#------------------------------------------------------------------------------ #$Date: 2024-12-07 19:06:06 +0200 (Sat, 07 Dec 2024) $ #$Revision: 296761 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/26/2312652.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312652 loop_ _publ_author_name 'Mohana, Marimuthu' 'Gomathi, Sundaramoorthy' 'Thomas Muthiah, Packianathan' 'Butcher, Ray J.' _publ_section_title ; Structural insights into supramolecular interactions in isostructural salts of 2,4,6-triaminopyrimidinium with various heterocyclic carboxylates. ; _journal_coeditor_code OV3176 _journal_issue 'Pt 11' _journal_name_full 'Acta crystallographica. Section C, Structural chemistry' _journal_page_first 734 _journal_page_last 741 _journal_paper_doi 10.1107/S2053229624008787 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C4 H8 N5 +, C5 H2 Cl O2 S -' _chemical_formula_moiety 'C4 H8 N5 +, C5 H2 Cl O2 S -' _chemical_formula_sum 'C9 H10 Cl N5 O2 S' _chemical_formula_weight 287.73 _chemical_name_systematic ; 2,4,6-Triaminopyrimidinium 5-chlorothiophene-2-carboxylate ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 78.406(4) _cell_angle_beta 87.357(4) _cell_angle_gamma 78.608(4) _cell_formula_units_Z 4 _cell_length_a 8.3306(5) _cell_length_b 10.4403(5) _cell_length_c 14.0361(5) _cell_measurement_reflns_used 4863 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 76.9 _cell_measurement_theta_min 3.2 _cell_volume 1172.28(10) _computing_cell_refinement ; CrysAlis PRO (Agilent, 2014) ; _computing_data_collection ; CrysAlis PRO (Agilent, 2014) ; _computing_data_reduction ; CrysAlis PRO (Agilent, 2014) ; _computing_molecular_graphics ; PLATON (Spek, 2020), Mercury (Macrae et al., 2020) and POVRay (Cason, 2004) ; _computing_publication_material ; PLATON (Spek, 2020) and publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2016 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device_type 'Rigaku XtaLAB Synergy Dualflex diffractometer with a HyPix detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0258 _diffrn_reflns_av_unetI/netI 0.0319 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 10298 _diffrn_reflns_theta_full 67.500 _diffrn_reflns_theta_max 76.869 _diffrn_reflns_theta_min 3.214 _exptl_absorpt_coefficient_mu 4.606 _exptl_absorpt_correction_T_max 0.608 _exptl_absorpt_correction_T_min 0.288 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Agilent, 2014) ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.630 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 592 _exptl_crystal_size_max 0.360 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.120 _refine_diff_density_max 0.677 _refine_diff_density_min -0.570 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 381 _refine_ls_number_reflns 4863 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0420 _refine_ls_R_factor_gt 0.0384 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0597P)^2^+0.7344P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1035 _refine_ls_wR_factor_ref 0.1075 _reflns_number_gt 4401 _reflns_number_total 4863 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ov3176sup1.cif _cod_data_source_block IV _cod_depositor_comments 'Adding full bibliography for 2312649--2312652.cif.' _cod_database_code 2312652 _cod_database_fobs_code 2312652 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.288 _shelx_estimated_absorpt_t_max 0.608 _shelx_hkl_file ; 0 0 -1 446.547 42.7856 28 0 0 -2 70471.3 890.656 28 0 0 -3 60493.9 962.294 28 0 0 -4 31691.3 770.549 28 0 0 -5 31803.8 873.319 28 0 0 -6 4510.96 367.274 28 0 0 -7 49651.6 1350.46 28 0 0 -8 92417.2 1886.70 26 0 0 -9 5502.49 470.010 26 0 0 10 762.337 219.347 25 0 0 10 785.024 114.948 22 0 0 11 165.011 67.3406 6 0 0 11 70.6228 36.2898 3 0 0 11 101.061 46.6558 22 0 0 11 215.277 135.358 25 0 0 12-31.1226 68.1583 22 0 0 12-5.12881 41.9094 3 0 0 12-33.6812 48.7456 6 0 0 13 1871.61 197.577 22 0 0 13 1810.87 178.400 3 0 0 13 1838.46 185.035 6 0 0 14 176.288 59.2204 3 0 0 14 140.334 68.6747 22 0 0 14 41.7090 51.8868 6 0 0 15 11724.0 400.529 6 0 0 15 12560.5 407.352 3 0 0 15 12257.9 472.372 22 0 0 16-2.70057 35.9547 19 0 0 16 49.4873 30.4029 3 0 0 16 53.5234 35.4830 6 0 0 16-37.1968 45.5188 24 0 0 17 830.885 81.8950 24 0 0 17 991.328 86.1474 19 0 -1 17 4293.70 163.814 24 0 -1 16 415.953 75.6908 24 0 -1 16 457.628 73.6094 19 0 -1 16 313.334 56.3257 6 0 -1 15 1126.41 113.671 3 0 -1 15 1109.45 128.308 6 0 -1 14 4266.80 293.924 22 0 -1 14 4600.38 277.477 6 0 -1 14 3974.94 239.520 3 0 -1 13 9091.93 382.194 3 0 -1 13 9471.27 451.518 22 0 -1 13 10023.7 440.333 6 0 -1 12 2010.87 211.740 22 0 -1 12 1810.88 180.212 3 0 -1 12 1826.50 194.849 6 0 -1 11 3437.01 255.217 6 0 -1 11 3390.55 234.862 3 0 -1 11 3495.79 261.480 22 0 1 -10 16096.0 958.047 26 0 -1 10 17169.2 509.352 3 0 -1 10 17123.9 546.783 6 0 -1 10 16592.5 536.344 22 0 1 -9 5954.05 546.749 26 0 1 -8 4058.29 422.137 26 0 1 -7 187.642 125.944 28 0 1 -6 56381.2 1465.53 28 0 1 -5 32953.6 1007.98 28 0 1 -4 7146.00 423.765 28 0 1 -3 537.108 112.897 28 0 1 -2 349716. 3174.77 28 0 1 -1 8963.39 293.310 28 0 1 -1 8932.29 287.313 27 0 1 0 1804.48 96.8511 28 0 1 0 1610.11 103.411 27 0 1 1 334.787 49.8702 25 0 1 2 35784.6 423.248 28 0 1 2 35246.9 581.450 25 0 -1 -2 35380.3 414.249 28 0 1 3 2931.45 187.538 25 0 -1 -3 3092.18 155.855 28 0 -1 -4 41.2431 35.8088 28 0 -1 -5 27692.7 716.622 28 0 -1 -6 1278.55 176.541 28 0 -1 -7 1002.39 151.545 26 0 -1 -7 807.369 166.708 28 0 -1 -8 21465.5 746.520 26 0 1 8 20916.4 901.112 25 0 1 9 9824.72 669.969 25 0 1 10 893.852 210.574 25 0 1 11 2839.24 226.129 22 0 1 11 2489.00 187.671 2 0 1 11 2598.20 397.888 25 0 1 11 2918.11 215.996 6 0 1 11 2545.91 210.196 3 0 1 12 3003.12 243.697 22 0 1 12 2979.02 234.954 3 0 1 12 2829.87 211.969 2 0 1 12 2987.09 221.842 6 0 1 13 1187.69 139.516 6 0 1 13 1383.59 166.751 22 0 1 13 1294.91 155.576 3 0 1 14 8637.24 411.437 22 0 1 14 7465.71 335.825 6 0 1 14 7756.12 363.967 3 0 1 15 2605.72 197.580 3 0 1 15 2703.49 224.512 22 0 1 16-9.14955 31.1583 3 0 1 16 49.5884 41.8146 19 0 1 17 62.1046 31.9417 19 0 1 17 53.4037 32.7408 24 0 1 17 33.4456 24.3193 3 0 -2 16 2069.43 137.390 24 0 -2 16 1948.48 128.883 19 0 -2 16 1940.78 126.299 6 0 -2 15 3142.78 211.155 24 0 -2 15 3031.28 197.762 6 0 -2 14 0.24538 31.1475 3 0 -2 14-17.9108 53.0063 6 0 -2 13 18.3937 62.2542 6 0 -2 13 55.4001 37.4451 3 0 -2 13-57.1966 82.8304 22 0 -2 12 1742.44 170.065 3 0 -2 12 1791.99 208.817 22 0 -2 12 1910.72 196.853 6 0 -2 11 6174.65 311.267 3 0 -2 11 6810.05 366.827 6 0 -2 11 6444.91 364.064 22 0 -2 10 14568.2 522.386 22 0 -2 10 14993.1 479.058 3 0 -2 10 15091.7 531.469 6 0 2 -10 15049.8 1012.14 26 0 2 -9 4062.37 498.350 26 0 2 -8 2434.42 355.875 26 0 2 -7 10710.2 697.991 26 0 2 -6 30826.6 1174.22 28 0 2 -5 178.688 102.579 28 0 2 -4 28239.6 937.635 28 0 2 -3 117687. 1861.45 28 0 2 -2 4801.93 309.695 27 0 2 -2 4205.79 296.174 28 0 2 -1 5718.78 305.740 27 0 2 -1 5753.97 299.669 28 0 2 -1 5638.25 191.412 23 0 2 0 107660. 1282.32 28 0 2 0 104849. 1377.10 27 0 2 1 1517.17 134.767 27 0 2 1 1648.33 154.712 25 0 2 1 1675.09 113.767 26 0 -2 -2 20177.1 278.393 28 0 2 2 19508.3 308.434 26 0 2 2 20183.1 464.570 27 0 2 2 20132.3 528.966 25 0 2 3 83377.1 1157.73 25 0 -2 -3 68691.2 647.383 28 0 2 4 83808.7 1316.13 25 0 -2 -4 83351.8 908.351 28 0 -2 -5 15129.7 306.589 26 0 -2 -5 15779.2 415.606 28 0 2 5 15990.8 586.380 25 0 -2 -6 33267.5 741.516 28 0 -2 -6 35447.2 597.313 26 0 2 6 35528.4 975.560 25 0 2 7 7327.56 479.718 25 0 2 8 297.753 112.922 25 0 2 9 4481.06 429.363 23 0 2 9 4531.60 451.439 25 0 2 10 11090.4 698.447 23 0 2 10 11837.2 784.605 25 0 2 11 124.826 65.5208 22 0 2 11 57.5777 41.4237 2 0 2 11-47.9536 58.2137 25 0 2 12 11891.5 477.842 22 0 2 12 11059.2 413.680 2 0 2 13 3629.07 265.408 22 0 2 13 3545.00 260.077 3 0 2 13 3266.06 225.368 2 0 2 14 1034.92 138.555 3 0 2 14 1075.94 152.127 22 0 2 15 1237.74 146.579 19 0 2 15 1136.42 149.626 22 0 2 15 1187.76 135.624 3 0 2 16 1695.51 152.128 19 0 2 16 1695.39 141.393 3 0 2 16 1411.47 144.002 22 0 2 17 1712.67 114.141 3 0 2 17 1746.06 120.107 24 0 2 17 2034.23 132.601 19 0 -3 15 2399.97 160.228 24 0 -3 15 2465.86 164.602 6 0 -3 14 3160.48 187.067 4 0 -3 14 3520.33 228.751 6 0 -3 14 3548.23 226.186 24 0 -3 13 148.276 60.7751 6 0 -3 12 2986.13 210.141 3 0 -3 12 3323.17 261.841 6 0 -3 11 7.55066 56.4392 6 0 -3 11 45.6602 56.0747 22 0 -3 11 97.4241 47.8874 3 0 -3 10 2335.80 221.955 22 0 -3 10 2258.05 189.403 3 0 -3 10 2831.24 236.025 6 0 3 -10 2269.93 428.620 26 0 -3 9 41948.9 915.927 22 0 3 -9 42555.9 1748.32 26 0 -3 9 40796.0 891.449 6 0 3 -8 137.923 111.498 26 0 3 -7 7689.00 651.473 26 0 3 -6 876.793 207.125 26 0 3 -5 30481.7 1126.97 26 0 3 -5 29958.0 1172.91 28 0 3 -4 83113.0 1860.69 28 0 3 -3 4132.13 361.468 28 0 3 -2 165502. 2364.59 27 0 3 -2 164296. 2323.06 28 0 3 -1 19281.1 682.695 27 0 3 -1 18866.5 466.454 23 0 3 0 22780.0 699.155 27 0 3 0 21216.9 624.392 26 0 3 1 13.9160 51.7026 26 0 3 1 16.0044 45.0931 27 0 3 2 46740.7 1027.18 25 0 3 2 44773.9 913.251 27 0 3 2 45471.3 717.236 26 0 3 3 368584. 3153.12 27 0 3 3 356581. 3486.09 25 0 3 4 76572.9 1368.94 25 0 3 4 77108.7 1181.02 27 0 3 5 51386.9 1157.23 25 0 3 6 1027.72 171.429 25 0 3 7 3674.00 344.310 25 0 3 8 8758.88 575.947 25 0 3 9 7677.46 579.171 25 0 3 10 365.386 145.259 25 0 3 10 368.968 136.763 23 0 3 11 36820.6 825.609 22 0 3 11 39290.9 1498.11 25 0 3 11 37618.7 776.237 2 0 3 12 24732.1 685.925 22 0 3 12 23964.4 620.909 2 0 3 13 39555.2 908.809 3 0 3 13 36489.0 923.224 19 0 3 13 37840.4 795.500 2 0 3 13 39310.1 888.366 22 0 3 14 103.617 54.4869 3 0 3 14 43.7660 49.3739 19 0 3 14 98.0464 46.9042 2 0 3 14 121.733 57.6095 22 0 3 15 1870.51 173.228 22 0 3 15 1829.43 176.340 19 0 3 15 1711.45 171.706 3 0 3 16 109.748 50.1420 24 0 3 16 116.237 56.8756 3 0 3 16 122.769 50.8118 19 0 3 16 55.6107 52.0743 22 0 3 17 439.703 61.2445 19 0 3 17 400.893 59.7657 3 0 -4 15 276.736 41.3563 19 0 -4 15 481.709 64.9622 6 0 -4 14 5028.21 249.996 6 0 -4 14 4635.27 219.301 24 0 -4 14 4498.18 206.723 4 0 -4 13 6026.15 294.562 24 0 -4 13 6228.54 294.933 4 0 -4 13 6999.68 334.670 6 0 -4 12-38.5021 49.1307 24 0 -4 12 137.020 75.0299 6 0 -4 11 22449.4 678.745 6 0 -4 10 11375.9 477.460 6 0 -4 9 15765.5 544.402 6 0 4 -9 15556.9 1116.60 26 0 -4 8 14158.7 493.699 6 0 4 -8 14244.5 1030.38 26 0 4 -8 15046.8 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344.503 19 0 4 12 5981.20 323.118 22 0 4 12 5955.05 305.983 2 0 4 13 184.562 66.1508 22 0 4 13 72.8687 41.9807 2 0 4 13 94.7025 64.8844 19 0 4 14 592.864 113.797 3 0 4 14 602.341 106.189 22 0 4 14 582.997 92.3823 2 0 4 14 711.239 117.688 19 0 4 15 1538.72 165.263 3 0 4 15 1490.78 153.285 19 0 4 15 1486.59 150.249 22 0 4 16 16677.6 443.114 22 0 4 16 17818.0 458.520 19 0 4 17 10579.0 292.029 3 0 -5 14 2197.65 120.985 4 0 -5 14 2560.96 150.078 6 0 -5 13 43.8818 34.3931 24 0 -5 13-24.2152 46.6072 6 0 -5 13-63.4818 43.2568 4 0 -5 12 300.126 70.5479 24 0 -5 12 333.040 85.9372 6 0 -5 12 386.878 86.0141 4 0 -5 11 724.413 109.158 24 0 -5 11 733.556 121.091 6 0 5 -11 684.060 103.174 10 0 -5 10 1399.25 158.278 24 0 -5 10 1667.52 181.027 6 0 5 -10 1277.33 147.981 10 0 5 -9 11696.7 425.146 20 0 -5 9 11570.9 468.671 6 0 -5 8 48617.1 973.172 6 0 5 -8 50689.0 2048.67 26 0 5 -8 45997.7 924.933 15 0 -5 7 37057.7 808.013 6 0 5 -7 36315.8 792.502 15 0 5 -7 37341.6 1684.87 26 0 5 -6 4998.41 575.166 26 0 5 -5 34785.9 1453.51 26 0 5 -4 3.67764 80.6170 26 0 5 -3 31539.4 1237.91 26 0 5 -2 21035.8 930.188 26 0 5 -1 1225.12 165.358 23 0 5 -1 1634.98 247.719 26 0 5 -1 1404.52 264.563 27 0 5 0 235.302 130.478 27 0 5 0 199.872 89.6975 23 0 5 0 278.258 112.819 26 0 5 1 29085.4 1026.16 27 0 5 1 27680.8 897.152 23 0 5 1 27268.2 864.013 26 0 5 2 70750.6 1572.18 23 0 5 2 69879.1 1325.97 26 0 5 3 6341.99 443.433 27 0 5 4 43353.5 1154.81 27 0 5 4 43299.4 1349.12 25 0 5 5 13779.2 627.073 27 0 5 5 14730.7 770.654 25 0 5 6 13866.0 753.351 25 0 5 7 20062.9 948.565 25 0 5 8 65324.9 1813.15 25 0 5 8 60255.8 1942.76 23 0 5 9 11567.4 881.426 23 0 5 9 13954.7 863.043 25 0 5 10 19265.5 570.914 19 0 5 10 19887.9 573.743 9 0 5 10 19366.3 558.943 1 0 5 11 16865.6 526.431 9 0 5 11 17188.0 555.309 19 0 5 11 17651.0 535.788 22 0 5 12 12030.8 447.551 22 0 5 12 11321.3 427.021 2 0 5 13 7838.99 354.650 22 0 5 13 7919.91 345.251 2 0 5 13 8302.01 379.197 19 0 5 14 1634.15 155.800 22 0 5 14 1465.75 138.001 2 0 5 14 1980.32 174.051 19 0 5 15 13861.4 380.313 2 0 5 15 14091.6 417.097 22 0 5 15 15784.9 487.661 3 0 5 15 15268.4 440.989 19 0 5 16-11.4609 40.7916 3 0 5 17 6205.30 208.240 3 0 -6 13 126.523 40.9875 6 0 -6 13 124.126 35.5918 4 0 -6 12 905.467 107.677 4 0 -6 12 844.568 102.673 6 0 -6 11 1107.05 131.267 6 0 6 -11 1044.50 114.705 10 0 -6 11 1246.66 147.328 4 0 -6 10 9464.53 394.998 6 0 6 -10 9655.71 376.856 10 0 6 -10 9433.78 352.815 20 0 -6 9 3566.49 249.281 6 0 6 -9 3587.18 234.410 20 0 6 -9 3736.02 248.752 10 0 6 -8 20481.5 611.526 15 0 6 -8 20467.9 589.997 20 0 -6 8 20476.8 606.112 6 0 6 -8 20382.0 602.886 10 0 6 -7 47102.1 946.597 15 0 6 -7 45400.5 911.228 20 0 6 -7 45010.4 926.665 10 0 -6 7 44528.0 904.899 6 0 -6 6 162.599 65.7695 6 0 6 -6 52.5834 47.4895 20 0 6 -6 113.753 122.793 26 0 6 -6 367.322 106.491 15 0 6 -6 194.576 73.0092 10 0 6 -5 2481.20 408.313 26 0 6 -5 2639.50 204.959 10 0 6 -5 2369.49 192.986 20 0 6 -5 2492.05 199.904 15 0 6 -4 4793.35 552.154 26 0 6 -3 222.838 102.821 26 0 6 -2 2609.58 367.510 26 0 6 -1 9465.18 721.877 27 0 6 -1 8954.02 644.777 26 0 6 0 24515.7 1106.26 27 0 6 0 24890.0 988.326 26 0 6 0 21702.8 823.310 23 0 6 1 5416.51 430.047 26 0 6 1 4347.41 395.365 23 0 6 1 5346.51 493.972 27 0 6 2 1715.38 275.900 27 0 6 2 1448.20 252.561 23 0 6 3 9559.96 639.251 23 0 6 3 10110.0 635.796 27 0 6 4 15196.5 851.962 23 0 6 4 17024.2 801.079 27 0 6 5 1964.37 264.814 27 0 6 5 1429.28 265.853 23 0 6 6 3400.66 429.585 23 0 6 7-54.0227 92.4728 25 0 6 7-160.387 145.837 23 0 6 8 800.947 115.450 9 0 6 8 834.248 131.066 16 0 6 8 910.707 120.692 1 0 6 8 841.933 249.591 23 0 6 9 23446.3 600.484 19 0 6 9 22489.7 616.222 1 0 6 9 21699.1 628.485 9 0 6 10 472.564 97.7185 19 0 6 10 564.416 211.664 23 0 6 10 574.620 103.044 9 0 6 10 582.005 103.806 1 0 6 11 2478.68 200.476 19 0 6 11 2358.66 205.156 9 0 6 