#------------------------------------------------------------------------------ #$Date: 2024-08-09 04:46:27 +0300 (Fri, 09 Aug 2024) $ #$Revision: 294065 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312564.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312564 loop_ _publ_author_name 'Jaconelli, Harry S.' 'Kennedy, Alan R.' _publ_section_title ; Salt forms of amides: protonation of acetanilide. ; _journal_coeditor_code EF3058 _journal_issue 9 _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_paper_doi 10.1107/S2053229624007332 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C8 H10 N1 O1 +, Cl-, C8 H9 N1 O1' _chemical_formula_moiety 'C8 H10 N1 O1 +, Cl-, C8 H9 N1 O1' _chemical_formula_sum 'C16 H19 Cl N2 O2' _chemical_formula_weight 306.78 _chemical_name_systematic ; N-(1-Hydroxyethylidene)anilinium chloride--N-phenylacetamide (1/1) ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 102.2450(10) _cell_angle_gamma 90 _cell_formula_units_Z 6 _cell_length_a 7.79360(10) _cell_length_b 18.3639(2) _cell_length_c 16.39220(10) _cell_measurement_reflns_used 17138 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 71.4480 _cell_measurement_theta_min 3.6420 _cell_volume 2292.69(4) _computing_cell_refinement ; Crysalis PRO (Rigaku OD, 2019) ; _computing_data_collection ; Crysalis PRO (Rigaku OD, 2019) ; _computing_data_reduction ; Crysalis PRO (Rigaku OD, 2019) ; _computing_molecular_graphics ; Mercury (Macrae et al., 2020) ; _computing_publication_material ; SHELXL2018 in WinGX (Farrugia, 2012) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device_type 'Rigaku Synergy-i' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0327 _diffrn_reflns_av_unetI/netI 0.0216 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 23203 _diffrn_reflns_theta_full 70.000 _diffrn_reflns_theta_max 71.561 _diffrn_reflns_theta_min 3.661 _diffrn_source 'microsource tube' _diffrn_standards_decay_% 0 _diffrn_standards_interval_count 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.262 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.72502 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2023) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.333 _exptl_crystal_description fragment _exptl_crystal_F_000 972 _exptl_crystal_size_max 0.20 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.262 _refine_diff_density_min -0.303 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 309 _refine_ls_number_reflns 4444 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.042 _refine_ls_R_factor_all 0.0332 _refine_ls_R_factor_gt 0.0308 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0491P)^2^+0.7515P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0862 _refine_ls_wR_factor_ref 0.0882 _reflns_number_gt 4113 _reflns_number_total 4444 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ef3058.cif _cod_data_source_block ACTHCl _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2312564 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 0 0 -1-1.82707 6.21022 18 0 0 -1 4.55726 7.51834 17 0 0 -1-1.45693 5.09295 14 0 0 -1 3.33048 7.17489 12 0 0 -1 1.43128 8.09575 5 0 0 -1-4.56226 7.21284 1 0 0 -2 440.827 35.4772 12 0 0 -2 453.621 29.2466 14 0 0 -2 505.046 37.3026 1 0 0 -2 435.197 40.9357 5 0 0 2 459.468 37.9187 37 0 0 -2 451.037 36.1653 17 0 0 -2 444.051 32.6232 18 0 0 -3-6.50593 13.8663 14 0 0 -3 3.41298 21.0986 12 0 0 -3 17.4877 21.8713 1 0 0 -3-8.77554 26.8072 5 0 0 3 7.68392 22.3270 37 0 0 -3 8.08904 19.6897 18 0 0 -3 27.4159 25.6429 17 0 0 -4 6264.14 239.758 12 0 0 -4 6222.80 215.259 14 0 0 -4 6411.18 240.638 1 0 0 -4 6036.15 252.925 5 0 0 4 6205.55 246.200 37 0 0 -4 6237.92 224.217 18 0 0 -4 6132.70 236.681 17 0 0 -5 25.9065 18.1301 14 0 0 -5-6.02783 34.0957 12 0 0 -5 7.66831 38.9300 5 0 0 -5-6.13996 35.2090 1 0 0 5 6.65945 30.7562 37 0 0 -5 18.2404 24.3189 18 0 0 -5-11.6528 30.5823 17 0 0 -6 20184.7 635.761 14 0 0 -6 21392.5 686.579 12 0 0 -6 20766.2 709.895 5 0 0 -6 20017.8 682.756 1 0 0 6 20734.7 693.031 37 0 0 -6 20877.8 677.509 17 0 0 -7-18.5030 34.8861 12 0 0 -7-18.5605 33.8835 1 0 0 -7 11.5185 44.7716 5 0 0 7-9.90754 43.8085 37 0 0 -7 33.8913 37.4645 17 0 0 -8 22.1745 34.6763 12 0 0 -8 55.5365 40.5630 1 0 0 -8 27.4074 51.6817 5 0 0 8 23.4614 50.6846 37 0 0 -8 29.7888 36.2641 17 0 0 -9-13.1047 34.9431 12 0 0 -9-26.2180 53.8679 1 0 0 -9 16.0812 50.2804 5 0 0 -9 11.4859 37.5097 17 0 0 -10 279.084 82.6357 5 0 0 -10 351.484 84.3627 1 0 0 -10 107.037 61.6504 12 0 0 -10 293.098 54.0519 34 0 0 -10 385.490 69.1165 8 0 0 -10 336.250 63.4348 9 0 0 -11-34.4013 30.3362 34 0 0 -11 7.69208 25.1198 30 0 0 -11 42.4232 59.9894 5 0 0 -11-8.62674 34.5036 6 0 0 -11 70.1685 52.2953 1 0 0 -11-17.5788 46.8722 12 0 0 -11 7.64657 27.9186 23 0 0 -11-10.3813 47.9444 9 0 0 -11 41.7923 41.7882 8 0 0 -12 2853.47 179.864 34 0 0 -12 2544.65 160.365 30 0 0 -12 2329.75 224.695 1 0 0 -12 2379.48 163.390 6 0 0 -12 2634.13 258.790 5 0 0 -12 2141.23 211.979 12 0 0 -12 2229.40 152.583 23 0 0 -12 2335.74 177.663 8 0 0 -12 2467.64 182.180 9 0 0 -13 19.0191 39.0774 30 0 0 -13 21.7947 50.3284 12 0 0 -13-37.9717 59.6613 8 0 0 -13-12.7174 53.6165 9 0 0 -13-25.8885 59.7816 5 0 0 -13 10.5736 45.6795 6 0 0 -13-27.9450 38.2780 23 0 0 -14 4824.33 286.402 9 0 0 -14 4992.47 289.319 8 0 0 -14 5253.49 274.118 6 0 0 -14 5334.70 263.507 23 0 0 -15-40.4196 52.3747 9 0 0 -15-13.2799 48.4923 8 0 0 -15-56.5523 48.8678 6 0 0 -15 19.6060 38.1110 23 0 0 -16 15859.2 616.582 8 0 0 -16 15602.4 613.183 9 0 0 -16 15533.8 588.026 6 0 0 -16 16470.7 576.829 23 0 0 -17 55.0108 46.3845 8 0 0 -17-11.3251 44.0197 9 0 0 -17 9.66853 44.6526 6 0 0 -17-24.2934 35.8063 23 0 0 -18 19270.0 676.290 9 0 0 -18 19533.3 674.457 8 0 0 -18 20138.1 663.017 6 0 0 -19 27.8178 32.1181 9 0 0 -19-39.6922 31.1821 8 0 0 -19 6.03445 23.4555 6 0 1 0 12.9909 8.18998 19 0 1 0 15.0714 6.17790 16 0 -1 0 12.4215 7.49067 11 0 -1 -1 737.849 35.7919 1 0 1 -1 778.396 36.7614 1 0 1 -1 717.467 39.0060 5 0 -1 -1 712.389 38.3274 5 0 -1 -1 752.958 39.6218 17 0 1 -1 767.987 36.2093 16 0 1 -1 766.136 40.8228 19 0 -1 -1 738.872 38.5432 13 0 -1 -1 757.647 35.4031 12 0 1 -1 818.230 37.0625 12 0 -1 -1 737.081 40.4272 11 0 -1 2 170.741 21.0149 37 0 1 -2 101.534 26.7923 5 0 -1 -2 173.461 28.7600 5 0 -1 -2 154.757 23.2898 1 0 1 -2 200.490 24.8384 1 0 1 -2 150.365 22.9145 18 0 -1 -2 160.298 24.4465 17 0 1 -2 201.247 27.6201 19 0 -1 -2 209.262 24.9332 12 0 1 -2 204.020 25.1840 12 0 -1 -2 172.479 24.2869 13 0 -1 -2 175.494 23.3222 15 0 -1 3 22737.8 679.292 37 0 1 3 23543.8 704.860 37 0 -1 -3 22439.4 697.033 5 0 -1 -3 22014.9 683.626 1 0 1 -3 21684.7 696.136 5 0 1 -3 21110.3 681.508 1 0 -1 -3 24345.4 692.186 17 0 1 -3 23684.2 681.937 18 0 1 -3 21862.8 682.093 12 0 1 -3 22594.5 665.334 14 0 -1 -3 23890.5 685.081 13 0 -1 -3 24479.6 687.495 12 0 -1 -3 24314.2 670.225 14 0 -1 4 3402.83 151.486 37 0 1 4 3446.92 169.421 37 0 1 -4 3522.24 158.855 1 0 -1 -4 3471.13 155.588 1 0 -1 -4 3244.40 165.987 5 0 1 -4 3111.61 164.475 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10.3379 37 0 -2 -2 20.2127 17.2100 1 0 -2 -2 13.9280 18.2029 5 0 2 -2 6.90560 13.7366 1 0 2 -2-2.89944 18.7479 5 0 -2 -2 35.6980 20.2313 17 0 2 -2 30.0832 15.4366 16 0 2 -2 12.6748 19.1361 19 0 -2 -2 41.0553 19.8276 15 0 2 -3 1034.97 65.8330 12 0 -2 -3 848.670 64.1512 13 0 -2 -3 1014.54 65.8499 12 0 -2 3 980.788 56.8261 37 0 2 -3 977.219 65.6662 1 0 -2 -3 1063.44 74.7518 5 0 2 -3 730.534 67.5646 5 0 -2 -3 971.427 64.8903 1 0 -2 -3 952.063 69.9989 17 0 2 -3 1055.90 72.8481 19 0 2 -3 977.153 60.4424 16 0 2 -3 946.477 68.1275 18 0 -2 -3 974.470 67.6178 15 0 -2 -4 897.127 70.6346 12 0 -2 -4 966.840 64.8521 14 0 2 -4 1038.67 75.4208 12 0 -2 -4 1030.29 75.5773 13 0 -2 4 872.440 65.2996 37 0 2 4 917.626 90.3573 37 0 2 -4 853.987 81.4566 5 0 -2 -4 908.567 80.0263 5 0 2 -4 838.761 71.8151 1 0 -2 -4 954.933 74.2022 1 0 2 -4 1002.47 64.8756 16 0 2 -4 1072.95 77.5526 18 0 -2 -4 1013.65 79.7988 17 0 -2 -5 228.844 37.9836 14 0 2 -5 195.559 43.8546 12 0 -2 -5 189.405 42.4974 12 0 2 5 212.065 53.3386 37 0 -2 -5 138.713 38.5485 1 0 2 -5 226.850 45.4882 1 0 -2 -5 157.345 48.2325 5 0 2 -5 199.173 51.8761 5 0 -2 -5 232.035 48.1707 17 0 2 -5 220.660 34.6350 16 0 2 -5 253.694 44.4704 18 0 2 -6 134413. 3528.29 12 0 -2 -6 125528. 3516.65 12 0 -2 -6 126515. 3481.08 14 0 2 6 125457. 3560.49 37 0 2 -6 118131. 3543.67 5 0 -2 -6 119672. 3543.06 5 0 -2 -6 120246. 3512.61 1 0 2 -6 124170. 3519.26 1 0 2 -6 124696. 3496.43 18 0 2 -6 119693. 3506.68 17 0 -2 -6 125272. 3521.28 17 0 2 -6 122531. 3472.92 16 0 2 -7 27.8875 32.8328 12 0 -2 -7 63.4006 35.2451 12 0 2 7 96.3589 49.5235 37 0 -2 -7 136.965 46.3860 1 0 2 -7 37.0619 41.9241 1 0 2 -7 57.6232 44.8270 5 0 -2 -7 56.5484 43.9921 5 0 2 -7 33.8252 36.5707 17 0 -2 -7 109.397 47.8800 17 0 -2 -8 10.8589 40.9472 12 0 2 -8-33.3836 43.2530 12 0 2 8 56.1995 54.6107 37 0 -2 -8-21.8581 39.9032 1 0 -2 -8 13.4569 42.0747 5 0 2 -8 11.0809 36.1866 1 0 2 -8 41.0943 50.0134 5 0 -2 -8 31.6425 38.5102 17 0 -2 -9 64.2035 45.3065 12 0 2 -9 105.100 47.9790 12 0 2 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0 -10 -6 14392.6 500.114 32 0 -10 -6 12624.1 489.177 35 0 10 -6 14414.0 623.218 19 0 10 -6 15031.3 578.176 16 0 -10 -7 2994.12 241.425 13 0 -10 -7 3433.91 192.697 32 0 -10 -7 3560.20 197.665 35 0 -10 -8 2520.82 163.528 35 0 -10 -8 2708.79 228.992 13 0 -10 -8 2621.03 162.646 21 0 10 -8 2400.72 200.631 16 0 10 9 1605.71 208.164 37 0 -10 -9 1421.05 125.322 35 0 10 -9 1406.82 156.347 16 0 -10 -9 1282.37 116.903 26 0 -10 -9 1268.86 115.182 25 0 10 9 1366.22 136.058 27 0 -10 -10 1850.02 147.376 35 0 10 10 1658.10 222.829 37 0 -10 -10 1660.17 134.728 30 0 -10 -10 1793.01 144.212 25 0 -10 -10 1902.50 147.826 26 0 10 -11 2925.17 209.681 34 0 -10 -11 3440.93 211.154 35 0 10 -11 3349.61 209.671 33 0 -10 -11 3326.54 199.996 30 0 -10 -11 3023.01 197.362 25 0 10 -12 5185.05 292.660 34 0 10 -12 5626.02 289.470 33 0 -10 -12 5292.80 280.065 35 0 -10 -12 5804.84 282.765 30 0 -10 -12 5762.41 289.108 25 0 10 -13 427.915 82.2742 34 0 10 -13 395.099 75.4163 33 0 -10 -13 322.752 62.7656 30 0 10 -13 387.834 69.9905 24 0 -10 -13 459.096 76.9365 25 0 10 -14 3461.73 204.546 33 0 10 -14 3407.53 215.604 34 0 -10 -14 3635.85 201.847 30 0 -10 -14 3305.87 200.995 25 0 10 -14 3402.29 201.124 24 0 10 -15 3757.13 212.054 34 0 10 -15 3545.61 196.765 33 0 -10 -15 3275.21 184.762 30 0 10 -15 3205.30 190.491 24 0 -10 -15 3707.25 200.396 25 0 10 -16 211.573 46.2400 33 0 10 -16 127.734 45.3381 34 0 -10 -16 96.6730 36.1724 30 0 10 -16 189.582 45.0775 24 0 10 -17 693.138 65.0915 33 0 10 -17 538.534 60.3945 24 0 11 0 32.6052 30.7394 16 0 11 0-14.8058 46.2936 19 0 11 -1 1474.09 157.732 19 0 11 -1 1491.93 134.057 16 0 11 1 1399.74 147.720 19 0 -11 -1 1757.48 146.150 13 0 11 -2 1670.63 147.409 16 0 11 -2 1888.13 174.942 19 0 -11 -2 1735.16 151.279 13 0 11 -3 4167.78 254.573 16 0 11 -3 4720.13 298.359 19 0 -11 -3 4518.03 217.696 32 0 -11 -3 5004.68 279.621 13 0 -11 -4 2642.26 160.066 32 0 -11 -4 2749.02 159.847 35 0 11 -4 2896.55 231.764 19 0 11 -4 2816.61 205.311 16 0 -11 -4 2731.91 207.198 13 0 -11 -5 491.887 70.4588 32 0 -11 -5 549.006 71.8887 35 0 11 -5 524.014 92.5424 16 0 11 -5 460.705 94.5432 19 0 -11 -5 439.135 89.7525 13 0 -11 -6 1857.99 139.044 32 0 -11 -6 2033.48 143.950 35 0 11 -6 2117.10 184.688 16 0 11 -6 2124.58 214.828 19 0 -11 -6 2154.54 197.267 13 0 -11 -7 835.839 95.2348 32 0 -11 -7 813.683 127.481 13 0 -11 -7 741.030 91.3515 35 0 11 -7 701.116 113.394 16 0 -11 -8 3851.37 221.928 35 0 11 8 4086.34 245.772 27 0 -11 -8 3625.96 285.030 13 0 -11 -8 4275.30 226.379 21 0 11 -8 3857.96 273.537 16 0 -11 -9 86859.3 2473.05 35 0 -11 -9 81804.4 2451.49 21 0 11 9 84311.5 2499.40 27 0 -11 -9 83155.3 2456.65 25 0 11 -9 83754.8 2577.71 16 0 11 -10 4185.68 228.382 24 0 -11 -10 3960.75 224.015 25 0 -11 -10 3501.00 218.506 35 0 11 -11 2263.54 161.356 24 0 -11 -11 1868.75 150.147 25 0 11 -11 1668.70 156.546 34 0 -11 -11 1868.72 153.507 35 0 -11 -12 3864.76 223.789 25 0 11 -12 4034.37 226.383 24 0 -11 -12 3822.25 224.755 35 0 11 -12 3601.50 232.213 34 0 -11 -13 159.210 54.7776 25 0 11 -13 128.505 44.7889 24 0 -11 -13 55.1483 36.8807 30 0 11 -13 155.385 52.6758 33 0 -11 -13 108.662 43.7797 35 0 11 -13 92.1754 55.4639 34 0 -11 -14 3183.16 189.299 25 0 11 -14 3489.06 194.253 24 0 -11 -14 3009.39 178.327 30 0 11 -14 2833.52 191.738 34 0 11 -14 3427.50 193.131 33 0 11 -15 916.436 89.8439 33 0 11 -15 867.312 96.5575 34 0 11 -15 817.722 88.1039 24 0 -11 -15 1064.42 96.2261 25 0 11 -16 76.6603 33.8648 33 0 11 -16 28.0069 32.3885 34 0 11 -16 98.9774 33.0403 24 0 11 -17 488.950 51.1827 24 0 12 0 14264.6 598.890 19 0 12 0 13189.0 496.635 22 0 -12 -1 1768.41 124.760 32 0 12 -1 1829.51 134.882 22 0 12 1 2027.27 145.065 22 0 12 -1 1662.86 173.811 19 0 12 -1 1568.32 148.796 16 0 -12 -2 82.3910 41.0531 13 0 -12 -2 131.777 38.7915 32 0 12 -2 87.4602 42.9539 22 0 12 2 118.316 47.8707 22 0 12 -2 104.174 51.8517 19 0 12 -2 172.374 53.1232 16 0 -12 -3 19671.9 732.284 13 0 -12 -3 18601.8 637.766 32 0 12 3 18320.5 652.858 22 0 12 -3 18573.5 764.170 19 0 12 -3 19175.6 718.171 16 0 -12 -4 506.882 95.7239 13 0 -12 -4 635.292 78.7670 32 0 12 4 558.167 77.7825 22 0 12 -4 531.633 95.7028 16 0 12 -4 611.892 123.253 19 0 -12 -5 2428.97 164.313 32 0 -12 -5 2715.10 167.782 35 0 12 -5 2432.37 204.838 16 0 12 -5 2430.52 230.744 19 0 -12 -5 2515.83 214.808 13 0 -12 -6 970.477 101.132 32 0 -12 -6 830.938 130.450 13 0 -12 -6 923.790 97.8647 35 0 12 -6 1078.30 139.594 16 0 12 -6 863.389 140.358 19 0 -12 -7 2996.34 193.302 32 0 -12 -7 3354.29 268.744 13 0 12 7 3282.31 215.440 27 0 -12 -7 3579.77 207.737 35 0 12 -7 3514.64 260.142 16 0 -12 -8 285.339 64.0995 35 0 -12 -8 287.613 64.5377 32 0 12 8 214.207 68.5245 27 0 -12 -8 125.104 62.4733 13 0 -12 -8 170.824 56.3914 21 0 12 -8 415.489 95.0252 16 0 -12 -9 46399.8 1429.59 35 0 -12 -9 45029.3 1416.68 21 0 12 -9 45741.6 1536.45 16 0 -12 -9 45572.7 1416.19 25 0 12 9 46295.4 1458.05 27 0 -12 -10 4410.90 250.355 35 0 12 -10 4717.88 245.422 24 0 -12 -10 4511.16 247.037 25 0 12 10 4700.83 272.448 27 0 12 -11 5497.99 269.072 24 0 -12 -11 5479.12 272.474 25 0 -12 -12 12837.3 506.063 35 0 12 -12 