#------------------------------------------------------------------------------ #$Date: 2024-12-07 19:03:28 +0200 (Sat, 07 Dec 2024) $ #$Revision: 296756 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/27/2312708.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312708 loop_ _publ_author_name 'Moya, Marielsys' 'Liendo-Polanco, Gustavo R' 'Atencio, Reinaldo' 'Silva, Pedro' 'Henao, Jose A.' 'Bruno-Colmenares, Julia' _publ_section_title ; Coordination geometry flexibility driving supramolecular isomerism of Cu/Mo pillared-layer hybrid networks. ; _journal_issue 6 _journal_name_full 'Acta crystallographica Section B, Structural science, crystal engineering and materials' _journal_page_first 782 _journal_page_last 792 _journal_paper_doi 10.1107/S2052520624009934 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'C40 H32 Cu4 Mo8 N8 O26' _chemical_formula_sum 'C40 H32 Cu4 Mo8 N8 O26' _chemical_formula_weight 2062.41 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-08-16 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 94.1363(14) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 10.86409(18) _cell_length_b 11.2440(2) _cell_length_c 21.9304(3) _cell_measurement_reflns_used 19103 _cell_measurement_temperature 100.00(14) _cell_measurement_theta_max 29.3590 _cell_measurement_theta_min 2.5540 _cell_volume 2671.95(7) _computing_cell_refinement 'CrysAlisPro 1.171.42.75a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.75a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.75a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(14) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.3196 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 9.00 69.00 1.00 9.92 -- 11.07-130.00 -30.00 60 2 \w 13.00 76.00 1.00 9.92 -- 11.07-139.00 155.00 63 3 \w -42.00 22.00 1.00 9.92 -- -10.68 -77.00 60.00 64 4 \w -85.00 14.00 1.00 9.92 -- -10.68 -37.00-180.00 99 5 \w -42.00 44.00 1.00 9.92 -- 11.07 -77.00-150.00 86 6 \w -39.00 -14.00 1.00 9.92 -- -10.68 57.00 -30.00 25 7 \w -17.00 84.00 1.00 9.92 -- 11.07 57.00 0.00 101 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0008865000 _diffrn_orient_matrix_UB_12 0.0627362000 _diffrn_orient_matrix_UB_13 -0.0034408000 _diffrn_orient_matrix_UB_21 0.0282762000 _diffrn_orient_matrix_UB_22 0.0063625000 _diffrn_orient_matrix_UB_23 0.0299939000 _diffrn_orient_matrix_UB_31 0.0590435000 _diffrn_orient_matrix_UB_32 -0.0021014000 _diffrn_orient_matrix_UB_33 -0.0118066000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0552 _diffrn_reflns_av_unetI/netI 0.0302 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 32759 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.681 _diffrn_reflns_theta_min 1.862 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 3.458 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.643 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.75a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic light yellow' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 2.563 _exptl_crystal_description block _exptl_crystal_F_000 1976 _exptl_crystal_size_max 0.181 _exptl_crystal_size_mid 0.112 _exptl_crystal_size_min 0.084 _refine_diff_density_max 0.651 _refine_diff_density_min -0.671 _refine_diff_density_rms 0.161 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.071 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 388 _refine_ls_number_reflns 5067 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.071 _refine_ls_R_factor_all 0.0284 _refine_ls_R_factor_gt 0.0230 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0196P)^2^+2.9699P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0461 _refine_ls_wR_factor_ref 0.0494 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4541 _reflns_number_total 5067 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 4_a.res in P2(1)/c 4.res created by SHELXL-2018/3 at 20:36:09 on 16-Aug-2024 REM Old TITL 4 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.096, Rweak 0.002, Alpha 0.029 REM 0.429 for 276 systematic absences, Orientation as input REM Formula found by SHELXT: C22 N4 O12 Cu2 Mo4 CELL 0.71073 10.864089 11.244006 21.930416 90 94.1363 90 ZERR 2 0.000177 0.000199 0.000331 0 0.0014 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cu Mo N O UNIT 80 64 8 16 16 52 L.S. 10 0 0 PLAN 10 TEMP -173.15(14) CONF list 4 MORE -1 BOND $H fmap 2 53 acta SHEL 999 0.82 OMIT -5 8 6 OMIT 4 2 19 REM REM REM WGHT 0.019600 2.969900 FVAR 1.29211 MO1 4 1.221721 0.930930 0.543054 11.00000 0.00473 0.00780 = 0.00685 0.00045 0.00104 -0.00004 MO2 4 1.480143 0.814084 0.607722 11.00000 0.00397 0.00853 = 0.00751 0.00169 0.00090 -0.00015 MO3 4 1.801218 0.872347 0.578108 11.00000 0.00556 0.00882 = 0.00828 0.00148 0.00124 -0.00045 MO4 4 1.471875 0.876246 0.451486 11.00000 0.00430 0.00722 = 0.00683 -0.00075 0.00099 -0.00081 CU1 3 1.524880 0.548440 0.407751 11.00000 0.00333 0.02376 = 0.01919 0.00081 0.00167 0.00026 CU2 3 1.447143 0.737247 0.274034 11.00000 0.00341 0.01926 = 0.01976 -0.00125 0.00153 0.00011 O1 6 1.087093 0.865607 0.517308 11.00000 0.00698 0.01238 = 0.01723 0.00116 0.00028 0.00041 O2 6 1.318165 0.793729 0.569257 11.00000 0.00713 0.00778 = 0.01046 0.00221 0.00149 -0.00173 O3 6 1.650160 0.874082 0.611119 11.00000 0.00695 0.01924 = 0.01150 0.00114 -0.00106 -0.00326 O4 6 1.790312 0.911597 0.496391 11.00000 0.00758 0.01012 = 0.01021 0.00148 0.00095 0.00074 O5 6 1.196525 0.983875 0.613590 11.00000 0.01171 0.01507 = 0.00968 -0.00091 0.00204 0.00294 O6 6 1.504086 0.670313 0.631301 11.00000 0.00708 0.01395 = 0.01779 0.00523 0.00026 0.00134 O7 6 1.444346 0.887605 0.672608 11.00000 0.00676 0.01465 = 0.01190 0.00044 -0.00015 -0.00088 O8 6 1.899127 0.962487 0.621056 11.00000 0.00850 0.01579 = 0.01312 0.00168 -0.00095 -0.00258 O9 6 1.860136 0.732333 0.584460 11.00000 0.02236 0.01263 = 0.02321 0.00641 0.00652 0.00377 O10 6 1.561758 1.014467 0.447080 11.00000 0.00669 0.00933 = 0.00939 0.00131 0.00047 0.00000 O11 6 1.489395 0.802123 0.384447 11.00000 0.01037 0.01554 = 0.01286 -0.00438 0.00358 -0.00176 O12 6 1.530285 0.779668 0.510626 11.00000 0.00751 0.00805 = 0.01268 -0.00003 0.00181 -0.00001 O13 6 1.310510 0.896915 0.454336 11.00000 0.00624 0.01108 = 0.00994 -0.00169 0.00039 -0.00195 N1 5 2.350923 0.549741 0.409834 11.00000 0.00996 0.00862 = 0.01635 0.00166 0.00256 0.00018 N2 5 1.699099 0.552819 0.407498 11.00000 0.00638 0.01483 = 0.01321 0.00141 0.00059 -0.00040 N3 5 0.621658 0.734866 0.272064 11.00000 0.00765 0.01668 = 0.00575 -0.00024 0.00042 0.00068 N4 5 1.272580 0.743432 0.271061 11.00000 0.00714 0.01370 = 0.01494 -0.00274 0.00129 -0.00019 C1 1 2.093393 0.555243 0.409060 11.00000 0.00717 0.00714 = 0.01355 0.00163 0.00081 0.00060 C2 1 2.152642 0.501694 0.362017 11.00000 0.00976 0.00758 = 0.01394 -0.00046 -0.00079 -0.00255 AFIX 43 H2 2 2.105447 0.466276 0.328661 11.00000 -1.20000 AFIX 0 C3 1 2.279337 0.499986 0.363756 11.00000 0.00923 0.00945 = 0.01605 0.00020 0.00355 0.00066 AFIX 43 H3 2 2.318011 0.462434 0.331364 11.00000 -1.20000 AFIX 0 C4 1 2.293906 0.602147 0.455148 11.00000 0.01015 0.00930 = 0.01471 0.00163 0.00057 -0.00298 AFIX 43 H4 2 2.343192 0.637631 0.487772 11.00000 -1.20000 AFIX 0 C5 1 2.167238 0.606863 0.456541 11.00000 0.00709 0.01035 = 0.01352 -0.00078 0.00258 0.00061 AFIX 43 H5 2 2.130747 0.644846 0.489475 11.00000 -1.20000 AFIX 0 C6 1 1.956997 0.555074 0.409272 11.00000 0.00658 0.01196 = 0.00958 0.00369 -0.00148 0.00007 C7 1 1.892706 0.649850 0.432876 11.00000 0.00843 0.01363 = 0.01602 -0.00367 -0.00063 -0.00159 AFIX 43 H7 2 1.935978 0.716779 0.449974 11.00000 -1.20000 AFIX 0 C8 1 1.765616 0.645441 0.431150 11.00000 0.01001 0.01534 = 0.02049 -0.00197 0.00373 0.00327 AFIX 43 H8 2 1.722922 0.710625 0.447360 11.00000 -1.20000 AFIX 0 C9 1 1.761228 0.460530 0.385373 11.00000 0.01184 0.01203 = 0.01449 0.00013 -0.00008 -0.00237 AFIX 43 H9 2 1.715736 0.394343 0.368925 11.00000 -1.20000 AFIX 0 C10 1 1.888300 0.458237 0.385633 11.00000 0.00860 0.01067 = 0.01464 0.00048 0.00264 0.00203 AFIX 43 H10 2 1.928837 0.391283 0.369849 11.00000 -1.20000 AFIX 0 C11 1 0.878214 0.737079 0.269020 11.00000 0.00628 0.01515 = 0.00648 0.00071 -0.00005 0.00115 C12 1 0.809591 0.637348 0.250709 11.00000 0.00878 0.01513 = 0.00730 -0.00284 0.00135 0.00105 AFIX 43 H12 2 0.849585 0.568146 0.237066 11.00000 -1.20000 AFIX 0 C13 1 0.683160 0.639617 0.252493 11.00000 0.00894 0.01399 = 0.00705 -0.00045 -0.00098 -0.00335 AFIX 43 H13 2 0.637308 0.571171 0.239378 11.00000 -1.20000 AFIX 0 C14 1 0.687977 0.831348 0.290204 11.00000 0.00908 0.01383 = 0.01044 -0.00384 0.00120 0.00268 AFIX 43 H14 2 0.646095 0.898889 0.304490 11.00000 -1.20000 AFIX 0 C15 1 0.814473 0.835507 0.288763 11.00000 0.00771 0.01513 = 0.01326 -0.00223 0.00098 -0.00032 AFIX 43 H15 2 0.858165 0.905588 0.301251 11.00000 -1.20000 AFIX 0 C16 1 1.014545 0.739850 0.268617 11.00000 0.00633 0.01005 = 0.01156 0.00054 0.00139 -0.00067 C17 1 1.085430 0.799901 0.314552 11.00000 0.01010 0.01194 = 0.01128 -0.00441 0.00321 0.00123 AFIX 43 H17 2 1.046356 0.840577 0.345849 11.00000 -1.20000 AFIX 0 C18 1 1.212090 0.799913 0.314295 11.00000 0.00957 0.01527 = 0.01238 -0.00500 -0.00009 -0.00207 AFIX 43 H18 2 1.258870 0.841344 0.345817 11.00000 -1.20000 AFIX 0 C19 1 1.203634 0.686124 0.226311 11.00000 0.00943 0.01810 = 0.01159 -0.00499 0.00185 0.00183 AFIX 43 H19 2 1.244758 0.647186 0.195144 11.00000 -1.20000 AFIX 0 C20 1 1.076143 0.681613 