#------------------------------------------------------------------------------
#$Date: 2024-08-13 04:58:08 +0300 (Tue, 13 Aug 2024) $
#$Revision: 294093 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312575.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2312575
loop_
_publ_author_name
'Dailey, Maegan'
'Jackson, Eric W.'
'Ramadhar, Timothy R.'
_publ_section_title
;
 Crystal structures, phase transition, and Hirshfeld surface analyses of
 the bromide and chloride congeners of
 aqua[2,4,6-tris(pyridin-4-yl)-1,3,5-triazine]zinc(II) halide.
;
_journal_coeditor_code           ZO3049
_journal_issue                   9
_journal_name_full
'Acta crystallographica. Section C, Structural chemistry'
_journal_paper_doi               10.1107/S205322962400737X
_journal_volume                  80
_journal_year                    2024
_chemical_formula_iupac          '[Zn (C18 H12 N6) (H2 O)] Cl2'
_chemical_formula_moiety         'C18 H14 N6 O Zn 2+, 2(Cl -)'
_chemical_formula_sum            'C18 H14 Cl2 N6 O Zn'
_chemical_formula_weight         466.62
_chemical_name_systematic
;
Aqua[2,4,6-tris(pyridin-4-yl)-1,3,5-triazine]zinc(II) dichloride
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           62
_space_group_name_Hall           '-P 2ac 2n'
_space_group_name_H-M_alt        'P n m a'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_audit_creation_method
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.1507(5)
_cell_length_b                   14.0162(5)
_cell_length_c                   9.8624(5)
_cell_measurement_reflns_used    4128
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      75.1110
_cell_measurement_theta_min      5.4530
_cell_volume                     1956.10(14)
_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2022)
;
_computing_data_collection
;
CrysAlis PRO (Rigaku OD, 2022)
;
_computing_data_reduction
;
CrysAlis PRO (Rigaku OD, 2022)
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov <i>et al.</i>,  2009)
;
_computing_publication_material
;
OLEX2 (Dolomanov <i>et al.</i>,  2009)
;
_computing_structure_refinement
;
SHELXL2019 (Sheldrick, 2015<i>b</i>)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015<i>a</i>)
;
_diffrn_ambient_temperature      100.00(10)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type
'Rigaku XtaLAB Synergy Dualflex diffractometer with a HyPix detector'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0575
_diffrn_reflns_av_unetI/netI     0.0458
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -6
_diffrn_reflns_number            7121
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         68.230
_diffrn_reflns_theta_min         5.467
_diffrn_source                   'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    4.445
_exptl_absorpt_correction_T_max  0.534
_exptl_absorpt_correction_T_min  0.316
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
[CrysAlis PRO (Rigaku OD, 2022) based on expressions derived by Clark &
Reid
(1995)]
;
_exptl_crystal_colour            'clear colourless'
_exptl_crystal_density_diffrn    1.584
_exptl_crystal_description       prism
_exptl_crystal_F_000             944
_exptl_crystal_size_max          0.49
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.201
_refine_diff_density_max         2.100
_refine_diff_density_min         -2.087
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.111
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     140
_refine_ls_number_reflns         1858
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.111
_refine_ls_R_factor_all          0.0820
_refine_ls_R_factor_gt           0.0738
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1309P)^2^+4.6756P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2117
_refine_ls_wR_factor_ref         0.2197
_reflns_number_gt                1578
_reflns_number_total             1858
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            zo3049sup1.cif
_cod_data_source_block           3
_cod_database_code               2312575
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.219
_shelx_estimated_absorpt_t_max   0.469
_shelx_hkl_file
;
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   0   0   2 172039. 7414.49   6
   0   0   3 7.38327 45.0503   6
   0   0   4 44904.4 2111.90   6
   0   0   5 29.6599 73.0845   6
   0   0   6 89681.8 4194.71   6
   0   0   7 78.5297 105.367   6
   0   0   8 5225.39 601.239   6
   0   0  10 3972.05 422.830   4
   0   1   0 14.4895 18.0725  10
   0   1   1 5650.22 299.192   6
   0   1   2 261.011 63.7742   6
   0   1   3 85745.9 3735.02   6
   0  -1   3 82242.0 3688.11   6
   0   1   4 112.689 79.9460   6
   0  -1   4 205.405 76.0067   6
   0   1   5 19266.9 1123.42   6
   0  -1   5 20000.1 1077.98   6
   0   1   6 22.9863 105.524   6
   0  -1   6 180.701 102.897   6
   0  -1   7 1492.50 265.512   6
   0   1   7 1436.07 288.353   6
   0   1   8-74.7648 116.503   6
   0  -1   8 31.0330 104.466   6
   0   1   9 265.961 195.534   6
   0  -1   9 154.755 147.899   6
   0  -1  10-16.7228 148.931   4
   0   2   0 96114.6 4202.76  10
   0   2   1 46.1838 42.8431  10
   0   2   1 6.43613 46.3358   6
   0   2   2 276679. 11936.5   6
   0   2   3 86.5693 75.4966   6
   0   2   4 43545.2 2105.62   6
   0  -2   4 42453.2 1998.50   6
   0  -2   5 353.263 107.203   6
   0   2   5 184.408 108.094   6
   0   2   6 18850.0 1235.69   6
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   0   2   7 277.727 171.383   6
   0  -2   7 228.594 133.690   6
   0   2   8 1782.16 410.315   6
   0  -2   8 2379.52 375.827   6
   0   2   9 331.419 241.355   6
   0   2  10 2816.71 347.064   4
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   0  -2  11-154.540 119.375   4
   0   2  11-85.0418 97.6397   4
   0   3   0 52.0399 67.1580  10
   0   3   1 3303.65 275.292  10
   0   3   2 110.722 74.7703  10
   0   3   2 68.1122 77.8712   6
   0   3   3 47598.4 2291.81   6
   0   3   4 75.9240 99.6201   6
   0   3   5 94271.8 4385.17   6
   0  -3   5 90247.0 4150.15   6
   0   3   6 98.4422 132.076   6
   0  -3   6 88.0146 89.6661   6
   0  -3   7 23868.2 1391.66   6
   0   3   7 23676.0 1645.56   6
   0  -3   8 116.152 122.533   6
   0   3   8-95.4007 191.912   6
   0   3   9 28540.9 2028.59  10
   0   3   9 25912.6 1872.00   6
   0   3  10-219.959 177.912   4
   0  -3  11 332.794 152.486   4
   0   3  11 242.403 112.991   4
   0   4   0 285.580 112.929  10
   0   4   1-12.2803 76.5420  10
   0   4   2 6673.38 498.132   6
   0   4   2 7416.20 515.275  10
   0   4   3 125.677 105.299   6
   0   4   3 163.550 100.445  10
   0   4  -3 387.265 72.9965   7
   0   4   4 168.952 134.043   6
   0   4   5 764.590 248.683   6
   0  -4   6 6889.81 561.813   6
   0   4   6 6862.48 775.356   6
   0   4   7 140.357 197.837   6
   0  -4   7 396.919 152.013   6
   0   4   8 1571.29 405.316  10
   0  -4   8 1517.00 294.355   6
   0   4   8 1657.76 433.868   6
   0  -4   9 411.437 212.204   4
   0  -4  10 4259.61 448.111   4
   0   4  10 4231.56 424.052   4
   0  -4  11-52.0250 117.677   4
   0   4  11-42.2523 87.3646   4
   0   5   0 31.1304 76.7080  10
   0   5   1 29726.3 1547.68  10
   0   5   2 52.6009 80.4612  10
   0   5  -3 29487.9 1402.30   7
   0   5   3 32525.8 1693.64  10
   0   5   4 26.8844 113.447   6
   0   5   4 25.3398 101.954  10
   0   5   5 51674.2 2893.97  10
   0   5   5 60607.5 3025.36   6
   0   5   6 39.3852 150.325  10
   0   5   6-43.2867 145.707   6
   0  -5   6-19.7670 79.5292   6
   0   5   7 5241.03 755.031   6
   0   5   7 6323.27 798.238  10
   0  -5   7 7568.72 637.730   6
   0   5   8 57.3789 206.492  10
   0   5   9 7092.33 601.254   4
   0  -5   9 7710.42 607.079   4
   0  -5  10 76.5610 123.642   4
   0   5  10-98.6760 119.518   4
   0   5  11 2175.98 209.133   4
   0  -5  11 2530.46 232.339   4
   0   6   0 146930. 6534.50  10
   0   6   0 144006. 6288.20   8
   0   6  -1 19.4658 57.1936   8
   0   6   1 19.7325 106.511  10
   0   6   1-19.7058 50.8332   8
   0   6   2 9545.59 723.792  10
   0   6   2 8240.56 513.366   8
   0   6  -2 9544.14 506.773   7
   0   6   3 25.2078 128.289  10
   0   6  -3 28.9765 52.1498   7
   0   6   4 28842.4 1739.36  10
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   0   6   6 2593.24 502.002  10
   0  -6   7 100.309 95.8363   6
   0   6   7 162.422 182.306  10
   0  -6   8 9593.46 679.034   4
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   0   6   9-14.4767 112.034   4
   0  -6   9-12.5566 114.087   4
   0  -6  10 5509.07 401.735   4
   0   6  10 5695.55 415.096   4
   0   7   0-46.8839 115.512  10
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   0   7  -2 168.084 72.4625   7
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   0   7   2 155.011 135.722  10
   0   7   3 417.305 110.125   8
   0   7   3 528.707 205.630  10
   0   7  -3 484.910 97.4293   7
   0   7   4 106.575 156.824  10
   0   7   4 222.101 53.6097   3
   0   7   5 1759.17 394.715  10
   0   7   5 1958.89 158.955   3
   0   7   6 71.6349 51.0760   3
   0  -7   6 22.5900 81.2910   6
   0   7   7 348.989 256.776  10
   0   7   9-49.9219 92.5015   4
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   0   8   0 136185. 6296.70  10
   0   8   0 135281. 5948.25   8
   0   8   1 29.4138 134.936  10
   0   8  -1-27.1174 72.7505   8
   0   8   1-68.0469 80.1671   8
   0   8   2 34852.9 1737.10   8
   0   8   2 37848.4 2104.10  10
   0   8  -2 37151.1 1711.40   7
   0   8   3 85.0781 43.2005   3
   0   8   3-33.9378 73.3975   8
   0   8   3-34.5706 124.408  10
   0   8  -3-8.75773 52.2747   7
   0   8   4 24325.9 1192.14   8
   0   8   4 21016.6 1022.84   3
   0   8   4 23460.2 1582.96  10
   0   8   5 30.9349 104.136   8
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   0   8   5 32.5457 39.6602   3
   0  -8   6 23.6095 84.9597   6
   0   8   6-12.9959 47.4926   3
   0   8   6-54.3287 207.361  10
   0   8   7 59.6365 214.616  10
   0   8   8 3177.80 371.525   8
   0   8   9 34.6446 107.976   8
   0   8  10 3775.55 351.653   8
   0   9   0 43.2213 75.3033   8
   0   9   0 16.1640 50.3840   3
   0   9   1 5255.21 398.027   8
   0   9  -1 5467.94 357.652   3
   0   9   1 5253.22 614.852  10
   0   9   2 19.9939 48.0066   3
   0   9   2 180.398 171.763  10
   0   9  -2 59.0192 62.6048   7
   0   9   2 71.1564 75.4674   8
   0   9   3 2298.63 188.786   3
   0   9   3 2674.60 279.982   8
   0   9  -3 2449.56 235.122   7
   0   9   3 2736.27 468.455  10
   0   9   4 45.4131 191.626  10
   0   9   4 5.50386 38.3575   3
   0   9   4 59.1584 101.330   8
   0   9   5 5353.45 461.111   8
   0   9   5 4029.60 653.239  10
   0   9   5 5120.31 312.474   3
   0   9   6 39.3851 50.1405   3
   0   9   6 55.4650 124.479   8
   0   9   6 56.9442 191.687  10
   0   9   7 3358.12 378.451   8
   0   9   8 36.5406 111.488   8
   0   9   9 4372.77 397.775   8
   0  10   0 5907.56 443.351   8
   0  10   0 6467.89 404.996   3
   0  10  -1-11.4386 68.2636   7
   0  10   1-12.7082 88.5598   8
   0  10  -1 64.5525 56.2347   3
   0  10   1-38.4424 138.337  10
   0  10  -2 20317.4 990.214   3
   0  10   2 20704.2 992.527   3
   0  10   2 19858.3 1467.59  10
   0  10   2 20009.7 1092.85   8
   0  10  -2 18364.2 1030.48   7
   0  10   3 90.3654 190.693  10
   0  10   3 118.147 111.228   8
   0  10  -3 77.8434 51.0265   3
   0  10   3 120.793 65.6972   3
   0  10  -3 73.8169 78.3282   7
   0  10   4 678.695 181.095   8
   0  10   4 596.632 277.704  10
   0  10   4 837.446 110.193   3
   0  10   5 290.907 77.2681   3
   0  10   5 491.868 295.236  10
   0  10   5 194.703 137.495   8
   0  10   6 6933.72 403.148   3
   0  10   6 6603.03 555.233   8
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   0  10   7 164.633 133.876   8
   0  10   8 410.023 147.103   8
   0  10   9-12.9259 98.6718   8
   0  11   0 13.4385 99.7283   8
   0  11   0 85.2400 69.4902   3
   0  11  -1 6562.23 468.302   7
   0  11   1 6368.36 482.466   8
   0  11  -1 6292.43 405.142   3
   0  11   1 6811.78 426.293   3
   0  11   2 59.7055 105.756   8
   0  11   2 135.920 163.050  10
   0  11  -2 47.2274 85.0018   7
   0  11   2 65.5359 63.4343   3
   0  11  -2 35.5703 50.4411   3
   0  11   3 1890.13 443.635  10
   0  11   3 2340.31 202.631   3
   0  11   3 2031.94 277.967   8
   0  11  -3 2166.69 184.915   3
   0  11  -3 2132.73 233.086   7
   0  11   4 52.3574 129.483   8
   0  11   4 40.0087 50.2220   3
   0  11   4 53.7417 167.489  10
   0  11   5 39341.4 1726.12   3
   0  11   5 35880.9 1916.23   8
   0  11   6-17.9654 125.203   8
   0  11   6 52.7672 51.0740   3
   0  11   7 2730.47 320.926   8
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   0  12  -1 167.993 97.3243   7
   0  12   1 175.425 124.810   8
   0  12  -2 3095.88 293.083   7
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   0  12  -2 3094.45 234.036   3
   0  12   3-50.6982 170.658  10
   0  12  -3 101.252 80.9750   7
   0  12  -3 17.1540 37.8177   3
   0  12   3 22.6267 53.4383   3
   0  12   3 33.0660 109.303   8
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   0  12   4 314.272 78.2033   3
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   0  12   6 7440.14 399.289   3
   0  12   7 102.354 106.955   8
   0  12   8 22.4753 75.6597   8
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   0  13   0-7.40235 48.9373   3
   0  13  -1 3909.18 279.349   3
   0  13  -1 4500.82 359.442   7
   0  13   1 4093.95 293.995   3
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   0  13  -2 29.7594 39.3489   3
   0  13  -2 11.6414 66.2374   7
   0  13  -3 2353.31 178.422   3
   0  13   3 2162.85 283.496   8
   0  13   3 2735.89 218.093   3
   0  13   4 60.6820 56.3364   3
   0  13   4 127.548 118.317   8
   0  13   5 688.173 178.124   8
   0  13   5 974.973 116.691   3
   0  13   6-13.6847 93.7584   8
   0  13   6-5.66446 43.8373   3
   0  13   7 2515.83 257.798   8
   0  14   0 52366.7 2395.87   7
   0  14   0 49991.6 2281.48   3
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   0  14  -1-11.2330 82.1003   7
   0  14  -1 34.5436 53.8309   3
   0  14   1 47.1675 56.8702   3
   0  14  -2 35231.9 1620.59   3
   0  14  -2 37201.4 1729.27   7
   0  14  -3 34.5711 35.2824   3
   0  14   3 42.1121 97.8336   8
   0  14   3 52.9052 53.2399   3
   0  14   4 15661.1 729.449   3
   0  14   4 11933.4 807.468   8
   0  14   5 49.2339 84.3293   8
   0  14   5-11.0499 42.7566   3
   0  14   6-102.494 94.1334   8
   0  15   0 10.3468 35.4452   3
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   0  15   1 432.451 76.7003   3
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   0  15  -1 352.639 64.7978   3
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   0  15  -2 41.6805 28.9890   3
   0  15   3 10.9691 41.2812   3
   0  15   3-10.7744 68.5391   7
   0  15   4 86.6400 49.0921   3
   0  15   5 1055.52 107.056   3
   0  16   0 4283.84 248.171   3
   0  16   0 4223.65 297.444   7
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   1  14   0 13.0006 42.1791   3
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   2   0   4 36286.2 1761.31   6
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   2   0   5 73527.4 3331.02   6
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   2   0   6 59226.0 2868.11   6
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   2  -1   6 4685.86 457.748   6
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   2   1   6 3879.21 446.374   6
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   2   2   1 449.244 92.1388  10
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   2   2   5 52756.6 2632.56   6
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   2  -2   6 2524.61 328.513   6
   2   2   6 2498.05 361.169   6
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   2   2   7 13033.0 1020.24   6
   2  -2   7 14585.8 994.435   6
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   2   2   8 6489.74 741.970   6
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   2  -2   9 11509.5 811.681   4
   2   2   9 11951.5 877.655   4
   2   2   9 10980.2 1131.56   6
   2   2  10 812.772 218.624   4
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   2   3   0 36192.4 1716.40  10
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   2  -3   6 1614.13 274.771   6
   2   3   6 929.025 262.197   6
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   2   3   7 13962.9 1139.18   6
   2  -3   8 226.505 182.395   4
   2  -3   8 657.864 225.498   6
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   2   3   8 563.958 271.919   4
   2   3   8 433.128 253.232   6
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   2   4   7 9016.41 827.350   4
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   2   4   7 7674.11 870.844  10
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   2   4   9 4540.71 523.097   4
