 2024-07-13 04:57:40 +0300 (Sat, 13 Jul 2024) $ #$Revision: 293406 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/25/2312553.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312553 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7734 _cell_length_b 7.0554 _cell_length_c 19.7544 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7790 _cod_data_source_file jx3084iHOFIsup2.hkl _cod_data_source_block iHOFI _shelx_title ' b22092404qcn2phmnbr_0ma_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.44 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 603.87 561.52 13.56 o 4 0 0 3769.74 3666.85 71.97 o 6 0 0 1736.19 1704.33 57.19 o 10 0 0 929.97 940.84 38.22 o 2 1 0 13702.40 13844.99 148.87 o 4 1 0 3425.07 3354.73 42.31 o 6 1 0 3023.63 3220.61 43.73 o 8 1 0 1247.07 1205.59 29.91 o 10 1 0 0.63 5.72 9.35 o 0 2 0 35334.25 37348.97 599.24 o 2 2 0 18344.23 18633.77 173.16 o 4 2 0 6370.01 6655.24 72.07 o 6 2 0 2939.05 2971.36 40.20 o 8 2 0 154.55 160.36 10.52 o 10 2 0 1328.09 1327.39 34.21 o 2 3 0 3316.10 3046.45 36.39 o 4 3 0 6042.00 6338.20 68.91 o 6 3 0 1398.00 1426.23 23.23 o 8 3 0 3421.88 3598.65 71.34 o 10 3 0 490.05 503.44 26.60 o 0 4 0 21558.60 21408.71 293.35 o 2 4 0 4736.97 5085.74 62.63 o 4 4 0 4089.43 4449.88 55.38 o 6 4 0 2037.00 2078.72 33.05 o 8 4 0 126.50 104.27 23.04 o 10 4 0 960.31 968.30 35.48 o 2 5 0 4977.59 4944.79 94.81 o 4 5 0 1479.29 1520.44 35.24 o 6 5 0 1233.64 1283.54 36.49 o 8 5 0 553.54 529.32 40.99 o 0 6 0 24696.77 25215.59 529.59 o 2 6 0 2.95 3.56 16.34 o 4 6 0 1253.24 1363.84 69.06 o 6 6 0 775.63 809.20 43.39 o 8 6 0 20.59 11.02 21.09 o 2 7 0 2375.30 2592.71 115.85 o 4 7 0 851.39 887.52 34.39 o 6 7 0 746.01 677.27 31.42 o 0 8 0 2845.93 2986.33 119.99 o 2 8 0 1476.50 1544.13 43.71 o 4 8 0 1308.80 1300.66 47.64 o 1 0 1 45.52 33.14 1.68 o 2 0 1 1394.82 1413.61 21.91 o 3 0 1 328.41 284.23 10.11 o 4 0 1 5057.37 4996.27 55.81 o 5 0 1 507.05 476.61 32.29 o 6 0 1 145.58 144.52 12.39 o 7 0 1 180.64 -49.71 80.28 o 8 0 1 5353.52 5582.62 91.82 o 9 0 1 122.96 126.42 8.78 o 10 0 1 60.60 56.88 10.60 o 11 0 1 10.93 -9.82 12.46 o 0 1 1 281.29 214.93 5.26 o 1 1 1 128.18 115.02 2.59 o 2 1 1 4762.42 4996.18 33.38 o 3 1 1 19.10 23.00 3.17 o 4 1 1 3034.70 2939.07 23.93 o 5 1 1 1.66 22.30 29.35 o 6 1 1 5142.26 5319.51 46.38 o 7 1 1 0.52 0.12 6.47 o 8 1 1 2.32 5.32 3.88 o 9 1 1 61.87 55.08 5.99 o 10 1 1 1343.00 1370.39 28.52 o 11 1 1 3.61 9.67 10.01 o 1 2 1 320.74 290.57 7.63 o 2 2 1 9634.96 9464.07 