12096.2 516.297 34 0 -12 -12 12984.6 501.475 25 0 12 -13 3330.63 210.306 34 0 -12 -13 3305.44 199.755 35 0 -12 -13 3182.75 192.864 25 0 12 -13 3641.10 200.483 24 0 12 -14 66.2954 42.8929 34 0 12 -14 80.7485 43.1357 24 0 -12 -14 138.168 47.2991 25 0 12 -15 93.5194 39.6195 34 0 -12 -15 80.8042 34.2490 25 0 12 -15 60.9396 33.2342 24 0 12 -16 427.480 57.3516 34 0 12 -16 560.893 59.5882 24 0 13 0 29.7937 35.0401 22 0 -13 -1 41.4632 34.0961 32 0 13 -1 28.3320 32.7325 16 0 13 -1 55.5684 62.9698 19 0 13 -1 39.3471 34.7170 22 0 13 1 70.2582 44.3957 22 0 -13 -2 2746.05 171.598 32 0 13 2 2995.40 188.304 22 0 13 -2 2662.28 177.381 22 0 13 -2 2715.01 234.847 19 0 13 -2 2763.08 213.871 16 0 -13 -3 193.651 64.7207 13 0 -13 -3 180.883 54.1350 32 0 13 3 123.468 49.6891 22 0 13 -3 217.370 65.6331 16 0 13 -3 198.408 72.5986 19 0 -13 -4 757.980 117.314 13 0 -13 -4 566.437 81.0509 32 0 13 4 698.171 94.3428 22 0 13 -4 640.524 106.485 16 0 13 -4 625.870 117.686 19 0 -13 -5 10583.5 426.821 32 0 -13 -5 9942.28 503.379 13 0 -13 -5 10271.7 416.639 35 0 13 -5 10393.8 545.311 19 0 13 -5 11233.2 512.434 16 0 -13 -6 61391.2 1854.14 32 0 -13 -6 59976.9 1986.01 13 0 13 6 62520.2 1892.04 27 0 -13 -6 61544.6 1850.86 35 0 13 -6 63191.0 1977.40 16 0 -13 -7 297.536 67.7903 32 0 -13 -7 330.537 89.6916 13 0 13 7 357.819 83.9414 27 0 -13 -7 338.001 68.1222 35 0 13 -7 315.922 93.1311 16 0 -13 -8 19564.9 708.923 35 0 -13 -8 19541.0 706.706 32 0 -13 -8 20191.4 842.431 13 0 13 8 20133.2 740.393 27 0 -13 -8 20382.9 710.600 21 0 13 -8 21105.2 823.028 16 0 13 9 223.337 71.3720 27 0 -13 -9 182.949 56.1578 25 0 -13 -9 203.048 66.3070 32 0 -13 -9 290.554 74.7097 35 0 -13 -9 178.526 57.1539 21 0 13 10 192.580 74.9762 27 0 -13 -10 324.755 64.6052 25 0 -13 -10 311.679 70.7830 35 0 -13 -10 246.581 58.5845 21 0 13 -11 1365.07 135.920 34 0 -13 -11 1589.37 138.313 35 0 13 11 1147.57 126.701 27 0 -13 -11 1435.83 126.196 25 0 13 -11 1341.65 119.187 24 0 -13 -12 983.914 106.911 35 0 13 -12 1075.82 119.302 34 0 -13 -12 1242.97 112.801 25 0 13 -12 1086.19 105.741 24 0 13 -13 938.722 103.618 34 0 -13 -13 941.638 93.4627 25 0 13 -13 958.347 93.5970 24 0 13 -14 16.5920 33.2017 34 0 -13 -14 56.2474 33.8178 25 0 13 -14 56.2182 31.7931 24 0 13 -15 792.682 79.3550 34 0 13 -15 1033.44 83.7675 24 0 13 -16 158.534 33.4223 24 0 14 0 142.595 51.8493 22 0 -14 -1 1925.56 139.890 32 0 14 -1 1799.73 146.221 22 0 -14 -2 515.893 73.8624 32 0 14 2 357.726 74.4592 22 0 14 -2 406.712 74.8307 22 0 14 -2 311.041 88.0046 19 0 14 -2 244.449 72.7646 16 0 -14 -3 396.844 69.2850 32 0 14 3 281.315 70.1113 22 0 14 -3 301.965 91.3547 19 0 14 -3 239.332 77.7843 16 0 14 3 366.992 77.7057 27 0 -14 -4 71.9163 43.3556 32 0 14 4 120.477 60.1288 27 0 14 4 11.2986 53.2907 22 0 14 -4 107.029 58.2845 16 0 14 -4 134.345 70.0340 19 0 -14 -5 10408.2 421.370 32 0 -14 -5 9810.29 502.638 13 0 14 5 9542.84 432.724 27 0 14 5 10093.7 426.603 22 0 14 -5 9773.29 494.223 16 0 14 -5 9501.18 534.488 19 0 -14 -6 101095. 2910.01 32 0 -14 -6 91903.4 3034.38 13 0 14 6 100978. 2942.08 27 0 -14 -6 100585. 2902.85 35 0 14 -6 101917. 3041.33 16 0 14 7 17325.7 673.483 27 0 -14 -7 17848.6 646.640 32 0 -14 -7 17766.7 645.164 35 0 14 8 79.7669 53.2011 27 0 -14 -8 33.2307 44.3373 32 0 -14 -8 73.9144 44.5511 21 0 -14 -8 77.7932 54.4663 35 0 -14 -9 4773.34 243.556 25 0 14 9 3852.33 254.377 27 0 -14 -9 4176.83 240.166 32 0 -14 -9 4506.64 250.229 35 0 -14 -9 4703.48 249.357 21 0 -14 -10 1774.08 138.380 25 0 14 10 1545.41 153.896 27 0 -14 -10 1870.87 149.723 35 0 -14 -10 1590.16 136.254 21 0 -14 -11 5903.16 282.996 35 0 14 -11 5308.61 282.406 34 0 14 11 5448.30 285.677 27 0 -14 -11 5262.01 260.464 25 0 14 -12 12156.9 486.138 34 0 -14 -12 12929.7 480.600 35 0 -14 -12 13019.2 468.085 25 0 14 -12 12293.4 456.702 24 0 14 -13 1088.30 104.002 34 0 14 -13 1140.50 96.0877 24 0 -14 -13 1124.16 96.6987 25 0 14 -14 737.232 79.0201 34 0 -14 -14 713.423 69.0539 25 0 14 -14 676.879 68.3396 24 0 14 -15 1055.55 82.7481 34 0 14 -15 1272.23 82.8046 24 0 15 0 23.7237 46.1104 22 0 15 -1 923.481 112.845 22 0 15 1 982.992 115.009 22 0 -15 -1 1012.50 105.508 32 0 15 -2 1009.94 114.292 22 0 15 2 1217.75 127.066 22 0 -15 -2 887.564 104.406 32 0 15 3 3629.64 233.461 27 0 -15 -3 4273.78 235.028 32 0 15 3 4015.14 242.404 22 0 15 -3 3708.52 276.921 16 0 15 -3 4250.32 322.612 19 0 15 4 1235.60 131.434 27 0 -15 -4 984.568 111.558 32 0 15 4 910.420 116.185 22 0 15 -4 890.312 135.223 16 0 15 5 1850.98 164.722 27 0 15 5 1874.17 158.956 22 0 -15 -5 1937.19 156.206 32 0 15 6 132.984 66.4247 27 0 -15 -6 159.045 59.2327 35 0 -15 -6 90.7710 53.5904 32 0 15 7 894.861 120.048 27 0 -15 -7 922.958 107.564 35 0 -15 -7 1105.50 113.989 21 0 -15 -7 1171.92 121.069 32 0 15 8 1367.75 142.346 27 0 -15 -8 1154.07 122.286 35 0 -15 -8 1265.19 120.519 21 0 -15 -8 1022.51 113.900 32 0 15 9 1224.27 134.574 27 0 -15 -9 1269.24 124.654 35 0 -15 -9 1106.40 112.799 21 0 -15 -9 1035.16 109.360 32 0 -15 -10 2165.88 150.908 25 0 15 10 2146.88 172.799 27 0 -15 -10 2484.04 170.716 35 0 -15 -10 2392.53 161.057 21 0 15 -11 875.496 100.173 34 0 15 11 1013.91 109.739 27 0 -15 -11 813.939 85.5524 25 0 15 -12 15444.5 562.483 34 0 -15 -12 16093.1 541.792 25 0 15 -13 233.307 51.3943 34 0 -15 -13 244.418 41.2130 25 0 15 -14 3831.78 178.985 34 0 16 0 46144.8 1460.70 22 0 16 -1 4976.45 279.015 22 0 16 1 5101.37 285.154 22 0 -16 -2 1200.82 120.313 32 0 16 2 1326.48 136.411 22 0 16 -2 1228.17 127.770 22 0 16 3 1139.78 126.350 27 0 -16 -3 1277.61 125.005 32 0 16 3 1304.88 134.446 22 0 16 4 191.389 64.0222 27 0 16 4 184.925 61.8855 22 0 16 5 6530.88 337.704 27 0 -16 -5 6702.51 324.085 32 0 16 5 6292.41 322.933 22 0 16 6 197.901 71.7338 27 0 -16 -6 261.857 63.8175 32 0 16 7 299.903 79.3292 27 0 -16 -7 456.680 76.4343 35 0 -16 -7 398.961 75.3532 21 0 -16 -7 299.466 69.2751 32 0 16 8 1145.06 130.144 27 0 -16 -8 1359.83 123.494 35 0 -16 -8 1102.37 111.362 21 0 -16 -8 1122.34 117.005 32 0 16 9 436.381 85.7742 27 0 -16 -9 666.914 88.2909 35 0 -16 -9 625.190 86.9790 32 0 -16 -9 377.936 65.3074 21 0 16 10 4663.25 251.631 27 0 -16 -10 4786.69 231.573 21 0 -16 -10 4235.94 224.320 32 0 16 11 249.040 58.2005 27 0 16 -11 313.867 63.0761 34 0 -16 -11 292.332 51.3398 21 0 16 -12 2467.34 150.614 34 0 16 12 2608.31 156.260 27 0 16 -13 711.275 70.7136 34 0 17 0-37.7618 45.9691 22 0 17 1 12.7456 49.5486 22 0 17 -1 61.5045 50.5541 22 0 -17 -2 2472.38 178.748 32 0 17 -2 2764.90 193.561 22 0 17 2 2779.41 201.672 22 0 -17 -3 1902.97 156.678 32 0 17 3 2291.26 180.260 22 0 17 4 1324.12 139.049 27 0 -17 -4 1712.07 145.422 32 0 17 4 1428.94 139.777 22 0 17 5 5040.23 286.437 27 0 -17 -5 5513.33 281.122 32 0 17 5 4849.95 272.720 22 0 17 6 7124.90 353.415 27 0 -17 -6 7131.31 337.383 32 0 -17 -6 7421.14 332.550 21 0 17 7 330.070 75.0773 27 0 -17 -7 251.518 67.4410 32 0 -17 -7 268.107 63.0042 21 0 17 8 5691.51 294.676 27 0 -17 -8 5534.82 274.474 32 0 -17 -8 5738.28 271.953 21 0 17 9 815.829 101.107 27 0 -17 -9 957.563 97.1113 32 0 -17 -9 621.630 79.9458 21 0 17 10 1688.30 135.288 27 0 -17 -10 1612.23 117.192 21 0 -17 -10 1692.33 120.348 32 0 17 11 288.270 55.7534 27 0 17 -11 223.987 49.9253 34 0 -17 -11 169.989 37.9234 21 0 17 -12 9041.20 338.716 34 0 17 12 9480.45 342.760 27 0 18 0 145.661 61.7515 22 0 18 -1 1852.83 155.325 22 0 18 1 1600.49 149.294 22 0 -18 -2 3260.62 202.960 32 0 18 -2 3503.66 217.189 22 0 18 2 3182.47 215.213 22 0 -18 -3 2536.29 177.402 32 0 18 3 2543.15 188.557 22 0 18 4 319.195 74.9943 27 0 -18 -4 351.252 69.3738 32 0 18 4 312.000 69.4786 22 0 18 5 4499.04 255.089 27 0 -18 -5 4132.27 238.631 32 0 18 5 4888.74 256.267 22 0 -18 -6 1027.26 109.684 32 0 18 6 990.583 114.416 27 0 -18 -7 2783.30 177.300 32 0 18 7 2785.95 188.429 27 0 18 8 670.073 89.9773 27 0 -18 -8 756.827 85.0732 32 0 -18 -8 762.213 84.8856 21 0 18 9 45.4461 42.0092 27 0 -18 -9 103.889 37.5433 21 0 -18 -9 30.1414 36.2591 32 0 18 10 310.553 57.5645 27 0 18 -10 263.407 50.2263 34 0 -18 -10 174.118 38.8957 21 0 -18 -10 314.930 52.5073 32 0 18 -11 2412.95 132.279 34 0 18 11 2255.00 133.513 27 0 19 0 11.0876 46.7458 22 0 19 1 878.964 108.253 22 0 19 -1 998.295 108.725 22 0 19 -2 4806.79 252.121 22 0 19 2 4429.20 255.304 22 0 -19 -3 5242.93 263.478 32 0 19 3 5230.80 277.372 22 0 -19 -4 2894.33 186.045 32 0 19 4 3345.28 204.659 22 0 19 5 2378.62 166.901 27 0 -19 -5 2446.50 165.062 32 0 19 5 2633.67 170.219 22 0 19 6-9.74136 49.4556 27 0 -19 -6-8.73698 43.5855 32 0 -19 -6 95.1949 39.5747 21 0 19 7 9.23152 36.9271 27 0 -19 -7 16.1222 37.2335 32 0 -19 -7 36.5226 33.7399 21 0 19 8 994.334 97.4371 27 0 -19 -8 1066.68 91.8168 32 0 19 9 220.455 50.2151 27 0 19 -9 206.192 45.7421 34 0 -19 -9 231.654 42.2300 21 0 -19 -9 120.559 37.1795 32 0 19 10 499.221 59.4872 27 0 19 -10 499.344 56.2001 34 0 -19 -10 421.490 48.5911 21 0 20 0 3802.46 213.973 22 0 20 -1 3726.88 208.501 22 0 20 1 3718.34 213.275 22 0 20 -2 1677.96 130.987 22 0 20 2 1936.57 146.841 22 0 20 3 93.6853 46.8195 22 0 -20 -3 97.8128 38.9533 21 0 -20 -3 120.060 44.7295 32 0 20 4 8.79053 37.0656 22 0 -20 -4 29.3178 31.6697 21 0 -20 -4 31.7421 34.2876 32 0 20 5 2324.70 148.341 22 0 -20 -5 2169.74 142.303 32 0 20 6 2096.21 140.952 27 0 -20 -6 2112.10 134.877 32 0 20 7 1429.13 109.938 27 0 -20 -7 1418.17 103.401 32 0 -20 -8 159.019 37.2446 21 0 20 8 180.947 44.2320 27 0 -20 -8 241.151 46.2106 32 0 -20 -9 398.538 43.5934 21 0 20 9 576.737 60.3531 27 0 21 0 7.68685 31.5874 22 0 -21 -1 622.101 69.6195 21 0 21 1 683.506 82.4844 22 0 21 2 3165.77 177.336 22 0 -21 -3 462.547 59.7860 21 0 21 3 600.597 74.5565 22 0 21 4 2101.69 131.689 22 0 -21 -4 1761.51 116.459 32 0 -21 -5 117.772 35.8990 21 0 21 5 158.044 42.2910 22 0 -21 -5 161.366 40.4813 32 0 -21 -6 2930.77 146.902 32 0 22 0 2273.14 128.191 22 0 22 1 1572.91 104.626 22 0 22 -1 1489.14 98.9524 22 0 22 2 1598.63 106.144 22 0 -22 -3 74.2733 26.2400 21 0 22 3 158.384 38.2831 22 0 -22 -4 550.124 52.9826 21 0 22 4 1151.63 77.6420 22 1 0 -20 13.6015 20.9421 6 1 0 -19 793.978 85.9087 9 1 0 -19 917.027 88.4432 8 1 0 -19 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37 1 3 -10 2389.15 147.722 34 1 3 -10 2088.13 154.033 33 1 3 -10 2329.75 156.103 9 1 -3 -10 2600.42 161.475 9 1 -3 -10 2669.83 207.636 17 1 3 -9 38932.6 1247.59 12 1 -3 -9 39046.1 1242.30 12 1 -3 -9 38047.9 1204.18 14 -1 3 9 38551.6 1311.80 37 1 -3 -9 39704.8 1294.86 5 1 -3 -9 38577.8 1245.82 1 1 3 -9 35823.6 1275.31 5 1 3 -9 40237.5 1254.58 1 1 3 -9 36941.9 1251.41 17 1 3 -9 37784.5 1234.59 18 1 3 -9 37293.1 1192.35 16 1 -3 -9 39091.1 1261.25 17 1 3 -8 829.499 96.5587 12 1 -3 -8 586.795 82.3586 12 1 -3 -8 713.717 83.9264 14 -1 3 8 769.049 116.248 37 1 -3 -8 732.783 91.0866 1 1 -3 -8 676.117 101.856 5 1 3 -8 676.684 103.118 5 1 3 -8 669.433 91.9767 1 1 -3 -8 689.628 96.7642 17 1 3 -8 805.329 96.9300 18 1 3 -8 725.733 80.6457 16 1 -3 -7 2217.66 142.130 14 1 3 -7 2041.79 145.327 12 1 -3 -7 2404.09 152.877 12 -1 3 7 1933.50 171.127 37 1 3 -7 2009.17 161.076 5 1 -3 -7 1921.99 158.101 5 1 3 -7 2049.81 148.441 1 1 -3 -7 1934.45 142.854 1 1 3 -7 2145.20 153.757 18 1 -3 -7 2122.92 157.386 17 1 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15 1 -3 -1 513.010 56.4143 15 1 -3 0 880.324 45.2274 13 -1 -3 0 837.013 64.9591 11 -1 3 0 867.383 55.4953 37 -1 3 0 798.493 52.7901 4 -1 -3 0 776.570 50.9355 2 -1 3 0 891.007 54.6332 2 -1 3 0 893.821 55.0882 3 -1 -3 0 788.561 53.0729 4 -1 -3 0 799.366 52.7313 3 -1 3 0 760.101 58.3581 16 1 -3 0 861.762 43.8559 17 1 3 0 822.310 50.6514 19 -1 -3 0 899.784 39.7008 15 -1 3 0 698.688 67.4708 19 1 -3 0 953.713 78.4917 15 1 3 0 893.264 47.8073 16 -1 -3 -1 3805.64 142.411 5 -1 3 -1 3679.94 141.916 2 -1 3 -1 3395.48 140.502 5 -1 3 -1 3836.96 146.618 4 -1 -3 -1 3447.90 143.958 4 -1 -3 -1 3314.61 140.321 2 -1 3 -1 3503.99 140.319 12 1 -3 1 3544.42 117.074 13 -1 -3 -1 3530.99 152.407 13 -1 -3 -1 3361.82 137.457 12 -1 -3 -1 3540.97 159.384 11 -1 3 -1 3420.57 147.236 16 1 3 1 3780.34 129.872 19 -1 3 -1 3490.13 164.056 19 -1 -3 -1 3642.61 126.628 15 1 -3 1 4357.35 179.733 15 1 3 1 3817.40 122.439 16 -1 -3 -2 9323.29 324.211 4 -1 -3 -2 9692.65 320.898 2 -1 -3 -2 9357.38 319.407 5 -1 3 -2 9497.81 323.601 5 -1 3 -2 9375.56 318.822 2 -1 3 -2 9333.28 323.812 4 -1 -3 -2 9111.45 312.447 12 -1 -3 -2 9205.28 331.552 11 -1 3 -2 10356.9 322.695 12 -1 -3 -2 9799.22 326.177 13 -1 3 -2 9667.60 321.789 16 -1 3 -2 9555.45 335.995 19 -1 3 -3 37411.6 1138.39 4 -1 -3 -3 38499.1 1140.65 4 -1 3 -3 38890.3 1141.90 5 -1 -3 -3 37623.9 1131.83 2 -1 -3 -3 38461.0 1138.55 5 -1 3 -3 36984.9 1128.03 12 -1 -3 -3 37706.4 1130.41 13 -1 -3 -3 37104.9 1138.61 11 -1 -3 -3 41396.0 1131.87 12 -1 3 -3 37274.2 1121.43 16 -1 3 -3 37885.9 1139.94 19 -1 -3 -3 38477.1 1135.08 17 -1 -3 -4 2037.07 129.541 5 -1 -3 -4 1999.64 129.534 4 -1 3 -4 1931.54 126.301 4 -1 -3 -4 1767.08 118.827 2 -1 3 -4 1970.85 129.990 5 -1 3 -4 2316.32 134.167 2 -1 3 -4 2301.77 128.818 12 -1 -3 -4 2120.67 122.639 12 -1 -3 -4 2003.03 119.242 13 -1 -3 -4 2027.00 124.867 11 -1 -3 -4 2002.00 121.761 17 -1 3 -4 1873.51 119.686 19 -1 3 -4 2159.26 115.255 16 -1 -3 -5 4922.76 236.273 5 -1 3 -5 4089.58 223.455 5 -1 3 -5 4752.10 221.903 12 -1 -3 -5 4905.36 220.201 12 -1 -3 -5 4450.14 211.297 13 -1 -3 -5 4350.23 212.017 17 -1 3 -5 4759.80 200.653 16 -1 3 -6 50996.8 1595.71 5 -1 -3 -6 52352.2 1593.10 5 -1 3 -6 55288.8 1581.81 12 -1 -3 -6 50926.5 1564.25 12 -1 -3 -6 51818.1 1558.22 13 -1 -3 -6 52289.9 1562.22 17 -1 3 -7 1439.30 132.720 12 -1 -3 -7 1727.64 140.140 12 1 3 7 1856.42 171.518 37 -1 -3 -7 1826.08 154.383 5 -1 3 -7 1843.51 157.684 5 -1 -3 -7 1978.38 144.390 17 -1 -3 -8 6626.44 329.343 12 -1 3 -8 6115.38 324.924 12 1 3 8 6524.64 373.192 37 -1 -3 -8 7512.34 334.428 17 -1 -3 -8 6970.86 357.062 5 -1 3 -8 7156.15 362.499 5 -1 3 -9 57942.3 1704.25 34 -1 3 -9 56780.9 1715.02 33 1 3 9 55678.3 1869.35 37 -1 3 -9 55631.8 1803.87 12 -1 3 -9 61092.7 1727.92 10 -1 -3 -9 59918.6 1813.75 12 -1 -3 -9 58588.1 1725.15 10 -1 -3 -9 57192.2 1718.16 9 -1 3 -9 59120.4 1724.54 9 -1 3 -9 57933.0 1721.55 8 -1 -3 -9 56059.8 1714.17 8 -1 -3 -9 59201.0 1849.21 5 -1 3 -9 56395.3 1844.85 5 -1 3 -10 134.314 47.2703 9 -1 -3 -10 141.632 49.8206 9 -1 3 -10 133.946 47.1424 8 -1 -3 -10 316.615 63.5088 8 -1 -3 -10 