0.223842 11.00000 0.00785 0.01336 = 0.01262 -0.00415 0.00003 -0.00226 AFIX 43 H20 2 1.031245 0.639320 0.192003 11.00000 -1.20000 AFIX 0 HKLF 4 REM 4_a.res in P2(1)/c REM wR2 = 0.0494, GooF = S = 1.071, Restrained GooF = 1.071 for all data REM R1 = 0.0230 for 4541 Fo > 4sig(Fo) and 0.0284 for all 5067 data REM 388 parameters refined using 0 restraints END WGHT 0.0196 2.9699 REM Highest difference peak 0.651, deepest hole -0.671, 1-sigma level 0.161 Q1 1 1.0000 1.0000 0.5000 10.50000 0.05 0.65 Q2 1 1.2733 0.8467 0.5759 11.00000 0.05 0.64 Q3 1 1.9270 0.9206 0.5821 11.00000 0.05 0.62 Q4 1 1.5545 0.5554 0.6138 11.00000 0.05 0.61 Q5 1 1.4015 0.9267 0.6245 11.00000 0.05 0.60 Q6 1 1.6350 0.9391 0.4338 11.00000 0.05 0.60 Q7 1 1.4386 0.6549 0.3615 11.00000 0.05 0.56 Q8 1 1.5434 0.7824 0.4821 11.00000 0.05 0.56 Q9 1 1.7630 0.9429 0.4809 11.00000 0.05 0.56 Q10 1 1.7426 0.8400 0.4992 11.00000 0.05 0.56 REM The information below was added by Olex2. REM REM R1 = 0.0230 for 4541 Fo > 4sig(Fo) and 0.0284 for all 38261 data REM 388 parameters refined using n/a restraints REM Highest difference peak 0.65, deepest hole -0.67 REM Mean Shift 0, Max Shift 0.002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0284 REM R1_gt = 0.0230 REM wR_ref = 0.0494 REM GOOF = 1.071 REM Shift_max = 0.002 REM Shift_mean = 0 REM Reflections_all = 38261 REM Reflections_gt = 4541 REM Parameters = 388 REM Hole = -0.67 REM Peak = 0.65 REM Flack = n/a ; _cod_data_source_file yv5021sup1.cif _cod_data_source_block 4 _cod_depositor_comments 'Adding full bibliography for 2312705--2312708.cif.' _cod_original_cell_volume 2671.95(8) _cod_database_code 2312708 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula C40H38Cu4Mo8N8O26 _chemical_oxdiff_usercomment Y1803d_ReinaldoAtencio_IVIC _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C7(H7), C8(H8), C9(H9), C10(H10), C12(H12), C13(H13), C14(H14), C15(H15), C17(H17), C18(H18), C19(H19), C20(H20) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.382 _oxdiff_exptl_absorpt_empirical_full_min 0.615 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mo1 Mo 1.22172(2) 0.93093(2) 0.54305(2) 0.00643(7) Uani 1 1 d . . . . . Mo2 Mo 1.48014(2) 0.81408(2) 0.60772(2) 0.00665(7) Uani 1 1 d . . . . . Mo3 Mo 1.80122(2) 0.87235(2) 0.57811(2) 0.00752(7) Uani 1 1 d . . . . . Mo4 Mo 1.47188(2) 0.87625(2) 0.45149(2) 0.00609(7) Uani 1 1 d . . . . . Cu1 Cu 1.52488(3) 0.54844(4) 0.40775(2) 0.01538(9) Uani 1 1 d . . . . . Cu2 Cu 1.44714(3) 0.73725(4) 0.27403(2) 0.01411(9) Uani 1 1 d . . . . . O1 O 1.08709(18) 0.86561(18) 0.51731(10) 0.0122(5) Uani 1 1 d . . . . . O2 O 1.31816(17) 0.79373(17) 0.56926(9) 0.0084(4) Uani 1 1 d . . . . . O3 O 1.65016(18) 0.87408(19) 0.61112(9) 0.0126(5) Uani 1 1 d . . . . . O4 O 1.79031(17) 0.91160(18) 0.49639(9) 0.0093(4) Uani 1 1 d . . . . . O5 O 1.19652(18) 0.98387(19) 0.61359(9) 0.0121(4) Uani 1 1 d . . . . . O6 O 1.50409(18) 0.67031(19) 0.63130(10) 0.0130(5) Uani 1 1 d . . . . . O7 O 1.44435(18) 0.88761(18) 0.67261(9) 0.0111(4) Uani 1 1 d . . . . . O8 O 1.89913(18) 0.96249(19) 0.62106(9) 0.0126(5) Uani 1 1 d . . . . . O9 O 1.8601(2) 0.7323(2) 0.58446(11) 0.0192(5) Uani 1 1 d . . . . . O10 O 1.56176(17) 1.01447(18) 0.44708(9) 0.0085(4) Uani 1 1 d . . . . . O11 O 1.48939(18) 0.80212(19) 0.38445(9) 0.0128(5) Uani 1 1 d . . . . . O12 O 1.53028(17) 0.77967(18) 0.51063(9) 0.0094(4) Uani 1 1 d . . . . . O13 O 1.31051(17) 0.89691(18) 0.45434(9) 0.0091(4) Uani 1 1 d . . . . . N1 N 2.3509(2) 0.5497(2) 0.40983(12) 0.0116(5) Uani 1 1 d . . . . . N2 N 1.6991(2) 0.5528(2) 0.40750(11) 0.0115(5) Uani 1 1 d . . . . . N3 N 0.6217(2) 0.7349(2) 0.27206(11) 0.0100(5) Uani 1 1 d . . . . . N4 N 1.2726(2) 0.7434(2) 0.27106(12) 0.0119(5) Uani 1 1 d . . . . . C1 C 2.0934(3) 0.5552(3) 0.40906(14) 0.0093(6) Uani 1 1 d . . . . . C2 C 2.1526(3) 0.5017(3) 0.36202(14) 0.0105(6) Uani 1 1 d . . . . . H2 H 2.105447 0.466276 0.328661 0.013 Uiso 1 1 calc R U . . . C3 C 2.2793(3) 0.5000(3) 0.36376(14) 0.0115(6) Uani 1 1 d . . . . . H3 H 2.318011 0.462434 0.331364 0.014 Uiso 1 1 calc R U . . . C4 C 2.2939(3) 0.6021(3) 0.45515(14) 0.0114(6) Uani 1 1 d . . . . . H4 H 2.343192 0.637631 0.487772 0.014 Uiso 1 1 calc R U . . . C5 C 2.1672(3) 0.6069(3) 0.45654(14) 0.0102(6) Uani 1 1 d . . . . . H5 H 2.130747 0.644846 0.489475 0.012 Uiso 1 1 calc R U . . . C6 C 1.9570(3) 0.5551(3) 0.40927(13) 0.0095(6) Uani 1 1 d . . . . . C7 C 1.8927(3) 0.6498(3) 0.43288(14) 0.0128(7) Uani 1 1 d . . . . . H7 H 1.935978 0.716779 0.449974 0.015 Uiso 1 1 calc R U . . . C8 C 1.7656(3) 0.6454(3) 0.43115(15) 0.0152(7) Uani 1 1 d . . . . . H8 H 1.722922 0.710625 0.447360 0.018 Uiso 1 1 calc R U . . . C9 C 1.7612(3) 0.4605(3) 0.38537(14) 0.0128(6) Uani 1 1 d . . . . . H9 H 1.715736 0.394343 0.368925 0.015 Uiso 1 1 calc R U . . . C10 C 1.8883(3) 0.4582(3) 0.38563(14) 0.0112(6) Uani 1 1 d . . . . . H10 H 1.928837 0.391283 0.369849 0.013 Uiso 1 1 calc R U . . . C11 C 0.8782(3) 0.7371(3) 0.26902(13) 0.0093(6) Uani 1 1 d . . . . . C12 C 0.8096(3) 0.6373(3) 0.25071(13) 0.0104(6) Uani 1 1 d . . . . . H12 H 0.849585 0.568146 0.237066 0.012 Uiso 1 1 calc R U . . . C13 C 0.6832(3) 0.6396(3) 0.25249(13) 0.0101(6) Uani 1 1 d . . . . . H13 H 0.637308 0.571171 0.239378 0.012 Uiso 1 1 calc R U . . . C14 C 0.6880(3) 0.8313(3) 0.29020(13) 0.0111(6) Uani 1 1 d . . . . . H14 H 0.646095 0.898889 0.304490 0.013 Uiso 1 1 calc R U . . . C15 C 0.8145(3) 0.8355(3) 0.28876(14) 0.0120(6) Uani 1 1 d . . . . . H15 H 0.858165 0.905588 0.301251 0.014 Uiso 1 1 calc R U . . . C16 C 1.0145(3) 0.7399(3) 0.26862(13) 0.0093(6) Uani 1 1 d . . . . . C17 C 1.0854(3) 0.7999(3) 0.31455(14) 0.0110(6) Uani 1 1 d . . . . . H17 H 1.046356 0.840577 0.345849 0.013 Uiso 1 1 calc R U . . . C18 C 1.2121(3) 0.7999(3) 0.31430(14) 0.0124(6) Uani 1 1 d . . . . . H18 H 1.258870 0.841344 0.345817 0.015 Uiso 1 1 calc R U . . . C19 C 1.2036(3) 0.6861(3) 0.22631(14) 0.0130(7) Uani 1 1 d . . . . . H19 H 1.244758 0.647186 0.195144 0.016 Uiso 1 1 calc R U . . . C20 C 1.0761(3) 0.6816(3) 0.22384(14) 0.0113(6) Uani 1 1 d . . . . . H20 H 1.031245 0.639320 0.192003 0.014 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Mo1 0.00473(13) 0.00780(14) 0.00685(13) 0.00045(10) 0.00104(9) -0.00004(9) Mo2 0.00397(13) 0.00853(14) 0.00751(13) 0.00169(10) 0.00090(9) -0.00015(9) Mo3 0.00556(13) 0.00882(14) 0.00828(13) 0.00148(10) 0.00124(9) -0.00045(9) Mo4 0.00430(13) 0.00722(13) 0.00683(12) -0.00075(9) 0.00099(9) -0.00081(9) Cu1 0.00333(19) 0.0238(2) 0.0192(2) 0.00081(17) 0.00167(15) 0.00026(15) Cu2 0.00341(18) 0.0193(2) 0.0198(2) -0.00125(17) 0.00153(15) 0.00011(15) O1 0.0070(11) 0.0124(11) 0.0172(11) 0.0012(9) 0.0003(8) 0.0004(8) O2 0.0071(10) 0.0078(11) 0.0105(10) 0.0022(8) 0.0015(8) -0.0017(8) O3 0.0070(11) 0.0192(12) 0.0115(11) 0.0011(9) -0.0011(8) -0.0033(8) O4 0.0076(10) 0.0101(11) 0.0102(10) 0.0015(9) 0.0009(8) 0.0007(8) O5 0.0117(11) 0.0151(12) 0.0097(11) -0.0009(9) 0.0020(8) 0.0029(8) O6 0.0071(10) 0.0139(12) 0.0178(11) 0.0052(9) 0.0003(8) 0.0013(8) O7 0.0068(10) 0.0147(12) 0.0119(11) 0.0004(9) -0.0002(8) -0.0009(8) O8 0.0085(11) 0.0158(12) 0.0131(11) 0.0017(9) -0.0009(8) -0.0026(8) O9 0.0224(12) 0.0126(12) 0.0232(13) 0.0064(10) 0.0065(10) 0.0038(9) O10 0.0067(10) 0.0093(11) 0.0094(10) 0.0013(8) 0.0005(8) 0.0000(8) O11 0.0104(11) 0.0155(12) 0.0129(11) -0.0044(9) 0.0036(8) -0.0018(8) O12 0.0075(10) 0.0081(11) 0.0127(11) 0.0000(8) 0.0018(8) 0.0000(8) O13 0.0062(10) 0.0111(11) 0.0099(10) -0.0017(8) 0.0004(8) -0.0019(8) N1 0.0100(13) 0.0086(13) 0.0164(14) 0.0017(11) 0.0026(10) 0.0002(10) N2 0.0064(13) 0.0148(14) 0.0132(13) 0.0014(11) 0.0006(10) -0.0004(10) N3 0.0076(13) 0.0167(14) 0.0058(12) -0.0002(10) 0.0004(10) 0.0007(10) N4 0.0071(13) 0.0137(14) 0.0149(13) -0.0027(11) 0.0013(10) -0.0002(10) C1 0.0072(15) 0.0071(15) 0.0136(15) 0.0016(12) 0.0008(12) 0.0006(11) C2 0.0098(16) 0.0076(15) 0.0139(15) -0.0005(12) -0.0008(12) -0.0025(11) C3 0.0092(16) 0.0095(16) 0.0160(16) 0.0002(13) 0.0035(12) 0.0007(12) C4 0.0101(16) 0.0093(16) 0.0147(16) 0.0016(12) 0.0006(12) -0.0030(12) C5 0.0071(15) 0.0103(16) 0.0135(15) -0.0008(12) 0.0026(12) 0.0006(12) C6 0.0066(15) 0.0120(16) 0.0096(14) 0.0037(12) -0.0015(11) 0.0001(11) C7 0.0084(16) 0.0136(17) 0.0160(16) -0.0037(13) -0.0006(12) -0.0016(12) C8 0.0100(16) 0.0153(17) 0.0205(17) -0.0020(14) 0.0037(13) 0.0033(12) C9 0.0118(16) 0.0120(16) 0.0145(16) 0.0001(13) -0.0001(12) -0.0024(12) C10 0.0086(15) 0.0107(16) 0.0146(16) 0.0005(13) 0.0026(12) 0.0020(12) C11 0.0063(15) 0.0152(16) 0.0065(14) 0.0007(12) 0.0000(11) 0.0012(12) C12 0.0088(15) 0.0151(17) 0.0073(14) -0.0028(12) 0.0014(11) 0.0010(12) C13 0.0089(15) 0.0140(16) 0.0071(14) -0.0005(12) -0.0010(11) -0.0033(12) C14 0.0091(15) 0.0138(16) 0.0104(15) -0.0038(12) 0.0012(12) 0.0027(12) C15 0.0077(15) 0.0151(17) 0.0133(15) -0.0022(13) 0.0010(12) -0.0003(12) C16 0.0063(15) 0.0100(16) 0.0116(15) 0.0005(12) 0.0014(11) -0.0007(11) C17 0.0101(15) 0.0119(16) 0.0113(15) -0.0044(12) 0.0032(12) 0.0012(12) C18 0.0096(16) 0.0153(17) 0.0124(15) -0.0050(13) -0.0001(12) -0.0021(12) C19 0.0094(16) 0.0181(17) 0.0116(15) -0.0050(13) 0.0019(12) 0.0018(12) C20 0.0078(15) 0.0134(16) 0.0126(15) -0.0041(13) 0.0000(12) -0.0023(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 0 0 -2 183895 997.22 5 0 0 -3 30.7113 64.3735 5 0 0 -4 9120.65 320.292 5 0 0 4 9427.44 406.493 3 0 0 -5 265.064 121.24 5 0 0 5 120.752 