58.61 o 3 2 1 153.37 126.02 5.26 o 4 2 1 1127.62 1054.18 22.87 o 5 2 1 98.51 99.89 12.36 o 6 2 1 627.40 643.42 14.05 o 7 2 1 14.22 15.16 6.21 o 8 2 1 2057.77 2108.53 31.39 o 9 2 1 61.19 46.62 7.39 o 10 2 1 645.47 688.86 29.75 o 0 3 1 13961.75 14013.42 116.48 o 1 3 1 4.25 -3.21 5.90 o 2 3 1 133.63 216.48 9.73 o 3 3 1 154.84 175.83 8.58 o 4 3 1 1256.81 1164.56 27.76 o 5 3 1 24.59 23.40 4.47 o 6 3 1 2598.67 2590.04 27.92 o 7 3 1 13.52 11.67 5.01 o 8 3 1 24.12 38.17 6.59 o 9 3 1 132.61 137.67 11.31 o 10 3 1 742.93 734.92 21.22 o 1 4 1 72.01 73.83 10.15 o 2 4 1 4576.06 4430.67 37.54 o 3 4 1 49.22 46.17 13.91 o 4 4 1 832.66 782.59 15.20 o 5 4 1 82.36 76.19 11.73 o 6 4 1 375.12 379.20 11.64 o 7 4 1 0.10 4.49 4.82 o 8 4 1 1682.94 1700.72 41.76 o 9 4 1 37.02 38.52 12.55 o 10 4 1 447.41 401.31 20.46 o 0 5 1 591.55 616.38 22.90 o 1 5 1 16.69 24.67 8.38 o 2 5 1 1619.63 1623.12 26.91 o 3 5 1 3.72 8.79 14.13 o 4 5 1 1621.55 1612.83 25.76 o 5 5 1 0.79 8.01 11.87 o 6 5 1 2439.94 2428.49 34.45 o 7 5 1 0.61 11.46 24.85 o 8 5 1 1.37 13.28 12.05 o 9 5 1 21.89 12.34 13.78 o 1 6 1 7.24 -2.53 12.70 o 2 6 1 1148.18 1176.06 20.59 o 3 6 1 33.85 22.34 10.28 o 4 6 1 1408.28 1456.81 28.06 o 5 6 1 61.17 48.84 27.12 o 6 6 1 149.16 137.05 14.23 o 7 6 1 76.75 59.81 13.50 o 8 6 1 2122.52 2058.81 47.30 o 0 7 1 461.30 491.02 45.18 o 1 7 1 6.45 11.20 36.78 o 2 7 1 517.25 532.60 49.56 o 3 7 1 1.13 -4.80 23.34 o 4 7 1 672.22 665.99 16.26 o 5 7 1 0.09 7.19 6.54 o 6 7 1 1394.26 1290.95 32.17 o 7 7 1 1.07 12.24 14.49 o 1 8 1 17.42 18.04 8.59 o 2 8 1 1382.62 1463.17 29.65 o 3 8 1 6.20 0.99 8.21 o 4 8 1 215.78 188.88 15.25 o 5 8 1 4.05 16.79 12.71 o 0 9 1 1640.67 1444.93 46.15 o 1 9 1 0.04 2.99 9.40 o 0 0 2 9553.97 9493.05 137.03 o 1 0 2 34.29 32.96 2.13 o 2 0 2 519.20 481.59 13.60 o 3 0 2 94.99 84.41 7.53 o 4 0 2 11390.87 11388.49 107.46 o 5 0 2 0.05 -4.15 12.58 o 6 0 2 2318.59 2170.19 43.31 o 7 0 2 38.99 38.90 10.53 o 8 0 2 294.58 319.00 15.31 o 9 0 2 19.74 14.32 6.74 o 10 0 2 1158.82 1182.57 28.80 o 11 0 2 33.53 29.78 13.56 o 1 1 2 16.38 21.91 2.52 o 2 1 2 36880.63 37216.91 316.10 o 3 1 2 231.03 240.16 6.46 o 4 1 2 3641.03 3539.24 29.21 o 5 1 2 1.24 -0.12 8.32 o 6 1 2 1078.35 1126.45 14.56 o 7 1 2 128.68 137.68 17.71 o 8 1 2 2153.94 2220.26 31.16 o 9 1 2 3.66 -1.11 4.97 o 10 1 2 5.92 7.57 7.21 o 11 1 2 1.00 -8.81 8.81 o 0 2 2 3539.15 3357.12 32.80 o 1 2 2 227.91 220.31 5.51 o 2 2 2 199.76 176.07 4.78 o 3 2 2 36.30 45.29 5.52 o 4 2 2 4709.70 4681.83 46.34 o 5 