12 7541.53 346.461 19 0 6 12 7400.84 344.670 9 0 6 13 6735.88 312.013 19 0 6 13 6454.81 303.159 2 0 6 14 6893.55 284.344 2 0 6 15 32.5747 41.2213 3 0 6 15 28.7195 18.8841 2 0 6 16 7843.30 229.199 13 0 6 16 8091.04 278.097 3 0 -7 12 1135.16 84.1503 6 0 -7 12 1238.24 100.797 4 0 -7 11 495.116 71.7913 6 0 -7 11 452.005 83.0221 4 0 7 -11 406.395 60.6537 10 0 7 -10 690.227 91.4276 10 0 7 -10 885.104 97.3370 20 0 -7 10 921.071 108.518 6 0 -7 10 790.457 109.232 4 0 7 -9 60.3863 47.4491 10 0 -7 9 40.9715 57.9715 4 0 -7 9 9.59113 44.0457 6 0 7 -9-30.6099 37.2717 20 0 7 -8 236.486 71.5466 10 0 -7 8 242.543 63.9369 6 0 7 -8 229.042 70.4206 20 0 7 -7 3313.67 248.450 10 0 -7 7 2819.28 209.695 6 0 7 -7 3165.25 239.953 15 0 7 -7 2998.77 230.137 20 0 7 -6 30106.2 766.906 10 0 7 -6 32476.5 778.962 15 0 7 -6 30784.2 760.974 20 0 7 -5 3474.50 253.861 10 0 7 -5 3667.31 257.094 20 0 7 -5 4031.60 279.426 15 0 7 -4 9794.35 405.384 15 0 7 -4 9051.35 820.159 26 0 7 -4 9269.43 396.746 20 0 7 -4 9302.03 403.805 10 0 7 -3 124.151 55.3329 20 0 7 -3 167.975 70.5441 10 0 7 -3 201.233 69.8392 15 0 7 -3 294.159 129.843 26 0 7 -2-14.7771 59.1804 20 0 7 -2 52.6059 42.2050 15 0 7 -2 55.9426 89.9670 26 0 7 -2 70.5417 45.7632 10 0 7 -1 29760.3 1280.14 26 0 7 0 3176.55 382.205 26 0 7 1 336.844 163.215 27 0 7 2 619.998 164.257 23 0 7 2 400.561 143.277 27 0 7 3 3001.39 389.420 23 0 7 3 3191.01 389.465 27 0 7 4 604.245 175.870 23 0 7 4 741.044 185.310 27 0 7 5 220.095 141.347 23 0 7 6 92.1416 46.2767 16 0 7 6 47.8603 98.4146 23 0 7 6 172.311 68.8998 8 0 7 6 115.185 52.2416 9 0 7 7 29403.4 715.921 8 0 7 7 29607.8 740.606 16 0 7 7 28956.8 734.062 9 0 7 8 1971.48 384.382 23 0 7 8 2679.32 237.147 16 0 7 8 2130.55 201.122 9 0 7 8 2124.31 196.476 1 0 7 8 2159.53 189.071 8 0 7 9 65.6980 94.8768 23 0 7 9 100.169 61.5165 9 0 7 9 66.3543 53.9109 1 0 7 10 2217.34 207.731 9 0 7 10 2300.11 197.275 1 0 7 11 14891.1 530.207 9 0 7 11 15846.7 520.185 1 0 7 12 15308.0 503.010 9 0 7 13 1726.89 148.539 2 0 7 13 1695.47 148.888 9 0 7 14 7465.60 273.133 13 0 7 14 7021.35 262.712 2 0 7 15 366.070 69.3857 3 0 7 15 466.467 60.4706 13 0 7 16 11.0995 21.5390 3 0 -8 11 3853.49 164.487 4 0 -8 10 3837.78 201.842 4 0 8 -9 406.127 75.9060 10 0 8 -9 482.893 75.2100 20 0 -8 9 458.888 87.2755 4 0 8 -8 8872.93 361.561 10 0 -8 8 9057.28 381.233 4 0 8 -8 8974.13 351.404 20 0 8 -7 4172.48 257.166 20 0 8 -7 4178.18 265.435 10 0 -8 7 4123.67 273.236 4 0 8 -6 12340.4 466.008 20 0 8 -6 13504.8 490.927 15 0 -8 6 12504.6 477.861 4 0 8 -6 13358.3 489.837 10 0 8 -5 524.780 118.241 15 0 -8 5 355.294 83.3333 4 0 8 -5 381.248 94.8573 20 0 8 -5 412.975 97.6801 10 0 8 -4 1.26710 50.6996 20 0 8 -4 50.8972 60.3288 15 0 -8 4-15.2084 41.4729 4 0 8 -4 15.8019 67.6274 10 0 8 -3 233.206 85.1886 15 0 8 -3 162.409 62.7299 20 0 8 -3 124.101 71.1222 10 0 -8 3 62.9508 52.9177 4 0 8 -2 413.633 98.6372 15 0 8 -2 364.743 81.3055 20 0 -8 2 372.436 69.3926 4 0 8 -2 392.502 100.524 10 0 8 -1 2085.01 192.706 20 0 8 -1 2171.19 201.845 10 0 8 -1 1982.06 176.908 15 0 8 0 8927.62 394.682 20 0 8 0 8600.56 354.288 15 0 8 0 8571.31 399.151 10 0 8 1 17003.0 541.956 20 0 8 1 18008.2 500.572 15 0 8 2 5660.62 302.512 20 0 8 2 5654.51 287.139 9 0 8 3 2939.23 217.540 9 0 8 3 3093.34 222.320 20 0 8 4 5304.12 300.747 9 0 8 4 5821.57 297.620 20 0 8 4 5696.43 293.919 16 0 8 4 5134.82 307.712 8 0 8 5 2193.81 202.445 8 0 8 5 2128.61 184.617 16 0 8 5 2142.61 372.133 23 0 8 5 2463.92 211.329 9 0 8 6 49869.1 979.913 16 0 8 6 51615.3 1020.07 9 0 8 7 521.287 108.685 9 0 8 7 529.947 116.407 16 0 8 7 369.351 91.3999 8 0 8 7 406.799 191.541 23 0 8 8 12569.9 475.906 8 0 8 8 13479.5 519.894 9 0 8 8 13082.9 491.144 1 0 8 9 4063.04 264.976 1 0 8 9 4058.01 285.373 9 0 8 10 1137.63 142.528 1 0 8 10 1218.75 156.651 9 0 8 11 17136.1 515.208 1 0 8 11 16522.8 548.062 9 0 8 12 4369.04 277.341 9 0 8 13 14558.8 396.458 2 0 8 13 16163.3 452.482 9 0 8 14 977.268 82.9916 2 0 8 15 2423.73 136.035 3 0 9 -10 96.7967 25.1655 21 0 -9 9 19530.5 408.426 4 0 -9 8 253.440 57.6951 4 0 9 -8 252.535 59.2534 20 0 9 -7 354.608 72.7460 20 0 9 -7 178.616 62.6252 10 0 -9 7 336.563 73.2734 4 0 9 -6 2451.96 194.078 10 0 -9 6 2367.08 184.938 4 0 9 -6 2258.82 186.630 20 0 9 -5 7942.55 365.699 20 0 9 -5 8245.48 364.720 15 0 9 -5 8505.74 381.615 10 0 -9 5 7300.50 338.278 4 0 9 -4 2957.62 232.998 20 0 9 -4 3070.55 243.403 10 0 -9 4 3012.66 216.068 4 0 9 -4 3297.43 236.522 15 0 9 -3 5132.60 298.910 15 0 9 -3 5293.16 317.979 10 0 -9 3 4540.01 266.988 4 0 9 -3 5084.24 308.949 20 0 9 -2 11482.0 475.507 10 0 9 -2 11151.3 431.619 15 0 9 -2 11303.1 457.612 20 0 9 -1 22104.4 646.386 20 0 9 -1 20684.5 582.036 15 0 9 0 609.097 102.994 15 0 9 0 721.376 122.429 20 0 9 0 713.366 112.891 21 0 9 1 149.286 59.9400 20 0 9 1 83.6641 54.9579 21 0 9 1 154.139 58.9440 15 0 9 2 4770.12 294.262 20 0 9 2 5412.59 299.782 21 0 9 3-43.6727 45.1817 9 0 9 3 93.1606 46.8784 20 0 9 4 18841.3 620.137 8 0 9 4 18470.1 574.112 9 0 9 5 8574.09 394.865 9 0 9 5 8313.46 397.463 8 0 9 5 7878.43 357.512 16 0 9 6 30524.2 762.276 8 0 9 6 32120.3 794.402 9 0 9 7 1278.19 160.513 8 0 9 7 1412.89 171.708 9 0 9 8 6395.47 351.648 9 0 9 8 5964.18 328.582 1 0 9 8 5614.75 311.124 8 0 9 9 7678.47 380.756 9 0 9 9 7175.50 343.820 1 0 9 10 1985.26 191.548 9 0 9 10 2011.51 170.860 1 0 9 11 6935.84 298.034 1 0 9 11 7222.77 336.620 9 0 9 12 1539.13 145.607 9 0 9 13 670.602 73.5312 14 0 9 13 666.434 69.8185 2 0 9 13 855.807 95.9223 9 0 9 14 318.879 55.5400 3 0 10 -8 3496.79 145.502 21 0 10 -7 3972.53 186.758 21 0 10 -7 3769.05 173.383 20 0 10 -6 432.653 73.9496 20 0 10 -6 436.312 74.4905 21 0 10 -5 6210.68 280.772 20 0 10 -5 6231.95 280.932 21 0 10 -4 13691.5 441.545 21 0 10 -4 14135.5 457.848 20 0 10 -3 658.656 109.115 20 0 10 -3 745.071 109.425 21 0 10 -3 751.896 106.741 15 0 10 -2 10497.3 402.866 21 0 10 -2 10311.4 386.236 15 0 10 -2 10697.9 422.192 20 0 10 -1 4205.25 267.192 20 0 10 -1 4303.71 248.086 15 0 10 -1 4165.11 257.383 21 0 10 0 384.284 83.2726 21 0 10 0 337.288 84.6868 20 0 10 0 327.029 74.3320 15 0 10 1 423.752 86.5845 15 0 10 1 437.779 103.891 20 0 10 1 477.024 91.7388 21 0 10 2 2841.38 258.963 8 0 10 2 2250.18 198.799 20 0 10 3 17136.3 516.042 9 0 10 3 19580.2 617.768 8 0 10 4 36633.4 839.787 8 0 10 4 35727.9 779.494 9 0 10 5 44.2620 58.0240 8 0 10 5 101.379 55.0419 9 0 10 6 2543.36 209.441 8 0 10 6 2866.96 222.250 9 0 10 7 121.159 79.3277 9 0 10 7 121.858 50.9332 8 0 10 8 281.711 71.2996 8 0 10 8 203.331 68.1448 1 0 10 8 424.755 97.5580 9 0 10 9 4968.21 257.615 1 0 10 9 5058.16 288.403 9 0 10 10 19805.9 489.130 1 0 10 10 22402.1 579.793 9 0 10 11 1302.16 129.956 9 0 10 12 1559.63 97.0151 2 0 10 12 1842.36 135.298 9 0 11 -5 7922.18 244.954 8 0 11 -5 7664.76 228.807 21 0 11 -4 2495.16 145.172 21 0 11 -3 1963.57 137.192 21 0 11 -3 2176.80 155.294 20 0 11 -2 414.920 71.6271 21 0 11 -2 333.899 69.8159 20 0 11 -1 141.770 51.3399 21 0 11 -1 268.877 83.4681 8 0 11 0 5536.02 247.377 21 0 11 0 6452.86 309.510 8 0 11 1 10564.5 405.897 8 0 11 2 12072.2 436.363 8 0 11 3 282.196 90.5360 8 0 11 4 3329.05 198.085 9 0 11 4 3902.87 240.029 8 0 11 5 102.525 44.6456 9 0 11 5 145.290 59.8766 8 0 11 6 1694.46 152.260 8 0 11 6 1560.09 144.014 9 0 11 7 2665.20 178.835 8 0 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9 169.209 51.9162 9 -1 11 9 116.784 38.9248 1 -1 11 8 205.798 51.9735 9 -1 11 8 208.886 51.9411 1 -1 11 7 2117.48 158.565 1 -1 11 7 1922.04 150.183 9 -1 11 6 11004.8 368.819 1 -1 11 6 9926.49 339.811 9 -1 11 5 4978.43 237.202 9 -1 11 5 5090.55 236.646 8 -1 11 4 8629.52 300.803 9 -1 11 4 9006.67 329.951 8 -1 11 3 5742.80 274.336 8 -1 11 2 10116.3 359.892 8 -1 11 2 8838.02 306.945 21 -1 11 1 334.863 65.1233 21 -1 11 1 455.537 87.6780 8 -1 11 0 163.643 51.6087 21 -1 11 0 52.5307 49.4947 8 -1 11 -1 52.1372 29.3963 21 -1 11 -1 190.298 67.9638 8 -1 11 -2 23.2835 29.4787 21 -1 11 -3 9409.55 293.984 21 -1 11 -4 5.55657 24.7605 21 -1 11 -5 700.117 62.3029 21 -1 11 -5 692.210 65.1404 8 -1 10 12 3698.26 151.255 2 -1 10 12 3946.90 178.720 9 -1 10 11 4804.06 228.624 9 -1 10 10 2082.92 155.697 1 -1 10 10 2098.66 165.738 9 -1 10 9 2046.84 163.701 1 -1 10 9 1899.78 170.836 9 -1 10 8 152.197 66.8214 9 -1 10 8 176.924 62.9884 1 -1 10 7 2087.98 186.162 1 -1 10 7 1897.57 179.511 9 -1 10 7 1720.52 146.600 8 -1 10 6 2316.72 194.553 9 -1 10 6 2041.86 170.499 8 -1 10 5 31776.0 716.402 8 -1 10 5 33192.0 749.493 9 -1 10 4 720.010 110.766 9 -1 10 4 702.520 115.901 8 -1 10 3 14712.4 459.314 9 -1 10 3 14981.3 504.075 8 -1 10 3 15815.4 490.552 21 -1 10 2 257.622 123.963 8 -1 10 2 20.3229 44.4873 21 -1 10 1 107.035 40.8968 21 -1 10 0 6047.59 310.905 21 -1 10 -1 1388.01 153.651 21 -1 10 -1 1396.04 155.988 20 -1 10 -2 17615.1 533.395 20 -1 10 -2 17274.7 522.428 21 -1 10 -3 712.815 109.736 21 -1 10 -3 843.507 118.628 20 -1 10 -4 9225.81 352.325 21 -1 10 -4 9445.64 349.060 20 -1 10 -5 494.520 82.9026 21 -1 10 -6 759.072 91.4209 21 -1 10 -7 372.576 56.2328 21 -1 9 14 1955.97 114.538 3 -1 9 13 2156.63 133.385 9 -1 9 13 2213.61 128.613 2 -1 9 12 1232.58 126.089 9 -1 9 11 4254.58 244.712 1 -1 9 11 4711.11 283.739 9 -1 9 10 323.319 89.2361 9 -1 9 10 403.029 85.4934 1 -1 9 9 281.432 85.1800 9 -1 9 9 393.092 95.9738 1 -1 9 8 7428.55 373.199 9 -1 9 8 7391.38 368.494 1 -1 9 7 9526.62 382.364 8 -1 9 7 10087.0 438.694 9 -1 9 6 92.8727 53.8790 8 -1 9 6 75.8582 58.7477 9 -1 9 5 6758.03 356.155 9 -1 9 5 6528.23 342.274 8 -1 9 4 8441.75 373.307 21 -1 9 4 7616.59 366.500 9 -1 9 4 7971.88 380.296 8 -1 9 3-18.7855 45.1454 9 -1 9 3 5.60527 47.6541 21 -1 9 2 2403.27 191.875 9 -1 9 2 2316.01 204.902 21 -1 9 1 9070.67 350.609 15 -1 9 1 8795.27 405.221 21 -1 9 1 9128.91 412.497 20 -1 9 0 7886.88 341.503 15 -1 9 0 8947.87 407.432 20 -1 9 0 8699.77 403.290 21 -1 9 -1 10390.2 439.997 21 -1 9 -1 9598.32 382.042 15 -1 9 -1 10670.2 444.556 20 -1 9 -1 9918.14 437.950 10 -1 9 -2 724.290 123.627 10 -1 9 -2 814.415 118.074 15 -1 9 -2 888.248 133.894 20 -1 9 -2 848.720 127.851 21 1 -9 3 3372.25 227.876 4 -1 9 -3 3512.87 252.114 20 -1 9 -3 3427.57 255.058 10 -1 9 -4 9394.37 410.674 10 -1 9 -4 8653.76 383.742 20 1 -9 4 8116.26 356.153 4 -1 9 -5 10510.2 427.230 10 -1 9 -5 10135.1 395.004 20 1 -9 5 9431.16 376.776 4 1 -9 6 344.348 75.1568 4 -1 9 -6 321.870 81.3250 10 -1 9 -6 334.412 74.0931 20 1 -9 7 9247.30 328.814 4 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916.558 20 -1 8 1 47691.2 842.385 15 -1 8 0 9586.16 422.917 10 -1 8 0 9202.11 366.888 15 -1 8 0 9496.63 424.561 21 -1 8 0 9347.64 413.484 20 -1 8 -1 45038.4 877.663 15 -1 8 -1 47130.5 966.645 20 -1 8 -1 45552.7 970.736 10 -1 8 -2 584.786 107.196 20 -1 8 -2 484.886 106.381 10 1 -8 2 602.169 104.400 4 -1 8 -2 638.792 117.578 15 -1 8 -3 1475.75 169.651 20 -1 8 -3 1484.38 177.806 10 -1 8 -3 1576.07 168.512 15 1 -8 3 1398.22 158.175 4 -1 8 -4 927.902 137.053 20 -1 8 -4 962.311 147.070 10 1 -8 4 950.572 141.217 4 -1 8 -4 1095.98 150.198 15 -1 8 -5 7115.78 364.222 10 -1 8 -5 6504.06 337.528 20 1 -8 5 6769.64 349.308 4 -1 8 -6 4728.54 278.124 20 -1 8 -6 5279.38 312.259 10 1 -8 6 4655.02 287.432 4 -1 8 -7 11249.6 407.164 20 1 -8 7 11927.9 445.539 4 -1 8 -8 569.929 82.9341 20 -1 8 -8 522.317 103.335 10 1 -8 8 394.559 85.4906 4 -1 8 -9 6822.19 279.351 10 1 -8 9 6920.41 289.811 4 1 -8 10 1247.18 107.187 4 -1 8 -10 1085.37 99.1733 10 -1 7 16 20.8178 17.7385 3 -1 7 15 99.9560 39.6009 3 -1 7 15 165.272 38.0056 2 -1 7 14 3110.50 181.144 2 -1 7 13 149.328 51.0554 9 -1 7 13 150.794 55.0684 2 -1 7 12 161.308 62.8679 9 -1 7 11 2671.14 219.342 1 -1 7 11 2789.86 222.887 9 -1 7 10 3687.56 265.552 9 -1 7 10 3912.71 268.309 1 -1 7 9 2795.11 235.590 1 -1 7 9 3089.01 243.730 9 -1 7 8 5655.28 329.212 9 -1 7 8 5322.87 316.571 1 -1 7 8 4729.65 601.862 23 -1 7 7 14040.7 510.791 9 -1 7 7 13021.6 988.097 23 -1 7 6-56.6407 59.8601 8 -1 7 6-79.2798 85.1226 23 -1 7 6 37.4812 50.3928 9 -1 7 5 4257.50 510.980 23 -1 7 5 5491.42 542.212 27 -1 7 5 4936.02 284.958 9 -1 7 4 1926.59 332.985 27 -1 7 4 1576.03 302.020 23 -1 7 3 12254.6 799.937 23 -1 7 3 15140.2 937.419 27 -1 7 2 28407.5 1157.38 23 -1 7 2 31217.6 1388.07 27 -1 7 1 13799.8 940.642 27 -1 7 0 86099.2 1304.66 10 -1 7 0 88461.2 1305.61 20 -1 7 0 89663.0 2509.85 27 -1 7 -1 19585.2 1196.71 27 -1 7 -1 17895.8 554.332 10 -1 7 -1 20650.2 1060.53 26 -1 7 -1 18491.0 559.843 20 -1 7 -1 19390.2 530.771 15 -1 7 -2 3560.53 462.266 26 -1 7 -2 3340.33 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6064.04 293.299 9 -2 10 5 5859.11 275.502 21 -2 10 4-23.6756 51.1576 9 -2 10 4 115.211 53.6619 8 -2 10 4 20.8961 38.3577 21 -2 10 3 1876.80 155.007 9 -2 10 3 2003.24 162.247 8 -2 10 3 2231.22 181.272 21 -2 10 2 293.889 75.6438 21 -2 10 2 392.615 82.8246 8 -2 10 1 2977.42 213.255 21 -2 10 0 5653.03 294.923 21 -2 10 -1 380.925 82.7190 21 -2 10 -2 14333.3 456.804 21 -2 10 -3 20.7645 41.7987 21 -2 10 -4 1388.18 131.432 21 -2 10 -5 22.5173 34.6423 21 -2 10 -6 7082.98 234.914 21 -2 9 13 12910.4 292.115 2 -2 9 12 174.428 51.8539 9 -2 9 11 2597.79 181.283 9 -2 9 10 7261.56 315.289 1 -2 9 10 7437.30 327.869 9 -2 9 9 747.227 118.766 9 -2 9 9 677.230 106.756 1 -2 9 8 12781.5 473.320 9 -2 9 8 12607.6 462.774 1 -2 9 7 15309.9 529.499 9 -2 9 7 14684.5 526.756 1 -2 9 6 4500.88 266.816 21 -2 9 6 4988.21 300.239 9 -2 9 5 3355.43 243.835 9 -2 9 5 3264.57 237.225 21 -2 9 4-23.9294 50.2678 21 -2 9 4-30.4269 54.3366 9 -2 9 4-1.99695 49.2506 8 -2 9 3-44.4747 54.1010 9 -2 9 3 123.997 62.4479 21 -2 9 3 52.7373 47.5692 8 -2 9 2 5273.49 311.461 21 -2 9 2 4394.03 255.609 9 -2 9 1 3271.79 248.889 21 -2 9 0 32051.3 802.371 21 -2 9 -1 374.269 98.2779 21 -2 9 -2 4930.32 292.709 10 -2 9 -2 5304.05 315.656 21 -2 9 -3 159.069 76.6884 10 -2 9 -3 276.504 82.1633 21 -2 9 -4 214.629 81.5685 21 -2 9 -4 6.69564 71.3574 10 -2 9 -5 2940.76 216.130 21 -2 9 -5 3360.95 225.826 10 -2 9 -6 181.910 61.3600 21 -2 9 -6 161.501 66.3274 10 -2 9 -7 3511.46 193.275 10 -2 9 -7 3732.44 202.087 21 -2 9 -8 1142.41 97.3413 21 -2 8 14 18.8710 19.8720 2 -2 8 13 113.080 44.3595 2 -2 8 13-42.5800 26.1738 9 -2 8 12 193.525 62.5002 9 -2 8 11 1766.02 165.637 1 -2 8 11 1653.33 161.100 9 -2 8 10 9568.35 399.082 1 -2 8 10 9224.29 402.461 9 -2 8 9 143.440 85.1111 9 -2 8 9 173.316 98.6700 1 -2 8 8 691.635 130.424 1 -2 8 8 476.434 112.113 9 -2 8 7 7780.45 393.482 9 -2 8 6 6055.29 