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   2   5   7 2873.98 550.789  10
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   2   5   7 3155.52 566.918   6
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   2   5   7 2420.43 396.939   4
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   2  -5   8 946.118 261.441   6
   2   5   8 601.399 244.387   4
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   2   5   8 292.784 259.571  10
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   2   5   9 1060.86 259.610   4
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   2   5  10 885.320 200.078   4
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   2   6  -1 26229.7 1263.93   8
   2   6   1 28934.8 1517.54  10
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   2   6   2 55667.0 2479.99   8
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   2   6   4 24932.8 1504.60   6
   2   6   5 2937.47 230.946   3
   2   6   5 2820.02 491.077  10
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   2   6   6 1475.38 389.644  10
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   2   6   7 368.964 232.452   6
   2   6   7-18.3547 134.408   4
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   2  -6   7 456.331 190.221   6
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   2   6   7 278.387 235.086  10
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   2  -6   8 1840.82 362.623   6
   2   6   8 1187.24 249.445   4
   2   6   8 739.878 336.721  10
   2  -6   9 824.521 181.554   4
   2   6   9 287.919 156.253   4
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   2   6  10 912.740 154.579   4
   2  -6  10 1106.36 158.411   4
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   2   7   0 88691.0 4133.65  10
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   2   7   0 85889.2 3839.15   8
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   2   7   1 450.108 178.594  10
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   2   7   1 658.645 116.494   8
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   2   7  -1 484.749 100.419   8
   2   7   2 43674.7 2242.67  10
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   2   7  -2 40963.9 1856.21   7
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   2   7   2 40807.7 1897.35   8
   2   7   3 1050.40 165.889   8
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   2   7  -3 1146.02 142.841   7
   2   7   3 936.304 273.205  10
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   2   7   4 35290.4 1990.11  10
   2   7   5 1639.48 160.026   3
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   2   7   5 1986.53 428.013  10
   2   7   6 1105.98 350.356  10
   2   7   6 875.963 125.962   3
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   2   7   7 4047.03 704.678  10
   2  -7   7 6216.62 639.737   6
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   2   7   8 256.772 125.939   4
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   2   7   9 232.125 100.811   4
   2   7  10 2256.00 267.656   8
   2  -7  10 1838.25 152.259   5
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   2   8   0 45645.1 2116.00   8
   2   8   1 5082.99 577.947  10
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  -2   8   1 5781.06 589.260  10
   2   8   1 5549.41 399.542   8
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   2   8   2 14854.7 1084.40  10
   2   8   2 14333.5 786.823   8
   2   8  -2 14040.9 740.744   7
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  -2   8  -2 13109.5 730.785   7
  -2   8  -3 1912.50 189.569   7
   2   8  -3 1925.42 191.035   7
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  -2   8   3 2114.92 382.478  10
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   2   8   3 2606.22 439.769  10
   2   8   3 1811.76 224.361   8
   2   8   3 1373.59 142.989   3
   2   8   4 4136.58 283.928   3
  -2   8   4 4627.83 270.329   3
   2   8   4 4827.12 399.211   8
  -2   8   4 3684.33 561.809  10
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   2   8   5 7799.69 458.081   3
   2   8   5 8981.77 608.594   8
  -2   8   5 9573.72 969.098  10
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  -2   8   5 7865.19 426.786   3
   2   8   5 7891.36 908.477  10
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  -2   8   6-6.10324 38.8251   3
   2   8   6 7.67426 49.7854   3
  -2   8   6-55.8035 200.808  10
   2   8   6 54.5174 117.890   8
   2   8   6 55.8602 201.012  10
   2   8   7 330.576 155.151   8
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   2  -8   7 447.619 182.469   6
  -2   8   7 183.354 206.217  10
   2   8   7 481.268 286.727  10
  -2   8   8 365.013 173.951   8
   2   8   8 575.577 185.341   8
   2   8   9 270.033 141.336   8
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  -2   8  10 984.495 176.818   8
   2   8  10 1133.68 188.214   8
   2   9   0 24765.2 1261.32   8
   2   9   0 24593.8 1217.84   3
  -2   9   0 25965.5 1262.77   8
  -2   9   1 497.062 212.386  10
   2   9   1 819.297 159.014   8
  -2   9   1 661.338 101.269   3
  -2   9   1 485.914 123.615   8
   2   9   1 456.721 215.924  10
   2   9   1 600.249 101.061   3
   2   9  -1 622.064 113.419   3
   2   9  -2 4091.50 305.644   3
  -2   9   2 3811.72 532.642  10
   2   9   2 4273.15 577.882  10
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   2   9  -2 3943.27 309.080   7
  -2   9   2 3742.99 265.049   3
   2   9   2 4128.23 352.465   8
   2   9   3 449.248 88.5214   3
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   3   3   6 25803.1 1730.43   4
   3  -3   6 29066.6 1569.09   6
   3  -3   6 24938.3 1504.51   4
   3   3   6 25654.3 1602.76   6
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   3   3   7 365.287 280.844   4
   3  -3   7 738.100 238.770   6
   3  -3   7 217.370 198.341   4
   3   3   7 478.328 238.567   6
   3   3   8 12458.8 975.528   4
   3  -3   8 9835.40 787.329   4
   3   3   8 11801.8 1124.50   6
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   3   4   5 8585.04 794.185  10
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   3   4   6 4327.43 561.985   4
   3   4   6 5291.16 643.478  10
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   3  -4   6 6193.83 575.677   6
   3   4   7 2058.40 448.144  10
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   3   4   7 2115.71 418.893   4
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   3   4   7 1581.52 393.346   6
   3   4   8 1030.68 317.424   4
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   3   4   8 1105.32 360.055  10
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   3   4   8 1147.33 362.702   6
   3   4   9 533.576 242.133   4
   3  -4   9 1042.17 232.771   4
   3  -4  10 1462.42 241.256   4
   3   4  10 1124.18 236.817   4
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   3   4  11 1611.08 196.097   4
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   3   5   3 11402.3 828.345  10
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   3   5   3 13067.8 836.001   6
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   3  -5  -4 31126.4 1444.81  11
   3   5   4 32995.8 1766.67   6
   3   5   4 29124.3 1764.65  10
   3  -5   4 28311.8 1465.01  11
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   3   5   6 24932.2 1520.52   4
   3   5   6 28004.5 1867.48  10
   3   5   7 524.777 231.577   4
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   3   5   7 951.753 337.937  10
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   3   6   1 156325. 6713.12   8
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   3  15   3 49.2676 65.1508   7
   3  15   4 104.875 74.4649   7
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   3 -15   5 51.5342 22.0710   5
  -3  15   5 33.0455 33.4276   3
  -3  16   0-10.2510 29.8164   3
   3  16   0-13.2807 54.1023   7
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   3  16   1 2769.25 217.780   7
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   3  16   1 2617.67 179.991   3
  -3  16  -1 2603.45 163.366   3
  -3  16  -2 132.985 30.8694   3
   3  16   2 146.920 46.7928   3
  -3  16   2 181.662 43.4545   3
  -3  16   3 1303.18 91.8886   3
  -3  16  -3 234.578 30.7660   3
   4   0   0 15579.7 787.844  11
   4   0  -1 4077.24 275.693  11
   4   0   1 3752.06 274.353  11
   4   0  -2 4088.04 285.710  11
   4   0   2 4328.91 303.176  11
   4   0   3 335.674 87.9816   6
  -4   0   4 71.6888 99.4370   6
  -4   0   5 3767.46 462.182   6
   4   0   6 5063.28 749.807   4
   4   0   6 4838.53 515.362   6
   4   0   7 391.047 186.447   6
   4   0   7 647.122 304.658   4
   4   0   8 673.462 225.472   4
   4   0   8 1052.37 304.900   6
   4   0   9 4816.23 457.737   4
   4   0  10 855.083 196.513   4
   4   0  11 2792.83 268.881   4
   4  -1   0 163941. 6977.14  11
   4   1   0 159853. 6899.67   6
   4  -1  -1 7242.31 398.300  11
   4  -1   1 6505.66 392.602  11
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   4   1   1 6244.32 364.164  10
   4   1   1 6844.71 369.857   6
   4  -1  -2 79186.0 3508.09  11
   4  -1   2 79470.6 3519.14  11
   4   1   2 79862.2 3528.73   6
   4  -1   3 4111.74 288.074  11
   4  -1  -3 3866.13 269.279  11
   4   1   3 3718.37 310.663   6
  -4  -1   4 36534.5 1646.11   6
   4   1   4 27158.1 1552.76   6
  -4   1   5 20915.2 1348.06   6
   4  -1   6 2325.20 509.383   4
   4   1   6 1912.16 623.752   4
   4  -1   6 2642.59 374.702   6
  -4   1   6 2825.59 435.278   6
   4  -1   7 4287.17 548.131   4
   4  -1   7 5674.81 602.467   6
   4   1   7 4556.61 569.773   6
   4  -1   8 369.846 189.904   4
   4  -1   8 783.608 258.082   6
   4   1   8 607.497 254.032   6
   4  -1   9 578.453 172.206   4
   4  -1  10 231.284 134.249   4
   4  -1  11 32.9508 97.8279   4
   4  -2   0 12340.2 613.029  11
   4   2   0 10782.3 543.509   6
   4  -2   1 17926.2 931.873  11
   4  -2  -1 20062.5 939.837  11
   4   2   1 18466.8 937.982  10
   4   2   1 19287.9 908.796   6
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   4  -2   2 15322.5 798.704  11
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   4  -2  -2 15774.1 791.746  11
   4   2   2 16017.9 813.935   6
   4   2   2 16508.7 851.095  10
   4  -2   3 713.764 105.103  11
   4  -2  -3 646.874 94.3538  11
   4   2   3 612.431 122.706   6
   4  -2  -4 4744.51 323.330  11
   4  -2   4 5614.48 357.476  11
   4   2   4 5313.40 442.291   6
   4  -2   5 23257.5 1326.39   6
   4  -2   6 2431.14 460.914   4
   4   2   6 2647.57 627.149   4
   4  -2   6 2131.26 341.057   6
   4  -2   7 15963.4 1103.45   6
   4   2   7 13472.4 1135.61   4
   4   2   7 13064.7 1059.54   6
   4  -2   8 20.5404 138.323   4
   4   2   8 57.3142 192.954   4
   4  -2   8 164.400 165.390   6
   4   2   8 92.4685 131.574   6
   4   2   9 2952.31 398.030   4
   4  -2   9 2931.75 349.378   4
   4   2  10 2629.72 332.839   4
   4  -2  10 2363.88 291.717   4
   4  -2  11 617.622 145.806   4
   4   2  11 578.034 133.067   4
   4   3   0 1070.60 150.246  10
   4  -3   0 1226.43 156.879  11
   4  -3   1 8822.29 502.900  11
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   4  -3  -1 8249.86 486.671  11
   4   3   1 7569.81 461.205   6
   4   3   1 6948.68 487.780  10
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   4   3   2 9180.27 614.798  10
   4  -3   2 9038.34 547.940  11
   4  -3  -2 9963.61 544.988  11
   4   3   2 9122.78 568.801   6
   4   3   3 747.722 175.928  10
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   4  -3  -3 899.033 120.811  11
   4   3   3 795.768 154.093   6
   4  -3   3 993.870 134.431  11
   4  -3  -4 174.060 55.0433  11
   4  -3   4 135.769 58.7800  11
   4   3   4 219.558 114.249   6
   4  -3   5 5907.56 508.512   6
   4   3   5 4395.98 490.749   6
   4  -3   6 11891.7 872.062   6
   4   3   6 10572.8 1047.81   4
   4  -3   6 9456.20 840.342   4
   4  -3   7 471.662 241.252   4
   4   3   7 669.641 336.700   4
   4  -3   7 340.227 194.478   6
   4   3   8 450.021 266.159   4
   4   3   8 527.107 269.356  10
   4  -3   8 461.595 190.329   4
  -4   3   8 925.532 322.954  10
   4  -3   8 614.999 245.880   6
   4   3   8 704.323 307.931   6
   4   3   9 284.846 208.615   4
   4  -3   9 215.751 155.478   4
   4   3  10 242.602 152.401   4
   4  -3  10 257.357 136.609   4
   4  -3  11 188.040 113.778   4
   4   3  11 228.954 100.884   4
  -4  -3  11 234.960 126.230   4
  -4   3  11 152.724 108.713   4
  -4   4   0 100325. 4448.04  10
   4   4   0 97115.5 4441.01  10
  -4   4   1 44951.0 2152.20  10
   4   4   1 44929.7 2090.33   6
   4   4   1 43400.3 2147.22  10
   4   4   2 3054.89 332.756  10
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   4  -4   2 2354.56 257.752  11
   4  -4  -2 3114.52 267.837  11
   4   4   2 2856.59 286.398   6
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   4  -4   3 23208.4 1207.49  11
   4  -4  -3 24421.8 1178.34  11
   4   4   3 24635.2 1317.83   6
   4   4   3 23751.9 1377.09  10
   4  -4  -4 11608.5 614.914  11
   4   4   4 11963.1 816.033   6
   4   4   4 12223.1 886.479  10
   4  -4   4 9805.67 611.541  11
  -4   4   4 9446.46 779.542  10
  -4   4   5 37582.1 2139.87  10
   4   4   5 36869.9 2161.84  10
   4   4   5 38791.8 2115.69   6
   4   4   6 1480.41 360.811  10
   4  -4   6 1667.78 327.634   4
   4   4   6 1746.61 391.426   4
   4  -4   6 1563.65 301.258   6
  -4   4   6 1164.59 325.694  10
   4   4   6 1659.76 360.257   6
   4  -4   7 20897.3 1309.66   4
   4   4   7 21884.5 1475.16   4
   4   4   7 18016.7 1555.26  10
  -4   4   7 21196.6 1618.04  10
  -4   4   8 2601.38 522.637  10
   4   4   8 2525.81 442.278   4
   4  -4   8 2351.54 356.740   4
   4  -4   8 3698.77 535.822   6
   4   4   8 1912.16 484.243  10
   4  -4   9 7064.67 540.502   4
   4   4   9 7079.47 636.244   4
   4  -4  10 1649.17 246.798   4
   4   4  10 1583.62 272.862   4
   4   4  11 267.395 97.9891   4
  -4  -4  11 459.031 127.841   4
   4  -4  11 548.255 127.082   4
  -4   4  11 647.207 135.440   4
   4   5   0 691.152 159.412  10
   4   5   1 28568.0 1529.95  10
  -4   5   1 28461.8 1526.66  10
  -4   5   2 1236.58 241.295  10
   4   5   2 1223.51 235.850  10
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   4   5  -2 833.151 106.236   7
  -4   5  -2 1207.38 127.833   7
   4   5   2 986.367 130.466   8
   4   5   2 1392.65 224.770   6
   4  -5   3 11826.2 712.221  11
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   4   5   3 10252.5 838.289  10
   4  -5  -3 10885.7 657.346  11
   4   5   3 12011.9 818.351   6
   4  -5  -4 1011.94 154.640  11
  -4   5   4 729.314 221.587  10
   4  -5   4 1018.00 166.832  11
   4   5   4 1524.54 330.561  10
   4   5   4 1405.41 278.654   6
   4   5   5 2417.22 302.428   4
  -4   5   5 3623.65 505.613  10
   4   5   5 2811.63 449.161   6
   4   5   5 2645.85 482.656  10
   4   5   6 1043.01 342.317  10
   4  -5   6 611.550 205.284   4
   4   5   6 724.449 225.234   4
  -4   5   6 459.737 256.439  10
   4  -5   6 705.279 225.833   6
   4   5   6 513.907 239.089   6
   4   5   7 2281.42 527.050  10
   4  -5   7 2308.42 355.340   4
   4   5   7 2803.80 403.658   4
   4  -5   7 3372.19 477.855   6
  -4   5   7 2735.29 550.277  10
   4   5   7 2163.18 485.213   6
   4   5   8 184.489 235.394  10
  -4   5   8 408.496 257.808  10
   4   5   8 489.335 213.098   4
   4  -5   8 387.814 177.079   4
   4  -5   8 641.917 240.075   6
   4  -5   9 1269.63 242.914   4
   4   5   9 1131.37 259.754   4
   4  -5   9 748.480 109.877   5
   4   5  10 2416.05 290.844   4
   4  -5  10 2534.50 279.186   4
  -4   5  11 13.5708 67.4577   4
   4  -5  11 117.482 62.3045   4
   4   5  11 97.7823 59.6896   4
  -4  -5  11-5.48820 59.6958   4
   4   5  11 33.8904 47.7598   2
   4   6   0 37045.8 1722.98   8
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   4   6   1 745.756 199.407  10
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  -4   6  -1 709.138 101.963   7
   4   6   1 619.124 107.773   8
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   4   6   2 5125.41 350.237   8
   4   6   2 5169.90 528.343  10
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   4   6  -2 4599.32 307.683   7
  -4   6   2 4988.84 516.096  10
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   4   6   3 4692.63 346.003   8
   4   6   3 4431.99 527.981  10
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   4   6  -3 4268.12 292.339   7
   4   6   3 5265.46 516.073   6
   4  -6   4 7444.57 509.646  11
   4   6   4 6047.74 708.655  10
   4  -6  -4 8695.11 513.012  11
   4   6   4 6018.39 398.203   3
   4   6   4 7454.98 702.549   6
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   4   6   5 7039.37 505.083   4
  -4   6   5 7334.95 796.415  10
   4   6   5 8238.98 808.930   6