299.515 86.6035 5 -1 3 -10 227.435 49.2946 6 -1 -3 -10 203.226 48.0248 6 -1 3 -10 153.707 67.9626 5 1 3 10 362.237 102.552 37 -1 3 -10 132.117 45.6745 34 -1 -3 -10 203.054 46.8413 30 -1 3 -10 184.061 53.0181 33 -1 3 -10 166.211 62.8821 12 -1 -3 -10 353.055 83.0191 12 -1 3 -10 139.979 45.4778 24 -1 -3 -10 215.647 45.6266 25 -1 -3 -10 157.364 45.8110 26 -1 -3 -10 199.036 52.4842 28 -1 3 -10 179.976 47.8122 23 -1 3 -10 194.678 48.8030 20 -1 -3 -11 1959.25 143.007 6 -1 -3 -11 2217.76 222.254 5 -1 3 -11 2059.44 220.184 5 -1 3 -11 2336.55 154.956 6 -1 3 -11 2422.78 159.545 34 -1 3 -11 1941.14 153.306 33 -1 -3 -11 2162.37 148.157 30 -1 3 -11 2593.63 222.796 12 -1 -3 -11 1980.16 198.177 12 -1 -3 -11 2458.55 155.538 25 -1 -3 -11 1982.30 147.430 26 -1 3 -11 2108.80 147.795 24 -1 3 -11 2010.42 149.048 23 -1 -3 -11 2104.48 159.306 9 -1 3 -11 2535.75 174.936 9 -1 3 -11 2011.11 158.600 8 -1 -3 -11 2167.47 161.772 8 -1 3 -12 36427.2 1359.60 5 -1 -3 -12 37981.7 1362.92 5 -1 -3 -12 35019.7 1165.77 6 -1 3 -12 37669.8 1181.04 6 -1 3 -12 37509.8 1186.52 34 -1 3 -12 37019.4 1196.55 33 -1 -3 -12 37226.8 1176.69 30 -1 -3 -12 36767.4 1321.98 12 -1 3 -12 38503.6 1335.60 12 -1 3 -12 38551.9 1174.42 24 -1 -3 -12 39710.7 1182.11 25 -1 3 -12 36835.9 1181.06 23 -1 -3 -12 37352.1 1203.01 8 -1 -3 -12 37348.9 1204.14 9 -1 3 -12 37373.6 1206.33 8 -1 3 -12 36836.3 1205.46 9 -1 -3 -13 1552.17 139.317 6 -1 3 -13 1497.88 133.228 6 -1 3 -13 1799.40 145.697 34 -1 3 -13 1407.78 133.874 33 -1 -3 -13 1687.10 138.005 30 -1 3 -13 1826.34 207.017 12 -1 -3 -13 1444.48 177.760 12 -1 -3 -13 1743.01 138.157 25 -1 3 -13 1424.11 132.853 23 -1 -3 -13 1639.67 148.788 8 -1 3 -13 1446.62 142.119 8 -1 -3 -13 1617.94 151.387 9 -1 3 -13 1539.07 147.165 9 -1 -3 -14 501.117 77.6192 6 -1 3 -14 485.319 82.2221 6 -1 3 -14 503.097 85.1618 33 -1 3 -14 316.288 68.6351 34 -1 3 -14 490.753 81.9651 23 -1 3 -14 388.344 80.2564 8 -1 3 -14 500.639 84.8207 9 -1 -3 -14 671.914 96.5246 8 -1 -3 -14 456.260 83.7685 9 -1 -3 -14 510.443 80.2108 30 -1 -3 -15 11881.6 484.265 6 -1 3 -15 12545.2 497.067 33 -1 3 -15 12635.5 492.416 23 -1 -3 -15 12986.8 515.859 9 -1 3 -15 11965.2 503.360 8 -1 3 -15 12709.7 514.466 9 -1 -3 -15 12499.4 505.432 8 -1 -3 -15 12970.1 491.635 30 -1 3 -16 419.417 74.5388 6 -1 -3 -16 572.134 81.4869 6 -1 3 -16 637.092 85.4437 23 -1 3 -16 626.209 87.0900 8 -1 -3 -16 507.630 81.9941 9 -1 3 -16 579.879 89.8668 9 -1 -3 -16 536.822 86.1235 8 -1 3 -16 595.214 80.5993 33 -1 3 -17 8.22190 38.7578 6 -1 -3 -17 15.8102 28.8668 6 -1 3 -17-7.98969 33.6879 23 -1 3 -17 17.8942 38.6552 8 -1 -3 -17 9.25403 41.8414 9 -1 -3 -17 34.8706 40.2642 8 -1 3 -17 27.9908 40.3104 9 -1 3 -17 54.0263 35.6481 33 -1 3 -18 335.296 53.6845 23 -1 3 -18 322.455 53.0109 6 -1 -3 -18 342.896 53.5970 6 -1 3 -18 310.908 51.3058 8 -1 3 -18 290.883 58.5625 9 -1 -3 -18 254.132 55.1525 9 -1 -3 -18 348.037 55.3514 8 1 4 -19 1445.12 99.3733 23 1 4 -19 1452.15 98.0191 6 1 4 -19 1548.64 103.728 8 1 -4 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42.4087 30 1 4 -14 228.739 57.3157 23 1 4 -14 160.759 65.0342 9 1 4 -14 199.056 64.3668 8 1 -4 -14 171.022 58.8610 9 1 -4 -14 109.236 50.0399 8 1 4 -13 827.570 94.6915 6 1 4 -13 742.592 102.935 8 1 -4 -13 654.104 99.2663 8 1 -4 -13 782.290 104.580 9 1 4 -13 698.195 97.3733 9 1 4 -13 707.940 129.453 1 1 4 -13 662.677 136.375 5 1 -4 -13 612.512 82.6261 6 -1 4 13 605.170 138.656 37 1 4 -13 820.484 101.628 34 1 4 -13 628.948 95.4316 33 1 -4 -13 809.811 91.1134 30 1 4 -13 634.676 120.631 12 1 -4 -13 780.523 94.7882 25 1 4 -13 794.241 97.5703 23 1 -4 -13 865.979 141.572 17 1 -4 -12 12209.7 487.482 9 1 4 -12 12657.7 493.637 9 1 4 -12 12755.4 471.425 6 1 4 -12 12431.1 493.320 8 1 -4 -12 11957.5 485.770 8 1 -4 -12 12040.8 462.296 6 1 4 -12 13584.8 589.613 1 1 -4 -12 12753.9 575.778 1 1 4 -12 12331.9 614.246 5 1 4 -12 11642.8 470.108 34 -1 4 12 11460.4 629.204 37 1 4 -12 11107.4 482.555 33 1 -4 -12 11943.1 460.436 30 1 -4 -12 12819.3 576.644 12 1 4 -12 13092.6 585.668 12 1 -4 -12 12556.1 470.591 25 1 4 -12 12770.8 480.937 23 1 -4 -12 11952.6 572.850 17 1 4 -11 5538.25 250.313 6 1 -4 -11 5570.63 268.116 9 1 4 -11 4869.87 257.433 9 1 -4 -11 5473.70 353.983 5 1 4 -11 5871.88 335.699 1 1 -4 -11 5263.03 319.966 1 1 4 -11 5440.58 355.354 5 1 4 -11 4602.41 257.911 33 -1 4 11 5239.03 374.884 37 1 4 -11 5114.37 251.950 34 1 -4 -11 5209.93 244.141 30 1 4 -11 4983.79 313.952 12 1 -4 -11 5500.88 321.750 12 1 -4 -11 4899.36 241.504 25 1 4 -11 5350.02 254.902 23 1 -4 -11 5038.44 322.134 17 1 -4 -10-17.6706 44.0737 5 1 4 -10-18.1052 59.1255 5 1 -4 -10 14.2785 40.3817 1 1 4 -10 14.5417 45.4666 1 1 4 -10 7.81356 28.5282 34 -1 4 10-21.1279 66.0592 37 1 4 -10 9.33558 43.1148 33 1 -4 -10 14.2864 26.9360 25 1 4 -10-15.5831 35.9840 23 1 -4 -10 15.6652 41.7697 17 1 -4 -10-14.0939 32.5452 12 1 4 -10 14.6452 39.0500 12 -1 4 9 93.4663 63.7419 37 1 -4 -9 260.418 72.3849 5 1 4 -9 188.493 66.4182 5 1 -4 -9 234.288 64.9226 1 1 4 -9 113.103 43.0175 1 1 -4 -9 264.089 70.7461 17 1 4 -9 164.993 61.2203 18 1 4 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86.8003 23 -2 -1 -9 958.011 91.5991 20 -2 1 -9 762.813 86.3193 20 -2 -1 -10 73.8159 47.6839 8 -2 1 -10 74.6037 43.8035 8 -2 1 -10 32.8287 44.9754 9 -2 -1 -10 54.3695 49.1700 9 -2 1 -10 21.0047 56.0139 5 -2 1 -10 46.8445 35.3400 6 -2 -1 -10-18.4637 31.3918 6 -2 -1 -10 20.7912 51.8647 5 -2 1 -10 35.7448 42.1309 33 -2 -1 -10 24.2244 32.3083 30 -2 -1 -10 37.5622 50.0858 12 -2 1 -10 32.7660 41.1949 10 -2 -1 -10 32.7403 39.8562 10 -2 1 -10 19.0336 47.4816 12 -2 1 -10 29.6328 36.0753 28 -2 -1 -10 19.7331 33.5484 28 -2 1 -10 17.2874 32.6063 23 -2 -1 -10 65.9255 34.7537 23 -2 -1 -10 71.7152 36.8472 20 -2 1 -10 18.1031 35.1938 20 -2 1 -11 210.157 60.4640 8 -2 -1 -11 336.014 74.3299 9 -2 1 -11 253.514 70.3078 9 -2 -1 -11 196.460 65.5316 8 -2 1 -11 139.582 72.8848 5 -2 -1 -11 193.551 54.5228 6 -2 1 -11 186.001 53.5579 6 -2 -1 -11 230.370 81.3914 5 -2 1 -11 107.882 48.2660 33 -2 -1 -11 151.752 43.1601 30 -2 1 -11 156.680 62.4048 10 -2 1 -11 210.769 77.0942 12 -2 -1 -11 84.2491 54.6120 10 -2 -1 -11 62.4224 55.6751 12 -2 -1 -11 249.923 61.6377 28 -2 1 -11 141.479 60.0031 28 -2 1 -11 143.122 50.2963 23 -2 -1 -11 181.402 50.0734 23 -2 1 -11 160.509 44.6005 20 -2 -1 -11 207.934 54.6262 20 -2 -1 -12 7805.33 383.078 8 -2 1 -12 8473.31 392.887 8 -2 -1 -12 8054.75 390.786 9 -2 1 -12 8838.54 400.863 9 -2 1 -12 8641.65 372.132 33 -2 -1 -12 8560.25 361.469 30 -2 1 -12 8963.83 384.576 6 -2 -1 -12 8025.92 370.177 6 -2 1 -12 8683.35 488.130 12 -2 -1 -12 8463.29 485.290 12 -2 1 -12 8346.69 365.078 23 -2 -1 -12 8727.25 364.681 23 -2 -1 -12 8167.61 369.489 20 -2 1 -12 8946.21 380.659 20 -2 -1 -13 2035.37 172.379 8 -2 -1 -13 2082.11 176.580 9 -2 1 -13 2321.23 187.059 9 -2 1 -13 2481.94 188.606 8 -2 -1 -13 2452.95 165.601 30 -2 1 -13 2458.60 169.446 33 -2 -1 -13 2357.18 174.802 6 -2 1 -13 2238.90 164.641 23 -2 -1 -13 1903.98 152.472 23 -2 -1 -13 2314.03 172.398 20 -2 1 -14 202.604 58.9799 33 -2 1 -14 80.2531 51.9584 6 -2 -1 -14 90.7313 51.4022 6 -2 1 -14 229.839 63.1658 23 -2 -1 -14 88.2899 45.4491 23 -2 1 -14 50.7534 52.2634 8 -2 1 -14 185.525 62.5670 9 -2 -1 -14 226.169 68.1408 8 -2 -1 -14 131.854 63.4835 9 -2 -1 -14 153.912 47.2588 30 -2 1 -15 53806.9 1586.26 33 -2 -1 -15 51924.2 1578.22 23 -2 1 -15 50964.1 1587.53 23 -2 1 -15 52174.4 1628.23 9 -2 1 -15 52432.4 1623.43 8 -2 -1 -15 52443.0 1629.70 9 -2 -1 -15 53240.4 1626.68 8 -2 -1 -16 2065.43 157.290 9 -2 1 -16 1699.99 146.886 9 -2 1 -16 1974.50 138.102 23 -2 -1 -16 1901.73 131.916 23 -2 1 -16 1787.52 140.172 6 -2 -1 -16 2018.91 145.805 6 -2 -1 -16 1947.18 148.685 8 -2 1 -16 1764.27 145.381 8 -2 1 -17 45.7799 30.8861 23 -2 -1 -17 51.7106 36.2369 6 -2 1 -17 45.0579 36.8358 6 -2 -1 -17 103.457 39.0302 8 -2 1 -17 152.808 47.9899 8 -2 1 -18 175.373 36.4347 23 -2 1 -18 370.830 49.3845 6 -2 -1 -18 279.088 43.8685 6 -2 1 -18 330.266 48.8433 8 -2 -1 -18 236.267 43.3544 8 2 2 -20 14438.2 465.955 6 2 2 -19 442.620 60.9557 6 2 -2 -19 546.716 63.3969 6 2 2 -19 401.587 63.6705 9 2 -2 -19 545.374 69.7025 8 2 -2 -19 486.542 68.5274 9 2 2 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262.067 9 2 -2 -14 4297.64 242.643 6 2 -2 -14 4171.65 261.709 8 2 2 -14 4079.32 258.537 8 2 -2 -14 4142.57 261.380 9 2 2 -14 4444.52 245.847 6 2 -2 -13 1993.87 165.700 9 2 -2 -13 2056.88 152.534 6 2 2 -13 1934.01 151.905 6 2 2 -13 2087.11 171.054 9 2 -2 -13 1567.89 207.780 5 2 2 -13 1629.12 216.083 5 2 2 -13 2008.27 208.374 1 2 -2 -13 2063.67 211.376 1 2 2 -13 1959.46 147.695 34 2 2 -13 1704.60 149.789 33 2 -2 -13 1525.23 185.271 12 2 2 -13 1503.62 188.668 12 2 2 -13 1692.06 139.575 23 2 -2 -13 1876.77 207.466 17 2 2 -13 1704.98 197.333 17 2 -2 -12 6516.12 295.597 6 2 2 -12 6024.32 308.835 9 2 2 -12 6602.53 299.714 6 2 -2 -12 5806.71 304.411 9 2 2 -12 7369.06 302.976 34 -2 2 12 5477.12 389.905 37 2 2 -12 5419.35 299.806 33 2 2 -12 6353.14 383.683 1 2 -2 -12 6610.99 386.910 1 2 2 -12 6407.65 420.254 5 2 -2 -12 7232.78 441.942 5 2 2 -12 6236.72 380.482 12 2 -2 -12 6168.74 372.871 12 2 2 -12 6053.78 285.869 23 2 2 -12 6503.33 396.905 17 2 -2 -12 6304.80 386.715 17 2 2 -11 10.2052 39.6666 9 2 -2 -11-20.3122 42.8176 9 2 2 -11 8.01878 28.2848 34 -2 2 11-21.0031 65.6689 37 2 2 -11-9.74600 38.9801 33 2 2 -11 16.9690 47.9907 12 2 -2 -11-16.7254 38.6217 12 2 -2 -11 27.2822 31.4996 14 2 2 -11 37.3185 60.9347 17 2 -2 -11 18.1823 45.3501 17 2 2 -11 41.0977 32.8748 23 2 2 -11 34.5745 51.5354 1 2 2 -11-21.6444 49.9805 5 2 -2 -11-21.4993 73.0761 5 2 -2 -11 17.1929 39.7013 1 2 2 -10 114.667 62.4268 5 2 -2 -10 37.9558 53.6912 5 2 -2 -10 30.2270 37.7229 1 2 2 -10 60.8120 49.6683 1 2 2 -10 29.7736 42.1261 12 2 -2 -10 73.3442 49.8798 12 2 -2 -10 48.7404 36.3533 14 -2 2 10 112.900 58.8499 37 2 -2 -10 53.7982 42.2877 9 2 2 -10 90.1419 45.7843 9 2 2 -10 43.7047 47.5963 18 2 -2 -10 16.2727 43.4128 17 2 2 -10 101.772 63.9772 17 2 -2 -9 12955.6 522.811 14 -2 2 9 13742.3 596.911 37 2 -2 -9 14015.8 562.163 1 2 2 -9 13664.8 558.240 1 2 2 -9 15014.0 571.945 18 2 -2 -9 13730.6 572.052 17 2 2 -9 13348.7 579.667 17 2 -2 -8 8564.69 370.717 14 -2 2 8 8950.80 430.662 37 2 2 -8 9700.53 408.648 1 2 -2 -8 8667.01 394.823 1 2 2 -8 8848.00 398.539 18 2 -2 -8 9304.19 415.867 17 2 2 -7 1298.67 109.463 14 2 -2 -7 1235.34 108.713 14 -2 2 7 1467.43 146.450 37 -2 -2 7 1223.78 121.260 37 2 -2 -7 1160.85 116.449 1 2 2 -7 1187.46 117.043 1 2 2 -7 1295.87 124.073 18 2 -2 -7 1301.55 126.780 17 2 -2 -6 431.335 65.7737 15 2 -2 -6 325.970 53.4630 14 2 2 -6 405.913 61.5292 14 -2 2 6 500.979 85.8876 37 -2 -2 6 439.385 71.3884 37 2 2 -6 348.256 66.0191 18 2 -2 -6 291.133 61.5707 17 2 -2 -5 16649.4 560.278 14 2 2 -5 17345.6 565.730 14 -2 -2 5 17097.8 585.935 37 -2 2 5 16854.2 606.494 37 2 -2 -5 16615.5 571.255 15 2 2 -5 17238.0 591.398 18 2 -2 -5 16882.7 584.716 17 2 -2 -4 154980. 4489.49 14 2 2 -4 168924. 4498.91 14 -2 2 4 158919. 4538.82 37 -2 -2 4 166752. 4520.75 37 2 -2 -4 154705. 4504.06 17 2 2 -4 161296. 4521.24 18 2 -2 -4 160503. 4499.18 15 2 -2 -3 10954.1 365.103 14 -2 2 3 10431.6 397.713 37 -2 -2 3 10551.0 385.533 37 2 2 -3 10063.6 380.498 18 2 -2 -3 9991.91 366.564 17 2 -2 -3 11334.8 375.631 15 2 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41283.7 1214.67 13 -2 3 -2 41721.3 1231.72 12 -2 -3 -2 39438.0 1228.15 11 -2 -3 -2 40616.4 1224.00 12 2 -3 2 41198.5 1262.00 15 -2 3 -2 40033.9 1226.76 19 -2 3 -2 40461.1 1238.72 4 -2 -3 -2 41050.9 1239.18 4 -2 -3 -2 42510.2 1231.67 2 -2 -3 -2 43088.4 1232.82 5 -2 3 -2 41043.2 1232.52 5 -2 3 -2 41943.3 1231.55 2 -2 3 -3 18247.8 641.549 12 -2 -3 -3 20415.7 647.981 12 -2 -3 -3 19966.7 645.625 11 -2 -3 -3 19221.6 626.195 13 -2 3 -3 17906.0 611.977 16 -2 3 -3 20235.2 663.318 4 -2 -3 -3 19748.6 661.340 4 -2 -3 -3 20357.8 655.407 2 -2 3 -3 20392.0 656.437 2 -2 -3 -3 20806.9 655.839 5 -2 3 -3 20170.4 658.735 5 -2 3 -4 55.5742 40.9814 4 -2 -3 -4 68.6917 41.3000 5 -2 3 -4 17.7604 37.4666 5 -2 -3 -4 67.2322 36.3350 2 -2 3 -4 84.7565 39.9770 2 -2 -3 -4 55.5206 37.0386 4 -2 -3 -4 47.6136 33.4876 12 -2 3 -4 32.9846 33.0133 12 -2 -3 -4 63.5935 28.7880 13 -2 -3 -4 51.4464 33.2596 11 -2 -3 -5 434.980 72.7337 5 -2 3 -5 354.671 72.9976 5 -2 -3 -5 275.992 60.3876 2 -2 3 -5 549.507 84.3937 4 -2 -3 -5 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533.648 6 3 3 -15 14490.6 537.407 6 3 3 -15 12630.2 524.801 23 3 3 -14 1799.34 167.642 33 3 3 -14 2210.79 163.893 23 3 3 -14 2265.52 167.725 6 3 -3 -14 2185.48 164.375 6 3 -3 -14 2133.69 178.710 9 3 3 -14 2101.97 177.436 9 3 -3 -13 2043.32 173.462 9 3 3 -13 2214.04 177.490 9 3 -3 -13 1994.50 154.665 6 3 -3 -13 1874.65 231.278 5 3 3 -13 1874.26 232.606 5 3 3 -13 2054.84 216.108 1 3 -3 -13 1972.15 212.600 1 -3 3 13 2100.89 243.661 37 3 3 -13 2094.04 217.418 12 3 -3 -13 2362.59 225.654 12 3 -3 -13 2282.19 207.293 14 3 3 -13 1994.31 154.326 23 3 3 -13 1893.24 221.523 17 3 -3 -13 1895.05 216.065 17 3 3 -12 1495.92 181.855 1 3 -3 -12 2016.65 204.061 1 3 3 -12 1303.01 188.255 5 3 -3 -12 1553.84 205.302 5 -3 3 12 1575.20 208.426 37 3 -3 -12 1343.10 159.703 14 3 3 -12 1997.81 201.206 12 3 -3 -12 1510.43 173.065 12 3 -3 -12 1759.39 198.993 17 3 3 -12 1674.04 205.307 17 3 -3 -12 1756.67 151.806 9 3 3 -12 1613.43 145.855 9 3 3 -11 2238.04 163.088 9 3 -3 -11 2155.25 163.279 9 3 3 -11 1761.41 212.644 5 3 -3 -11 2013.89 226.502 5 3 3 -11 2220.52 206.202 1 3 -3 -11 2673.90 224.522 1 -3 3 11 2029.31 232.417 37 3 3 -11 2299.34 210.484 12 3 -3 -11 2185.67 208.986 12 3 -3 -11 1954.10 184.779 14 3 3 -11 2146.29 153.786 23 3 3 -11 2250.65 211.658 18 3 -3 -11 2247.71 217.347 17 3 3 -11 1554.43 193.943 17 3 -3 -10 4197.72 226.345 9 3 3 -10 4337.93 228.335 9 3 3 -10 3827.30 270.408 1 3 -3 -10 3682.86 267.041 1 -3 3 10 3238.10 285.427 37 3 -3 -10 3952.66 256.717 14 3 3 -10 4183.33 212.454 23 3 3 -10 4498.61 291.963 18 3 -3 -10 4583.60 303.202 17 3 3 -10 3578.51 286.586 17 3 3 -9 325.728 79.3809 1 3 -3 -9 400.335 80.7139 1 3 -3 -9 243.275 66.6190 14 3 -3 -9 270.545 52.2312 35 -3 3 9 352.833 96.3687 37 3 -3 -9 386.577 67.7853 9 3 3 -9 298.499 57.9241 9 3 3 -9 171.777 71.0764 18 3 -3 -9 334.738 85.3988 17 -3 3 8 18402.4 748.284 37 3 3 -8 18489.3 710.713 18 3 -3 -8 18223.6 