#------------------------------------------------------------------------------ #$Date: 2024-08-20 04:47:31 +0300 (Tue, 20 Aug 2024) $ #$Revision: 294175 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/25/2312584.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312584 loop_ _publ_author_name 'Atencio, Reinaldo' 'Linares, Marciel M.' 'González, Teresa' 'Briceño, Alexander' _publ_section_title ; Multivalent hydrogen-bonded architectures directed by self-complementarity between [Cu(2,2'-biimidazole)] and malonate building blocks. ; _journal_coeditor_code OJ3021 _journal_issue 9 _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_paper_doi 10.1107/S2053229624007897 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '[Cu (C3 H2 O4) (C6 H6 N4) (H2 O1)], 2H2 O' _chemical_formula_moiety 'C9 H10 Cu N4 O5, 1.25[H~2~O], 0.75[H~2~O]' _chemical_formula_sum 'C9 H14 Cu N4 O7' _chemical_formula_weight 353.78 _chemical_name_systematic 'Aqua(2,2'-biimidazole-\k^2^N,N')(malonato-\k^2^O,O')copper(II) dihydrate' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 91.770(4) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 7.0587(4) _cell_length_b 20.3107(12) _cell_length_c 18.9523(10) _cell_measurement_reflns_used 6782 _cell_measurement_temperature 298.0(3) _cell_measurement_theta_max 26.9480 _cell_measurement_theta_min 3.1820 _cell_volume 2715.8(3) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2022) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) and DIAMOND (Brandenburg, 1996) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 298.3(3) _diffrn_detector 'Mercury CCD 2x2 bin detector' _diffrn_measured_fraction_theta_full 0.900 _diffrn_measured_fraction_theta_max 0.900 _diffrn_measurement_device '4-circle diffractometer' _diffrn_measurement_device_type 'Rigaku AFC' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0473 _diffrn_reflns_av_unetI/netI 0.0393 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 21646 _diffrn_reflns_theta_full 24.833 _diffrn_reflns_theta_max 24.833 _diffrn_reflns_theta_min 2.150 _diffrn_source 'sealed X-ray tube' _exptl_absorpt_coefficient_mu 1.649 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.90296 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2022) ; _exptl_crystal_colour green _exptl_crystal_density_diffrn 1.730 _exptl_crystal_description plate _exptl_crystal_F_000 1448 _exptl_crystal_size_max 0.364 _exptl_crystal_size_mid 0.112 _exptl_crystal_size_min 0.092 _refine_diff_density_max 0.577 _refine_diff_density_min -0.396 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 343 _refine_ls_number_reflns 4229 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0704 _refine_ls_R_factor_gt 0.0397 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0411P)^2^+6.8869P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0907 _refine_ls_wR_factor_ref 0.1079 _reflns_number_gt 2925 _reflns_number_total 4229 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file oj3021sup1.cif _cod_data_source_block 2 _cod_database_code 2312584 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.585 _shelx_estimated_absorpt_t_max 0.863 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu11 0.42536(8) 0.82052(3) 0.18851(3) 0.02555(17) Uani d 1 . . Cu Cu12 0.92614(8) 0.68105(3) 0.31015(3) 0.02619(17) Uani d 1 . . O O11 0.1067(4) 0.83742(16) 0.17496(17) 0.0351(8) Uani d 1 . . H H11A 0.023623 0.867206 0.190546 0.053 Uiso d 1 . . H H11B 0.043803 0.800356 0.185467 0.053 Uiso d 1 . . O O12 0.6085(4) 0.66516(16) 0.32368(17) 0.0347(8) Uani d 1 . . H H12A 0.555383 0.704161 0.312489 0.052 Uiso d 1 . . H H12B 0.539873 0.630551 0.308019 0.052 Uiso d 1 . . O O21 0.5061(5) 0.90321(16) 0.22934(16) 0.0365(8) Uani d 1 . . O O22 0.9078(4) 0.72406(16) 0.21856(15) 0.0319(8) Uani d 1 . . O O31 0.5118(6) 0.97758(19) 0.31415(19) 0.0542(11) Uani d 1 . . O O32 0.8681(5) 0.72086(17) 0.10302(16) 0.0379(8) Uani d 1 . . O O41 0.4120(4) 0.77879(15) 0.28048(15) 0.0307(8) Uani d 1 . . O O42 0.9960(5) 0.59806(16) 0.26836(16) 0.0354(8) Uani d 1 . . O O51 0.3819(5) 0.78240(17) 0.39580(16) 0.0388(9) Uani d 1 . . O O52 0.9763(6) 0.52341(18) 0.18392(18) 0.0483(10) Uani d 1 . . N N11 0.4949(5) 0.85173(19) 0.09227(19) 0.0295(9) Uani d 1 . . N N12 0.8997(5) 0.76600(19) 0.36224(19) 0.0274(9) Uani d 1 . . N N21 0.5017(6) 0.8291(2) -0.02103(19) 0.0336(10) Uani d 1 . . H H21 0.491782 0.806685 -0.061870 0.040 Uiso calc 1 . . N N22 0.8726(6) 0.8133(2) 0.4657(2) 0.0348(10) Uani d 1 . . H H22 0.873093 0.818880 0.512802 0.042 Uiso calc 1 . . N N31 0.3884(5) 0.73506(18) 0.13670(18) 0.0255(9) Uani d 1 . . N N32 0.9974(5) 0.64836(19) 0.4071(2) 0.0308(9) Uani d 1 . . N N41 0.3615(6) 0.6865(2) 0.0335(2) 0.0352(10) Uani d 1 . . H H41 0.363092 0.680094 -0.013424 0.042 Uiso calc 1 . . N N42 1.0034(6) 0.6685(2) 0.52080(19) 0.0348(10) Uani d 1 . . H H42 0.994689 0.690364 0.561843 0.042 Uiso calc 1 . . C C11 0.4664(6) 0.8059(2) 0.0432(2) 0.0274(11) Uani d 1 . . C C12 0.9147(6) 0.7577(2) 0.4316(2) 0.0284(11) Uani d 1 . . C C21 0.5500(7) 0.9069(3) 0.0567(3) 0.0350(12) Uani d 1 . . H H21A 0.578086 0.946011 0.076628 0.042 Uiso calc 1 . . C C22 0.8458(7) 0.8305(2) 0.3522(3) 0.0328(11) Uani d 1 . . H H22A 0.825031 0.849872 0.309989 0.039 Uiso calc 1 . . C C31 0.5555(7) 0.8933(3) -0.0131(3) 0.0405(13) Uani d 1 . . H H31 0.588315 0.921123 -0.047484 0.049 Uiso calc 1 . . C C32 0.8287(7) 0.8603(3) 0.4159(3) 0.0378(12) Uani d 1 . . H H32 0.795376 0.902330 0.423785 0.045 Uiso calc 1 . . C C41 0.4080(6) 0.7420(2) 0.0676(2) 0.0271(11) Uani d 1 . . C C42 0.9688(6) 0.6929(2) 0.4563(2) 0.0279(11) Uani d 1 . . C C51 0.3279(7) 0.6716(2) 