   4   6   5 6485.36 799.628  10
   4   6   6 8524.74 617.471   4
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   4  -6   6 8461.50 623.662   4
   4   6   6 7161.31 904.122  10
   4   6   6 9523.67 959.754   6
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   4   6   7 54.7197 124.971   4
   4   6   7-59.6778 169.777  10
   4  -6   7 136.761 142.624   4
   4  -6   7 70.2129 126.334   6
   4   6   7-52.2632 175.924   6
   4  -6   8-173.987 175.531   4
   4   6   8-112.461 167.032   4
   4  -6   9-176.349 171.109   4
   4   6   9-94.4728 182.503   4
   4  -6   9 38.1170 44.2693   5
   4   6  10 284.226 119.301   8
   4   6  10 488.105 114.590   4
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   4   7   0 34898.4 1649.82   8
  -4   7   0 35357.0 1652.97   8
   4   7   1 5493.94 559.332  10
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   4   7   1 5134.68 356.860   8
   4   7  -1 4504.83 321.926   7
  -4   7  -1 4833.28 328.566   7
  -4   7   1 4991.87 538.663  10
   4   7   2 24268.3 1128.37   8
   4   7   2 23333.9 1438.22  10
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   4   7  -2 20326.4 1055.42   7
  -4   7  -2 20808.4 1057.66   7
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   4   7   3 20362.4 1024.12   8
  -4   7   3 17807.8 976.872   8
  -4   7   3 18380.9 1271.96  10
   4   7  -3 17780.6 934.970   7
   4   7   3 20599.7 1382.74  10
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   4  -7  -4 13515.8 710.108  11
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   4   7   4 10089.9 971.127  10
   4   7   4 11320.1 671.792   8
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   4   7   4 7118.22 514.784   3
   4  -7   4 10542.8 670.140  11
  -4   7   4 10737.3 510.782   3
  -4   7   5 16453.7 1265.59  10
  -4   7   5 15015.7 841.745   8
   4   7   5 14260.8 1247.21  10
   4   7   5 12082.4 705.645   3
  -4   7   6-53.8834 216.786  10
   4   7   6 56.6543 176.557  10
  -4   7   7 2283.05 533.745  10
   4   7   7 3209.37 320.634   4
   4   7   7 2144.59 520.923  10
   4  -7   7 3749.35 501.685   6
  -4   7   8 168.733 130.975   8
   4   7   8 233.438 119.343   4
   4   7   8 254.469 141.184   8
   4   7   9 3587.43 375.775   8
  -4   7   9 3624.26 359.351   8
   4  -7   9 3808.07 265.562   5
   4  -7  10 2869.50 177.606   5
  -4   7  10 2317.30 243.147   8
   4   7  10 2629.33 271.978   8
  -4   8   0 4905.42 360.379   8
   4   8   0 4915.78 358.966   8
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   4   8  -1 4697.84 323.426   7
   4   8   1 4513.36 341.604   8
   4   8   1 4468.95 537.404  10
   4   8   1 3241.04 265.419   3
  -4   8   1 4006.53 325.719   8
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  -4   8   2 1805.42 212.045   8
   4   8   2 2127.58 382.656  10
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   4   8  -2 1719.30 181.381   7
   4   8   2 1997.87 227.151   8
   4   8   2 901.401 122.223   3
   4   8   3-40.6241 155.123  10
   4   8   3 79.9084 100.351   8
  -4   8   3 155.056 51.9868   3
  -4   8   3 247.409 185.461  10
   4   8  -3 102.599 62.6610   7
  -4   8   3 69.6345 94.6602   8
  -4   8  -3 84.4455 69.7826   7
   4  -8  -4 626.930 138.465  11
   4  -8   4 190.943 91.0119  11
  -4   8   4 194.941 56.9316   3
   4   8   4 47.6012 160.500  10
   4   8   4 239.565 77.2834   3
  -4   8   4 368.561 208.610  10
  -4   8   4 146.951 102.402   8
   4   8   4 201.308 120.199   8
  -4   8   5 729.941 298.370  10
   4   8   5 1082.44 384.507  10
   4   8   5 1094.84 216.324   8
   4   8   5 531.583 109.741   3
  -4   8   5 761.781 178.463   8
   4   8   6-19.1703 109.081   8
  -4   8   6-18.2008 111.061   8
   4   8   6-58.9802 183.809  10
  -4   8   6-55.9938 188.484  10
   4   8   7 412.158 156.453   8
  -4   8   7 212.797 135.402   8
  -4   8   8 799.177 191.457   8
   4   8   8 628.553 187.663   8
   4  -8   9 102.735 59.0874   5
  -4   8   9-13.4333 90.4550   8
   4   8   9-29.9231 100.741   8
   4   8  10 319.697 98.2200   2
   4  -8  10 266.405 47.8443   5
  -4   9   0 12321.3 673.926   8
   4   9   0 11277.3 659.085   8
  -4   9   1 7356.12 490.792   8
   4   9   1 8148.53 514.775   8
  -4   9  -1 7490.96 470.780   7
   4   9  -1 7748.48 474.683   7
   4   9   1 6066.13 427.733   3
   4   9  -1 6027.11 458.834   3
   4   9  -2 1012.81 150.157   7
   4   9   2 983.914 178.398   8
  -4   9   2 675.948 159.552   8
  -4   9   2 976.602 289.095  10
   4   9   2 831.693 292.122  10
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  -4   9  -2 801.168 135.107   7
   4   9   2 726.354 115.530   3
  -4   9   3 2099.59 174.245   3
   4   9   3 2416.29 484.345  10
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   4   9   3 2006.88 265.097   8
   4   9  -3 1791.53 204.836   7
  -4   9  -3 2336.50 224.676   7
  -4   9   3 1941.56 249.185   8
   4   9   4 333.844 86.5009   3
  -4   9   4 315.419 229.947  10
   4  -9  -4 381.878 153.954  11
  -4   9   4 508.245 80.0098   3
   4   9   4 372.976 150.410   8
  -4   9   4 483.860 145.504   8
   4  -9   4 239.084 133.260  11
   4   9   4 468.513 265.470  10
   4   9   5 3596.21 386.160   8
   4   9   5 3196.99 271.065   3
   4   9   5 3108.38 611.424  10
  -4   9   5 2743.15 549.280  10
  -4   9   5 3085.28 347.698   8
  -4   9   5 3477.50 236.636   3
   4   9   6 2289.93 533.552  10
  -4   9   6 2300.58 525.478  10
  -4   9   6 2125.34 300.392   8
   4   9   6 2093.16 304.837   8
   4   9   7 1733.42 279.405   8
  -4   9   7 2169.51 294.884   8
  -4   9   8 191.858 119.009   8
   4   9   8 283.203 142.512   8
  -4   9   9 33.5705 83.0345   8
   4   9   9 50.1224 88.7814   8
   4  -9   9 44.8534 46.2651   5
   4  10   0 14194.1 812.366   3
  -4  10   1 5304.90 412.192   8
   4 -10   1 5062.38 325.140   5
   4  10   1 5120.21 415.055   8
   4  10  -1 5030.57 381.350   7
  -4  10  -1 5441.50 396.062   7
   4  10   1 4445.73 365.806   3
   4  10  -1 4777.08 374.664   3
  -4  10   2 9463.42 514.201   3
   4  10   2 10108.0 644.979   8
  -4  10   2 9956.68 620.405   8
   4  10  -2 8770.55 561.535   7
  -4  10  -2 9395.38 567.798   7
   4  10   2 8928.79 930.064  10
   4  10   2 7802.53 534.694   3
  -4  10   2 7951.63 867.552  10
  -4  10   3 2489.39 195.194   3
   4  10  -3 1967.02 217.840   7
   4  10   3 2527.36 508.304  10
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  -4  10   3 1963.74 261.248   8
   4  10   3 2261.89 289.808   8
  -4  10  -3 2121.21 225.230   7
   4 -10   4 3615.21 390.495  11
   4  10   4 2541.90 570.587  10
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   4 -10  -4 4493.64 423.014  11
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   4  13   6 109.905 73.4699   2
   4 -13   7 653.077 80.5119   5
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   5   0   0 231.499 76.0766  11
   5   0   1 153894. 6624.28  11
   5   0  -1 148363. 6612.51  11
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   5   0   4 65333.5 3072.26   6
   5   0   5 43263.4 2207.88   6
   5   0   6 52532.4 3167.52   4
   5   0   7 2998.31 552.313   4
   5   0   8 963.352 266.336   4
   5   0   8 2616.25 472.938   6
   5   0   9 482.134 175.707   4
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   5   0  11 1181.08 176.250   4
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   5   1   2 309.095 79.5547   6
   5  -1  -3 1560.77 174.165  11
   5   1   3 1662.28 201.519   6
   5  -1   3 1612.97 187.897  11
   5  -1   4 122.207 75.4766   6
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   5   1   6 220.502 161.106   6
   5  -1   7 33.0805 230.522   4
   5  -1   7-33.5534 95.4600   6
   5  -1   8 2781.54 468.767   6
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   5   1   8 3109.97 525.448   6
   5  -1   9 948.820 212.863   4
   5  -1  10 410.030 141.276   4
   5  -1  11 1289.48 180.878   4
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   5   2   6 13560.1 1061.41   6
   5   2   6 18332.9 1568.64   4
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   5  -3   6 12005.4 904.742   6
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   5   3   6 10601.3 998.149  10
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   5   3   7-48.4412 326.209  10
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   5  -3   8 3954.79 453.169   4
   5  -3   9 3132.49 368.410   4
   5   3   9 4110.09 504.258   4
   5   3  10 813.178 161.406   2
   5  -3  10 1208.73 213.280   4
   5   3  10 834.597 223.349   4
   5  -3  11 783.730 151.690   4
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   5   3  11 719.647 138.348   4
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   5   4   6 3649.43 581.404  10
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   5   4   6 4194.69 560.554   4
   5  -4   6 4814.37 512.959   6
   5   4   6 4469.41 579.769   6
   5   4   7 324.119 238.210  10
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   5  -4   7 254.592 202.435   4
   5   4   7 146.438 259.449   4
   5  -4   7 301.734 153.994   6
   5   4   7 189.114 199.654   6
   5  -4   8 1385.07 178.305   5
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   5  -4   8 2175.96 337.815   4
   5   4   8 2311.78 436.807   4
   5   4   8 1917.06 484.383  10
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   5   4   8 1918.77 460.213   6
   5  -4   9 92.2427 47.1324   5
   5  -4   9 72.7062 132.912   4
   5   4   9 334.255 221.352   4
   5   4  10 385.546 119.468   2
   5  -4  10 425.932 143.450   4
   5   4  10 619.074 201.485   4
   5  -4  11 168.246 84.1669   4
   5   4  11 110.518 71.9430   4
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   5   5   2 5857.82 551.648  10
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   5  -5   3 6414.67 492.699  11
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   5   5   4 224.656 133.692   6
   5   5   5 86.2592 145.339  10
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   5  -5   5 327.880 147.476   4
   5   5   5 129.817 111.388   4
   5   5   5 105.629 141.822   6
   5   5   6 1071.64 333.526  10
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   5  -5   6 1179.57 259.337   4
   5   5   6 911.807 236.819   4
   5  -5   6 1027.96 236.923   6
   5   5   6 872.421 316.550   6
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   5   5   7 2145.84 366.721   4
   5   5   7 2115.04 520.559  10
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   5  -5   7 2071.81 367.302   6
   5   5   7 2128.85 471.401   6
   5   5   8 1869.30 353.506   4
   5  -5   8 1177.29 153.949   5
   5   5   9 2881.71 386.774   4
   5  -5   9 2421.03 308.185   4
   5   5  10 142.982 110.804   8
   5  -5  10 112.872 107.618   4
   5   5  10 122.503 93.8372   2
   5   5  10 175.316 121.460   4
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   5   6   0 164.491 70.8815   8
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   5   6   1 19646.0 953.042   8
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   5  -6   2 2777.50 339.944  11
   5   6   2 2430.83 233.208   8
   5   6   3 51783.6 2840.26  10
   5  -6   3 57501.7 2619.43  11
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   5  -6  -3 61560.2 2583.57  11
   5   6   3 52956.1 2479.37   8
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   5   6   3 56422.3 2750.65   6
   5   6   4 2362.67 445.672  10
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   5   6   4 2549.43 278.463   8
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   5   6   4 2132.31 206.895   3
   5  -6  -4 3500.65 313.888  11
   5  -6   4 2884.41 311.217  11
   5   6   4 2569.38 405.993   6
   5   6   5 867.449 309.106  10
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   5   6   5 778.685 166.809   4
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   6   0  -1 42870.8 1980.54  11
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   6   0   3 41294.5 2153.10   6
   6   0   4 35492.2 1804.34   6
   6   0  -4 35061.2 1588.06   9
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   6   0   5 15349.5 992.810   6
   6   0   6 7876.67 1095.05   4
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   6   0   6 7335.27 655.415   6
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   6   0   7 17973.6 1229.59   6
   6   0   7 16141.0 1377.18   4
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   6   0   9 3714.31 404.292   4
   6   0  10 642.802 156.692   4
   6   0  11 106.601 82.4051   4
   6   1   0 30927.5 1357.05   9
   6   1   0 27872.2 1316.75   6
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   6   1   5 10334.4 803.111   6
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   6   1   6 147.013 149.786   6
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   6   1   8-52.2911 161.450   2
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   6  -2  -4 11954.5 755.977  11
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   6  -2   5 923.499 156.216   5
   6  -2   5 819.806 287.908   4
   6   2   5 1114.80 332.176   4
   6  -2   5 1416.92 251.977   6
   6   2   5 1113.24 235.484   6
   6  -2   6 407.282 118.327   5
   6  -2   6 385.968 357.949   4
   6   2   6 324.055 553.430   4
   6   2   6 506.437 198.110   6
   6  -2   7 61.7881 72.9941   5
   6   2   7 148.841 199.625  10
   6  -2   7-251.888 360.489   4
   6   2   7-243.130 578.697   4
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   6   2   7 275.090 180.289   6
   6   2   8 1592.85 439.235  10
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   6   2   8 1602.93 426.956   4
   6  -2   8 2116.22 393.505   6
   6   2   8 1603.26 390.082   6
   6   2   9-59.0382 109.504   2
   6   2   9 171.449 192.095   4
   6  -2   9 138.169 130.005   4
   6  -2  10 1205.76 205.632   4
   6   2  10 1295.67 238.505   4
   6  -2  11 52.2810 78.4053   4
   6   2  11 26.1660 71.9325   4
   6   3   0 51497.5 2328.11   9
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   6   3   4 16698.5 1102.26   6
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   6   3   5 23022.4 1365.33   4
   6  -3   5 20828.3 1244.30   6
   6  -3   5 18588.7 1133.39   5
   6   3   5 22274.9 1353.47   6
   6   3   6 352.685 217.582  10
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   6  -3   6 437.397 278.517   4
   6   3   6 345.355 376.816   4
   6   3   6 244.498 154.436   6
   6  -3   7 2576.13 267.803   5
   6   3   7 2902.76 567.522  10
   6  -3   7 2922.87 494.943   4
   6   3   7 4015.38 754.712   4
   6   3   7 3326.55 539.546   6
   6  -3   8 8.95870 56.9985   5
   6  -3   8 146.255 167.009   4
   6   3   8 162.689 253.503   4
   6  -3   8 36.2652 122.076   6
   6   3   8-50.9294 183.272   6
   6   3   9 1221.92 210.944   2
   6  -3   9 1439.14 259.870   4
   6   3   9 2042.68 383.385   4
   6   3  10 785.474 146.426   2
   6  -3  10 718.494 177.035   4
   6   3  10 685.502 206.566   4
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   6   4   5 4665.16 478.126   4
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   6   4   7 2203.25 457.912   6
   6  -4   8 150.233 65.0016   5
   6  -4   8 309.727 189.438   4
   6   4   8 264.353 249.764   4
   6   4   9 5305.21 572.466   4
   6  -4   9 4829.95 438.803   4
   6   4  10 2448.82 317.830   4
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   6   5   6 327.719 251.463  10
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   6  -5   6 514.473 223.294   4
   6   5   6 727.390 233.875   4
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   6   5   6 596.319 268.291   6
   6   5   7 1486.13 441.541  10
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   6  -5   7 1386.86 307.491   4
   6   5   7 1466.25 333.064   4
   6  -5   7 1597.86 316.820   6
   6   5   7 1399.51 398.899   6
   6  -5   8 883.434 130.806   5
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   6   5   8 1654.63 347.297   4
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   6  -5   9 233.848 63.8717   5
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   6   5   9 613.386 216.558   4
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   6   6   3 5768.51 443.976   8
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   6   6   5 393.312 140.731   4
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   6   6   7 1195.66 250.786   4
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   6  -6   8 22.7671 52.8853   5
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   6   8   0 26564.7 1276.36   7
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   6  -8   0 27118.5 1207.65   5
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   6  -8  -2 13679.3 899.858  11
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   6  -8  -4 8200.41 591.872  11
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   6   8   8 16.7113 99.7317   8