702.675 17 3 -3 -8 18549.5 676.620 14 -3 3 7 43298.4 1433.76 37 3 3 -7 41817.1 1380.30 18 3 -3 -7 41753.8 1370.54 17 3 -3 -7 41938.7 1348.44 14 -3 3 6 5281.70 297.910 37 3 -3 -6 5178.59 259.244 15 3 3 -6 5216.55 277.544 18 3 -3 -6 4535.53 253.042 17 3 -3 -6 4547.12 243.142 14 -3 3 5 7759.47 392.592 37 -3 3 5 8494.06 390.348 3 -3 -3 5 9974.86 416.257 3 3 3 -5 8259.88 374.453 18 3 -3 -5 9374.95 368.181 15 3 -3 -5 8792.76 362.730 17 3 -3 -5 8306.58 349.911 14 -3 3 4 6978.21 331.871 37 -3 3 4 6315.92 310.779 3 -3 -3 4 6526.57 318.860 3 3 3 -4 6466.78 302.864 18 3 -3 -4 6656.48 290.933 15 3 -3 -4 6615.73 283.482 14 -3 -3 3 24557.1 876.814 4 -3 3 3 24811.0 872.902 4 -3 3 3 25785.6 874.151 3 -3 -3 3 25551.7 874.918 3 3 3 -3 26752.8 866.613 18 3 -3 -3 28422.8 861.730 15 3 -3 -3 26916.8 837.492 14 -3 3 2 1113.25 108.495 37 -3 -3 2 891.772 93.5755 2 -3 3 2 971.955 99.3630 2 -3 3 2 1051.70 103.868 4 -3 -3 2 1125.64 108.159 4 -3 3 2 1152.51 105.578 3 -3 -3 2 1186.51 108.561 3 3 3 -2 1019.65 95.7822 18 3 -3 -2 1057.75 95.6352 15 -3 -3 2 1036.41 97.7866 11 -3 -3 1 2766.13 168.371 2 -3 3 1 2853.76 169.087 2 -3 3 1 2593.50 167.644 4 -3 -3 1 2444.92 165.817 4 -3 3 1 2823.91 169.669 3 -3 -3 1 2521.45 167.634 3 3 -3 -1 2771.29 165.142 15 -3 -3 1 3008.85 167.408 11 -3 3 0 68093.5 2004.41 3 -3 3 0 65895.1 2005.34 4 -3 -3 0 67768.0 2010.96 4 -3 -3 0 69913.8 2003.21 2 -3 3 0 67001.9 1998.69 2 -3 -3 0 67646.0 2006.50 3 3 -3 0 71146.0 2015.52 15 -3 -3 0 66772.9 1987.84 11 -3 -3 -1 303.267 58.8535 2 -3 3 -1 276.575 58.8675 2 -3 3 -1 383.692 66.3612 4 -3 -3 -1 290.213 63.0774 4 3 -3 1 288.853 63.5785 15 -3 -3 -1 303.649 55.8793 11 -3 3 -2 21915.4 767.266 4 -3 -3 -2 22142.3 765.869 4 -3 3 -2 21026.3 746.307 2 -3 -3 -2 24386.5 766.219 2 3 -3 2 21493.4 773.756 15 -3 -3 -2 22421.4 740.799 11 -3 3 -3 39948.0 1293.05 4 -3 -3 -3 40600.4 1294.77 4 -3 -3 -3 39864.2 1275.38 2 -3 3 -3 42133.2 1285.16 2 3 -3 3 42082.0 1305.78 15 -3 3 -3 41065.7 1280.20 12 -3 -3 -3 39231.3 1271.94 12 -3 3 -4 2514.99 190.337 4 -3 -3 -4 2262.15 181.787 4 -3 -3 -4 2372.58 176.893 2 -3 3 -4 2418.66 179.774 2 -3 -3 -4 2406.15 178.450 5 -3 3 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113.362 10 -3 3 -7 1083.45 137.253 12 -3 -3 -7 1239.58 142.890 12 -3 -3 -7 977.043 97.2390 26 -3 3 -7 1231.53 102.928 24 -3 -3 -7 1103.78 94.3048 21 -3 -3 -7 1064.62 94.6650 23 -3 3 -7 987.188 92.1591 21 -3 3 -7 1083.11 97.8653 23 -3 3 -7 1139.47 97.3870 20 -3 -3 -8 4136.08 223.704 8 -3 3 -8 4193.41 227.180 8 -3 -3 -8 4168.53 227.509 9 -3 3 -8 4341.13 234.429 9 -3 3 -8 4030.51 237.037 7 -3 -3 -8 3962.71 234.503 7 -3 3 -8 3717.97 210.429 6 -3 -3 -8 3844.23 210.565 6 -3 -3 -8 4230.22 292.643 5 -3 3 -8 4386.09 299.687 5 -3 3 -8 3955.05 215.230 33 -3 3 -8 3959.93 217.396 28 -3 -3 -8 3311.32 202.707 28 -3 3 -8 4001.23 227.099 10 -3 -3 -8 3786.81 224.546 10 -3 3 -8 4149.88 286.374 12 -3 -3 -8 3892.65 275.989 12 -3 -3 -8 4230.83 222.066 26 -3 3 -8 3864.40 212.916 24 -3 -3 -8 4128.46 207.663 23 -3 -3 -8 3947.90 207.578 21 -3 3 -8 3935.08 209.761 23 -3 3 -8 4291.30 214.355 21 -3 -3 -8 4210.34 219.216 20 -3 3 -8 4159.69 214.306 20 -3 -3 -9 730.775 94.6585 8 -3 3 -9 547.531 83.0399 8 -3 -3 -9 751.136 106.723 7 -3 3 -9 692.569 101.015 7 -3 -3 -9 694.983 92.5169 9 -3 3 -9 772.515 100.712 9 -3 -3 -9 745.400 128.729 5 -3 3 -9 704.199 126.375 5 -3 3 -9 609.951 84.4691 6 -3 -3 -9 502.499 77.0201 6 -3 3 -9 605.305 84.1314 33 -3 -3 -9 1048.35 108.849 28 -3 -3 -9 1000.22 109.606 10 -3 3 -9 590.593 91.4585 10 -3 3 -9 849.782 133.020 12 -3 -3 -9 592.424 114.009 12 -3 3 -9 597.995 83.2763 24 -3 3 -9 701.223 88.8839 28 -3 -3 -9 590.632 79.9346 21 -3 3 -9 798.010 93.1751 23 -3 3 -9 618.259 78.7694 21 -3 -3 -9 751.803 85.0986 23 -3 -3 -9 569.804 82.4952 20 -3 3 -9 690.923 85.9656 20 -3 -3 -10 35.6841 51.3865 9 -3 -3 -10-11.1960 46.0071 8 -3 3 -10-46.0604 49.7465 8 -3 3 -10-12.0727 54.5823 9 -3 -3 -10 43.6462 54.4314 5 -3 3 -10 22.4343 55.9558 5 -3 3 -10-10.6049 38.7206 6 -3 -3 -10-10.2184 38.5328 6 -3 3 -10 10.5775 38.6205 33 -3 3 -10 24.4555 52.8252 10 -3 -3 -10 24.1820 44.1463 10 -3 3 -10 21.4009 53.3784 12 -3 -3 -10-20.7509 55.3306 12 -3 -3 -10-10.9375 37.1773 28 -3 3 -10 10.0057 40.0197 24 -3 3 -10-11.0816 43.0740 28 -3 -3 -10-36.8525 42.5501 23 -3 -3 -10-47.8241 33.7390 21 -3 3 -10-10.2640 42.1775 23 -3 -3 -10-20.7162 42.5643 20 -3 3 -10 40.7603 38.4261 20 -3 -3 -11 1212.82 128.407 8 -3 3 -11 1259.29 130.790 8 -3 3 -11 1321.20 138.856 9 -3 -3 -11 1289.72 132.859 9 -3 3 -11 1505.78 136.669 6 -3 -3 -11 1325.19 127.150 6 -3 3 -11 1463.68 135.920 33 -3 -3 -11 1443.61 134.629 28 -3 3 -11 1032.99 116.877 28 -3 3 -11 1142.72 127.670 10 -3 -3 -11 1218.10 134.510 10 -3 3 -11 1078.95 115.755 24 -3 -3 -11 1552.00 126.706 23 -3 -3 -11 1186.07 115.978 21 -3 3 -11 1221.11 123.368 23 -3 -3 -11 1280.99 124.731 20 -3 3 -11 1265.77 121.800 20 -3 3 -12 1290.83 132.762 8 -3 -3 -12 1404.86 136.436 8 -3 3 -12 1355.16 127.426 33 -3 -3 -12 1259.66 135.538 9 -3 3 -12 1367.36 139.436 9 -3 3 -12 1012.45 108.539 24 -3 -3 -12 1207.55 121.712 20 -3 3 -12 1386.18 130.200 20 -3 -3 -12 1412.16 122.529 21 -3 3 -12 1318.41 126.556 23 -3 -3 -12 1121.19 110.473 23 -3 3 -12 795.117 109.536 6 -3 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323.240 48.2799 6 3 4 -18 2826.66 169.776 33 3 4 -18 2974.60 166.603 23 3 -4 -18 2876.16 171.866 8 3 4 -18 3432.26 185.518 8 3 -4 -18 2968.15 175.248 9 3 4 -18 2862.94 172.161 9 3 4 -18 3129.49 167.200 6 3 4 -17 1939.41 151.356 33 3 4 -17 1779.98 132.151 6 3 -4 -17 1820.12 132.923 6 3 4 -17 1756.77 137.608 23 3 -4 -17 1747.11 144.941 8 3 4 -17 2145.84 156.993 8 3 -4 -17 1718.51 142.991 9 3 4 -17 1786.41 144.158 9 3 -4 -16 140.854 46.1530 6 3 4 -16 194.470 55.1287 6 3 4 -16 121.768 55.9071 23 3 -4 -16 137.914 54.3040 8 3 4 -16 116.549 52.8283 8 3 4 -16 138.066 57.5180 9 3 -4 -16 195.188 65.0531 9 3 4 -16 92.3546 47.5882 33 3 4 -15 10826.1 443.374 23 3 4 -15 11267.8 437.269 6 3 -4 -15 10506.4 426.915 6 3 -4 -15 10413.5 453.046 8 3 4 -15 10121.8 451.765 8 3 -4 -15 11032.3 460.646 9 3 4 -15 10573.2 458.110 9 3 4 -15 9316.64 441.677 33 3 4 -14 2319.25 168.203 23 3 4 -14 1887.74 150.862 6 3 -4 -14 2111.68 170.346 9 3 4 -14 2078.40 171.878 9 3 -4 -14 1610.77 139.779 6 3 4 -14 1784.72 164.546 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81.0076 33 3 6 -17 520.030 74.4681 23 3 6 -16 122.178 49.2384 33 3 6 -16 134.892 49.0406 23 3 6 -15 3700.74 235.291 33 3 6 -15 3671.23 220.140 23 3 6 -14 21.9682 51.7882 23 3 6 -14 64.7423 50.3438 33 3 6 -13 65.4097 41.1556 23 3 6 -13 90.7257 69.1454 33 3 -6 -12 407.597 76.1865 35 -3 6 12 385.668 131.472 37 3 -6 -12 386.452 87.1848 14 3 6 -12 174.313 63.8166 33 3 6 -12 511.900 79.2758 23 3 6 -12 259.749 84.5925 18 3 6 -12 308.689 78.9345 16 3 -6 -12 212.799 78.1904 17 3 6 -12 401.035 106.036 17 3 -6 -11 2625.37 175.682 35 -3 6 11 1974.32 247.622 37 3 6 -11 2634.97 174.967 23 3 6 -11 2581.55 240.452 18 3 -6 -11 2712.30 238.471 17 3 6 -11 2474.98 215.266 16 3 -6 -11 2872.97 230.057 14 3 -6 -10 1006.01 103.663 35 -3 6 10 792.408 151.016 37 3 6 -10 1032.35 104.105 23 3 6 -10 855.684 135.411 18 3 6 -10 854.348 118.470 16 3 -6 -10 1139.88 145.277 17 3 -6 -10 1316.76 147.113 14 3 -6 -9 13582.3 509.083 35 -3 6 9 12593.2 644.645 37 3 -6 -9 13698.4 580.530 14 3 6 -9 13562.4 497.986 23 3 6 -9 14405.3 630.533 18 3 -6 -9 13955.4 597.865 17 3 -6 -9 15337.7 630.363 15 3 6 -9 14228.2 576.619 16 3 -6 -8 943.007 117.999 14 -3 6 8 563.860 117.349 37 3 -6 -8 1041.08 97.9172 35 3 -6 -8 975.582 129.352 15 3 6 -8 701.915 120.621 18 3 6 -8 853.583 108.165 16 3 6 -8 1001.66 90.5774 23 3 -6 -7 6470.43 279.256 35 -3 6 7 6466.57 386.539 37 3 -6 -7 6959.83 358.417 15 3 6 -7 6013.17 356.001 18 3 6 -7 6665.34 325.243 16 3 -6 -7 6476.96 334.462 14 -3 6 6 1411.68 168.154 37 3 6 -6 1712.05 166.839 18 3 -6 -6 1572.20 150.329 15 3 -6 -6 1741.41 147.394 14 -3 -6 6 1165.47 130.471 11 -3 6 5 10278.6 484.609 37 3 6 -5 11125.4 485.746 18 3 -6 -5 11499.9 475.729 15 -3 -6 5 10239.6 449.381 11 3 -6 -5 10881.2 443.883 14 -3 6 4 5971.39 312.193 37 3 6 -4 5105.16 293.707 18 3 -6 -4 4949.10 280.898 15 3 -6 -4 5471.47 267.205 14 -3 -6 4 5194.56 280.550 11 3 6 -3 10111.4 437.677 18 3 -6 -3 10030.9 432.561 15 3 -6 -3 9847.32 397.975 14 -3 -6 3 10298.2 433.425 11 3 6 -2 2715.21 189.076 18 3 -6 -2 2845.60 194.129 15 -3 -6 2 2456.38 178.498 11 -3 6 1 298.985 72.8422 19 3 -6 -1 311.340 70.8498 15 -3 -6 1 200.559 56.0276 11 -3 6 0 50431.4 1687.31 19 -3 -6 0 53218.0 1676.20 11 -3 -6 0 56091.0 1664.93 13 -3 6 -1 37.3979 43.9763 19 3 -6 1-14.0611 47.7982 15 -3 -6 -1 20.2107 31.6026 13 -3 -6 -1 69.6681 46.4454 11 3 -6 2 2009.12 186.414 15 -3 -6 -2 1935.05 162.095 11 -3 -6 -2 1979.82 152.475 13 3 -6 3 10310.2 499.299 15 -3 -6 -3 10904.0 463.484 11 3 -6 4 9257.12 478.909 15 -3 -6 -4 10171.7 446.519 11 -3 -6 -5 300.973 54.2491 32 3 -6 5 372.268 99.8438 15 -3 6 -6 410.329 64.1925 33 -3 6 -6 381.872 64.3475 24 -3 -6 -6 639.491 81.6773 26 -3 -6 -6 502.294 70.0827 31 -3 -6 -6 370.342 65.5522 29 -3 -6 -6 504.659 66.7932 21 -3 6 -6 490.046 66.6696 21 3 -6 6 299.402 95.3582 15 -3 6 -7 195.526 51.2752 33 -3 6 -7 232.031 56.0902 24 -3 -6 -7 182.357 49.8777 26 -3 -6 -7 156.297 42.1410 30 -3 -6 -7 264.959 56.1370 31 -3 -6 -7 329.093 61.6705 29 -3 -6 -7 180.884 46.9863 21 -3 6 -7 248.282 52.6133 21 3 -6 7 93.4976 73.3006 15 -3 6 -8 1555.34 131.475 33 -3 -6 -8 1687.10 138.645 26 -3 6 -8 1786.16 140.345 24 -3 -6 -8 1608.64 129.848 31 -3 -6 -8 1317.72 115.762 30 -3 -6 -8 1619.29 130.691 21 -3 6 -8 1638.53 129.185 21 3 -6 8 2006.50 231.333 15 3 6 9 9707.69 581.081 37 -3 6 -9 10237.9 418.461 33 -3 -6 -9 9609.22 415.001 26 -3 6 -9 10588.9 424.587 24 -3 -6 -9 9769.75 401.029 30 -3 -6 -9 9896.05 406.343 21 3 -6 9 9337.78 565.324 15 3 6 10 5138.81 401.881 37 -3 6 -10 4689.90 255.985 33 -3 -6 -10 4743.85 260.606 26 -3 6 -10 4575.92 255.883 24 -3 -6 -10 4420.13 241.512 30 -3 -6 -10 4263.54 240.409 21 -3 6 -10 5221.22 260.522 23 3 -6 10 5263.30 403.243 15 -3 -6 -11 310.376 62.7020 30 -3 -6 -11 389.854 73.0689 21 -3 6 -11 453.887 80.2308 23 -3 6 -11 370.291 71.6671 33 -3 6 -11 348.972 73.4439 24 -3 -6 -11 364.295 71.8932 26 -3 -6 -12 13939.0 522.953 30 -3 -6 -12 13849.0 522.361 21 -3 6 -12 14108.8 530.635 23 -3 6 -12 13734.0 535.694 33 -3 -6 -12 13986.2 539.866 26 -3 6 -12 14186.7 541.764 24 -3 -6 -13 172.415 47.7790 30 -3 -6 -13 160.165 46.8560 21 -3 6 -13 76.3371 40.4053 23 -3 6 -13 121.991 49.9401 33 -3 6 -13 175.325 60.8335 24 -3 -6 -13 161.801 53.2125 26 -3 -6 -14 850.106 88.4143 30 -3 6 -14 925.558 93.2950 23 -3 6 -14 800.757 92.0558 33 -3 6 -14 775.365 90.4537 24 -3 -6 -15 3516.22 178.337 30 -3 6 -15 3668.50 183.259 23 -3 6 -15 3483.71 183.453 33 -3 6 -16 3372.20 160.357 33 -3 6 -16 3435.85 161.755 24 3 7 -19 82.1207 24.8869 23 3 7 -18 5036.64 229.025 33 3 7 -18 5253.49 223.495 23 3 7 -17 105.069 44.4768 33 3 7 -17 30.7064 32.4009 23 3 7 -16 63.4192 45.6852 33 3 7 -16 45.4987 37.4204 23 3 7 -15 998.011 115.847 33 3 7 -15 1003.75 107.379 23 3 7 -14 1434.08 146.026 33 3 7 -14 1581.98 137.013 23 3 7 -13 863.489 115.020 33 3 7 -13 1055.38 114.434 23 3 -7 -13 1260.25 121.024 35 3 -7 -12 7517.17 344.335 35 -3 7 12 6716.44 486.239 37 3 7 -12 7911.55 346.022 23 3 7 -12 7790.14 425.283 16 3 -7 -12 6656.62 400.529 14 3 -7 -11 1023.01 112.927 35 -3 7 11 1114.37 185.382 37 3 7 -11 1194.23 114.116 23 3 7 -11 1428.45 179.780 18 3 -7 -11 1096.27 151.262 17 3 7 -11 1412.37 160.994 16 3 -7 -11 981.222 140.602 14 3 -7 -10 1315.62 123.716 35 -3 7 10 1374.37 197.971 37 3 7 -10 1218.03 115.748 23 3 7 -10 1359.46 176.056 18 3 -7 -10 1451.12 167.361 17 3 7 -10 1383.89 154.718 16 3 -7 -10 1351.14 154.722 14 3 -7 -9 37.6191 41.5898 35 -3 7 9 24.0990 60.1106 37 3 -7 -9 37.9081 50.5428 15 3 -7 -9-16.0457 40.0257 14 3 7 -9 16.8712 32.7940 23 3 7 -9 20.1289 50.2090 18 3 7 -9 89.2797 52.4898 16 -3 -7 8 2105.95 183.143 11 3 -7 -8 1866.97 176.436 14 3 -7 -8 2009.44 144.905 35 3 7 -8 2103.17 208.474 18 3 -7 -8 2282.78 204.370 15 3 7 -8 2221.72 181.274 16 -3 7 8 2278.35 160.604 27 3 7 -8 2408.23 146.327 23 3 -7 -7 4031.58 213.246 35 -3 7 7 4545.50 313.605 37 3 -7 -7 4313.82 281.964 15 3 7 -7 4585.56 304.604 18 3 7 -7 4910.68 267.551 16 -3 -7 7 4360.92 273.040 11 3 -7 -7 4033.57 260.845 14 3 -7 -6 55182.2 1602.60 35 -3 7 6 51437.9 1742.32 37 3 7 -6 53671.7 1746.38 18 3 -7 -6 53146.1 1713.90 15 3 7 -6 54436.1 1662.50 16 -3 -7 6 57428.9 1711.75 11 3 -7 -6 52116.7 1676.59 14 3 7 -5 6793.19 368.358 18 3 -7 -5 6813.78 357.968 15 3 7 -5 7258.53 322.810 16 -3 -7 5 5997.98 330.116 11 3 -7 -5 6671.54 327.985 14 3 7 -4 503.218 95.7375 18 3 7 -4 505.395 73.6625 16 3 -7 -4 575.135 93.3250 15 3 -7 -4 733.335 93.1982 14 -3 -7 4 396.313 80.3507 11 3 7 -3 8865.57 419.709 18 3 -7 -3 8855.79 413.460 15 -3 -7 3 8848.63 409.076 11 3 -7 -3 9334.92 384.465 14 -3 7 2 657.613 104.467 19 3 7 -2 629.731 97.7753 18 3 -7 -2 599.133 91.1208 15 -3 -7 2 713.833 102.408 11 3 -7 -1 2939.46 207.265 15 -3 7 1 2474.05 200.630 19 -3 -7 1 2271.36 182.722 11 -3 -7 1 2356.43 174.103 13 3 -7 0 47181.9 1481.64 15 -3 7 0 45334.7 1477.57 19 -3 -7 0 45757.6 1431.09 13 -3 -7 0 45093.6 1452.03 11 -3 7 -1 2759.92 208.891 19 3 -7 1 2810.34 218.942 15 -3 -7 -1 2689.14 199.657 11 -3 -7 -1 2574.80 183.147 13 3 -7 2 1626.79 174.574 15 -3 -7 -2 1673.23 156.476 11 -3 -7 -2 1852.20 153.937 13 3 -7 3 11352.1 542.635 15 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5635.25 275.109 30 -3 -7 -9 5813.40 282.043 21 3 -7 9 5791.59 430.933 15 -3 -7 -10 92.3006 45.4059 30 -3 -7 -10 31.4636 38.3615 21 -3 7 -10 140.064 52.8271 33 -3 7 -10 144.613 55.5387 24 -3 -7 -10 80.0171 43.1661 26 -3 -7 -11 245.553 59.6577 30 -3 -7 -11 207.234 57.1664 21 -3 7 -11 151.319 55.0880 33 -3 7 -11 180.000 59.2509 24 -3 -7 -11 125.287 52.8280 26 -3 -7 -12 11746.9 457.671 30 -3 -7 -12 11019.1 450.052 21 -3 7 -12 12346.9 461.055 23 -3 7 -12 11081.0 458.483 33 -3 -7 -12 11460.5 468.230 26 -3 7 -12 12194.3 475.243 24 -3 -7 -13 4004.68 219.606 30 -3 7 -13 4712.72 232.272 23 -3 -7 -13 4273.76 222.442 21 -3 7 -13 4322.56 230.772 33 -3 -7 -13 4407.45 236.454 26 -3 7 -13 4265.32 237.500 24 -3 -7 -14 301.582 53.9767 30 -3 7 -14 349.161 59.8226 23 -3 7 -14 471.585 67.3621 