0.1463(3) 0.0325(11) Uani d 1 . . H H51 0.303094 0.653035 0.188085 0.039 Uiso calc 1 . . C C52 1.0499(7) 0.5913(3) 0.4426(3) 0.0360(12) Uani d 1 . . H H52 1.076370 0.552414 0.422532 0.043 Uiso calc 1 . . C C61 0.3114(7) 0.6413(2) 0.0825(3) 0.0382(12) Uani d 1 . . H H61 0.274612 0.599514 0.074336 0.046 Uiso calc 1 . . C C62 1.0544(7) 0.6044(3) 0.5127(3) 0.0413(13) Uani d 1 . . H H62 1.085312 0.575909 0.547534 0.050 Uiso calc 1 . . C C71 0.4595(7) 0.9246(2) 0.2899(3) 0.0323(11) Uani d 1 . . C C72 0.8653(6) 0.6937(2) 0.1613(2) 0.0277(11) Uani d 1 . . C C81 0.3289(7) 0.8815(2) 0.3334(2) 0.0345(12) Uani d 1 . . H H81A 0.328492 0.897521 0.377589 0.041 Uiso calc 1 . . H H81B 0.210354 0.885224 0.315109 0.041 Uiso calc 1 . . C C82 0.8027(7) 0.6227(2) 0.1651(2) 0.0342(12) Uani d 1 . . H H82A 0.790993 0.606745 0.120926 0.041 Uiso calc 1 . . H H82B 0.687436 0.621334 0.183962 0.041 Uiso calc 1 . . C C91 0.3782(6) 0.8096(2) 0.3374(2) 0.0278(11) Uani d 1 . . C C92 0.9343(7) 0.5781(2) 0.2076(2) 0.0315(11) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu11 0.0366(4) 0.0268(3) 0.0133(3) -0.0022(2) 0.0012(2) -0.0010(2) Cu12 0.0373(4) 0.0280(3) 0.0133(3) 0.0027(2) -0.0001(2) 0.0002(2) O11 0.036(2) 0.0307(19) 0.038(2) 0.0037(14) 0.0036(15) 0.0009(15) O12 0.039(2) 0.0272(19) 0.038(2) -0.0038(14) 0.0010(15) 0.0026(15) O21 0.052(2) 0.036(2) 0.0213(18) -0.0115(16) 0.0045(15) -0.0037(15) O22 0.046(2) 0.032(2) 0.0171(17) -0.0025(15) 0.0007(14) 0.0000(14) O31 0.085(3) 0.039(2) 0.040(2) -0.020(2) 0.0131(19) -0.0156(18) O32 0.058(2) 0.042(2) 0.0135(18) -0.0001(17) -0.0006(15) 0.0021(15) O41 0.049(2) 0.0278(19) 0.0149(17) 0.0024(14) -0.0008(13) 0.0008(14) O42 0.051(2) 0.036(2) 0.0190(18) 0.0114(15) -0.0057(14) -0.0023(15) O51 0.063(2) 0.039(2) 0.0148(18) 0.0030(17) 0.0038(15) 0.0059(15) O52 0.072(3) 0.035(2) 0.037(2) 0.0136(18) -0.0130(18) -0.0087(17) N11 0.038(3) 0.032(2) 0.019(2) -0.0023(17) 0.0051(16) 0.0005(18) N12 0.035(2) 0.031(2) 0.017(2) -0.0024(17) 0.0002(15) 0.0024(17) N21 0.043(3) 0.044(3) 0.014(2) 0.0042(19) 0.0061(16) 0.0030(18) N22 0.050(3) 0.037(3) 0.017(2) -0.0001(19) -0.0030(17) -0.0068(19) N31 0.034(2) 0.026(2) 0.017(2) 0.0038(16) 0.0005(15) 0.0039(16) N32 0.036(3) 0.032(2) 0.024(2) 0.0037(17) -0.0033(16) -0.0003(18) N41 0.052(3) 0.037(3) 0.017(2) -0.002(2) 0.0019(17) -0.0063(19) N42 0.046(3) 0.045(3) 0.013(2) -0.004(2) -0.0042(17) 0.0013(18) C11 0.030(3) 0.036(3) 0.017(2) 0.004(2) 0.0047(18) 0.001(2) C12 0.029(3) 0.038(3) 0.018(3) -0.005(2) 0.0001(19) -0.006(2) C21 0.034(3) 0.036(3) 0.034(3) -0.007(2) 0.002(2) 0.003(2) C22 0.040(3) 0.030(3) 0.028(3) -0.003(2) -0.001(2) 0.003(2) C31 0.044(3) 0.048(4) 0.030(3) -0.001(2) 0.010(2) 0.015(3) C32 0.048(3) 0.031(3) 0.033(3) 0.000(2) 0.003(2) -0.004(2) C41 0.034(3) 0.034(3) 0.014(2) 0.007(2) 0.0008(18) -0.003(2) C42 