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   6   9   7 669.135 176.591   8
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   6  -9   8-6.61989 47.6434   5
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   6 -10   0 41745.2 1914.76   5
   6 -10   0 36897.8 2380.93  11
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   6  10   0 38724.7 2086.46   3
   6 -10   1 141.341 134.989  11
   6 -10  -1 34.8068 99.1875  11
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   6 -10   3 44.2127 68.9392  11
   6 -10   3 21.6969 71.7627   5
   6  10   3 130.289 81.1905   3
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   6  10   3 32.9242 98.2694   2
   6 -10  -3 67.8616 76.1852  11
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   6 -10   5 308.236 125.665   5
   6  10   5 203.372 131.321   8
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   6 -10   6 68.1805 72.2948   5
   6  10   6-69.3797 136.036   8
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   6  10   7 985.903 245.984   2
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   6  10   8 509.432 181.635   2
   6 -10   8 403.079 79.6734   5
   6 -11   0 7949.38 822.194  11
   6  11   0 9558.02 608.246   7
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   6  11   0 9905.49 653.192   3
   6 -11   1 5220.64 350.376   5
   6 -11  -1 4450.51 567.357  11
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   6 -11   1 5691.64 629.488  11
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   6  11  -1 4922.53 401.135   7
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   7   0   5 2585.44 354.619   6
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   7   0   6 2727.03 396.787   6
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   7   1   4 15802.3 998.674   6
   7  -1   4 16588.6 826.629   9
   7   1  -4 18827.3 809.322   1
   7  -1   5 1219.40 226.689   2
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   7   1   5 2064.69 438.439   4
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   7  -1   6 17710.4 979.773   5
   7  -1   6 17584.1 1095.88   2
   7   1   6 23054.4 1302.14   2
   7  -1   6 21596.0 1318.90   6
   7   1   6 21116.6 1347.73   6
   7   1   7-21.8899 189.224   2
   7  -1   7 105.344 402.234   4
   7  -1   7 469.958 196.038   6
   7   1   7 489.224 203.446   6
   7   1   8 3654.65 387.063   2
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   7   2   1 54948.0 2512.38   9
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   7   2  -3 41529.1 1894.59   9
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   7  -2   4 12646.9 850.829  11
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   7   2   4 12669.3 839.348   4
   7  -2   4 13047.4 823.702   4
   7   2  -4 15238.2 686.328   1
   7   2   4 11391.9 855.479   2
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   7   2   4 14221.8 910.279   6
   7  -2   5 235.119 98.4641   5
   7  -2   5 129.276 208.225   4
   7   2   5 133.680 240.681   4
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   7   2   5 162.350 129.102   6
   7  -2   6 3450.27 326.713   5
   7  -2   6 6801.62 807.134   4
   7   2   6 7662.27 1152.70   4
   7   2   6 3859.56 520.211   2
   7  -2   6 4196.07 492.489   6
   7   2   6 4134.61 541.703   6
   7  -2   7 102.735 73.9443   5
   7  -2   7-304.257 370.959   4
   7   2   7-167.037 552.128   4
   7   2   7-68.3885 174.018   2
   7  -2   7-32.0775 81.6275   6
   7   2   7 80.9155 145.590   6
   7   2   8 1642.96 273.469   2
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   7   2   8 2784.16 536.651   4
   7   2   9 54.6346 111.269   2
   7  -2   9-85.3338 130.280   4
   7   2   9 25.0232 168.460   4
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   7   3   1 2800.08 252.806   9
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   7   3   3 1728.71 278.509  10
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   7  -3   4 894.509 184.590  11
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   7   3   4 522.812 167.741   4
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   7  -3   5 79.8269 109.449   5
   7  -3   5-22.8209 207.379   4
   7   3   5 145.110 224.629   4
   7  -3   5 93.4972 103.085   6
   7   3   5 206.199 149.955   6
   7   3   5 41.2037 138.746  10
   7  -3   6 44.1425 83.7348   5
   7  -3   6 70.2789 244.872   4
   7   3   6 56.7638 338.737   4
   7  -3   6 27.7537 78.9718   6
   7   3   6 37.1449 105.684   6
   7  -3   7 177.340 89.2313   5
   7   3   7-23.3943 154.797   2
   7  -3   7 371.503 291.434   4
   7   3   7-278.574 468.897   4
   7  -3   7 280.116 148.308   6
   7   3   7 177.431 149.457   6
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   7   3   8 516.737 338.238   4
   7  -3   9-34.8989 127.533   4
   7   3   9 86.9512 221.250   4
   7   3   9-26.4573 95.2097   2
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   7  -4  -3 45653.1 2139.22  11
   7  -4   3 43301.7 2026.02   5
   7  -4   3 44756.6 2194.63  11
   7   4  -3 42999.6 1928.60   1
   7   4   3 42935.2 2204.87   6
   7  -4   4 5399.00 478.491  11
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   7  -4   4 5001.73 437.004   5
   7   4   4 4557.38 577.627  10
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   7   4   5 2089.49 332.849   4
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   7   4   5 2123.80 389.892   6
   7  -4   6 18344.6 1141.64   4
   7   4   6 19649.4 1295.12   4
   7  -4   6 13834.2 1001.11   6
   7  -4   6 11195.8 827.755   5
   7   4   6 14906.3 1204.07   6
   7  -4   7 83.2636 84.3440   5
   7  -4   7 31.2974 206.937   4
   7   4   7 94.3249 268.367   4
   7   4   7 146.131 151.848   6
   7  -4   8 2825.92 414.079   4
   7   4   8 1952.08 291.303   2
   7  -4   8 2522.51 226.392   5
   7   4   9 801.357 180.803   2
   7  -4   9 1617.07 260.741   4
   7   4   9 1498.43 334.647   4
   7   4  10 902.450 132.519   2
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   7   4  10 752.473 180.673   4
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   7  -5   2 2867.72 375.213  11
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   7   5   2 2723.71 292.993   2
   7   5  -2 2883.89 209.049   1
   7   5   3 7718.98 520.641   4
   7   5  -3 8891.75 468.253   1
   7  -5   3 8216.38 536.408   4
   7  -5   3 9132.56 693.203  11
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   7  -5  -3 8901.45 637.552  11
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   7   5   4 3643.03 347.144   4
   7  -5   4 3406.09 388.592   5
   7  -5  -4 4030.17 392.742  11
   7   5   4 3771.38 503.273   6
   7  -5   5 401.627 180.164   5
   7  -5   5 259.871 182.017   4
   7   5   5 515.204 185.495   4
   7   5   5 335.346 126.136   8
   7   5   5 280.154 177.024   6
   7  -5   6 1858.21 279.289   5
   7   5   6 2716.61 400.624   4
   7  -5   6 3132.59 412.465   4
   7   5   6 2852.18 511.706   6
   7  -5   7 711.765 139.254   5
   7  -5   7 1307.53 299.310   4
   7   5   7 932.501 220.975   8
   7   5   7 1519.02 337.012   4
   7   5   7 1337.08 389.102   6
   7  -5   8 1458.49 165.127   5
   7   5   8 1371.38 246.722   2
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   7   5   8 2605.62 405.001   4
   7   5   9 239.582 120.324   2
   7  -5   9 188.507 52.2073   5
   7  -5   9 136.505 133.643   4
   7   5   9 194.322 178.461   4
   7  -5  10 1148.74 137.531   4
   7   5  10 911.029 137.466   4
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   7   6   1 2867.78 283.415   2
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   7  -6  -2 5861.87 338.200   5
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   7   6   2 5326.44 448.613   2
   7  -6   3 119.640 142.822  11
   7  -6   3 61.4914 88.5641   5
   7   6   3 140.810 134.395  10
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   7   6   3 57.0982 125.860   2
   7   6  -3 6.15743 55.4794   1
   7   6   4 171.840 151.937   6
   7  -6   4 296.541 124.069  11
   7  -6  -4 327.869 121.007  11
   7   6   4 216.127 198.642  10
   7   6   4 304.497 109.129   4
   7  -6   5 156.177 144.741   5
   7  -6   5-123.987 207.744   4
   7   6   5-29.9325 180.642   4
   7   6   5 153.764 128.599   8
   7   6   5-41.2667 138.911   6
   7   6   6 982.225 316.642   6
   7  -6   6 564.233 161.747   5
   7  -6   6 1206.21 242.819   4
   7   6   6 1007.62 213.600   4
   7   6   6 598.897 182.020   8
   7  -6   7 5122.94 451.505   4
   7   6   7 4422.40 435.270   4
   7   6   7 3714.04 423.697   8
   7  -6   7 3058.63 290.808   5
   7  -6   8 6305.79 417.518   5
   7  -6   8 9537.86 582.497   4
   7   6   8 8974.68 605.775   4
   7   6   8 6341.16 564.311   2
   7   6   9 700.552 161.039   2
   7  -6   9 354.487 64.8388   5
   7  -6   9 410.159 108.339   4
   7   6   9 573.319 132.781   4
   7   7   0 28.8240 66.9575   2
   7   7   0 12.4916 50.2629   1
   7  -7   0 34.8553 50.9544   5
   7  -7   0-37.8336 136.146  11
   7  -7  -1 19369.3 1012.58   5
   7  -7  -1 21544.7 1409.73  11
   7  -7   1 21341.7 1049.18   5
   7   7  -1 20890.4 1014.05   1
   7  -7   1 20715.4 1435.05  11
   7   7   1 22765.8 1036.65   1
   7  -7   2 14738.2 1087.84  11
   7  -7  -2 15483.1 1066.08  11
   7  -7   2 15845.2 838.319   5
   7   7  -2 15867.8 785.036   1
   7   7   2 17384.9 953.282   2
   7  -7   3 12685.7 976.613  11
   7  -7   3 16075.9 870.516   5
   7   7   3 12441.4 1153.42  10
   7   7   3 18248.6 1028.72   2
   7  -7  -3 15315.3 987.836  11
   7  -7   4 13609.1 928.267  11
   7   7   4 12345.7 830.395   8
   7   7   5 287.691 131.983   8
   7  -7   6 15237.0 929.466   5
   7   7   6 16652.0 905.203   4
   7   7   6 16396.5 1014.41   8
   7  -7   7 9.64487 57.5587   5
   7   7   7-101.138 214.456   2
   7   7   7 45.7354 83.5676   4
   7  -7   8 6787.29 410.864   5
   7   7   8 8321.78 647.398   2
   7   7   9-40.2968 123.233   2
   7  -7   9 4.22406 34.8281   5
   7  -8   0 43.4188 174.694  11
   7  -8   0 43.8468 53.4420   5
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   7   8   2 2007.90 262.390   2
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   7  -8  -4 795.476 181.376  11
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   7   8   4 828.895 275.678   2
   7   8   4 774.483 182.677   8
   7   8   5-37.5482 128.637   8
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   7   8   6 3097.68 369.906   8
   7  -8   7 191.646 80.0157   5
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   7   8   9 156.206 117.135   2
   7  -8   9 53.3520 36.0535   5
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   7  -9   0 44.3276 51.5308   5
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   7   9   4 1742.90 270.454   8
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   7  10  -1 36771.9 1785.42   7
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   7 -10   2 3749.50 484.982  11
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   7  10   3 19130.4 1276.81   8
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   7 -10   3 18121.6 1358.64  11
   7  10   4 6316.24 564.524   2
   7 -10   4 6104.77 460.924   5
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   7 -11   0 501.721 86.6162   5
   7  11   0 590.926 121.832   7
   7 -11   1 284.781 150.323  11
   7 -11  -1 279.140 153.892  11
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   7  11   3 1234.89 199.119   2
   7 -11   3 1272.44 172.082   5
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   7  11   4 511.258 164.755   2
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   7 -11   4 337.713 117.583   5
   7  11   5 135.255 123.578   2
   7 -11   5 10.9996 72.7399   5
   7  11   6 145.277 119.784   2
   7 -11   6 44.6814 66.3575   5
   7  11   7 131.105 112.032   2
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   7 -12   1 29291.5 1390.40   5
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   7 -12   2 4611.47 327.774   5
   7 -12   3 1389.66 171.691   5
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   7  12   4 1013.72 163.014   2
   7 -12   4 910.757 137.223   5
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   7 -12   5 2246.82 206.908   5
   7  12   5 1757.60 213.744   2
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   7 -12   6 1236.44 135.973   5
   7  12   6 1105.03 155.933   2
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   7 -13   2 1008.44 123.121   5
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   7 -13   3 736.579 108.240   5
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   7 -13   4 535.737 93.2243   5
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   7 -13   5 760.554 101.389   5
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   7 -14   3 61.2681 32.8136   5
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   8   0   0 105374. 4679.22   9
   8   0   0 109352. 4938.00  11
   8   0   1 2850.09 236.170   9
   8   0  -1 2953.72 237.245   9
   8   0   1 2522.18 236.615   6
   8   0   2 1070.60 149.998   9
   8   0  -2 1044.52 142.064   9
   8   0   2 1149.62 172.766   6
   8   0   3 34384.0 1698.74   4
   8   0  -3 34058.1 1602.84   9
   8   0   3 34104.9 1720.13   2
   8   0   3 33170.0 1752.61   6
   8   0   3 35211.5 1632.38   9
   8   0   4 1242.63 140.943   5
   8   0   4 1059.52 234.241   2
   8   0  -4 1534.11 165.237   9
   8   0   4 1381.24 184.169   9
   8   0   4 1126.10 243.818   4
   8   0  -4 1804.83 161.629   1
   8   0   4 1419.92 247.552   6
   8   0   5 53635.1 2854.47   2
   8   0   5 57908.9 2969.46   6
   8   0   6 500.679 203.571   2
   8   0   6 732.158 219.897   6
   8   0   7 9097.04 694.326   2
   8   0   7 9383.65 886.995   6
   8   0   8 490.112 309.281   4
   8   0   9 9338.31 674.328   4
   8   0  10 112.166 93.6721   4
   8  -1   0 7130.11 573.451  11
   8   1   0 6595.50 424.248   9
   8  -1  -1 1189.23 218.909  11
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   8  -1   1 848.699 193.456  11
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   8   1  -2 626.608 114.963   9
   8   1   2 409.941 105.355   9
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   8   1   2 449.116 110.425   6
   8  -1  -3 8687.56 484.598   9
   8   1  -3 8183.92 493.717   9
   8  -1   3 8995.23 504.892   9
   8  -1   3 6151.92 519.053   4
   8   1   3 7343.00 545.741   4
   8   1   3 8373.00 523.362   9
   8   1   3 8165.73 593.047   2
   8   1  -3 9782.56 480.322   1
   8  -1   3 7519.44 590.296   6
   8   1   3 7254.72 577.205   6
   8  -1   4 189.825 127.476   2
   8   1   4 59.8284 174.029   2
   8  -1   4 244.342 75.2331   5
   8  -1  -4 134.872 70.7445   9
   8  -1   4 114.382 84.6882   9
   8   1  -4 24.9577 70.4178   9
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   8  -1   4 433.054 179.122   4
   8   1   4 128.375 134.144   4
   8  -1  -4 59.8529 60.2050   1
   8   1  -4 135.133 67.8953   1
   8  -1   4 174.576 107.664   6
   8   1   4 174.822 114.760   6
   8  -1   5 328.363 157.747   2
   8   1   5 411.262 231.268   2
   8  -1   5 36.8731 65.4072   5
   8  -1   5 95.4540 265.476   4
   8  -1   5 52.8065 106.293   6
   8   1   5 83.1280 105.827   6
   8  -1   6 1486.82 253.864   2
   8  -1   6 1702.53 185.857   5
   8   1   6 1676.74 353.297   2
   8  -1   6 1500.77 310.409   6
   8   1   6 2178.39 379.498   6
   8  -1   7-192.348 399.633   4
   8   1   7 88.9400 157.539   2
   8  -1   7 137.805 131.535   6
   8   1   7 39.0814 131.593   6
   8   1   8 859.583 190.782   2
   8  -1   8 553.177 278.381   4
   8  -1   9 64.3720 119.417   4
   8  -1  10 791.455 149.152   4
   8  -2   0 1386.86 237.193  11
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   8   2   1 14199.4 794.135   9
   8  -2  -1 14910.3 947.568  11
   8  -2   2 65.9232 88.4643  11
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   8   2   2 116.584 94.4415   9
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   8  -2   3 5412.04 386.875   5
   8  -2   3 6900.30 586.170  11
   8  -2   3 4792.18 433.556   4
   8   2   3 4694.89 431.448   4
   8   2  -3 7043.43 428.165   9
   8   2   3 7117.35 467.913   9
   8   2   3 5716.38 499.629   2
   8   2  -3 7704.17 393.563   1
   8  -2   3 5238.08 483.112   6
   8  -2  -3 6457.24 541.692  11
   8   2   3 5665.59 498.561   6
   8  -2   4 239.310 120.637   2
   8   2   4 389.171 185.955   2
   8  -2   4 542.983 122.332   5
   8  -2  -4 705.216 108.877   9
   8  -2   4 685.499 120.207   9
   8  -2  -4 732.630 116.328   1
   8   2  -4 941.698 117.432   1
   8  -2   4 406.386 168.802   4
   8   2   4 368.985 171.165   4
   8  -2   4 514.706 158.009   6
   8   2   4 657.830 176.139   6
   8  -2   5 16236.0 929.145   5
   8  -2   5 19565.2 1215.42   4
   8   2   5 22238.8 1388.26   4
   8   2   5 17613.3 1244.71   2
   8  -2   5 14433.0 1083.81   6
   8   2   5 15967.7 1157.80   6