105.283 3 0 0 -6 586905 3132.27 5 0 0 6 619860 3924.92 3 0 0 -7 413.942 126.337 5 0 0 7 402.831 121.681 5 0 0 7 327.664 141.656 3 0 0 -8 3508.98 285.127 5 0 0 8 3036.12 264.807 5 0 0 8 3227.16 335.064 3 0 0 9 -24.7318 63.3134 5 0 0 -9 7.70082 71.7057 5 0 0 9 -18.3762 99.1652 3 0 0 10 882.979 168.757 5 0 0 -10 735.055 166.253 5 0 0 10 533.817 146.16 3 0 0 11 -46.797 84.6746 5 0 0 11 -65.5739 139.043 3 0 0 12 18081.4 794.11 5 0 0 12 18923.9 984.341 3 0 0 13 6.28558 61.132 5 0 0 13 33.8689 93.1468 3 0 0 -13 136.572 129.201 6 0 0 14 31711 1376.97 3 0 0 -14 28611.6 1147.61 6 0 0 15 2.46981 66.6812 5 0 0 15 78.6471 109.779 3 0 0 -15 179.732 155.744 6 0 0 16 14230.5 828.729 5 0 0 16 16039.6 1043.92 3 0 0 16 14689.3 886.348 7 0 0 -16 14939 903.543 6 0 0 17 391.131 169.201 5 0 0 17 483.428 202.574 3 0 0 17 497.266 229.19 4 0 0 -17 802.458 270.304 6 0 0 17 523.567 216.454 7 0 0 18 36477.6 1416.67 5 0 0 18 40270.8 1709.42 3 0 0 18 36407.7 1580.17 4 0 0 -18 36151.5 1505.54 6 0 0 18 38766.8 1541.4 7 0 0 19 395.548 169.744 5 0 0 19 643.978 245.892 3 0 0 19 512.621 213.091 7 0 0 -19 676.923 262.284 6 0 0 19 570.978 238.251 4 0 0 20 6609.24 710.051 3 0 0 20 5375.43 621.878 7 0 0 -20 5341.65 624.764 6 0 0 20 5958 689.421 4 0 0 21 315.685 186.387 3 0 0 21 395.956 235.45 4 0 0 21 384.947 218.954 7 0 0 -21 266.027 194.321 6 0 0 22 57140.6 2264.57 4 0 0 -22 53918.9 2106.21 6 0 0 22 54526.8 2078.92 7 0 0 23 1.33845 174.558 4 0 0 23 314.674 203.172 7 0 0 -23 105.519 167.844 6 0 0 24 7618.44 885.923 4 0 0 -24 8876.91 923.271 6 0 0 24 8626.32 888.809 7 0 0 25 99.6192 191.818 4 0 0 -25 174.685 232.402 6 0 0 25 -114.508 215.103 7 0 0 26 28633.1 1803.3 4 0 0 -26 26753.4 1952.34 1 0 0 -26 25461.9 1640.89 6 0 0 26 27064.1 1642.35 7 0 0 27 -121.729 222.669 4 0 0 -27 -272.425 287.636 1 0 0 27 139.27 198.321 7 0 0 -27 12.4645 245.28 6 0 0 -28 437.826 266.504 6 0 0 28 425.24 277.433 7 0 -1 0 18.5049 19.5075 4 0 -1 1 128896 951.67 7 0 -1 -1 133689 967.44 5 0 -1 -1 132889 1022.36 4 0 -1 -2 20879.5 426.561 5 0 -1 2 20242.1 424.047 7 0 -1 -2 20428.2 454.093 4 0 -1 -3 59189.7 798.618 5 0 1 3 60488 840.334 6 0 -1 3 57364.6 780.232 7 0 1 -3 57703.4 793.952 7 0 -1 -3 59645.5 870.804 4 0 -1 -4 63506.5 912.432 5 0 -1 4 59993.1 890.899 7 0 1 4 62032.9 936.754 6 0 1 -4 60425.8 908.386 7 0 -1 -4 62067.3 939 6 0 -1 -4 61875.1 985.228 4 0 -1 -5 41875.8 804.948 5 0 -1 -5 41564.3 835.86 6 0 -1 5 39982 796.626 7 0 1 5 42572.4 846.733 6 0 1 -5 40871.8 818.24 7 0 -1 -5 41427.9 880.536 4 0 1 6 152558 1663.98 5 0 -1 -6 163057 1716 5 0 -1 -6 160598 1785.18 6 0 -1 6 156098 1712.1 7 0 1 6 161639 1782.26 6 0 -1 7 11460.1 494.448 5 0 1 7 11492.2 484.397 5 0 -1 -7 11526.1 495.69 5 0 -1 7 12013.8 481.895 3 0 1 -7 12275.8 477.855 3 0 -1 7 11285.2 500.72 7 0 -1 -7 10992.7 507.442 6 0 1 8 92.7465 69.1308 5 0 -1 8 231.567 85.3201 5 0 -1 -8 4.28978 72.1323 5 0 -1 8 67.9837 85.737 3 0 1 8 31.6184 51.2768 4 0 -1 8 189.482 104.244 7 0 -1 -8 107.377 95.6057 6 0 -1 9 45507 1095.77 5 0 1 9 43294.8 1063.58 5 0 -1 -9 46200.2 1110.8 5 0 -1 9 46897.8 1090.32 3 0 -1 -9 45702.3 1151.31 6 0 -1 9 45043.3 1122.44 7 0 -1 10 16488.6 695.41 5 0 1 10 17301.3 703.832 5 0 -1 -10 18065.5 733.417 5 0 1 10 17600 1032.16 3 0 -1 10 17296.1 707.43 3 0 -1 10 17447.3 742.129 7 0 -1 -10 17124.5 751.994 6 0 1 11 54483 1313.98 5 0 -1 -11 57920.4 1366.79 5 0 -1 11 55538 1341.72 5 0 1 11 61654.3 1970.11 3 0 -1 11 59644.5 1381.08 3 0 -1 11 55940.4 1395.07 7 0 -1 -11 55337.7 1410.35 6 0 -1 12 62135.7 1485.22 5 0 1 12 60225.2 1440.2 5 0 -1 -12 62721.8 1493.79 5 0 -1 12 65413 1516.56 3 0 1 12 65440.7 2091.17 3 0 -1 12 61370.9 1519.13 7 0 -1 -12 59720.9 1527.53 6 0 -1 13 8165.73 568.81 5 0 1 13 19157.7 853.096 5 0 -1 -13 45879.4 1327.68 5 0 1 13 48493 1854.9 3 0 -1 13 46370.3 1335.42 3 0 1 13 39683.7 1368.32 4 0 -1 13 43104 1334.92 7 0 -1 -13 42500.1 1350.74 6 0 1 14 33.4551 56.7075 5 0 -1 14 28.4233 54.7988 5 0 -1 -14 11.0445 104.307 5 0 -1 14 111.497 110.98 3 0 1 14 7.31479 161.202 3 0 1 14 272.341 168.657 4 0 -1 -14 164.235 124.162 6 0 -1 14 164.192 156.876 7 0 -1 -15 -1.88089 109.384 5 0 1 15 -85.5762 88.0936 5 0 -1 15 43.5256 83.9156 5 0 1 15 34.4532 131.991 3 0 -1 15 148.857 121.322 3 0 1 15 -3.86723 109.363 4 0 -1 15 4.74222 118.404 7 0 -1 -15 -7.0787 130.915 6 0 -1 16 13289.9 807.828 5 0 1 16 13165.6 793.067 5 0 -1 -16 15159.3 853.574 5 0 -1 16 13890 801.887 3 0 1 16 15642 1154.69 3 0 1 16 13049.5 891.888 4 0 -1 16 14741.4 881.537 7 0 -1 -16 13039.2 851.476 6 0 -1 -17 25321.5 1148.78 5 0 1 17 23812.7 1111.84 5 0 -1 17 22652.7 1092.15 5 0 -1 17 24280.9 1076.07 3 0 1 17 25145.8 1499.62 3 0 1 17 21503.9 1180.21 4 0 -1 -17 23051.1 1164.88 6 0 -1 17 23039.6 1141.99 7 0 1 18 1329.2 279.996 5 0 -1 18 1106.86 274.764 5 0 1 18 1427.25 397.711 3 0 1 18 1137.44 310.444 4 0 -1 18 773.481 250.189 7 0 -1 -18 1282.5 313.293 6 0 1 19 14255.4 914.724 5 0 -1 19 14583.5 929.339 5 0 1 19 16471.9 1284.53 3 0 1 -19 14106.3 979.122 6 0 -1 -19 14918.4 1005.58 6 0 -1 19 12033.8 880.8 7 0 1 19 13422.2 1000.82 4 0 1 20 9230.73 975.639 3 0 -1 -20 8041.77 765.457 6 0 -1 20 9483.51 812.947 7 0 1 -20 9432.38 832.798 6 0 1 20 8316.06 813.344 4 0 1 21 77.4835 136.978 4 0 -1 21 -24.4887 194.628 7 0 -1 -21 -61.7271 156.365 6 0 1 21 -75.5444 199.401 7 0 1 -21 -341.412 213.648 6 0 -1 22 3061.71 541.03 4 0 1 22 2476.12 489.961 4 0 1 -22 2806.99 508.832 6 0 1 22 2971.71 511.82 7 0 -1 -22 2158.19 446.822 6 0 -1 22 2601.5 462.132 7 0 -1 23 2544.97 509.059 4 0 1 23 2651.76 524.49 4 0 1 -23 3406.58 558.922 6 0 -1 23 4193.24 599.318 7 0 1 23 3103.94 531.387 7 0 -1 -23 2806.04 518.771 6 0 1 24 21457.1 1480.23 4 0 -1 24 21849.9 1500.46 4 0 -1 24 21631.1 1375.84 7 0 -1 -24 21753.8 1426.66 6 0 1 -24 23449.9 1495.24 6 0 1 24 21844.8 1413.6 7 0 -1 25 20168.7 1493.52 4 0 1 25 18100 1397.47 4 0 -1 25 20262.7 1369.87 7 0 1 25 20793.3 1425.94 7 0 1 -25 20736.3 1446.06 6 0 -1 -25 22144.7 1471.85 6 0 1 26 5579.24 810.432 4 0 -1 26 4996.07 779.77 4 0 -1 -26 5036.54 860.202 1 0 1 -26 3406.17 724.388 1 0 -1 -26 4869.65 735.044 6 0 1 26 4732.57 710.056 7 0 1 -26 5139.2 744.967 6 0 -1 26 4995.81 710.707 7 0 1 27 16532.3 1409.22 4 0 -1 27 16824.7 1438.65 4 0 1 -27 17131.7 1586.9 1 0 -1 -27 17089.8 1602.45 1 0 -1 27 17863.3 1365.19 7 0 -1 -27 17178.4 1375.1 6 0 1 27 16355.4 1324.55 7 0 1 -27 16518.7 1367.18 6 0 1 28 228.165 234.026 7 0 -1 28 148.554 204.697 7 0 -1 -28 443.256 294.124 6 0 1 -28 -377.106 269.611 6 0 -2 0 8815.58 350.692 4 0 -2 0 8838.36 338.572 7 0 -2 -1 122155 1332.43 4 0 -2 1 121012 1322.3 4 0 -2 -1 118707 1264.33 7 0 -2 1 118376 1253.68 7 0 2 -2 211711 1738.66 7 0 -2 2 206379 1700.36 7 0 -2 -2 217824 1846.14 4 0 -2 2 206569 1801.69 4 0 -2 -2 214663 1753.77 5 0 -2 -3 161368 1695.76 4 0 -2 -3 155868 1572.66 5 0 2 -3 161190 1621.26 7 0 -2 3 153022 1531.84 7 0 2 -4 90932.7 1285.98 7 0 -2 -4 88914.3 1339.03 4 0 -2 4 84832.8 1210.2 7 0 -2 -4 89625.5 1265.82 5 0 -2 -5 71268.7 1195.18 5 0 2 5 66417.4 1133.59 5 0 2 -5 71032.4 1182.91 7 0 2 5 70377.8 1225.21 6 0 -2 -5 71623.7 1276.15 4 0 -2 -6 6179.03 371.436 5 0 2 6 5693.04 347.273 5 0 -2 -6 5668.64 385.356 4 0 2 6 3999.49 319.832 4 0 2 6 5901.67 377.088 6 0 -2 6 5650.13 357.923 7 0 2 -6 5884.81 364.98 7 0 2 7 88909.9 1431.81 5 0 -2 -7 93300.5 1516.96 5 0 2 -7 92663.2 1429.89 3 0 -2 -7 95607.8 1659.21 4 0 2 7 93545.6 1564.09 6 0 -2 7 88955.1 1465 7 0 2 -7 91598.9 1514.52 7 0 -2 -8 18305.9 702.799 5 0 2 8 17420.2 672.866 5 0 2 -8 18619.4 631.905 3 0 -2 -8 18970.7 779.888 4 0 2 -8 18297.3 718.23 7 0 -2 8 16801.7 669.705 7 0 2 8 17773.3 721.202 6 0 2 9 34219.8 986.774 5 0 -2 -9 37684.6 1057.26 5 0 2 -9 36048.7 852.761 3 0 -2 -9 35586.6 1061.59 6 0 -2 9 35063.5 1012.87 7 0 2 9 37573.9 1093.38 6 0 2 10 7446.24 485.014 5 0 -2 -10 7641.98 498.761 5 0 2 -10 7746.22 403.972 3 0 -2 10 8024.51 512.703 7 0 -2 -10 7723.46 520.649 6 0 -2 -11 1294.49 235.369 6 0 -2 11 1435.93 239.238 7 0 -2 11 1101.69 202.872 5 0 -2 -11 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34308.7 1287.58 2 -3 5 2 65949 1741.45 2 3 5 -2 72008.3 1844.79 2 3 -5 -2 69468.1 1825.49 2 -3 -5 2 69729.9 1771.48 2 -3 5 2 72531.5 1380.74 1 -3 -5 2 68505 1340.05 1 -3 -5 2 72625.8 1677.97 7 -3 5 2 72876.4 1515.19 7 3 5 -2 78159.7 2880.39 3 3 -5 -2 74097.7 1731.78 5 3 -5 -2 74952.9 1738.85 4 -3 -5 2 71673.9 1568.85 4 -3 5 2 76638.6 1717.37 4 3 5 -1 7967.45 610.318 2 3 -5 -1 8381.35 624.23 2 -3 5 1 8515.41 609.724 2 -3 -5 1 8246.57 601.056 2 -3 5 1 8797.23 475.188 1 -3 -5 1 8425.95 466.876 1 -3 5 1 9301.55 534.366 7 -3 -5 1 8823.69 586.69 7 3 5 -1 9889.96 1070.97 3 3 -5 -1 9579.94 618.381 5 3 -5 -1 9306.88 616.751 4 -3 5 1 9271.47 604.671 4 3 5 -1 8508.6 542.533 4 -3 -5 1 9243.81 557.996 4 -3 5 0 85794.9 1913.1 2 3 -5 0 82433.3 1907.97 2 3 5 0 83475.8 1926.24 2 -3 5 0 80886.8 1462.72 1 -3 -5 0 81108.5 1445.24 1 -3 5 0 88048.2 1623.57 7 -3 -5 0 85157.2 1785.93 7 3 5 0 89214.4 3234.81 3 3 -5 0 84599.3 1790.43 5 -3 -5 0 80899.1 1656.78 4 3 -5 0 87021 1846.82 4 -3 5 0 87061.2 1826.9 4 3 5 0 87535.6 1712.96 4 3 5 1 2861.82 379.375 2 3 -5 1 2552.8 355.296 2 -3 -5 -1 2542.85 262.522 1 3 5 1 3648.71 679.116 3 -3 -5 -1 2991.69 343.373 7 3 -5 1 3173.7 314.019 7 3 5 1 1960.05 281.696 7 -3 5 -1 3132.67 307.887 7 3 -5 1 3120.89 352.188 5 -3 5 -1 2946.1 342.693 4 -3 -5 -1 2897.43 314.506 4 3 -5 1 2912.21 341.972 4 3 5 1 3075.25 324.408 4 3 5 2 21529 1014.63 2 3 -5 2 21271.8 1012.09 2 3 5 2 21811.6 1667.32 3 -3 5 -2 21989.6 801.771 7 3 -5 2 21229.6 791.842 7 -3 -5 -2 20809.2 883.29 7 3 -5 2 21236.7 880.321 5 3 -5 2 20412.8 901.925 4 -3 5 -2 21948 934.154 4 -3 -5 -2 23052.2 890.137 4 3 5 2 20426 832.082 4 -3 5 -3 5206.73 397.79 7 -3 -5 -3 5098.67 447.966 7 3 -5 3 5316.8 403.196 7 3 -5 3 4286.23 472.764 2 3 5 3 5659.37 546.626 2 3 -5 3 4976.45 457.891 4 3 5 3 4812.6 410.308 4 -3 -5 -3 5291.69 436.609 4 3 5 3 4986.94 823.582 3 3 -5 4 684.152 146.263 7 -3 5 -4 987.603 177.453 7 3 5 4 1427.46 514.314 3 -3 -5 -4 1021.22 196.918 4 3 -5 4 782.559 195.255 4 3 5 4 977.428 188.791 4 3 5 4 852.239 229.617 2 3 -5 4 1024.07 256.886 2 3 -5 5 1750.46 331.063 2 3 5 5 1402.04 300.697 2 3 -5 5 1756.33 241.241 7 -3 5 -5 1930.86 249.718 7 3 5 5 2010.32 585.805 3 -3 -5 -5 1789.18 253.124 5 3 -5 5 1639.26 275.118 4 3 5 5 1901.15 274.564 4 -3 -5 -5 1744.68 271.557 4 3 -5 6 3293.44 330.525 7 3 5 6 1599.2 261.473 7 3 5 6 2916.4 720.778 3 -3 5 -6 3427.03 348.661 7 -3 -5 -6 3240.82 337.928 5 -3 -5 -6 3502.34 390.862 4 3 5 6 2856.29 338.186 4 3 -5 6 2705.44 355.736 4 3 -5 7 38821.1 1129.46 7 3 5 7 38831.8 1279.16 7 3 5 7 47180.4 2688.07 3 -3 5 -7 44909.6 1282.21 7 -3 -5 -7 43024 1378.6 4 -3 -5 -7 39273.2 1186.01 5 3 -5 7 39355.9 1356.93 4 3 5 8 18403.2 896.805 7 3 -5 8 17806.7 784.992 7 -3 5 -8 19087.6 825.017 7 3 5 8 19560.2 1754.53 3 -3 -5 -8 19946.7 958.623 4 -3 -5 -8 18656.8 832.724 5 3 5 8 17412.7 870.445 4 3 -5 8 18292.9 944.512 4 3 -5 9 101854 1900.34 7 3 5 9 102064 2146.78 7 3 5 9 106547 2085.38 6 -3 5 -9 107543 1998.79 7 3 5 9 114617 4320.1 3 -3 -5 -9 104478 2012.14 5 -3 -5 -9 110551 2331.83 4 3 5 9 95813.7 2091.37 4 3 5 10 389.157 145.696 7 3 -5 10 187.21 108.725 7 -3 5 -10 227.909 112.512 7 3 5 10 219.351 117.781 6 3 5 10 110.439 244.65 3 -3 -5 -10 472.826 153.738 5 -3 -5 -10 55.1293 127.353 4 3 5 10 171.17 118.685 4 3 5 11 19763.9 989.51 7 3 -5 11 19489.9 882.227 7 -3 5 -11 21578 960.145 7 3 5 11 21895.8 998.177 6 3 5 11 21277.9 1957 3 -3 5 -11 21121.8 1637.24 3 -3 -5 -11 21097.7 943.72 5 -3 -5 -11 22263.2 1113.84 4 3 5 11 19541.1 998.237 4 3 5 12 5620.04 525.806 6 -3 5 -12 5167.71 492.029 7 -3 5 -12 4407.37 764.667 3 3 5 12 3766.01 851.065 3 -3 -5 -12 4920.52 469.943 5 3 5 12 4721.45 513.678 4 -3 -5 -12 5447.05 570.916 4 3 -5 12 4841.97 456.579 7 3 5 13 36859.7 1365.11 6 -3 5 -13 37474.8 1350.55 7 3 5 13 41184.9 2770.54 3 -3 5 -13 35388.7 2092.09 3 -3 -5 -13 38498.1 1330.42 5 3 5 13 33724.2 1392.95 4 -3 -5 -13 38340.7 1550.29 4 3 -5 13 33896 1232.31 7 3 5 14 67146.4 1890.48 6 -3 5 -14 63992.3 2799.39 3 3 -5 14 62785.5 1721.28 7 -3 -5 -14 67391.1 1795.76 5 -3 5 -15 44353.5 2314.89 3 3 5 15 39977.8 1612.54 4 3 -5 15 40615.1 1423.04 7 -3 -5 -15 43885.6 1482.22 5 -3 5 -16 14620.2 1313.57 3 3 5 16 16771.4 1076.59 4 3 -5 16 17481 963.824 7 -3 -5 -16 17056.5 952.901 5 -3 5 -17 11044 1132.47 3 3 5 17 9333.58 832.064 4 3 5 17 10111.4 719.898 5 3 -5 17 9652.84 741.431 7 -3 -5 -17 12043 819.837 5 -3 5 -18 8500.95 973.543 3 -3 -5 -18 9870.72 764.565 5 3 -5 18 11815.3 849.484 5 3 5 18 10206.8 735.05 5 3 5 18 9718.63 865.858 4 3 -5 18 10262 788.564 7 3 -5 19 975.759 268.648 7 -3 5 -19 985.435 331.75 3 3 -5 19 220.758 121.978 5 -3 -5 -19 671.492 208.706 5 3 5 19 1010.13 235.923 5 3 5 19 826.322 277.455 4 -3 -5 -20 2483 400.544 5 -3 5 -20 1897.08 436.987 3 3 5 20 1706.05 397.633 4 3 -5 20 1833.49 372.416 7 -3 -5 -21 436.975 214.135 5 3 5 21 348.993 217.921 4 3 -5 21 459.643 223.233 7 -3 -5 -22 5544.67 635.351 5 3 -5 22 5321.93 647.672 7 3 5 22 4760.03 700.228 4 -3 -5 -23 7057.58 737.243 5 3 5 23 5683.51 789.25 4 3 -5 23 7030.93 751.706 7 3 5 24 22759.2 1574.08 4 3 -5 24 24337.6 1440.42 7 3 -5 25 1901.37 423.995 7 3 5 25 2312.44 535.097 4 3 -5 26 15816.5 1220.88 7 3 -5 27 5874.43 768.398 7 3 -6 -26 -166.884 221.991 1 3 6 -26 -118.904 222.406 1 3 6 -25 61.3865 174.595 1 3 -6 -25 -233.624 265.2 1 3 -6 -25 29.0568 167.155 5 -3 -6 24 9507.35 1031.68 7 3 -6 -24 11069.8 1157.63 5 -3 6 24 9912.92 1079.45 4 3 -6 -24 10544.2 1211.62 1 3 6 -24 11168.9 1218.08 1 3 -6 -23 2252.55 526.126 5 -3 6 23 2851.81 583.022 4 3 6 -23 2203.6 571.14 1 3 -6 -23 1499.73 446.062 1 -3 -6 23 2065.79 505.744 7 -3 -6 22 8985.9 935.894 7 -3 6 22 8163.98 944.945 4 3 6 -22 8309.96 996.845 1 3 -6 -22 7582.19 960.557 1 3 -6 -22 9606.75 1038.3 5 -3 -6 21 8690.16 904.99 7 3 -6 -21 8288.49 944.027 5 -3 6 21 7749.08 885.462 4 3 6 -21 7150.34 901.936 1 3 -6 -21 6282.23 862.513 1 3 -6 -20 871.886 324.234 5 -3 6 20 154.893 186.947 4 -3 -6 20 720.287 267.473 7 3 6 -20 903.59 334.146 1 3 -6 -20 690.354 319.412 1 3 -6 -19 2239.88 471.733 5 -3 6 19 1508.42 394.795 4 3 6 -19 1594.72 421.602 1 3 -6 -19 1434.32 391.809 1 -3 -6 19 2013.67 429.75 7 3 -6 -18 9579.61 944.417 5 -3 -6 18 9284.78 868.627 7 -3 6 18 8729.39 870.395 4 3 6 -18 8289.93 886.334 1 3 -6 -18 8486.61 897.297 1 3 -6 -17 70774.1 2486.58 5 -3 -6 17 62892.5 2198.07 7 -3 6 17 66323.1 2325.75 4 3 -6 -17 66624 2408.76 1 3 6 -17 70256.9 2476.82 1 -3 -6 16 16000.8 1087.69 7 3 -6 -16 15457 1120.82 1 3 6 -16 15745 1143.04 1 -3 6 16 15861.1 1122.4 4 3 -6 -16 16863.5 1196.17 5 -3 -6 15 34503.1 1560.58 7 3 -6 -15 37734.4 1747.99 5 3 6 -15 35857.8 1650.64 1 3 -6 -15 34283.8 1608.95 1 -3 6 15 34123.7 1591.75 4 -3 -6 14 1272.43 311.769 7 3 -6 -14 1295.52 329.222 5 -3 6 14 973.87 294.327 4 3 -6 -14 1158.6 309.881 1 3 6 -14 1086.36 297.818 1 3 6 -14 881.114 151.724 3 3 6 -13 353.283 165.978 3 -3 -6 13 357.58 174.025 7 3 -6 -13 401.294 213.279 5 3 -6 -13 371.79 177.657 1 3 6 -13 97.5169 128.124 1 -3 6 13 148.956 139.454 4 3 6 -12 234.796 135.053 3 -3 -6 12 180.051 146.305 7 3 -6 -12 78.4904 141.746 5 -3 6 12 103.589 126.983 4 3 -6 -12 143.87 141.824 1 3 6 -12 130.235 141.346 1 3 -6 -11 65755.5 1898.72 1 3 6 -11 65966.8 1951.3 1 -3 -6 11 62042.9 1909.94 7 3 6 -11 65689.1 2162.47 3 3 -6 -11 69703.3 2183.08 5 3 -6 -11 72893 2224.4 4 -3 6 11 63564.9 1972.45 4 -3 6 10 -61.0635 84.693 2 -3 -6 10 -51.8764 143.523 2 3 -6 -10 -33.9935 121.978 1 3 6 -10 -86.4829 137.931 1 -3 -6 10 28.4119 110.603 7 3 6 -10 103.532 159.249 7 3 6 -10 -23.1152 146.801 3 -3 6 10 51.307 116.925 6 3 -6 -10 203.721 177.425 5 3 -6 -10 289.956 192.856 4 -3 6 10 159.231 139.708 5 -3 6 10 -55.7423 140.363 4 -3 6 9 56857.6 2196.97 2 -3 -6 9 58555.7 2225.85 2 3 -6 -9 52864.4 1581.61 1 3 6 -9 59329.1 1668.13 1 -3 -6 9 58057.3 1778.37 7 3 6 -9 63757.4 1963.25 7 3 6 -9 56758.5 2199.5 3 3 -6 -9 61669.8 1976.6 5 -3 6 9 58509.6 1775.35 5 3 -6 -9 61698 1958.21 4 -3 6 9 58890.1 1822.32 4 -3 -6 8 3914.91 560.165 2 -3 6 8 3620.51 544.72 2 3 6 -8 4118.53 430.477 1 3 -6 -8 3385.23 389.755 1 -3 -6 8 3678.25 452.52 7 3 6 -8 3651.1 470.6 7 3 6 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234.802 4 4 -3 4 2265.75 260.466 4 4 3 4 1822.53 206.173 4 4 3 5 121569 3001.71 2 4 -3 5 125616 3053.82 2 4 3 5 125888 1847.11 7 4 -3 5 123494 1369.67 7 4 3 5 132886 4115.2 3 -4 3 -5 128392 1380.97 7 -4 -3 -5 125491 1535.54 5 4 -3 5 125207 1625.47 5 -4 -3 -5 126700 1796.29 4 4 3 5 123502 1718.68 4 4 -3 5 125011 1961.64 4 4 -3 6 1693.67 173.994 7 4 3 6 1599.96 220.089 7 -4 3 -6 1610.45 165.828 7 4 3 6 1957.06 193.724 6 4 3 6 1724.41 511.209 3 -4 -3 -6 1064.01 393.302 3 -4 3 -6 1762.09 491.078 3 -4 -3 -6 1554.22 210.691 4 -4 -3 -6 1690.29 182.179 5 4 3 6 1593.89 213.77 4 4 3 7 46058.9 970.153 6 -4 3 -7 45267.2 923.577 7 -4 3 -7 45576.2 2366.16 3 -4 -3 -7 42339.7 2251.7 3 4 3 7 49072.6 2603.55 3 -4 -3 -7 45922.8 950.686 5 -4 -3 -7 48868.8 1216.09 4 4 3 7 44128.6 1140.79 4 4 -3 7 43110.5 902.839 7 4 3 7 46691.9 1182.81 7 4 -3 8 21698.3 673.025 7 4 3 8 21670.7 827.447 7 4 3 8 22004.6 703.463 6 -4 -3 -8 22526.8 682.933 5 -4 3 -8 18813.4 1520.51 3 4 3 8 23475.2 1840.41 3 4 3 8 21161.4 829.117 4 -4 -3 -8 21241.8 1620.53 3 4 3 9 8022.44 1103.46 3 4 3 9 7436.17 521.917 4 4 -3 9 7068.87 405.172 7 4 3 9 7243.23 495.923 7 -4 -3 -9 7458.29 405.643 5 4 3 10 34488.4 2303.56 3 -4 3 -10 -91.2374 154.877 3 4 3 10 290.247 127.087 4 4 -3 10 30672.1 891.525 7 -4 -3 -10 30436.4 843.476 5 4 3 11 27122.4 1074.91 4 4 -3 11 29566.3 928.141 7 -4 -3 -11 29469.5 855.882 5 4 3 12 10355.7 1321.52 3 -4 -3 -12 9688.6 510.443 5 4 3 12 9714.86 673.887 4 4 -3 12 9957.06 574.806 7 -4 -3 -13 1063.43 181.676 5 4 3 13 931.195 233.517 4 4 -3 13 994.73 205.011 7 -4 -3 -14 20116.8 791.162 5 4 -3 14 18499.5 784.857 5 -4 3 -14 17330.8 1516.83 3 4 3 14 21683.3 1981.31 3 4 3 14 19350.5 1022.87 4 4 -3 14 20217 905.535 7 4 -3 15 7135.39 505.118 5 -4 -3 -15 7114.09 489.324 5 4 3 15 8031.05 1233.53 3 -4 3 -15 7136.88 974.487 3 4 3 15 6490.6 457.584 5 4 3 15 7130.08 652.182 4 4 -3 15 7023.15 568.394 7 -4 -3 -16 1416.8 231.886 5 4 -3 16 1181.87 224.259 5 -4 3 -16 1271.15 430.266 3 4 3 16 1687.35 651.216 3 4 3 16 1367.13 216.547 5 4 3 16 1224.6 280.273 4 4 -3 16 1441.02 286.722 7 -4 -3 -17 1225.72 224.596 5 -4 3 -17 789.782 327.586 3 4 3 17 1338.1 229.235 5 4 3 17 1071.16 283.465 4 4 -3 17 1372.35 285.221 7 4 -3 18 2008.21 298.613 5 -4 -3 -18 1734.15 275.236 5 -4 3 -18 1740.85 483.341 3 4 3 18 1413.22 332.553 4 4 -3 18 1485.51 300.422 7 4 -3 19 10956.7 711.249 5 -4 3 -19 10732.7 1203.36 3 4 -3 19 11373.9 832.115 7 4 3 19 10167 650.592 5 4 3 19 10064 885.481 4 -4 3 -20 33368.1 2090.37 3 4 -3 20 37139.1 1554.96 7 4 3 20 33480.6 1648.9 4 -4 3 -21 6297.64 938.573 3 4 3 21 5093.07 668.35 4 4 -3 21 6176.89 663.857 7 4 3 22 14589.3 1163.87 4 4 -3 22 15929.3 1087.2 7 4 3 23 360.537 245.431 4 4 -3 23 532.901 234.76 7 4 3 24 