341.009 9 -2 8 6 5683.27 320.417 21 -2 8 5 537.971 104.132 21 -2 8 5 407.944 94.7362 9 -2 8 4 10217.3 426.524 9 -2 8 4 10561.8 449.865 21 -2 8 4 10122.2 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52.6285 15 2 -7 2 3900.10 266.693 4 -2 7 -2 3803.10 263.174 10 -2 7 -2 3615.16 234.703 15 -2 7 -2 4686.59 622.740 27 -2 7 -2 3925.64 266.703 20 2 -7 3 9701.57 431.281 4 -2 7 -3 10019.4 423.627 20 -2 7 -3 9418.62 414.790 10 2 -7 4 36970.8 869.198 4 -2 7 -4 36618.7 835.284 20 -2 7 -4 36382.3 852.148 10 2 -7 5 5220.30 320.222 4 -2 7 -5 4856.32 308.062 10 -2 7 -5 5021.70 298.582 20 -2 7 -6 377.929 89.0668 20 2 -7 6 279.615 78.5649 4 -2 7 -6 311.242 85.8377 10 2 -7 7 40175.5 885.772 4 -2 7 -7 42157.7 880.399 10 2 -7 7 37977.2 775.965 6 -2 7 -7 36495.1 772.531 20 2 -7 8 687.510 98.8692 6 2 -7 8 722.486 120.526 4 -2 7 -8 766.117 97.8969 20 -2 7 -8 694.595 115.552 10 2 -7 9 4432.14 258.253 4 -2 7 -9 4425.99 251.374 10 2 -7 10 763.063 100.427 4 -2 7 -10 962.790 110.021 10 -2 7 -11 890.964 80.8254 21 -2 7 -11 980.053 92.1186 10 -2 6 16 58.3925 24.7008 3 -2 6 15 97.6865 37.7133 2 -2 6 15 90.2811 31.2204 22 -2 6 15 155.150 53.7685 3 -2 6 14 703.254 89.2658 22 -2 6 14 699.586 92.6330 2 -2 6 13 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138.222 101.199 26 -2 6 -5 42599.6 877.409 20 2 -6 5 46029.5 900.120 6 -2 6 -5 44178.8 1834.97 26 2 -6 5 42679.8 942.036 4 2 -6 6 9982.70 413.312 6 2 -6 6 10057.4 453.823 4 -2 6 -6 9971.71 406.468 20 2 -6 7 1236.40 161.429 4 2 -6 7 1199.11 148.036 6 -2 6 -7 1042.00 127.522 20 2 -6 8 1129.12 142.979 6 2 -6 8 1348.46 168.159 4 2 -6 9 3591.54 255.018 4 -2 6 -9 3374.48 249.732 10 2 -6 9 3232.93 231.774 6 2 -6 10 6679.63 324.151 4 2 -6 10 6841.49 314.632 6 -2 6 -10 6779.85 320.415 10 2 -6 11 124.611 56.9919 4 2 -6 11 164.276 50.2779 6 -2 6 -11 206.625 63.9088 10 -2 6 -12 87.7558 40.4347 10 -2 6 -12 106.137 31.0581 21 -2 5 16 139.462 48.1159 22 -2 5 16 276.455 52.3528 3 -2 5 15 422.145 93.8622 3 -2 5 15 512.123 82.0887 22 -2 5 15 257.983 57.9546 2 -2 5 14 1973.73 169.071 2 -2 5 14 2006.78 168.695 22 -2 5 13 656.415 107.556 2 -2 5 13 843.917 124.408 22 -2 5 12 163.698 54.0003 22 -2 5 11 1207.83 143.668 9 -2 5 11 1192.10 142.109 7 -2 5 10 112.179 63.1043 1 -2 5 10 75.0702 57.2300 9 -2 5 10 47.0115 37.4361 7 -2 5 9 127.693 50.3767 9 -2 5 9 147.456 70.0969 1 -2 5 9 129.699 117.883 25 -2 5 9 7.60322 62.7658 11 -2 5 8 11031.7 430.501 1 -2 5 8 11909.4 911.982 25 -2 5 8 11902.6 443.248 11 -2 5 7 214.152 129.338 25 -2 5 7 217.971 142.679 27 -2 5 6 23466.7 1195.42 25 -2 5 6 22657.6 1031.97 27 -2 5 5 2400.83 333.634 27 -2 5 5 1998.59 348.342 25 -2 5 4 153.249 106.605 27 -2 5 4 131.422 119.810 25 -2 5 3 81.3404 106.123 27 -2 5 2 1172.21 250.298 27 -2 5 1 16028.3 900.940 27 -2 5 0 8515.75 676.469 27 -2 5 0 9185.09 554.672 28 -2 5 -1 98292.1 2101.13 28 -2 5 -1 102598. 2464.62 27 -2 5 -2 72196.9 2096.09 27 -2 5 -2 69597.6 1876.25 28 -2 5 -3 31885.4 1420.50 27 -2 5 -3 31237.6 1323.93 28 -2 5 -4 11309.6 839.087 28 -2 5 -4 10802.2 857.832 27 2 -5 5 936.166 128.537 4 -2 5 -5 965.478 257.208 28 -2 5 -6 955.913 114.271 20 2 -5 6 884.830 135.565 4 2 -5 6 799.170 116.856 6 -2 5 -6 647.629 235.365 28 2 -5 7 1133.72 146.705 6 2 -5 7 880.865 137.958 4 -2 5 -7 746.113 246.983 26 2 -5 7 944.015 132.143 24 -2 5 -7 1008.74 121.534 20 2 -5 8 6613.04 355.802 6 2 -5 8 6966.37 374.147 4 2 -5 8 6397.69 335.266 24 2 -5 9 1270.49 151.732 24 2 -5 9 1366.12 171.919 4 2 -5 9 1463.28 172.934 6 2 -5 10 5439.28 315.593 4 2 -5 10 5411.64 312.485 6 2 -5 10 4922.51 281.010 24 2 -5 11 1633.97 160.544 4 2 -5 11 1613.75 151.758 24 2 -5 11 1718.04 169.790 6 2 -5 12 7720.14 303.755 4 -2 5 -12 7910.27 311.413 10 2 -5 12 8069.74 330.225 6 2 -5 13 369.158 67.3297 6 -2 5 -13 263.208 50.2267 10 -2 4 16 679.611 85.8397 22 -2 4 16 549.552 68.5608 3 -2 4 15 206.653 62.6625 3 -2 4 15 143.479 67.0057 22 -2 4 14 6906.03 287.274 19 -2 4 14 7498.21 332.308 2 -2 4 14 7773.00 357.330 22 -2 4 13 22888.4 638.205 2 -2 4 13 21836.2 566.723 19 -2 4 12 26001.3 725.902 22 -2 4 12 25899.7 700.383 2 -2 4 12 25590.7 632.550 19 -2 4 12 25536.2 709.325 7 -2 4 11 5815.55 326.454 7 -2 4 10 3405.86 507.007 25 -2 4 10 3301.12 243.350 1 -2 4 10 3152.04 236.184 7 -2 4 9 4764.37 287.549 11 -2 4 9 6177.03 303.244 9 -2 4 9 5197.61 293.490 1 -2 4 9 5446.11 603.904 25 -2 4 9 5386.81 292.163 7 -2 4 8 483.153 168.318 25 -2 4 7 22773.6 1128.85 25 -2 4 6 1501.61 294.124 25 -2 4 5 76265.7 1988.37 25 -2 4 4 19318.1 954.697 25 -2 4 4 19481.6 861.342 27 -2 4 3 66274.9 1629.15 27 -2 4 3 65752.6 1811.47 25 -2 4 2 1180.23 224.043 27 -2 4 2 1518.50 289.677 25 -2 4 1 17321.7 825.571 27 -2 4 1 15757.1 594.276 28 -2 4 0 121646. 2344.19 27 -2 4 0 108919. 1902.97 28 -2 4 -1 18286.1 795.092 28 -2 4 -1 19470.0 932.399 27 -2 4 -2 94157.8 2031.43 28 -2 4 -2 94504.1 2192.45 27 -2 4 -3 18384.7 966.937 27 -2 4 -3 18603.4 938.393 28 -2 4 -4 2718.59 382.486 28 -2 4 -4 2598.99 382.859 27 -2 4 -5 123.862 84.8423 28 -2 4 -6 10788.9 884.155 28 2 -4 7 4588.40 281.484 6 2 -4 7 4539.75 283.710 4 -2 4 -7 4880.23 627.427 28 2 -4 7 4809.53 286.297 24 2 -4 8 28058.7 739.145 6 2 -4 8 28053.8 745.450 4 -2 4 -8 27397.9 1562.41 28 2 -4 8 27050.1 725.268 24 2 -4 9 4401.38 296.192 6 2 -4 9 4169.33 285.060 4 2 -4 9 3935.05 276.257 24 2 -4 10-14.8957 54.6455 4 2 -4 10-69.0836 67.9883 6 2 -4 10-34.6091 63.5546 24 2 -4 11 1.18625 46.8104 4 2 -4 11 5.99183 59.0876 6 2 -4 11 7.12844 48.3330 24 2 -4 12-9.74135 35.2793 4 2 -4 12-17.7409 54.2870 6 2 -4 12 41.8939 47.8179 24 2 -4 13 5146.40 230.534 4 2 -4 13 5296.73 257.002 24 2 -4 14 26.4918 16.8732 18 -2 4 -14 53.8160 31.0342 10 -2 3 17 422.358 56.0274 22 -2 3 16 172.183 43.9438 3 -2 3 16 122.228 34.9458 19 -2 3 16 185.823 57.7942 22 -2 3 15 4980.66 271.728 22 -2 3 15 4468.48 223.622 19 -2 3 15 4599.81 238.799 3 -2 3 14-56.4117 68.4847 22 -2 3 14-43.6373 43.1377 19 -2 3 14 48.0683 47.5336 3 -2 3 14-5.92551 48.1732 2 -2 3 13 3801.42 260.645 2 -2 3 13 3309.41 241.878 19 -2 3 13 3702.27 278.345 22 -2 3 12 156.410 71.0693 2 -2 3 12 62.1608 62.1188 22 -2 3 12 78.7052 63.1357 7 -2 3 11 433.589 93.9707 2 -2 3 11 473.099 110.051 22 -2 3 11 513.675 104.448 7 -2 3 10 6352.46 334.747 7 -2 3 10 6159.09 641.261 25 -2 3 9 1781.26 178.909 11 -2 3 9 1588.62 303.558 25 -2 3 9 1920.09 170.962 1 -2 3 8-42.9256 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2 7 8 182.986 68.9102 16 2 7 8 27.7302 55.1539 8 2 7 8 107.125 39.3982 13 2 7 8 158.904 137.113 23 2 7 9 14766.0 549.006 16 2 7 9 14429.8 530.633 9 2 7 9 13676.0 1030.32 23 2 7 10 774.589 148.733 16 2 7 10 696.045 117.802 9 2 7 11 6871.33 357.228 9 2 7 12 1680.39 167.913 9 2 7 12 1587.08 162.468 14 2 7 13 5963.38 298.942 3 2 7 13 6268.92 292.954 14 2 7 14 1989.38 163.182 13 2 7 14 1737.57 148.834 3 2 7 15 2526.03 156.357 3 2 7 15 2896.56 172.172 13 2 7 16 129.991 30.7589 3 2 7 16 221.840 38.6704 13 -2 -8 11 1133.75 91.4405 4 -2 -8 10 10426.2 340.609 4 2 8 -10 9958.45 301.575 20 2 8 -9 7600.01 306.114 20 2 8 -8 9320.72 370.963 20 2 8 -8 8776.83 349.577 15 2 8 -7 1967.94 185.099 20 2 8 -7 1897.36 178.061 15 2 8 -6 773.630 141.231 15 2 8 -6 360.912 80.8111 20 2 8 -5 2722.45 214.492 10 2 8 -5 2672.57 217.268 15 2 8 -4 8834.16 389.484 10 2 8 -4 9691.24 417.926 15 2 8 -3 23480.7 656.963 15 2 8 -2 46970.3 934.361 15 2 8 -2 47120.3 1897.58 26 2 8 -1 84.3795 64.5688 20 2 8 -1 88.3398 46.4093 15 2 8 -1 80.3116 46.3562 16 2 8 -1 98.9608 108.101 26 2 8 0 6976.99 330.949 15 2 8 0 7528.80 347.088 16 2 8 0 7913.10 713.064 26 2 8 0 6844.61 329.942 20 2 8 1 11784.5 423.053 20 2 8 1 11658.4 438.886 16 2 8 1 11330.0 416.461 15 2 8 2 8204.70 372.411 16 2 8 2 8314.23 344.019 15 2 8 2 7908.77 367.316 13 2 8 3 1159.03 249.036 23 2 8 3 1323.65 150.753 9 2 8 3 1416.11 157.030 16 2 8 3 1401.38 136.365 15 2 8 3 1375.67 159.940 8 2 8 3 1272.62 145.541 13 2 8 4 8607.53 753.463 23 2 8 4 8979.95 391.346 9 2 8 4 8641.37 397.743 16 2 8 4 9147.57 409.970 8 2 8 4 9120.34 390.004 13 2 8 5 69339.8 1214.41 8 2 8 5 71264.4 1204.23 9 2 8 5 72263.5 1246.67 16 2 8 5 72803.3 1176.44 13 2 8 5 67708.7 2212.51 23 2 8 6 4363.15 284.910 9 2 8 6 4231.82 287.861 16 2 8 6 4144.38 287.624 8 2 8 6 4082.69 260.409 13 2 8 6 3673.75 525.695 23 2 8 7 29945.6 1533.21 23 2 8 7 32153.7 819.257 16 2 8 7 32976.4 822.122 9 2 8 7 32909.2 825.426 8 2 8 7 31743.6 759.426 13 2 8 8 36993.9 897.726 16 2 8 8 37216.8 879.237 9 2 8 8 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5437.70 305.144 15 2 9 -1 8201.11 379.533 20 2 9 -1 8266.18 373.407 15 2 9 0 7115.46 334.327 16 2 9 0 7546.32 356.777 20 2 9 0 7624.22 359.108 15 2 9 1 11937.8 447.552 20 2 9 1 11876.2 444.723 16 2 9 1 12176.0 441.019 15 2 9 2 4370.84 275.736 16 2 9 2 4422.98 260.821 15 2 9 2 4650.35 312.163 8 2 9 2 4219.61 256.992 20 2 9 3 10831.5 427.482 9 2 9 3 10792.5 446.392 16 2 9 3 10765.2 393.470 15 2 9 3 10918.9 428.918 13 2 9 3 11546.2 484.338 8 2 9 4 13574.5 497.057 9 2 9 4 13741.2 512.111 16 2 9 4 14622.4 537.282 8 2 9 4 13674.5 486.293 13 2 9 4 14767.4 1025.27 23 2 9 5 2961.23 236.348 16 2 9 5 2306.77 415.095 23 2 9 5 3090.50 262.517 8 2 9 5 2761.55 215.143 13 2 9 5 3190.42 242.097 9 2 9 6 54984.5 1009.84 13 2 9 6 56167.8 1083.76 9 2 9 6 56290.1 1094.47 16 2 9 6 54267.3 1110.03 8 2 9 7 32746.4 757.692 13 2 9 7 33920.9 838.151 9 2 9 7 33476.0 835.277 16 2 9 7 33468.1 845.516 8 2 9 8 196.001 71.3222 16 2 9 8 321.048 94.3345 9 2 9 8 223.514 106.435 8 2 9 8 351.719 83.3667 13 2 9 9 826.972 138.725 16 2 9 9 778.747 125.827 9 2 9 9 730.142 112.397 13 2 9 10 14287.5 462.498 13 2 9 10 13793.8 509.746 9 2 9 11 2741.57 191.921 13 2 9 11 2872.72 221.217 9 2 9 12 58.6345 38.7479 13 2 9 12-75.2557 66.8013 14 2 9 12 66.0832 49.2560 9 2 9 13 53.6373 32.9982 13 2 9 13-26.2279 42.8978 14 2 9 14 0.85821 20.5057 13 2 10 -8 527.939 58.4554 20 -2 -10 7 340.068 48.5408 4 2 10 -7 389.005 66.3858 20 -2 -10 6 14411.6 350.207 4 2 10 -6 16385.7 437.453 20 2 10 -6 16048.3 426.249 15 2 10 -6 13724.2 351.990 8 2 10 -5 434.570 85.8297 20 2 10 -5 475.326 90.2635 15 2 10 -4 4713.48 263.336 20 2 10 -4 4737.40 265.416 15 2 10 -3 4373.28 265.668 20 2 10 -3 4370.29 257.731 15 2 10 -2 7783.38 354.701 20 2 10 -2 7574.36 349.116 15 2 10 -1 488.226 98.3381 20 2 10 -1 363.627 85.0966 15 2 10 0 1712.51 166.947 20 2 10 0 1821.53 192.726 8 2 10 0 1625.42 160.522 15 2 10 1 6377.51 316.163 20 2 10 1 6100.70 294.482 16 2 10 1 6435.74 309.198 15 2 10 1 7147.41 372.499 8 2 10 2 573.862 100.137 20 2 10 2 458.244 82.4261 15 2 10 2 474.750 95.2145 16 2 10 2 518.331 122.012 8 2 10 3 4736.70 269.079 9 2 10 3 4983.43 285.315 16 2 10 3 4285.00 236.286 15 2 10 3 5422.90 329.771 8 2 10 4 223.500 95.3627 8 2 10 4 231.667 73.2470 16 2 10 4 273.029 76.5534 9 2 10 5 1647.75 184.396 8 2 10 5 1550.82 168.140 9 2 10 5 1596.76 166.375 16 2 10 6 1310.71 166.712 8 2 10 6 1269.20 155.679 9 2 10 6 1215.97 155.015 16 2 10 6 1229.25 138.363 13 2 10 7 4332.07 280.168 9 2 10 7 3927.16 263.020 16 2 10 7 4148.99 281.680 8 2 10 7 3727.83 230.955 13 2 10 8 880.294 134.510 16 2 10 8 705.693 103.357 13 2 10 8 775.033 124.825 9 2 10 8 691.365 123.563 8 2 10 9 1.00095 60.3882 9 2 10 9-29.7589 36.3556 13 2 10 10 112.276 50.1680 13 2 10 10 82.6323 56.0768 9 2 10 11 145.232 61.9858 9 2 10 11 169.878 46.1980 13 2 10 12 3908.43 171.234 13 2 10 12 3872.10 202.655 14 2 10 13 920.593 81.7835 14 2 11 -6 3184.34 142.626 20 2 11 -5 88.4363 36.0375 20 2 11 -5 68.2790 32.4110 8 2 11 -4 27489.0 545.650 20 2 11 -4 26788.8 531.465 15 2 11 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37.7757 8 2 12 0 5853.63 242.657 8 2 12 0 4636.55 190.283 15 2 12 1 1709.51 141.902 8 2 12 1 1307.34 98.5923 15 2 12 2 4464.69 228.404 8 2 12 3 1769.02 154.842 8 2 12 4 6037.24 271.112 8 2 12 4 4034.92 185.479 14 2 12 5 5699.88 259.587 8 2 12 5 4591.67 209.923 14 2 12 6 820.638 103.434 8 2 12 6 516.806 74.6691 14 2 12 7 5011.33 223.598 14 2 12 8 1432.31 120.876 14 2 12 9 10032.6 286.981 14 2 12 10-71.6144 32.7842 14 2 13 1 154.852 33.0754 8 2 13 2 2907.61 131.358 8 2 13 3 135.188 34.8056 8 2 13 4 2074.93 113.818 8 -3 11 7 665.015 62.9388 9 -3 11 7 722.131 69.4105 1 -3 11 6 2561.53 135.805 1 -3 11 6 2181.28 114.837 9 -3 11 5 20348.7 408.356 1 -3 11 5 17974.7 335.734 9 -3 11 4 1178.76 97.9349 1 -3 11 3 1537.06 111.013 1 -3 11 2 336.097 52.3226 21 -3 11 1 113.392 32.4092 21 -3 11 0 1400.53 98.7317 21 -3 11 -1 799.548 72.0675 21 -3 11 -2 22.5273 17.3440 21 -3 10 10 1192.76 98.8183 9 -3 10 9 9770.51 291.611 1 -3 10 9 9200.53 293.954 9 -3 10 8 512.177 75.7471 9 -3 10 8 658.380 86.3488 1 -3 10 7 23515.7 525.228 1 -3 10 7 21885.9 514.084 9 -3 10 6 35.4283 52.7885 1 -3 10 6 25.0711 37.1853 9 -3 10 5 1366.02 127.700 9 -3 10 5 1504.05 140.661 1 -3 10 4 1392.39 126.798 9 -3 10 4 1414.92 132.401 21 -3 10 3 2100.30 146.985 9 -3 10 3 2472.15 181.735 21 -3 10 2 17591.1 493.845 21 -3 10 1-55.3300 52.9969 21 -3 10 1 73.9203 35.4682 8 -3 10 0 5829.05 279.691 21 -3 10 0 5240.43 228.733 8 -3 10 -1 843.022 106.468 21 -3 10 -2 2207.97 160.977 21 -3 10 -3 1337.65 120.643 21 -3 10 -4 6031.82 229.913 21 -3 10 -5 1726.39 106.749 21 -3 9 12 169.997 36.1049 2 -3 9 12 148.902 31.2949 9 -3 9 11 3746.70 185.274 9 -3 9 10 10594.6 352.021 9 -3 9 10 10203.7 341.420 1 -3 9 9 9418.81 358.827 9 -3 9 9 8921.63 346.846 1 -3 9 8 18691.0 538.734 9 -3 9 8 19768.8 538.570 1 -3 9 7 3918.32 251.639 1 -3 9 7 3826.57 246.317 9 -3 9 6 3974.63 255.064 9 -3 9 6 3592.80 243.184 1 -3 9 5 7137.70 342.286 9 -3 9 5 7182.17 340.719 21 -3 9 4 17622.4 555.906 21 -3 9 4 17223.1 524.514 9 -3 9 3 15899.5 534.466 21 -3 9 3 14393.3 464.569 9 -3 9 2 1946.44 197.122 21 -3 9 2 1989.39 166.645 9 -3 9 2 2127.61 179.289 8 -3 9 1 14308.0 513.101 21 -3 9 0 2479.75 215.582 21 -3 9 -1 1795.55 182.452 21 -3 9 -2-45.0773 53.9975 21 -3 9 -3 27.6176 47.3082 10 -3 9 -3 30.7201 49.6410 21 -3 9 -4 3176.95 201.302 10 -3 9 -4 3295.75 218.214 21 -3 9 -5 27.3418 43.8445 21 -3 9 -5 56.9905 44.8869 10 -3 9 -6 12.8836 35.7343 10 -3 9 -6-11.0130 33.4130 21 -3 9 -7 4447.19 184.168 21 -3 8 13 735.811 76.3288 2 -3 8 12 1763.72 128.040 9 -3 8 11 230.207 64.1490 9 -3 8 10 14786.0 470.799 1 -3 8 10 14962.3 474.854 9 -3 8 9 135.257 70.3020 9 -3 8 9 28.8459 53.1493 1 -3 8 8 6806.43 345.368 1 -3 8 8 7052.78 357.418 9 -3 8 7 1410.63 167.454 9 -3 8 7 1113.48 149.932 1 -3 8 6 36.9989 57.8093 21 -3 8 6 157.293 68.7348 