   8  -2   6 2222.30 250.959   5
   8   2   6 2677.93 467.717   2
   8  -2   6 2888.49 587.498   4
   8  -2   6 2751.05 402.987   6
   8   2   6 2464.55 423.649   6
   8  -2   7 3631.99 305.316   5
   8  -2   7 4222.34 696.209   4
   8   2   7 3245.10 431.572   2
   8  -2   7 3405.54 479.782   6
   8   2   7 4838.27 628.475   6
   8  -2   8-140.211 201.839   4
   8   2   8 191.382 291.945   4
   8   2   8-67.9821 138.482   2
   8   2   9 678.837 150.345   2
   8  -2   9 501.059 163.808   4
   8   2   9 576.661 223.003   4
   8  -2  10-9.40043 75.6402   4
   8   2  10 12.0691 101.853   4
   8  -3   0 125886. 5777.47  11
   8   3   0 126195. 5578.57   9
   8   3  -1 94.2753 88.4100   9
   8  -3   1-22.4463 75.5666  11
   8   3   1 67.6905 84.9246   9
   8  -3  -1 83.8213 84.3176  11
   8  -3   2 40530.8 1917.74   5
   8  -3  -2 45726.8 2174.82  11
   8  -3   2 42857.3 2200.11  11
   8   3   2 40629.5 2052.68   6
   8  -3   3 1237.44 169.224   5
   8   3   3 1299.30 241.424   2
   8  -3  -3 1388.17 236.893  11
   8  -3   3 1211.93 194.832   4
   8   3   3 862.367 173.253   4
   8   3  -3 1147.39 133.183   1
   8  -3   3 1035.53 226.298  11
   8   3   3 1187.36 221.819   6
   8  -3  -4 25169.6 1474.60  11
   8  -3   4 28830.8 1470.16   4
   8   3   4 29031.1 1491.25   4
   8  -3   4 30237.5 1439.87   5
   8   3  -4 28181.2 1292.49   1
   8   3   4 23643.5 1568.45   2
   8  -3   4 26025.1 1534.94  11
   8  -3   4 24246.4 1516.22   6
   8   3   4 26308.2 1587.35   6
   8  -3   5 771.199 177.703   5
   8   3   5 760.356 350.617   2
   8  -3   5 757.539 237.047   4
   8   3   5 894.843 273.993   4
   8  -3   5 666.662 194.754   6
   8   3   5 914.197 254.833   6
   8  -3   6 764.996 166.543   5
   8   3   6 1374.43 396.982   2
   8  -3   6 1727.16 432.105   4
   8   3   6 1787.40 588.401   4
   8  -3   6 945.724 241.723   6
   8   3   6 1311.68 326.691   6
   8   3   7 479.647 222.884   2
   8  -3   7 255.143 103.021   5
   8  -3   7 830.459 326.311   4
   8   3   7 314.078 479.259   4
   8  -3   7 311.504 148.837   6
   8   3   7 139.170 187.075   6
   8   3   8 216.777 137.920   2
   8  -3   8 360.504 236.494   4
   8   3   8 285.412 378.102   4
   8   3   9 500.936 132.042   2
   8  -3   9 413.924 165.683   4
   8   3   9 653.623 254.730   4
   8  -3  10 1194.42 163.940   4
   8   3  10 1302.20 194.307   4
   8  -4   0 16235.3 822.825   5
   8  -4   0 18059.2 1105.45  11
   8   4  -1 5956.45 352.264   1
   8  -4  -1 5514.42 328.574   5
   8  -4   1 4622.08 330.900   5
   8  -4  -1 5261.84 508.396  11
   8  -4   1 4831.08 516.510  11
   8   4   1 5939.63 435.239   2
   8  -4  -2 883.681 106.348   5
   8  -4   2 543.490 188.934  11
   8   4   2 1043.40 191.615   2
   8   4   2 629.998 120.638   1
   8  -4  -2 627.292 172.575  11
   8   4  -2 1239.82 144.147   1
   8   4   2 302.447 127.957   6
   8  -4   3 2376.89 245.776   5
   8  -4   3 3051.81 396.696  11
   8  -4  -3 2447.78 320.205  11
   8  -4   3 1591.53 240.446   4
   8   4   3 1713.85 237.950   4
   8   4   3 1951.82 323.146   6
   8  -4  -4 376.067 128.713  11
   8  -4   4 238.704 129.156  11
   8  -4   4 198.246 133.997   5
   8   4   4 189.892 224.366   2
   8  -4   4 94.5124 127.063   4
   8   4   4 114.885 122.081   4
   8   4   4 273.576 150.047   6
   8  -4   5 2615.42 366.631   4
   8   4   5 2925.23 405.731   4
   8   4   5 2830.39 631.835   2
   8  -4   5 2899.81 368.207   5
   8  -4   5 2219.00 347.456   6
   8   4   5 3269.01 491.174   6
   8  -4   6 660.059 169.455   5
   8   4   6 639.825 345.287   2
   8  -4   6 884.933 315.412   4
   8   4   6 737.790 321.565   4
   8  -4   6 607.725 225.948   6
   8   4   6 845.398 284.622   6
   8  -4   7 23.4740 66.7892   5
   8   4   7 80.0761 173.162   2
   8  -4   7-30.9446 212.014   4
   8   4   7 46.7749 259.399   4
   8   4   8 312.211 146.416   2
   8  -4   8 108.968 56.2109   5
   8  -4   8-112.386 189.747   4
   8   4   8 36.5720 271.348   4
   8   4   9 33.1118 94.1983   2
   8  -4   9-13.8012 111.051   4
   8   4   9-43.6655 171.228   4
   8   4  10 480.819 85.1454   2
   8  -4  10 661.048 115.253   4
   8   4  10 671.361 130.201   4
   8  -5   0 100636. 4410.94   5
   8  -5   0 102582. 4823.70  11
   8   5   0 97215.5 4406.39   1
   8   5   0 104577. 4493.69   2
   8  -5  -1 79.7755 101.508  11
   8  -5  -1 43.9552 43.7880   5
   8  -5   1 45.3675 48.1275   5
   8   5   1 21.0314 52.7919   1
   8   5  -1 23.6307 60.9802   1
   8   5   1 39.5963 90.4438   2
   8  -5   1 29.6123 92.2978  11
   8   5  -1 53.5916 65.3003   2
   8  -5  -2 22630.0 1108.56   5
   8  -5   2 21988.6 1432.63  11
   8  -5  -2 25703.4 1414.02  11
   8  -5   2 25652.0 1181.90   5
   8   5  -2 21534.5 1149.61   2
   8   5   2 23260.2 1143.56   1
   8   5   2 23919.1 1270.95   2
   8   5  -2 24949.5 1138.75   1
   8   5   3 192.635 77.3860   1
   8  -5   3 165.772 145.084  11
   8   5   3 281.905 162.162   2
   8  -5  -3 194.350 60.3415   5
   8  -5  -3 174.415 124.226  11
   8  -5   3 65.8076 106.481   4
   8   5   3 86.5303 93.5714   4
   8   5  -3 126.910 61.8452   1
   8   5   3 185.530 126.347   6
   8  -5   4 10321.1 830.150  11
   8  -5   4 10748.5 709.023   4
   8  -5  -4 10480.1 777.975  11
   8  -5   4 10733.2 782.195   5
   8   5   4 10217.1 693.886   4
   8   5  -4 13121.4 643.029   1
   8   5   4 9647.85 907.267   6
   8  -5   5 48.4166 147.780   5
   8   5   5 326.322 439.395   2
   8  -5   5 148.436 145.591   4
   8   5   5 134.615 138.481   4
   8  -5   5 78.6298 88.3465   6
   8   5   5 165.771 158.246   6
   8  -5   6 2724.98 336.605   5
   8  -5   6 3961.35 454.417   4
   8   5   6 3122.90 423.109   4
   8   5   6 3675.08 721.493   2
   8  -5   6 3207.30 423.187   6
   8   5   6 3680.96 589.045   6
   8  -5   7 1862.41 213.380   5
   8   5   7 1536.94 341.773   2
   8  -5   7 2177.43 355.601   4
   8   5   7 2169.71 378.782   4
   8   5   8 218.600 145.187   2
   8  -5   8 101.137 56.8850   5
   8  -5   8 206.301 148.433   4
   8   5   8 45.8627 162.517   4
   8   5   9 10.9016 84.4172   2
   8  -5   9 111.619 99.2065   4
   8   5   9 125.517 121.677   4
   8  -6   0 20087.5 995.091   5
   8  -6   0 19390.5 1388.04  11
   8   6   0 19968.5 1055.52   2
   8   6   0 20600.1 1000.35   1
   8  -6   1 175.879 168.467  11
   8  -6  -1 189.961 167.105  11
   8  -6  -1 285.743 73.1128   5
   8  -6   1 279.605 84.0039   5
   8   6   1 813.746 168.312   2
   8   6  -1 776.349 114.322   1
   8   6   1 557.901 101.828   1
   8   6  -1 665.570 118.244   2
   8   6  -2 228.047 70.4717   1
   8   6   2 94.1342 121.538   2
   8  -6  -2 40.9376 44.3564   5
   8   6   2 214.100 74.1605   1
   8  -6   2 264.375 90.0602   5
   8  -6   2 30.9602 180.588  11
   8  -6  -3 6627.97 432.611   5
   8  -6   3 9694.41 591.148   5
   8  -6   3 7333.76 691.511  11
   8  -6  -3 9080.56 692.760  11
   8   6  -3 9249.86 477.707   1
   8   6   3 8224.17 482.081   1
   8   6   3 8121.53 652.314   2
   8  -6  -4 4533.03 474.053  11
   8  -6   4 4980.84 393.987   4
   8   6   4 4530.87 376.093   4
   8  -6   4 4596.32 511.479  11
   8   6   4 4913.34 340.222   1
   8   6   4 5621.31 677.694   2
   8   6   5 42354.9 2130.31   4
   8  -6   5 43552.1 2143.39   4
   8  -6   5 42140.6 2292.25   5
   8   6   5 46788.5 2040.02   1
   8   6   5 40493.5 2527.89   6
   8   6   6 2686.02 493.801   6
   8  -6   6 1999.58 279.064   5
   8  -6   6 1965.90 288.478   4
   8   6   6 2217.83 289.662   4
   8  -6   6 2509.47 361.103   6
   8  -6   7 1166.46 162.913   5
   8   6   7 1320.01 353.520   2
   8  -6   7 1093.05 211.314   4
   8   6   7 1222.86 219.491   4
   8  -6   8 1410.16 147.954   5
   8   6   8 1395.70 256.418   2
   8  -6   8 1782.59 222.304   4
   8   6   8 1515.43 216.316   4
   8   6   9 65.6210 90.1761   2
   8  -6   9-3.39298 10.5746   5
   8  -7   0 12679.4 677.402   5
   8  -7   0 11582.6 1068.56  11
   8   7   0 12618.6 725.576   2
   8   7   0 12802.6 669.275   1
   8  -7  -1 1388.76 152.226   5
   8  -7   1 1612.33 178.083   5
   8  -7   1 1604.59 363.248  11
   8  -7  -1 1434.06 324.025  11
   8   7  -1 1288.24 165.049   2
   8   7   1 1747.09 225.962   2
   8   7  -1 1740.74 159.737   1
   8   7   1 1640.46 168.637   1
   8  -7   2 97.9270 137.827  11
   8  -7  -2 114.798 115.571  11
   8   7   2 130.391 119.224   2
   8  -7  -2 65.9029 49.6460   5
   8  -7   2 136.938 77.8725   5
   8   7   2 175.396 70.3718   1
   8   7  -2 134.667 58.4885   1
   8  -7   3 1935.32 329.569  11
   8  -7  -3 2308.97 333.942  11
   8  -7   3 2532.31 279.436   5
   8   7   3 1939.47 307.401   2
   8   7   4 1282.77 351.477   2
   8  -7   4 772.643 201.587  11
   8  -7  -4 875.337 205.409  11
   8  -7   5 1848.04 316.584   5
   8   7   5 3516.33 778.631   2
   8  -7   6 401.254 137.119   5
   8   7   6 305.407 110.635   4
   8  -7   7 1683.13 189.931   5
   8   7   7 1936.01 204.605   4
   8   7   8 77.1019 143.089   2
   8  -7   8 128.276 54.7587   5
   8  -7   9 1252.23 103.121   5
   8   7   9 1765.57 207.126   2
   8   8   0 507.093 86.8628   1
   8  -8   0 145.835 139.124  11
   8  -8   0 315.141 83.6342   5
   8   8   0 319.155 99.1878   2
   8  -8  -1 6410.60 395.079   5
   8  -8  -1 5373.82 684.197  11
   8  -8   1 6812.84 428.129   5
   8   8  -1 6918.71 388.858   1
   8  -8   1 5434.00 707.542  11
   8   8   1 6948.46 491.532   2
   8  -8   2 2110.79 228.489   5
   8  -8   2 1571.88 328.974  11
   8  -8  -2 1989.66 348.586  11
   8   8  -2 2671.90 217.487   1
   8   8   2 2429.40 300.671   2
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   8  -8  -3 14392.0 1022.58  11
   8  -8   3 16159.9 901.308   5
   8   8   3 17895.6 1055.42   2
   8  -8   4 685.740 202.124  11
   8  -8  -4 1184.23 246.376  11
   8   8   4 1336.01 323.824   2
   8  -8   4 1217.62 226.097   5
   8   8   5 22703.6 1733.59   2
   8   8   6 158.958 363.108   2
   8  -8   6 186.884 114.197   5
   8  -8   7 4904.72 338.620   5
   8   8   8 39.4546 141.982   2
   8  -8   8 26.5699 42.2371   5
   8  -9   0 26074.5 1198.64   5
   8  -9   0 17474.4 1625.24  11
   8   9   1 24.1575 76.8365   2
   8  -9   1-129.051 225.651  11
   8  -9  -1-83.6427 206.072  11
   8  -9  -1 20.3966 45.7709   5
   8  -9   1 8.93268 62.2468   5
   8  -9   2 4659.28 570.965  11
   8  -9  -2 4700.69 570.967  11
   8  -9   2 5974.62 406.148   5
   8   9   2 6636.15 490.752   2
   8  -9   3-100.160 114.864  11
   8  -9  -3-49.9977 110.176  11
   8   9   3 39.4937 109.510   2
   8  -9   3 74.9498 81.0377   5
  -8   9   3 37.3476 45.5776   3
   8  -9   4 4824.32 415.010   5
   8   9   4 4007.39 522.771   2
   8   9   5-36.0628 199.993   2
   8  -9   5-15.9218 99.2406   5
   8   9   6 443.401 290.404   2
   8   9   7 303.064 216.082   2
   8  -9   7 15.0439 54.1524   5
   8  -9   8-33.3560 42.4611   5
   8 -10   0 3020.28 237.679   5
   8 -10   0 2485.98 482.549  11
   8 -10   1 2123.36 201.859   5
   8 -10   1 1839.91 391.042  11
   8 -10  -1 1415.11 339.529  11
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   8 -10   2 1492.35 186.051   5
   8 -10   2 1565.44 314.641  11
   8 -10  -2 1843.64 331.502  11
   8  10   2 2446.95 259.110   2
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   8  10   3 843.460 183.038   2
   8 -10   3 456.228 120.116   5
   8 -10   4 1415.87 209.059   5
   8  10   4 1820.97 303.971   2
   8 -10   5 3396.70 325.949   5
   8  10   5 3613.88 441.806   2
   8  10   6 2017.92 340.928   2
   8 -10   7 217.216 69.1696   5
   8  10   7 218.428 153.892   2
   8 -11   0 35625.7 1638.12   5
  -8  11   1 748.674 115.778   3
   8 -11   1 610.301 107.352   5
  -8  11   2 9944.40 554.365   3
   8 -11   2 10397.0 587.859   5
   8  11   3 49.6722 83.6614   2
  -8  11   3 100.575 52.7851   3
   8 -11   3 49.9583 67.3413   5
   8 -11   4 5123.94 379.351   5
   8  11   4 4826.66 417.331   2
   8 -11   5 2794.98 258.448   5
   8  11   5 2691.45 305.013   2
   8  11   6 79.9341 104.516   2
   8 -11   6 55.3923 60.4625   5
   8  11   7 304.465 103.097   2
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   8 -12   1 175.316 61.0073   5
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   8 -12   2 1342.16 154.444   5
   8 -12   3 1636.81 172.033   5
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   8 -12   4 1015.03 141.990   5
   8  12   4 1074.36 150.028   2
   8 -12   5 3097.83 241.609   5
   8  12   5 2831.16 248.464   2
   8  12   6 59.5936 61.3403   2
   8 -12   6 16.6525 42.3880   5
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  -8  13  -1 37.4488 38.5294   3
   8 -13   2 268.647 60.7853   5
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   8 -13   3 1197.90 129.359   5
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   8 -13   4 82.5251 48.6037   5
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   8 -13   5 86.6164 43.6557   5
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   9   0   0 101.594 51.9497   5
   9   0   0 48.7559 75.6158   9
   9   0   0 137.851 63.4645   1
   9   0   0 196.287 96.2401   2
   9   0   1 1494.49 158.780   5
   9   0   1 1695.76 201.820   9
   9   0  -1 1939.80 180.710   1
   9   0  -1 2022.80 212.641   9
   9   0  -2 9728.21 520.841   1
   9   0   2 8573.07 500.465   5
   9   0   2 7145.96 545.088   4
   9   0  -2 10996.2 623.250   2
   9   0  -2 10211.6 563.015   9
   9   0   2 10194.2 577.087   9
   9   0   2 8233.65 585.500   2
   9   0   2 7412.02 575.745   6
   9   0   3 8125.50 469.712   5
   9   0   3 7503.26 553.211   4
   9   0  -3 8230.01 504.830   9
   9   0   3 8044.02 526.419   9
   9   0   3 7573.22 581.860   2
   9   0  -3 8469.55 480.038   1
   9   0   3 7890.92 614.158   6
   9   0   4 2541.95 351.079   4
   9   0   4 2953.49 242.135   5
   9   0  -4 3138.53 276.678   9
   9   0   4 2843.09 303.340   9
   9   0   4 2424.60 337.436   2
   9   0   4 2422.41 352.004   6
   9   0   5 1035.08 137.047   5
   9   0   5 1019.89 256.495   2
   9   0   5 1414.24 391.579   4
   9   0   5 1395.89 286.650   6
   9   0   6 18629.0 1200.84   2
   9   0   6 20932.7 1426.77   6
   9   0   7 1150.11 223.544   2
   9   0   7 2400.06 810.462   4
   9   0   8 7717.60 771.848   4
   9   0   9 115.839 126.392   4
   9   0  10 233.659 82.5344   4
   9   1   0 183.720 72.2519   1
   9   1   0 204.850 60.9195   5
   9   1   0 125.051 89.2907   9
   9  -1   0 128.936 113.926  11
   9  -1   0 246.433 101.405   2
   9  -1   0 193.226 71.5528   1
   9  -1  -1 51.4710 86.6459  11
   9   1  -1 28.6388 58.3531   1
   9  -1  -1 6.37879 38.1065   5
   9   1   1 57.6493 39.9635   5
   9  -1  -1 47.8387 55.7019   1
   9  -1   1 42.1815 43.8540   5
   9  -1   1-26.8429 108.010  11
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   9   1  -1 117.073 83.4890   2
   9  -1   1 11.2210 80.7771   2
   9  -1   1 125.448 68.0778   6
   9   1   1 61.7966 83.2238   2
   9  -1  -2 12850.0 660.653   1
   9   1   2 11895.9 640.687   5
   9  -1   2 12368.9 657.981   5
   9  -1   2 10801.4 702.910   4
   9   1   2 12049.1 717.055   4
   9  -1  -2 13496.9 703.181   9
   9  -1   2 12992.6 715.042   9
   9   1  -2 13147.5 710.255   9
   9   1   2 13117.9 730.093   9
   9   1  -2 13097.4 730.477   2
   9  -1   2 12558.0 742.293   2
   9   1   2 11974.2 756.197   2
   9  -1   2 10163.6 742.763   6
   9   1   2 10764.9 732.166   6
   9   1  -2 12458.8 658.323   1
   9   1   3 1427.42 147.464   5
   9   1   3 1156.64 236.872   2
   9  -1   3 1508.56 169.734   5
   9   1   3 1563.90 226.537   4
   9  -1  -3 1399.28 174.957   9
   9  -1   3 1239.62 187.956   9
   9   1  -3 1148.00 180.972   9
   9   1   3 1427.90 210.492   9
   9  -1   3 1420.94 219.827   4
   9   1  -3 1343.44 155.853   1
   9  -1  -3 1631.31 165.258   1
   9   1   3 1386.01 230.098   6
   9  -1   3 903.023 196.332   6
   9  -1   3 1268.66 212.509   2
   9   1   4 12865.9 709.493   5
   9  -1   4 13832.7 759.517   5
   9  -1   4 14796.2 912.636   4
   9  -1  -4 14504.1 756.427   9
   9  -1   4 13610.0 781.150   9
   9   1  -4 13547.1 768.830   9
   9  -1  -4 15947.5 743.835   1
   9   1  -4 15995.5 743.522   1
   9  -1   4 11120.4 817.595   2
   9   1   4 12119.0 909.838   2
   9  -1   4 13537.7 965.659   6
   9   1   4 13662.1 962.064   6
   9  -1   5 2758.49 248.444   5
   9   1   5 2200.73 385.872   2
   9  -1   5 3134.52 499.342   4
   9  -1   5 2055.82 296.367   2
   9  -1   5 2692.99 403.586   6
   9   1   5 2249.54 378.671   6
   9  -1   6 5983.94 402.305   5
   9  -1   6 4998.87 461.979   2
   9   1   6 5288.74 576.654   2
   9  -1   6 6938.97 694.228   6
   9   1   6 6109.89 684.199   6
   9   1   7 1207.71 248.844   2
   9  -1   7 695.624 511.049   4
   9  -1   8 3750.05 490.002   4
   9   1   8 3105.95 323.086   2
   9  -1   9 13.3885 107.731   4
   9  -1  10 468.173 96.7290   4
   9  -2   0 385.294 90.1878   1
   9  -2   0 436.575 170.428  11
   9  -2   0 242.985 71.1335   5
   9   2   0 277.050 106.955   9