2 2 2.35 0.35 11.24 o 6 2 2 4250.20 4297.28 42.73 o 7 2 2 22.40 19.38 13.30 o 8 2 2 459.80 492.66 11.69 o 9 2 2 62.83 60.19 8.96 o 10 2 2 1325.70 1408.38 40.83 o 1 3 2 0.97 4.33 4.60 o 2 3 2 13981.93 14265.55 86.15 o 3 3 2 246.21 254.03 8.41 o 4 3 2 5804.43 5969.21 48.31 o 5 3 2 6.75 4.10 5.19 o 6 3 2 1202.66 1264.64 23.02 o 7 3 2 45.01 46.48 6.81 o 8 3 2 1939.57 2009.79 30.50 o 9 3 2 463.46 490.92 22.07 o 10 3 2 2.19 9.98 14.02 o 0 4 2 2940.33 2819.13 55.47 o 1 4 2 80.29 80.13 10.56 o 2 4 2 242.56 249.39 9.88 o 3 4 2 26.76 29.83 3.39 o 4 4 2 3475.94 3513.53 32.43 o 5 4 2 0.84 2.39 9.84 o 6 4 2 2773.38 2863.40 31.90 o 7 4 2 9.15 14.75 6.96 o 8 4 2 341.89 360.45 30.82 o 9 4 2 30.51 28.70 12.75 o 10 4 2 975.57 895.29 26.68 o 1 5 2 11.43 3.03 6.61 o 2 5 2 9473.33 9602.30 113.10 o 3 5 2 63.69 56.21 13.11 o 4 5 2 1670.41 1730.44 24.46 o 5 5 2 3.26 6.82 11.15 o 6 5 2 431.60 475.04 28.74 o 7 5 2 77.80 77.63 11.27 o 8 5 2 1095.49 1088.62 33.16 o 9 5 2 8.81 12.92 21.30 o 0 6 2 2676.43 2798.14 64.15 o 1 6 2 7.85 -0.78 7.50 o 2 6 2 193.68 205.22 18.09 o 3 6 2 4.65 2.39 14.34 o 4 6 2 2568.04 2611.50 74.53 o 5 6 2 2.23 3.55 39.26 o 6 6 2 809.29 842.04 24.52 o 7 6 2 12.39 -0.87 20.50 o 8 6 2 97.71 89.80 34.80 o 1 7 2 0.55 -0.20 45.47 o 2 7 2 4611.47 4879.87 145.80 o 3 7 2 33.03 28.51 6.61 o 4 7 2 855.30 882.49 21.32 o 5 7 2 0.51 1.26 7.72 o 6 7 2 278.19 289.13 13.09 o 7 7 2 20.79 21.04 17.02 o 0 8 2 1071.42 1195.24 42.42 o 1 8 2 17.58 7.48 8.07 o 2 8 2 125.61 120.39 13.38 o 3 8 2 5.01 -1.36 9.27 o 4 8 2 710.32 720.26 24.12 o 5 8 2 0.04 31.23 15.71 o 1 0 3 227.03 156.50 4.00 o 2 0 3 930.77 866.18 16.45 o 3 0 3 20.22 31.52 4.83 o 4 0 3 7283.97 7505.71 75.74 o 5 0 3 18.35 6.49 14.26 o 6 0 3 2463.82 2558.07 44.03 o 7 0 3 349.37 328.98 46.02 o 8 0 3 2021.73 2064.70 39.35 o 9 0 3 0.44 1.35 6.46 o 10 0 3 402.80 413.69 23.55 o 11 0 3 182.36 146.27 16.64 o 0 1 3 21716.00 22009.33 259.78 o 1 1 3 15.31 17.55 2.91 o 2 1 3 1597.39 1788.45 14.42 o 3 1 3 159.79 141.87 5.27 o 4 1 3 4418.73 4336.25 34.65 o 5 1 3 482.73 442.47 14.30 o 6 1 3 4234.68 4307.86 41.24 o 7 1 3 0.36 1.94 11.48 o 8 1 3 5.82 -0.51 4.07 o 9 1 3 104.38 101.63 7.06 o 10 1 3 1417.29 1447.96 27.09 o 11 1 3 33.79 29.44 9.13 o 1 2 3 28.40 35.93 2.68 o 2 2 3 3522.81 3299.13 24.32 o 3 2 3 4.14 6.40 6.05 o 4 2 3 2459.72 2462.86 26.09 o 5 2 3 34.28 22.89 6.80 o 6 2 3 882.25 925.43 26.09 o 7 2 3 22.36 20.68 9.68 o 8 2 3 3254.92 3427.55 42.82 o 9 2 3 312.16 301.42 13.82 o 10 2 3 69.02 62.59 