9 -3 8 5 3805.33 270.298 21 -3 8 4 234.869 78.3774 21 -3 8 3 7440.19 391.339 21 -3 8 2 351.969 102.562 21 -3 8 1 1070.01 153.849 21 -3 8 0 6400.12 326.220 10 -3 8 0 7673.10 397.071 21 -3 8 -1 2054.91 188.843 10 -3 8 -1 2409.59 223.377 21 -3 8 -2 3.28842 52.8691 21 -3 8 -2 26.0415 51.5790 10 -3 8 -3 457.107 98.8831 10 -3 8 -3 610.860 118.325 21 -3 8 -4 19.7138 60.6230 21 -3 8 -4 154.548 75.3116 10 -3 8 -5 2020.35 186.139 21 -3 8 -5 1949.54 177.838 10 -3 8 -6 25.9966 43.9788 21 -3 8 -6-9.45830 53.9856 10 -3 8 -7 2806.27 187.698 21 -3 8 -7 3068.88 198.897 10 -3 8 -8 864.870 95.6026 21 -3 8 -8 954.500 104.114 10 -3 8 -9 2904.34 134.843 21 -3 8 -9 3166.96 153.125 10 -3 7 14 671.746 72.9628 2 -3 7 13 6466.00 234.677 22 -3 7 13 6703.88 265.637 2 -3 7 12 2295.44 164.794 9 -3 7 12 2181.75 158.287 22 -3 7 11 17086.2 508.818 9 -3 7 10 4059.02 267.599 1 -3 7 10 4139.93 265.917 9 -3 7 9 11812.6 436.800 11 -3 7 9 12242.8 481.072 9 -3 7 9 11744.8 467.701 1 -3 7 8 6935.33 334.613 11 -3 7 8 7189.19 366.565 1 -3 7 8 7114.28 374.899 9 -3 7 7 7621.81 347.751 11 -3 7 7 7166.78 378.670 1 -3 7 6 3431.78 257.614 21 -3 7 6 3732.10 241.896 11 -3 7 5 10829.9 464.448 21 -3 7 4 16404.2 577.242 21 -3 7 3 13451.1 1016.89 27 -3 7 3 13585.2 526.960 21 -3 7 2 23789.2 1368.40 27 -3 7 2 23895.0 706.694 21 -3 7 1 23929.6 705.545 21 -3 7 1 21830.3 1328.38 27 -3 7 1 22102.5 607.200 10 -3 7 0 3091.54 230.910 10 -3 7 0 3034.22 248.410 21 -3 7 -1 1727.82 193.148 21 -3 7 -1 1649.09 175.283 10 -3 7 -2 7112.57 354.147 10 -3 7 -2 7643.89 396.482 21 -3 7 -3 448.959 105.255 10 -3 7 -3 559.336 116.629 21 -3 7 -4 18717.4 584.353 10 -3 7 -4 19854.1 629.814 21 -3 7 -5 275.541 91.0733 21 -3 7 -5 267.456 89.6560 10 3 -7 5 331.936 88.6974 4 -3 7 -6 14350.5 496.268 10 3 -7 6 14870.8 523.235 4 -3 7 -6 15098.1 523.027 21 -3 7 -7 33442.2 754.167 21 -3 7 -7 31882.1 743.800 10 -3 7 -8-6.67605 42.0272 21 -3 7 -8-19.3533 53.3221 10 -3 7 -9 4968.95 234.098 21 -3 7 -9 5326.93 253.521 10 -3 7 -10 61.6734 31.5545 21 -3 7 -10 82.8440 44.5063 10 -3 7 -11 8718.80 227.806 10 -3 6 15 2659.82 133.972 3 -3 6 15 2993.01 143.673 2 -3 6 14 3914.04 191.311 22 -3 6 14 3853.76 197.174 2 -3 6 13 69292.6 1038.63 22 -3 6 13 70298.4 1051.70 2 -3 6 12 3483.80 232.675 22 -3 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529.931 16 3 7 10 13891.0 527.142 14 3 7 11 7158.91 366.483 9 3 7 11 7177.88 365.451 14 3 7 11 7164.43 356.157 13 3 7 12 646.605 113.711 13 3 7 12 455.337 85.2735 3 3 7 12 444.502 81.1896 14 3 7 13 4440.22 230.591 3 3 7 13 4970.30 259.299 14 3 7 13 4975.31 271.681 13 3 7 14 3696.31 190.532 3 3 7 14 4318.89 230.634 13 3 7 15 49.6123 25.2744 3 3 7 15 13.5321 30.6624 13 3 7 16 181.775 36.5805 13 -3 -8 11 372.273 50.1856 4 3 8 -10 2018.50 132.446 20 3 8 -9 403.506 75.6995 20 3 8 -8 14496.0 457.919 20 3 8 -8 12422.1 397.585 15 3 8 -7 688.329 105.109 15 3 8 -6 2437.42 198.824 15 3 8 -5-21.0902 72.4794 15 3 8 -4 291.293 84.9001 16 3 8 -4 456.256 99.7881 15 3 8 -3 634.569 112.102 16 3 8 -3 830.831 133.513 15 3 8 -2 9579.76 414.245 16 3 8 -2 10233.9 424.518 15 3 8 -1 24105.2 672.433 16 3 8 -1 25888.9 675.229 15 3 8 -1 25832.1 1420.79 26 3 8 0 1194.17 152.544 16 3 8 0 1300.82 146.198 15 3 8 1 1064.70 124.525 20 3 8 1 974.583 129.881 12 3 8 1 929.189 139.702 16 3 8 1 1128.99 132.948 15 3 8 1 1235.66 148.021 8 3 8 2 4817.13 281.334 9 3 8 2 4491.76 291.913 16 3 8 2 4615.89 267.358 15 3 8 2 4564.81 294.055 8 3 8 2 4483.08 283.278 13 3 8 2 4609.23 270.515 12 3 8 3 34022.3 734.255 15 3 8 3 34444.5 789.468 9 3 8 3 33801.0 825.284 16 3 8 3 34333.0 809.849 8 3 8 3 35224.7 810.466 13 3 8 3 35171.2 756.238 12 3 8 4 27683.1 716.254 9 3 8 4 27798.1 750.578 16 3 8 4 28736.5 654.289 15 3 8 4 28269.3 738.755 8 3 8 4 28086.5 717.103 13 3 8 4 26728.2 1391.26 23 3 8 4 28586.9 676.654 12 3 8 5 8723.34 403.184 9 3 8 5 9205.44 427.790 16 3 8 5 9012.75 414.400 8 3 8 5 9464.21 409.436 13 3 8 5 8877.04 816.666 23 3 8 5 9285.29 369.579 12 3 8 6 7925.98 397.492 8 3 8 6 7791.81 387.808 9 3 8 6 7610.63 393.907 16 3 8 6 8083.86 380.580 13 3 8 6 7370.52 764.355 23 3 8 6 7939.87 339.216 12 3 8 7 33033.0 829.140 9 3 8 7 32393.7 786.305 13 3 8 7 34256.0 858.613 16 3 8 7 33567.7 843.732 8 3 8 7 31300.7 695.906 12 3 8 8 22740.7 689.950 9 3 8 8 23357.9 709.709 16 3 8 8 22901.5 653.136 13 3 8 8 22102.4 572.775 12 3 8 9 5057.87 304.008 13 3 8 9 5182.37 326.651 9 3 8 9 5179.95 325.704 16 3 8 10 12220.1 494.082 9 3 8 10 12942.6 509.703 16 3 8 10 12116.9 499.239 14 3 8 10 12248.6 466.751 13 3 8 11 7390.19 366.095 9 3 8 11 7858.08 377.232 14 3 8 11 7812.72 359.745 13 3 8 12 32502.4 740.103 14 3 8 12 33490.7 728.787 13 3 8 13 2038.39 159.083 14 3 8 13 2252.03 171.013 13 3 8 14 3010.31 176.113 13 3 8 15 314.791 49.0323 13 3 9 -9 2276.65 132.300 20 -3 -9 9 2237.92 124.591 4 3 9 -8 812.270 97.8879 20 -3 -9 8 713.732 84.8051 4 3 9 -7 544.681 90.7800 15 3 9 -7 469.001 82.9122 20 3 9 -6 1340.03 149.904 20 3 9 -6 1566.06 152.080 15 3 9 -5 8099.25 362.586 20 3 9 -5 7900.34 352.707 15 3 9 -4 7735.69 359.411 20 3 9 -4 7349.10 353.148 15 3 9 -3 3317.19 240.164 20 3 9 -3 3356.37 222.893 16 3 9 -3 3520.87 242.789 15 3 9 -2 7876.74 367.289 20 3 9 -2 7449.87 345.993 16 3 9 -2 8454.56 385.523 15 3 9 -1 8381.96 375.271 20 3 9 -1 8303.32 378.054 16 3 9 -1 9161.27 399.898 15 3 9 -1 9222.77 404.413 8 3 9 0 348.385 76.0313 20 3 9 0 451.396 94.7660 16 3 9 0 467.798 93.7408 15 3 9 0 360.435 90.2682 8 3 9 1 555.489 96.0474 20 3 9 1 495.655 94.3756 15 3 9 1 548.117 107.820 16 3 9 1 618.780 119.206 8 3 9 2 8315.69 400.625 8 3 9 2 7836.94 389.264 16 3 9 2 8102.65 358.814 15 3 9 3 8451.79 384.795 9 3 9 3 8665.22 411.579 16 3 9 3 8384.34 362.324 12 3 9 3 8434.07 358.623 15 3 9 3 8939.53 410.068 13 3 9 3 9082.47 422.691 8 3 9 4 31516.1 805.050 8 3 9 4 29364.7 752.211 9 3 9 4 31509.6 807.145 16 3 9 4 29666.9 671.260 15 3 9 4 31461.4 771.669 13 3 9 4 30058.5 692.589 12 3 9 5 4900.02 306.416 9 3 9 5 5198.65 326.434 16 3 9 5 5583.47 337.111 8 3 9 5 5350.45 312.870 13 3 9 5 5256.40 274.315 12 3 9 6 39867.0 881.272 13 3 9 6 39794.6 908.141 9 3 9 6 39232.0 920.522 16 3 9 6 42058.2 958.171 8 3 9 7 19250.8 629.151 9 3 9 7 19211.3 633.967 16 3 9 7 20479.0 659.054 8 3 9 7 19732.8 605.608 13 3 9 8 405.881 96.8259 16 3 9 8 274.087 94.2362 9 3 9 8 297.994 84.8971 13 3 9 9 667.824 114.760 13 3 9 9 764.638 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297.408 8 3 10 2 26416.8 692.005 16 3 10 2 26955.9 649.423 15 3 10 3 2409.08 209.648 16 3 10 3 2416.04 186.395 15 3 10 3 2806.41 234.304 8 3 10 4 1383.26 155.763 9 3 10 4 1683.19 179.100 16 3 10 4 1365.47 136.649 15 3 10 4 1758.37 189.581 8 3 10 5 11593.6 450.106 9 3 10 5 10845.7 451.237 16 3 10 5 12326.2 487.113 8 3 10 5 11579.5 441.067 13 3 10 6 1386.88 167.113 9 3 10 6 1601.68 172.785 16 3 10 6 1746.18 189.804 8 3 10 6 1530.53 162.555 13 3 10 7 19366.3 598.327 9 3 10 7 18984.9 597.384 16 3 10 7 20440.8 622.084 8 3 10 7 19866.4 563.419 13 3 10 8 3411.11 247.076 9 3 10 8 3353.67 243.811 16 3 10 8 3281.65 221.377 13 3 10 9 24307.8 591.138 13 3 10 9 24819.3 656.483 9 3 10 9 25072.1 671.198 14 3 10 10 117.863 64.0405 14 3 10 10 201.740 58.9592 13 3 10 11 8357.83 299.500 13 3 10 11 8646.08 337.202 14 3 10 12 1905.02 128.500 13 3 10 12 1880.29 139.470 14 3 10 13 2367.81 125.900 14 3 10 13 2573.31 123.408 13 3 11 -6 2625.66 122.437 20 3 11 -5 4839.07 192.985 20 3 11 -5 4500.61 185.345 15 3 11 -4 268.563 55.0229 20 3 11 -4 458.733 76.4036 15 3 11 -3 282.820 59.8139 20 3 11 -3 289.268 54.2229 8 3 11 -3 371.996 75.0038 15 3 11 -2 42.4971 33.6595 20 3 11 -2-7.38840 54.9510 15 3 11 -2-2.02717 36.2173 8 3 11 -1 1334.25 125.859 20 3 11 -1 1161.97 122.249 15 3 11 -1 1286.43 128.936 8 3 11 0 3651.73 206.883 20 3 11 0 4060.20 236.546 8 3 11 0 3680.49 213.118 15 3 11 1 7255.86 327.490 8 3 11 1 6425.70 266.672 20 3 11 1 6222.10 268.255 16 3 11 1 6425.42 279.080 15 3 11 2 5495.82 299.280 8 3 11 2 4751.04 247.222 16 3 11 2 4756.57 237.972 15 3 11 3 18600.5 512.511 16 3 11 3 17237.1 443.629 15 3 11 4 839.263 115.099 16 3 11 4 924.662 128.082 8 3 11 4 846.449 104.273 14 3 11 5 105.676 55.1132 16 3 11 5 28.9010 72.1557 8 3 11 5-31.7428 58.0983 14 3 11 6 2928.31 202.886 16 3 11 6 3270.53 234.930 8 3 11 6 2865.39 206.544 14 3 11 7 322.323 71.6300 16 3 11 7 308.770 81.5363 14 3 11 8 8095.03 328.790 16 3 11 8 7931.10 332.886 14 3 11 9 9216.83 346.176 14 3 11 10 34928.3 657.178 14 3 11 11 6658.42 242.562 14 3 11 12 44.8996 24.3545 14 3 12 -3 249.602 35.1493 20 3 12 -2 10260.5 246.464 20 3 12 -2 10466.5 268.191 15 3 12 -1 131.571 40.0446 15 3 12 -1 183.702 38.5593 20 3 12 -1 105.097 35.6894 8 3 12 0 6047.56 232.168 8 3 12 0 5748.84 212.302 15 3 12 1 1228.42 110.961 8 3 12 1 1216.49 98.6716 15 3 12 2 2765.64 175.738 8 3 12 2 2201.88 127.751 15 3 12 3 764.165 76.6746 16 3 12 3 1300.16 142.241 8 3 12 4 1644.04 118.211 16 3 12 4 1918.42 153.749 8 3 12 5 795.554 88.1462 16 3 12 5 757.277 98.3656 8 3 12 5 627.540 71.1061 14 3 12 6 9784.13 300.989 16 3 12 6 9468.77 295.580 14 3 12 7 106.443 36.1732 14 3 12 8 9020.85 280.368 14 3 12 9 22407.6 424.389 14 3 12 10 531.777 56.4230 14 -4 10 8 2403.97 126.428 9 -4 10 7 6887.96 219.284 1 -4 10 7 6916.13 230.339 9 -4 10 6 164.371 45.0161 9 -4 10 6 148.882 43.2313 1 -4 10 5 503.609 66.1511 9 -4 10 5 506.839 68.0793 1 -4 10 4 6300.70 230.155 1 -4 10 4 5730.51 210.125 9 -4 10 3 1621.19 118.356 1 -4 10 2 1495.28 125.148 21 -4 10 2 1464.83 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437.569 4 -4 4 -4 11408.9 440.594 21 -4 4 -4 9544.54 838.751 27 -4 4 -4 10508.4 875.568 28 4 -4 5 7824.29 387.185 4 -4 4 -5 7124.87 763.190 28 -4 4 -5 7110.79 729.972 27 4 -4 6 29984.2 778.692 4 4 -4 7-73.8035 75.7017 6 4 -4 7-43.3240 64.5754 4 4 -4 7-3.87399 38.2226 18 4 -4 8 3315.92 249.064 4 4 -4 8 3166.64 254.351 6 4 -4 8 2974.24 221.115 18 4 -4 9 14.4785 49.7330 18 4 -4 10 6418.98 292.424 18 4 -4 11 8094.31 293.450 18 -4 4 -12 352.349 58.1885 11 4 -4 12 256.530 47.6511 18 -4 4 -13 5496.11 204.447 10 -4 3 15 782.849 91.1141 22 -4 3 14 1047.96 109.420 2 -4 3 14 969.188 119.085 22 -4 3 13 765.637 109.480 2 -4 3 13 676.538 115.402 22 -4 3 13 638.923 113.862 7 -4 3 12 10415.7 436.454 7 -4 3 12 10014.3 442.164 22 -4 3 12 9344.27 398.423 2 -4 3 11 49895.6 1023.39 7 -4 3 11 48305.3 958.711 2 -4 3 10 52999.1 1088.12 11 -4 3 10 56234.0 1093.31 7 -4 3 9 1724.17 189.346 11 -4 3 9 1884.10 194.190 7 -4 3 8 8843.45 408.956 11 -4 3 8 9637.88 401.087 1 -4 3 8 9652.72 860.599 25 -4 3 8 9542.09 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544.118 16 4 5 8 16647.1 566.472 14 4 5 9 7807.26 356.988 16 4 5 9 7755.76 388.687 14 4 5 10 4793.90 304.745 14 4 5 11 154.601 56.6373 3 4 5 11 356.756 105.706 14 4 5 12 3.84208 39.5548 3 4 5 13 15697.7 469.104 3 4 5 14 10960.4 359.718 3 4 5 15 2555.27 149.533 3 4 5 15 2812.49 168.939 13 4 5 16 1535.19 99.0804 13 4 6 -12 577.827 63.4124 20 -4 -6 12 652.339 75.4506 6 -4 -6 11 8069.67 307.816 6 -4 -6 10 3659.79 230.109 6 -4 -6 9 9662.46 394.394 6 -4 -6 8 349.311 87.6145 6 -4 -6 7 219.278 72.6013 6 4 6 -7 263.156 65.7066 15 -4 -6 6 2495.83 207.675 6 4 6 -6 2437.23 203.292 15 -4 -6 5 970.001 124.113 6 4 6 -5 1116.92 142.631 15 4 6 -5 1156.18 323.013 26 4 6 -4 277.389 73.6652 17 -4 -6 4 284.134 71.5901 6 4 6 -4 218.592 67.1129 15 4 6 -4 187.954 117.380 26 4 6 -3 47183.4 938.830 17 4 6 -3 46810.2 921.298 15 4 6 -3 48733.5 1950.86 26 4 6 -2 1424.02 151.387 15 4 6 -2 1087.39 257.991 26 4 6 -1 17709.6 1101.46 26 4 6 0 72161.8 2167.35 26 4 6 1 419.060 156.514 26 4 6 2 4809.85 526.922 26 4 6 3 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4 7 4 28887.5 762.827 16 4 7 4 27969.7 654.979 15 4 7 4 27428.2 714.281 13 4 7 4 28013.5 686.278 12 4 7 5 52367.0 1038.47 9 4 7 5 53739.3 1075.26 16 4 7 5 55130.9 1036.97 8 4 7 5 51422.5 1002.41 13 4 7 5 54969.4 937.947 15 4 7 5 51945.5 966.415 12 4 7 6 126.315 73.7679 16 4 7 6 66.5401 54.6764 9 4 7 6 145.336 55.7125 12 4 7 6 113.311 62.2713 8 4 7 6 86.6184 47.5213 15 4 7 6-68.0871 82.7645 14 4 7 6 37.0506 44.7460 13 4 7 7 1713.57 186.194 9 4 7 7 1612.34 181.627 16 4 7 7 1500.64 187.736 14 4 7 7 1674.72 179.849 13 4 7 7 1583.96 162.893 12 4 7 8 133.276 67.1417 16 4 7 8-37.6133 83.5738 14 4 7 8 117.999 69.3835 13 4 7 9 13062.5 507.354 16 4 7 9 13844.5 532.656 14 4 7 9 13102.4 491.338 13 4 7 10 2341.77 206.483 16 4 7 10 2432.47 218.146 14 4 7 10 2283.95 208.435 13 4 7 11 1682.95 176.265 14 4 7 11 1615.74 171.885 13 4 7 12 3720.48 245.311 14 4 7 12 3638.02 239.041 13 4 7 13 8070.87 331.512 13 4 7 13 7364.78 275.017 12 4 7 14 362.657 51.7708 12 4 7 14 557.411 85.6350 13 4 7 15 2264.22 134.195 13 4 8 -10 624.569 69.3102 20 4 8 -9 332.172 63.6103 20 4 8 -8 4176.93 203.145 15 4 8 -7 9.53035 55.3431 15 4 8 -6 9128.82 369.923 16 4 8 -6 9116.75 367.953 15 4 8 -5 5811.90 312.782 16 4 8 -5 6462.14 326.621 15 4 8 -4 25677.1 698.649 16 4 8 -4 27173.3 703.140 15 4 8 -3 4127.20 285.177 16 4 8 -3 4256.01 278.715 15 4 8 -2 951.544 145.094 16 4 8 -2 950.051 142.585 15 4 8 -1 4315.04 294.430 16 4 8 -1 4338.12 280.668 15 4 8 0 642.111 227.564 26 4 8 0 1100.46 150.924 16 4 8 0 1083.08 139.740 15 4 8 0 861.525 119.741 8 4 8 1 1366.38 171.983 16 4 8 1 1565.04 167.700 15 4 8 1 1377.88 155.862 8 4 8 1 1336.80 158.983 12 4 8 1 1139.07 291.873 26 4 8 2 2405.04 225.584 13 4 8 2 2580.24 235.031 16 4 8 2 2625.10 226.568 15 4 8 2 2512.30 233.210 8 4 8 2 2901.83 234.034 14 4 8 2 2631.59 218.741 12 4 8 3 73638.3 1300.68 16 4 8 3 70803.8 1157.96 15 4 8 3 71618.2 1205.67 8 4 8 3 72560.8 1235.07 14 4 8 3 75727.6 1277.55 13 4 8 3 72409.9 1210.54 12 4 8 4 7104.60 383.107 16 4 8 4 6820.24 355.204 8 4 8 4 6569.82 318.395 15 4 8 4 6231.20 351.545 14 4 8 4 7153.83 368.136 13 4 8 4 6920.69 344.575 12 4 8 5 240.712 72.0097 12 4 8 5 222.926 71.3818 9 4 8 5 131.922 70.6188 16 4 8 5 352.456 83.1131 15 4 8 5 225.318 90.1439 8 4 8 5 282.778 84.8612 13 4 8 6 1759.89 188.305 9 4 8 6 1672.14 194.411 16 4 8 6 1579.83 182.303 8 4 8 6 1706.83 183.486 14 4 8 6 1686.92 184.912 13 4 8 6 1586.21 163.436 12 4 8 7 3902.59 284.328 9 4 8 7 3875.85 286.100 16 4 8 7 3756.94 280.314 14 4 8 7 4004.89 279.150 13 4 8 7 3819.78 246.821 12 4 8 8 4118.99 290.054 16 4 8 8 3923.97 289.381 14 4 8 8 3947.39 276.413 13 4 8 8 3675.21 239.252 12 4 8 9 2163.58 207.437 16 4 8 9 2066.06 205.442 14 4 8 9 2242.99 204.315 13 4 8 9 