   9  -2   0 529.466 126.546   2
   9   2   0 510.560 127.015   2
   9   2   1 27252.5 1251.78   5
   9  -2  -1 25159.9 1243.82   5
   9  -2   1 26015.0 1260.19   5
   9  -2   1 26316.8 1572.49  11
   9  -2  -1 28528.6 1579.28  11
   9   2  -1 26277.2 1264.62   1
   9  -2  -1 24582.7 1244.44   1
   9  -2  -1 30794.3 1366.42   2
   9   2  -1 26233.3 1335.00   9
   9   2   1 27344.5 1358.97   9
   9  -2   1 26553.5 1324.28   2
   9   2  -1 26357.6 1319.80   2
   9  -2   2 84.2807 123.826  11
   9   2   2-14.7252 100.900   2
   9  -2  -2 74.6479 94.9853  11
   9  -2  -2 26.1955 49.3189   5
   9  -2   2 33.2751 46.1618   5
   9   2  -2 65.4547 72.8841   1
   9   2   2 63.9413 44.5870   5
   9   2  -2-22.6232 92.1636   9
   9   2   2-12.9224 95.8783   9
   9  -2  -2 100.503 70.7647   1
   9   2  -2-10.5447 87.9871   2
   9  -2   2-11.7022 103.161   2
   9  -2   2 52.3649 62.8327   6
   9   2   3 6582.45 392.834   5
   9  -2   3 7058.29 455.633   5
   9  -2   3 6472.79 650.417  11
   9  -2  -3 6486.64 610.866  11
   9  -2   3 6807.11 462.149   9
   9  -2   3 6633.87 495.195   4
   9   2   3 6643.55 495.501   4
   9  -2  -3 7946.46 456.187   9
   9   2  -3 6624.23 463.324   9
   9  -2   3 6179.16 482.063   2
   9   2   3 6640.23 558.537   2
   9   2  -3 6807.87 409.997   1
   9  -2  -3 6682.49 414.147   1
   9  -2   3 6029.66 559.889   6
   9   2   3 6510.94 565.705   6
   9  -2   4 1887.14 226.646   5
   9   2   4 1600.16 344.061   2
   9  -2  -4 2137.81 213.404   9
   9  -2   4 1758.77 212.892   9
   9  -2  -4 3073.99 227.773   1
   9  -2   4 1397.71 266.465   4
   9   2   4 1695.73 288.661   4
   9   2  -4 2597.82 204.896   1
   9  -2   4 1517.49 232.303   2
   9  -2   4 1399.89 281.683   6
   9   2   4 1566.65 290.383   6
   9   2   5 803.142 312.064   2
   9  -2   5 1053.18 174.610   5
   9  -2   5 1477.24 329.289   4
   9   2   5 1256.22 352.617   4
   9  -2   5 850.328 228.188   6
   9  -2   5 586.733 155.620   2
   9   2   5 682.549 217.904   6
   9   2   6 613.707 280.146   2
   9  -2   6 620.288 136.958   5
   9  -2   6 1194.01 455.591   4
   9   2   6 83.5596 553.123   4
   9  -2   6 766.685 226.185   6
   9   2   6 702.667 234.660   6
   9   2   7 426.892 197.030   2
   9  -2   7 492.402 103.033   5
   9  -2   7 515.078 395.695   4
   9   2   7 390.450 734.991   4
   9   2   8 510.091 158.665   2
   9  -2   8 968.997 278.757   4
   9   2   8 858.272 357.546   4
   9  -2   9 1238.59 196.728   4
   9   2   9 1191.40 239.518   4
   9   2   9 900.761 145.923   2
   9  -3   0 576.044 105.752   1
   9  -3   0 429.199 92.3033   5
   9   3   0 686.792 114.719   1
   9  -3   0 335.906 157.280  11
   9   3   0 569.373 157.360   9
   9  -3   0 1080.72 167.576   2
   9   3   0 808.127 158.523   2
   9  -3  -1 47973.6 2138.01   5
   9  -3   1 49227.2 2535.69  11
   9  -3  -1 50166.3 2507.45  11
   9  -3  -1 45592.4 2127.45   1
   9   3  -1 50721.8 2258.96   9
   9  -3   1 47508.1 2197.75   2
   9   3  -1 47902.6 2212.43   2
   9   3   1 42940.7 2143.71   1
   9   3   1 48525.0 2258.58   2
   9  -3  -2 729.283 103.445   5
   9  -3   2 574.319 222.675  11
   9  -3  -2 591.231 200.881  11
   9  -3   2 446.519 104.211   5
   9   3  -2 742.018 150.066   2
   9  -3   2 847.223 160.015   2
   9   3   2 522.746 120.223   1
   9  -3  -2 886.634 131.877   1
   9  -3   3 21538.7 1072.29   5
   9  -3   3 21539.4 1352.55  11
   9  -3  -3 21510.9 1274.63  11
   9  -3   3 17844.0 1066.08   4
   9   3   3 18160.9 1071.16   4
   9  -3   3 18054.4 1040.40   2
   9   3   3 20420.8 1193.35   2
   9   3  -3 23889.3 1005.86   1
   9  -3   3 17423.1 1194.16   6
   9   3   3 17503.4 1198.01   6
   9  -3   4 156.883 99.8691   5
   9  -3  -4 130.295 75.0478   9
   9  -3   4 124.213 79.1054   9
   9   3   4-29.2691 229.580   2
   9  -3   4-17.0841 128.644   4
   9   3   4 165.497 130.312   4
   9   3  -4 229.249 78.4962   1
   9  -3   4-27.5427 92.7874   6
   9   3   4 58.7870 99.0124   6
   9   3   5 1870.82 470.499   2
   9  -3   5 1294.98 242.610   5
   9  -3   5 2104.45 346.653   4
   9   3   5 1828.03 364.062   4
   9  -3   5 1578.64 312.859   6
   9   3   5 1646.92 344.882   6
   9   3   6 1557.71 424.720   2
   9  -3   6 1211.37 203.219   5
   9  -3   6 1997.72 430.019   4
   9   3   6 1948.94 547.506   4
   9  -3   6 1241.92 282.345   6
   9   3   6 1743.81 398.541   6
   9   3   7 96.4487 165.277   2
   9  -3   7 129.927 76.8607   5
   9  -3   7 70.7433 238.180   4
   9   3   7 65.3053 389.736   4
   9   3   8-14.6113 105.173   2
   9  -3   8 129.893 158.233   4
   9   3   8 149.353 242.230   4
   9   3   9 247.913 98.4502   2
   9  -3   9 494.110 134.528   4
   9   3   9 218.689 164.482   4
   9  -4   0 528.952 199.815  11
   9  -4   0 473.092 94.0994   5
   9  -4   0 722.704 115.716   1
   9   4   0 672.640 117.589   1
   9   4  -1 87011.0 3690.55   1
   9  -4  -1 80576.7 3661.71   5
   9  -4   1 82828.6 3683.90   5
   9  -4   1 80581.5 4103.07  11
   9  -4  -1 83576.3 4074.65  11
   9  -4   1 83700.4 3713.22   2
   9   4   1 79360.3 3676.92   1
   9   4  -1 81330.1 3731.04   2
   9   4   1 87541.5 3808.09   2
   9  -4   2 665.503 225.040  11
   9   4   2 710.405 169.408   2
   9  -4  -2 603.968 189.311  11
   9   4  -2 483.122 106.655   1
   9  -4  -2 372.829 80.5461   5
   9  -4   2 481.259 127.893   2
   9   4  -2 551.554 129.728   2
   9   4   2 632.325 120.181   1
   9  -4   3 5521.42 422.225   5
   9  -4   3 4086.59 536.814  11
   9  -4  -3 4659.55 511.691  11
   9  -4   3 4868.04 402.376   4
   9   4   3 4699.00 391.210   4
   9  -4   4 88.5469 130.109  11
   9  -4  -4 143.386 105.356  11
   9   4   4 68.4288 230.352   2
   9  -4   4 19.6144 111.631   5
   9  -4   4-95.6449 154.477   4
   9   4   4-33.1728 136.783   4
   9  -4   4 284.703 140.310   6
   9   4   4 202.170 142.204   6
   9  -4   5 4437.85 483.833   5
   9  -4   5 5382.02 514.136   4
   9   4   5 5518.22 538.999   4
   9   4   5 5103.00 791.162   2
   9  -4   5 3791.37 506.392   6
   9   4   5 4716.60 625.848   6
   9   4   6 520.821 362.977   2
   9  -4   6 616.119 164.783   5
   9  -4   6 1262.32 307.457   4
   9   4   6 1070.44 327.521   4
   9  -4   6 662.272 222.299   6
   9   4   6 1131.15 324.642   6
   9  -4   7 1949.59 221.172   5
   9   4   7 1870.17 351.769   2
   9  -4   7 2919.30 441.495   4
   9   4   7 2343.11 493.711   4
   9  -4   8 968.010 121.503   5
   9   4   8 995.701 191.953   2
   9  -4   8 1121.68 244.483   4
   9   4   8 978.725 298.541   4
   9  -4   9 1331.22 190.302   4
   9   4   9 1347.94 237.692   4
   9   4   9 1220.92 163.999   2
   9  -5   0 179.703 152.262  11
   9  -5   0 256.709 74.1429   5
   9   5   0 405.775 99.2056   1
   9   5   0 470.380 133.087   2
   9  -5  -1 16083.6 829.543   5
   9  -5   1 15832.6 842.788   5
   9  -5   1 14042.5 1169.56  11
   9  -5  -1 17647.6 1213.25  11
   9   5   1 15671.2 838.558   1
   9   5  -1 15198.0 871.244   2
   9   5   1 17051.4 945.734   2
   9   5  -1 18426.7 878.950   1
   9  -5  -2 1869.55 169.236   5
   9  -5   2 1108.92 174.227   5
   9  -5   2 1856.55 363.353  11
   9  -5  -2 1585.57 306.974  11
   9   5  -2 1373.25 180.267   2
   9   5   2 1293.80 168.234   1
   9   5   2 1482.64 236.842   2
   9   5  -2 1785.43 177.019   1
   9  -5   3 30666.6 1884.21  11
   9  -5  -3 31238.9 1784.30  11
   9   5  -3 32019.6 1470.88   1
   9   5   3 32069.3 1516.69   1
   9   5   3 27988.2 1680.67   2
   9  -5   4 389.633 162.439  11
   9  -5  -4 341.027 139.365  11
   9  -5   4 429.220 173.064   5
   9  -5   4 481.278 150.308   4
   9   5   4 312.106 120.614   4
   9   5   4 342.254 103.494   1
   9   5  -4 268.934 94.7885   1
   9  -5   5 4200.71 481.762   5
   9  -5   5 3490.70 397.921   4
   9   5   5 4128.45 419.898   4
   9  -5  -5 5018.87 325.565   9
   9  -5   5 3832.89 494.109   6
   9   5   6 2386.78 609.130   2
   9  -5   6 1445.24 239.253   5
   9  -5   6 1683.34 295.015   4
   9   5   6 1930.15 316.689   4
   9   5   7 247.072 221.273   2
   9  -5   7 464.539 109.029   5
   9  -5   7 36.9982 171.829   4
   9   5   7 261.893 186.710   4
   9   5   7 298.171 90.3068   1
   9  -5   8 1224.74 134.579   5
   9  -5   8 1772.57 234.492   4
   9   5   8 1720.76 263.951   4
   9   5   8 1614.12 238.092   2
   9   5   9-16.9602 68.2386   2
   9  -6   0 83.4921 141.123  11
   9  -6   0 226.224 77.2337   5
   9   6   0 511.176 112.883   1
   9   6   0 443.041 128.489   2
   9  -6  -1 3582.08 292.856   5
   9   6   1 4688.54 328.697   1
   9  -6   1 4525.80 324.528   5
   9  -6   1 3088.47 520.490  11
   9  -6  -1 4532.06 577.683  11
   9   6  -1 5039.37 362.767   2
   9   6   1 4893.61 402.183   2
   9   6  -1 4632.81 320.500   1
   9  -6  -2 34097.1 1539.57   5
   9  -6   2 31086.1 1593.01   5
   9  -6   2 28362.8 1945.90  11
   9  -6  -2 32413.4 1911.50  11
   9   6   2 33952.9 1571.87   1
   9   6  -2 30545.3 1559.97   2
   9   6   2 34559.1 1723.69   2
   9   6  -2 34863.3 1546.06   1
   9  -6   3 14581.9 1199.11  11
   9  -6  -3 16230.7 1158.67  11
   9   6   3 17844.2 924.946   1
   9   6  -3 19410.8 908.674   1
   9   6   3 17163.4 1125.47   2
   9  -6   4 297.678 153.061  11
   9  -6  -4 276.672 141.190  11
   9   6   4 1095.76 400.544   2
   9  -6   4 800.299 238.699   5
   9   6   4 747.775 134.158   1
   9  -6   5 8925.33 739.915   5
   9   6   5 9141.41 534.647   1
   9  -6   5 7683.83 726.487   6
   9   6   6 182.579 73.8303   1
   9   6   6 193.086 384.132   2
   9  -6   6 202.793 114.206   5
   9  -6   6 140.075 122.359   4
   9   6   6 70.1174 110.186   4
   9  -6   7 1349.44 167.739   5
   9   6   7 1136.01 210.363   4
   9  -6   8 2669.03 200.634   5
   9   6   8 3056.87 329.888   2
   9   6   9 8.24171 62.9144   2
   9   7   0 713.572 116.332   1
   9  -7   0 328.210 94.0248   5
   9  -7   0 291.485 196.749  11
   9   7   0 930.949 160.522   2
   9   7   1 303.517 121.230   2
   9   7  -1 381.542 88.9645   1
   9  -7   1 407.420 244.671  11
   9  -7  -1 41.3057 189.892  11
   9  -7  -1 241.388 77.6256   5
   9  -7   1 285.832 87.8964   5
   9   7   1 357.773 95.0339   1
   9   7  -1 317.521 103.322   2
   9   7   2 340.920 139.785   2
   9  -7   2 258.296 163.411  11
   9  -7  -2 354.506 169.813  11
   9  -7  -2 290.729 78.4283   5
   9  -7   2 443.196 118.590   5
   9   7   2 578.945 112.594   1
   9   7  -2 378.302 89.5134   1
   9  -7   3 2917.39 316.449   5
   9  -7  -3 2038.58 340.605  11
   9   7   3 2867.01 243.062   1
   9  -7   3 1995.04 362.379  11
   9   7  -3 2752.91 248.366   1
   9   7   3 3011.38 399.513   2
   9  -7  -4 7681.73 689.407  11
   9   7   4 10323.2 960.211   2
   9   7   5 1968.04 612.417   2
   9  -7   5 1001.58 246.701   5
   9  -7   6 3555.07 342.022   5
   9   7   7-124.320 246.950   2
   9  -7   7 79.9574 65.9751   5
   9  -7   8 3950.55 245.893   5
   9   7   8 3531.45 373.353   2
   9   8   0 202.367 66.2725   1
   9  -8   0-53.2147 302.853  11
   9  -8   0 130.512 70.3422   5
   9   8   0 193.050 92.7610   2
   9  -8  -1 6240.02 386.068   5
   9  -8   1 5873.11 399.774   5
   9  -8   1 5387.92 717.574  11
   9   8  -1 6139.00 364.865   1
   9   8   1 6313.72 469.677   2
   9   8   1 5633.86 364.775   1
   9  -8  -2 1433.45 148.836   5
   9   8   2 1403.84 227.286   2
   9  -8   2 1143.60 167.778   5
   9  -8   2 744.166 283.426  11
   9  -8  -2 626.528 250.865  11
   9   8  -2 1739.62 172.199   1
   9   8   3 564.277 189.502   2
   9  -8   3 613.128 195.178  11
   9  -8  -3 742.223 202.990  11
   9  -8   3 780.447 167.980   5
   9  -8   4 5793.68 520.261   5
   9   8   4 6701.24 703.354   2
   9   8   5 50.1974 299.556   2
   9   8   6 2317.57 555.083   2
   9  -8   6 1062.24 174.533   5
   9  -8   7 1177.84 138.479   5
   9   8   8 224.770 134.859   2
   9  -8   8 75.9815 43.1324   5
   9  -9   0 177.354 70.7466   5
   9   9   0 166.293 57.7979   1
   9  -9  -1 6643.51 420.128   5
   9  -9   1 7559.87 458.822   5
   9  -9   1 5909.45 761.314  11
   9  -9  -1 5730.77 739.778  11
   9   9   1 8141.61 517.548   2
   9  -9   2 2078.35 222.756   5
   9  -9   2 1705.78 338.443  11
   9  -9  -2 1764.14 341.387  11
   9   9   2 2496.44 287.673   2
  -9   9   3 5566.46 353.969   3
   9  -9   3 6698.61 463.750   5
   9   9   3 5773.03 517.990   2
   9   9   4 1322.69 296.399   2
   9  -9   4 1274.61 218.891   5
   9   9   5 358.074 238.181   2
   9  -9   5 242.342 123.911   5
   9   9   6 4962.57 595.335   2
   9   9   7 171.765 170.596   2
   9  -9   7 25.2352 46.1325   5
   9 -10   0 77.6479 58.5373   5
   9 -10  -1 15364.7 806.991   5
   9 -10   1 17381.2 859.412   5
   9  10   1 16852.9 881.699   2
   9 -10   2 234.161 84.2724   5
  -9  10   2 53.4693 49.7237   3
   9  10   2 50.3957 76.9638   2
  -9  10   3 5531.24 335.481   3
   9 -10   3 5924.71 421.921   5
   9  10   3 5829.83 472.372   2
   9  10   4-18.1168 108.115   2
   9 -10   4-25.6349 81.5414   5
   9 -10   5 1777.56 223.742   5
   9  10   5 1569.78 280.583   2
   9  10   6-18.2685 137.505   2
   9  10   7 144.744 112.681   2
   9 -10   7 238.195 62.0425   5
   9 -11   0 65.2966 51.2857   5
   9 -11   1 9433.31 520.943   5
  -9  11   1 8732.85 497.672   3
  -9  11   2 1788.15 160.737   3
   9 -11   2 1679.22 182.367   5
   9 -11   3 3295.25 278.999   5
   9  11   3 3546.14 304.113   2
  -9  11   3 3198.39 213.995   3
   9  11   4 129.819 92.5727   2
   9 -11   4-9.98596 67.2474   5
   9  11   5-11.6429 92.5765   2
   9 -11   5 198.539 79.6286   5
   9  11   6 49.2035 78.2034   2
   9 -11   6 32.6980 52.6454   5
  -9  12   0 5.79288 39.6896   3
  -9  12   1 5863.35 345.564   3
   9 -12   1 5983.50 354.129   5
   9 -12   2 114.557 59.0292   5
  -9  12   2 137.614 48.4342   3
   9 -12   3 8167.37 440.119   5
  -9  12   3 6718.29 363.352   3
   9 -12   4 28.7538 59.9725   5
   9  12   4 6.64204 16.9044   2
   9 -12   5 153.315 57.4920   5
   9  12   5 65.1190 47.2268   2
  -9  13   0 95.7494 43.9848   3
  -9  13   1 53.4078 36.2480   3
  -9  13  -1 23.3059 34.6161   3
   9 -13   2 859.409 94.7672   5
  -9  13  -2 759.236 89.6709   3
  -9  13   2 666.804 74.5962   3
  -9  13  -3 1009.19 95.5501   3
  -9  13   3 818.966 72.9774   3
  -9  13  -4 1790.98 123.524   3
   9 -13   4 1850.31 146.237   5
  -9  14   0 25.6280 27.6641   3
  -9  14  -1 432.816 58.9324   3
  -9  14   1 409.102 52.7251   3
  -9  14   2 362.371 43.5614   3
  10   0   0 6861.98 411.890   5
  10   0   0 6867.50 478.243   9
  10   0   0 6156.29 414.430   1
  10   0   0 6123.27 465.550   2
  10   0   1 6154.37 394.072   5
  10   0  -1 5732.42 389.537   1
  10   0  -1 6194.90 454.713   9
  10   0   1 6243.34 456.005   9
  10   0   1 6746.37 486.985   2
  10   0   1 5670.80 408.861   1
  10   0   2 2121.34 205.439   5
  10   0  -2 2309.07 249.580   9
  10   0   2 2045.15 253.202   9
  10   0   2 1900.53 270.150   2
  10   0  -2 2329.63 219.174   1
  10   0  -3 75.8855 62.5708   1
  10   0   3 70.5252 56.0811   5
  10   0  -3-115.196 126.076   9
  10   0   3-27.4917 142.076   9
  10   0   3-72.2009 119.063   4
  10   0   3 20.8983 65.1289   6
  10   0   3-51.7838 129.923   2
  10   0   4 411.097 96.3471   5
  10   0  -4 55.4006 75.2873   9
  10   0   4 234.917 120.959   9
  10   0   4 372.216 174.765   4
  10   0  -4 422.167 97.7322   1
  10   0   4 187.417 113.434   6
  10   0   4 118.703 165.366   2
  10   0   5 4614.79 336.720   5
  10   0   5 4456.53 479.251   2
  10   0   5 4552.62 561.031   6
  10   0   6-281.278 529.281   4
  10   0   6 39.1318 111.330   6
  10   0   6 58.8598 132.089   2
  10   0   7 10147.5 1199.34   4
  10   0   7 5334.59 460.337   2
  10   0   8 775.604 281.182   4
  10   0   9 201.678 100.520   4
  10   1   0 10431.9 575.245   5
  10  -1   0 10314.1 635.612   9
  10   1   0 10158.2 642.999   9
  10   1   0 10214.8 590.259   1
  10  -1   0 9756.41 636.545   2
  10  -1   0 10110.3 586.466   1
  10  -1  -1 8234.37 500.799   5
  10   1   1 8774.85 507.703   5
  10  -1   1 8606.28 513.482   5
  10   1  -1 8433.78 511.338   1
  10  -1  -1 8802.93 513.287   1
  10  -1  -1 9097.74 573.689   9
  10  -1   1 8777.27 576.289   9
  10  -1  -1 9297.58 587.718   2
  10   1  -1 8258.32 571.229   9
  10   1   1 9561.03 601.742   9
  10   1  -1 9091.47 586.342   2
  10  -1   1 8648.58 586.546   2
  10   1   1 9074.23 609.554   2
  10   1   1 8314.50 525.433   1
  10  -1   1 8364.70 531.901   1
  10   1   2 516.756 98.9654   5
  10  -1   2 637.464 115.495   5
  10   1  -2 740.741 135.714   1
  10  -1  -2 614.469 142.014   9
  10  -1   2 848.533 170.290   9
  10   1  -2 486.480 144.043   9
  10   1   2 398.457 145.731   9
  10  -1  -2 717.152 125.223   1
  10   1  -2 482.273 148.208   2
  10  -1   2 414.868 152.739   2
  10   1   2 383.418 152.670   2
  10   1   3 10520.0 608.696   5
  10  -1   3 11216.3 646.718   5
  10  -1   3 9007.62 675.654   4
  10  -1  -3 12621.0 686.486   9
  10  -1   3 11633.7 703.926   9
  10   1  -3 11661.5 693.711   9
  10   1   3 11094.6 721.207   9