10.06 o 0 3 3 2367.51 2175.05 28.73 o 1 3 3 0.20 3.40 4.64 o 2 3 3 1407.69 1469.60 13.45 o 3 3 3 2.11 -1.17 8.65 o 4 3 3 7616.22 7740.86 64.13 o 5 3 3 157.02 148.80 9.25 o 6 3 3 1742.50 1684.03 20.59 o 7 3 3 105.86 90.59 8.16 o 8 3 3 49.20 58.43 6.53 o 9 3 3 170.33 183.76 14.75 o 10 3 3 1165.30 1146.61 25.88 o 1 4 3 3.07 1.04 9.39 o 2 4 3 2023.03 1816.20 19.99 o 3 4 3 0.24 0.94 3.89 o 4 4 3 1939.41 1933.79 23.93 o 5 4 3 3.09 3.65 9.80 o 6 4 3 776.82 790.35 25.71 o 7 4 3 29.33 25.81 5.97 o 8 4 3 2240.10 2170.20 117.32 o 9 4 3 202.45 139.00 18.18 o 10 4 3 71.73 79.23 30.29 o 0 5 3 7184.34 7077.00 85.26 o 1 5 3 22.00 17.48 7.79 o 2 5 3 60.21 71.79 15.36 o 3 5 3 21.83 23.82 16.97 o 4 5 3 1612.86 1615.37 25.97 o 5 5 3 175.38 173.21 18.35 o 6 5 3 2225.87 2256.36 48.43 o 7 5 3 0.02 3.54 10.69 o 8 5 3 0.48 -6.17 10.95 o 9 5 3 61.94 51.03 15.88 o 1 6 3 26.72 18.22 17.49 o 2 6 3 1093.54 1170.15 30.18 o 3 6 3 0.30 -10.34 15.14 o 4 6 3 1583.09 1563.81 26.59 o 5 6 3 0.51 85.02 113.85 o 6 6 3 836.62 844.26 20.54 o 7 6 3 97.46 114.01 24.45 o 8 6 3 809.84 808.02 52.44 o 0 7 3 2964.66 3143.17 220.85 o 1 7 3 12.55 0.56 48.30 o 2 7 3 1.03 6.14 12.17 o 3 7 3 14.13 15.42 6.38 o 4 7 3 1037.71 1102.87 24.11 o 5 7 3 91.47 54.92 12.22 o 6 7 3 1018.71 940.04 27.32 o 7 7 3 0.34 -5.08 11.13 o 1 8 3 0.03 -5.76 7.62 o 2 8 3 701.82 696.15 22.75 o 3 8 3 2.05 5.35 12.38 o 4 8 3 485.61 441.25 25.29 o 5 8 3 1.39 7.21 10.95 o 0 0 4 6480.54 6721.49 88.37 o 1 0 4 101.16 112.24 4.97 o 2 0 4 37986.11 39242.61 421.49 o 3 0 4 9.93 20.12 7.16 o 4 0 4 5607.56 5525.49 75.20 o 5 0 4 62.52 80.61 14.60 o 6 0 4 3625.17 3580.39 51.27 o 7 0 4 119.81 135.69 8.76 o 8 0 4 93.81 103.14 9.07 o 9 0 4 1.30 -6.38 6.38 o 10 0 4 1145.74 1137.71 29.70 o 11 0 4 1.40 25.76 11.44 o 1 1 4 31.04 28.89 3.05 o 2 1 4 6470.13 6209.25 41.98 o 3 1 4 4.89 4.61 3.99 o 4 1 4 2100.51 1950.55 17.39 o 5 1 4 1.59 1.72 12.34 o 6 1 4 573.44 543.26 13.07 o 7 1 4 231.02 238.16 10.55 o 8 1 4 2656.96 2827.58 39.49 o 9 1 4 92.68 85.03 6.11 o 10 1 4 3.57 9.39 6.68 o 11 1 4 35.25 13.23 9.35 o 0 2 4 48154.82 47860.41 569.05 o 1 2 4 127.64 136.67 3.96 o 2 2 4 2706.13 2737.47 22.17 o 3 2 4 0.07 -4.20 6.40 o 4 2 4 1368.42 1298.59 16.64 o 5 2 4 135.77 145.29 8.71 o 6 2 4 3429.47 3510.98 38.06 o 7 2 4 89.12 87.96 7.90 o 8 2 4 68.66 69.29 5.50 o 9 2 4 133.75 129.38 19.57 o 10 2 4 796.44 791.75 23.08 o 1 3 4 446.86 478.80 8.24 o 2 3 4 7847.03 7898.43 54.77 o 3 3 4 2.03 4.46 8.91 o 4 3 4 936.42 842.65 27.54 o 5 