2055.80 174.284 12 4 8 10 1001.31 147.111 16 4 8 10 890.171 129.159 13 4 8 10 1071.95 140.954 14 4 8 10 1129.49 125.214 12 4 8 11 66.0207 41.2405 12 4 8 11 99.3659 57.7937 14 4 8 11 108.307 62.9935 13 4 8 12 6166.68 299.726 14 4 8 12 6036.14 291.975 13 4 8 12 5418.81 228.699 12 4 8 13 1512.21 134.794 13 4 8 14 57.6041 32.7360 13 4 8 15 30.6462 23.4498 13 4 9 -9 418.727 52.7404 20 4 9 -8 587.408 78.0550 20 -4 -9 8 465.327 60.3786 4 4 9 -7 9363.58 331.107 20 4 9 -7 8581.01 290.291 15 4 9 -6 235.499 78.4375 20 4 9 -6 269.515 72.2049 15 4 9 -5 18312.6 526.293 20 4 9 -5 19159.4 524.807 15 4 9 -4 315.564 80.4255 16 4 9 -4 1286.79 188.225 15 4 9 -3 14968.5 496.533 16 4 9 -3 16691.1 532.254 15 4 9 -2 4106.16 264.634 16 4 9 -2 4578.71 280.845 15 4 9 -1 1177.19 138.127 20 4 9 -1 1182.17 152.019 16 4 9 -1 1381.28 158.733 15 4 9 -1 1105.59 130.427 8 4 9 0 11744.6 426.753 20 4 9 0 12945.8 496.735 16 4 9 0 12034.7 446.567 8 4 9 1 1139.51 163.348 16 4 9 1 1163.15 146.358 15 4 9 1 1182.50 152.596 8 4 9 2 7270.10 388.734 16 4 9 2 6900.25 341.733 15 4 9 2 7444.13 365.749 8 4 9 3 9932.08 445.116 16 4 9 3 10125.2 427.592 8 4 9 3 9372.04 385.223 15 4 9 3 9046.26 402.490 14 4 9 3 9445.34 396.849 12 4 9 4 8177.94 405.727 16 4 9 4 7701.04 340.408 15 4 9 4 8192.07 393.217 8 4 9 4 7462.52 380.173 14 4 9 4 8426.66 407.522 13 4 9 4 7937.46 360.042 12 4 9 5 1732.23 192.071 16 4 9 5 2134.16 206.163 8 4 9 5 1847.30 160.511 15 4 9 5 1913.66 191.814 14 4 9 5 2087.33 203.526 13 4 9 5 2078.02 185.334 12 4 9 6 2166.64 214.980 16 4 9 6 2081.41 206.815 8 4 9 6 2287.00 215.393 14 4 9 6 2162.88 209.512 13 4 9 6 1924.12 173.062 12 4 9 7 27.0315 67.5418 16 4 9 7-62.8094 92.3048 14 4 9 7 85.7439 52.5772 13 4 9 7 114.550 56.4335 12 4 9 8 5859.33 321.140 13 4 9 8 6197.72 345.619 16 4 9 8 5522.36 329.213 14 4 9 8 5235.66 267.442 12 4 9 9 2014.06 195.219 16 4 9 9 1806.76 183.260 14 4 9 9 2069.76 190.424 13 4 9 9 1794.50 147.944 12 4 9 10 2170.79 198.780 16 4 9 10 1812.91 181.780 14 4 9 10 1772.35 170.837 13 4 9 10 1865.17 142.436 12 4 9 11 5925.93 302.816 14 4 9 11 6120.99 290.046 13 4 9 12 719.657 105.713 14 4 9 12 606.292 89.3851 13 4 9 13 13.0098 34.0409 13 4 9 14 4312.57 162.895 13 4 10 -7 80.5163 30.6976 20 4 10 -6 3499.24 179.557 20 4 10 -6 3284.22 168.971 15 4 10 -5 1494.08 176.427 20 4 10 -5 967.683 134.528 15 4 10 -4 18411.4 481.702 20 4 10 -4 19499.8 501.000 15 4 10 -3 113.055 49.5937 20 4 10 -3 143.320 42.7865 16 4 10 -3 72.2737 58.0938 15 4 10 -2 1340.57 135.226 20 4 10 -2 1304.59 132.870 16 4 10 -2 1397.26 144.922 15 4 10 -1 216.407 62.7433 8 4 10 -1 223.373 66.0739 20 4 10 -1 210.907 70.7551 16 4 10 -1 239.642 81.4554 15 4 10 0 2757.38 189.940 20 4 10 0 2766.19 211.897 16 4 10 0 3022.51 217.481 15 4 10 0 2872.77 209.567 8 4 10 1 4836.49 278.658 8 4 10 1 4635.96 280.651 16 4 10 1 5150.05 282.437 15 4 10 2 1586.56 170.971 16 4 10 2 1676.62 162.736 15 4 10 2 1682.85 173.486 8 4 10 3 5116.82 305.166 16 4 10 3 4847.81 263.348 15 4 10 3 5193.94 299.007 8 4 10 3 4776.16 266.940 14 4 10 4 336.148 92.4554 16 4 10 4 289.830 69.7644 15 4 10 4 194.694 77.4755 8 4 10 4 218.769 55.9680 14 4 10 5 124.157 73.2418 16 4 10 5-51.9382 35.8246 15 4 10 5 34.6748 72.5831 8 4 10 5-50.7031 66.9551 14 4 10 6 1117.01 145.593 16 4 10 6 869.492 129.084 14 4 10 6 1132.85 150.453 8 4 10 6 1199.77 147.253 13 4 10 6 874.630 108.110 12 4 10 7 1702.59 182.914 16 4 10 7 1418.80 164.391 14 4 10 7 1529.02 162.284 13 4 10 7 1252.30 120.840 12 4 10 8 13929.9 488.724 16 4 10 8 13984.1 486.672 14 4 10 8 14043.4 460.491 13 4 10 9 5748.69 296.415 16 4 10 9 5598.00 296.426 14 4 10 9 5579.24 277.151 13 4 10 10 2261.34 181.485 14 4 10 10 2126.10 160.256 13 4 10 11 297.426 72.2264 14 4 10 11 334.472 64.1624 13 4 10 12 505.059 79.2642 14 4 10 12 389.200 60.0289 13 4 10 13 1164.56 78.3704 13 4 11 -5 280.067 43.7678 20 4 11 -5 234.402 44.6188 15 4 11 -4 82.9573 31.4771 20 4 11 -4 142.805 47.3914 15 4 11 -3 674.024 78.5465 20 4 11 -3 558.622 88.7378 15 4 11 -2 1651.08 124.581 20 4 11 -2 1660.32 136.368 15 4 11 -1 13719.6 365.814 20 4 11 -1 13193.7 358.388 16 4 11 0 3201.00 189.898 8 4 11 0 3342.63 195.123 16 4 11 0 3431.57 202.371 15 4 11 1 8401.71 323.552 16 4 11 1 8435.18 326.618 8 4 11 1 8465.44 318.580 15 4 11 2 2073.71 168.267 16 4 11 2 2019.89 150.771 15 4 11 2 2169.63 174.382 8 4 11 3 77.3220 55.9349 16 4 11 3-36.2241 51.9061 8 4 11 4 1425.93 146.245 16 4 11 4 1052.60 103.415 15 4 11 4 1235.76 137.931 8 4 11 4 1317.67 124.139 14 4 11 5 2946.97 208.751 16 4 11 5 2935.28 207.725 8 4 11 5 2559.16 179.389 14 4 11 6 13753.1 441.648 16 4 11 6 13097.8 419.865 14 4 11 7 15592.9 462.860 16 4 11 7 15254.9 450.815 14 4 11 8 2232.49 176.845 16 4 11 8 3598.04 243.898 14 4 11 9 5979.88 264.285 16 4 11 9 5233.64 243.842 14 4 11 10 9147.29 301.350 14 4 11 11 3232.14 156.516 14 4 12 -2 9362.63 236.559 15 4 12 -1 227.528 47.9106 15 4 12 0 15399.3 337.849 15 4 12 0 13929.2 302.995 8 4 12 1 174.742 42.4001 15 4 12 1 180.331 45.6196 8 4 12 2 940.848 81.8744 16 4 12 2 956.522 84.2846 15 4 12 2 1141.43 101.904 8 4 12 3 2220.02 134.294 16 4 12 3 2063.01 113.933 15 4 12 4 400.923 60.3762 16 4 12 5 975.264 95.4676 16 4 12 6 13732.9 353.401 16 4 12 6 13450.7 315.447 14 4 12 7 476.138 80.0612 16 4 12 7 237.899 51.1228 14 4 12 8 11605.1 286.241 14 4 12 9 1400.14 91.6340 14 -5 9 8 745.775 78.8368 9 -5 9 7 3813.86 178.673 9 -5 9 6 180.899 38.4661 1 -5 9 6 125.195 42.3482 9 -5 9 5 669.071 80.3159 9 -5 9 5 530.055 61.4595 1 -5 9 4 923.263 93.9392 9 -5 9 4 916.910 80.6764 1 -5 9 3 8087.03 261.218 9 -5 9 3 7990.32 238.040 1 -5 9 2 1398.54 129.062 21 -5 9 2 1117.94 91.9806 9 -5 9 1-6.92978 32.5559 21 -5 9 0 5599.03 244.022 21 5 -9 0 4715.90 187.512 5 -5 9 -1 2052.40 141.592 21 5 -9 1 1855.83 115.737 5 -5 9 -2 561.237 71.8626 21 5 -9 2 437.038 54.6746 5 -5 9 -3 626.032 67.6227 21 5 -9 3 567.531 58.0960 5 -5 8 10 305.534 43.7281 2 -5 8 10 252.478 43.1689 9 -5 8 9 472.531 72.8661 9 -5 8 8 4279.55 216.585 9 -5 8 7 1129.89 101.867 11 -5 8 7 1114.37 106.036 1 -5 8 7 1293.38 127.995 9 -5 8 6 668.616 86.1622 11 -5 8 6 673.987 104.204 9 -5 8 6 771.417 91.8534 1 -5 8 5 1504.83 125.486 11 -5 8 5 2028.78 169.963 9 -5 8 5 1855.43 143.876 1 -5 8 4 1336.29 118.193 11 -5 8 4 1475.11 127.268 1 -5 8 3 20185.7 582.694 21 -5 8 3 18939.3 466.415 1 -5 8 2 7551.44 352.739 21 -5 8 2 7324.52 279.149 1 5 -8 -2 7919.37 321.468 5 -5 8 1-29.2215 36.1736 1 5 -8 -1 16.8160 33.8257 5 -5 8 0 1474.10 155.409 21 5 -8 0 1625.34 150.695 5 5 -8 1 658.152 96.5175 5 -5 8 -1 706.288 110.386 21 -5 8 -2 3069.18 206.393 21 5 -8 2 2909.38 195.337 5 -5 8 -3 2839.40 186.892 21 5 -8 3 2715.52 181.796 5 -5 8 -4 13.8971 31.5932 21 -5 8 -5 11618.5 310.624 21 5 -8 6 973.614 85.8790 5 -5 7 12 2498.58 108.248 2 -5 7 11 40.5989 31.9456 22 -5 7 11 83.2584 30.1365 2 -5 7 11 38.9557 23.0652 9 -5 7 10 2029.03 143.542 9 -5 7 10 1941.46 133.448 2 -5 7 9 24.6459 40.1805 9 -5 7 8 1240.75 132.780 11 -5 7 8 1314.61 151.285 9 -5 7 7 54.6869 55.0742 11 -5 7 7 29.5831 34.8995 1 -5 7 6 2103.75 175.122 11 -5 7 6 1906.74 163.728 1 -5 7 5 5979.58 295.372 11 -5 7 5 5622.66 279.640 1 -5 7 4 60.1909 39.7791 1 -5 7 4 107.379 59.4612 11 5 -7 -4 36.1934 35.5436 5 -5 7 3 413.725 94.6768 21 -5 7 3 434.874 86.6596 11 -5 7 3 455.366 84.5640 1 5 -7 -3 447.703 92.1360 5 -5 7 2 20605.1 641.504 21 -5 7 2 20499.5 550.011 11 5 -7 -2 19483.9 597.550 5 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205.298 10 -5 6 -10 1702.60 93.8354 10 -5 5 14 688.916 61.0799 22 -5 5 13 153.325 48.3758 22 -5 5 13 147.975 34.4416 2 -5 5 12 64.6904 48.6025 22 -5 5 12 63.9278 32.3837 2 -5 5 12 28.0011 29.0602 7 -5 5 11 497.119 80.5953 2 -5 5 11 456.394 70.0635 9 -5 5 11 472.584 81.3602 7 -5 5 10 2235.35 176.114 7 -5 5 10 2067.26 169.675 9 -5 5 10 2349.52 202.395 11 -5 5 10 2330.46 180.549 2 -5 5 9 1650.90 178.016 11 -5 5 9 1670.01 159.048 7 -5 5 8 91.4920 64.5199 11 -5 5 8 124.095 55.5339 7 -5 5 7 539.845 96.2591 7 -5 5 7 736.603 126.682 11 -5 5 7 520.597 92.5822 1 -5 5 6 5610.76 324.895 11 5 -5 -6 4769.50 300.954 5 -5 5 6 5158.42 286.811 1 -5 5 6 5098.53 281.356 7 -5 5 5 313.063 76.0637 7 -5 5 5 382.835 88.0800 11 -5 5 5 250.672 71.4255 1 5 -5 -5 232.758 70.6063 5 -5 5 4 3176.99 257.449 21 -5 5 4 3777.30 266.885 11 -5 5 4 3290.23 222.363 1 5 -5 -4 3204.64 258.652 5 -5 5 3 4744.60 310.729 21 -5 5 3 5103.08 312.035 11 5 -5 -3 4561.29 310.070 5 5 -5 -2 1.03498 45.5319 5 -5 5 2 106.778 61.7972 21 -5 5 2 106.084 72.6158 11 -5 5 1 37823.5 899.702 21 -5 5 1 40186.9 877.991 11 -5 5 0 17173.7 586.915 21 -5 5 0 17935.9 580.963 11 -5 5 -1 847.070 131.905 21 -5 5 -1 1024.90 141.781 11 -5 5 -2 362.758 93.8269 21 -5 5 -2 333.104 88.8375 11 -5 5 -3 1110.25 150.002 21 -5 5 -3 1149.84 148.568 11 -5 5 -3 1052.29 131.679 10 -5 5 -4 4062.23 270.341 21 -5 5 -4 4521.41 290.045 11 -5 5 -4 4033.41 253.151 10 -5 5 -5 171.270 60.0072 21 -5 5 -5-29.0508 58.7013 11 -5 5 -6 2053.96 180.572 21 -5 5 -6 2538.82 215.596 11 -5 5 -7 4447.33 243.454 21 -5 5 -7 5246.61 280.212 11 -5 5 -8 22737.6 557.668 11 -5 5 -8 25748.1 615.344 10 -5 5 -9 275.188 59.2107 11 -5 5 -9 279.221 70.1480 10 -5 5 -10 4965.70 183.290 11 -5 5 -10 7321.96 268.597 10 -5 5 -11 1307.87 93.4581 10 -5 4 14 6912.20 233.217 22 -5 4 13 236.408 61.3382 22 -5 4 13 263.318 52.9288 2 -5 4 12 8212.83 348.674 22 -5 4 12 8218.57 309.432 2 -5 4 12 8288.21 330.072 7 -5 4 11 374.038 77.2144 2 -5 4 11 250.148 68.9742 7 -5 4 10 7172.69 369.068 11 -5 4 10 7100.79 326.887 2 -5 4 10 7202.96 347.957 7 -5 4 9 3834.21 274.715 11 -5 4 9 3794.72 260.655 7 -5 4 8 18344.8 611.268 11 -5 4 8 17762.9 573.014 7 -5 4 7 170.859 63.1895 7 -5 4 7 182.850 74.6952 11 -5 4 7 179.238 61.6158 1 -5 4 6 19502.6 618.078 11 -5 4 6 18685.4 545.031 1 -5 4 6 19062.6 582.997 7 -5 4 5 1374.46 162.380 11 -5 4 5 1686.00 355.214 27 5 -4 -5 1185.92 160.270 5 -5 4 5 1272.96 135.531 1 -5 4 5 1235.45 308.845 25 -5 4 4 3989.24 277.986 21 -5 4 4 4176.53 277.957 11 -5 4 4 4351.56 581.483 27 5 -4 -4 3473.68 270.515 5 -5 4 3 27871.5 739.834 21 -5 4 3 29278.9 750.066 11 -5 4 3 30316.6 1486.38 27 -5 4 2 1627.17 175.181 21 -5 4 2 1662.71 178.142 11 -5 4 2 1359.90 313.816 27 5 -4 -2 1545.28 180.099 5 -5 4 1 9111.10 407.784 21 -5 4 1 9761.08 421.865 11 -5 4 1 9048.58 815.735 27 -5 4 0 7961.29 378.627 21 -5 4 0 8053.74 386.345 11 -5 4 0 8325.64 787.106 27 -5 4 -1 69260.7 1193.41 21 -5 4 -1 71951.5 1238.87 11 -5 4 -1 70373.3 2368.43 27 -5 4 -2 22405.1 641.093 21 -5 4 -2 24084.3 688.555 11 -5 4 -2 23648.2 1369.38 27 -5 4 -3 26467.2 700.894 21 -5 4 -3 27182.0 759.755 11 -5 4 -4 9475.09 410.416 21 -5 4 -4 10544.9 466.223 11 -5 4 -5 590.411 102.555 21 -5 4 -5 564.677 125.401 11 -5 4 -6 11573.4 430.646 21 -5 4 -6 14803.6 565.913 11 5 -4 7 798.118 110.533 18 5 -4 8 956.717 118.967 18 -5 4 -9-1.51434 51.5913 11 5 -4 9 41.0034 34.8000 18 -5 4 -10 157.645 50.4537 11 5 -4 10 231.541 49.3378 18 -5 4 -11 3986.86 189.218 11 -5 4 -12 47.9922 30.8905 10 -5 3 14 1112.12 104.926 22 -5 3 13 2127.39 170.838 22 -5 3 13 2104.70 147.075 2 -5 3 13 2122.45 163.597 7 -5 3 12-9.67373 42.2272 2 -5 3 12 49.6670 67.0835 22 -5 3 12-44.5613 60.0270 7 -5 3 11 8496.99 387.534 7 -5 3 11 8090.06 342.689 2 -5 3 10 478.864 96.3597 2 -5 3 10 431.286 103.142 11 -5 3 10 427.512 95.7664 7 -5 3 9 1609.15 183.446 11 -5 3 9 1546.71 173.911 7 -5 3 9 1578.23 162.411 2 -5 3 8 968.845 143.384 11 -5 3 8 1183.61 153.786 7 -5 3 7 17194.2 585.077 11 -5 3 7 18656.4 598.281 7 -5 3 6 12583.0 492.804 11 -5 3 6 14231.5 459.185 1 -5 3 6 13628.4 1040.33 25 -5 3 5 10613.6 441.502 11 5 -3 -5 10576.7 462.990 5 -5 3 5 10682.0 908.425 25 -5 3 4 5539.49 316.530 11 5 -3 -4 5590.38 335.625 5 -5 3 4 5378.03 637.591 25 -5 3 3 7103.82 351.849 21 -5 3 3 7372.72 364.087 11 5 -3 -3 7495.75 380.071 5 -5 3 3 7792.97 760.368 25 5 -3 -2 159.442 58.7323 5 -5 3 2 65.1700 43.4586 21 -5 3 2 155.942 55.3345 11 -5 3 2 113.618 96.3868 27 -5 3 1 11217.7 441.483 11 -5 3 1 11954.0 884.141 27 5 -3 -1 11145.5 455.580 5 -5 3 0 99824.7 1470.93 11 -5 3 0 95591.1 2558.37 27 -5 3 -1 5973.47 329.457 11 -5 3 -1 5797.86 553.565 28 -5 3 -1 5919.68 628.735 27 -5 3 -2 4931.32 277.680 21 -5 3 -2 4383.44 282.653 11 -5 3 -2 3884.61 484.004 28 -5 3 -2 4251.72 544.639 27 -5 3 -3 16698.3 516.767 21 -5 3 -3 15636.7 558.098 11 5 -3 3 17579.1 545.202 18 -5 3 -3 13710.8 963.730 28 -5 3 -3 14665.1 1025.04 27 5 -3 4 17744.3 558.271 18 -5 3 -4 16507.1 1110.44 28 -5 3 -4 17176.0 1095.61 27 5 -3 5 13450.8 499.733 18 -5 3 -5 13228.2 1064.32 28 5 -3 6 2712.65 225.538 18 5 -3 7 932.685 135.773 18 5 -3 8 32.3093 51.8208 18 5 -3 9 798.237 122.906 18 5 -3 10 425.549 82.1325 18 5 -3 11 18.4684 31.6761 18 -5 3 -12 546.400 77.3210 11 5 -3 12 470.048 64.4561 18 -5 3 -13 396.651 48.1590 11 -5 3 -13 782.261 74.4002 10 -5 2 15 2544.99 121.818 22 -5 2 14 2339.01 152.769 22 -5 2 13 227.712 62.3762 22 -5 2 13 180.485 58.9983 7 -5 2 12 4129.32 262.639 22 -5 2 12 4051.25 234.326 2 -5 2 12 4046.86 261.493 7 -5 2 11 6519.80 310.929 2 -5 2 11 6926.83 364.378 7 -5 2 10 4210.81 287.193 11 -5 2 10 4689.84 272.947 2 -5 2 10 4902.16 311.578 7 -5 2 9 12095.7 487.019 11 -5 2 9 12142.7 445.475 2 -5 2 9 12664.7 506.265 7 -5 2 8 12081.5 486.226 11 -5 2 8 11851.8 428.671 2 -5 2 8 12843.4 507.423 7 -5 2 7 751.853 123.487 7 -5 2 7 628.073 118.374 11 -5 2 7 895.640 275.849 25 -5 2 6 6306.67 335.550 11 -5 2 6 6501.92 700.020 25 -5 2 5 19794.2 589.808 11 5 -2 -5 21026.3 643.290 5 -5 2 4 11640.0 871.839 25 -5 2 3 113.650 58.8154 25 -5 2 2 16926.8 1031.68 25 -5 2 1 667.625 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4 7 7296.40 370.815 11 -6 4 7 6755.90 337.367 7 -6 4 6 113.646 64.5917 7 -6 4 6 109.416 69.4576 11 -6 4 5 5979.04 338.549 11 6 -4 -5 5297.17 336.191 5 -6 4 4 193.226 71.6084 11 6 -4 -4 204.211 77.9925 5 -6 4 3 8147.92 396.836 11 6 -4 -3 7452.64 401.346 5 -6 4 2 29866.9 780.991 21 6 -4 -2 31529.2 845.210 5 -6 4 1 6918.78 361.002 21 -6 4 1 7692.46 395.962 11 6 -4 -1 6867.38 392.426 5 -6 4 0 12851.6 489.885 21 6 -4 0 13719.9 550.146 5 -6 4 -1 5155.36 304.914 21 -6 4 -1 5841.98 340.414 11 6 -4 1 5554.87 347.687 5 -6 4 -2 5340.77 303.390 21 -6 4 -2 6164.29 347.312 11 -6 4 -3 9360.58 391.852 21 -6 4 -3 10909.1 465.918 11 -6 4 -4 157.710 57.1056 21 -6 4 -4 185.977 77.3263 11 -6 4 -5 2890.24 236.793 11 -6 4 -6 53445.5 1015.55 11 -6 4 -7 1340.69 156.631 11 -6 4 -8 14827.9 