  10  -1   3 10083.3 720.534   2
  10   1   3 9078.42 731.129   2
  10   1  -3 12957.8 631.457   1
  10  -1  -3 13080.2 633.999   1
  10  -1   3 8586.47 754.154   6
  10   1   4 290.544 180.002   2
  10   1   4 238.801 69.0422   5
  10  -1   4 307.430 90.8082   5
  10  -1  -4 168.383 93.0873   9
  10  -1   4 141.765 109.039   9
  10  -1   4 75.9326 145.117   4
  10  -1  -4 124.671 75.0450   1
  10   1  -4 115.949 70.6445   1
  10  -1   4 249.617 132.258   6
  10  -1   4 192.623 139.347   2
  10   1   4 163.223 115.052   6
  10  -1   5 16195.0 834.267   5
  10  -1  -5 13945.5 796.788   9
  10  -1   5 13265.9 906.409   2
  10   1   5 14777.8 1040.22   2
  10  -1   5 14824.8 1131.31   6
  10   1   5 15367.1 1147.36   6
  10   1   6 285.549 186.795   2
  10  -1   6 152.665 72.2616   5
  10  -1   6-108.785 453.853   4
  10  -1   6 285.278 144.220   2
  10  -1   6 229.803 161.810   6
  10   1   6 200.332 135.103   6
  10  -1   7 4849.01 749.967   4
  10   1   7 3118.89 362.445   2
  10  -1   8 106.801 158.519   4
  10   1   8 100.226 91.9228   2
  10  -1   9 879.307 154.789   4
  10  -2   0 31840.7 1947.85  11
  10  -2   0 34834.5 1660.81   2
  10   2   0 34938.3 1695.06   9
  10   2   0 32391.4 1661.83   2
  10  -2   0 32355.6 1576.26   1
  10  -2   1 452.495 194.613  11
  10  -2  -1 453.515 194.890  11
  10  -2  -1 641.689 105.511   5
  10  -2   1 479.263 105.211   5
  10   2  -1 759.023 171.452   9
  10   2   1 607.949 155.252   9
  10   2  -1 563.276 118.075   1
  10  -2   1 871.219 173.702   2
  10   2  -1 560.781 143.515   2
  10  -2  -1 541.766 111.184   1
  10   2   2 10570.5 584.923   5
  10  -2   2 10597.5 615.130   5
  10  -2   2 9823.40 917.676  11
  10  -2  -2 10733.2 887.692  11
  10  -2  -2 10766.0 649.832   9
  10  -2   2 9800.09 655.244   9
  10   2  -2 9803.05 645.431   2
  10   2  -2 11966.2 697.551   9
  10   2   2 10688.5 698.381   9
  10  -2   2 10040.6 670.830   2
  10   2   2 9206.79 680.859   2
  10   2   2 10579.6 631.799   1
  10  -2   2 7738.59 683.877   6
  10   2  -2 11667.6 630.828   1
  10  -2  -2 11248.6 602.928   1
  10   2   3 410.028 172.692   2
  10   2  -3 385.017 93.5131   1
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  10  -2   5 2931.64 291.021   5
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  10   2   5 3134.03 489.971   4
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  10  -2   5 2619.64 422.934   6
  10   2   6 86.0229 196.460   2
  10  -2   6 23.6468 58.2700   5
  10  -2   6 80.4753 270.888   4
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  10   2   8 117.601 105.837   2
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  10  -4   2 39406.6 1848.74   2
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  10   4   6 699.195 355.914   2
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  10   4   8-11.5139 93.7971   2
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  10   5   0 7474.91 542.511   2
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  10  -6   0 30991.4 1509.74   5
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  10   6   0 30705.1 1587.84   2
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  10   6   1 44511.0 1980.69   1
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  10  -6  -1 40855.7 2519.92  11
  10   6  -1 41884.7 2010.17   2
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  10   6   2 12226.8 652.962   1
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  10 -11   4 2381.84 214.385   5
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  11   0   0 601.437 121.869   5
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  11   0   2 6616.23 450.702   5
  11   0  -2 6650.36 514.773   9
  11   0   2 6960.40 547.797   9
  11   0   2 5920.54 531.313   2
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  11   0   3 2546.24 351.433   2
  11   0  -3 3395.74 261.785   1
  11   0   4 31458.1 1534.63   5
  11   0  -4 29576.7 1573.60   9
  11   0   4 29329.7 1620.65   9
  11   0   4 28117.4 1687.38   2
  11   0   5 303.691 86.0158   5
  11   0   5 157.643 216.321   4
  11   0   5 215.250 160.099   2
  11   0   6 10139.2 1099.56   4
  11   0   6 8882.62 677.159   2
  11   0   7 344.722 308.330   4
  11   0   7 192.815 117.137   2
  11   0   8 2464.14 308.867   4
  11   1   0 99.0478 91.9646   1
  11  -1   0 87.5708 62.1183   5
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  11   1   0 177.067 129.631   9
  11  -1   0 216.366 102.209   1
  11  -1   0 334.901 139.758   2
  11   1   1 4801.36 345.388   5
  11  -1   1 4749.08 345.786   5
  11   1  -1 4234.34 339.850   1
  11  -1  -1 4290.18 340.499   1
  11  -1  -1 4984.06 418.404   2
  11  -1  -1 4002.19 388.332   9
  11  -1   1 4109.55 401.474   9
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  11   1   1 3561.45 396.094   9
  11   1  -1 5067.36 421.714   2
  11  -1   1 4357.09 409.484   2
  11   1   1 4599.15 366.129   1
  11   1   1 4924.71 438.605   2
  11  -1   1 4841.15 371.334   1
  11   1   2 1296.30 162.675   5
  11  -1   2 1307.70 172.941   5
  11   1  -2 1110.43 170.356   1
  11  -1  -2 780.161 182.040   9
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  11   1  -2 1105.82 210.267   9
  11   1   2 836.419 209.704   9
  11   1   2 1026.82 181.433   1
  11  -1   2 1199.58 229.316   2
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  11  -1  -3 609.235 155.153   9
  11  -1   3 821.010 190.852   9
  11   1  -3 500.492 164.406   9
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  11  -1   5-11.4156 59.8846   5
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  11   2   0 612.054 134.941   1
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  11   2   0 813.669 186.456   9
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  11  -2   1 197.352 84.4478   5
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  11  -2   1 339.661 138.569   9
  11   2  -1 609.887 175.520   9
  11   2   1 231.214 141.828   9
  11   2  -1 260.773 103.504   1
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  11   2  -1 284.679 128.444   2
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  11   2  -2 4170.05 377.063   2
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  11  -2   3 170.586 142.708   9
  11   2   3 219.723 118.969   1
  11  -2   3 204.261 139.069   2
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  11  -2   4 3775.23 362.531   5
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  11  -2  -4 5115.20 334.232   1
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  11   2   4 3078.73 456.358   2
  11   2   5 89.8395 205.229   2
  11  -2   5 113.871 85.0750   5
  11  -2   5 98.7290 160.192   4
  11   2   5 119.502 174.247   4
  11  -2   5 122.710 118.801   2
  11  -2   6 2520.25 256.977   5
  11  -2   6 2681.61 461.556   4
  11   2   6 2796.16 565.256   4
  11   2   6 1698.69 343.448   2
  11  -2   7 74.4383 194.600   4
  11   2   7 37.5231 261.478   4
  11   2   7-15.4441 111.152   2
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  11  -3  -1 58710.1 2775.73   1
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  11   3   1 61419.9 2827.76   1
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  11   3   3 21896.1 1156.79   1
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  11  -3   4 709.827 231.424   6
  11   3   5 2962.75 508.253   2
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  11   3   6 817.090 271.961   2
  11  -3   6 1155.86 185.946   5
  11  -3   7 701.492 114.413   5
  11   3   7 770.164 170.443   1
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  11   4  -4 1099.59 153.747   1
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  11   4   4 1550.28 219.895   1
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  11   4   5 352.668 302.783   2
  11   4   5 453.843 132.672   1
  11  -4   5 657.892 189.821   5
  11   4   6 1260.21 358.484   2
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  11   4   7 79.8004 77.2902   1
  11   4   8-6.06328 24.3947   1
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  11   5  -1 28764.7 1419.94   2
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  11   5   1 25741.7 1430.86   2
  11   5  -1 27794.9 1337.56   1
  11  -5  -2 15967.2 833.882   5
  11  -5   2 12613.1 1263.47  11
  11  -5  -2 15168.5 1217.63  11
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  11   5   3 329.802 177.799   2
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  11  -5  -3 209.794 154.664  11
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  11   5   3 240.143 98.6981   1
  11   5  -3 333.398 91.8424   1
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  11  -5   4 675.730 216.127   5
  11  -5  -4 894.604 161.197   9
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  11   5   4 854.317 164.522   1
  11   5   5-104.136 310.737   2
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  11   5   5 77.6801 82.4181   1
  11   5   6-107.250 269.092   2
  11  -5   6 50.2371 69.6839   5
  11   5   6 76.6686 77.1451   1
  11   5   7 388.827 171.552   2
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  11   5   7 409.730 97.0254   1
  11   5   8 470.417 109.569   2
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  11  -6   1 27951.4 2238.12  11
  11  -6  -1 31013.3 2213.70  11
  11   6  -1 34668.2 1680.98   2
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  11  -6   4 26724.9 1585.84   5
  11   6   4 30236.9 1379.72   1
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  11  -6   4 25728.0 1383.19   9
  11  -6   5 1621.23 279.700   5
  11   6   5 1515.25 181.218   1
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  11   7   3 681.975 129.340   1
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  11  -8   0 47.1121 60.0020   5
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  12  -2   6 99.9516 74.2707   5
  12   2   6 139.636 136.736   1
  12   2   6 41.2581 166.045   2
  12   2   7 248.780 149.481   1
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  12   3   3 71.7415 146.029   2
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  13   7  -1 921.679 127.694   1
  13   7   1 706.452 162.363   2
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  13  -7  -2 2487.57 289.289   9
  13  -7   2 2252.51 290.204   9
  13   7   2 2139.74 281.719   2
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  13   7   3 5184.24 495.984   2
  13   7   3 4955.76 328.177   1
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  13   7   4 4791.00 514.215   2
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  13  -8   0 177.550 75.0315   5
  13  -8   0 27.5456 175.442   9
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  13  -8  -1 6786.75 597.721   9
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  13  -8  -2-40.1521 111.787   9
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  13   8   2 161.118 57.8975   1
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  13  -8   3 1432.45 182.108   9
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  13   8   4 3417.46 385.941   2
  13  -8   5 891.608 126.610   5
  13   8   5 687.216 206.116   2
  13  -9   0 341.686 165.905   9
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  13  -9  -3 395.770 91.6546   9
  13   9   3 614.336 136.404   2
  13  -9   4 2571.86 233.210   5
  13   9   4 2125.18 244.681   2
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  13 -10   0 322.735 132.892   9
  13 -10   1 7295.58 400.655   5
  13 -10  -1 6176.69 472.496   9
  13 -10   1 6523.32 482.135   9
  13 -10   2 99.9316 64.1330   5
  13 -10   3 2847.40 190.221   5
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  14   0   0 2583.61 275.208   1
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  14   0  -2 11814.6 687.045   1
  14   0   3 4223.19 402.718   1
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  14   0  -3 3389.32 273.529   1
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  14   0   4 3259.46 422.167   2
  14   0   5 12176.1 836.951   2
  14   0   5 15644.4 1072.55   1
  14   0   6 9.35014 78.0068   2
  14   1   0 24753.5 1235.47   1
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  14  -1   1-28.1548 179.157   9
  14   1   1 96.1372 83.9175   1
  14   1   1 98.2322 147.942   2
  14  -1   1 115.533 105.938   1
  14   1   2 5442.26 437.405   1
  14  -1   2 4914.48 415.847   1
  14  -1   2 6383.23 553.200   2
  14  -1  -2 4726.27 477.862   9
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  14   1   2 5302.78 513.239   2
  14   1  -2 5391.33 376.259   1
  14  -1  -2 4844.66 362.370   1
  14   1   3 136.321 130.678   1
  14  -1   3 128.905 141.097   1
  14  -1   3 307.172 187.674   2
  14   1   3 168.219 176.079   2
  14  -1  -3 284.552 91.0724   1
  14   1  -3 576.636 112.816   1
  14  -1   4 785.846 226.365   2
  14  -1   4 1231.26 266.276   1
  14   1   4 1232.40 291.355   2
  14  -1   5 235.900 160.780   2
  14   1   5 275.354 168.349   2
  14  -1   5 575.445 278.157   1
  14   1   6-37.4128 150.535   1
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  14  -2   1 3918.95 351.674   1
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  14   2  -1 4804.14 370.332   1
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  14   2  -2-9.48641 64.9949   1
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  14   2   2-21.1010 131.518   2
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  14  -2   3 680.834 239.602   9
  14   2  -3 1364.29 166.050   1
  14  -2   3 537.605 166.798   1
  14   2   3 713.943 250.735   2
  14   2   4 93.6085 128.271   1
  14   2   4-28.3307 200.685   2
  14  -2   4-40.5470 159.001   1
  14   2   5 2105.32 309.420   1
  14   2   5 1442.07 290.836   2
  14  -2   5 1890.89 381.521   1
  14   2   6-29.4632 118.543   1
  14   2   6-11.2551 101.261   2
  14  -2   6-56.6052 161.038   1
  14   3   0 46538.3 2366.24   2
  14  -3   0 44368.9 2550.67   9
  14  -3   0 51342.9 2284.84   1
  14  -3   1 1262.47 188.204   1
  14   3  -1 1005.01 166.320   1
  14  -3  -1 926.331 255.013   9
  14  -3   1 900.850 291.394   9
  14  -3  -1 1137.67 159.460   1
  14  -3   2 17973.6 1012.69   5
  14   3   2 17103.4 938.614   1
  14  -3   2 15599.1 888.911   1
  14  -3  -2 14968.2 988.661   9
  14  -3   2 14029.1 1088.36   9
  14  -3  -2 15640.7 806.695   1
  14   3  -2 16359.6 846.467   1
  14  -3   3 1915.48 313.589   5
  14   3   3 1936.84 258.340   1
  14  -3   3 1942.79 254.477   1
  14  -3  -3 2050.53 265.320   9
  14   3  -3 2386.14 218.352   1
  14  -3   3 1408.60 283.936   9
  14   3   3 1821.65 360.650   2
  14  -3   4 5690.49 544.970   5
  14   3   4 7331.01 537.100   1
  14  -3   4 7866.20 583.558   1
  14   3   4 5608.82 661.085   2
  14   3   5 2152.75 270.308   1
  14   3   5 1640.55 331.226   2
  14  -3   5 1916.86 335.520   1
  14   3   6-11.7749 93.5631   2
  14  -3   6 43.5906 128.082   1
  14   3   6 64.5005 95.7463   1
  14   4   0 2401.37 294.825   2
  14  -4   0 2240.34 409.192   9
  14   4   0 2572.44 265.110   1
  14  -4   0 2509.68 261.462   1
  14  -4   1 2191.55 241.143   1
  14   4   1 2340.22 295.785   2
  14  -4  -1 2285.14 363.233   9
  14  -4   1 2311.93 416.859   9
  14  -4  -1 2389.91 205.776   1
  14   4   1 2753.10 295.270   1
  14  -4   2 164.705 125.599   5
  14  -4  -2 278.704 135.994   9
  14  -4   2 127.805 156.135   9
  14   4   2 91.1081 103.673   1
  14  -4   2 213.279 98.1119   1
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  14  -4   3 333.925 123.737   1
  14  -4  -3 505.800 135.056   9
  14  -4   3 321.058 158.656   9
  14   4   3 363.488 129.282   1
  14   4  -3 643.771 123.926   1
  14   4   4 1714.46 220.448   1
  14  -4   4 1564.75 279.727   5
  14  -4   4 1976.07 261.482   1
  14  -4  -4 1125.50 176.567   9
  14   4   4 1177.68 363.385   2
  14  -4   5 1552.39 201.759   5
  14   4   5 1922.27 220.585   1
  14  -4   5 2193.61 290.858   1
  14   4   5 1540.96 362.148   2
  14   4   6 268.722 87.0423   1
  14  -4   6 331.935 125.096   1
  14   4   6 276.974 124.120   2
  14   5   0 10924.2 707.952   2
  14  -5   0 10815.8 945.061   9
  14   5   0 10960.1 630.788   1
  14  -5   1 37.9423 72.0439   5
  14   5   1 43.4163 80.5955   1
  14  -5  -1 53.5548 148.538   9
  14  -5   1 31.7190 184.961   9
  14  -5   1 103.631 76.2001   1
  14   5   1 111.645 109.328   2
  14   5  -1 139.704 71.2152   1
  14  -5   2 4182.02 328.391   1
  14  -5  -2 3527.16 391.563   9
  14  -5   2 3473.19 429.963   9
  14   5   2 4037.27 422.292   2
  14   5  -2 4993.82 330.077   1
  14   5   2 5715.02 411.404   1
  14  -5   3 773.907 148.316   1
  14  -5   3 498.092 192.719   5
  14   5   3 755.407 154.814   1
  14  -5  -3 565.835 143.799   9
  14  -5   3 494.404 158.300   9
  14  -5   4 3065.98 375.466   5
  14  -5   4 3102.30 285.931   1
  14   5   4 3117.35 266.984   1