0.029(3) 0.039(3) 0.016(2) -0.003(2) -0.0045(18) 0.001(2) C51 0.037(3) 0.032(3) 0.029(3) 0.004(2) 0.005(2) 0.002(2) C52 0.039(3) 0.035(3) 0.033(3) 0.006(2) -0.002(2) 0.007(2) C61 0.052(4) 0.027(3) 0.036(3) -0.002(2) 0.001(2) -0.005(2) C62 0.045(4) 0.049(4) 0.029(3) -0.001(2) -0.008(2) 0.017(3) C71 0.039(3) 0.030(3) 0.028(3) 0.002(2) -0.003(2) 0.000(2) C72 0.031(3) 0.032(3) 0.020(3) 0.007(2) -0.0005(19) 0.002(2) C81 0.049(3) 0.032(3) 0.023(3) 0.000(2) 0.009(2) -0.004(2) C82 0.045(3) 0.035(3) 0.022(3) 0.001(2) -0.009(2) -0.001(2) C91 0.031(3) 0.032(3) 0.020(3) -0.002(2) 0.0004(19) 0.000(2) C92 0.034(3) 0.034(3) 0.027(3) 0.001(2) 0.002(2) 0.004(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l 0 0 2 0 0 -2 0 0 2 0 0 -2 0 0 -3 0 0 3 0 0 -3 0 0 3 0 0 -4 0 0 4 0 0 -4 0 0 4 0 0 -5 0 0 5 0 0 -5 0 0 5 0 0 6 0 0 -6 0 0 6 0 0 -6 0 0 7 0 0 -7 0 0 -7 0 0 -8 0 0 -8 0 0 8 0 0 -9 0 0 9 0 0 -9 0 0 10 0 0 -10 0 0 -10 0 0 -11 0 0 11 0 0 -11 0 0 12 0 0 -12 0 0 -12 0 0 -13 0 0 -13 0 0 13 0 0 -14 0 0 -15 0 0 -16 0 0 16 0 0 -17 0 0 17 0 0 -18 0 0 18 0 0 -19 0 0 19 0 0 -20 0 0 20 0 0 -21 0 0 21 0 1 2 0 1 -2 0 -1 2 0 1 -2 0 -1 2 0 -1 -2 0 -1 -2 0 1 2 0 -1 3 0 1 -3 0 1 3 0 -1 -3 0 -1 -3 0 1 3 0 -1 3 0 1 -3 0 -1 4 0 1 -4 0 -1 4 0 1 -4 0 -1 -4 0 1 4 0 1 4 0 -1 -4 0 1 5 0 1 -5 0 -1 5 0 1 5 0 -1 -5 0 -1 -5 0 1 -5 0 -1 5 0 -1 6 0 1 -6 0 -1 -6 0 1 -6 0 1 6 0 1 6 0 -1 -6 0 1 -7 0 1 -7 0 -1 -7 0 -1 7 0 -1 -8 0 1 -8 0 -1 8 0 1 8 0 1 -8 0 -1 -8 0 1 -9 0 1 9 0 -1 -9 0 -1 9 0 -1 -9 0 1 -9 0 -1 -10 0 1 -10 0 -1 10 0 1 10 0 -1 -10 0 1 -10 0 1 11 0 -1 11 0 -1 -11 0 1 -11 0 1 -11 0 -1 -11 0 -1 12 0 1 12 0 1 -12 0 -1 -12 0 1 -12 0 -1 -12 0 -1 13 0 1 13 0 1 -13 0 -1 -13 0 -1 -13 0 1 -13 0 -1 -14 0 1 -14 0 1 -15 0 -1 -15 0 1 -16 0 -1 -16 0 -1 16 0 -1 17 0 1 17 0 1 -17 0 -1 -17 0 -1 -18 0 1 -18 0 -1 18 0 1 18 0 1 -19 0 -1 -19 0 1 19 0 -1 19 0 1 -20 0 -1 -20 0 1 20 0 -1 20 0 -1 -21 0 1 -21 0 -1 21 0 1 21 0 2 0 0 -2 0 0 -2 0 0 2 0 0 -2 1 0 2 -1 0 2 1 0 -2 -1 0 -2 -1 0 2 1 0 -2 1 0 2 -1 0 2 2 0 -2 -2 0 -2 2 0 2 -2 0 -2 -2 0 2 2 0 -2 3 0 2 -3 0 2 -3 0 -2 3 0 2 3 0 -2 -3 0 2 3 0 -2 -3 0 -2 4 0 2 -4 0 -2 -4 0 2 4 0 -2 4 0 2 -4 0 2 4 0 -2 -4 0 2 -5 0 2 5 0 -2 -5 0 -2 -5 0 2 5 0 2 -5 0 -2 5 0 2 6 0 -2 -6 0 2 -6 0 -2 -6 0 2 6 0 -2 6 0 2 -6 0 2 -7 0 2 7 0 -2 -7 0 -2 -7 0 2 7 0 -2 7 0 2 -7 0 -2 -8 0 2 8 0 2 -8 0 2 -8 0 -2 -8 0 -2 8 0 2 -9 0 -2 -9 0 2 9 0 -2 -9 0 -2 9 0 2 -9 0 -2 -10 0 2 -10 0 -2 10 0 -2 -10 0 2 10 0 2 -10 0 2 -11 0 -2 -11 0 2 -11 0 -2 -11 0 2 11 0 -2 11 0 2 -12 0 -2 -12 0 2 -12 0 -2 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-6 -7 -5 6 -7 5 6 7 6 -6 -7 -6 6 7 7 -6 -7 -7 6 -7 7 6 7 8 6 7 9 6 7 10 6 7 11 6 7 12 -6 -8 15 6 -8 -15 6 8 -15 -6 -8 14 6 8 -14 6 -8 -13 -6 8 13 6 8 -13 -6 -8 13 6 -8 -12 6 8 -12 -6 -8 12 -6 8 12 6 -8 -11 -6 8 11 6 8 -11 -6 -8 11 -6 8 10 -6 -8 10 6 8 -10 6 -8 -10 6 -8 -9 -6 8 9 6 8 -9 -6 -8 9 6 8 -8 -6 8 8 -6 -8 8 6 8 -8 6 -8 -8 6 8 -7 -6 -8 7 6 -8 -7 -6 8 7 6 8 -7 6 8 -6 6 -8 -6 6 8 -6 -6 8 6 6 8 -5 6 -8 -5 6 -8 -5 6 8 -5 -6 -8 5 -6 8 5 -6 -8 4 -6 8 4 6 8 -4 6 -8 -4 6 8 -4 6 -8 -4 -6 -8 3 6 8 -3 6 8 -3 6 -8 -3 6 -8 -3 -6 8 3 6 -8 -2 6 8 -2 -6 8 2 -6 -8 2 6 8 -2 6 8 -1 -6 -8 1 6 -8 -1 6 8 -1 -6 -8 0 6 8 0 6 -8 0 6 8 0 6 -8 0 -6 -8 -1 6 8 1 6 8 1 -6 -8 -2 6 8 2 6 8 2 6 -8 2 6 -8 2 -6 -8 -3 6 -8 3 6 8 3 6 -8 3 6 8 3 6 8 4 6 8 4 6 -8 4 -6 -8 -4 -6 -8 -5 6 8 5 6 -8 6 -6 -8 -6 6 8 6 -6 -8 -7 6 8 7 6 -8 7 6 8 8 6 8 9 6 8 10 6 8 11 6 -9 -14 6 9 -14 -6 -9 14 6 -9 -13 6 9 -13 -6 -9 13 6 -9 -12 -6 -9 12 6 9 -12 6 -9 -11 6 9 -11 -6 -9 11 -6 9 11 6 9 -10 -6 -9 10 -6 9 10 6 -9 -10 6 9 -9 6 -9 -9 -6 -9 9 -6 9 9 6 9 -8 -6 -9 8 6 9 -8 6 -9 -8 -6 9 8 6 9 -7 -6 -9 7 6 9 -7 6 -9 -7 -6 9 7 6 9 -6 6 9 -6 -6 -9 6 6 -9 -6 -6 9 6 6 9 -5 -6 -9 5 6 9 -5 6 -9 -5 -6 9 5 -6 -9 4 6 9 -4 6 9 -4 6 -9 -4 -6 9 4 6 -9 -3 6 9 -3 -6 9 3 -6 -9 3 6 9 -3 6 -9 -2 6 9 -2 6 -9 -2 6 9 -2 -6 -9 2 -6 -9 1 6 -9 -1 6 9 -1 6 9 -1 6 -9 -1 -6 -9 0 6 9 0 6 9 0 6 -9 0 -6 -9 -1 6 9 1 6 9 1 -6 -9 -2 6 9 2 6 9 2 6 9 3 -6 -9 -3 6 -9 3 6 9 3 6 -9 4 6 9 4 -6 -9 -4 6 -9 5 6 9 5 -6 -9 -5 6 9 6 -6 -9 -6 6 -9 6 6 9 7 -6 -9 -7 6 9 8 6 9 9 6 9 10 6 9 11 6 -10 -14 6 10 -14 -6 -10 14 6 -10 -13 6 10 -13 -6 -10 13 6 -10 -12 -6 -10 12 6 -10 -11 -6 -10 11 6 10 -11 6 -10 -10 -6 -10 10 6 10 -10 6 -10 -9 -6 -10 9 6 10 -9 -6 -10 8 6 -10 -8 -6 10 8 6 10 -8 -6 -10 7 6 -10 -7 -6 10 7 6 10 -6 -6 -10 6 6 10 -6 6 -10 -6 -6 10 6 6 10 -5 -6 10 5 6 10 -5 -6 -10 5 6 -10 -5 6 10 -4 6 10 -4 -6 -10 4 6 -10 -4 6 10 -3 6 10 -3 -6 -10 3 6 -10 -3 6 10 -2 6 -10 -2 -6 -10 2 6 10 -2 6 10 -1 6 10 -1 6 -10 -1 -6 -10 1 6 -10 0 6 10 0 6 10 0 -6 -10 0 6 10 1 -6 -10 -1 6 -10 1 6 10 1 6 10 2 -6 -10 -2 6 -10 2 6 10 2 -6 -10 -3 6 -10 3 6 10 3 -6 -10 -4 6 -10 4 6 10 4 6 -10 5 6 10 5 6 10 6 -6 -10 -6 6 10 7 -6 -10 -7 6 10 8 6 10 9 6 10 10 6 10 11 6 11 -13 6 -11 -13 -6 -11 13 6 11 -12 6 -11 -12 -6 -11 12 6 -11 -11 -6 -11 11 6 11 -11 6 -11 -10 -6 -11 10 6 11 -10 6 -11 -9 -6 -11 9 6 11 -9 6 -11 -8 -6 -11 8 6 11 -8 6 -11 -7 -6 -11 7 6 11 -7 6 -11 -6 6 11 -6 -6 -11 6 6 -11 -5 -6 -11 5 6 11 -5 6 11 -4 6 -11 -4 -6 -11 4 6 11 -4 6 11 -3 6 11 -3 -6 -11 3 6 -11 -3 6 11 -2 6 -11 -2 6 11 -2 -6 -11 2 6 -11 -1 6 11 -1 6 11 -1 -6 -11 1 6 -11 0 6 11 0 6 11 0 -6 -11 0 6 11 1 -6 -11 -1 6 11 2 -6 -11 -2 6 -11 2 6 11 3 -6 -11 -3 -6 -11 -4 6 -11 4 6 11 4 6 11 5 -6 -11 -5 6 11 6 -6 -11 -6 -6 -11 -7 6 11 7 6 11 8 6 11 9 6 11 10 6 -12 -12 -6 -12 12 6 12 -12 6 -12 -11 -6 -12 11 6 12 -11 6 -12 -10 -6 -12 10 6 12 -10 6 -12 -9 -6 -12 9 6 12 -9 6 -12 -8 -6 -12 8 6 12 -8 6 -12 -7 -6 -12 7 6 12 -7 6 12 -6 -6 -12 6 6 -12 -6 6 12 -5 -6 -12 5 6 -12 -5 6 12 -4 -6 -12 4 6 -12 -4 6 12 -3 6 -12 -3 -6 -12 3 6 -12 -2 6 12 -2 -6 -12 2 6 -12 -1 6 12 -1 -6 -12 1 6 -12 0 6 12 0 -6 -12 0 6 12 1 -6 -12 -1 6 -12 1 6 -12 2 -6 -12 -2 6 12 2 -6 -12 -3 6 12 3 -6 -12 -4 6 12 4 -6 -12 -5 6 12 5 -6 -12 -6 6 12 6 6 12 7 6 12 8 6 12 9 6 12 10 6 -13 -11 -6 -13 11 6 13 -11 6 -13 -10 -6 -13 10 6 13 -10 6 -13 -9 -6 -13 9 6 13 -9 6 -13 -8 -6 -13 8 6 13 -8 6 -13 -7 -6 -13 7 6 13 -7 6 13 -6 -6 -13 6 6 -13 -6 6 13 -5 -6 -13 5 6 -13 -5 6 13 -4 6 -13 -4 -6 -13 4 6 -13 -3 6 13 -3 -6 -13 3 6 -13 -2 -6 -13 2 6 -13 -1 6 13 -1 -6 -13 1 6 -13 0 6 13 0 -6 -13 0 6 13 1 -6 -13 -1 -6 -13 -2 6 13 2 -6 -13 -3 6 13 3 -6 -13 -4 6 13 4 -6 -13 -5 6 13 5 -6 -13 -6 6 13 6 6 13 7 6 13 8 6 13 9 6 13 10 -6 -14 10 6 14 -10 6 -14 -9 -6 -14 9 6 14 -9 6 -14 -8 -6 -14 8 6 14 -8 6 14 -7 -6 -14 7 6 -14 -7 6 14 -6 -6 -14 6 6 -14 -6 6 14 -5 -6 -14 5 6 -14 -5 6 14 -4 6 -14 -4 -6 -14 4 6 -14 -3 6 14 -3 -6 -14 3 6 -14 -2 6 14 -2 -6 -14 2 6 14 -1 -6 -14 1 6 14 0 -6 -14 0 -6 -14 -1 6 14 1 6 14 2 -6 -14 -2 6 14 3 -6 -14 -3 6 14 4 -6 -14 -4 6 14 5 -6 -14 -5 6 14 6 6 14 7 6 14 8 6 14 9 -6 -15 9 6 15 -9 -6 -15 8 6 15 -8 6 15 -7 -6 -15 7 6 15 -6 -6 -15 6 6 15 -5 -6 -15 5 6 15 -4 -6 -15 4 6 15 -3 -6 -15 3 6 15 -2 -6 -15 2 6 15 -1 -6 -15 1 6 15 0 -6 -15 0 6 15 1 -6 -15 -1 6 15 2 -6 -15 -2 6 15 3 -6 -15 -3 6 15 4 -6 -15 -4 6 15 5 6 15 6 6 15 7 6 15 8 6 16 -7 -6 -16 7 6 16 -6 -6 -16 6 6 16 -5 -6 -16 5 6 16 -4 -6 -16 4 6 16 -3 -6 -16 3 6 16 -2 -6 -16 2 6 16 -1 -6 -16 1 6 16 0 -6 -16 0 6 16 1 -6 -16 -1 6 16 2 -6 -16 -2 6 16 3 -6 -16 -3 6 16 4 6 16 5 6 16 6 6 17 -5 -6 -17 5 6 17 -4 -6 -17 4 -6 -17 3 6 17 -3 6 17 -2 -6 -17 2 6 17 -1 -6 -17 1 6 17 0 -6 -17 0 -6 -17 -1 6 17 1 -6 -17 -2 6 17 2 6 17 3 6 17 4 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O21 Cu11 O11 . . 101.09(13) ? O21 Cu11 O41 . . 92.40(13) ? O21 Cu11 N11 . . 90.69(15) ? O21 Cu11 N31 . . 169.11(15) ? O41 Cu11 O11 . . 95.25(12) ? O41 Cu11 N11 . . 166.75(15) ? O41 Cu11 N31 . . 93.00(14) ? N11 Cu11 O11 . . 96.79(14) ? N11 Cu11 N31 . . 81.97(15) ? N31 Cu11 O11 . . 87.83(13) ? O22 Cu12 O12 . . 97.18(12) ? O22 Cu12 N12 . . 92.78(14) ? O22 Cu12 N32 . . 167.40(15) ? O42 Cu12 O12 . . 100.73(13) ? O42 Cu12 O22 . . 92.11(13) ? O42 Cu12 N12 . . 169.67(15) ? O42 Cu12 N32 . . 91.53(14) ? N12 Cu12 O12 . . 87.68(13) ? N12 Cu12 N32 . . 81.83(15) ? N32 Cu12 O12 . . 93.99(14) ? Cu11 O11 H11A . . 135.7 ? Cu11 O11 H11B . . 109.9 ? H11A O11 H11B . . 99.1 ? Cu12 O12 H12A . . 104.6 ? Cu12 O12 H12B . . 126.4 ? H12A O12 H12B . . 113.2 ? C71 O21 Cu11 . . 125.1(3) ? C72 O22 Cu12 . . 123.4(3) ? C91 O41 Cu11 . . 124.0(3) ? C92 O42 Cu12 . . 124.0(3) ? C11 N11 Cu11 . . 112.3(3) ? C11 N11 C21 . . 105.6(4) ? C21 N11 Cu11 . . 141.9(3) ? C12 N12 Cu12 . . 111.9(3) ? C12 N12 C22 . . 105.8(4) ? C22 N12 Cu12 . . 141.5(3) ? C11 N21 H21 . . 126.4 ? C11 N21 C31 . . 107.2(4) ? C31 N21 H21 . . 126.4 ? C12 N22 H22 . . 126.2 ? C12 N22 C32 . . 