33 -3 7 -14 354.732 63.9415 24 -3 -7 -15 683.338 70.6189 30 -3 7 -15 696.037 71.6032 23 -3 7 -15 688.961 73.8717 33 -3 7 -16 173.693 34.4320 33 -3 7 -16 164.943 34.0709 24 3 8 -18 7409.93 294.381 33 3 8 -18 7924.64 288.757 23 3 8 -17 2167.74 149.420 33 3 8 -17 2642.16 150.694 23 3 8 -16 343.240 69.4616 33 3 8 -16 471.079 69.5748 23 3 8 -15 2293.88 171.999 33 3 8 -15 2111.03 156.325 23 3 8 -14 221.224 62.8801 33 3 8 -14 297.859 66.8382 23 3 -8 -14 348.743 68.8184 35 3 8 -13 841.542 98.8683 23 3 -8 -13 600.258 89.1533 35 3 8 -13 924.729 115.801 33 3 8 -12 1524.89 131.424 23 3 8 -12 1117.44 131.256 33 3 -8 -12 1459.23 133.106 35 3 8 -11 771.029 114.846 33 3 -8 -11 1163.90 119.074 35 -3 8 11 750.379 158.449 37 3 8 -11 894.028 100.743 23 3 8 -11 881.624 147.398 18 3 8 -11 1100.35 144.924 16 3 -8 -11 1152.94 151.332 14 3 -8 -10 549.453 83.3216 35 -3 8 10 538.341 130.521 37 3 -8 -10 755.262 119.900 14 3 8 -10 661.631 84.6348 23 3 8 -10 787.581 136.911 18 3 8 -10 564.669 104.704 16 3 -8 -9 6751.83 320.056 35 -3 8 9 6969.21 447.987 37 -3 8 9 7150.15 341.726 27 3 -8 -9 7186.89 392.286 14 3 8 -9 6620.40 303.981 23 3 8 -9 7411.51 436.718 18 3 -8 -9 7317.50 421.039 15 3 8 -9 6873.00 373.946 16 3 -8 -8 11182.2 438.324 35 3 -8 -8 11419.2 515.094 14 -3 8 8 11388.7 461.882 27 3 8 -8 11176.6 422.141 23 3 8 -8 10163.4 543.548 18 3 -8 -8 10997.8 539.156 15 3 8 -8 11161.6 495.399 16 3 -8 -7 77.8946 38.2185 32 -3 -8 7 92.4098 52.3953 11 3 -8 -7 134.747 50.9360 14 -3 8 7 42.5957 44.9479 27 3 -8 -7 128.667 45.0755 35 -3 8 7 20.2753 76.4860 37 3 -8 -7 70.7662 55.3577 15 3 8 -7 39.4894 55.8831 18 3 8 -7 93.5021 51.9647 16 3 -8 -6 17811.7 590.613 32 -3 -8 6 16538.4 673.071 11 3 -8 -6 17664.1 671.231 14 3 -8 -6 16589.0 588.729 35 3 8 -6 17577.2 729.067 18 3 -8 -6 18212.9 711.497 15 3 8 -6 17108.1 648.602 16 -3 8 6 16538.7 616.323 27 3 -8 -5 1272.98 105.445 35 3 8 -5 1058.17 143.730 18 3 -8 -5 1263.28 147.517 15 3 8 -5 1381.62 128.770 16 3 -8 -5 1594.90 147.461 14 -3 -8 5 1414.05 147.180 11 3 8 -4 3771.46 265.489 18 3 -8 -4 3838.67 254.891 15 3 -8 -4 3506.62 223.636 14 -3 -8 4 3533.63 242.481 11 3 8 -3 30813.3 1128.23 18 3 -8 -3 34735.3 1139.84 15 -3 8 3 33363.1 1177.46 19 -3 -8 3 34073.5 1131.29 11 3 8 -2 6454.84 352.686 18 3 -8 -2 7707.75 373.465 15 -3 8 2 7031.73 388.168 19 -3 -8 2 6376.84 348.976 11 -3 8 1-16.5438 49.3424 19 3 -8 -1 43.8199 41.3376 15 -3 -8 1 97.6387 52.6193 11 -3 -8 1 99.4354 45.4067 13 3 -8 0 3243.29 235.840 15 -3 8 0 3100.84 237.939 19 -3 -8 0 3055.61 222.826 11 -3 -8 0 3312.46 217.606 13 -3 8 -1 408.539 88.7658 19 3 -8 1 510.208 97.9188 15 -3 -8 -1 552.781 94.5942 11 -3 -8 -1 602.375 91.1998 13 -3 -8 -2 3352.08 236.769 11 -3 -8 -2 3397.53 225.844 13 -3 8 -2 3477.53 248.284 19 3 -8 2 3809.86 274.744 15 -3 -8 -2 3039.64 177.510 32 -3 -8 -3 11756.6 504.656 13 -3 -8 -3 11899.8 440.502 32 3 -8 3 10932.7 554.480 15 -3 -8 -4 626.395 75.3388 31 -3 -8 -4 572.316 76.2868 32 -3 -8 -4 620.447 80.9928 29 -3 -8 -4 535.902 90.6809 13 -3 -8 -4 458.121 67.7060 26 -3 -8 -4 582.591 71.1550 21 3 -8 4 409.523 112.215 15 -3 -8 -5 8.66977 31.6544 31 -3 -8 -5-9.42721 40.7262 29 -3 -8 -5 9.07658 36.3027 32 -3 -8 -5 16.9797 42.3506 11 -3 -8 -5-8.96456 33.8042 26 -3 -8 -5-8.35174 27.2740 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2948.89 168.998 28 -8 1 -5 3021.02 170.183 28 -8 1 -5 3030.27 177.045 10 -8 -1 -5 3293.50 183.441 10 -8 -1 -6 1488.10 117.596 7 -8 1 -6 1770.98 114.866 28 -8 1 -6 1587.07 114.128 10 -8 -1 -6 1624.97 115.675 10 -8 -1 -7 1684.36 102.711 28 -8 1 -7 1667.95 101.752 28 -8 -2 14 2153.71 118.510 28 -8 -2 13 1552.65 106.129 28 -8 2 13 1496.04 107.755 7 -8 -2 13 1512.20 108.147 7 8 -2 -13 1401.45 106.105 9 8 2 -13 1629.43 113.019 9 8 -2 -13 1527.90 101.714 35 -8 2 13 1491.29 108.881 10 -8 -2 13 1674.75 114.965 10 -8 -2 12 7575.25 298.973 28 -8 2 12 7153.28 295.009 28 -8 2 12 6953.04 298.091 7 -8 -2 12 7153.30 302.271 7 8 -2 -12 7561.47 307.420 9 8 2 -12 6721.64 297.981 9 8 -2 -12 6995.14 290.109 35 -8 2 12 7268.24 305.118 10 -8 -2 12 7273.58 304.954 10 -8 -2 11 2388.17 151.914 28 -8 2 11 2224.63 149.575 28 -8 2 11 2527.60 161.942 7 -8 -2 11 2623.32 165.491 7 8 -2 -11 2520.55 163.825 9 8 2 -11 2540.47 164.537 9 8 -2 -11 2298.06 149.427 35 8 2 -11 2358.70 146.082 35 -8 2 11 2476.23 161.639 10 -8 -2 11 2414.99 161.715 10 -8 -2 10 1681.45 130.898 28 -8 2 10 1633.41 130.748 28 -8 2 10 1919.00 143.655 7 -8 -2 10 1880.43 148.562 7 8 -2 -10 1765.04 142.527 9 8 2 -10 1576.31 136.441 9 8 -2 -10 1847.72 133.641 35 8 2 -10 1708.13 129.755 35 -8 2 10 1762.30 141.538 10 -8 -2 10 1883.60 144.239 10 -8 -2 9 139.365 52.3620 28 -8 2 9 299.431 64.6593 28 -8 2 9 262.540 63.5912 7 -8 -2 9 276.154 65.8275 7 8 -2 -9 328.092 67.3523 9 8 2 -9 331.116 76.3934 9 8 -2 -9 431.518 68.2167 35 8 2 -9 213.784 58.0602 35 -8 -2 9 290.169 67.3986 10 -8 2 9 310.027 67.9150 10 -8 -2 8 117.631 50.6394 28 -8 2 8-9.86506 43.6488 28 -8 -2 8 113.962 48.9163 29 -8 2 8 139.423 60.6829 7 -8 -2 8 75.9434 47.9972 7 8 -2 -8 47.1000 44.4296 35 8 2 -8 66.4636 43.8783 35 -8 2 8 21.7883 49.2786 10 -8 -2 8 43.7009 44.9213 10 -8 -2 7 448.413 76.0259 28 -8 2 7 307.460 66.6668 28 -8 -2 7 317.320 65.0948 29 -8 2 7 258.381 67.4054 7 -8 -2 7 281.849 72.4790 7 8 -2 -7 174.647 54.6393 35 -8 2 7 249.328 67.9926 10 -8 -2 7 261.449 69.0325 10 -8 -2 6 5111.63 261.214 29 -8 -2 6 5328.77 270.879 28 -8 2 6 5608.52 276.735 28 -8 2 6 4945.30 275.981 7 -8 -2 6 4875.75 275.749 7 8 -2 -6 5176.86 264.667 35 -8 2 6 5291.91 281.884 10 -8 -2 6 4712.58 271.156 10 -8 -2 5 1579.12 137.090 29 -8 -2 5 1679.05 143.779 28 -8 2 5 1783.17 146.117 28 -8 2 5 1600.34 147.659 7 -8 -2 5 1709.82 150.512 7 8 -2 -5 1604.92 138.312 35 -8 2 5 1935.03 158.875 10 -8 -2 5 1488.97 143.993 10 -8 2 4 162.332 54.4159 29 -8 -2 4 102.600 45.7369 29 -8 -2 4 162.302 57.0888 28 -8 2 4 358.427 72.6347 28 -8 2 4 467.844 84.0691 10 -8 -2 4 276.920 70.2083 10 -8 2 4 446.418 83.0085 7 -8 -2 4 158.077 63.0545 7 8 -2 -4 174.889 56.0166 35 -8 -2 3 1129.25 119.950 26 -8 2 3 1323.31 135.792 10 -8 -2 3 1256.18 129.471 10 -8 2 3 1376.83 142.844 7 -8 -2 3 1351.34 135.525 7 -8 -2 3 1274.65 123.949 29 -8 -2 3 1531.33 134.556 28 -8 2 3 1481.67 133.769 28 -8 2 3 1363.91 125.886 29 -8 -2 2 1731.73 147.105 26 -8 2 2 1952.82 163.593 10 -8 -2 2 1998.01 164.275 10 -8 2 2 1714.95 157.153 7 -8 -2 2 1751.40 160.678 7 -8 2 2 1986.63 152.357 29 -8 -2 2 2093.26 156.045 29 -8 -2 2 2107.01 158.725 28 -8 2 2 2046.81 158.717 28 -8 -2 1 10.3623 41.4576 26 -8 2 1 59.1371 55.7588 10 -8 -2 1 11.8922 50.1474 10 -8 2 1 12.2667 43.2808 7 -8 -2 1 98.7814 52.0672 7 -8 -2 1 21.3463 43.8701 28 -8 2 1 10.6865 43.9248 28 -8 2 1 77.0566 41.6238 29 -8 -2 1 71.6973 47.3143 29 -8 -2 0 974.622 104.939 26 -8 -2 0 650.374 95.8277 10 -8 2 0 761.577 104.150 10 -8 -2 0 679.313 103.063 7 -8 2 0 920.521 113.746 7 -8 -2 0 818.447 97.8921 29 -8 -2 0 1137.53 113.334 28 -8 2 0 1064.57 111.623 28 -8 -2 -1 110.898 50.5292 28 -8 2 -1 231.601 59.4846 28 -8 2 -1 288.481 67.9642 10 -8 -2 -1 167.700 61.6507 10 -8 2 -1 152.626 62.8010 7 -8 -2 -1 118.187 61.2217 7 -8 -2 -1 229.319 59.2697 29 -8 -2 -2 95.7495 47.0303 28 -8 2 -2 143.324 56.3585 28 -8 2 -2 189.225 57.8899 10 -8 -2 -2 95.4418 51.0930 10 -8 -2 -2 116.107 45.4734 29 -8 2 -2 168.559 60.0260 7 -8 -2 -2 112.568 54.2212 7 -8 2 -3 985.877 111.483 7 -8 -2 -3 1308.71 124.268 7 -8 2 -3 1268.28 120.222 10 -8 -2 -3 1310.32 121.672 10 -8 2 -4 17.6495 39.0233 10 -8 -2 -4 17.8504 41.2221 10 -8 -2 -4 40.3012 36.4441 28 -8 2 -4 24.0700 37.8214 28 -8 2 -4 28.7692 44.2911 7 -8 -2 -4 48.2120 43.5967 7 -8 -2 -4-13.3581 30.2002 20 -8 2 -5 1128.46 100.732 10 -8 -2 -5 1165.01 102.322 10 -8 2 -5 1179.49 107.632 7 -8 -2 -5 1141.63 107.129 7 -8 -2 -5 1040.94 93.5980 28 -8 2 -5 1169.13 98.2156 28 -8 2 -6 41453.0 1218.31 10 -8 -2 -6 41736.8 1220.77 10 -8 -2 -6 39368.3 1191.88 20 -8 -2 -6 38636.1 1223.54 7 -8 -2 -6 41686.1 1209.28 28 -8 2 -6 41131.7 1208.08 28 -8 -2 -7 1434.72 90.6248 28 -8 3 13 2579.24 141.982 10 -8 -3 13 2643.90 145.029 10 -8 -3 13 2661.44 138.595 28 8 -3 -13 2457.16 134.485 35 -8 3 13 2299.06 136.251 7 -8 -3 13 2553.88 143.195 7 8 -3 -13 2590.95 142.746 9 8 3 -13 2780.38 147.705 9 -8 3 12 9908.15 367.096 10 -8 -3 12 9746.69 367.805 10 -8 -3 12 9844.94 359.214 28 8 -3 -12 9432.46 355.807 35 -8 3 12 8927.37 355.804 7 -8 -3 12 9388.62 363.463 7 8 -3 -12 9471.31 364.474 9 8 3 -12 9281.28 366.009 9 8 -3 -11 5914.31 261.896 35 -8 3 11 5959.03 268.696 10 -8 -3 11 6200.01 272.409 10 -8 -3 11 5795.20 257.160 28 -8 3 11 5683.81 257.464 28 8 3 -11 5725.72 246.295 23 -8 3 11 5605.48 261.934 7 -8 -3 11 6214.06 273.108 7 8 -3 -11 5587.73 263.835 9 8 3 -11 5690.84 269.663 9 8 -3 -10 98.7199 42.5074 35 8 3 -10 46.6155 37.3795 35 -8 3 10 57.4848 37.9592 28 -8 -3 10 105.692 44.0571 28 -8 3 10 9.03093 39.9635 10 -8 -3 10 18.1711 38.3367 10 8 3 -10 71.8009 35.2070 23 -8 3 10 140.758 54.4064 7 -8 -3 10 26.9818 42.4229 7 8 -3 -10 82.6458 45.8348 9 8 3 -10 37.4353 47.5379 9 -8 -3 9 1007.44 100.208 28 -8 3 9 840.071 94.3497 28 -8 3 9 866.866 99.6794 10 -8 -3 9 812.719 95.8355 10 8 3 -9 868.527 89.2899 23 -8 3 9 860.777 102.432 7 -8 -3 9 726.152 94.3788 7 8 -3 -9 800.552 99.1841 9 8 3 -9 803.879 101.683 9 8 -3 -9 879.716 96.7751 35 8 3 -9 586.683 80.2926 35 -8 -3 8 3238.99 194.639 28 -8 3 8 2910.83 189.063 28 -8 3 8 3334.12 205.085 7 -8 -3 8 3453.18 208.385 7 8 -3 -8 3288.59 195.633 35 -8 3 8 3435.53 208.077 10 -8 -3 8 3494.78 210.320 10 -8 -3 7 125.998 50.4178 28 -8 3 7 302.697 66.6599 28 -8 -3 7 291.686 59.8477 29 -8 3 7 266.282 62.1993 7 -8 -3 7 313.699 68.6803 7 8 -3 -7 217.958 60.2397 35 -8 3 7 215.314 63.6750 10 -8 -3 7 140.624 58.0097 10 -8 -3 6 769.980 98.5098 28 -8 3 6 774.972 96.3550 28 -8 -3 6 661.373 87.9142 29 -8 3 6 906.934 107.979 7 -8 -3 6 946.853 113.195 7 8 -3 -6 748.513 94.2957 35 -8 3 6 942.853 109.786 10 -8 -3 6 669.302 97.0545 10 -8 -3 5 3086.62 191.031 29 -8 -3 5 2401.02 174.983 28 -8 3 5 2753.50 184.622 28 -8 3 5 2568.64 186.058 10 -8 -3 5 3244.13 204.900 10 -8 3 5 2763.04 192.561 7 -8 -3 5 2858.88 195.873 7 8 -3 -5 3041.39 187.635 35 -8 -3 4 180.983 59.6548 26 -8 3 4 148.793 65.8858 10 -8 -3 4 184.281 57.7429 10 -8 3 4 173.927 63.9981 7 -8 -3 4 222.883 66.6027 7 -8 -3 4 193.036 56.9560 29 -8 -3 4 289.587 67.0907 28 -8 3 4 332.517 69.5073 28 -8 -3 3 6419.23 310.761 26 -8 3 3 6286.17 314.686 10 -8 -3 3 6600.26 323.216 10 -8 3 3 6216.13 317.307 7 -8 -3 3 6436.24 322.407 7 -8 -3 3 6360.58 303.014 29 -8 -3 3 5900.78 298.710 28 -8 3 3 6391.63 306.145 28 -8 3 3 6245.20 299.112 29 -8 -3 2 3201.30 203.149 26 -8 3 2 3179.47 208.709 10 -8 -3 2 3398.99 214.162 10 -8 3 2 3012.93 207.883 7 -8 -3 2 3398.94 217.494 7 -8 -3 2 3193.53 200.209 29 -8 -3 2 3024.08 195.977 28 -8 3 2 3260.03 201.431 28 -8 3 2 3148.47 194.617 29 -8 -3 1 1478.56 130.575 26 -8 3 1 1318.51 131.412 10 -8 -3 1 1409.10 136.684 10 -8 3 1 1246.05 130.632 7 -8 -3 1 1533.74 141.505 7 -8 -3 1 1285.05 124.204 29 -8 -3 1 1517.36 129.845 28 -8 3 1 1448.25 129.311 28 -8 -3 0 6495.91 306.200 26 -8 3 0 6269.43 311.296 10 -8 -3 0 6357.62 312.535 10 -8 3 0 6152.50 313.553 7 -8 -3 0 6311.72 316.073 7 -8 -3 0 5976.14 294.246 29 -8 -3 0 6093.52 296.094 28 -8 3 0 6650.63 305.308 28 -8 -3 -1 1688.74 136.586 29 -8 -3 -1 1541.43 133.692 28 -8 3 -1 1739.95 139.473 28 -8 3 -1 2061.56 153.784 10 -8 -3 -1 2030.82 154.645 10 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46.2289 7 8 4 -13 307.879 48.1615 9 8 -4 -12 6944.46 274.043 35 -8 -4 12 7152.69 277.065 10 -8 -4 12 6678.94 263.818 28 -8 4 12 6340.88 260.786 28 8 4 -12 6284.58 256.443 23 -8 -4 12 6226.02 266.731 7 8 4 -12 6774.58 274.873 9 8 -4 -11 21.7011 34.7826 35 -8 -4 11 37.4728 35.3368 10 -8 -4 11 20.0718 32.7854 28 -8 4 11 74.2747 35.4519 28 8 4 -11 38.2032 31.7739 23 -8 -4 11 29.7832 36.4835 7 8 -4 -11 15.0307 31.6961 9 8 4 -11 23.2419 34.2675 9 8 -4 -10 533.545 73.9639 35 -8 -4 10 626.462 72.9905 28 -8 4 10 519.579 72.2787 28 -8 -4 10 750.965 85.6708 10 -8 4 10 659.513 79.9125 10 8 4 -10 644.465 75.2526 23 -8 -4 10 744.676 87.4514 7 8 -4 -10 614.952 80.8042 9 8 4 -10 537.179 80.5613 9 -8 -4 9 1448.85 117.864 28 -8 4 9 1593.14 121.554 28 -8 4 9 1703.93 131.103 10 -8 -4 9 1458.81 122.307 10 8 4 -9 1524.44 119.050 23 8 -4 -9 1465.59 123.113 35 8 4 -9 1435.62 120.023 35 -8 4 9 1449.58 122.960 7 -8 -4 9 1480.60 126.288 7 8 -4 -9 1208.76 121.541 9 8 4 -9 1373.71 127.919 9 -8 -4 8 4993.34 244.384 28 -8 4 8 4696.46 240.436 28 8 -4 -8 5048.13 249.948 35 -8 4 8 4687.51 249.838 7 -8 -4 8 4797.49 251.780 7 -8 4 8 5366.58 260.118 10 -8 -4 8 4946.57 254.137 10 -8 -4 7 1292.94 115.425 29 -8 -4 7 1391.27 120.084 28 -8 4 7 1219.33 113.334 28 8 -4 -7 1429.49 123.475 35 -8 4 7 1236.26 119.711 7 -8 -4 7 1374.79 128.287 7 -8 4 7 1321.03 124.989 10 -8 -4 7 1273.34 123.201 10 -8 -4 6 1557.27 131.509 29 -8 -4 6 1683.23 135.040 28 -8 4 6 1721.54 137.488 28 -8 4 6 1458.76 133.357 10 -8 -4 6 1630.24 140.550 10 8 -4 -6 1813.01 137.662 35 -8 4 6 1525.15 136.396 7 -8 -4 6 1692.67 142.699 7 -8 -4 5 9.70945 36.6134 29 -8 -4 5 9.57657 39.3525 28 -8 4 5-9.62318 39.5440 28 -8 4 5 52.9032 43.4784 10 -8 -4 5-10.6908 57.0121 10 -8 -4 5-10.2650 43.2772 26 8 -4 -5-9.17839 44.9606 35 -8 4 5 10.6205 41.2812 7 -8 -4 5 64.8980 50.9839 7 -8 -4 4 2551.80 176.296 26 -8 4 4 2485.86 180.314 10 -8 -4 4 2501.69 178.496 10 -8 -4 4 2625.41 174.733 29 -8 -4 4 2514.10 169.933 28 -8 4 4 2640.80 172.942 28 -8 4 4 2635.98 182.509 7 -8 -4 4 2238.83 171.483 7 -8 -4 3 1876.08 148.867 29 -8 -4 3 1674.75 139.125 28 -8 4 3 1679.63 139.783 28 -8 4 3 1807.23 141.239 29 -8 4 3 2022.83 155.005 10 -8 -4 3 1860.29 153.497 10 -8 -4 3 1735.54 145.161 26 -8 -4 3 1553.48 129.343 20 -8 4 3 1981.49 156.612 7 -8 -4 3 1994.98 158.968 7 -8 -4 2 2298.34 165.826 29 -8 -4 2 2586.55 172.018 28 -8 4 2 2222.51 162.282 28 -8 4 2 2268.86 168.761 10 -8 -4 2 2652.41 180.523 10 -8 -4 2 2397.04 169.546 26 -8 -4 2 2424.14 162.359 20 -8 4 2 2085.84 166.352 7 -8 -4 2 2333.29 172.451 7 -8 -4 1 1098.24 113.696 29 -8 -4 1 992.255 105.455 28 -8 4 1 1021.55 109.660 28 -8 4 1 1388.52 128.315 10 -8 -4 1 1086.17 119.289 10 -8 -4 1 1169.56 117.849 26 -8 -4 1 1169.60 109.124 20 -8 4 1 999.819 113.767 7 -8 -4 1 1190.00 120.657 7 -8 -4 0 510.513 