10733.1 1067.08 4 4 -3 24 12652 1051.73 7 4 3 25 2002.23 486.501 4 -4 3 -25 2597.27 521.262 6 4 -3 25 2674.53 505.635 7 4 3 26 834.986 312.728 4 4 -3 26 1070.93 328.024 7 -4 3 -26 1135.36 366.411 6 4 3 27 3500.73 620.334 7 -4 3 -27 3841.06 646.147 6 4 -4 -26 11471.9 1193.04 5 4 4 -26 13147.3 1421.04 1 4 -4 -26 11382.7 1333.56 1 4 -4 -25 22034.7 1611.93 5 4 -4 -25 18702.5 1679.71 1 4 4 -25 20921.8 1740.27 1 -4 4 25 19978.1 1518.72 4 4 4 -25 17874.4 1472.5 6 -4 -4 25 21990.9 1647.12 7 4 -4 -24 3064.76 614.976 5 4 -4 -24 2373.4 593.769 1 4 4 -24 2806.48 641.208 1 -4 4 24 2322.62 555.646 4 -4 -4 24 2537.77 579.064 7 4 -4 -23 9765.57 1029.8 5 4 -4 -23 8326.47 1064.15 1 4 4 -23 10460.1 1179.34 1 -4 4 23 9810.7 1024.28 4 -4 -4 23 11392.1 1108.02 7 4 -4 -22 1085.32 379.88 5 4 4 -22 694.132 303.359 1 4 -4 -22 768.244 338.411 1 -4 4 22 543.131 276.845 4 -4 -4 22 548.78 220.377 7 4 -4 -21 6481.98 811.892 5 4 -4 -21 6924.43 918.32 1 4 4 -21 6158.86 863.363 1 -4 4 21 5489.94 733.917 4 -4 -4 21 7498.44 863.985 7 4 -4 -20 42.8035 165.674 5 4 -4 -20 286.267 200.453 1 -4 4 20 30.8781 143.204 4 -4 -4 20 109.6 208.655 7 4 -4 -19 21507.4 1384.24 5 4 -4 -19 22549.4 1547.19 1 4 4 -19 22873.5 1553.72 1 -4 4 19 21560.7 1341.54 4 -4 -4 19 25688.1 1504.8 7 4 -4 -18 35.5215 169.904 5 4 -4 -18 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68575.7 1572.09 7 5 -3 10 68004.2 1237 7 5 -3 11 1887.38 224.812 7 -5 -3 -11 1984.59 199.895 5 -5 3 -11 1575.25 485.136 3 5 3 11 2707.88 715.5 3 5 3 11 1083.29 219.691 4 -5 -3 -11 2318.87 644.289 3 -5 3 -12 27094.8 2051.74 3 5 3 12 29031.6 2350.41 3 5 3 12 25155.1 1081.36 4 5 -3 12 25562.6 853.805 7 -5 -3 -12 26454.8 746.943 5 -5 3 -13 2429.45 636.024 3 5 3 13 3709.58 887.505 3 5 3 13 3039.87 399.166 4 5 -3 13 3255.75 323.584 7 -5 -3 -13 2388.82 241.098 5 5 -3 13 3178.18 292.28 5 -5 3 -14 9803.46 1264.2 3 5 3 14 8662.63 687.397 4 5 -3 14 8740.27 559.335 7 5 -3 14 8711.02 495.704 5 -5 -3 -14 9974.88 496.18 5 -5 3 -15 7765.01 1123.25 3 -5 -3 -15 7879.89 463.232 5 5 -3 15 8088.71 492.807 5 5 3 15 6422.05 621.212 4 5 -3 15 7578.79 549.372 7 5 -3 16 460.332 126.666 5 -5 -3 -16 740.635 163.324 5 -5 3 -16 686.503 372.928 3 5 3 16 411.671 194.635 4 5 -3 16 500.914 165.867 7 5 -3 17 1910.02 259.119 5 -5 3 -17 1338.54 505.566 3 5 3 17 1587.67 342.178 4 5 -3 17 2281.67 336.982 7 5 -3 18 12476.9 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806.857 3 -5 4 0 4533.63 457.589 1 -5 -4 0 3751.62 415.193 1 5 -4 0 5026.17 432.897 5 -5 4 0 4158.09 561.976 2 5 -4 0 4247.73 586.589 2 -5 -4 0 4700.12 607.333 2 5 4 0 4882.57 616.952 2 -5 -4 0 5157.46 351.52 4 -5 4 0 4869.88 405.458 4 5 -4 0 5490.94 437.024 4 -5 -4 -1 15468.4 1337.09 3 5 4 1 18846.3 1643.16 3 -5 -4 -1 16399.7 745.778 7 -5 4 -1 16749.2 587.545 7 5 4 1 17115.3 781.352 7 5 -4 1 16911.8 766.798 5 5 4 1 16002.5 617.754 4 -5 4 -1 15146.5 715.19 4 5 -4 1 16461.7 746.267 4 -5 -4 -1 16913 637.627 4 5 -4 1 14588.6 1070.82 2 5 4 1 16173.9 1130.84 2 5 -4 2 1288.41 341.369 2 5 4 2 1218.39 324.669 2 5 4 2 1537.64 565.694 3 -5 -4 -2 1157.44 465.826 3 -5 -4 -2 1170.47 223.339 7 5 4 2 1007.63 199.359 7 -5 4 -2 1289.58 162.119 7 5 -4 2 1375.26 219.987 5 5 -4 2 1186.97 205.839 4 5 4 2 1110.79 170.706 4 -5 -4 -2 1118.4 170.562 4 5 -4 3 30636.3 1587.38 2 5 4 3 30094 1578.9 2 -5 -4 -3 32033.4 2002.43 3 5 4 3 32170.9 2226.97 3 5 4 3 31043.9 1041.19 7 -5 4 -3 31789.4 769.634 7 -5 -4 -3 30836.7 1016.03 7 5 -4 3 30992.9 987.328 5 -5 -4 -3 33663.3 944.292 4 5 -4 3 31386.6 1053.57 4 5 4 3 30946.3 889.371 4 5 -4 4 4947.41 659.497 2 5 4 4 5078.87 677.801 2 -5 4 -4 4543.97 293.563 7 5 4 4 4137.33 386.003 7 5 4 4 5218.86 926.737 3 -5 -4 -4 5803.12 892.293 3 -5 -4 -4 4308.92 348.055 4 5 -4 4 4723.54 383.848 5 5 -4 4 4367.49 401.054 4 5 4 4 5139.73 374.455 4 5 -4 5 11904.8 1043.48 2 5 4 5 11693.8 1025.65 2 -5 4 -5 14294.1 530.113 7 5 4 5 13535.6 690.986 7 5 -4 5 12806.4 488.15 7 -5 -4 -5 13609.2 1366.94 3 5 4 5 15034.5 1593.67 3 5 -4 5 13766.3 639.177 5 -5 -4 -5 13295.2 632.279 4 5 4 5 13555.5 630.141 4 5 -4 5 12998.7 707.739 4 5 -4 6 15304 1199.23 2 5 4 6 16467 1242.99 2 -5 -4 -6 16530.4 1533.02 3 5 -4 6 15917.4 556.048 7 5 4 6 17004.6 786.509 7 -5 4 -6 17467.2 582.142 7 5 4 6 17198.5 617.179 6 5 4 6 19712.9 1845.79 3 5 -4 6 15846.8 677.326 5 -5 -4 -6 16704.2 652.173 5 -5 -4 -6 17181.8 744.314 4 5 4 6 15837.3 700.741 4 -5 4 -6 16258.6 1615.6 3 5 -4 6 17427.3 835.744 4 5 -4 7 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538.655 2 9 -6 2 2445.58 371.937 4 9 6 3 15156.1 958.736 7 9 -6 3 15421.7 932.545 5 -9 6 -3 15742.5 2226.78 3 9 -6 3 14021.4 1500.79 2 9 6 3 13968 1486.54 2 9 -6 3 13976.8 878.73 4 9 6 4 3577.59 479.268 7 -9 6 -4 3707.8 1085.47 3 9 -6 4 4365.68 494.884 5 9 -6 4 3926.24 476.589 4 9 -6 4 4446.51 875.305 2 9 6 4 3354.29 755.355 2 9 6 5 151.276 144.56 7 9 -6 5 291.555 147.229 5 9 -6 5 -31.5215 90.5913 4 9 -6 5 225.379 348.376 2 9 6 5 27.4565 306.247 2 9 -6 6 3451.88 796.062 2 9 6 6 4617.7 884.833 2 9 6 6 3317.22 441.009 7 9 -6 6 4401.09 471.244 5 -9 -6 -6 4829.29 438.283 5 9 6 6 3828.38 360.816 4 9 -6 6 3764.77 478.25 4 9 6 7 34502 1124.08 4 9 -6 7 33304.5 1248.24 5 -9 6 -7 36881.8 3384.83 3 -9 -6 -7 37236.8 1157.25 5 9 -6 7 34888.5 2464.56 2 9 6 7 36319.6 2499.79 2 -9 6 -8 -300.31 384.817 3 9 -6 8 -492.514 368.606 2 9 6 8 -125.332 334.72 2 9 6 8 -94.5071 60.5492 4 9 -6 8 142.451 111.61 5 -9 6 -9 68953.5 4600.93 3 9 -6 9 71491.2 3619.14 2 9 6 9 62885.4 3362.32 2 9 -6 9 68229.5 1686.04 5 -9 6 -10 1280.55 659.092 3 9 6 10 1418.47 264.767 4 9 -6 10 305.879 358.964 2 9 6 10 1067.96 517.296 2 9 -6 11 8892.57 1322.98 2 9 6 11 8379.99 1298.94 2 -9 6 -11 9729.52 1729.53 3 9 -6 12 1072.29 520.375 2 9 6 12 319.193 349.66 2 -9 6 -12 1346.59 532.696 3 9 -6 13 14751.8 1792.74 2 9 6 13 18148.1 1956.75 2 -9 6 -13 15876.5 2251.33 3 9 -6 14 3018.76 846.351 2 9 6 14 2433.27 765.523 2 -9 6 -14 1920.76 824.312 3 9 -6 15 13206.7 1776.76 2 9 6 15 11754.3 1642.24 2 -9 6 -15 15110.7 2246.15 3 9 -6 16 6402.25 1226.27 2 9 6 16 6978 1316.18 2 -9 6 -16 6498.74 1454.26 3 9 6 17 5068.09 1136.8 2 9 -6 17 4426.15 1066.21 2 -9 6 -17 5708.05 1419.94 3 9 -6 18 3833.69 1035.06 2 9 6 18 2985.67 913.526 2 -9 6 -18 2549.88 910.066 3 -9 6 -19 -345.265 361.476 3 9 -7 -20 893.901 412.037 1 9 7 -20 373.621 313.481 1 -9 7 20 990.036 393.552 4 9 7 -19 652.566 395.802 1 -9 7 19 9.06183 198.843 4 9 -7 -18 2247.33 579.016 1 9 7 -18 3749.85 713.739 1 -9 -7 18 3519.27 640.099 7 -9 7 18 3025.49 573.78 4 9 -7 -17 19076.2 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467.629 5 -9 -7 6 229.352 158.42 7 -9 7 6 215.426 184.401 4 9 -7 -6 322.192 208.537 5 -9 -7 5 1419.77 334.351 7 -9 7 5 929.921 282.305 4 9 -7 -5 1065.28 325.144 5 -9 -7 4 1757.19 371.374 7 9 -7 -4 1467.61 544.521 2 9 7 -4 454.035 287.422 2 -9 7 4 1434.42 322.637 4 9 -7 -4 1627.46 402.011 5 -9 -7 3 7906.65 746.057 7 9 -7 -3 6719.75 1048.98 2 9 7 -3 7228.18 1051.47 2 -9 7 3 7309.49 695.364 4 9 -7 -3 7342.27 772.725 5 9 -7 -2 619.477 234.133 5 9 -7 -2 183.852 280.506 2 9 7 -2 563.934 365.664 2 -9 -7 2 1002.89 286.41 7 9 -7 -1 2171.8 418.925 5 9 -7 -1 1800.75 578.083 2 9 7 -1 3086.34 751.024 2 -9 -7 1 2124.59 392.647 7 9 -7 0 5494.78 639.73 5 9 -7 0 6306.8 1029.6 2 9 7 0 5042.86 912.308 2 -9 -7 0 5948.33 637.445 7 9 -7 1 4302.84 548.852 5 9 -7 1 5075.16 895.129 2 9 7 1 4258.88 815.43 2 -9 -7 -1 4735.08 566.885 7 9 -7 2 5655.54 621.075 5 9 -7 2 5393.71 953.049 2 9 7 2 6422.29 1008.46 2 -9 -7 -2 5735.59 613.249 7 9 -7 3 12237.2 902.23 5 9 -7 3 10968 1328.51 2 9 7 3 11588.9 1351.64 2 9 -7 4 8271.96 723.905 5 -9 7 -4 7329.95 1517.04 3 9 -7 4 6433.83 1037.24 2 9 7 4 7360.39 1097.45 2 9 -7 5 1762.11 344.074 5 -9 7 -5 2122.85 751.751 3 9 -7 5 1878.74 568.796 2 9 7 5 1898.96 599.584 2 9 -7 6 11346.8 828.502 5 -9 7 -6 12638.1 2081.19 3 -9 -7 -6 13289.4 787.563 5 9 -7 6 9356.81 1258.4 2 9 7 6 12311.5 1456.47 2 9 7 7 8248.99 611.947 4 9 -7 7 8004.99 688.742 5 -9 -7 -7 8663.8 631.317 5 9 -7 7 6856.36 1098.91 2 9 7 7 8529.08 1211.92 2 -9 7 -8 13454.4 2124.42 3 9 -7 8 12684 1513.33 2 9 7 8 12130.9 1476.14 2 9 7 8 11663.8 750.162 4 9 -7 8 12900 852.085 5 9 -7 9 31347 2403.89 2 9 7 9 33293.7 2458.15 2 -9 7 -9 30928.3 3201.2 3 9 -7 10 18666.5 1896.62 2 9 7 10 16815.1 1783.55 2 -9 7 -10 18541.8 2484.76 3 9 -7 11 12260.6 1566.67 2 9 7 11 13416.4 1625.15 2 -9 7 -11 15139.1 2259.98 3 9 -7 12 12201.5 1608.57 2 9 7 12 15008.9 1738.28 2 -9 7 -12 14265.8 2166.69 3 9 -7 13 296.383 317.488 2 -9 7 -13 -252.52 314.162 3 9 -7 14 2608.55 776.712 2 9 7 14 2810.47 796.219 2 9 -7 15 10485.3 1568.68 2 9 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9 -8 2 785.733 274.005 5 9 -8 2 301.071 236.213 2 9 8 2 764.515 386.771 2 -9 -8 -2 438.795 206.059 7 9 -8 3 99.9696 171.209 5 9 -8 3 314.248 267.819 2 9 8 3 -76.3352 198.014 2 9 -8 4 281.353 235.382 5 9 -8 4 325.47 199.561 2 9 8 4 536.361 345.508 2 9 -8 5 1327.46 329.296 5 9 -8 5 1680.08 523.065 2 9 8 5 1950.89 608.78 2 -9 8 -5 844.873 556.104 3 9 -8 6 9774.56 833.463 5 9 8 6 7618.72 1133.19 2 9 -8 6 9771.01 1280.8 2 -9 -8 -6 9868.94 753.318 5 -9 8 -6 7019.81 1583.86 3 9 -8 7 654.068 230.802 5 -9 8 -7 470.104 494.866 3 9 -8 7 419.029 338.487 2 9 8 7 457.322 365.517 2 9 -8 8 5973.66 650.4 5 9 -8 8 5962.3 1049.89 2 9 8 8 4918.52 966.363 2 -9 8 -8 7491.98 1685.78 3 9 -8 9 -300.996 306.864 2 9 8 9 342.502 311.802 2 -9 8 -9 40.3077 272.842 3 9 -8 10 36180.5 2615.5 2 9 8 10 37203 