  14  -5   5 334.489 104.092   5
  14  -5   5 470.769 129.874   1
  14   5   5 314.299 89.5261   1
  14   5   5 195.566 230.820   2
  14   6   0 7229.71 499.714   2
  14   6   0 6596.95 417.401   1
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  14   6   1 2347.15 281.240   2
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  14   6  -1 3168.88 241.370   1
  14   6   1 2611.38 238.337   1
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  14   6   3 5905.71 577.187   2
  14   6   3 6540.22 393.388   1
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  14   6   4 1446.70 150.990   1
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  14   7   1 202.329 104.611   2
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  14   7   1 168.805 71.0844   1
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  14  -7  -2 457.935 141.641   9
  14  -7   2 583.201 153.775   9
  14   7   2 859.341 112.047   1
  14   7   2 878.333 185.501   2
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  14   7   4 596.249 233.055   2
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  14  -8  -2 6654.10 368.949   9
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  14   8   2 7700.02 398.377   2
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  14  -9   0 12662.0 832.977   9
  14  -9  -1-13.9380 98.7337   9
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  15   0   0 35.1317 85.6005   1
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  15   0  -2 4283.32 299.781   1
  15   0   3 1041.43 275.356   2
  15   0  -3 766.277 134.378   1
  15   0   3 1197.53 224.213   1
  15   0   4 887.492 253.725   1
  15   0   5 68.3057 173.829   1
  15   1   0 34.6510 88.2134   1
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  15   1  -1 21042.5 1097.87   1
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  15   1   1 23515.5 1179.79   1
  15  -1   1 21801.3 1139.02   1
  15   1   2 6474.81 489.963   1
  15  -1   2 6397.88 473.689   1
  15   1   2 6526.81 582.575   2
  15  -1  -2 6389.91 405.263   1
  15   1  -2 6564.85 416.661   1
  15   1   3 9023.94 670.916   1
  15  -1   3 9731.53 669.834   1
  15   1   3 7928.14 744.837   2
  15  -1   4 3976.23 459.582   1
  15   1   4 3991.28 474.107   2
  15  -1   5 1549.02 307.125   1
  15   1   5 1104.80 204.885   2
  15  -2   0 689.956 275.060   9
  15   2   0 1232.92 182.160   1
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  15  -2   1 5731.80 661.762   9
  15   2  -1 5515.93 389.599   1
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  15   2   1 6745.14 472.545   1
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  15  -2   2 151.430 99.9461   1
  15   2   2 171.815 173.119   2
  15  -2  -2 299.445 80.0828   1
  15   2  -2 257.304 84.4465   1
  15   2  -3 1909.89 204.842   1
  15   2   3 1327.97 333.081   2
  15  -2   3 1541.29 235.844   1
  15   2   4 4495.49 431.279   1
  15  -2   4 4302.83 443.801   1
  15   2   4 3792.32 511.602   2
  15  -2   5 927.644 244.644   1
  15   2   5 775.003 191.432   2
  15   2   5 834.383 195.850   1
  15  -3   0 239.317 88.8267   1
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  15  -3  -1 781.097 267.493   9
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  15   3  -2 528.806 108.726   1
  15   3   3 717.724 168.134   1
  15  -3   3 725.387 172.511   1
  15   3   4 233.197 123.740   1
  15   3   4 192.272 273.644   2
  15  -3   4 192.096 147.111   1
  15   3   5 44.3372 94.6123   1
  15   3   5-69.4128 154.552   2
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  15   4   0 9.12670 71.5847   1
  15  -4   0-25.9015 62.2057   1
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  15  -4   1 14580.6 1162.74   9
  15   4   1 14560.1 820.062   1
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  15  -5   1 2808.39 454.652   9
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  15   5   1 2525.87 231.935   1
  15   5   2-8.57572 65.4633   1
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  15   5   3 241.266 89.0251   1
  15  -5  -3 124.091 88.7248   9
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  15   5   4 67.1327 64.0213   1
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  15   6  -1 586.762 105.031   1
  15   6   1 442.275 89.4333   1
  15   6   2 105.262 54.5911   1
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  15   6   3 70.4572 50.1238   1
  15   6   3 220.026 189.225   2
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  15   7   0 87.0368 59.2789   1
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  15  -7   1 11609.9 862.922   9
  15   7   2 1330.85 120.585   1
  16   0   0 30054.1 1426.50   1
  16   0  -1 1646.36 169.364   1
  16   0   1 2143.78 221.801   1
  16   0  -2 7051.32 413.602   1
  16   0   2 6638.74 493.940   1
  16   0   3 359.364 146.875   1
  16   0   4 623.809 198.164   1
  16   1   0 948.837 137.835   1
  16  -1   0 1105.60 136.931   1
  16   1   1 669.821 133.667   1
  16  -1   1 729.079 139.698   1
  16  -1  -1 786.675 110.667   1
  16   1  -1 815.404 120.625   1
  16  -1  -2 3232.78 236.606   1
  16   1  -2 3299.56 247.551   1
  16   1   2 3172.88 325.238   1
  16  -1   2 3009.71 301.078   1
  16   1   3 744.189 191.101   1
  16  -1   3 887.911 185.286   1
  16  -1   4 365.690 161.808   1
  16   2   0 8768.55 509.651   1
  16  -2   0 8679.49 485.935   1
  16   2   1 454.407 112.366   1
  16  -2   1 545.607 110.054   1
  16  -2  -1 409.194 82.1749   1
  16   2  -1 620.872 104.452   1
  16   2  -2 3988.68 278.960   1
  16  -2   2 3280.14 309.253   1
  16  -2   3 171.092 120.655   1
  16  -3   0 3653.26 244.046   1
  16   3   0 3621.05 274.192   1
  16  -3   1 604.980 106.819   1
  16  -3  -1 862.065 95.5999   1
  16   3  -1 844.328 120.404   1
  16   3   2 1656.01 215.621   1
  16  -3   2 2010.69 206.093   1
  16   3   3 1925.11 229.628   1
  16  -3   3 1906.17 217.794   1
  16  -4   0 10968.2 1043.96   9
  16   4   1 745.102 118.374   1
  16   4   2 130.439 73.5005   1
  16  -4   2 102.349 61.4895   1
  16  -5   0 583.368 317.934   9
  16   5   0 627.116 100.309   1
  16   5  -1 2198.27 185.781   1
  16   5   1 1356.58 150.629   1
  16   5   2 566.986 94.5787   1
  17   0   0 231.098 66.2072   1
  17  -1   0 41.7697 44.2593   1
  17   1   0 85.5243 52.8704   1
   0   0   0    0.00    0.00   0
TITL SC2(3) in Pnma
REM Pnma (#62, found as Pcmn in -cba setting)
CELL 1.54184  14.150747  14.016202   9.862408  90.0000  90.0000  90.0000
ZERR    4.00   0.000530   0.000544   0.000516   0.0000   0.0000   0.0000
LATT  1
SYMM -x+1/2,-y, z+1/2
SYMM -x, y+1/2,-z
SYMM  x+1/2,-y+1/2,-z+1/2
SFAC C H N O Cl Zn
UNIT 72.00 56.00 24.00 4.00 8.00 4.00
REM  CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0
TEMP -173
SIZE 0.20 0.24 0.49
TREF
HKLF 4
END
;
_shelx_hkl_checksum              63549
_shelx_res_file
;
TITL sc2(3)_a.res in Pnma
    sc2(3).res
    created by SHELXL-2019/2 at 06:00:11 on 18-Nov-2023
REM Old TITL SC2(3) in Pnma
REM SHELXT solution in Pnma: R1 0.202, Rweak 0.216, Alpha 0.021
REM <I/s> 2.211 for 209 systematic absences, Orientation as input
REM Formula found by SHELXT: C21 N3 O Cl2 Zn
CELL 1.54184 14.1507 14.0162 9.8624 90 90 90
ZERR 4 0.0005 0.0005 0.0005 0 0 0
LATT 1
SYMM 0.5-X,-Y,0.5+Z
SYMM -X,0.5+Y,-Z
SYMM 0.5+X,0.5-Y,0.5-Z
SFAC C H N O Cl Zn
UNIT 72 56 24 4 8 4
EQIV $1 1.5-X,1-Y,0.5+Z
L.S. 10
PLAN  5
SIZE 0.201 0.24 0.49
TEMP -173.15(10)
CONF
HTAB O1 N4_$1
list 4
MORE -1
BOND $H
fmap 2
acta
REM <olex2.extras>
REM <HklSrc "%.\\SC2(3).hkl">
REM </olex2.extras>
WGHT    0.130900    4.675600
FVAR       2.67726
ZN1   6    0.342632    0.250000    0.542356    10.50000    0.01735    0.02634 =
         0.05509    0.00000   -0.00009    0.00000
CL1   5    0.292652    0.109442    0.468745    11.00000    0.02863    0.03765 =
         0.07018   -0.01143    0.00017   -0.00862
O1    4    0.336369    0.250000    0.744274    10.50000    0.01877    0.02047 =
         0.05709    0.00000   -0.00008    0.00000
N1    3    0.487326    0.250000    0.511190    10.50000    0.01720    0.02686 =
         0.05497    0.00000   -0.00072    0.00000
N2    3    0.823573    0.334965    0.403024    11.00000    0.02083    0.02550 =
         0.05166    0.00008   -0.00190   -0.00100
N4    3    1.058723    0.594674    0.306574    11.00000    0.03304    0.02863 =
         0.05193    0.00358    0.00060   -0.00583
N3    3    0.962641    0.250000    0.342954    10.50000    0.02061    0.02674 =
         0.04873    0.00000   -0.00013    0.00000
C4    1    0.781730    0.250000    0.420656    10.50000    0.02507    0.02574 =
         0.04707    0.00000   -0.00182    0.00000
C2    1    0.631470    0.335792    0.474143    11.00000    0.02210    0.02505 =
         0.05376    0.00217    0.00123   -0.00168
AFIX  43
H2    2    0.663437    0.395235    0.467974    11.00000   -1.20000
AFIX   0
C5    1    0.913846    0.330555    0.363508    11.00000    0.02018    0.02631 =
         0.05006    0.00013   -0.00352   -0.00095
C3    1    0.680766    0.250000    0.458473    10.50000    0.02335    0.02594 =
         0.04683    0.00000   -0.00102    0.00000
C1    1    0.535350    0.332452    0.498779    11.00000    0.02443    0.02308 =
         0.05921   -0.00108    0.00010    0.00180
AFIX  43
H1    2    0.501758    0.390828    0.507312    11.00000   -1.20000
AFIX   0
C8    1    0.964336    0.422457    0.342110    11.00000    0.02709    0.02766 =
         0.04857   -0.00461    0.00165   -0.00289
C9    1    0.914891    0.508245    0.341288    11.00000    0.02495    0.02957 =
         0.05482    0.00153   -0.00196   -0.00188
AFIX  43
H9    2    0.848244    0.509272    0.352790    11.00000   -1.20000
AFIX   0
C6    1    1.105526    0.512330    0.307620    11.00000    0.02272    0.03351 =
         0.05467    0.00617    0.00577   -0.00330
AFIX  43
H6    2    1.172110    0.513512    0.295422    11.00000   -1.20000
AFIX   0
C7    1    1.061475    0.424864    0.325716    11.00000    0.02610    0.02784 =
         0.05377    0.00141   -0.00002   -0.00003
AFIX  43
H7    2    1.097345    0.367576    0.326843    11.00000   -1.20000
AFIX   0
C10   1    0.965001    0.591955    0.323344    11.00000    0.03219    0.02888 =
         0.05617   -0.00035   -0.00003   -0.00038
AFIX  43
H10   2    0.931152    0.650487    0.322906    11.00000   -1.20000
AFIX   0
H11   2    0.367023    0.297914    0.770648    11.00000    0.06470
HKLF 4
REM  sc2(3)_a.res in Pnma
REM wR2 = 0.2197, GooF = S = 1.111, Restrained GooF = 1.111 for all data
REM R1 = 0.0738 for 1578 Fo > 4sig(Fo) and 0.0820 for all 1858 data
REM 140 parameters refined using 0 restraints
END
WGHT      0.1309      4.6756
REM Highest difference peak  2.100,  deepest hole -2.087,  1-sigma level  0.139
Q1    1   0.3413  0.2500  0.6452  10.50000  0.05    2.10
Q2    1   0.3431  0.2500  0.4436  10.50000  0.05    1.62
Q3    1   0.4064  0.2500  0.5448  10.50000  0.05    0.98
Q4    1   0.2842  0.2500  0.5431  10.50000  0.05    0.97
Q5    1   0.2944  0.1089  0.5699  11.00000  0.05    0.88
;
_shelx_res_checksum              71131
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z'
'-x-1/2, y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Zn Zn1 0.34263(6) 0.250000 0.54236(11) 0.0329(4) Uani d 1 . .
Cl Cl1 0.29265(9) 0.10944(9) 0.46875(16) 0.0455(5) Uani d 1 . .
O O1 0.3364(3) 0.250000 0.7443(6) 0.0321(11) Uani d 1 . .
N N1 0.4873(4) 0.250000 0.5112(7) 0.0330(13) Uani d 1 . .
N N2 0.8236(3) 0.3350(3) 0.4030(5) 0.0327(9) Uani d 1 . .
N N4 1.0587(3) 0.5947(3) 0.3066(5) 0.0379(10) Uani d 1 . .
N N3 0.9626(4) 0.250000 0.3430(7) 0.0320(13) Uani d 1 . .
C C4 0.7817(5) 0.250000 0.4207(8) 0.0326(15) Uani d 1 . .
C C2 0.6315(3) 0.3358(3) 0.4741(6) 0.0336(11) Uani d 1 . .
H H2 0.663437 0.395235 0.467974 0.040 Uiso calc 1 . .
C C5 0.9138(3) 0.3306(3) 0.3635(6) 0.0322(11) Uani d 1 . .
C C3 0.6808(5) 0.250000 0.4585(7) 0.0320(15) Uani d 1 . .
C C1 0.5354(3) 0.3325(3) 0.4988(6) 0.0356(11) Uani d 1 . .
H H1 0.501758 0.390828 0.507312 0.043 Uiso calc 1 . .
C C8 0.9643(3) 0.4225(3) 0.3421(6) 0.0344(11) Uani d 1 . .
C C9 0.9149(3) 0.5082(3) 0.3413(6) 0.0364(12) Uani d 1 . .
H H9 0.848244 0.509272 0.352790 0.044 Uiso calc 1 . .
C C6 1.1055(3) 0.5123(4) 0.3076(6) 0.0370(12) Uani d 1 . .
H H6 1.172110 0.513512 0.295422 0.044 Uiso calc 1 . .
C C7 1.0615(3) 0.4249(3) 0.3257(6) 0.0359(11) Uani d 1 . .
H H7 1.097345 0.367576 0.326843 0.043 Uiso calc 1 . .
C C10 0.9650(4) 0.5920(4) 0.3233(6) 0.0391(12) Uani d 1 . .
H H10 0.931152 0.650487 0.322906 0.047 Uiso calc 1 . .
H H11 0.367(5) 0.298(5) 0.771(8) 0.06(2) Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Zn1 0.0174(6) 0.0263(6) 0.0551(7) 0.000 -0.0001(3) 0.000
Cl1 0.0286(7) 0.0377(7) 0.0702(11) -0.0086(5) 0.0002(5) -0.0114(6)
O1 0.019(2) 0.020(2) 0.057(3) 0.000 0.000(2) 0.000
N1 0.017(3) 0.027(3) 0.055(4) 0.000 -0.001(2) 0.000
N2 0.0208(19) 0.0255(19) 0.052(3) -0.0010(15) -0.0019(17) 0.0001(18)
N4 0.033(2) 0.0286(19) 0.052(3) -0.0058(17) 0.001(2) 0.0036(18)
N3 0.021(3) 0.027(3) 0.049(4) 0.000 0.000(2) 0.000
C4 0.025(3) 0.026(3) 0.047(4) 0.000 -0.002(3) 0.000
C2 0.022(2) 0.025(2) 0.054(3) -0.0017(19) 0.001(2) 0.002(2)
C5 0.020(2) 0.026(2) 0.050(3) -0.0009(18) -0.0035(19) 0.000(2)
C3 0.023(3) 0.026(3) 0.047(4) 0.000 -0.001(3) 0.000
C1 0.024(2) 0.023(2) 0.059(3) 0.0018(19) 0.000(2) -0.001(2)
C8 0.027(2) 0.028(2) 0.049(3) -0.0029(19) 0.002(2) -0.005(2)
C9 0.025(2) 0.030(2) 0.055(3) -0.0019(19) -0.002(2) 0.002(2)
C6 0.023(2) 0.034(2) 0.055(3) -0.0033(19) 0.006(2) 0.006(2)
C7 0.026(2) 0.028(2) 0.054(3) 0.0000(19) 0.000(2) 0.001(2)
C10 0.032(3) 0.029(2) 0.056(3) 0.000(2) 0.000(2) 0.000(2)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-2 -1 -2 0.0993
0 2 -1 0.1535
0 1 -2 0.1299
0 1 -1 0.1407
-2 2 -1 0.1425
1 0 0 0.3673
0 -1 -2 0.0850
-2 -1 -1 0.1054
-2 1 -2 0.1316
-1 0 0 0.1225
-2 1 2 0.1249
0 -2 -1 0.0704
0 -1 0 0.0565
0 2 1 0.1563
0 -1 2 0.0725
2 1 1 0.3170
-2 -1 0 0.0955
2 -1 -1 0.2755
1 -1 1 0.1766
1 2 2 0.1936
2 -1 0 0.2993
0 -1 1 0.0629
-2 2 1 0.1452
-2 -2 1 0.0655
1 0 1 0.1936
0 -2 1 0.0473
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Cl1 Zn1 Cl1 . 7_565 125.55(9) ?
O1 Zn1 Cl1 . 7_565 108.25(7) ?
O1 Zn1 Cl1 . . 108.25(7) ?
O1 Zn1 N1 . . 101.1(2) ?
N1 Zn1 Cl1 . . 105.49(8) ?
N1 Zn1 Cl1 . 7_565 105.49(8) ?
Zn1 O1 H11 . . 107(5) ?
Zn1 O1 H11 . 7_565 107(5) ?
H11 O1 H11 . 7_565 106(10) ?
C1 N1 Zn1 . . 120.8(3) ?
C1 N1 Zn1 7_565 . 120.8(3) ?
C1 N1 C1 7_565 . 118.3(6) ?
C5 N2 C4 . . 114.7(4) ?
C6 N4 C10 . . 117.9(4) ?
C5 N3 C5 . 7_565 115.0(6) ?
N2 C4 N2 7_565 . 125.2(6) ?
N2 C4 C3 . . 117.4(3) ?
N2 C4 C3 7_565 . 117.4(3) ?
C3 C2 H2 . . 120.6 ?
C1 C2 H2 . . 120.6 ?
C1 C2 C3 . . 118.7(4) ?
N2 C5 N3 . . 125.2(4) ?
N2 C5 C8 . . 117.4(4) ?
N3 C5 C8 . . 117.4(4) ?
C2 C3 C4 7_565 . 120.7(3) ?
C2 C3 C4 . . 120.7(3) ?
C2 C3 C2 . 7_565 118.6(6) ?
N1 C1 C2 . . 122.8(4) ?
N1 C1 H1 . . 118.6 ?
C2 C1 H1 . . 118.6 ?
C9 C8 C5 . . 120.5(4) ?
C7 C8 C5 . . 121.0(4) ?
C7 C8 C9 . . 118.5(4) ?
C8 C9 H9 . . 120.8 ?
C10 C9 C8 . . 118.4(5) ?
C10 C9 H9 . . 120.8 ?
N4 C6 H6 . . 118.5 ?
N4 C6 C7 . . 123.0(4) ?
C7 C6 H6 . . 118.5 ?
C8 C7 C6 . . 118.9(4) ?
C8 C7 H7 . . 120.6 ?
C6 C7 H7 . . 120.6 ?
N4 C10 C9 . . 123.3(5) ?
N4 C10 H10 . . 118.4 ?
C9 C10 H10 . . 118.4 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Zn1 Cl1 . 2.2155(13) ?
Zn1 Cl1 7_565 2.2156(13) ?
Zn1 O1 . 1.993(6) ?
Zn1 N1 . 2.070(6) ?
O1 H11 7_565 0.84(7) ?
O1 H11 . 0.84(7) ?
N1 C1 . 1.346(5) ?
N1 C1 7_565 1.346(5) ?
N2 C4 . 1.341(5) ?
N2 C5 . 1.337(6) ?
N4 C6 . 1.331(7) ?
N4 C10 . 1.337(7) ?
N3 C5 . 1.339(5) ?
N3 C5 7_565 1.339(5) ?
C4 C3 . 1.477(10) ?
C2 H2 . 0.9500 ?
C2 C3 . 1.399(6) ?
C2 C1 . 1.382(7) ?
C5 C8 . 1.488(6) ?
C1 H1 . 0.9500 ?
C8 C9 . 1.391(7) ?
C8 C7 . 1.384(7) ?
C9 H9 . 0.9500 ?
C9 C10 . 1.382(7) ?
C6 H6 . 0.9500 ?
C6 C7 . 1.387(7) ?
C7 H7 . 0.9500 ?
C10 H10 . 0.9500 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
O1 H11 N4 2_665 0.84(7) 1.87(7) 2.706(5) 173(8) yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Zn1 N1 C1 C2 . . . . -178.1(5) ?
N2 C4 C3 C2 7_565 . . 7_565 -0.4(10) ?
N2 C4 C3 C2 7_565 . . . -177.8(6) ?
N2 C4 C3 C2 . . . . 0.4(10) ?
N2 C4 C3 C2 . . . 7_565 177.8(6) ?
N2 C5 C8 C9 . . . . -10.5(8) ?
N2 C5 C8 C7 . . . . 168.0(5) ?
N4 C6 C7 C8 . . . . 0.7(9) ?
N3 C5 C8 C9 . . . . 170.2(6) ?
N3 C5 C8 C7 . . . . -11.3(8) ?
C4 N2 C5 N3 . . . . -0.7(9) ?
C4 N2 C5 C8 . . . . 180.0(5) ?
C5 N2 C4 N2 . . . 7_565 0.7(11) ?
C5 N2 C4 C3 . . . . -177.4(6) ?
C5 N3 C5 N2 7_565 . . . 0.7(10) ?
C5 N3 C5 C8 7_565 . . . -179.9(4) ?
C5 C8 C9 C10 . . . . 178.9(5) ?
C5 C8 C7 C6 . . . . -179.3(5) ?
C3 C2 C1 N1 . . . . 1.4(9) ?
C1 N1 C1 C2 7_565 . . . -0.1(12) ?
C1 C2 C3 C4 . . . . 174.8(6) ?
C1 C2 C3 C2 . . . 7_565 -2.7(11) ?
C8 C9 C10 N4 . . . . 0.1(9) ?
C9 C8 C7 C6 . . . . -0.7(8) ?
C6 N4 C10 C9 . . . . -0.1(9) ?
C7 C8 C9 C10 . . . . 0.4(8) ?
C10 N4 C6 C7 . . . . -0.2(9) ?

_cod_database_fobs_code 2312575