3 4 47.28 57.74 8.32 o 6 3 4 643.46 630.97 12.78 o 7 3 4 68.10 59.35 9.96 o 8 3 4 886.10 883.81 16.48 o 9 3 4 30.20 39.76 8.28 o 10 3 4 165.13 116.56 10.18 o 0 4 4 16820.04 17761.71 164.50 o 1 4 4 73.88 78.92 8.35 o 2 4 4 1952.33 1849.36 23.37 o 3 4 4 9.50 6.27 4.82 o 4 4 4 1399.52 1408.70 24.98 o 5 4 4 54.39 57.47 8.40 o 6 4 4 2359.92 2391.54 32.83 o 7 4 4 58.91 35.60 12.64 o 8 4 4 47.66 40.53 6.93 o 9 4 4 101.49 93.39 13.93 o 1 5 4 0.10 -5.10 5.40 o 2 5 4 2842.13 2875.07 32.20 o 3 5 4 13.58 13.72 13.21 o 4 5 4 1217.99 1267.18 18.88 o 5 5 4 1.40 2.60 13.23 o 6 5 4 258.56 259.01 12.12 o 7 5 4 93.27 95.67 10.70 o 8 5 4 1438.73 1527.88 38.93 o 9 5 4 43.11 46.95 28.19 o 0 6 4 2072.50 2236.38 47.22 o 1 6 4 25.12 28.77 22.84 o 2 6 4 4028.51 4184.42 75.19 o 3 6 4 0.70 3.85 5.74 o 4 6 4 1813.52 1924.50 36.49 o 5 6 4 3.63 25.66 122.48 o 6 6 4 1321.49 1339.24 26.72 o 7 6 4 46.42 32.27 12.62 o 8 6 4 37.83 60.97 22.68 o 1 7 4 1.32 2.25 35.39 o 2 7 4 1526.97 1602.09 94.98 o 3 7 4 3.70 -4.59 6.35 o 4 7 4 548.28 625.74 17.70 o 5 7 4 5.57 14.52 7.23 o 6 7 4 137.53 120.73 13.58 o 0 8 4 4555.51 4834.00 127.98 o 1 8 4 24.24 19.69 12.17 o 2 8 4 193.53 157.93 10.07 o 3 8 4 0.08 -4.53 9.04 o 4 8 4 281.61 241.62 14.40 o 1 0 5 1488.68 1303.39 21.46 o 2 0 5 35167.63 35408.90 421.25 o 3 0 5 2071.91 1990.56 25.14 o 4 0 5 122.15 85.49 10.76 o 5 0 5 407.43 452.29 24.61 o 6 0 5 1020.47 1072.97 18.25 o 7 0 5 0.17 11.67 9.19 o 8 0 5 1639.06 1624.22 32.21 o 9 0 5 70.98 55.30 14.06 o 10 0 5 342.94 386.12 18.77 o 11 0 5 53.09 17.25 15.69 o 0 1 5 15549.30 15603.61 210.00 o 1 1 5 323.92 272.51 5.17 o 2 1 5 688.17 637.39 12.04 o 3 1 5 98.92 83.43 6.27 o 4 1 5 3273.74 3225.42 27.25 o 5 1 5 258.73 234.89 22.44 o 6 1 5 2433.29 2384.44 37.67 o 7 1 5 82.76 79.61 10.88 o 8 1 5 83.93 104.15 7.54 o 9 1 5 5.37 1.85 4.91 o 10 1 5 819.20 829.99 23.73 o 1 2 5 12.54 6.33 4.17 o 2 2 5 8521.04 8593.37 62.34 o 3 2 5 785.34 710.81 11.89 o 4 2 5 3645.27 3588.48 43.35 o 5 2 5 47.27 40.25 6.47 o 6 2 5 1600.51 1638.58 20.25 o 7 2 5 415.00 380.52 8.84 o 8 2 5 2618.19 2758.20 36.98 o 9 2 5 7.29 11.34 5.80 o 10 2 5 24.19 20.55 8.61 o 0 3 5 1259.64 974.69 13.40 o 1 3 5 128.92 119.55 8.25 o 2 3 5 4237.01 4620.65 35.89 o 3 3 5 6.74 6.13 7.73 o 4 3 5 2182.33 2179.59 23.15 o 5 3 5 26.59 12.65 7.90 o 6 3 5 3793.94 3873.35 46.28 o 7 3 5 619.89 632.14 26.09 o 8 3 5 268.37 283.14 9.80 o 9 3 5 230.56 214.23 11.50 o 10 3 5 953.94 927.13 23.22 o 1 4 5 20.75 16.36 8.15 o 2 4 5 5964.49 6087.41 