2622.08 2 -9 8 -10 36527.2 3620.11 3 9 -8 11 -35.0578 285.457 2 -9 8 -11 775.382 544.806 3 9 -8 12 31595.7 2537.61 2 9 8 12 32183.6 2544.87 2 -9 8 -12 30119.1 3269.73 3 9 -8 13 -322.851 368.983 2 9 8 13 -251.061 297.163 2 -9 8 -13 -993.384 613.683 3 9 -8 14 592.725 361.494 2 9 8 14 1262.37 620.714 2 -9 8 -14 218.121 293.508 3 9 8 15 -730.915 454.733 2 9 -8 15 -528.857 437.208 2 -9 8 -15 513.58 452.988 3 9 -8 16 33062.3 2785.86 2 9 8 16 31804 2710.56 2 -9 8 -16 35171.5 3490.27 3 9 8 17 935.511 546.504 2 -9 9 17 8179.42 976.843 4 -9 9 16 -203.759 225.1 4 -9 9 15 36288.2 1974.7 4 -9 -9 14 5366.85 785.739 7 -9 9 14 4560.89 704.88 4 9 -9 -13 4493.01 770.457 5 -9 -9 13 4144.37 682.045 7 -9 9 13 3035.14 585.507 4 9 -9 -12 4203.54 750.028 5 -9 -9 12 5019.69 729.891 7 -9 9 12 3775.36 629.84 4 9 -9 -11 975.264 371.534 5 -9 -9 11 933.231 358.298 7 -9 9 11 626.572 273.84 4 9 -9 -10 8835.77 1031.57 5 -9 -9 10 8900.41 946.112 7 -9 9 10 8692.94 917.248 4 9 -9 -9 11560.8 1164.47 5 -9 -9 9 9747.71 979.703 7 -9 9 9 9258.38 924.724 4 9 -9 -8 6736.17 881.794 5 -9 -9 8 6969.48 828.549 7 -9 9 8 7106.87 809.008 4 9 -9 -7 617.369 309.938 5 -9 -9 7 1080.12 365.532 7 -9 9 7 370.654 218.259 4 9 -9 -6 5418.76 772.057 5 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1276.16 5 9 -9 6 20164.5 1816.83 2 9 9 6 21112.2 1850.21 2 -9 9 -6 23926.6 3055.49 3 9 -9 7 6491.07 730.623 5 -9 9 -7 6903.7 1639.71 3 9 -9 7 6233.81 1044.35 2 9 9 7 7534.62 1154.33 2 -9 9 -8 33174.5 3595.76 3 9 -9 8 26973.3 2154.46 2 9 9 8 28382.2 2225.59 2 -9 9 -9 7170.62 1789.23 3 9 9 9 8568.05 1249.37 2 9 -9 9 9758.46 1315.65 2 -9 9 -10 26872.4 3228.53 3 9 -9 10 27318.8 2251.5 2 9 9 10 26056.5 2193.7 2 -9 9 -11 16409 2527.23 3 9 -9 11 15605.4 1728.6 2 9 9 11 14721.1 1673.71 2 -9 9 -12 7972.34 1774.89 3 9 -9 12 8205.93 1288.72 2 9 9 12 5556.71 1046.58 2 -9 9 -13 -63.5629 223.201 3 9 -9 13 326.308 388.1 2 9 9 13 -397.614 356.33 2 -9 9 -14 4083.74 1219.73 3 9 -9 14 5050.45 1075.93 2 9 9 14 6011.88 1152.94 2 -9 9 -15 7809.58 1743.36 3 -9 10 14 -289.913 252.685 4 -9 10 13 626.553 293.853 4 -9 10 12 8628.46 983.081 4 9 -10 -11 2139.05 584.371 5 -9 -10 11 2359.54 523.049 7 -9 10 11 1844.05 465.353 4 9 -10 -10 4405.39 780.574 5 -9 -10 10 4263.28 692.236 7 -9 10 10 3089.17 577.534 4 9 -10 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409.437 4 10 -4 2 4280.93 874.15 2 10 4 2 3759.77 849.986 2 10 -4 3 134.794 83.9582 5 -10 4 -3 382.893 443.021 3 -10 -4 -3 53.9986 270.004 3 10 -4 3 130.954 293.397 2 10 4 3 127.774 306.987 2 10 4 3 -60.8799 54.6453 7 10 -4 4 3624.29 368.019 5 -10 4 -4 3901.82 1085.61 3 -10 -4 -4 3801.17 1011.4 3 10 -4 4 2847.66 753.197 2 10 4 4 4064.31 883.982 2 10 4 4 3838.8 391.826 7 10 -4 5 58.2831 63.5423 5 -10 4 -5 193.509 341.658 3 -10 -4 -5 -79.7548 314.941 3 10 -4 5 -489.766 377.223 2 10 4 5 -402.377 350.209 2 10 -4 6 50979.1 1142.83 5 10 -4 6 50173.1 3098.06 2 10 4 6 48083.3 3024.71 2 -10 -4 -6 49250.2 3445.7 3 -10 4 -6 53812.2 4027.02 3 10 -4 7 -196.854 344.085 2 10 4 7 809.113 488.35 2 -10 4 -7 452.458 501.944 3 -10 -4 -7 782.617 521.93 3 10 -4 8 4607.65 992.886 2 10 4 8 3567.66 853.075 2 -10 -4 -8 2442.46 833.537 3 -10 4 -8 3414.53 1100.51 3 10 -4 9 355.304 371.729 2 10 4 9 405.065 323.716 2 -10 -4 -9 -222.334 341.174 3 -10 4 -9 584.318 603.729 3 10 -4 10 483.63 408.003 2 10 4 10 -538.569 434.465 2 -10 4 -10 837.045 636.117 3 -10 -4 -10 -130.689 282.021 3 10 -4 11 7263.5 1287.04 2 10 4 11 6888.89 1230.33 2 -10 -4 -11 8085.53 1525.69 3 -10 4 -11 8250.47 1644.71 3 10 -4 12 12926.6 1755.43 2 10 4 12 11549.7 1638.49 2 -10 -4 -12 12439.8 1896.91 3 -10 4 -12 13861.4 2115.31 3 10 -4 13 33853.4 2876.71 2 10 4 13 35959.9 2907 2 -10 4 -13 32890.9 3248.9 3 -10 -4 -13 35338.6 3204.8 3 10 -4 14 25867.9 2550.16 2 10 4 14 26193.3 2529.15 2 -10 -4 -14 26588 2830.72 3 -10 4 -14 27509.2 2975.1 3 10 4 15 9961.58 1623.65 2 10 -4 15 11853.9 1748.87 2 -10 4 -15 12471.1 2006.7 3 10 -4 16 2503.15 856.306 2 10 4 16 2965.73 928.702 2 -10 4 -16 2731.26 947.968 3 -10 4 -17 2715.07 923.802 3 -10 4 -18 1171.52 592.868 3 -10 4 -19 5648.38 1333.2 3 -10 5 20 7552.32 891.893 4 10 5 -20 7586.25 961.761 6 -10 5 20 7154.42 931.501 7 -10 -5 19 9997.88 1060.89 7 10 5 -19 10632.8 1113.34 6 -10 5 19 10713.7 1091.25 7 10 -5 -19 9543.5 1233.13 1 10 5 -19 10896.3 1326.52 1 -10 5 19 9387 951.351 4 -10 -5 18 9708.4 1019.36 7 10 -5 -18 9539.08 1113.37 5 10 5 -18 10093.4 1066.27 6 -10 5 18 9199.56 1004.79 7 10 -5 -18 11257.5 1323.24 1 10 5 -18 9957.63 1256.96 1 -10 5 18 7876.46 862.791 4 -10 -5 17 38547.6 1988.7 7 10 -5 -17 39872 2208.76 5 10 5 -17 36611.3 1947.91 6 -10 5 17 38508.5 1967.66 7 10 -5 -17 36678.6 2331.07 1 10 5 -17 37829 2393.23 1 -10 5 17 38331.9 1836.5 4 -10 -5 16 1252.88 383.818 7 10 -5 -16 2124.34 536.914 5 -10 5 16 1143.45 346.251 7 10 5 -16 1338.64 378.341 6 10 -5 -16 779.48 338.848 1 10 5 -16 893.207 362.656 1 -10 5 16 1136.73 337.786 4 -10 5 15 4494.18 635.489 7 10 5 -15 4085.25 623.41 6 -10 -5 15 3586.84 596.881 7 -10 5 15 3979.82 576.494 4 10 -5 -15 4291.83 700.108 5 10 5 -14 9034.79 894.811 6 -10 5 14 10269 939.564 7 10 -5 -14 11611.7 1146.2 5 -10 -5 14 9785.1 949.634 7 -10 5 14 9328.16 849.983 4 10 5 -13 2290.68 442.716 6 -10 -5 13 2495.83 636.852 3 10 -5 -13 2631.08 555.311 5 -10 -5 13 2414.91 467.991 7 -10 5 13 2768.9 465.135 4 10 5 -12 7742.91 780.285 6 -10 -5 12 6593.46 1058.66 3 10 -5 -12 8034.16 909.524 5 -10 -5 12 6350.58 727.827 7 -10 5 12 7453.53 717.238 4 10 5 -11 9605.8 835.539 6 -10 -5 11 8627.3 1219.51 3 10 -5 -11 10671 1033.98 5 -10 -5 11 9609.82 884.905 7 -10 5 11 10409.7 826.676 4 10 5 -10 26655.5 1332.83 6 -10 -5 10 26829.3 2155.39 3 10 -5 -10 26829.9 1583.01 5 -10 -5 10 25227.9 1386.48 7 -10 5 10 26666.5 1276.08 4 10 5 -9 1031.56 262.883 6 -10 -5 9 1316.36 531.547 3 10 -5 -9 942.662 306.178 5 -10 -5 9 908.905 282.693 7 -10 5 9 724.33 207.902 4 10 5 -8 3415.39 452.767 6 -10 -5 8 3038.18 785.944 3 10 -5 -8 2995.25 520.831 5 -10 -5 8 3088.72 473.551 7 -10 5 8 2951.54 412.514 4 10 5 -7 145.639 125.154 6 10 -5 -7 89.3219 170.994 5 -10 -5 7 1.8867 126.959 7 -10 5 7 14.0235 111.154 4 -10 -5 6 17022 1058.65 7 10 5 -6 16106.6 879.159 6 -10 -5 6 16616.7 1803.94 3 10 -5 -6 16599 1148.22 5 10 -5 -6 15695.6 1693.26 2 10 5 -6 16295.5 1734.9 2 -10 5 6 17042 931.652 4 -10 -5 5 1840.67 361.462 7 10 5 -5 45.7277 51.7065 6 -10 -5 5 2275.02 731.089 3 -10 5 5 2501.78 975.226 3 10 -5 -5 1563.01 353.166 5 -10 5 5 1287.19 261.25 4 10 -5 -5 785.73 370.077 2 10 5 -5 422.101 317.48 2 10 -5 -4 11013.2 1404.73 2 10 5 -4 10416.1 1381.33 2 -10 -5 4 12247.3 862.867 7 10 5 -4 11783.4 670.053 6 10 5 -4 12408 892.836 7 -10 5 4 11552.4 663.417 7 -10 -5 4 10336.1 1443.69 3 -10 5 4 13679.4 2166.77 3 10 -5 -4 11914.1 930.551 5 10 -5 -4 12292.5 767.681 4 -10 5 4 12623.1 775.974 4 -10 -5 3 47222.8 1662.46 7 10 5 -3 50501.2 1276.98 6 10 5 -3 50392.8 1745.26 7 -10 5 3 49414.5 1243.93 7 -10 5 3 51804.3 4047.2 3 -10 -5 3 45820.7 3071.94 3 10 -5 -3 48614.6 1820.5 5 10 -5 -3 47674.9 1481.18 4 10 -5 -3 47027.5 2899.99 2 10 5 -3 42434 2762.8 2 -10 -5 2 34319.4 1384.36 7 10 5 -2 36041.4 1459.17 7 10 5 -2 37397.5 998.556 6 -10 5 2 36575.3 965.443 7 -10 5 2 34878.7 1445.58 6 -10 5 2 38345.2 3503.8 3 -10 -5 2 34473 2696.53 3 10 -5 -2 34970.9 1508.68 5 10 -5 -2 35639.3 1260.03 4 10 -5 -2 32838.9 2420.79 2 10 5 -2 32949.3 2427 2 -10 5 1 8339.69 691.859 6 10 5 -1 7835.95 669.674 7 10 5 -1 8368.97 409.312 6 -10 5 1 9457.42 1736.97 3 -10 -5 1 8613.7 1377.67 3 10 -5 -1 9484.25 774.331 5 -10 -5 1 8985.09 733.504 5 10 -5 -1 8206.15 1218.64 2 10 5 -1 7556.93 1154.03 2 -10 -5 1 8260.76 666.855 7 10 5 0 69251.3 1943 7 -10 5 0 71253.5 1977.19 6 -10 5 0 71919 4782.78 3 -10 -5 0 64683.2 3754.4 3 10 -5 0 67172.2 1979.12 5 -10 -5 0 72637.4 1995.45 5 10 -5 0 64468.1 3367.35 2 10 5 0 68338.6 3469.51 2 -10 -5 0 71135.4 1903.53 7 10 5 1 4799.01 511.304 7 -10 5 -1 4132.51 1242.01 3 -10 -5 -1 4296.61 1037.46 3 10 -5 1 4334.17 492.092 5 10 -5 1 4062.39 859.847 2 10 5 1 3825.9 848.292 2 -10 -5 -1 4389.63 468.899 7 10 5 2 12073.4 798.175 7 -10 -5 -2 13341.5 1745.47 3 -10 5 -2 12059.5 1958.63 3 10 -5 2 11196.7 764.959 5 10 -5 2 9344.93 1314.75 2 10 5 2 10878.9 1423.14 2 -10 -5 -2 12548.5 781.871 7 10 -5 3 3255.39 401.168 5 -10 5 -3 1438.81 752.27 3 -10 -5 -3 2177.85 749.393 3 10 -5 3 3363.03 809.296 2 10 5 3 1302.32 525.269 2 10 5 3 2973.46 406.384 7 10 -5 4 10220.8 675.696 5 -10 5 -4 12491.8 1995.3 3 -10 -5 -4 9572.64 1526.04 3 10 -5 4 11294.2 1453.19 2 10 5 4 9494.91 1326.74 2 10 -5 5 4778.76 443.422 5 -10 -5 -5 2133.18 810.483 3 -10 5 -5 5475.09 1330.48 3 10 -5 5 3388.54 825.16 2 10 5 5 4075.79 882.71 2 10 -5 6 3725.92 372.772 5 -10 5 -6 5239.86 1298.6 3 -10 -5 -6 3309.49 955.837 3 10 -5 6 3541.85 865.363 2 10 5 6 3578.42 834.306 2 -10 5 -7 507.177 461.991 3 -10 -5 -7 -201.1 356.13 3 10 -5 7 413.776 311.396 2 10 5 7 1142.33 518.882 2 -10 -5 -8 2964.38 923.049 3 -10 5 -8 1172.88 644.496 3 10 -5 8 2053.99 700.521 2 10 5 8 3258.81 830.202 2 -10 5 -9 10814.7 1909.6 3 -10 -5 -9 9817.4 1646.62 3 10 -5 9 9382.97 1420.75 2 10 5 9 10619.5 1479.07 2 -10 5 -10 3259.02 1062.24 3 10 -5 10 1748.63 610.862 2 10 5 10 2188 694.736 2 -10 -5 -10 3852.45 1083.15 3 -10 5 -11 83.1803 326.823 3 10 5 11 351.971 317.487 2 -10 5 -12 12987.7 2067.9 3 10 5 12 12248.1 1665.06 2 10 -5 12 9916.28 1538.46 2 -10 5 -13 7063.59 1562.09 3 10 -5 13 6230.27 1232.48 2 10 5 13 5374.97 1164.73 2 -10 5 -14 17928.9 