76.6961 28 -8 4 0 677.124 85.5996 28 -8 -4 0 432.577 75.5891 29 -8 4 0 520.712 79.5658 10 -8 -4 0 589.727 87.3859 10 -8 -4 0 608.790 84.0902 26 -8 -4 0 420.654 69.6958 20 -8 4 0 626.203 90.5152 7 -8 -4 0 564.776 89.2975 7 -8 -4 -1 546.346 80.9588 29 -8 4 -1 409.546 74.0983 10 -8 -4 -1 544.444 83.4237 10 -8 -4 -1 463.138 76.2019 28 -8 4 -1 399.931 69.7853 28 -8 -4 -1 418.497 72.9163 26 -8 -4 -1 457.831 75.2384 20 -8 4 -1 602.351 90.1260 7 -8 -4 -1 493.087 80.7773 7 -8 -4 -2 2839.57 176.473 29 -8 4 -2 2954.78 176.936 28 -8 4 -2 2982.99 182.014 10 -8 -4 -2 3235.19 190.510 10 -8 -4 -2 2839.55 176.328 26 -8 -4 -2 3004.37 174.359 20 -8 4 -2 2877.16 186.093 7 -8 -4 -2 2722.19 182.073 7 -8 -4 -3 9549.78 375.696 28 -8 4 -3 10133.5 381.189 28 -8 -4 -3 9717.36 382.527 29 -8 4 -3 10200.1 394.739 10 -8 -4 -3 9816.00 390.484 10 -8 -4 -3 9488.97 377.211 26 -8 -4 -3 10011.5 379.345 20 -8 4 -3 9456.18 392.072 7 -8 -4 -3 10635.8 405.939 7 -8 4 -4 969.242 91.8095 10 -8 -4 -4 829.059 88.4392 10 -8 4 -4 874.867 94.2438 7 -8 -4 -4 1175.47 104.365 7 -8 -4 -4 774.963 80.4701 28 -8 4 -4 960.245 86.6429 28 -8 -4 -5-17.6524 26.0207 28 -8 4 -5 17.4927 29.0891 28 -8 -4 -5 41.5761 27.9984 20 -8 -4 -5 35.4432 37.8041 7 -8 -4 -5 19.5425 28.1440 10 -8 -4 -6 2138.85 117.372 20 8 5 -13 230.284 36.7406 23 8 -5 -13 349.525 46.3816 35 8 5 -12 2963.02 152.461 23 8 -5 -12 3552.92 169.067 35 8 5 -11 5821.56 246.537 23 8 -5 -11 5860.80 254.882 35 8 5 -10 913.848 87.6041 23 8 -5 -10 980.022 92.5599 35 8 -5 -9 3536.45 190.935 35 8 5 -9 3138.61 179.471 35 -8 -5 9 3249.40 185.356 7 8 5 -9 3155.11 180.863 23 -8 -5 8 853.817 95.8670 7 8 -5 -8 912.730 96.8400 35 -8 -5 7 2016.50 146.958 10 8 -5 -7 1749.09 137.069 35 -8 -5 7 2087.89 148.459 7 -8 -5 6 1091.71 105.578 29 -8 -5 6 854.449 99.3523 10 -8 -5 6 895.326 101.657 26 8 -5 -6 896.517 98.0236 35 -8 -5 6 817.393 98.5044 7 -8 -5 5 5394.66 265.211 29 -8 -5 5 4972.92 261.485 10 -8 -5 5 5141.79 265.891 26 -8 -5 5 5401.33 259.804 20 -8 -5 5 5462.90 270.448 7 -8 -5 4 155.194 53.5023 29 -8 -5 4 159.832 51.7707 10 -8 -5 4 88.9024 41.2971 20 -8 -5 4 194.781 57.3471 7 -8 -5 3 7540.92 345.403 29 -8 -5 3 8215.11 355.789 10 -8 -5 3 7800.61 351.572 26 -8 -5 3 8500.98 346.966 20 -8 -5 3 7605.79 350.629 7 -8 -5 2 139.014 53.1331 29 -8 -5 2 169.575 57.3669 10 -8 -5 2 191.234 57.0985 26 -8 -5 2 144.546 48.3757 20 -8 -5 2 165.676 58.7330 7 -8 -5 1 236.778 62.6866 26 -8 -5 1 254.393 61.4864 10 -8 -5 1 167.375 55.2472 29 -8 -5 1 241.577 56.2801 20 -8 -5 0 66.6749 44.9429 26 -8 -5 0 76.7897 42.4917 29 -8 -5 0 78.6401 39.5569 20 -8 -5 -1 1741.36 133.668 26 -8 -5 -1 1606.17 132.635 29 -8 -5 -2 743.003 86.5923 26 -8 -5 -2 725.448 84.3069 29 -8 -5 -2 659.039 83.2519 20 -8 -5 -3 4076.39 208.257 26 -8 -5 -3 4294.72 213.581 29 -8 -5 -3 4466.27 212.198 20 -8 -5 -4 219.418 43.8719 26 -8 -5 -4 190.667 46.3681 20 -8 -5 -4 262.339 49.0628 29 -8 -5 -5 4804.11 208.512 20 -8 -5 -6 112.170 30.6795 20 8 6 -12 150.087 35.5291 23 8 -6 -12 148.441 37.5968 35 8 6 -11 664.265 67.2055 23 8 -6 -11 619.991 69.1013 35 8 6 -10 19.9143 31.9318 23 8 -6 -10 78.2612 36.1391 35 8 6 -9 21.8971 33.7366 23 8 -6 -9 107.248 44.5385 35 -8 -6 8 5148.11 249.562 20 -8 -6 8 5707.83 264.907 26 8 6 -8 5982.44 264.854 23 8 -6 -8 6187.90 269.395 35 -8 -6 7 217.728 52.8556 26 -8 -6 7 181.170 48.4349 20 8 -6 -7 205.516 52.2745 35 -8 -6 6 45.6432 41.2922 26 -8 -6 6 49.7077 37.4785 20 -8 -6 5 1194.64 109.784 20 -8 -6 5 1339.11 120.082 26 -8 -6 5 1313.47 116.171 29 -8 -6 4 4531.02 237.073 20 -8 -6 4 5058.10 254.869 26 -8 -6 4 4817.23 246.673 29 -8 -6 3 38.7368 39.7969 26 -8 -6 3 9.49690 40.0410 29 -8 -6 3 8.89919 34.5933 20 -8 -6 2 6924.44 318.390 20 -8 -6 2 7670.46 330.436 26 -8 -6 2 7053.34 322.880 29 -8 -6 1-9.43098 44.4553 26 -8 -6 1 66.3660 50.5609 29 -8 -6 1 17.5330 36.9611 20 -8 -6 0 979.482 94.9320 20 -8 -6 0 790.732 92.2182 26 -8 -6 0 701.542 90.2790 29 -8 -6 -1 8124.70 339.945 26 -8 -6 -1 8435.24 346.260 29 -8 -6 -1 7805.09 334.282 20 -8 -6 -2 95.2685 41.8072 26 -8 -6 -2 162.916 48.0751 29 -8 -6 -2 122.137 38.9002 20 -8 -6 -3 6195.63 269.171 26 -8 -6 -3 6001.81 267.939 29 -8 -6 -3 6736.69 272.429 20 -8 -6 -4 660.583 68.3305 26 -8 -6 -4 723.474 72.8561 29 -8 -6 -4 662.143 70.5354 20 -8 -6 -5 1248.86 88.0309 20 -8 -6 -5 1068.54 80.4728 26 8 7 -12 2627.89 132.321 23 8 -7 -12 2873.96 140.145 35 8 7 -11 37.8782 28.8713 23 8 -7 -11 28.9838 29.9455 35 8 7 -10 332.315 51.4810 23 8 -7 -10 234.097 48.4876 35 8 7 -9 1107.93 94.1392 23 8 -7 -9 1182.20 97.7766 35 -8 -7 8 900.844 89.6142 26 8 7 -8 1095.32 97.3638 23 8 -7 -8 1020.38 90.7463 32 -8 -7 8 922.547 87.3398 20 8 -7 -8 894.400 88.2066 35 -8 -7 7 16.0666 31.2315 26 8 -7 -7 45.6327 36.5644 32 -8 -7 7 15.2067 31.2503 20 -8 -7 6 33.9453 43.1216 26 -8 -7 6 96.0543 39.9720 20 -8 -7 5 264.388 59.6845 26 -8 -7 5 215.908 52.3309 20 -8 -7 4 27.0551 37.0707 26 -8 -7 4 34.8558 37.6571 29 -8 -7 4 42.4611 33.9792 20 -8 -7 3 12180.7 454.379 20 -8 -7 3 11899.3 457.195 26 -8 -7 3 11323.3 448.629 29 -8 -7 2 836.292 88.2350 20 -8 -7 2 615.223 79.9801 26 -8 -7 2 741.481 88.9721 29 -8 -7 1 8.85528 33.3920 26 -8 -7 1-7.73610 33.4204 31 -8 -7 1 8.96945 34.8635 29 -8 -7 1-16.7564 35.3221 20 -8 -7 0 1173.42 104.379 20 -8 -7 0 1013.56 102.769 26 -8 -7 0 975.902 98.6549 29 -8 -7 -1 64.2142 39.3626 26 -8 -7 -1 115.719 43.4244 29 -8 -7 -1 38.4216 35.5371 20 -8 -7 -2-7.37904 29.5132 26 -8 -7 -2 30.4321 32.0751 29 -8 -7 -2-21.4008 29.3134 20 -8 -7 -3 4865.96 221.159 26 -8 -7 -3 5165.51 228.241 29 -8 -7 -3 4952.75 220.959 20 -8 -7 -4 1637.60 105.613 26 -8 -7 -5 149.593 34.1046 20 -8 -7 -5 153.964 33.5993 26 8 -8 -11 45.4490 29.7578 35 -8 -8 11 26.6207 27.7743 20 8 8 -11 67.2597 26.4401 23 8 -8 -10 3769.90 177.936 35 8 8 -10 3689.57 174.100 23 8 -8 -9 300.923 53.1190 35 8 8 -9 307.717 51.1901 23 -8 -8 9 259.040 49.8108 20 8 8 -8 3415.19 172.354 23 8 -8 -8 2920.74 160.858 32 8 -8 -7 7.08984 34.7404 32 8 8 -7 49.9471 30.8373 23 -8 -8 7 42.7764 32.2446 20 -8 -8 6 214.839 48.8560 26 8 -8 -6 252.453 53.7875 32 -8 -8 6 165.482 48.9466 20 -8 -8 5 88.3474 40.7895 26 -8 -8 5 7.80969 34.5509 20 -8 -8 4 638.558 78.4896 20 -8 -8 4 652.421 78.4817 26 -8 -8 3 100.271 42.4498 26 -8 -8 3-7.91535 40.9010 31 -8 -8 3 32.9260 33.8616 29 -8 -8 3 128.654 43.5737 20 -8 -8 2 5520.31 249.511 20 -8 -8 2 4955.69 246.427 26 -8 -8 2 5133.71 247.553 29 -8 -8 1 162.653 46.8306 26 -8 -8 1 124.002 45.6425 29 -8 -8 1 187.017 49.4633 20 -8 -8 0 2213.41 140.054 20 -8 -8 0 2083.30 141.893 26 -8 -8 0 2108.79 142.375 29 -8 -8 -1 278.258 52.6335 26 -8 -8 -1 211.959 53.9073 29 -8 -8 -1 316.566 54.3766 20 -8 -8 -2 461.185 61.6937 26 -8 -8 -2 650.566 72.4983 29 -8 -8 -2 593.837 66.4604 20 -8 -8 -3 6172.87 248.115 20 -8 -8 -3 5838.95 247.250 26 -8 -8 -4 1379.99 90.3802 20 -8 -8 -4 1315.02 89.5762 26 8 9 -11 4332.55 176.378 23 8 -9 -10 759.168 67.7057 35 8 9 -10 720.420 62.9723 23 8 9 -9 2392.43 131.265 23 -8 -9 8 1939.09 122.477 20 8 9 -8 2029.32 122.544 23 8 -9 -8 2155.39 123.388 32 -8 -9 7 1907.44 121.968 20 8 -9 -7 1694.96 115.199 32 8 9 -7 1764.09 118.419 23 -8 -9 6 1874.97 124.486 20 -8 -9 6 1752.53 123.242 31 8 -9 -6 1858.98 125.113 32 -8 -9 5 720.999 79.3003 20 -8 -9 5 776.964 81.8461 31 8 -9 -5 1012.50 94.4005 32 -8 -9 5 790.939 81.5613 26 -8 -9 4 1238.52 103.028 31 8 -9 -4 1453.49 112.693 32 -8 -9 4 1207.79 102.384 26 -8 -9 3 14288.3 505.193 20 -8 -9 3 14193.9 504.133 31 8 -9 -3 14946.2 510.566 32 -8 -9 3 14445.4 508.500 26 -8 -9 2 4178.83 209.934 29 8 -9 -2 4121.37 206.818 32 -8 -9 2 4680.17 218.820 26 -8 -9 1 2782.31 159.265 20 -8 -9 1 2952.98 164.330 29 8 -9 -1 2925.08 156.868 32 -8 -9 1 2574.17 156.325 26 -8 -9 0 2904.26 158.470 20 -8 -9 0 2586.22 155.726 29 -8 -9 0 3003.96 162.003 26 -8 -9 -1 765.190 78.4263 29 -8 -9 -1 628.550 68.9651 20 -8 -9 -1 782.966 76.7610 26 -8 -9 -2 22.4677 25.9417 20 -8 -9 -2-5.85819 25.3086 26 -8 -9 -3 2943.21 141.259 20 -8 -9 -3 2799.15 141.402 26 -8 -10 9 1059.82 77.2166 31 8 10 -9 958.163 72.9972 23 -8 -10 8 1499.30 97.8008 31 8 -10 -8 1187.14 86.0796 32 -8 -10 8 1207.01 90.2652 20 8 10 -8 1369.50 92.5707 23 8 -10 -7 181.909 40.3134 32 -8 -10 7 142.934 39.9123 31 8 10 -7 165.334 38.5108 23 -8 -10 7 120.024 34.7442 20 8 -10 -6 440.497 60.5711 32 -8 -10 6 479.143 60.9260 31 -8 -10 6 479.901 61.5394 20 8 10 -6 563.310 62.2406 23 -8 -10 5 1086.97 90.6754 31 8 -10 -5 989.939 88.4101 32 -8 -10 4 4834.91 216.990 20 -8 -10 4 4827.83 218.408 31 8 -10 -4 4585.14 215.018 32 -8 -10 3 1992.03 125.598 20 -8 -10 3 1946.71 125.537 31 8 -10 -3 2076.67 128.553 32 -8 -10 3 1798.55 120.239 26 -8 -10 2 4852.56 216.444 20 -8 -10 2 4828.78 215.827 31 8 -10 -2 4705.32 212.896 32 -8 -10 2 4768.51 216.865 26 -8 -10 1-5.98124 26.4570 31 -8 -10 1 12.6210 32.0443 29 -8 -10 1 61.2349 30.0043 20 -8 -10 1 55.8153 34.5953 26 -8 -10 0 1568.04 103.936 31 -8 -10 0 1738.81 112.565 29 -8 -10 0 1689.53 107.962 20 -8 -10 0 1642.87 109.329 26 -8 -10 -1 2940.81 143.186 31 -8 -10 -1 2783.87 145.283 26 -8 -10 -2 148.569 33.4386 20 -8 -10 -2 63.6497 27.0446 26 -8 -11 8 711.586 59.9900 31 -8 -11 8 600.464 57.2102 20 -8 -11 7 328.549 48.4479 20 8 -11 -7 451.602 52.4683 32 -8 -11 7 476.224 54.1617 31 -8 -11 6 3454.35 164.690 31 8 -11 -6 3492.99 164.873 32 -8 -11 5 1254.06 92.0300 31 8 -11 -5 1297.86 93.0760 32 -8 -11 4 747.498 68.7857 20 -8 -11 4 796.724 72.7505 31 8 -11 -4 562.743 62.9106 32 -8 -11 3 3160.25 158.203 20 -8 -11 3 3273.24 161.257 31 8 -11 -3 3321.25 160.855 32 -8 -11 2 1220.36 87.8646 20 -8 -11 2 1345.14 93.2280 31 8 -11 -2 1104.23 83.5158 32 -8 -11 1 1976.35 113.438 31 -8 -11 1 1769.06 107.441 20 -8 -11 1 1865.07 110.074 26 -8 -11 0 1857.43 107.868 31 8 11 0 2134.45 121.174 22 -8 -11 0 2011.89 111.335 20 -8 -11 0 2075.80 113.269 26 -8 -11 -1 1718.38 98.2103 31 -8 -11 -1 1992.13 103.754 20 -8 -11 -1 1775.31 100.207 26 -8 -12 6 107.721 29.1155 20 -8 -12 5 6652.36 248.409 31 8 12 -5 6652.49 262.527 22 -8 -12 5 6685.94 247.459 20 -8 -12 4 141.556 31.7965 20 -8 -12 4 210.925 37.6982 31 8 12 -4 141.924 39.2139 22 -8 -12 3 32.1124 22.9073 31 8 12 -3-5.71574 27.4945 22 -8 -12 2 59.1289 21.8788 20 8 12 -2 43.6593 30.9188 22 -8 -12 2 84.6161 24.9001 31 -8 -12 1 422.484 45.9182 31 -9 0 10-5.32370 22.4444 28 9 0 -10 4.96553 23.8689 35 -9 0 10 5.91185 22.2927 7 9 0 -10-23.2547 29.0007 9 -9 0 10 29.3186 28.7233 10 -9 0 9 383.629 51.1758 29 -9 0 9 450.013 57.2981 28 -9 0 9 410.416 59.1907 10 9 0 -9 343.198 51.7250 35 -9 0 9 427.105 62.2540 7 9 0 -9 363.625 57.4531 9 -9 0 8 41.4991 34.4538 29 -9 0 8 13.1203 30.9238 28 -9 0 8 36.2094 32.7432 10 -9 0 8-6.32491 27.9694 26 9 0 -8 6.10890 28.7971 35 -9 0 8-14.7105 33.9709 7 9 0 -8 43.8555 35.8061 9 -9 0 7 645.371 69.4036 29 -9 0 7 734.993 76.7331 28 -9 0 7 564.555 74.4464 10 -9 0 7 466.604 64.0061 26 9 0 -7 468.838 62.3916 35 -9 0 7 479.114 71.0745 7 9 0 -7 569.070 76.3820 9 -9 0 6 29.2839 30.8651 28 -9 0 6 20.4974 31.5550 29 -9 0 6 8.10575 35.8416 10 -9 0 6-6.86351 30.3489 26 9 0 -6 13.1534 36.6798 35 -9 0 6-16.5782 35.8096 7 -9 0 5 905.467 85.4208 29 -9 0 5 963.778 91.0832 28 -9 0 5 717.820 85.3563 10 -9 0 5 815.290 82.3009 26 9 0 -5 750.022 78.6878 35 -9 0 5 1014.71 99.6724 7 -9 0 4 22.8633 34.4558 28 -9 0 4 7.18266 32.4736 29 9 0 -4-19.2481 28.3700 35 -9 0 4 8.44826 39.8215 10 -9 0 4-35.0669 45.2667 7 -9 0 3 29521.0 924.562 10 -9 0 3 28897.8 904.894 29 -9 0 3 28884.5 907.790 28 -9 0 3 28030.6 922.966 7 -9 0 2 24.6355 35.4765 10 -9 0 2 6.92208 30.6087 29 -9 0 2 37.1096 37.6795 28 -9 0 2-25.8843 35.4555 7 -9 0 1 2855.91 168.052 10 -9 0 1 2907.32 174.421 7 -9 0 1 2642.24 151.407 29 -9 0 0-6.68870 28.8957 28 -9 0 0-7.37087 35.4312 10 -9 0 0 7.87304 36.3604 7 -9 0 -1 274.220 47.9774 28 -9 0 -1 154.676 42.8183 10 -9 0 -1 130.502 45.0936 7 -9 0 -2-10.7384 27.2579 28 -9 0 -2 6.41161 28.3506 7 -9 0 -2-5.91840 27.3335 10 -9 1 10 3499.43 156.978 29 -9 -1 10 3355.80 163.578 28 -9 1 10 3191.58 159.588 28 -9 1 10 3389.55 167.633 10 -9 -1 10 3655.07 172.471 10 9 -1 -10 3244.47 157.942 35 9 -1 -10 3861.18 173.778 9 9 1 -10 3814.42 173.898 9 -9 1 10 3513.57 170.557 7 -9 1 9 1120.54 85.7359 29 -9 -1 9 1388.50 90.2268 29 -9 -1 9 1041.47 88.4589 28 -9 1 9 1045.35 88.7420 28 -9 1 9 1322.72 101.715 10 -9 -1 9 1295.70 100.608 10 -9 -1 9 1179.41 91.9193 26 9 -1 -9 1274.89 92.6392 35 9 1 -9 1305.49 93.2559 35 9 -1 -9 1341.76 101.319 9 9 1 -9 1174.25 97.3447 9 -9 1 9 1241.36 99.6758 7 -9 -1 9 1257.59 98.7302 7 -9 1 8 7227.17 277.217 29 -9 -1 8 6799.83 270.273 29 -9 -1 8 6432.82 274.415 28 -9 1 8 6713.29 277.600 28 -9 1 8 7142.90 289.803 10 -9 -1 8 7040.07 289.000 10 -9 1 8 6546.64 272.701 26 -9 -1 8 6766.73 277.509 26 9 -1 -8 6953.14 275.717 35 9 1 -8 7205.05 278.509 35 9 -1 -8 7259.97 293.878 9 9 1 -8 6742.93 289.434 9 -9 1 8 6660.57 286.436 7 -9 -1 8 6819.80 288.336 7 -9 -1 7 240.628 49.2511 28 -9 1 7 337.916 56.5770 28 -9 1 7 395.406 58.6004 29 -9 -1 7 335.580 50.6688 29 -9 1 7 235.581 54.7608 10 -9 -1 7 312.599 58.1347 10 -9 1 7 262.311 47.8781 26 -9 -1 7 343.606 55.6673 26 9 -1 -7 295.702 52.0737 35 9 1 -7 284.254 53.4334 35 -9 1 7 388.142 60.9514 7 -9 -1 7 336.286 60.9518 7 9 -1 -7 325.903 61.3639 9 9 1 -7 382.796 68.8314 9 -9 -1 6 93.6179 37.8043 28 -9 1 6 14.4423 36.0276 28 -9 1 6-6.82673 29.4991 29 -9 -1 6 54.0054 34.8629 29 -9 1 6 15.9423 33.6122 10 -9 -1 6 7.99651 36.9363 10 -9 -1 6 55.8728 37.2505 26 9 -1 -6 32.0846 33.1400 35 9 1 -6-6.64502 36.5330 35 -9 1 6 24.4139 39.1240 7 -9 -1 6 24.5742 40.1307 7 -9 1 5 5820.59 251.717 29 -9 -1 5 5625.05 249.269 29 -9 -1 5 5995.48 259.111 28 -9 1 5 5891.12 257.806 28 -9 1 5 5280.26 258.007 10 -9 -1 5 6269.06 271.055 10 -9 -1 5 5781.42 253.549 26 9 -1 -5 5165.88 237.155 35 9 1 -5 5627.98 246.207 35 -9 1 5 5635.63 264.468 7 -9 -1 5 5617.53 265.722 7 -9 1 4 3518.06 183.059 29 -9 -1 4 3416.52 180.621 29 -9 -1 4 3279.00 180.744 28 -9 1 4 3654.36 186.899 28 -9 1 4 3458.23 192.639 10 -9 -1 4 3552.67 194.230 10 -9 -1 4 3444.71 179.880 26 9 1 -4 3213.20 172.374 35 -9 1 4 3498.86 194.567 7 -9 -1 4 2876.12 181.187 7 -9 1 3 97.2949 44.7852 28 -9 1 3 147.353 45.5089 29 -9 -1 3 114.432 41.7366 29 -9 -1 3 171.825 46.3390 28 9 1 -3 143.936 41.8901 35 -9 1 3 173.621 48.8228 10 -9 -1 3 58.0664 42.2841 10 -9 1 3 163.941 50.2872 7 -9 -1 3 242.737 