48.38 o 3 4 5 489.99 473.98 14.18 o 4 4 5 1831.87 1871.71 27.64 o 5 4 5 5.56 0.91 16.41 o 6 4 5 1133.54 1156.23 19.95 o 7 4 5 279.13 272.66 12.25 o 8 4 5 1876.35 1844.94 31.68 o 9 4 5 1.26 1.08 9.43 o 0 5 5 5892.13 5855.40 93.24 o 1 5 5 122.88 119.77 10.14 o 2 5 5 256.92 249.32 15.99 o 3 5 5 16.82 13.84 9.39 o 4 5 5 1491.06 1452.80 19.64 o 5 5 5 118.90 118.77 7.62 o 6 5 5 1205.03 1238.42 33.13 o 7 5 5 28.86 18.43 7.08 o 8 5 5 31.15 18.15 9.12 o 9 5 5 0.06 -9.78 21.96 o 1 6 5 162.53 167.92 18.71 o 2 6 5 5893.13 6087.15 75.47 o 3 6 5 285.84 248.65 22.30 o 4 6 5 131.47 130.61 13.83 o 5 6 5 110.75 92.45 11.06 o 6 6 5 404.76 414.45 14.42 o 7 6 5 0.42 13.98 9.21 o 8 6 5 683.80 652.82 29.42 o 0 7 5 2335.99 2442.27 70.58 o 1 7 5 58.37 57.01 19.55 o 2 7 5 177.28 168.84 45.66 o 3 7 5 15.37 19.11 11.80 o 4 7 5 930.80 921.28 24.00 o 5 7 5 45.72 19.64 8.90 o 6 7 5 687.99 719.05 34.71 o 1 8 5 1.76 3.01 7.47 o 2 8 5 1278.17 1204.91 40.24 o 3 8 5 90.85 79.90 9.08 o 4 8 5 664.22 647.22 33.62 o 0 0 6 5145.86 5223.72 88.53 o 1 0 6 71.22 56.54 6.18 o 2 0 6 38.72 68.21 7.11 o 3 0 6 937.80 888.73 18.68 o 4 0 6 188.23 147.02 12.88 o 5 0 6 276.73 249.79 28.14 o 6 0 6 5027.13 5178.05 76.65 o 7 0 6 54.81 56.94 13.95 o 8 0 6 57.03 60.89 7.44 o 9 0 6 165.36 149.45 15.03 o 10 0 6 1631.60 1641.43 134.77 o 1 1 6 109.64 113.58 4.23 o 2 1 6 2622.38 2370.15 21.88 o 3 1 6 213.19 185.57 9.95 o 4 1 6 10515.27 11005.50 82.02 o 5 1 6 770.47 814.36 25.33 o 6 1 6 652.81 659.95 16.61 o 7 1 6 21.79 16.38 15.48 o 8 1 6 1967.41 2085.31 29.51 o 9 1 6 22.78 8.27 10.04 o 10 1 6 17.61 9.54 6.79 o 0 2 6 6716.96 6541.14 73.10 o 1 2 6 542.89 510.58 10.18 o 2 2 6 94.41 84.04 5.11 o 3 2 6 0.05 -1.10 8.48 o 4 2 6 3906.51 3732.69 33.87 o 5 2 6 73.80 74.45 5.77 o 6 2 6 781.71 760.87 22.81 o 7 2 6 4.96 6.63 11.24 o 8 2 6 42.40 53.15 5.20 o 9 2 6 20.26 18.66 6.05 o 10 2 6 1109.34 1115.30 22.32 o 1 3 6 258.22 263.97 10.00 o 2 3 6 8772.90 8754.15 64.53 o 3 3 6 487.51 447.23 13.54 o 4 3 6 1723.67 1688.32 23.10 o 5 3 6 2.46 1.32 8.08 o 6 3 6 18.18 18.77 8.38 o 7 3 6 677.72 707.48 18.68 o 8 3 6 1340.80 1370.13 21.12 o 9 3 6 102.02 97.24 8.22 o 10 3 6 77.71 68.35 11.66 o 0 4 6 4336.57 4438.97 58.56 o 1 4 6 167.50 156.94 11.49 o 2 4 6 32.73 29.49 9.00 o 3 4 6 4.39 6.11 4.05 o 4 4 6 2037.96 2078.20 23.42 o 5 4 6 67.44 61.93 6.28 o 6 4 6 717.83 714.57 17.17 o 7 4 6 7.48 7.11 7.36 o 8 4 6 23.96 20.78 6.50 o 9 4 6 22.26 23.33 9.60 o 1 5 6 40.95 38.34 6.20 o 2 5 6 1599.11 1667.96 27.16 