2446.91 3 10 -5 14 13338.3 1836.8 2 10 5 14 14788.3 1916.31 2 -10 5 -15 24938.6 2917.65 3 10 -5 15 28460 2702.76 2 10 5 15 24534.6 2489.03 2 -10 5 -16 14039.1 2175.15 3 10 -5 16 15024.6 1990.04 2 10 5 16 17339.9 2120.13 2 -10 5 -17 4181.27 1135.92 3 -10 5 -18 2774.68 958.539 3 10 6 -20 6009.51 885.4 6 -10 6 19 296.417 194.299 7 10 6 -19 752.641 332.598 6 -10 6 19 533.599 332.186 4 10 6 -18 12621.5 1202.4 6 -10 -6 18 13280.6 1216.62 7 10 -6 -18 13581.9 1425.65 1 10 6 -18 12627.8 1398.91 1 -10 6 18 10761.4 1040.23 4 10 6 -17 12594.7 1181.39 6 10 -6 -17 13235.6 1313.08 5 -10 -6 17 10793.4 1070.25 7 10 -6 -17 11070 1288.09 1 10 6 -17 11276.7 1292.19 1 -10 6 17 11372.3 1045.33 4 -10 -6 16 10941.3 1064.55 7 -10 6 16 8901.69 907.214 4 10 -6 -16 11615.8 1224.63 5 -10 -6 15 15788.5 1259.65 7 -10 6 15 14641.5 1129.64 4 10 -6 -15 16881.1 1437.02 5 -10 -6 14 3622.19 604.446 7 -10 6 14 2634.89 470.922 4 10 -6 -14 3363.65 646.2 5 -10 -6 13 2240.73 471.763 7 -10 6 13 3018.82 491.107 4 10 -6 -13 3232.27 627.196 5 -10 -6 12 4465.99 649.074 7 -10 6 12 3889.22 555.092 4 10 -6 -12 4456.38 709.167 5 -10 -6 11 63513.6 2323.54 7 -10 6 11 60366.6 2091.04 4 10 -6 -11 64907.3 2604.28 5 -10 -6 10 627.096 254.057 7 -10 6 10 401.533 175.763 4 -10 -6 9 61777 2217.16 7 -10 6 9 62258 2032.55 4 10 -6 -9 64742.9 2509.89 5 -10 -6 8 -6.4197 158.802 7 -10 6 8 -74.9243 160.86 4 10 -6 -8 -103.342 172.109 5 -10 -6 7 22.8026 126.741 7 10 -6 -7 224.403 195.557 5 -10 -6 7 2.73697 331.528 3 -10 6 7 199.15 177.871 4 10 -6 -6 8592.1 878.325 5 -10 -6 6 9402.47 824.878 7 -10 6 6 9095.92 742.102 4 -10 -6 6 10095.3 1460.01 3 -10 -6 5 49581 3176.22 3 -10 -6 5 51950.9 1899.7 7 10 -6 -5 47064.7 2908.83 2 10 6 -5 45342.6 2885.93 2 -10 6 5 49166.3 1684.92 4 10 -6 -5 51224.6 2054.77 5 -10 -6 4 5927.95 641.825 7 10 -6 -4 6397.56 727.812 5 10 -6 -4 5790.85 1049.56 2 10 6 -4 5654.88 1043.5 2 -10 -6 4 5722.62 1123.27 3 -10 6 4 6853.22 632.321 4 10 -6 -3 33673.1 1597.66 5 -10 -6 3 31148.3 1427.93 7 10 -6 -3 28249.5 2240.41 2 10 6 -3 29304.2 2298.54 2 -10 -6 3 33201.1 2662.31 3 -10 -6 2 22849.3 2239.07 3 -10 -6 2 22282.9 1188.13 7 10 -6 -2 21892.9 1257.97 5 10 -6 -2 22653.2 2019.31 2 10 6 -2 22581.4 2011.08 2 -10 6 2 22164.8 2772.45 3 10 -6 -1 6063.5 655.415 5 -10 -6 1 6741.58 647.208 7 10 -6 -1 5721.15 1055.48 2 10 6 -1 6143.51 1054.35 2 -10 -6 1 6408.11 1223.87 3 -10 6 1 6828.81 1529.93 3 10 -6 0 7935.24 727.142 5 -10 -6 0 8523.15 714.821 7 10 -6 0 7145.17 1131.44 2 10 6 0 7623.26 1165.02 2 -10 -6 0 5488.3 1153.96 3 -10 6 0 8317.77 1679.47 3 10 -6 1 255.909 128.272 5 -10 -6 -1 121.569 125.457 7 10 -6 1 -349.778 332.767 2 10 6 1 -671.038 423.647 2 -10 -6 -1 304.176 350.053 3 -10 6 -1 307.081 390.587 3 10 -6 2 -71.2878 151.693 5 -10 -6 -2 -186.979 138.785 7 -10 6 -2 -96.2257 326.875 3 10 -6 2 -167.066 297.174 2 10 6 2 333.17 346.721 2 -10 -6 -2 264.444 359.484 3 10 -6 3 11345.3 807.042 5 -10 6 -3 13169.7 2115.5 3 10 -6 3 10714.7 1393.33 2 10 6 3 12533.7 1507.31 2 -10 -6 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32784.1 2828.68 2 12 5 6 31803.6 2809.68 2 -12 5 -7 10983.3 2086.13 3 12 -5 7 11108 1683.78 2 12 5 7 12816 1803.67 2 -12 5 -8 14840.8 2421.39 3 12 -5 8 15785.3 2029.4 2 12 5 8 15185.8 1942.26 2 12 -5 9 1256.45 612.447 2 12 5 9 1891.5 668.623 2 -12 -6 15 986.611 314.151 7 -12 -6 14 -265.526 213.97 7 -12 -6 13 -125.245 169.065 7 12 -6 -13 1048.65 377.71 5 -12 -6 12 13600.1 1158.84 7 -12 6 12 12896.6 2360.95 3 12 -6 -12 14762.4 1344.4 5 -12 -6 11 -140.074 165.261 7 -12 6 11 216.135 406.454 3 12 -6 -11 51.9032 173.929 5 -12 -6 10 186.896 187.102 7 12 -6 -10 318.636 249.817 5 -12 6 9 3467.91 1232.61 3 -12 -6 9 2850.23 518.552 7 -12 -6 9 2327.31 782.535 3 12 -6 -9 2290.6 499.745 5 -12 -6 8 2232.53 440.379 7 -12 -6 8 2081.93 716.184 3 12 -6 -8 1439.38 400.918 5 -12 -6 7 1083.25 321.449 7 -12 -6 7 177.979 352.248 3 12 -6 -7 1167.38 377.843 5 -12 -6 6 10248.8 896.931 7 -12 6 6 8965.39 2009.3 3 -12 -6 6 7986.42 1445.54 3 12 -6 -6 10196 986.454 5 -12 6 5 12187 2303.63 3 -12 -6 5 10753.8 1658.55 3 -12 -6 5 12620.4 976.984 7 12 -6 -5 10757.1 1577.7 2 12 6 -5 10891.3 1588.38 2 12 -6 -5 12402.2 1073.77 5 12 -6 -4 2348.87 788.936 2 12 6 -4 2962.96 836.371 2 -12 6 4 3074.74 1245.84 3 -12 -6 4 3736.4 1020.99 3 12 -6 -4 3294.74 557.478 5 12 -6 -3 5773.33 1172.28 2 12 6 -3 4798.9 1048.28 2 -12 6 3 5838.89 1709.43 3 -12 -6 3 4519.12 1122.09 3 12 -6 -3 5878.95 706.837 5 12 -6 -2 -556.388 516.58 2 12 6 -2 -79.2295 268.13 2 -12 6 2 191.33 468.208 3 -12 -6 2 889.793 720.076 3 12 -6 -2 -449.858 205.959 5 -12 6 1 -243.724 784.75 3 -12 -6 1 1334.1 703.057 3 12 -6 -1 41.3862 358.829 2 12 6 -1 -443.425 397.191 2 -12 6 0 13504.9 2349.77 3 -12 -6 0 10794.8 1781.38 3 12 -6 0 10626.8 1561.68 2 12 6 0 11199.5 1620.36 2 -12 6 -1 2001.59 960.813 3 -12 -6 -1 1548.3 701.197 3 12 -6 1 -9.5805 323.582 2 12 6 1 900.036 391.962 2 -12 6 -2 691.299 350.274 3 12 -6 2 -182.94 384.047 2 12 6 2 15.9821 257.321 2 -12 -6 -2 281.79 464.294 3 -12 6 -3 4869.28 1430.97 3 12 -6 3 6999.57 1266.04 2 12 6 3 5339.58 1098.78 2 -12 -6 -3 5789.29 1356.93 3 -12 6 -4 490.027 449.499 3 12 -6 4 957.663 532.894 2 12 6 4 451.027 441.014 2 -12 -6 -4 1818.57 809.927 3 12 -6 5 -616.813 424.071 2 12 6 5 -410.554 456.633 2 12 -6 6 19571.4 2190.61 2 12 6 6 17681.4 2089.13 2 12 -6 7 4016.45 1003.1 2 12 6 7 2855.66 914.646 2 12 -6 8 998.943 549.12 2 12 6 8 1084.97 584.889 2 12 -6 9 40102.8 3213.27 2 12 6 9 41176.3 3250.1 2 -12 -7 13 18016 1386.14 7 -12 -7 12 -5.80652 212.825 7 -12 -7 11 495.634 315.801 7 12 -7 -11 -93.9669 197.034 5 -12 -7 10 176.733 161.158 7 12 -7 -10 226.872 299.094 5 -12 -7 9 7459.09 837.086 7 12 -7 -9 7296.95 931.72 5 -12 -7 8 7947.33 861.83 7 12 -7 -8 7789.52 943.632 5 -12 -7 7 43251.8 1960.03 7 12 -7 -7 40867.9 2106.18 5 -12 -7 6 1760.11 419.386 7 12 -7 -6 2143.48 500.467 5 12 -7 -5 15071.9 1235.6 5 12 -7 -4 -176.999 455.491 2 12 7 -4 147.997 380.973 2 12 -7 -4 501.221 255.201 5 12 -7 -3 8842.99 1436.63 2 12 7 -3 8365.02 1441.25 2 12 -7 -3 9534.54 948.631 5 12 -7 -2 4190.27 995.314 2 12 7 -2 5419.32 1124.42 2 12 -7 -1 2300.52 833.586 2 12 7 -1 743.191 492.849 2 12 -7 0 140.146 326.139 2 12 7 0 -773.12 536.15 2 12 -7 1 317.104 399.998 2 12 7 1 598.36 423.363 2 12 -7 2 10628.1 1580.77 2 12 7 2 16579.7 1971.15 2 12 -7 3 -400.789 398.077 2 12 7 3 -64.363 308.42 2 12 -7 4 300.075 383.628 2 12 7 4 647.43 478.171 2 12 -7 5 -237.988 385.795 2 12 7 5 -482.236 442.067 2 12 -7 6 5943.98 1194.12 2 12 7 6 5946.87 1192.86 2 12 -7 7 1672.75 692.742 2 12 7 7 1947.93 734.738 2 12 -7 8 17735.6 2120.82 2 12 7 8 18676.4 2142.43 2 -12 -8 9 3832.65 626.173 7 12 -8 -9 2909.35 645.091 5 -12 -8 8 7983.79 898.511 7 12 -8 -8 8177.63 1012.28 5 -12 -8 7 1080.96 360.655 7 12 -8 -7 1201.27 418.026 5 -12 -8 6 10107.8 986.56 7 12 -8 -6 10753.6 1112.59 5 12 -8 -5 900.966 360.822 5 12 -8 -4 29675.5 1768.14 5 12 -8 -3 1434.68 610.354 2 12 8 -3 2999.1 810.523 2 12 -8 -2 18563.6 2056.14 2 12 8 -2 18675.8 2061.22 2 12 -8 -1 -194.117 444.009 2 12 8 -1 -419.776 412.398 2 12 -8 0 5376.76 1137.95 2 12 8 0 6005.38 1176.84 2 12 -8 1 -1485.87 654.215 2 12 8 1 -142.338 344.66 2 12 -8 2 12551 1691.73 2 12 8 2 13230.3 1755.56 2 12 -8 3 -61.1606 219.258 2 12 8 3 156.992 372.567 2 12 -8 4 16117.6 1925.37 2 12 8 4 16418.9 1957.55 2 12 -8 5 2619.57 835.362 2 12 8 5 3353.07 904.98 2 12 -8 6 714.849 480.943 2 12 8 6 1622.38 710.689 2 12 8 7 279.629 426.399 2 12 9 -2 1432.3 595.782 2 12 9 -1 -1083.16 539.884 2 12 9 0 7838.33 1321.28 2 -13 0 14 3189.18 1043.71 3 -13 0 13 4.11668 268.955 3 -13 0 12 3601.08 1091.96 3 -13 0 11 788.911 478.846 3 -13 0 10 16678.7 2277.61 3 -13 0 9 684.801 508.413 3 -13 0 8 104999 5709.11 3 13 0 -7 226.75 454.912 2 -13 0 7 1164.65 665.759 3 13 0 -6 15236 1982.78 2 -13 0 6 14416.7 2180.3 3 13 0 -5 -399.019 494.159 2 -13 0 5 107.465 323.765 3 13 0 -4 5979.56 1266 2 -13 0 4 7848.6 1626.47 3 13 0 -3 -698.374 552.338 2 -13 0 3 209.69 427.566 3 13 0 -2 30723.9 2785.23 2 -13 0 2 26396.3 2959.6 3 13 0 -1 -902.354 588.551 2 -13 0 1 37.1594 391.432 3 13 0 0 8250.39 1476.45 2 -13 0 0 8437.48 1681.68 3 13 0 1 -297.923 440.331 2 -13 0 -1 -785.052 656.852 3 13 0 2 604.734 497.785 2 -13 0 -2 1635.96 793.427 3 13 0 3 -320.177 410.216 2 -13 0 -3 364.172 484.519 3 13 0 4 16120.9 2037.56 2 -13 0 -4 14554.6 2268.91 3 13 0 5 -768.043 517.129 2 -13 0 -5 525.493 629.212 3 13 0 6 29273.2 2795.88 2 -13 0 -6 31378.7 3299.28 3 -13 1 15 918.884 547.076 3 -13 1 14 2990.91 1036.59 3 -13 -1 13 4445.42 1133.74 3 -13 1 13 4069.03 1104.07 3 -13 -1 12 2223.9 776.393 3 -13 1 12 822.374 542.599 3 -13 -1 11 15638.4 2117.78 3 -13 1 11 13070.6 2057.6 3 -13 -1 10 -4.02658 183.129 3 -13 1 10 894.785 578.734 3 -13 1 9 18938.7 2505.59 3 -13 -1 9 18460 2328.8 3 -13 -1 8 1885.93 780.191 3 -13 1 8 1130.59 683.224 3 13 -1 -7 3537.23 964.991 2 13 1 -7 4610.27 1106.63 2 -13 -1 7 3053.39 974.171 3 -13 1 7 3207.47 1028.69 3 13 -1 -6 361.083 413.269 2 13 1 -6 830.184 532.187 2 -13 -1 6 651.048 507.988 3 -13 1 6 542.236 506.968 3 13 -1 -5 71.2452 370.441 2 13 1 -5 -959.157 586.794 2 -13 -1 5 119.832 400.289 3 -13 1 5 247.17 373.049 3 13 -1 -4 3336.67 900.559 2 13 1 -4 3015.94 944.957 2 -13 -1 4 5121.44 1311.43 3 -13 1 4 4160.09 1181.05 3 13 -1 -3 -230.461 421.659 2 13 1 -3 -720.125 530.493 2 -13 -1 3 431.538 451.276 3 -13 1 3 -838.47 639.85 3 13 -1 -2 28253.5 2670.51 2 13 1 -2 31833.3 2839.18 2 -13 1 2 33185.3 3377.41 3 -13 -1 2 