466.661 11 -6 4 -9 1434.44 129.555 11 -6 4 -9 1406.93 118.199 10 6 -4 10 20.1745 17.4837 5 -6 4 -10-10.3435 33.6029 10 -6 3 13 86.7301 29.9561 22 -6 3 12 9.17375 36.5452 22 -6 3 12 21.6368 34.6097 7 -6 3 11 4403.68 250.757 22 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181.946 11 6 -3 2 1487.38 163.381 18 -6 3 -3 6448.99 365.427 11 6 -3 3 5862.60 323.555 18 -6 3 -4 4961.91 332.915 11 6 -3 4 4272.45 275.607 18 -6 3 -5 2705.18 252.142 11 6 -3 5 2184.47 196.231 18 -6 3 -6 304.773 98.2263 11 6 -3 6 263.005 73.4685 18 -6 3 -7 16585.8 567.951 11 6 -3 7 13813.3 474.758 18 -6 3 -8 5671.93 316.707 11 6 -3 8 4683.17 265.157 18 -6 3 -9 115.142 82.9263 11 6 -3 9 111.459 61.7320 18 -6 3 -10 1360.34 135.336 11 6 -3 10 1296.37 115.219 18 -6 3 -11 9763.80 300.398 11 6 -3 11 8540.16 238.562 18 -6 3 -12 2339.67 109.545 10 -6 2 13 808.001 83.2118 22 -6 2 12 495.944 83.0674 22 -6 2 12 451.651 79.0542 7 -6 2 11 2833.74 208.534 22 -6 2 11 2610.70 166.654 2 -6 2 11 2823.21 211.140 7 -6 2 10 13353.9 406.361 2 -6 2 10 14360.7 501.854 7 -6 2 9-45.1152 41.7788 2 -6 2 9 87.5390 57.1546 11 -6 2 9 68.6571 64.4842 7 -6 2 8 4222.57 281.278 11 -6 2 8 4197.51 232.324 2 -6 2 8 4384.35 294.004 7 -6 2 7 3946.32 270.570 11 -6 2 7 4171.16 285.915 7 -6 2 6 5998.77 335.724 11 -6 2 5-18.4763 66.9991 11 -6 2 4 35608.0 846.653 11 6 -2 -4 37020.9 915.566 5 -6 2 3 41465.6 917.442 11 6 -2 -3 44084.8 993.438 5 -6 2 2 70236.6 1222.95 11 6 -2 -2 71563.8 1288.67 5 -6 2 1 887.728 120.118 21 -6 2 1 967.331 138.047 11 6 -2 -1 773.198 122.808 18 -6 2 1 1032.93 276.642 27 6 -2 -1 1131.08 154.929 5 -6 2 0-116.886 53.6553 21 -6 2 0-64.8166 62.8785 11 6 -2 0-70.2343 80.8717 18 -6 2 0-23.4246 98.0153 27 6 -2 0-40.3251 55.0430 5 -6 2 -1 22769.0 681.085 11 6 -2 1 22748.0 663.084 18 -6 2 -1 22766.0 1187.73 28 -6 2 -1 22610.3 1262.44 27 6 -2 1 22480.4 684.591 5 -6 2 -2 43870.0 976.855 11 6 -2 2 43069.7 943.668 18 -6 2 -2 43057.3 1715.11 28 -6 2 -2 47052.0 1827.26 27 -6 2 -3 16784.2 600.200 11 6 -2 3 16154.0 563.137 18 -6 2 -3 16618.0 1090.29 28 -6 2 -4 2144.57 216.962 11 6 -2 4 2042.92 201.967 18 6 -2 5 15101.1 543.717 18 6 -2 6 1234.61 157.833 18 6 -2 7 6189.65 341.043 18 6 -2 8 8043.27 375.637 18 6 -2 9 8677.04 374.299 18 6 -2 10 13267.8 432.553 18 -6 2 -11 143.311 60.4708 11 6 -2 11 103.641 43.7890 18 -6 2 -12 5287.71 221.749 11 6 -2 12 4865.81 195.502 18 -6 1 13 74.6441 34.4838 22 -6 1 12 3036.00 187.374 22 -6 1 12 3253.10 208.877 7 -6 1 11 1229.01 137.552 22 -6 1 11 1030.17 111.351 6 -6 1 11 1351.10 157.482 7 -6 1 10 2700.77 180.770 2 -6 1 10 2539.79 194.560 6 -6 1 10 2724.95 227.388 7 -6 1 9 1024.77 139.188 11 -6 1 9 1060.09 116.106 2 -6 1 9 1199.98 142.287 6 -6 1 9 1291.52 166.061 7 -6 1 8 3240.13 245.411 11 -6 1 8 3284.57 260.018 7 -6 1 7 493.468 103.460 7 -6 1 7 308.549 85.1650 11 -6 1 6 5610.48 313.332 11 -6 1 5 69.6217 50.5456 11 -6 1 5 457.200 186.827 25 -6 1 4 7201.62 360.852 11 6 -1 -4 7056.13 386.669 5 -6 1 4 8162.91 740.996 25 -6 1 3 6215.05 330.984 11 6 -1 -3 6778.85 328.295 17 6 -1 -3 7052.77 377.475 5 -6 1 2 1692.99 173.927 11 6 -1 -2 2074.26 203.134 5 -6 1 1 4370.44 274.511 11 6 -1 -1 4086.18 286.262 18 -6 1 1 4321.32 497.001 28 6 -1 -1 4539.08 299.538 5 -6 1 0 3686.86 261.085 11 6 -1 0 3667.59 266.882 18 -6 1 0 3647.76 459.615 28 6 -1 0 4198.89 280.624 5 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389.349 12 7 4 3 28050.1 774.096 18 7 4 3 28144.8 710.056 17 7 4 3 27404.7 691.135 12 7 4 4 157.329 64.9989 18 7 4 4 167.198 59.6578 17 7 4 5 14096.5 526.365 18 7 4 5 13032.1 472.192 12 7 4 6 2513.11 218.926 18 7 4 7 1388.62 161.974 18 7 4 8 15183.7 525.309 18 7 4 9 3515.02 239.635 18 7 4 10 10117.0 385.559 18 7 4 11-2.80438 39.7317 18 7 4 12 1870.80 133.009 18 7 4 13 3278.79 136.004 18 7 4 13 3433.91 155.475 12 -7 -5 10 81.1267 33.6425 6 -7 -5 9 262.050 57.4538 6 -7 -5 8 1166.96 126.265 6 -7 -5 7 3725.26 236.622 6 7 5 -6 423.205 104.150 17 -7 -5 6 457.308 91.0088 6 7 5 -5-6.38622 57.0717 17 -7 -5 5 54.5273 63.8660 6 7 5 -4 347.723 99.9895 17 7 5 -4 241.559 63.0603 15 7 5 -3 25718.5 713.440 17 7 5 -3 23081.2 621.552 15 7 5 -2-41.6364 57.8290 17 7 5 -2-15.6054 48.3774 15 7 5 -1 777.466 127.978 17 7 5 -1 891.829 132.279 15 7 5 -1 706.034 116.394 12 7 5 0 21365.7 622.540 17 7 5 0 19846.2 594.546 15 7 5 0 19738.1 595.353 12 7 5 1 1639.64 172.221 17 7 5 1 1377.41 165.369 16 7 5 1 1825.24 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60.0972 12 7 7 -8-18.8925 30.4289 16 -7 -7 7 1413.65 99.1360 6 7 7 -7 1849.27 144.745 16 -7 -7 6 6595.17 242.651 6 -7 -7 5 438.007 68.5455 6 7 7 -5 380.022 67.5445 15 -7 -7 4 4337.36 216.141 6 7 7 -4 4462.73 235.348 15 7 7 -3 20309.7 599.915 17 7 7 -3 19901.1 545.076 15 7 7 -2 2252.38 208.975 17 7 7 -2 2147.58 228.538 16 7 7 -2 2375.90 200.398 15 7 7 -1 1963.89 180.848 17 7 7 -1 1942.15 207.632 16 7 7 -1 1822.46 179.617 15 7 7 0 784.491 121.024 17 7 7 0 848.748 142.503 16 7 7 0 865.471 127.589 15 7 7 1 41221.2 836.141 17 7 7 1 44006.6 956.927 16 7 7 1 42510.4 884.434 15 7 7 1 41817.9 897.221 12 7 7 2 5045.48 271.618 17 7 7 2 5368.06 319.759 16 7 7 2 5265.52 297.174 15 7 7 2 5324.72 309.869 12 7 7 3 1930.27 165.116 17 7 7 3 1991.65 191.550 16 7 7 3 2066.34 187.740 15 7 7 3 1839.70 181.794 12 7 7 4 140.091 71.6455 16 7 7 4 74.1146 51.8138 15 7 7 4 105.291 59.8019 12 7 7 5 1328.53 147.724 16 7 7 5 1730.70 166.300 15 7 7 5 1483.79 167.317 12 7 7 6 3903.88 243.080 16 7 7 6 4339.05 251.232 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4084.70 253.537 15 7 8 3 3877.13 257.754 12 7 8 4 4322.13 271.849 16 7 8 4 4593.80 263.013 15 7 8 4 4417.54 267.390 12 7 8 5 5697.52 300.400 16 7 8 5 6442.80 299.503 15 7 8 5 6119.27 309.431 12 7 8 6 4523.06 254.608 16 7 8 6 5038.00 254.093 15 7 8 6 4849.31 277.211 12 7 8 7 6494.64 285.106 16 7 8 7 7022.16 285.084 15 7 8 7 7009.09 312.300 12 7 8 8 2284.92 149.208 16 7 8 8 2440.91 152.279 15 7 8 8 2515.17 170.591 13 7 8 8 2652.89 186.891 12 7 8 9 4194.20 203.386 13 7 8 9 4771.06 230.591 12 7 8 10 1408.59 117.328 12 7 8 11 129.108 39.8012 12 7 9 -5 1.97695 15.6847 20 7 9 -5-32.5415 26.3403 16 7 9 -4 98.0286 26.4959 20 7 9 -4 20.1611 28.8754 15 7 9 -3 1969.20 151.003 16 7 9 -3 1881.57 132.384 15 7 9 -2 35235.8 696.476 16 7 9 -2 34337.8 635.701 15 7 9 -1 3132.15 210.000 16 7 9 -1 3285.51 199.948 15 7 9 0 46.9649 52.7220 16 7 9 0 27.1065 53.7217 15 7 9 1-3.52124 49.9503 16 7 9 1-25.9489 48.2820 15 7 9 2 7603.30 338.328 16 7 9 2 7232.71 308.163 15 7 9 3 1821.06 171.157 16 7 9 3 1638.21 147.531 15 7 9 4 1679.80 155.583 16 7 9 4 1759.53 150.382 15 7 9 4 1613.17 152.631 12 7 9 5 8781.49 345.563 16 7 9 5 8791.47 317.864 15 7 9 5 8930.77 345.327 12 7 9 6 982.907 110.554 16 7 9 6 1139.10 109.815 15 7 9 6 1173.46 123.158 12 7 9 7 6121.41 255.931 16 7 9 7 6150.91 229.238 15 7 9 7 6848.80 279.020 12 7 9 8 15.1252 31.0072 16 7 9 8 26.5824 37.0788 12 7 9 9-38.7926 29.9053 12 7 9 10-11.9347 21.5609 12 7 10 -3 1466.08 97.3061 16 7 10 -3 1402.74 86.5815 15 7 10 -2 6260.58 225.790 16 7 10 -2 5793.46 206.312 15 7 10 -1 695.112 85.4959 16 7 10 -1 734.825 81.4132 15 7 10 0 7801.65 284.411 16 7 10 0 7895.97 268.157 15 7 10 1 130.447 49.2605 16 7 10 1 87.7520 44.9711 15 7 10 2 2245.80 163.009 16 7 10 2 2071.38 145.199 15 7 10 3 6009.02 264.407 16 7 10 3 6045.65 240.627 15 7 10 4 4074.30 209.294 16 7 10 4 3780.52 183.778 15 7 10 5 1161.27 112.346 16 7 10 5 1219.88 99.8589 15 7 10 6 9105.67 292.172 16 7 10 6 8046.10 231.907 15 7 10 7-39.7849 36.9641 16 7 10 8 750.975 70.3786 16 7 11 0 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530.292 7 -8 3 3 12386.0 428.158 11 -8 3 2 9423.07 375.830 11 8 -3 -2 9189.62 407.139 5 -8 3 1 1541.12 155.991 11 8 -3 -1 1664.71 173.465 5 -8 3 0 16043.3 499.453 11 8 -3 0 14851.6 414.869 17 8 -3 0 15147.1 512.097 5 -8 3 -1 20887.0 569.518 11 8 -3 1 19176.9 577.521 5 -8 3 -2 8284.44 347.994 11 8 -3 2 7625.42 349.819 5 -8 3 -3 36539.6 751.427 11 8 -3 3 34680.5 736.180 5 -8 3 -4 722.136 105.767 11 8 -3 4 519.055 85.6264 5 -8 3 -5 7375.79 298.408 11 8 -3 5 6890.42 275.092 5 -8 3 -6 3418.02 187.278 11 8 -3 6 2921.09 158.032 5 -8 3 -7 1075.58 96.8749 11 8 -3 7 822.185 68.0394 5 -8 3 -8 1363.97 89.9055 11 -8 2 10 617.580 63.5315 7 -8 2 9 247.243 42.9519 22 -8 2 9 177.339 43.6469 7 -8 2 8 775.060 87.6004 11 -8 2 8 1034.69 109.123 7 -8 2 7 601.196 89.5836 7 -8 2 7 674.991 89.0363 11 -8 2 7 516.738 70.5839 6 -8 2 6 13808.7 427.242 11 -8 2 6 14637.3 458.971 7 -8 2 5 784.113 117.163 7 -8 2 5 764.863 108.397 11 -8 2 4 13888.4 457.337 11 -8 2 3 755.757 120.326 11 -8 2 2 73.5920 57.7181 11 8 -2 -2 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6186.75 283.596 11 8 1 8 6928.69 323.145 18 -8 -1 -9 410.422 73.6791 11 8 1 9 378.563 76.1671 18 -8 -1 -10 316.628 55.5827 11 8 1 10 378.091 65.4814 18 -8 -1 -11 1540.10 93.3025 11 8 1 11 1852.34 116.102 18 -8 -2 10 74.6034 31.8560 6 -8 -2 9 5875.13 242.207 6 -8 -2 9 4980.25 195.091 7 -8 -2 8 3008.18 194.763 6 -8 -2 8 2738.17 166.791 7 8 2 -7 123.688 51.4265 17 -8 -2 7 141.779 67.9573 6 -8 -2 7 260.363 61.8383 7 8 2 -6 7562.09 331.407 17 -8 -2 6 8818.01 349.263 7 8 2 -5 1365.70 153.814 17 -8 -2 5 1407.37 150.832 7 8 2 -4 11199.1 434.896 17 -8 -2 4 11400.8 432.972 7 8 2 -3 6860.59 346.752 17 8 2 -2 2102.29 194.254 17 8 2 -1 15618.9 539.966 17 8 2 0 251.767 81.6817 17 8 2 1 787.900 126.835 17 8 2 2 16977.9 619.792 18 8 2 2 16782.9 562.853 17 8 2 3 1672.97 194.859 18 -8 -2 -4 1593.42 152.349 11 8 2 4 1755.69 199.056 18 -8 -2 -5 9397.58 373.379 11 8 2 5 11307.3 476.689 18 -8 -2 -6 101.481 60.6542 11 8 2 6 87.7426 62.8761 18 -8 -2 -7 5763.20 279.749 11 8 2 7 6549.91 339.816 18 -8 -2 -8 1615.05 148.923 11 8 2 8 1761.57 169.911 18 8 2 8 1862.64 132.090 12 -8 -2 -9 2110.15 148.404 11 8 2 9 2461.74 182.029 18 8 2 9 2239.27 135.595 12 8 2 10 2941.71 180.333 18 8 2 10 2767.28 133.670 12 8 2 11 6954.18 242.085 18 -8 -3 10 3787.80 154.288 6 -8 -3 9 6236.63 241.673 6 -8 -3 8 1228.54 123.648 6 -8 -3 7 1573.43 149.795 6 -8 -3 7 1324.68 111.382 7 8 3 -6 11809.3 421.449 17 -8 -3 6 12310.8 377.177 7 -8 -3 5 430.186 78.9120 7 8 3 -5 522.908 98.9465 17 8 3 -4 19471.5 591.293 17 -8 -3 4 19178.1 527.670 7 8 3 -3 1278.49 157.336 17 8 3 -2 610.852 116.278 17 8 3 -2 717.225 104.614 15 8 3 -1 57.7507 67.6103 17 8 3 -1 78.0965 48.1269 15 8 3 0 361.578 93.6146 17 8 3 1 476.719 105.694 17 8 3 2-3.82004 68.3717 18 8 3 2 59.9762 65.5561 17 8 3 3 3033.40 252.882 18 8 3 3 3195.25 237.894 17 8 3 4 74.1647 59.4650 18 8 3 4 80.8771 61.2232 17 8 3 5 3978.63 279.840 18 8 3 5 3478.31 209.146 12 8 3 6 256.846 62.2344 12 8 3 6 375.021 99.0788 18 8 3 7 7781.77 368.192 18 8 3 7 7447.91 299.928 12 8 3 8-13.8563 39.3032 12 8 3 8-10.1906 44.2240 18 8 3 9 519.814 72.2280 12 8 3 9 616.775 99.0755 18 8 3 9 525.386 72.7988 17 8 3 10 140.634 39.5134 12 8 3 10 140.640 46.4139 18 8 3 11 1724.53 118.717 18 8 3 11 1728.79 100.676 12 -8 -4 9 39.9016 32.0272 6 -8 -4 8 174.488 49.9594 6 -8 -4 7 3465.69 208.148 6 8 4 -6 1834.94 166.705 17 -8 -4 6 2196.59 179.657 6 8 4 -5 5708.04 306.597 17 8 4 -4 114.867 57.6005 17 8 4 -3 13919.4 501.650 17 8 4 -2 1687.96 179.043 17 8 4 -2 1741.38 162.458 15 8 4 -1 786.433 129.278 17 8 4 -1 690.550 110.754 15 8 4 0 563.476 106.700 17 8 4 0 604.536 97.8477 15 8 4 1 575.175 104.789 17 8 4 2 1.36608 51.6706 17 8 4 2 3.16752 34.8943 12 8 4 3 9859.86 443.725 18 8 4 3 9925.95 406.474 17 8 4 3 9574.22 365.827 12 8 4 4 6829.29 368.805 18 8 4 4 7347.18 341.320 17 8 4 4 6882.26 309.966 12 8 4 5 22045.6 594.112 17 8 4 5 20920.0 553.988 12 8 4 6 1654.09 175.271 18 8 4 6 1602.93 149.696 17 8 4 6 1510.51 145.231 12 8 4 7 1633.79 164.504 18 8 4 7 1499.67 140.942 17 8 4 7 1662.13 147.832 12 8 4 8 2625.43 196.941 18 8 4 8 2476.28 160.391 17 8 4 8 2753.21 181.498 12 8 4 9 2695.32 181.319 18 8 4 9 2749.93 168.352 12 8 4 10 1535.57 125.022 18 8 4 10 1566.05 115.143 12 8 4 11 2390.24 131.282 18 8 4 11 2683.78 133.333 12 -8 -5 8 3939.30 177.043 6 -8 -5 7 5816.05 242.231 6 -8 -5 6 299.723 70.2928 6 8 5 -5 367.564 91.8051 17 -8 -5 5 341.763 77.4634 6 8 5 -4 1298.31 151.776 17 8 5 -3 2079.80 194.453 17 8 5 -3 1909.83 153.766 15 8 5 -2-8.56194 54.0269 17 8 5 -2-26.7578 42.5773 15 8 5 -1 4422.39 292.878 16 8 5 -1 5046.74 277.845 15 8 5 0 1180.51 149.228 17 8 5 0 916.147 126.773 16 8 5 0 1009.56 134.076 15 8 5 1 15529.5 511.977 17 8 5 1 13879.6 470.060 16 8 5 1 15362.1 499.664 15 8 5 1 14106.4 453.925 12 8 5 2-63.7983 60.9254 17 8 5 2-31.8471 50.9392 15 8 5 2-12.8893 38.0102 12 8 5 3 3596.51 236.097 17 8 5 3 3313.03 220.914 12 8 5 4 8578.79 355.742 17 8 5 4 8063.79 343.997 12 8 5 5 355.281 81.0866 12 8 5 5 375.763 88.0451 18 8 5 5 341.959 74.6264 17 8 5 6 20646.2 570.146 18 8 5 6 20304.6 513.991 17 8 5 6 21409.9 553.159 12 8 5 7 35581.0 738.946 18 8 5 7 36447.1 659.460 17 8 5 8 1079.42 116.869 18 8 5 8 1410.02 132.227 12 8 5 9 2184.51 149.867 18 8 5 9 2614.91 166.385 12 8 5 10 747.700 74.8242 18 8 5 10 886.625 78.8509 15 8 5 10 876.618 89.6801 12 8 5 11 1342.89 94.9354 12 8 6 -8 4778.48 174.604 16 8 6 -7 219.731 50.7190 16 -8 -6 7 188.237 37.2829 6 -8 -6 6 21565.0 445.926 6 -8 -6 5 6945.05 263.681 6 8 6 -4 1116.38 135.804 17 -8 -6 4 1288.45 123.884 6 -8 -6 3 173.964 52.0845 6 8 6 -3 173.107 52.1192 15 8 6 -2 72.7633 69.9718 17 8 6 -2 125.628 66.8398 16 8 6 -2 140.958 58.9657 15 8 6 -1 1832.35 182.596 17 8 6 -1 1557.36 169.757 16 8 6 -1 2032.88 171.818 15 8 6 0 1412.59 154.167 17 8 6 0 1343.82 149.543 16 8 6 0 1391.46 149.588 15 8 6 1 7317.99 333.494 17 8 6 1 6829.97 329.358 16 8 6 1 7331.41 334.841 15 8 6 1 6951.26 319.322 12 8 6 2 32916.1 718.879 17 8 6 2 30106.6 692.765 16 8 6 2 33368.6 736.017 15 8 6 2 31191.2 700.029 12 8 6 3 18392.9 511.676 17 8 6 3 18178.3 537.826 15 8 6 3 17453.1 514.710 12 8 6 4 2.53691 32.3435 17 8 6 4 89.3343 59.2834 15 8 6 4-14.7440 45.9932 12 8 6 5 7271.88 291.489 17 8 6 5 8441.79 346.282 15 8 6 5 8034.96 339.148 12 8 6 6 1353.98 135.969 15 8 6 6 1333.22 137.030 12 8 6 7 4897.57 243.717 15 8 6 7 4873.22 250.205 12 8 6 8 97.8162 49.2029 12 8 6 8 96.9870 41.1433 15 8 6 9 8809.86 270.304 15 8 6 9 9738.42 313.229 12 8 6 10 10.5477 26.6965 12 8 6 11 375.997 50.9485 12 8 7 -7 25.6977 20.1446 16 8 7 -6-12.0060 32.2276 16 8 7 -5 458.162 74.1715 16 8 7 -4 6556.47 282.540 16 8 7 -4 5763.10 201.939 15 8 7 -3 2185.19 178.682 16 8 7 -3 1936.26 136.937 15 