107.7(4) ? C32 N22 H22 . . 126.2 ? C41 N31 Cu11 . . 112.0(3) ? C41 N31 C51 . . 105.8(4) ? C51 N31 Cu11 . . 141.6(3) ? C42 N32 Cu12 . . 112.4(3) ? C42 N32 C52 . . 106.0(4) ? C52 N32 Cu12 . . 141.2(3) ? C41 N41 H41 . . 126.1 ? C41 N41 C61 . . 107.7(4) ? C61 N41 H41 . . 126.1 ? C42 N42 H42 . . 126.5 ? C42 N42 C62 . . 107.1(4) ? C62 N42 H42 . . 126.5 ? N11 C11 N21 . . 111.2(4) ? N11 C11 C41 . . 116.4(4) ? N21 C11 C41 . . 132.3(4) ? N12 C12 N22 . . 111.0(4) ? N12 C12 C42 . . 116.7(4) ? N22 C12 C42 . . 132.3(4) ? N11 C21 H21A . . 125.3 ? C31 C21 N11 . . 109.3(4) ? C31 C21 H21A . . 125.3 ? N12 C22 H22A . . 125.3 ? C32 C22 N12 . . 109.4(4) ? C32 C22 H22A . . 125.3 ? N21 C31 H31 . . 126.7 ? C21 C31 N21 . . 106.7(4) ? C21 C31 H31 . . 126.7 ? N22 C32 H32 . . 127.0 ? C22 C32 N22 . . 106.1(4) ? C22 C32 H32 . . 127.0 ? N31 C41 N41 . . 110.8(4) ? N31 C41 C11 . . 116.8(4) ? N41 C41 C11 . . 132.3(4) ? N32 C42 N42 . . 111.4(4) ? N32 C42 C12 . . 116.2(4) ? N42 C42 C12 . . 132.3(4) ? N31 C51 H51 . . 125.5 ? C61 C51 N31 . . 109.1(4) ? C61 C51 H51 . . 125.5 ? N32 C52 H52 . . 125.9 ? C62 C52 N32 . . 108.1(5) ? C62 C52 H52 . . 125.9 ? N41 C61 H61 . . 126.7 ? C51 C61 N41 . . 106.6(4) ? C51 C61 H61 . . 126.7 ? N42 C62 H62 . . 126.3 ? C52 C62 N42 . . 107.4(4) ? C52 C62 H62 . . 126.3 ? O21 C71 C81 . . 117.6(4) ? O31 C71 O21 . . 123.6(5) ? O31 C71 C81 . . 118.8(4) ? O22 C72 C82 . . 118.8(4) ? O32 C72 O22 . . 122.4(4) ? O32 C72 C82 . . 118.8(4) ? C71 C81 H81A . . 108.2 ? C71 C81 H81B . . 108.2 ? H81A C81 H81B . . 107.4 ? C91 C81 C71 . . 116.2(4) ? C91 C81 H81A . . 108.2 ? C91 C81 H81B . . 108.2 ? C72 C82 H82A . . 108.5 ? C72 C82 H82B . . 108.5 ? C72 C82 C92 . . 114.9(4) ? H82A C82 H82B . . 107.5 ? C92 C82 H82A . . 108.5 ? C92 C82 H82B . . 108.5 ? O41 C91 C81 . . 118.9(4) ? O51 C91 O41 . . 122.6(4) ? O51 C91 C81 . . 118.5(4) ? O42 C92 C82 . . 118.4(4) ? O52 C92 O42 . . 122.0(4) ? O52 C92 C82 . . 119.6(4) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cu11 O11 . 2.282(3) ? Cu11 O21 . 1.928(3) ? Cu11 O41 . 1.943(3) ? Cu11 N11 . 2.006(4) ? Cu11 N31 . 2.007(4) ? Cu12 O12 . 2.287(3) ? Cu12 O22 . 1.944(3) ? Cu12 O42 . 1.933(3) ? Cu12 N12 . 1.999(4) ? Cu12 N32 . 2.003(4) ? O11 H11A . 0.8990 ? O11 H11B . 0.8995 ? O12 H12A . 0.8991 ? O12 H12B . 0.8991 ? O21 C71 . 1.281(5) ? O22 C72 . 1.276(5) ? O31 C71 . 1.222(6) ? O32 C72 . 1.235(5) ? O41 C91 . 1.275(5) ? O42 C92 . 1.283(6) ? O51 C91 . 1.237(5) ? O52 C92 . 1.239(6) ? N11 C11 . 1.327(6) ? N11 C21 . 1.370(6) ? N12 C12 . 1.327(5) ? N12 C22 . 1.375(6) ? N21 H21 . 0.8990 ? N21 C11 . 1.336(6) ? N21 C31 . 1.365(6) ? N22 H22 . 0.8990 ? N22 C12 . 1.340(6) ? N22 C32 . 1.371(6) ? N31 C41 . 1.329(5) ? N31 C51 . 1.372(6) ? N32 C42 . 1.319(6) ? N32 C52 . 1.384(6) ? N41 H41 . 0.8990 ? N41 C41 . 1.336(6) ? N41 C61 . 1.361(6) ? N42 H42 . 