#------------------------------------------------------------------------------ #$Date: 2024-10-05 04:58:16 +0300 (Sat, 05 Oct 2024) $ #$Revision: 295070 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/26/2312661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312661 _cell_angle_alpha 100.870 _cell_angle_beta 101.489 _cell_angle_gamma 110.186 _cell_length_a 10.7102 _cell_length_b 13.1376 _cell_length_c 17.1385 _exptl_crystal_F_000 978.00 _reflns_d_resolution_high 0.7207 _cod_data_source_file dg30626_Zn_Phsup4.hkl _cod_data_source_block 6_Zn_Ph _shelx_title ' 24omg_06b_autored_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.36 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7863.31 7095.75 61.31 o 3 0 0 38.14 21.72 7.01 o 4 0 0 1857.56 1910.32 37.89 o 5 0 0 0.73 5.95 8.36 o 6 0 0 998.02 1050.89 30.01 o 7 0 0 2489.87 2522.36 50.26 o 8 0 0 12.69 34.27 15.35 o 9 0 0 114.34 81.08 21.16 o 10 0 0 387.95 382.65 36.68 o 11 0 0 107.79 132.30 31.56 o 12 0 0 28.63 82.97 48.02 o -12 1 0 27.63 65.61 63.74 o -11 1 0 0.41 22.62 23.56 o -10 1 0 1672.00 1898.23 71.52 o -9 1 0 48.52 34.00 16.66 o -8 1 0 622.79 613.16 28.70 o -7 1 0 120.19 116.98 11.43 o -6 1 0 1239.20 1146.05 30.42 o -5 1 0 3841.36 3704.71 52.75 o -4 1 0 4292.81 4544.82 53.67 o -3 1 0 1130.45 982.08 20.83 o -2 1 0 819.81 793.62 16.14 o 1 1 0 4414.69 4614.92 68.97 o 2 1 0 73017.27 75521.36 283.75 o 3 1 0 2940.60 3343.73 56.11 o 4 1 0 533.98 487.95 25.39 o 5 1 0 442.29 437.48 21.00 o 6 1 0 72.05 70.23 12.52 o 7 1 0 69.78 41.73 12.22 o 8 1 0 0.20 17.98 15.79 o 9 1 0 1312.01 1461.15 63.59 o 10 1 0 430.45 490.66 50.43 o 11 1 0 0.48 -23.01 29.82 o 12 1 0 90.87 147.60 52.18 o -13 2 0 0.95 27.61 63.33 o -12 2 0 17.54 47.30 36.49 o -11 2 0 558.85 611.49 51.99 o -10 2 0 567.74 714.71 44.47 o -9 2 0 138.41 124.74 16.28 o 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