54.3444 7 -9 1 2 7623.91 319.971 10 -9 -1 2 7756.11 322.067 10 -9 1 2 7311.08 301.638 29 -9 -1 2 7982.84 312.174 29 -9 -1 2 8000.84 315.772 28 -9 1 2 7990.98 315.888 28 -9 1 2 6904.80 317.279 7 -9 -1 2 7845.68 329.395 7 -9 1 1 1894.25 132.596 10 -9 -1 1 2017.90 134.826 10 -9 -1 1 1885.09 123.279 29 -9 1 1 1551.69 126.327 7 -9 -1 1 2027.42 139.000 7 -9 1 0 6772.04 274.629 10 -9 -1 0 6328.55 269.938 10 -9 1 0 6231.19 274.210 7 -9 -1 0 6431.26 275.484 7 -9 -1 0 6597.28 256.821 29 -9 1 0 5746.11 253.883 28 -9 -1 -1 17.9542 27.6398 28 -9 1 -1 11.9727 29.3242 28 -9 1 -1-6.58922 26.3545 10 -9 -1 -1 13.2431 32.4357 10 -9 1 -1 21.3300 30.7158 7 -9 -1 -1-28.5280 41.9880 7 -9 -1 -2 31.5740 23.2737 28 -9 1 -2 15.7809 23.2648 28 -9 1 -2 18.8217 28.3691 7 -9 -1 -2 31.4541 31.3848 7 -9 1 -2-5.78223 25.5721 10 -9 -1 -2 40.7128 26.8652 10 -9 -2 10 284.783 43.2111 26 -9 2 10 252.632 39.3466 29 -9 -2 10 282.778 41.6907 28 -9 2 10 196.380 41.7177 28 -9 2 9 10446.9 360.874 29 -9 -2 9 10020.1 360.517 28 -9 2 9 9120.54 354.997 28 -9 2 9 10068.5 369.191 10 -9 -2 9 10191.7 369.615 10 -9 -2 9 10319.8 364.667 26 9 -2 -9 10466.8 362.271 35 9 2 -9 9947.47 358.658 35 9 -2 -9 10612.4 372.487 9 9 2 -9 10176.4 369.986 9 -9 2 9 10140.5 369.959 7 -9 -2 9 10493.5 374.298 7 -9 2 8 2029.03 120.915 29 -9 -2 8 1854.37 113.667 29 -9 -2 8 2022.33 123.134 28 -9 2 8 1678.63 115.205 28 -9 2 8 1947.00 125.528 10 -9 -2 8 2159.37 131.597 10 -9 -2 8 1885.43 120.379 26 9 -2 -8 1942.37 119.791 35 9 2 -8 1882.26 119.099 35 9 2 -8 1832.58 128.290 9 -9 2 8 1763.69 124.020 7 -9 -2 8 1815.84 124.650 7 -9 -2 7 157.102 42.9225 28 -9 2 7 164.597 43.6134 28 -9 2 7 173.237 42.5111 29 -9 -2 7 134.767 36.7210 29 -9 2 7 123.020 43.3133 10 -9 -2 7 167.473 44.1175 10 -9 -2 7 252.324 47.4127 26 9 -2 -7 139.575 38.1382 35 9 2 -7 108.801 37.3869 35 -9 2 7 117.946 44.6598 7 -9 -2 7 82.3164 42.4984 7 9 -2 -7 88.5396 37.6500 9 9 2 -7 149.954 50.1244 9 -9 2 6 981.955 88.4455 29 -9 -2 6 842.188 80.4646 29 -9 -2 6 1030.77 89.9809 28 -9 2 6 780.524 81.0109 28 -9 2 6 980.558 92.9353 10 -9 -2 6 841.823 86.8862 10 -9 -2 6 761.794 80.9401 26 9 -2 -6 992.628 83.7339 35 9 2 -6 974.042 86.1162 35 -9 2 6 1015.55 96.4579 7 -9 -2 6 965.753 95.4918 7 -9 2 5 2597.03 152.332 29 -9 -2 5 2710.72 155.063 29 -9 -2 5 2662.92 155.133 28 -9 2 5 3165.93 164.931 28 -9 2 5 2689.37 162.810 10 -9 -2 5 3054.93 172.247 10 -9 -2 5 2651.66 156.090 26 9 -2 -5 2776.79 149.980 35 9 2 -5 2927.96 159.760 35 -9 2 5 2540.41 162.876 7 -9 -2 5 2812.94 169.493 7 -9 -2 4 49.4710 33.9859 26 -9 2 4-7.94114 37.4438 10 -9 -2 4 39.9788 37.7012 10 -9 2 4 16.4512 41.0438 7 -9 -2 4 33.2516 42.2132 7 -9 -2 4 64.5775 38.2767 28 -9 2 4 36.0163 32.5813 28 -9 2 4 62.1457 37.9692 29 -9 -2 4 35.2192 33.2160 29 -9 -2 3 462.298 63.3654 26 -9 -2 3 556.613 72.6518 10 -9 2 3 418.448 68.6111 10 -9 2 3 521.484 72.6623 7 -9 -2 3 324.276 64.0086 7 -9 -2 3 550.032 67.2177 28 -9 2 3 486.407 63.3879 29 -9 -2 3 493.696 64.7118 29 -9 2 3 444.336 63.9561 28 -9 -2 2-13.9731 31.5871 28 -9 2 2 7.00502 33.0189 28 -9 -2 2 26.2373 34.9798 26 -9 2 2 7.70334 35.5768 10 -9 -2 2 7.76174 30.1694 10 -9 2 2-16.2627 40.5625 7 -9 -2 2 32.8091 36.2684 7 -9 2 2 19.2408 27.0397 29 -9 -2 2-13.8161 28.3867 29 -9 -2 1 194.033 47.7084 28 -9 2 1 194.401 47.7969 28 -9 2 1 323.619 55.4697 10 -9 -2 1 229.885 53.6908 10 -9 -2 1 276.350 53.0882 29 -9 2 1 250.106 54.5868 7 -9 -2 1 378.138 63.3975 7 -9 2 0 1736.36 118.478 10 -9 -2 0 2064.08 128.516 10 -9 2 0 1775.80 123.896 7 -9 -2 0 1995.56 130.560 7 -9 -2 0 1716.96 112.182 29 -9 -2 0 1400.92 107.915 28 -9 2 0 1521.39 110.559 28 -9 -2 -1 368.227 53.0550 28 -9 2 -1 373.907 51.6957 28 -9 2 -1 261.109 46.9725 10 -9 -2 -1 345.578 53.0423 10 -9 2 -1 221.652 48.6020 7 -9 -2 -1 398.875 58.0255 7 -9 -2 -2 1776.08 105.470 28 -9 2 -2 1521.64 98.8701 28 -9 -3 10 93.3549 29.4404 26 -9 3 10 212.608 36.3883 29 -9 3 9 2629.92 145.132 28 -9 3 9 3311.92 157.088 29 -9 3 9 2979.78 154.349 10 -9 -3 9 3292.72 159.401 10 -9 -3 9 3314.62 157.876 26 9 -3 -9 3516.19 158.392 35 9 3 -9 3306.10 155.912 35 9 -3 -9 3304.46 160.762 9 9 3 -9 3080.10 158.711 9 -9 3 9 2887.90 154.064 7 -9 -3 9 3357.35 163.024 7 -9 -3 8 117.398 34.6817 28 -9 3 8 39.4404 28.2575 28 -9 3 8 145.745 38.5815 29 -9 3 8 166.163 42.7331 10 -9 -3 8 74.8675 31.8075 10 -9 -3 8 95.2601 31.3863 26 9 -3 -8 127.031 36.9324 35 9 3 -8 143.730 38.0511 35 -9 3 8 99.9789 33.9654 7 -9 -3 8 141.507 42.5460 7 9 -3 -8 74.6666 32.7895 9 9 3 -8 179.371 44.4743 9 9 -3 -7 229.938 44.3872 35 9 3 -7 198.876 43.8170 35 -9 -3 7 229.139 45.4728 28 -9 3 7 188.301 45.0797 28 -9 3 7 162.226 40.2928 29 -9 -3 7 191.885 41.7698 29 -9 3 7 192.830 45.1212 10 -9 -3 7 175.109 44.8024 10 -9 -3 7 159.953 41.7355 26 9 3 -7 240.038 42.7476 23 -9 3 7 304.264 55.4901 7 -9 -3 7 325.577 54.9287 7 9 -3 -7 203.139 48.9425 9 9 3 -7 181.368 46.3787 9 -9 -3 6 611.983 68.7796 29 -9 -3 6 673.618 70.5337 28 -9 3 6 614.058 69.1532 28 -9 3 6 546.134 67.2190 29 -9 3 6 582.504 73.4491 10 -9 -3 6 603.739 73.0739 10 -9 -3 6 684.722 71.5492 26 9 -3 -6 540.270 63.4231 35 9 3 -6 603.959 67.9792 35 -9 3 6 532.673 68.1765 7 -9 -3 6 698.373 76.7632 7 -9 -3 5 89.6105 37.9273 26 -9 3 5 65.2552 39.3004 10 -9 -3 5 22.0102 39.1605 10 -9 3 5 46.3150 31.8479 29 -9 -3 5 66.3973 37.0681 29 -9 -3 5 85.3643 37.6908 28 -9 3 5 72.6380 34.7000 28 -9 3 5 52.4889 36.0825 7 -9 -3 5 45.8409 41.4084 7 -9 -3 4 865.960 83.0323 26 -9 3 4 822.345 84.5943 10 -9 -3 4 795.773 83.8706 10 -9 3 4 716.377 75.3587 29 -9 -3 4 812.524 80.3919 29 -9 -3 4 838.930 81.7438 28 -9 3 4 789.325 77.8704 28 -9 3 4 803.194 87.5952 7 -9 -3 4 933.605 91.3803 7 -9 -3 3 129.353 39.1666 26 -9 3 3 94.8150 39.6234 10 -9 -3 3 103.389 39.5085 10 -9 -3 3 119.243 39.6235 28 -9 3 3 69.8570 36.0593 29 -9 -3 3 185.140 45.8176 29 -9 3 3 126.333 39.2719 28 -9 3 3 122.434 44.5804 7 -9 -3 3 116.569 46.4414 7 -9 -3 2 912.724 84.2175 26 -9 3 2 1029.18 90.2283 10 -9 -3 2 1078.87 93.3190 10 -9 -3 2 982.849 87.1541 29 -9 -3 2 892.264 82.9232 28 -9 3 2 901.120 84.0149 28 -9 3 2 1132.90 95.9855 7 -9 -3 2 920.808 90.3970 7 -9 -3 1 792.993 73.0836 26 -9 -3 1 339.334 60.0839 28 -9 3 1 451.056 61.5602 28 -9 3 1 709.596 74.9580 10 -9 -3 1 726.767 75.7220 10 -9 3 1 671.473 76.5951 7 -9 -3 1 618.791 74.4048 7 -9 -3 1 623.482 68.3156 29 -9 3 0 16443.4 558.585 10 -9 -3 0 17369.9 564.353 10 -9 -3 0 16310.8 552.785 29 -9 -3 0 17378.4 557.801 28 -9 3 0 16567.5 566.320 7 -9 -3 0 17649.3 570.974 7 -9 -3 -1 36.0145 25.6672 28 -9 3 -1 10.2726 25.1625 28 -9 3 -1 28.0798 28.5125 10 -9 -3 -1 45.7866 29.0575 10 -9 -3 -1-5.16989 27.1380 29 -9 3 -1-6.10494 31.5245 7 -9 -3 -1-6.14691 27.1821 7 -9 -4 9 59.4935 28.0601 26 9 4 -9 16.6151 21.8248 23 -9 4 9 45.2636 27.6633 29 9 -4 -8 440.158 54.3085 35 9 4 -8 423.651 53.3287 35 -9 4 8 377.983 53.6903 29 -9 -4 8 401.832 52.1659 10 -9 -4 8 350.353 50.2785 26 9 4 -8 395.066 48.6246 23 -9 -4 8 443.325 55.3740 7 9 4 -8 261.816 47.9299 9 -9 -4 7 1074.75 82.8725 28 -9 4 7 925.239 79.2066 28 -9 4 7 930.322 81.9166 29 -9 -4 7 983.928 82.6365 10 -9 -4 7 1079.21 86.2457 26 9 -4 -7 940.706 79.0033 35 9 4 -7 1103.29 87.2785 35 9 4 -7 969.098 87.1635 9 -9 -4 7 853.159 81.3169 7 -9 4 6 1399.42 103.290 29 -9 -4 6 1534.10 103.162 29 -9 -4 6 1469.21 101.484 28 -9 4 6 1437.16 99.3557 28 -9 -4 6 1431.06 106.459 10 -9 -4 6 1477.13 107.898 26 9 4 -6 1703.91 111.332 35 -9 -4 6 1509.21 108.871 7 -9 -4 5 3850.81 193.754 26 -9 -4 5 4165.04 198.739 10 -9 4 5 4298.37 196.033 29 -9 -4 5 4088.87 194.409 29 -9 -4 5 4144.79 190.833 28 -9 4 5 4210.99 191.074 28 -9 -4 5 4230.65 202.888 7 -9 -4 4 364.863 57.2800 26 -9 -4 4 327.347 54.4915 10 -9 -4 4 358.019 54.6355 28 -9 4 4 334.340 51.9728 29 -9 4 4 233.468 44.1924 28 -9 -4 4 266.620 49.0305 29 -9 -4 4 391.828 62.1222 7 -9 -4 3 5506.53 247.759 26 -9 -4 3 5722.23 250.570 10 -9 -4 3 6255.12 256.650 29 -9 -4 3 6106.88 247.419 28 -9 4 3 6331.10 249.361 28 -9 -4 3 5735.25 254.186 7 -9 -4 2 86.5369 34.4546 28 -9 4 2 28.8506 29.8603 28 -9 -4 2 132.291 37.1405 26 -9 -4 2 70.7795 34.3717 10 -9 -4 2 45.0787 34.9315 29 -9 -4 2 102.492 39.2320 7 -9 -4 1 2331.02 131.736 26 -9 -4 1 2332.67 133.491 10 -9 -4 1 2288.33 134.172 29 -9 -4 1 1913.44 120.640 28 -9 -4 1 2435.53 140.403 7 -9 -4 0 79.3513 29.9537 26 -9 -4 0 55.9802 31.6937 10 -9 -4 0 17.9490 28.7925 7 -9 -4 0 50.9517 29.7468 29 -9 -4 -1 6806.89 258.167 29 -9 5 9 310.518 44.0783 29 9 5 -8 2811.62 139.469 23 -9 -5 8 2868.45 145.317 26 -9 5 8 3113.36 148.826 29 -9 -5 7 77.5235 31.7687 26 9 -5 -7 14.0314 22.0684 32 -9 5 7 59.9661 28.6310 29 9 5 -7 40.1831 25.5190 23 9 5 -7 10.8636 29.8749 35 -9 -5 6 648.562 66.6549 26 -9 5 6 689.929 68.7304 29 -9 -5 6 668.449 64.8676 29 9 5 -6 666.068 67.2353 35 -9 -5 5 446.688 57.5507 26 -9 -5 5 528.554 60.2396 29 -9 5 5 391.947 52.3653 29 -9 -5 4 967.862 82.1838 26 -9 -5 4 871.516 79.7500 29 -9 -5 3 2376.74 136.076 26 -9 -5 3 2325.27 135.569 29 -9 -5 2 29.6263 24.9855 26 -9 -5 2 6.02294 26.0243 29 -9 -5 1 127.582 36.0098 26 -9 -5 1 120.633 33.5541 29 -9 -5 0 2458.05 131.739 26 -9 -5 0 2626.00 136.058 29 9 6 -8 381.049 45.8112 23 -9 -6 8 346.002 43.0750 31 -9 6 8 397.891 47.9844 29 9 6 -7 13.9029 22.2768 23 -9 -6 7 9.81879 21.7080 26 -9 -6 7-18.3322 24.4406 31 -9 6 7-9.59761 25.1881 29 9 6 -6 602.143 62.6286 35 -9 6 6 587.865 59.8620 29 -9 -6 6 588.732 57.8160 31 9 -6 -6 584.337 58.7255 32 9 6 -6 647.882 62.7834 23 -9 -6 6 656.559 64.5320 26 -9 -6 5 1099.87 80.8865 31 -9 -6 5 1157.50 83.9075 29 9 -6 -5 1127.97 84.5671 32 -9 -6 5 1102.37 85.7353 26 -9 -6 4-5.45063 24.6449 29 -9 -6 4-16.9254 29.6143 26 -9 -6 3 38.8514 26.7007 29 -9 -6 3 39.2009 28.4500 26 -9 -6 2 710.476 67.3833 29 -9 -6 2 680.635 62.4922 20 -9 -6 2 822.065 71.6285 26 -9 -6 1 936.593 74.7492 29 -9 -6 1 784.792 66.1040 20 -9 -6 1 834.845 72.1012 26 -9 -6 0 787.569 66.2129 29 -9 -6 0 563.261 57.0725 26 9 7 -7 258.579 38.3710 23 -9 -7 6 1353.26 86.1202 31 -9 -7 6 1417.43 89.9687 26 9 7 -6 1443.04 89.5558 23 -9 -7 5 944.843 70.6021 31 -9 -7 5 968.174 74.4975 26 -9 -7 4 761.156 66.1184 26 -9 -7 4 784.009 64.2236 29 9 -7 -4 699.279 62.7035 32 -9 -7 3 723.460 63.5183 26 -9 -7 3 711.627 62.8206 29 -9 -7 2 1477.55 94.0335 26 -9 -7 2 1305.66 86.2663 20 -9 -7 2 1626.37 97.2575 29 -9 -7 1 2922.96 138.008 26 0 0 0 0.00 0.00 0 TITL harry_ACT_HCl_smart in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 7.795531 18.364163 16.395440 90.0000 102.2495 90.0000 ZERR 12.00 0.000056 0.000161 0.000118 0.0000 0.0007 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Cl UNIT 96.00 120.00 12.00 12.00 12.00 REM CrysAlisPro recorded range (K): Min=99.6; max=100.3; aver:99.9 TEMP -173 TREF HKLF 4 END ; _shelx_hkl_checksum 10026 _shelx_res_file ; TITL shelx.res created by SHELXL-2018/3 at 12:20:14 on 01-May-2024 CELL 1.54184 7.7936 18.3639 16.3922 90.000 102.245 90.000 ZERR 6.00 0.0001 0.0002 0.0001 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC CL O N C H UNIT 6 12 12 96 114 MERG 2 OMIT -3.00 180.00 MORE -1 EQIV $1 -x+1, -y+1, -z+2 HTAB N1 Cl2_$1 HTAB N2 Cl1 HTAB N3 Cl2 HTAB O1 O2 EQIV $2 -x, -y+1, -z+1 HTAB O3 O3_$2 dfix .88 .01 o1 h1h o3 h2h FMAP 2 PLAN 20 ACTA 140.00 BOND $H CONF L.S. 4 TEMP -173.00 WGHT 0.049100 0.751500 FVAR 2.97040 CL1 1 -0.500000 0.500000 0.500000 10.50000 0.02145 0.02864 = 0.01870 0.01083 -0.00286 0.00005 CL2 1 0.483093 0.513875 0.839536 11.00000 0.01927 0.02283 = 0.01485 0.00524 -0.00154 0.00253 O1 2 0.067587 0.552048 0.892252 11.00000 0.01794 0.01310 = 0.01354 -0.00050 -0.00322 -0.00025 O2 2 -0.072765 0.464512 0.784591 11.00000 0.01893 0.01572 = 0.01404 -0.00154 -0.00374 -0.00132 O3 2 0.055476 0.545739 0.552875 11.00000 0.02088 0.01454 = 0.01577 -0.00288 -0.00497 -0.00022 N1 3 0.265207 0.561320 1.013597 11.00000 0.01587 0.01155 = 0.01188 0.00096 -0.00148 0.00053 N2 3 -0.254323 0.436027 0.661440 11.00000 0.01483 0.01326 = 0.01223 0.00092 -0.00131 0.00113 N3 3 0.226947 0.568687 0.678555 11.00000 0.01773 0.01294 = 0.01248 0.00142 -0.00206 -0.00073 C1 4 0.267594 0.639486 1.016641 11.00000 0.01309 0.01076 = 0.01317 -0.00074 -0.00297 -0.00041 C2 4 0.328389 0.678771 0.956151 11.00000 0.01659 0.01585 = 0.01259 -0.00087 -0.00032 -0.00022 AFIX 43 H2 5 0.363096 0.654464 0.911101 11.00000 -1.20000 AFIX 0 C3 4 0.337697 0.754152 0.962499 11.00000 0.01973 0.01624 = 0.01545 0.00287 0.00077 -0.00234 AFIX 43 H3 5 0.378720 0.781593 0.921355 11.00000 -1.20000 AFIX 0 C4 4 0.287441 0.789850 1.028624 11.00000 0.01860 0.01187 = 0.01976 -0.00105 -0.00132 -0.00080 AFIX 43 H4 5 0.293194 0.841450 1.032342 11.00000 -1.20000 AFIX 0 C5 4 0.228837 0.749650 1.089146 11.00000 0.01775 0.01684 = 0.01555 -0.00416 0.00061 0.00040 AFIX 43 H5 5 0.194935 0.773926 1.134420 11.00000 -1.20000 AFIX 0 C6 4 0.219459 0.674135 1.083914 11.00000 0.01586 0.01602 = 0.01319 0.00020 0.00051 -0.00202 AFIX 43 H6 5 0.180757 0.646587 1.125651 11.00000 -1.20000 AFIX 0 C7 4 0.175772 0.521624 0.952656 11.00000 0.01424 0.01446 = 0.01338 -0.00016 0.00417 -0.00030 C8 4 0.198608 0.441009 0.957230 11.00000 0.01866 0.01284 = 0.01657 -0.00047 0.00198 -0.00032 AFIX 137 H8A 5 0.087714 0.418050 0.962105 11.00000 -1.50000 H8B 5 0.290077 0.428440 1.006073 11.00000 -1.50000 H8C 5 0.233041 0.423554 0.906519 11.00000 -1.50000 AFIX 0 C9 4 -0.236715 0.359033 0.659641 11.00000 0.01487 0.01378 = 0.01100 0.00017 0.00321 -0.00010 C10 4 -0.104506 0.319764 0.712138 11.00000 0.01490 0.01717 = 0.01294 0.00012 0.00015 0.00036 AFIX 43 H10 5 -0.019600 0.344153 0.753194 11.00000 -1.20000 AFIX 0 C11 4 -0.098411 0.244565 0.703695 11.00000 0.01817 0.01825 = 0.01526 0.00299 0.00270 0.00430 AFIX 43 H11 5 -0.008348 0.217709 0.739280 11.00000 -1.20000 AFIX 0 C12 4 -0.221775 0.207944 0.644099 11.00000 0.02252 0.01271 = 0.01783 -0.00084 0.00770 -0.00018 AFIX 43 H12 5 -0.216216 0.156513 0.638978 11.00000 -1.20000 AFIX 0 C13 4 -0.353134 0.247319 0.592167 11.00000 0.01774 0.01800 = 0.01519 -0.00329 0.00271 -0.00313 AFIX 43 H13 5 -0.438269 0.222712 0.551424 11.00000 -1.20000 AFIX 0 C14 4 -0.360670 0.322413 0.599481 11.00000 0.01460 0.01796 = 0.01258 0.00088 0.00040 0.00051 AFIX 43 H14 5 -0.450426 0.349080 0.563465 11.00000 -1.20000 AFIX 0 C15 4 -0.181100 0.483805 0.719540 11.00000 0.01344 0.01456 = 0.01417 0.00004 0.00449 -0.00195 C16 