o 3 5 6 98.57 124.00 5.39 o 4 5 6 4381.31 4493.70 48.52 o 5 5 6 332.25 339.75 10.47 o 6 5 6 364.45 359.97 11.54 o 7 5 6 0.33 -6.91 7.28 o 8 5 6 987.35 943.58 37.87 o 9 5 6 25.67 32.08 16.98 o 0 6 6 1699.11 1777.78 45.36 o 1 6 6 39.38 43.46 7.08 o 2 6 6 41.91 56.40 16.39 o 3 6 6 76.27 70.62 10.42 o 4 6 6 217.52 238.93 16.69 o 5 6 6 118.53 101.53 7.98 o 6 6 6 1820.65 1808.04 55.07 o 7 6 6 18.40 39.60 12.26 o 1 7 6 24.67 19.10 15.57 o 2 7 6 813.01 883.92 19.47 o 3 7 6 41.94 43.47 8.11 o 4 7 6 2074.56 2004.42 49.01 o 5 7 6 116.55 106.04 13.98 o 6 7 6 143.00 118.42 12.89 o 0 8 6 1254.08 1363.08 41.39 o 1 8 6 65.96 57.66 9.87 o 2 8 6 57.15 26.60 13.48 o 3 8 6 0.89 2.38 8.68 o 4 8 6 647.85 592.32 27.32 o 1 0 7 232.67 196.22 10.35 o 2 0 7 19186.96 19854.05 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7 8 842.66 905.69 25.66 o 3 7 8 85.54 86.69 9.99 o 4 7 8 359.74 351.62 27.93 o 5 7 8 5.56 14.16 20.51 o 6 7 8 54.20 48.82 11.33 o 0 8 8 735.92 685.06 28.95 o 1 8 8 66.36 33.07 8.55 o 2 8 8 601.27 537.84 25.02 o 3 8 8 0.95 18.59 15.02 o 1 0 9 1503.14 1528.96 22.09 o 2 0 9 6465.58 6279.58 70.58 o 3 0 9 112.43 90.47 13.36 o 4 0 9 6778.05 6844.83 99.28 o 5 0 9 5.50 0.21 6.85 o 6 0 9 3660.43 3713.00 67.94 o 7 0 9 683.53 657.59 21.74 o 8 0 9 1461.70 1562.59 34.97 o 9 0 9 18.00 20.42 7.71 o 10 0 9 1.05 -8.31 8.31 o 0 1 9 13580.47 13552.70 149.01 o 1 1 9 218.00 211.47 7.51 o 2 1 9 534.40 459.46 13.63 o 3 1 9 146.14 138.80 10.84 o 4 1 9 2518.51 2527.37 40.12 o 5 1 9 967.06 918.13 15.19 o 6 1 9 1280.00 1300.38 34.94 o 7 1 9 181.86 183.94 14.93 o 8 1 9 79.92 71.20 6.52 o 9 1 9 146.84 114.36 7.24 o 10 1 9 813.43 767.13 19.21 o 1 2 9 532.19 508.88 12.83 o 2 2 9 8083.47 8176.75 68.61 o 3 2 9 746.40 673.25 15.85 o 4 2 9 2186.84 2190.73 25.26 o 5 2 9 363.12 375.92 20.11 o 6 2 9 1145.35 1159.11 16.98 o 7 2 9 127.75 122.59 11.66 o 8 2 9 2212.34 2263.89 31.52 o 9 2 9 82.66 78.36 6.70 o 10 2 9 0.68 0.85 9.09 o 0 3 9 10241.71 10415.70 119.97 o 1 3 9 400.80 384.24 10.60 o 2 3 9 357.09 308.06 24.75 o 3 3 9 136.96 142.11 11.29 o 4 3 9 2074.20 2047.29 24.90 o 5 3 9 1239.67 1186.12 21.79 o 6 3 9 822.64 867.20 30.11 o 7 3 9 6.04 4.51 23.86 o 8 3 9 20.77 17.82 5.08 o 9 3 9 5.77 15.50 7.22 o 1 4 9 478.89 476.58 12.80 o 2 4 9 4793.90 4993.95 46.56 o 3 4 9 409.41 397.64 11.83 o 4 4 9 1723.48 1777.65 22.99 o 5 4 9 266.58 256.45 9.81 o 6 4 9 1024.69 1059.79 21.48 o 7 4 9 107.25 101.66 18.92 o 8 4 9 1578.13 1584.28 33.58 o 9 4 9 49.16 17.53 11.36 o 0 5 