0.8990 ? N42 C42 . 1.335(6) ? N42 C62 . 1.362(6) ? C11 C41 . 1.442(6) ? C12 C42 . 1.443(6) ? C21 H21A . 0.8990 ? C21 C31 . 1.352(7) ? C22 H22A . 0.8990 ? C22 C32 . 1.361(7) ? C31 H31 . 0.8990 ? C32 H32 . 0.8990 ? C51 H51 . 0.8990 ? C51 C61 . 1.358(7) ? C52 H52 . 0.8990 ? C52 C62 . 1.356(7) ? C61 H61 . 0.8990 ? C62 H62 . 0.8990 ? C71 C81 . 1.531(7) ? C72 C82 . 1.511(6) ? C81 H81A . 0.8990 ? C81 H81B . 0.8990 ? C81 C91 . 1.502(6) ? C82 H82A . 0.8990 ? C82 H82B . 0.8990 ? C82 C92 . 1.512(6) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cu11 O21 C71 O31 . . . . -179.4(4) ? Cu11 O21 C71 C81 . . . . -0.2(6) ? Cu11 O41 C91 O51 . . . . -175.5(3) ? Cu11 O41 C91 C81 . . . . 5.5(6) ? Cu11 N11 C11 N21 . . . . 175.9(3) ? Cu11 N11 C11 C41 . . . . -5.0(5) ? Cu11 N11 C21 C31 . . . . -173.8(4) ? Cu11 N31 C41 N41 . . . . -172.9(3) ? Cu11 N31 C41 C11 . . . . 5.0(5) ? Cu11 N31 C51 C61 . . . . 169.9(4) ? Cu12 O22 C72 O32 . . . . -174.5(3) ? Cu12 O22 C72 C82 . . . . 7.7(6) ? Cu12 O42 C92 O52 . . . . -177.0(4) ? Cu12 O42 C92 C82 . . . . 1.5(6) ? Cu12 N12 C12 N22 . . . . -172.1(3) ? Cu12 N12 C12 C42 . . . . 7.2(5) ? Cu12 N12 C22 C32 . . . . 168.4(4) ? Cu12 N32 C42 N42 . . . . 175.2(3) ? Cu12 N32 C42 C12 . . . . -6.9(5) ? Cu12 N32 C52 C62 . . . . -172.2(4) ? O21 C71 C81 C91 . . . . 45.7(6) ? O22 C72 C82 C92 . . . . -51.8(6) ? O31 C71 C81 C91 . . . . -135.1(5) ? O32 C72 C82 C92 . . . . 130.4(5) ? N11 C11 C41 N31 . . . . 0.0(6) ? N11 C11 C41 N41 . . . . 177.3(5) ? N11 C21 C31 N21 . . . . 0.5(5) ? N12 C12 C42 N32 . . . . -0.2(6) ? N12 C12 C42 N42 . . . . 177.1(5) ? N12 C22 C32 N22 . . . . -0.1(5) ? N21 C11 C41 N31 . . . . 178.8(5) ? N21 C11 C41 N41 . . . . -3.8(9) ? N22 C12 C42 N32 . . . . 178.9(5) ? N22 C12 C42 N42 . . . . -3.8(9) ? N31 C51 C61 N41 . . . . -0.2(5) ? N32 C52 C62 N42 . . . . 0.6(6) ? C11 N11 C21 C31 . . . . -0.6(5) ? C11 N21 C31 C21 . . . . -0.3(5) ? C12 N12 C22 C32 . . . . -0.1(5) ? C12 N22 C32 C22 . . . . 0.2(5) ? C21 N11 C11 N21 . . . . 0.4(5) ? C21 N11 C11 C41 . . . . 179.5(4) ? C22 N12 C12 N22 . . . . 0.2(5) ? C22 N12 C12 C42 . . . . 179.5(4) ? C31 N21 C11 N11 . . . . -0.1(5) ? C31 N21 C11 C41 . . . . -179.0(5) ? C32 N22 C12 N12 . . . . -0.2(5) ? C32 N22 C12 C42 . . . . -179.4(5) ? C41 N31 C51 C61 . . . . -0.2(5) ? C41 N41 C61 C51 . . . . 0.5(5) ? C42 N32 C52 C62 . . . . -1.1(5) ? C42 N42 C62 C52 . . . . 0.2(5) ? C51 N31 C41 N41 . . . . 0.5(5) ? C51 N31 C41 C11 . . . . 178.4(4) ? C52 N32 C42 N42 . . . . 1.3(5) ? C52 N32 C42 C12 . . . . 179.1(4) ? C61 N41 C41 N31 . . . . -0.6(5) ? C61 N41 C41 C11 . . . . -178.1(5) ? C62 N42 C42 N32 . . . . -0.9(5) ? C62 N42 C42 C12 . . . . -178.3(5) ? C71 C81 C91 O41 . . . . -48.7(6) ? C71 C81 C91 O51 . . . . 132.3(5) ? C72 C82 C92 O42 . . . . 46.4(6) ? C72 C82 C92 O52 . . . . -135.0(5) ? _cod_database_fobs_code 2312584