4 -0.234443 0.561611 0.703131 11.00000 0.01988 0.01375 = 0.01797 -0.00022 0.00260 -0.00046 AFIX 137 H16A 5 -0.291679 0.579119 0.747181 11.00000 -1.50000 H16B 5 -0.316379 0.565393 0.648967 11.00000 -1.50000 H16C 5 -0.130206 0.591275 0.702497 11.00000 -1.50000 AFIX 0 C17 4 0.201330 0.645986 0.675498 11.00000 0.01345 0.01294 = 0.01238 -0.00019 -0.00368 -0.00244 C18 4 0.239528 0.686485 0.609969 11.00000 0.01704 0.01739 = 0.01315 -0.00149 0.00058 -0.00285 AFIX 43 H18 5 0.280695 0.663189 0.566039 11.00000 -1.20000 AFIX 0 C19 4 0.216683 0.761451 0.609611 11.00000 0.02080 0.01713 = 0.01519 0.00312 0.00087 -0.00430 AFIX 43 H19 5 0.242217 0.789559 0.565000 11.00000 -1.20000 AFIX 0 C20 4 0.156837 0.795860 0.673829 11.00000 0.01746 0.01240 = 0.02088 -0.00066 -0.00044 -0.00159 AFIX 43 H20 5 0.140390 0.847137 0.672841 11.00000 -1.20000 AFIX 0 C21 4 0.121230 0.754743 0.739483 11.00000 0.01709 0.01880 = 0.01626 -0.00336 0.00216 -0.00154 AFIX 43 H21 5 0.081215 0.778060 0.783725 11.00000 -1.20000 AFIX 0 C22 4 0.143912 0.679727 0.740663 11.00000 0.01610 0.01752 = 0.01311 0.00060 0.00000 -0.00378 AFIX 43 H22 5 0.120315 0.651685 0.785735 11.00000 -1.20000 AFIX 0 C23 4 0.158594 0.522933 0.618277 11.00000 0.01413 0.01435 = 0.01482 -0.00018 0.00256 -0.00176 C24 4 0.204855 0.444209 0.630256 11.00000 0.02147 0.01298 = 0.01873 0.00012 0.00300 0.00028 AFIX 137 H24A 5 0.097099 0.415107 0.621524 11.00000 -1.50000 H24B 5 0.272889 0.436418 0.687104 11.00000 -1.50000 H24C 5 0.274947 0.429423 0.590004 11.00000 -1.50000 AFIX 0 H1N 5 0.331322 0.539210 1.054252 11.00000 0.03040 H2N 5 -0.323726 0.452188 0.618039 11.00000 0.02783 H3N 5 0.293567 0.553549 0.722755 11.00000 0.02720 H1H 5 0.010890 0.521519 0.852465 11.00000 0.11297 PART -1 H2H 5 0.010982 0.512685 0.515601 10.50000 0.06577 HKLF 4 REM REM wR2 = 0.0882, GooF = S = 1.041, Restrained GooF = 1.042 for all data REM R1 = 0.0308 for 4113 Fo > 4sig(Fo) and 0.0332 for all 4444 data REM 309 parameters refined using 2 restraints END WGHT 0.0491 0.7515 REM Highest difference peak 0.262, deepest hole -0.303, 1-sigma level 0.047 Q1 1 -0.1699 0.5937 0.7467 11.00000 0.05 0.26 Q2 1 -0.2764 0.3420 0.6219 11.00000 0.05 0.25 Q3 1 0.1864 0.6613 0.6399 11.00000 0.05 0.22 Q4 1 0.3460 0.6579 0.9989 11.00000 0.05 0.20 Q5 1 -0.1852 0.3403 0.6903 11.00000 0.05 0.20 Q6 1 0.1356 0.6606 0.6990 11.00000 0.05 0.20 Q7 1 0.2692 0.6558 1.0569 11.00000 0.05 0.20 Q8 1 0.2074 0.6588 1.0424 11.00000 0.05 0.18 Q9 1 -0.1987 0.5243 0.7123 11.00000 0.05 0.18 Q10 1 -0.3187 0.2868 0.5835 11.00000 0.05 0.17 Q11 1 -0.1762 0.2262 0.6808 11.00000 0.05 0.17 Q12 1 -0.1469 0.2346 0.6653 11.00000 0.05 0.17 Q13 1 -0.2886 0.2318 0.6150 11.00000 0.05 0.17 Q14 1 0.1945 0.4842 0.6237 11.00000 0.05 0.17 Q15 1 0.2587 0.7660 1.0602 11.00000 0.05 0.16 Q16 1 -0.4308 0.5117 0.5639 11.00000 0.05 0.16 Q17 1 -0.1310 0.2804 0.7175 11.00000 0.05 0.16 Q18 1 0.2171 0.6606 0.7177 11.00000 0.05 0.16 Q19 1 0.1384 0.4198 0.9029 11.00000 0.05 0.16 Q20 1 0.5556 0.5230 0.9038 11.00000 0.05 0.16 ; _shelx_res_checksum 73872 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl1 -0.500000 0.500000 0.500000 0.02398(12) Uani d 1 . . Cl Cl2 0.48309(4) 0.51388(2) 0.83954(2) 0.01975(10) Uani d 1 . . O O1 0.06759(11) 0.55205(5) 0.89225(5) 0.01583(19) Uani d 1 . . O O2 -0.07277(11) 0.46451(5) 0.78459(5) 0.01730(19) Uani d 1 . . O O3 0.05548(12) 0.54574(5) 0.55287(5) 0.0184(2) Uani d 1 . . N N1 0.26521(14) 0.56132(6) 1.01360(6) 0.0138(2) Uani d 1 . . N N2 -0.25432(13) 0.43603(6) 0.66144(6) 0.0141(2) Uani d 1 . . N N3 0.22695(14) 0.56869(6) 0.67856(6) 0.0152(2) Uani d 1 . . C C1 0.26759(15) 0.63949(6) 1.01664(7) 0.0132(2) Uani d 1 . . C C2 0.32839(16) 0.67877(7) 0.95615(7) 0.0155(2) Uani d 1 . . H H2 0.363096 0.654464 0.911101 0.019 Uiso calc 1 . . C C3 0.33770(16) 0.75415(7) 0.96250(7) 0.0176(3) Uani d 1 . . H H3 0.378720 0.781593 0.921355 0.021 Uiso calc 1 . . C C4 0.28744(16) 0.78985(7) 1.02862(8) 0.0175(3) Uani d 1 . . H H4 0.293194 0.841450 1.032342 0.021 Uiso calc 1 . . C C5 0.22884(16) 0.74965(7) 1.08915(7) 0.0171(3) Uani d 1 . . H H5 0.194935 0.773926 1.134420 0.021 Uiso calc 1 . . C C6 0.21946(15) 0.67413(7) 1.08391(7) 0.0154(2) Uani d 1 . . H H6 0.180757 0.646587 1.125651 0.018 Uiso calc 1 . . C C7 0.17577(15) 0.52162(7) 0.95266(7) 0.0138(2) Uani d 1 . . C C8 0.19861(16) 0.44101(7) 0.95723(8) 0.0163(3) Uani d 1 . . H H8A 0.087714 0.418050 0.962105 0.024 Uiso calc 1 . . H H8B 0.290077 0.428440 1.006073 0.024 Uiso calc 1 . . H H8C 0.233041 0.423554 0.906519 0.024 Uiso calc 1 . . C C9 -0.23672(15) 0.35903(7) 0.65964(7) 0.0131(2) Uani d 1 . . C C10 -0.10451(16) 0.31976(7) 0.71214(7) 0.0154(2) Uani d 1 . . H H10 -0.019600 0.344153 0.753194 0.019 Uiso calc 1 . . C C11 -0.09841(16) 0.24457(7) 0.70370(7) 0.0173(3) Uani d 1 . . H H11 -0.008348 0.217709 0.739280 0.021 Uiso calc 1 . . C C12 -0.22177(16) 0.20794(7) 0.64410(7) 0.0172(3) Uani d 1 . . H H12 -0.216216 0.156513 0.638978 0.021 Uiso calc 1 . . C C13 -0.35313(16) 0.24732(7) 0.59217(7) 0.0171(3) Uani d 1 . . H H13 -0.438269 0.222712 0.551424 0.021 Uiso calc 1 . . C C14 -0.36067(16) 0.32241(7) 0.59948(7) 0.0154(2) Uani d 1 . . H H14 -0.450426 0.349080 0.563465 0.018 Uiso calc 1 . . C C15 -0.18110(15) 0.48381(7) 0.71954(7) 0.0138(2) Uani d 1 . . C C16 -0.23444(17) 0.56161(7) 0.70313(8) 0.0174(3) Uani d 1 . . H H16A -0.291679 0.579119 0.747181 0.026 Uiso calc 1 . . H H16B -0.316379 0.565393 0.648967 0.026 Uiso calc 1 . . H H16C -0.130206 0.591275 0.702497 0.026 Uiso calc 1 . . C C17 0.20133(15) 0.64599(7) 0.67550(7) 0.0139(2) Uani d 1 . . C C18 0.23953(16) 0.68648(7) 0.60997(7) 0.0162(3) Uani d 1 . . H H18 0.280695 0.663189 0.566039 0.019 Uiso calc 1 . . C C19 0.21668(16) 0.76145(7) 0.60961(8) 0.0181(3) Uani d 1 . . H H19 0.242217 0.789559 0.565000 0.022 Uiso calc 1 . . C C20 0.15684(16) 0.79586(7) 0.67383(8) 0.0176(3) Uani d 1 . . H H20 0.140390 0.847137 0.672841 0.021 Uiso calc 1 . . C C21 0.12123(16) 0.75474(7) 0.73948(8) 0.0176(3) Uani d 1 . . H H21 0.081215 0.778060 0.783725 0.021 Uiso calc 1 . . C C22 0.14391(16) 0.67973(7) 0.74066(7) 0.0160(3) Uani d 1 . . H H22 0.120315 0.651685 0.785735 0.019 Uiso calc 1 . . C C23 0.15859(15) 0.52293(7) 0.61828(7) 0.0145(2) Uani d 1 . . C C24 0.20486(17) 0.44421(7) 0.63026(8) 0.0179(3) Uani d 1 . . H H24A 0.097099 0.415107 0.621524 0.027 Uiso calc 1 . . H H24B 0.272889 0.436418 0.687104 0.027 Uiso calc 1 . . H H24C 0.274947 0.429423 0.590004 0.027 Uiso calc 1 . . H H1N 0.331(2) 0.5392(10) 1.0543(11) 0.030(5) Uiso d 1 . . H H2N -0.324(2) 0.4522(10) 0.6180(11) 0.028(4) Uiso d 1 . . H H3N 0.294(2) 0.5535(9) 0.7228(11) 0.027(4) Uiso d 1 . . H H1H 0.011(4) 0.5215(13) 0.8525(14) 0.113(11) Uiso d 1 . . H H2H 0.011(8) 0.513(3) 0.516(3) 0.066(14) Uiso d 0.5 A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.0214(2) 0.0286(2) 0.0187(2) 0.00005(18) -0.00286(17) 0.01083(18) Cl2 0.01927(16) 0.02283(18) 0.01485(16) 0.00253(12) -0.00154(11) 0.00524(11) O1 0.0179(4) 0.0131(4) 0.0135(4) -0.0002(3) -0.0032(3) -0.0005(3) O2 0.0189(4) 0.0157(4) 0.0140(4) -0.0013(4) -0.0037(3) -0.0015(3) O3 0.0209(4) 0.0145(5) 0.0158(4) -0.0002(4) -0.0050(3) -0.0029(4) N1 0.0159(5) 0.0116(5) 0.0119(5) 0.0005(4) -0.0015(4) 0.0010(4) N2 0.0148(5) 0.0133(5) 0.0122(5) 0.0011(4) -0.0013(4) 0.0009(4) N3 0.0177(5) 0.0129(5) 0.0125(5) -0.0007(4) -0.0021(4) 0.0014(4) C1 0.0131(5) 0.0108(6) 0.0132(5) -0.0004(4) -0.0030(4) -0.0007(4) C2 0.0166(6) 0.0159(6) 0.0126(5) -0.0002(5) -0.0003(4) -0.0009(5) C3 0.0197(6) 0.0162(6) 0.0154(6) -0.0023(5) 0.0008(5) 0.0029(5) C4 0.0186(6) 0.0119(6) 0.0198(6) -0.0008(5) -0.0013(5) -0.0011(5) C5 0.0178(6) 0.0168(6) 0.0156(6) 0.0004(5) 0.0006(5) -0.0042(5) C6 0.0159(6) 0.0160(6) 0.0132(5) -0.0020(5) 0.0005(4) 0.0002(5) C7 0.0142(6) 0.0145(6) 0.0134(5) -0.0003(5) 0.0042(4) -0.0002(4) C8 0.0187(6) 0.0128(6) 0.0166(6) -0.0003(5) 0.0020(5) -0.0005(5) C9 0.0149(5) 0.0138(6) 0.0110(5) -0.0001(5) 0.0032(4) 0.0002(4) C10 0.0149(6) 0.0172(6) 0.0129(5) 0.0004(5) 0.0001(4) 0.0001(5) C11 0.0182(6) 0.0182(6) 0.0153(6) 0.0043(5) 0.0027(5) 0.0030(5) C12 0.0225(6) 0.0127(6) 0.0178(6) -0.0002(5) 0.0077(5) -0.0008(5) C13 0.0177(6) 0.0180(6) 0.0152(6) -0.0031(5) 0.0027(5) -0.0033(5) C14 0.0146(5) 0.0180(6) 0.0126(5) 0.0005(5) 0.0004(4) 0.0009(5) C15 0.0134(5) 0.0146(6) 0.0142(6) -0.0020(5) 0.0045(4) 0.0000(4) C16 0.0199(6) 0.0137(6) 0.0180(6) -0.0005(5) 0.0026(5) -0.0002(5) C17 0.0134(5) 0.0129(6) 0.0124(5) -0.0024(5) -0.0037(4) -0.0002(4) C18 0.0170(6) 0.0174(6) 0.0132(5) -0.0028(5) 0.0006(4) -0.0015(5) C19 0.0208(6) 0.0171(6) 0.0152(6) -0.0043(5) 0.0009(5) 0.0031(5) C20 0.0175(6) 0.0124(6) 0.0209(6) -0.0016(5) -0.0004(5) -0.0007(5) C21 0.0171(6) 0.0188(6) 0.0163(6) -0.0015(5) 0.0022(5) -0.0034(5) C22 0.0161(6) 0.0175(6) 0.0131(5) -0.0038(5) 0.0000(4) 0.0006(5) C23 0.0141(6) 0.0143(6) 0.0148(6) -0.0018(5) 0.0026(4) -0.0002(5) C24 0.0215(6) 0.0130(6) 0.0187(6) 0.0003(5) 0.0030(5) 0.0001(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C7 O1 H1H . . 115(2) ? C23 O3 H2H . . 116(4) ? C7 N1 C1 . . 125.65(10) ? C7 N1 H1N . . 117.7(12) ? C1 N1 H1N . . 116.6(12) ? C15 N2 C9 . . 129.93(10) ? C15 N2 H2N . . 117.9(12) ? C9 N2 H2N . . 112.1(12) ? C23 N3 C17 . . 124.98(10) ? C23 N3 H3N . . 120.7(12) ? C17 N3 H3N . . 114.3(12) ? C2 C1 C6 . . 121.23(11) ? C2 C1 N1 . . 119.89(11) ? C6 C1 N1 . . 118.73(11) ? C1 C2 C3 . . 118.99(11) ? C1 C2 H2 . . 120.5 ? C3 C2 H2 . . 120.5 ? C2 C3 C4 . . 120.58(12) ? C2 C3 H3 . . 119.7 ? C4 C3 H3 . . 119.7 ? C5 C4 C3 . . 119.68(12) ? C5 C4 H4 . . 120.2 ? C3 C4 H4 . . 120.2 ? C4 C5 C6 . . 120.46(11) ? C4 C5 H5 . . 119.8 ? C6 C5 H5 . . 119.8 ? C5 C6 C1 . . 119.04(11) ? C5 C6 H6 . . 120.5 ? C1 C6 H6 . . 120.5 ? O1 C7 N1 . . 120.10(11) ? O1 C7 C8 . . 121.50(11) ? N1 C7 C8 . . 118.37(11) ? C7 C8 H8A . . 109.5 ? C7 C8 H8B . . 109.5 ? H8A C8 H8B . . 109.5 ? C7 C8 H8C . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? C10 C9 C14 . . 119.74(11) ? C10 C9 N2 . . 124.28(11) ? C14 C9 N2 . . 115.97(10) ? C11 C10 C9 . . 119.25(11) ? C11 C10 H10 . . 120.4 ? C9 C10 H10 . . 120.4 ? C10 C11 C12 . . 121.17(11) ? C10 C11 H11 . . 119.4 ? C12 C11 H11 . . 119.4 ? C13 C12 C11 . . 119.29(12) ? C13 C12 H12 . . 120.4 ? C11 C12 H12 . . 120.4 ? C14 C13 C12 . . 120.29(11) ? C14 C13 H13 . . 119.9 ? C12 C13 H13 . . 119.9 ? C13 C14 C9 . . 120.26(11) ? C13 C14 H14 . . 119.9 ? C9 C14 H14 . . 119.9 ? O2 C15 N2 . . 121.86(11) ? O2 C15 C16 . . 122.03(11) ? N2 C15 C16 . . 116.11(11) ? C15 C16 H16A . . 109.5 ? C15 C16 H16B . . 109.5 ? H16A C16 H16B . . 109.5 ? C15 C16 H16C . . 109.5 ? H16A C16 H16C . . 109.5 ? H16B C16 H16C . . 109.5 ? C22 C17 C18 . . 120.84(12) ? C22 C17 N3 . . 118.71(11) ? C18 C17 N3 . . 120.41(11) ? C19 C18 C17 . . 119.06(11) ? C19 C18 H18 . . 120.5 ? C17 C18 H18 . . 120.5 ? C18 C19 C20 . . 120.72(12) ? C18 C19 H19 . . 119.6 ? C20 C19 H19 . . 119.6 ? C21 C20 C19 . . 119.57(12) ? C21 C20 H20 . . 120.2 ? C19 C20 H20 . . 120.2 ? C22 C21 C20 . . 120.27(12) ? C22 C21 H21 . . 119.9 ? C20 C21 H21 . . 119.9 ? C21 C22 C17 . . 119.53(11) ? C21 C22 H22 . . 120.2 ? C17 C22 H22 . . 120.2 ? O3 C23 N3 . . 120.38(11) ? O3 C23 C24 . . 121.57(11) ? N3 C23 C24 . . 118.04(11) ? C23 C24 H24A . . 109.5 ? C23 C24 H24B . . 109.5 ? H24A C24 H24B . . 109.5 ? C23 C24 H24C . . 109.5 ? H24A C24 H24C . . 109.5 ? H24B C24 H24C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C7 . 1.2843(15) ? O1 H1H . 0.901(10) ? O2 C15 . 1.2624(15) ? O3 C23 . 1.2670(15) ? O3 H2H . 0.879(10) ? N1 C7 . 1.3114(16) ? N1 C1 . 1.4363(15) ? N1 H1N . 0.854(18) ? N2 C15 . 1.3312(16) ? N2 C9 . 1.4215(16) ? N2 H2N . 0.851(18) ? N3 C23 . 1.3202(16) ? N3 C17 . 1.4329(16) ? N3 H3N . 0.844(18) ? C1 C2 . 1.3883(17) ? C1 C6 . 1.3918(17) ? C2 C3 . 1.3889(18) ? C2 H2 . 0.9500 ? C3 C4 . 1.3922(18) ? C3 H3 . 0.9500 ? C4 C5 . 1.3893(18) ? C4 H4 . 0.9500 ? C5 C6 . 1.3904(17) ? C5 H5 . 0.9500 ? C6 H6 . 0.9500 ? C7 C8 . 1.4910(17) ? C8 H8A . 0.9800 ? C8 H8B . 0.9800 ? C8 H8C . 0.9800 ? C9 C10 . 1.3950(16) ? C9 C14 . 1.3978(16) ? C10 C11 . 1.3897(18) ? C10 H10 . 0.9500 ? C11 C12 . 1.3902(17) ? C11 H11 . 0.9500 ? C12 C13 . 1.3878(18) ? C12 H12 . 0.9500 ? C13 C14 . 1.3865(18) ? C13 H13 . 0.9500 ? C14 H14 . 0.9500 ? C15 C16 . 1.4964(17) ? C16 H16A . 0.9800 ? C16 H16B . 0.9800 ? C16 H16C . 0.9800 ? C17 C22 . 1.3885(17) ? C17 C18 . 1.3897(17) ? C18 C19 . 1.3880(18) ? C18 H18 . 0.9500 ? C19 C20 . 1.3904(18) ? C19 H19 . 0.9500 ? C20 C21 . 1.3900(18) ? C20 H20 . 0.9500 ? C21 C22 . 1.3885(18) ? C21 H21 . 0.9500 ? C22 H22 . 0.9500 ? C23 C24 . 1.4928(17) ? C24 H24A . 0.9800 ? C24 H24B . 0.9800 ? C24 H24C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N Cl2 3_667 0.854(18) 2.237(19) 3.0899(11) 176.6(16) yes N2 H2N Cl1 . 0.851(18) 2.297(18) 3.1464(10) 177.0(16) yes N3 H3N Cl2 . 0.844(18) 2.275(18) 3.1189(11) 177.6(16) yes O1 H1H O2 . 0.901(10) 1.566(10) 2.4650(12) 175(3) yes O3 H2H O3 3_566 0.879(10) 1.560(11) 2.4370(16) 176(7) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C7 N1 C1 C2 . . . . -61.24(17) ? C7 N1 C1 C6 . . . . 123.03(13) ? C6 C1 C2 C3 . . . . -1.26(18) ? N1 C1 C2 C3 . . . . -176.88(11) ? C1 C2 C3 C4 . . . . 0.21(18) ? C2 C3 C4 C5 . . . . 0.53(18) ? C3 C4 C5 C6 . . . . -0.24(18) ? C4 C5 C6 C1 . . . . -0.77(17) ? C2 C1 C6 C5 . . . . 1.54(17) ? N1 C1 C6 C5 . . . . 177.21(11) ? C1 N1 C7 O1 . . . . -6.34(18) ? C1 N1 C7 C8 . . . . 175.79(11) ? C15 N2 C9 C10 . . . . -15.5(2) ? C15 N2 C9 C14 . . . . 165.71(12) ? C14 C9 C10 C11 . . . . -0.04(17) ? N2 C9 C10 C11 . . . . -178.82(11) ? C9 C10 C11 C12 . . . . -0.15(18) ? C10 C11 C12 C13 . . . . 0.04(18) ? C11 C12 C13 C14 . . . . 0.26(18) ? C12 C13 C14 C9 . . . . -0.46(18) ? C10 C9 C14 C13 . . . . 0.34(18) ? N2 C9 C14 C13 . . . . 179.22(11) ? C9 N2 C15 O2 . . . . 2.7(2) ? C9 N2 C15 C16 . . . . -177.45(11) ? C23 N3 C17 C22 . . . . 127.72(13) ? C23 N3 C17 C18 . . . . -54.59(17) ? C22 C17 C18 C19 . . . . -1.09(18) ? N3 C17 C18 C19 . . . . -178.72(11) ? C17 C18 C19 C20 . . . . 0.14(18) ? C18 C19 C20 C21 . . . . 0.65(18) ? C19 C20 C21 C22 . . . . -0.50(18) ? C20 C21 C22 C17 . . . . -0.42(18) ? C18 C17 C22 C21 . . . . 1.23(18) ? N3 C17 C22 C21 . . . . 178.90(10) ? C17 N3 C23 O3 . . . . -3.28(19) ? C17 N3 C23 C24 . . . . 177.45(11) ?