9 4635.77 4804.36 68.02 o 1 5 9 168.72 168.70 10.05 o 2 5 9 269.89 308.42 8.14 o 3 5 9 52.17 66.93 6.77 o 4 5 9 1204.23 1278.37 19.55 o 5 5 9 385.15 373.71 10.19 o 6 5 9 743.05 780.35 21.20 o 7 5 9 113.14 92.61 8.48 o 8 5 9 48.83 25.40 14.03 o 1 6 9 234.71 209.49 8.69 o 2 6 9 1881.16 1947.13 28.94 o 3 6 9 42.32 59.05 7.63 o 4 6 9 1876.60 1915.01 30.90 o 5 6 9 3.62 13.03 7.04 o 6 6 9 1292.99 1287.14 73.49 o 7 6 9 306.74 222.41 18.40 o 0 7 9 2509.42 2491.92 74.10 o 1 7 9 75.87 80.78 12.97 o 2 7 9 80.38 91.01 11.19 o 3 7 9 16.96 14.53 7.79 o 4 7 9 728.70 801.99 28.19 o 5 7 9 264.81 247.34 18.25 o 1 8 9 84.22 80.64 13.41 o 2 8 9 1400.20 1183.17 50.93 o 3 8 9 141.24 127.21 13.07 o 0 0 10 2531.04 2387.08 50.25 o 1 0 10 1742.94 1688.56 22.97 o 2 0 10 2030.83 2108.05 53.55 o 3 0 10 457.75 416.42 21.80 o 4 0 10 3256.85 3199.35 56.81 o 5 0 10 80.51 87.87 11.56 o 6 0 10 374.94 399.29 30.74 o 7 0 10 1.24 351.38 190.77 o 8 0 10 26.24 30.51 8.95 o 9 0 10 6.76 19.98 8.04 o 10 0 10 622.44 640.21 34.68 o 1 1 10 60.31 56.19 11.29 o 2 1 10 5042.05 4957.58 41.93 o 3 1 10 1165.59 1114.52 25.65 o 4 1 10 1077.75 1027.38 16.33 o 5 1 10 407.50 402.34 17.61 o 6 1 10 18.20 35.47 9.46 o 7 1 10 105.26 101.76 21.74 o 8 1 10 1212.10 1268.21 20.91 o 9 1 10 78.38 58.70 6.41 o 10 1 10 34.31 38.06 7.21 o 0 2 10 4075.81 3942.01 50.32 o 1 2 10 358.02 323.44 14.01 o 2 2 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9 1 12 135.70 137.65 14.41 o 0 2 12 3305.31 3330.89 66.38 o 1 2 12 431.02 435.32 15.71 o 2 2 12 266.55 249.74 12.95 o 3 2 12 570.04 545.51 12.28 o 4 2 12 680.29 630.63 22.28 o 5 2 12 668.77 623.90 20.83 o 6 2 12 1382.08 1366.17 30.40 o 7 2 12 89.15 90.53 21.59 o 8 2 12 10.38 16.14 5.46 o 9 2 12 52.31 35.30 6.14 o 1 3 12 66.39 56.16 8.86 o 2 3 12 1104.00 1089.10 15.75 o 3 3 12 428.01 415.81 20.14 o 4 3 12 1548.76 1562.07 21.65 o 5 3 12 2.71 2.74 3.39 o 6 3 12 462.66 448.71 26.87 o 7 3 12 461.02 452.80 13.50 o 8 3 12 1286.39 1278.40 24.05 o 9 3 12 145.79 106.96 11.38 o 0 4 12 2544.34 2569.97 42.15 o 1 4 12 310.43 320.01 8.13 o 2 4 12 157.61 158.48 7.43 o 3 4 12 268.51 280.34 10.47 o 4 4 12 549.93 561.77 12.12 o 5 4 12 447.38 433.70 21.59 o 6 4 12 889.50 928.02 22.07 o 7 4 12 69.39 74.76 8.30 o 8 4 12 2.87 0.47 6.58 o 1 5 12 435.67 403.30 10.20 o 2 5 12 1473.65 1525.61 24.01 o 3 5 12 196.48 205.68 8.85 o 4 5 12 580.53 601.29 12.68 o 5 5 12 62.63 56.67 6.86 o 6 5 12 485.60 477.96 15.61 o 7 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