8 7 -2 1136.28 130.142 17 8 7 -2 1405.27 147.247 16 8 7 -2 1217.78 122.344 15 8 7 -1 4059.19 238.157 17 8 7 -1 4025.73 244.198 16 8 7 -1 4228.44 231.506 15 8 7 0 86.0524 46.6509 17 8 7 0 118.029 61.2747 16 8 7 0 9.33057 47.7776 15 8 7 1 7073.56 305.961 17 8 7 1 6802.10 321.585 16 8 7 2 663.723 94.2755 17 8 7 2 724.725 102.235 16 8 7 2 702.200 117.275 15 8 7 2 646.987 98.2017 12 8 7 3 2376.16 168.215 17 8 7 3 2236.40 174.659 16 8 7 3 2621.22 195.463 15 8 7 3 2701.68 197.065 12 8 7 4 10529.6 337.872 17 8 7 4 9681.49 347.142 16 8 7 4 11373.6 398.107 15 8 7 4 12055.8 408.646 12 8 7 5 12932.7 410.893 15 8 7 5 13003.5 417.081 12 8 7 6 2322.46 165.998 15 8 7 6 2420.51 175.396 12 8 7 7 21.4534 42.2003 15 8 7 7 40.6704 42.3424 12 8 7 8 9380.82 287.952 15 8 7 8 10495.0 329.899 12 8 7 9 2730.93 128.812 15 8 7 9 3224.99 170.162 12 8 7 10 16435.2 350.312 12 8 8 -5 3961.39 166.032 16 8 8 -4 396.904 61.6190 16 8 8 -3 70.1094 39.3847 16 8 8 -3 64.9144 28.4319 15 8 8 -2 77.9467 54.0973 16 8 8 -2 44.8892 40.3791 15 8 8 -1 5602.85 264.855 16 8 8 -1 5613.32 240.533 15 8 8 0 882.823 97.4693 17 8 8 0 968.182 115.577 16 8 8 0 927.676 107.087 15 8 8 1-32.6087 36.6291 17 8 8 1-37.9017 44.7479 16 8 8 1-27.0391 58.4137 15 8 8 2 2152.01 146.611 17 8 8 2 2587.85 180.868 16 8 8 2 2771.21 187.073 15 8 8 3 6420.69 278.874 16 8 8 3 7303.44 300.402 15 8 8 4 16848.8 447.251 15 8 8 4 17021.7 460.414 12 8 8 5 993.923 99.8008 16 8 8 5 1108.95 112.100 15 8 8 5 1163.60 118.475 12 8 8 6 3614.29 187.016 15 8 8 6 3816.83 202.158 12 8 8 7 137.506 41.5709 15 8 8 7 135.445 42.7510 12 8 8 8 5315.80 179.325 15 8 8 8 6238.83 232.094 12 8 8 9 13812.5 317.806 12 8 8 10 7179.20 190.493 12 8 9 -3 287.942 48.3453 16 8 9 -2 17471.4 380.477 16 8 9 -2 16050.4 325.417 15 8 9 -1 1979.48 134.502 16 8 9 -1 1938.32 123.970 15 8 9 0 2208.80 146.481 16 8 9 0 2130.22 135.889 15 8 9 1 4587.05 214.085 16 8 9 1 4965.08 210.861 15 8 9 2 102.655 34.9092 16 8 9 2 145.522 53.8934 15 8 9 3 2815.80 164.431 16 8 9 3 3015.70 165.703 15 8 9 4 240.261 49.2625 16 8 9 4 277.558 51.9443 15 8 9 5 7570.39 241.158 16 8 9 5 8437.51 259.469 15 8 9 6 12344.2 273.322 16 8 9 6 12603.0 295.626 15 8 9 7 790.765 62.0820 15 8 9 7 826.435 78.2594 12 8 9 8 3916.77 151.969 12 8 10 0 2647.05 122.113 16 8 10 0 2693.44 115.635 15 8 10 1 57.8775 26.0993 16 8 10 1 88.1526 28.8496 15 8 10 2 1128.80 85.2038 16 8 10 2 1270.92 87.7749 15 8 10 3 4565.41 168.670 16 8 10 3 5072.88 170.489 15 8 10 4 271.560 40.5573 16 8 10 4 231.754 37.3066 15 -9 4 4 2978.92 122.544 11 -9 4 3 620.938 61.6483 11 -9 4 2 2609.41 128.681 11 -9 4 1-27.0527 25.8038 11 -9 4 0 2902.90 134.289 11 -9 4 -1 288.553 44.5766 11 -9 4 -2 5619.14 170.801 11 -9 3 5-3.89389 20.6542 11 -9 3 5 54.4753 25.4780 7 -9 3 4 691.639 73.7212 11 -9 3 4 749.578 73.9665 7 -9 3 3 88.6189 33.0466 7 -9 3 3 71.8994 35.3917 11 -9 3 2 1254.29 105.954 11 -9 3 2 1141.23 97.8297 7 -9 3 1-15.1703 34.0748 11 -9 3 0 706.051 80.6181 11 -9 3 -1 851.859 88.3047 11 -9 3 -2 172.105 41.7111 11 -9 3 -3 111.184 33.1848 11 -9 3 -4 848.408 73.7522 11 -9 2 7 167.160 33.9748 7 -9 2 6 1969.77 106.125 11 -9 2 6 2132.40 126.587 7 -9 2 5 3983.78 171.709 11 -9 2 5 4546.86 199.889 7 -9 2 4 1934.88 128.305 11 -9 2 4 2051.53 141.971 7 -9 2 3 2023.35 139.542 11 -9 2 3 2086.25 148.640 7 -9 2 2 287.212 59.8007 11 -9 2 1 353.815 66.7618 11 -9 2 0 758.949 90.2785 11 9 -2 0 736.817 76.7162 17 -9 2 -1 6479.28 260.064 11 9 -2 1 5915.55 224.080 17 -9 2 -2 785.139 95.6467 11 9 -2 2 787.926 82.4240 17 -9 2 -3 49.5741 36.7814 11 9 -2 3 77.7678 37.7629 17 -9 2 -4 3529.63 177.230 11 9 -2 4 3462.08 162.574 17 -9 2 -5 7006.09 229.802 11 9 -2 5 6994.39 218.217 17 -9 2 -6 10066.1 245.343 11 9 -2 6 10100.5 237.290 17 -9 1 8-15.5047 16.5281 7 -9 1 7 23.7263 26.8164 7 -9 1 6 395.139 63.5179 7 -9 1 6 284.387 40.2477 11 -9 1 6 302.106 47.8020 6 -9 1 5 93.8349 45.2051 7 -9 1 5 110.329 30.1852 11 -9 1 4 50.5802 40.9977 7 -9 1 4-3.23936 30.6101 11 -9 1 3 24.0356 52.8940 7 -9 1 3 55.6489 36.8995 11 -9 1 2 1132.54 111.295 11 9 -1 -2 1274.54 107.309 17 -9 1 1 181.343 51.9374 11 9 -1 -1 183.621 45.9624 17 -9 1 0 3726.25 205.352 11 9 -1 0 3817.44 204.342 17 -9 1 -1 776.371 97.9017 11 9 -1 1 702.270 97.7500 17 -9 1 -2 2659.49 174.535 11 9 -1 2 2649.10 174.609 17 -9 1 -3 9768.77 329.561 11 9 -1 3 9713.41 324.499 17 -9 1 -4 3046.25 177.304 11 -9 1 -5 5496.72 224.161 11 -9 1 -6 22.4957 30.5093 11 -9 1 -7 8537.81 227.594 11 9 -1 7 9514.42 245.758 17 -9 0 8 2282.05 113.359 7 -9 0 7 8.45862 22.4096 6 -9 0 7 37.6559 26.0186 7 -9 0 6 462.831 73.5001 7 -9 0 6 311.043 53.0771 6 -9 0 5 4584.06 226.902 7 -9 0 4 25.8654 41.4788 7 9 0 -4 8.96857 23.6277 17 -9 0 3 125.978 44.9698 11 9 0 -3 155.393 48.6971 17 -9 0 2 989.996 99.4303 11 9 0 -2 1132.63 115.212 17 -9 0 1 725.850 90.6465 11 9 0 -1 762.206 98.4168 17 -9 0 0 1143.89 113.902 11 9 0 0 1130.22 123.167 17 -9 0 -1 11579.2 368.325 11 9 0 1 12320.3 403.142 17 -9 0 -2 1463.36 130.798 11 9 0 2 1707.09 152.855 17 -9 0 -3 26258.6 562.780 11 9 0 3 27345.7 606.285 17 -9 0 -4 9485.80 318.891 11 -9 0 -5 19383.1 445.273 11 9 0 5 19594.7 505.847 18 -9 0 -6 209.696 52.3869 11 9 0 6 91.1167 47.4777 18 -9 0 -7 844.516 78.9117 11 9 0 7 907.239 91.9133 18 9 0 8 749.857 71.7442 18 9 0 8 820.306 70.7416 17 -9 -1 8 401.921 47.3707 6 -9 -1 7 1041.88 94.7816 6 -9 -1 7 946.281 84.7285 7 -9 -1 6-71.5907 54.1926 6 -9 -1 6-12.8577 34.0093 7 9 1 -5 972.186 91.7828 17 -9 -1 5 1054.95 111.496 7 -9 -1 4 32.2591 41.1768 7 9 1 -4 8.28064 31.0179 17 9 1 -3 15665.5 437.155 17 -9 -1 3 15775.0 463.465 7 9 1 -2 77.2199 45.5795 17 9 1 -1 4788.26 255.054 17 9 1 0 1401.43 142.522 17 -9 -1 -1 8624.97 301.869 11 9 1 1 8966.07 360.148 17 -9 -1 -2 10332.9 335.510 11 9 1 2 10605.9 389.884 17 -9 -1 -3 1698.73 134.635 11 9 1 3 1951.37 166.372 17 -9 -1 -4 7232.29 271.838 11 9 1 4 7445.09 344.650 18 9 1 4 7749.57 321.750 17 -9 -1 -5 67.0777 37.1591 11 9 1 5 105.936 58.5306 18 9 1 5 109.129 63.1417 17 -9 -1 -6 1.42078 30.0830 11 9 1 6 26.4412 41.2786 18 9 1 7 5912.34 253.503 18 9 1 7 5522.95 222.548 17 9 1 8 9017.15 282.871 18 9 1 8 8202.51 241.583 17 9 1 9 264.817 41.3523 18 -9 -2 8 4200.40 158.105 6 -9 -2 7 369.685 59.0246 6 -9 -2 7 279.651 41.6060 7 -9 -2 6-73.6140 50.3056 6 -9 -2 6 22.7738 22.0079 7 9 2 -5 2604.72 160.253 17 -9 -2 5 2766.76 163.333 7 9 2 -4 589.707 86.3584 17 -9 -2 4 673.969 92.2886 7 -9 -2 3 349.741 73.2301 7 9 2 -3 382.418 75.2181 17 9 2 -2 9.11174 47.9093 17 9 2 -1 8685.76 354.743 17 9 2 0 5280.87 281.930 17 9 2 1 5342.79 283.143 17 9 2 2 7738.68 341.330 17 9 2 3 2202.64 175.088 17 9 2 4 68.4414 51.5574 18 9 2 4 168.480 63.4278 17 9 2 5-29.0863 45.8606 18 9 2 5-16.1866 43.1541 17 9 2 6 10084.9 373.267 18 9 2 6 10799.9 343.701 17 9 2 7 357.866 73.2039 18 9 2 7 394.795 67.6316 17 9 2 8-27.7207 28.8774 18 9 2 8 57.3514 30.4871 17 9 2 9 4607.39 183.568 18 -9 -3 8 3.54324 18.6673 6 -9 -3 7 1246.57 100.650 6 -9 -3 6 7466.87 272.539 6 9 3 -5 0.72701 32.7139 17 -9 -3 5 86.8351 28.8756 7 9 3 -4 10063.2 351.441 17 -9 -3 4 9474.31 292.769 7 9 3 -3 10960.1 384.679 17 -9 -3 3 9912.93 322.098 7 9 3 -2 650.785 102.706 17 -9 -3 2 699.160 95.8390 7 9 3 -1 5902.36 293.384 17 9 3 -1 5900.64 247.264 15 9 3 0 9112.01 372.700 17 9 3 0 8664.60 320.043 15 9 3 1 8971.12 364.021 17 9 3 2 1317.15 142.931 17 9 3 3 8610.34 346.921 17 9 3 4 5518.29 271.459 17 9 3 5-9.25619 44.8160 18 9 3 5 10.0863 37.3852 17 9 3 6 4103.81 232.875 18 9 3 6 4000.29 207.686 17 9 3 7 2456.10 171.829 18 9 3 7 2517.77 150.146 17 9 3 8 2139.67 145.850 18 9 3 8 1980.12 115.342 17 9 3 9 241.125 44.6054 18 -9 -4 7 649.765 65.2420 6 -9 -4 6 6545.61 234.942 6 9 4 -6 5542.36 197.891 16 9 4 -5 1473.04 125.158 17 -9 -4 5 1607.68 129.377 6 9 4 -5 1257.53 99.5549 16 9 4 -4 172.309 51.4912 17 9 4 -4 85.7818 38.2980 16 9 4 -3 159.489 54.9348 17 9 4 -3 135.735 39.0860 16 9 4 -2 1040.21 125.460 17 9 4 -1 4844.34 263.002 17 9 4 -1 4738.32 223.105 15 9 4 0 20650.2 549.997 17 9 4 0 20509.9 499.666 15 9 4 1 1025.35 132.133 17 9 4 1 959.965 117.118 15 9 4 2 1360.39 138.751 17 9 4 2 1382.78 134.017 15 9 4 3 1620.10 146.610 17 9 4 4 69.3316 45.5326 17 9 4 5 6359.62 266.398 17 9 4 6 48.8131 28.7902 17 9 4 7 143.846 41.6211 17 9 4 8 1566.09 90.6719 17 9 4 9 519.617 54.2358 15 -9 -5 6 989.046 76.0608 6 9 5 -6 880.915 72.7624 16 -9 -5 5 884.535 84.3391 6 9 5 -5 832.429 79.5820 16 9 5 -4 13070.0 379.986 17 -9 -5 4 12328.9 340.220 6 -9 -5 3 6768.34 262.771 6 9 5 -3 6110.58 240.233 16 9 5 -2 4780.81 249.136 17 9 5 -2 4036.22 197.240 16 9 5 -2 4679.84 195.070 15 9 5 -1 316.572 79.8540 17 9 5 -1 356.209 64.3692 15 9 5 0 7852.60 321.783 17 9 5 0 7647.37 294.606 15 9 5 1 7111.60 305.366 17 9 5 1 7289.65 293.825 15 9 5 2 2360.93 176.990 17 9 5 2 2704.75 179.802 15 9 5 3 5731.14 264.629 17 9 5 3 6267.69 274.732 15 9 5 4 515.021 78.4287 17 9 5 4 455.710 79.4818 15 9 5 4 283.293 52.5976 12 9 5 5 1543.00 120.685 17 9 5 5 1680.66 137.945 15 9 5 5 1429.60 108.381 12 9 5 6 32.5742 28.9872 17 9 5 6-8.69942 40.8495 15 9 5 6-18.5347 25.5947 12 9 5 7 9317.52 238.125 17 9 5 7 8896.20 248.551 12 9 5 8 131.058 36.5184 15 9 5 8 177.823 35.4208 12 9 5 9 1858.07 92.1723 15 9 6 -5 1913.00 107.152 16 -9 -6 4 1257.01 81.6992 6 9 6 -4 1190.10 94.3908 16 9 6 -3 9066.57 307.726 17 -9 -6 3 8470.85 237.861 6 9 6 -3 8368.44 266.371 16 9 6 -2 6040.86 261.914 17 -9 -6 2 5538.52 202.076 6 9 6 -2 5316.40 218.225 16 9 6 -2 5627.61 199.950 15 9 6 -1 684.239 109.446 17 9 6 -1 448.815 78.5758 16 9 6 -1 660.104 91.8952 15 -9 -6 1 429.631 63.9518 6 9 6 0 4611.90 231.101 17 9 6 0 4505.72 213.951 15 9 6 1 11957.8 372.657 17 9 6 1 12016.0 365.932 15 9 6 2 114.690 49.1789 17 9 6 2 82.6277 51.4687 15 9 6 3 5023.54 224.446 17 9 6 3 5673.44 249.121 15 9 6 4 273.105 53.4908 17 9 6 4 267.041 50.4655 12 9 6 5 188.952 41.5072 17 9 6 5 179.795 55.7516 15 9 6 5 98.7824 36.9984 12 9 6 6 2672.38 154.397 15 9 6 6 2245.70 131.477 12 9 6 7 157.027 39.1630 15 9 6 7 132.563 31.7868 12 9 6 8 2268.71 114.531 15 9 6 8 2163.05 106.492 12 9 7 -3 1031.33 81.6571 16 9 7 -2 482.055 62.9452 16 9 7 -2 425.076 50.1534 15 9 7 -1 1615.82 124.765 17 9 7 -1 1474.65 108.412 16 9 7 -1 1525.90 106.319 15 9 7 0 1053.81 101.680 17 9 7 0 903.753 83.6748 16 9 7 0 1233.18 102.326 15 9 7 1 21.3525 27.6844 17 9 7 1 62.4410 27.8423 16 9 7 1 17.1184 30.4909 15 9 7 2 101.324 34.9078 17 9 7 2 102.729 43.7539 15 9 7 3 1071.76 89.5724 17 9 7 3 1341.81 115.900 15 9 7 4 398.162 68.4154 15 9 7 5 977.672 90.9684 15 9 7 6 35.6429 29.2434 15 9 7 6 60.3182 26.5705 12 9 7 7 1398.92 91.4086 15 9 7 7 1366.40 88.0796 12 9 8 -1 4811.23 160.331 16 9 8 0 498.945 52.0900 16 9 8 0 612.636 63.7428 15 9 8 1 699.162 61.7476 16 9 8 1 819.433 78.5023 15 9 8 2 1752.81 112.023 15 9 8 3 332.790 54.2892 15 9 8 4 2633.82 135.081 15 9 8 5 2198.86 116.083 15 9 8 6 4619.69 151.007 15 -10 1 2 3243.89 135.638 7 -10 1 1 25.1909 19.8824 7 -10 1 0 104.514 29.0279 7 -10 0 3 1797.93 103.918 7 -10 0 2 1091.25 87.1929 7 -10 0 1 648.147 71.2297 7 10 0 0 210.591 37.1368 17 10 0 1 201.789 37.3464 17 10 0 2 761.209 67.3399 17 10 0 3 420.422 49.7457 17 10 0 4 3772.87 135.252 17 -10 -1 4 90.4797 25.4774 6 -10 -1 3 129.764 31.7479 7 -10 -1 2 43.2603 28.0266 7 10 1 -2-5.64941 19.0217 17 -10 -1 1 160.266 39.1829 7 10 1 -1 168.842 35.1557 17 10 1 0 43.4893 26.6593 17 10 1 1 122.086 36.5438 17 10 1 2 2494.48 136.203 17 10 1 3 2649.55 137.306 17 10 1 3 2874.24 117.144 15 10 1 4 453.589 55.7396 17 10 1 5 1635.15 92.3817 17 -10 -2 4 3785.73 154.690 6 10 2 -3 1432.34 89.2610 17 -10 -2 2 11.4693 19.0630 7 10 2 -2-6.79627 21.2532 17 -10 -2 1 252.486 47.5574 7 10 2 -1 279.987 49.4106 17 -10 -2 0 20.0395 24.5497 7 10 2 0 80.5767 38.8471 17 10 2 1 142.223 41.5744 17 10 2 2 3943.23 181.228 17 10 2 2 4002.85 151.004 15 10 2 3 762.912 79.0220 17 10 2 3 708.502 64.4177 15 10 2 4 177.977 37.5855 17 10 2 4 213.144 36.9746 15 10 2 5 1239.79 86.3443 17 10 2 5 1285.30 82.4269 15 -10 -3 4 848.990 70.4533 6 10 3 -3 294.329 43.8837 17 -10 -3 3 298.791 50.9194 6 10 3 -2 520.729 65.7081 17 10 3 -1 347.522 59.4162 17 10 3 0 744.175 82.2340 17 -10 -3 0 459.903 52.2437 7 -10 -3 -1 35.3741 29.1589 7 10 3 1 11.2636 28.2526 17 10 3 1 13.0778 20.3004 15 10 3 2 1909.50 127.371 17 10 3 2 1858.20 108.449 15 10 3 3 60.3143 36.0338 17 10 3 3-12.8394 25.8875 15 10 3 4 15598.2 344.290 17 10 3 4 15775.2 329.606 15 10 3 5 1703.86 100.390 17 10 3 5 1774.78 102.038 15 10 3 6 9411.18 217.964 15 10 4 -3 243.166 40.8394 17 -10 -4 3 257.547 39.0945 6 10 4 -2 3726.20 164.694 17 -10 -4 2 3419.80 147.360 6 10 4 -1 1034.05 93.0302 17 10 4 0 598.469 74.6136 17 10 4 1 9526.85 284.792 17 10 4 1 9122.63 231.926 15 10 4 2 2667.22 147.597 17 10 4 2 2664.88 130.847 15 10 4 3 6473.16 220.665 17 10 4 3 6369.07 206.807 15 10 4 4 3751.51 156.574 17 10 4 4 3693.16 154.529 15 10 4 5 913.185 69.0634 17 10 4 5 1004.03 76.9047 15 10 4 6 834.037 63.8629 15 10 5 -2 1625.91 98.7495 17 10 5 -1 76.0695 31.7033 17 10 5 0 311.077 61.8030 17 10 5 1 15114.7 339.777 17 10 5 1 14200.0 283.479 15 10 5 2 2393.69 128.954 17 10 5 2 2274.18 116.046 15 10 5 3 12196.6 284.836 17 10 5 3 12636.0 285.988 15 10 5 4 1888.45 98.9381 17 10 5 4 2141.57 113.171 15 10 5 5 2774.38 121.558 15 10 6 0 1305.64 83.6661 17 10 6 1 7398.54 200.854 17 10 6 3 2660.47 114.410 15 10 6 4 873.790 64.6493 15 0 0 0 0.00 0.00 0 TITL tctca in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 8.330610 10.440330 14.036088 78.4056 87.3574 78.6082 ZERR 4.00 0.000482 0.000464 0.000545 0.0035 0.0041 0.0044 LATT 1 SFAC C H N O S Cl UNIT 36.00 40.00 20.00 8.00 4.00 4.00 TREF HKLF 4 END ; _shelx_hkl_checksum 22372 _shelx_res_file ; TITL shelxt_a.res in P-1 shelx.res created by SHELXL-2016/6 at 19:23:16 on 11-Mar-2017 CELL 1.54184 8.3306 10.4403 14.0361 78.406 87.357 78.608 ZERR 4.00 0.0005 0.0005 0.0005 0.004 0.004 0.004 LATT 1 SFAC C H N O S CL UNIT 36 40 20 8 4 4 MERG 2 SIZE 0.12 0.15 0.36 ACTA 135.00 L.S. 10 TEMP -153.00 WGHT 0.059700 0.734400 FVAR 4.71378 CL1 6 0.970918 0.929576 1.148322 11.00000 0.05267 0.03015 = 0.03448 -0.01227 -0.00059 -0.02005 S1 5 0.847260 0.794814 1.006263 11.00000 0.03209 0.02231 = 0.02125 -0.00517 0.00240 -0.01014 O1A 4 0.741891 0.627143 0.882371 11.00000 0.02957 0.02613 = 0.02107 -0.00290 -0.00087 -0.00924 O2A 4 0.724121 0.451432 1.000783 11.00000 0.03737 0.02469 = 0.02093 -0.00411 -0.00157 -0.01321 C11A 1 0.754142 0.567004 0.969136 11.00000 0.01988 0.02260 = 0.02127 -0.00538 0.00107 -0.00449 C7A 1 0.809479 0.635126 1.041921 11.00000 0.02008 0.02203 = 0.02277 -0.00549 -0.00012 -0.00384 C8A 1 0.842645 0.587683 1.138532 11.00000 0.03987 0.02128 = 0.02752 -0.00290 -0.00677 -0.00815 AFIX 43 H8A 2 0.828531 0.501787 1.171564 11.00000 -1.20000 AFIX 0 C9A 1 0.899879 0.678484 1.184573 11.00000 0.03962 0.02700 = 0.02752 -0.00686 -0.00726 -0.00681 AFIX 43 H9A 2 0.928577 0.661076 1.251303 11.00000 -1.20000 AFIX 0 C10A 1 0.908575 0.793386 1.121451 11.00000 0.02394 0.02527 = 0.02886 -0.01063 0.00009 -0.00634 CL2 6 -0.315922 0.449092 0.452437 11.00000 0.01694 0.03241 = 0.05821 -0.01911 -0.00569 0.00100 S2 5 0.039867 0.386732 0.404893 11.00000 0.01766 0.02000 = 0.02549 -0.00501 -0.00296 -0.00281 O1B 4 0.392697 0.287118 0.376493 11.00000 0.01727 0.03157 = 0.02104 0.00044 0.00067 -0.00341 O2B 4 0.443172 0.167243 0.526499 11.00000 0.01806 0.02922 = 0.02063 -0.00097 -0.00100 -0.00092 C11B 1 0.350005 0.241980 0.462447 11.00000 0.01749 0.02073 = 0.02064 -0.00588 -0.00014 -0.00532 C7B 1 0.174330 0.279718 0.488175 11.00000 0.01741 0.01777 = 0.02303 -0.00604 0.00055 -0.00391 C8B 1 0.095244 0.233870 0.572011 11.00000 0.02204 0.02265 = 0.02394 -0.00691 0.00266 -0.00508 AFIX 43 H8B 2 0.149814 0.174212 0.626188 11.00000 -1.20000 AFIX 0 C9B 1 -0.075216 0.283758 0.570233 11.00000 0.02167 0.02570 = 0.03247 -0.01204 0.00725 -0.00656 AFIX 43 H9B 2 -0.148465 0.261771 0.622115 11.00000 -1.20000 AFIX 0 C10B 1 -0.120322 0.367268 0.484524 11.00000 0.01611 0.02120 = 0.03984 -0.01452 0.00002 -0.00349 N1A 3 0.636882 0.293867 0.885826 11.00000 0.02319 0.01949 = 0.01954 -0.00284 -0.00209 -0.00604 N3A 3 0.529618 0.103891 0.875016 11.00000 0.02604 0.02063 = 0.01765 -0.00183 -0.00130 -0.00634 N2A 3 0.600532 0.137850 1.022667 11.00000 0.04094 0.02522 = 0.01872 -0.00171 -0.00404 -0.01450 N4A 3 0.457251 0.073094 0.726678 11.00000 0.02787 0.02513 = 0.02017 -0.00375 -0.00205 -0.00915 N5A 3 0.678343 0.455398 0.754487 11.00000 0.02809 0.02093 = 0.02097 -0.00131 -0.00098 -0.00778 C2A 1 0.587436 0.178092 0.926244 11.00000 0.02205 0.02095 = 0.02007 -0.00265 -0.00047 -0.00415 C4A 1 0.516795 0.150161 0.777243 11.00000 0.01798 0.02108 = 0.01868 -0.00361 -0.00042 -0.00154 C5A 1 0.563428 0.268732 0.730586 11.00000 0.01993 0.02247 = 0.01863 -0.00304 -0.00032 -0.00345 AFIX 43 H5A 2 0.552917 0.298355 0.662196 11.00000 -1.20000 AFIX 0 C6A 1 0.625543 0.341716 0.787407 11.00000 0.01661 0.01952 = 0.01986 -0.00111 0.00137 -0.00130 N1B 3 0.702322 0.188097 0.329635 11.00000 0.01647 0.02101 = 0.01985 -0.00336 -0.00015 -0.00355 N3B 3 0.979788 0.089825 0.367712 11.00000 0.01727 0.01745 = 0.02067 -0.00341 -0.00015 -0.00343 N2B 3 0.772755 0.062192 0.480774 11.00000 0.01676 0.02167 = 0.02093 -0.00056 0.00021 -0.00233 N4B 3 1.180596 0.137309 0.255585 11.00000 0.01638 0.02906 = 0.02193 -0.00192 0.00138 -0.00361 N5B 3 0.618925 0.315981 0.179520 11.00000 0.01740 0.02751 = 0.02271 -0.00241 -0.00186 -0.00161 C2B 1 0.821404 0.112753 0.392707 11.00000 0.01801 0.01592 = 0.02132 -0.00464 -0.00096 -0.00460 C4B 1 1.020496 0.153863 0.278773 11.00000 0.01886 0.01648 = 0.02149 -0.00643 0.00091 -0.00433 C5B 1 0.905202 0.233414 0.211402 11.00000 0.01944 0.02009 = 0.01790 -0.00418 0.00071 -0.00356 AFIX 43 H5B 2 0.937720 0.275665 0.149122 11.00000 -1.20000 AFIX 0 C6B 1 0.743097 0.248026 0.238861 11.00000 0.02062 0.01749 = 0.01892 -0.00670 -0.00069 -0.00364 H1A 2 0.673563 0.344852 0.922195 11.00000 0.03819 H2A 2 0.620414 0.190578 1.056774 11.00000 0.03504 H2B 2 0.561103 0.068273 1.051067 11.00000 0.02488 H4A 2 0.416980 -0.002587 0.762393 11.00000 0.02487 H4B 2 0.436290 0.102292 0.662540 11.00000 0.02583 H5D 2 0.710115 0.500137 0.794039 11.00000 0.02481 H5C 2 0.659699 0.500260 0.694935 11.00000 0.02649 H1B 2 0.599558 0.212894 0.352324 11.00000 0.04045 H2C 2 0.671935 0.086541 0.496247 11.00000 0.03550 H2D 2 0.845634 0.018505 0.523968 11.00000 0.02215 H4C 2 1.251019 0.094655 0.299990 11.00000 0.02718 H4D 2 1.208377 0.192296 0.207291 11.00000 0.04340 H5F 2 0.645848 0.376932 0.123614 11.00000 0.03614 H5E 2 0.519860 0.332484 0.202346 11.00000 0.03339 HKLF 4 REM shelxt_a.res in P-1 REM R1 = 0.0384 for 4401 Fo > 4sig(Fo) and 0.0420 for all 4863 data REM 381 parameters refined using 0 restraints END WGHT 0.0597 0.7343 REM Highest difference peak 0.677, deepest hole -0.570, 1-sigma level 0.073 Q1 1 -0.3011 0.4851 0.3971 11.00000 0.05 0.68 Q2 1 -0.0226 0.4395 0.4804 11.00000 0.05 0.31 Q3 1 0.9272 0.9754 1.2237 11.00000 0.05 0.31 Q4 1 0.0607 0.4783 0.4214 11.00000 0.05 0.30 Q5 1 0.5892 0.2989 0.7601 11.00000 0.05 0.27 Q6 1 -0.0563 0.3021 0.4167 11.00000 0.05 0.27 Q7 1 0.1298 0.2575 0.5318 11.00000 0.05 0.26 Q8 1 0.8030 0.6166 1.0972 11.00000 0.05 0.26 Q9 1 -0.2883 0.3939 0.3711 11.00000 0.05 0.25 Q10 1 0.7704 0.6113 1.0029 11.00000 0.05 0.25 Q11 1 0.9527 0.7261 1.1459 11.00000 0.05 0.24 Q12 1 -0.1044 0.4171 0.5325 11.00000 0.05 0.24 Q13 1 0.5332 0.2105 0.7566 11.00000 0.05 0.24 Q14 1 0.8151 0.1616 0.4648 11.00000 0.05 0.23 Q15 1 0.9303 0.2595 0.0660 11.00000 0.05 0.23 Q16 1 0.7937 1.0385 1.1010 11.00000 0.05 0.23 Q17 1 0.8043 0.8344 1.0785 11.00000 0.05 0.23 Q18 1 0.9582 0.7820 1.0644 11.00000 0.05 0.22 Q19 1 0.0531 0.3550 0.3359 11.00000 0.05 0.22 Q20 1 0.4803 0.1191 0.7610 11.00000 0.05 0.22 ; _shelx_res_checksum 59030 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl1 0.97092(8) 0.92958(5) 1.14832(4) 0.03655(15) Uani d 1 . . S S1 0.84726(6) 0.79481(5) 1.00626(3) 0.02449(13) Uani d 1 . . O O1A 0.74189(18) 0.62714(14) 0.88237(10) 0.0253(3) Uani d 1 . . O O2A 0.72412(19) 0.45143(14) 1.00078(10) 0.0267(3) Uani d 1 . . C C11A 0.7541(2) 0.56700(19) 0.96914(14) 0.0211(4) Uani d 1 . . C C7A 0.8095(2) 0.63513(19) 1.04192(14) 0.0215(4) Uani d 1 . . C C8A 0.8426(3) 0.5877(2) 1.13853(16) 0.0293(4) Uani d 1 . . H H8A 0.828531 0.501787 1.171564 0.035 Uiso calc 1 . . C C9A 0.8999(3) 0.6785(2) 1.18457(16) 0.0309(4) Uani d 1 . . H H9A 0.928577 0.661076 1.251303 0.037 Uiso calc 1 . . C C10A 0.9086(2) 0.7934(2) 1.12145(15) 0.0250(4) Uani d 1 . . Cl Cl2 -0.31592(6) 0.44909(5) 0.45244(5) 0.03503(15) Uani d 1 . . S S2 0.03987(5) 0.38673(4) 0.40489(3) 0.02099(12) Uani d 1 . . O O1B 0.39270(16) 0.28712(15) 0.37649(10) 0.0243(3) Uani d 1 . . O O2B 0.44317(16) 0.16724(14) 0.52650(10) 0.0237(3) Uani d 1 . . C C11B 0.3500(2) 0.24198(19) 0.46245(14) 0.0191(3) Uani d 1 . . C C7B 0.1743(2) 0.27972(18) 0.48818(14) 0.0191(3) Uani d 1 . . C C8B 0.0952(2) 0.2339(2) 0.57201(14) 0.0225(4) Uani d 1 . . H H8B 0.149814 0.174212 0.626188 0.027 Uiso calc 1 . . C C9B -0.0752(2) 0.2838(2) 0.57023(16) 0.0257(4) Uani d 1 . . H H9B -0.148465 0.261771 0.622115 0.031 Uiso calc 1 . . C C10B -0.1203(2) 0.3673(2) 0.48452(16) 0.0245(4) Uani d 1 . . N N1A 0.6369(2) 0.29387(16) 0.88583(12) 0.0205(3) Uani d 1 . . N N3A 0.5296(2) 0.10389(16) 0.87502(11) 0.0214(3) Uani d 1 . . N N2A 0.6005(2) 0.13785(19) 1.02267(13) 0.0274(4) Uani d 1 . . N N4A 0.4573(2) 0.07309(17) 0.72668(13) 0.0239(3) Uani d 1 . . N N5A 0.6783(2) 0.45540(17) 0.75449(13) 0.0233(3) Uani d 1 . . C C2A 0.5874(2) 0.17809(19) 0.92624(14) 0.0212(4) Uani d 1 . . C C4A 0.5168(2) 0.15016(18) 0.77724(13) 0.0196(4) Uani d 1 . . C C5A 0.5634(2) 0.26873(19) 0.73059(14) 0.0206(4) Uani d 1 . . H H5A 0.552917 0.298355 0.662196 0.025 Uiso calc 1 . . C C6A 0.6255(2) 0.34172(19) 0.78741(14) 0.0194(3) Uani d 1 . . N N1B 0.70232(19) 0.18810(16) 0.32963(12) 0.0192(3) Uani d 1 . . N N3B 0.97979(19) 0.08982(15) 0.36771(11) 0.0185(3) Uani d 1 . . N N2B 0.7728(2) 0.06219(16) 0.48077(12) 0.0205(3) Uani d 1 . . N N4B 1.1806(2) 0.13731(18) 0.25558(13) 0.0230(3) Uani d 1 . . N N5B 0.6189(2) 0.31598(18) 0.17952(13) 0.0232(3) Uani d 1 . . C C2B 0.8214(2) 0.11275(18) 0.39271(14) 0.0181(3) Uani d 1 . . C C4B 1.0205(2) 0.15386(18) 0.27877(13) 0.0185(3) Uani d 1 . . C C5B 0.9052(2) 0.23341(18) 0.21140(13) 0.0191(3) Uani d 1 . . H H5B 0.937720 0.275665 0.149122 0.023 Uiso calc 1 . . C C6B 0.7431(2) 0.24803(18) 0.23886(13) 0.0186(3) Uani d 1 . . H H1A 0.674(4) 0.345(3) 0.922(2) 0.038(8) Uiso d 1 . . H H2A 0.620(4) 0.191(3) 1.057(2) 0.035(7) Uiso d 1 . . H H2B 0.561(3) 0.068(3) 1.051(2) 0.025(6) Uiso d 1 . . H H4A 0.417(3) -0.003(3) 0.7624(19) 0.025(6) Uiso d 1 . . H H4B 0.436(3) 0.102(3) 0.663(2) 0.026(6) Uiso d 1 . . H H5D 0.710(3) 0.500(3) 0.794(2) 0.025(6) Uiso d 1 . . H H5C 0.660(3) 0.500(3) 0.695(2) 0.026(6) Uiso d 1 . . H H1B 0.600(4) 0.213(3) 0.352(2) 0.040(8) Uiso d 1 . . H H2C 0.672(4) 0.087(3) 0.496(2) 0.035(7) Uiso d 1 . . H H2D 0.846(3) 0.019(3) 0.5240(19) 0.022(6) Uiso d 1 . . H H4C 1.251(4) 0.095(3) 0.300(2) 0.027(6) Uiso d 1 . . H H4D 1.208(4) 0.192(3) 0.207(3) 0.043(8) Uiso d 1 . . H H5F 0.646(4) 0.377(3) 0.124(2) 0.036(7) Uiso d 1 . . H H5E 0.520(4) 0.332(3) 0.202(2) 0.033(7) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl1 0.0527(3) 0.0301(3) 0.0345(3) -0.0201(2) -0.0006(2) -0.0123(2) S1 0.0321(3) 0.0223(2) 0.0213(2) -0.01014(18) 0.00240(18) -0.00517(17) O1A 0.0296(7) 0.0261(7) 0.0211(7) -0.0092(6) -0.0009(5) -0.0029(5) O2A 0.0374(8) 0.0247(7) 0.0209(6) -0.0132(6) -0.0016(6) -0.0041(5) C11A 0.0199(8) 0.0226(9) 0.0213(9) -0.0045(7) 0.0011(7) -0.0054(7) C7A 0.0201(8) 0.0220(9) 0.0228(9) -0.0038(7) -0.0001(7) -0.0055(7) C8A 0.0399(12) 0.0213(9) 0.0275(10) -0.0081(8) -0.0068(9) -0.0029(8) C9A 0.0396(12) 0.0270(10) 0.0275(10) -0.0068(9) -0.0073(9) -0.0069(8) C10A 0.0239(9) 0.0253(10) 0.0289(10) -0.0063(7) 0.0001(8) -0.0106(8) Cl2 0.0169(2) 0.0324(3) 0.0582(3) 0.00100(18) -0.0057(2) -0.0191(2) S2 0.0177(2) 0.0200(2) 0.0255(2) -0.00281(16) -0.00296(16) -0.00501(17) O1B 0.0173(6) 0.0316(7) 0.0210(6) -0.0034(5) 0.0007(5) 0.0004(5) O2B 0.0181(6) 0.0292(7) 0.0206(6) -0.0009(5) -0.0010(5) -0.0010(5) C11B 0.0175(8) 0.0207(8) 0.0206(8) -0.0053(7) -0.0001(7) -0.0059(7) C7B 0.0174(8) 0.0178(8) 0.0230(9) -0.0039(7) 0.0006(7) -0.0060(7) C8B 0.0220(9) 0.0227(9) 0.0239(9) -0.0051(7) 0.0027(7) -0.0069(7) C9B 0.0217(9) 0.0257(10) 0.0325(10) -0.0066(7) 0.0072(8) -0.0120(8) C10B 0.0161(8) 0.0212(9) 0.0398(11) -0.0035(7) 0.0000(8) -0.0145(8) N1A 0.0232(8) 0.0195(8) 0.0195(7) -0.0060(6) -0.0021(6) -0.0028(6) N3A 0.0260(8) 0.0206(8) 0.0177(7) -0.0063(6) -0.0013(6) -0.0018(6) N2A 0.0409(10) 0.0252(9) 0.0187(8) -0.0145(8) -0.0040(7) -0.0017(7) N4A 0.0279(8) 0.0251(8) 0.0202(8) -0.0092(7) -0.0020(6) -0.0038(6) N5A 0.0281(8) 0.0209(8) 0.0210(8) -0.0078(7) -0.0010(6) -0.0013(7) C2A 0.0220(9) 0.0209(9) 0.0201(9) -0.0042(7) -0.0005(7) -0.0027(7) C4A 0.0180(8) 0.0211(9) 0.0187(8) -0.0015(7) -0.0004(7) -0.0036(7) C5A 0.0199(8) 0.0225(9) 0.0186(8) -0.0034(7) -0.0003(7) -0.0030(7) C6A 0.0166(8) 0.0195(8) 0.0199(8) -0.0013(6) 0.0014(6) -0.0011(7) N1B 0.0165(7) 0.0210(8) 0.0199(7) -0.0035(6) -0.0002(6) -0.0034(6) N3B 0.0173(7) 0.0174(7) 0.0207(7) -0.0034(6) -0.0002(6) -0.0034(6) N2B 0.0168(8) 0.0217(8) 0.0209(8) -0.0023(6) 0.0002(6) -0.0006(6) N4B 0.0164(7) 0.0291(9) 0.0219(8) -0.0036(6) 0.0014(6) -0.0019(7) N5B 0.0174(8) 0.0275(8) 0.0227(8) -0.0016(6) -0.0019(6) -0.0024(7) C2B 0.0180(8) 0.0159(8) 0.0213(8) -0.0046(6) -0.0010(7) -0.0046(6) C4B 0.0189(8) 0.0165(8) 0.0215(9) -0.0043(7) 0.0009(7) -0.0064(7) C5B 0.0194(8) 0.0201(8) 0.0179(8) -0.0036(7) 0.0007(7) -0.0042(7) C6B 0.0206(9) 0.0175(8) 0.0189(8) -0.0036(7) -0.0007(7) -0.0067(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C10A S1 C7A . . 90.95(10) ? O1A C11A O2A . . 125.25(18) ? O1A C11A C7A . . 118.03(17) ? O2A C11A C7A . . 116.72(17) ? C8A C7A C11A . . 129.13(19) ? C8A C7A S1 . . 110.81(15) ? C11A C7A S1 . . 120.03(15) ? C7A C8A C9A . . 113.66(19) ? C10A C9A C8A . . 111.33(19) ? C9A C10A S1 . . 113.25(16) ? C9A C10A Cl1 . . 126.07(17) ? S1 C10A Cl1 . . 120.67(13) ? C10B S2 C7B . . 90.48(10) ? O2B C11B O1B . . 125.24(17) ? O2B C11B C7B . . 117.78(17) ? O1B C11B C7B . . 116.97(17) ? C8B C7B C11B . . 128.11(18) ? C8B C7B S2 . . 111.38(14) ? C11B C7B S2 . . 120.40(14) ? C7B C8B C9B . . 113.55(18) ? C10B C9B C8B . . 110.91(18) ? C9B C10B S2 . . 113.68(15) ? C9B C10B Cl2 . . 125.95(16) ? S2 C10B Cl2 . . 120.37(13) ? C2A N1A C6A . . 120.59(17) ? C2A N3A C4A . . 116.78(17) ? N3A C2A N2A . . 119.10(18) ? N3A C2A N1A . . 123.42(17) ? N2A C2A N1A . . 117.47(18) ? N4A C4A N3A . . 115.69(17) ? N4A C4A C5A . . 121.19(17) ? N3A C4A C5A . . 123.12(17) ? C6A C5A C4A . . 117.80(17) ? N5A C6A N1A . . 116.21(17) ? N5A C6A C5A . . 125.52(18) ? N1A C6A C5A . . 118.27(17) ? C6B N1B C2B . . 120.42(16) ? C2B N3B C4B . . 116.74(16) ? N2B C2B N3B . . 120.65(17) ? N2B C2B N1B . . 116.83(17) ? N3B C2B N1B . . 122.52(17) ? N4B C4B N3B . . 116.96(17) ? N4B C4B C5B . . 119.64(17) ? N3B C4B C5B . . 123.40(17) ? C6B C5B C4B . . 117.41(17) ? N5B C6B N1B . . 117.04(17) ? N5B C6B C5B . . 123.62(18) ? N1B C6B C5B . . 119.31(17) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cl1 C10A . 1.720(2) ? S1 C10A . 1.714(2) ? S1 C7A . 1.728(2) ? O1A C11A . 1.252(2) ? O2A C11A . 1.269(2) ? C11A C7A . 1.492(3) ? C7A C8A . 1.368(3) ? C8A C9A . 1.413(3) ? C9A C10A . 1.353(3) ? Cl2 C10B . 1.718(2) ? S2 C10B . 1.717(2) ? S2 C7B . 1.7236(19) ? O1B C11B . 1.266(2) ? O2B C11B . 1.250(2) ? C11B C7B . 1.486(2) ? C7B C8B . 1.369(3) ? C8B C9B . 1.412(3) ? C9B C10B . 1.356(3) ? N1A C2A . 1.361(3) ? N1A C6A . 1.372(2) ? N3A C2A . 1.324(3) ? N3A C4A . 1.362(2) ? N2A C2A . 1.337(3) ? N4A C4A . 1.348(3) ? N5A C6A . 1.335(3) ? C4A C5A . 1.397(3) ? C5A C6A . 1.387(3) ? N1B C6B . 1.362(2) ? N1B C2B . 1.371(2) ? N3B C2B . 1.337(2) ? N3B C4B . 1.355(2) ? N2B C2B . 1.322(3) ? N4B C4B . 1.344(2) ? N5B C6B . 1.349(3) ? C4B C5B . 1.400(3) ? C5B C6B . 1.375(3) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1A H1A O2A . 0.91(3) 1.83(3) 2.736(2) 173(3) yes N1B H1B O1B . 0.90(3) 1.80(3) 2.687(2) 169(3) yes N2A H2A N5B 1_556 0.85(3) 2.36(3) 3.181(3) 165(3) yes N2A H2B N3A 2_657 0.87(3) 2.14(3) 3.014(2) 177.8(14) yes N2B H2C O2B . 0.86(3) 1.99(3) 2.844(2) 173(3) yes N2B H2D N3B 2_756 0.87(3) 2.14(3) 3.008(2) 178(3) yes N4A H4B O2B . 0.90(3) 1.90(3) 2.784(2) 167(2) yes N4B H4D O1A 2_766 0.85(4) 2.15(4) 2.969(2) 161(3) yes N5B H5C O1B 2_666 0.87(3) 2.21(3) 2.906(2) 136(3) yes N5A H5D O1A . 0.87(3) 2.05(3) 2.911(2) 169(3) yes N5B H5E O1A 2_666 0.87(3) 2.45(3) 3.077(2) 130(2) yes N5B H5F O2A . 0.95(3) 1.89(3) 2.815(2) 163(3) yes