29439.8 3046.32 3 13 -1 -1 -325.681 375.8 2 13 1 -1 -169.924 329.95 2 -13 -1 1 -333.201 448.297 3 -13 1 1 -727.512 579.126 3 13 -1 0 3305.96 927.439 2 13 1 0 2551.6 851.137 2 -13 1 0 4993.27 1357.63 3 -13 -1 0 2929.46 986.142 3 13 -1 1 4198.23 1040.05 2 13 1 1 5846.48 1279.65 2 -13 1 -1 4123.96 1288.83 3 -13 -1 -1 4799.3 1276.81 3 13 -1 2 970.335 549.908 2 13 1 2 1297.76 648.613 2 -13 1 -2 1713.81 849.462 3 -13 -1 -2 1928.83 863.783 3 13 -1 3 15382.1 2003.77 2 13 1 3 17276.8 2138.1 2 -13 1 -3 17022.9 2493.55 3 -13 -1 -3 15500.1 2296.44 3 13 -1 4 23634.9 2506.27 2 13 1 4 23601.4 2495.73 2 -13 1 -4 23819.1 2932.9 3 -13 -1 -4 25109.4 2891.03 3 13 -1 5 30861.4 2852.01 2 13 1 5 25253.7 2581.54 2 -13 1 -5 31111.8 3354.47 3 -13 -1 -5 24557.9 2888.78 3 13 -1 6 4937.36 1170.08 2 13 1 6 6755.11 1369.28 2 -13 1 -6 6139.42 1517.5 3 -13 2 15 -1231.99 710.549 3 -13 2 14 -755.714 593.612 3 -13 2 13 630.678 472.148 3 -13 -2 13 114.559 308.739 3 -13 2 12 1096.02 610.859 3 -13 -2 12 428.968 415.254 3 -13 2 11 1444.1 718.042 3 -13 -2 11 768.695 529.939 3 -13 2 10 9180.92 1799.03 3 -13 -2 10 9580.33 1621.28 3 -13 2 9 1759.4 786.133 3 -13 -2 9 715.783 526.252 3 -13 2 8 318.403 444.891 3 -13 -2 8 -1051.44 582.515 3 13 2 -7 5864.74 1288.54 2 -13 2 7 5912.99 1479.74 3 -13 -2 7 6276.71 1368.59 3 13 -2 -6 2707.22 903.546 2 13 2 -6 1929.3 779.191 2 -13 2 6 2624.57 975.001 3 -13 -2 6 1375.16 657.436 3 13 -2 -5 4172.69 1072.57 2 13 2 -5 5105.35 1162.35 2 -13 2 5 4337.43 1265.26 3 -13 -2 5 4722.19 1178.52 3 13 -2 -4 1088.69 594.645 2 13 2 -4 1102.45 543.169 2 -13 2 4 1563.34 797.643 3 -13 -2 4 1284.56 707.203 3 13 -2 -3 3090.16 935.992 2 13 2 -3 3979.21 1040.72 2 -13 2 3 6001.78 1513.09 3 -13 -2 3 4826.47 1241.95 3 13 -2 -2 -1245.38 656.809 2 13 2 -2 -283.054 386.119 2 -13 -2 2 21.164 439.335 3 13 -2 -1 24825.9 2524.84 2 13 2 -1 23633.1 2448.14 2 -13 2 1 26802.1 3092.43 3 -13 -2 1 23739.1 2711.99 3 13 2 0 -45.9805 263.678 2 -13 2 0 -248.288 393.558 3 -13 -2 0 446.748 471.613 3 13 -2 1 11506.1 1709.49 2 13 2 1 10383.6 1602.87 2 -13 -2 -1 8470.91 1614.93 3 -13 2 -1 12475.7 2154.01 3 13 -2 2 11409 1736.7 2 13 2 2 11043.3 1684.73 2 -13 -2 -2 9989.24 1837.07 3 13 -2 3 3486.46 952.878 2 13 2 3 2253.91 766.161 2 -13 -2 -3 3168.96 1061.37 3 -13 2 -3 1123.84 769.154 3 13 -2 4 -91.1492 589.562 2 13 2 4 130.732 397.957 2 -13 -2 -4 -259.309 490.205 3 -13 2 -4 1167.61 767.776 3 13 -2 5 25065.1 2600.52 2 13 2 5 25036 2578.15 2 -13 -2 -5 27781.2 3022.17 3 -13 2 -5 23783.6 3001.23 3 13 -2 6 1247.69 580.78 2 13 2 6 569.659 515.669 2 -13 3 14 11998.2 2098.57 3 -13 3 13 -130.536 353.221 3 -13 3 12 -1377.28 738.07 3 -13 -3 12 -34.8062 319.151 3 -13 3 11 1485.12 788.057 3 -13 -3 11 1228.55 633.971 3 -13 -3 10 6461.1 1301.61 3 -13 3 10 7982.77 1700.31 3 -13 -3 9 2669.33 875.757 3 -13 3 9 5236.67 1351.05 3 -13 -3 8 3936.34 1058.21 3 -13 3 8 3349.46 1201.62 3 -13 -3 7 4941.63 1154.27 3 -13 3 7 5680.24 1475.15 3 13 -3 -6 -1143.38 640.549 2 13 3 -6 -522.693 486.82 2 -13 -3 6 346.778 460.559 3 13 -3 -5 -60.6861 432.668 2 13 3 -5 178.249 391.001 2 -13 -3 5 233.437 411.067 3 -13 3 5 1008.19 676.834 3 13 -3 -4 21505.7 2351.72 2 13 3 -4 20774.6 2299.41 2 -13 -3 4 18676.8 2349.71 3 -13 3 4 25324.3 3071.71 3 13 3 -3 13222.3 1843.08 2 13 -3 -3 15808.7 2013.8 2 -13 -3 3 17297.9 2241.12 3 -13 3 3 15883.7 2443.09 3 13 -3 -2 -88.8135 428.408 2 13 3 -2 3.54481 571.842 2 -13 -3 2 555.978 506.439 3 -13 3 2 535.87 608.51 3 13 -3 -1 5078.87 1163.61 2 13 3 -1 4434.71 1110.09 2 -13 -3 1 3523.92 1065.5 3 -13 3 1 5444.04 1437.92 3 13 -3 0 -53.3549 518.76 2 13 3 0 7.09133 410.879 2 -13 -3 0 160.629 287.294 3 -13 3 0 -53.2193 636.557 3 13 -3 1 1402.13 605.188 2 13 3 1 1930.39 749.234 2 -13 3 -1 4123.97 1346.58 3 -13 -3 -1 1947.94 787.941 3 13 -3 2 9719.5 1625.32 2 13 3 2 10177 1644.29 2 -13 3 -2 9966.48 2018.68 3 -13 -3 -2 6086.75 1371.42 3 13 -3 3 15111.7 1965.14 2 13 3 3 14806.7 1981.45 2 -13 3 -3 17909 2600.06 3 -13 -3 -3 13699.4 2075.57 3 13 -3 4 -318.372 384.144 2 13 3 4 589.218 449.123 2 -13 -3 -4 -850.723 637.761 3 13 -3 5 3172.53 975.785 2 13 3 5 4665.15 1133.79 2 -13 4 13 14524.8 2361.66 3 -13 4 12 8923.99 1860.55 3 -13 4 11 3546.29 1193.03 3 -13 -4 11 4005.16 1023.97 3 -13 4 10 20473.5 2831.83 3 -13 -4 10 17463.3 2097.39 3 -13 -4 9 788.905 520.268 3 -13 4 9 71.0177 369.806 3 -13 -4 8 883.458 499.073 3 -13 4 8 1167.31 490.608 3 -13 -4 7 2246.27 813.845 3 -13 4 7 1517.51 857.376 3 13 -4 -6 -921.453 603.24 2 13 4 -6 -375.584 415.344 2 -13 -4 6 -921.253 539.24 3 -13 4 6 -220.322 345.028 3 13 -4 -5 -885.37 581.568 2 13 4 -5 -99.7061 373.3 2 -13 -4 5 367.733 434.204 3 13 -4 -4 2338.67 807.463 2 13 4 -4 1913.42 771.032 2 -13 -4 4 2676.46 911.646 3 -13 4 4 1073.57 736.567 3 13 -4 -3 1325.86 646.233 2 13 4 -3 -288.012 478.988 2 -13 -4 3 1445.67 707.582 3 -13 4 3 266.392 540.562 3 13 -4 -2 -460.082 465.273 2 13 4 -2 -696.141 571.589 2 -13 -4 2 834.977 532.252 3 -13 4 2 390.387 821.192 3 13 -4 -1 12028.6 1772.07 2 13 4 -1 13386.1 1871.2 2 -13 -4 1 9533.93 1683.78 3 -13 4 1 11429.3 2125.42 3 13 -4 0 572.076 432.986 2 13 4 0 -138.758 417.162 2 -13 -4 0 1586.56 854.077 3 -13 4 0 1152.91 758.093 3 13 -4 1 7100.16 1341.54 2 13 4 1 6518.25 1304.22 2 -13 -4 -1 8949.52 1671.16 3 13 -4 2 1673.71 729.756 2 13 4 2 4498.73 1135.55 2 -13 -4 -2 5006.88 1274.42 3 13 -4 3 2353.81 836.885 2 13 4 3 1861.22 648.497 2 13 -4 4 641.782 556.172 2 13 4 4 1164.3 579.779 2 13 -5 -12 9103.23 1051.48 5 13 -5 -11 23062.9 1631.42 5 13 -5 -10 2397.2 548.423 5 -13 -5 10 4561.71 1128.06 3 13 -5 -9 4192.68 672.332 5 -13 -5 9 5591.68 1215.93 3 13 -5 -8 -416.842 226.89 5 -13 -5 8 386.048 395.3 3 13 -5 -7 -86.9072 142.209 5 -13 -5 7 1134.52 564.373 3 13 -5 -6 -207.043 181.319 5 -13 -5 6 1231.16 587.231 3 13 -5 -5 -1231.26 649.482 2 13 5 -5 -1245.56 638.13 2 13 -5 -4 10897.9 1683.26 2 13 5 -4 12049.8 1759.55 2 -13 -5 4 11728.7 1850.01 3 13 -5 -3 1614.08 667.704 2 13 5 -3 1529.75 498.356 2 -13 -5 3 2289.76 832.898 3 13 -5 -2 25780.1 2587.24 2 13 5 -2 22968.1 2436.45 2 -13 -5 2 22594.2 2579.82 3 13 -5 -1 153.794 406.44 2 13 5 -1 -742.52 553.607 2 -13 -5 1 637.126 595.203 3 13 -5 0 35505.7 3018.86 2 13 5 0 34842.5 2988.88 2 -13 -5 0 39233.6 3430.91 3 13 -5 1 2156.67 783.196 2 13 5 1 2774.12 803.148 2 13 -5 2 -1091.27 592.619 2 13 5 2 848.769 346.921 2 13 -5 3 13257.3 1901.23 2 13 5 3 13863 1900.64 2 13 -6 -11 16483.9 1420.39 5 13 -6 -10 3581.11 670.606 5 -13 -6 9 23072.8 2454.32 3 13 -6 -9 21456.5 1556.72 5 -13 -6 8 4670.54 1158.73 3 13 -6 -8 4176.45 690.744 5 13 -6 -7 1018.47 343.494 5 -13 -6 7 -175.185 314.315 3 -13 -6 6 461.784 436.307 3 -13 -6 5 27337.4 2771.22 3 13 6 -5 29176.3 2738.17 2 -13 -6 4 2024.8 805.444 3 13 6 -4 1663.31 700.473 2 13 -6 -4 1037.17 495.44 2 -13 -6 3 55598.4 4020.47 3 13 -6 -3 49680.5 3572.84 2 13 6 -3 51156.8 3608.79 2 -13 -6 2 1958.48 895.29 3 13 -6 -2 227.534 370.887 2 13 -6 -1 14390.3 1932.47 2 13 6 -1 16844.1 2097.16 2 13 -6 0 5949.47 1269.82 2 13 6 0 5632.63 1217.99 2 13 -6 1 -481.146 482.449 2 13 6 1 -736.448 552.051 2 13 -6 2 12602.3 1816.03 2 13 6 2 11636.1 1728.58 2 13 7 -4 10501.9 1656.38 2 13 7 -3 214.322 460.915 2 13 -7 -2 12681.6 1816.64 2 13 7 -2 14026.9 1898.19 2 13 -7 -1 1453.92 648.698 2 13 7 -1 922.882 606.254 2 13 7 0 -199.054 459.084 2 -14 0 11 313.249 398.086 3 -14 0 10 16271.8 2346.27 3 -14 0 9 252.966 444.959 3 -14 0 8 23145.1 2811.32 3 -14 0 7 648.337 551.519 3 -14 0 6 39144.3 3716.51 3 -14 0 5 472.797 493.403 3 -14 0 4 19552 2627.68 3 -14 1 12 14585.1 2253.09 3 -14 -1 11 1197.4 606.745 3 -14 1 11 1116.67 404.138 3 -14 -1 10 2889.23 991.218 3 -14 1 10 3808.51 1187.22 3 -14 -1 9 848.656 591.451 3 -14 1 9 -623.449 589.962 3 -14 -1 8 5098.48 1277.77 3 -14 1 8 4056.68 1253.55 3 -14 -1 7 1303.72 692.941 3 -14 1 7 719.031 643.148 3 -14 -1 6 12598.4 2071.86 3 -14 -1 5 14264.8 2201.35 3 -14 -1 4 613.512 524.717 3 -14 -2 10 173.278 302.727 3 -14 -2 9 16643.5 2233 3 -14 -2 8 2168.36 814.068 3 -14 -2 7 23707.8 2727.49 3 -14 -2 6 5499.5 1349.41 3 -14 -2 5 5293.09 1401.69 3 -14 -2 4 1737.81 798.666 3 -14 -3 9 1816.85 721.226 3 -14 -3 8 7267.05 1454.59 3 -14 -3 7 9533.97 1758.75 3 -14 -3 6 18235.4 2375.64 3 -14 -3 5 5830.96 1348.94 3 -14 -4 8 1663.29 786.856 3 -14 -4 7 4420.98 1176.79 3 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 15 2 3 0.0701 2 -5 -29 0.0623 -2 5 29 0.0482 -15 -3 -4 0.0974 -9 -5 -21 0.0817 -1 -4 30 0.0407 0 4 -30 0.0494 14 -4 10 0.0618 -7 -3 28 0.0671 -3 -14 13 0.0294 -1 15 -10 0.0391 12 -10 -4 0.0673 13 4 -15 0.0870 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Mo1 O2 100.93(9) . . ? O1 Mo1 O4 102.39(9) . 3_876 ? O1 Mo1 O5 105.26(10) . . ? O1 Mo1 O10 161.17(9) . 3_876 ? O1 Mo1 O13 92.94(9) . . ? O2 Mo1 O4 150.07(8) . 3_876 ? O2 Mo1 O10 70.94(7) . 3_876 ? O2 Mo1 O13 82.25(8) . . ? O4 Mo1 O10 81.08(7) 3_876 3_876 ? O4 Mo1 O13 78.09(8) 3_876 . ? O5 Mo1 O2 97.40(9) . . ? O5 Mo1 O4 94.30(9) . 3_876 ? O5 Mo1 O10 92.81(8) . 3_876 ? O5 Mo1 O13 161.46(9) . . ? O13 Mo1 O10 69.46(7) . 3_876 ? O2 Mo2 O3 153.21(8) . . ? O2 Mo2 O10 74.23(8) . 3_876 ? O2 Mo2 O12 80.85(8) . . ? O3 Mo2 O10 83.22(8) . 3_876 ? O3 Mo2 O12 78.77(8) . . ? O6 Mo2 O2 97.78(9) . . ? O6 Mo2 O3 101.02(9) . . ? O6 Mo2 O7 104.08(10) . . ? O6 Mo2 O10 165.86(9) . 3_876 ? O6 Mo2 O12 94.64(9) . . ? O7 Mo2 O2 99.64(9) . . ? O7 Mo2 O3 94.13(9) . . ? O7 Mo2 O10 88.93(9) . 3_876 ? O7 Mo2 O12 160.97(9) . . ? O12 Mo2 O10 72.80(7) . 3_876 ? O3 Mo3 O4 112.56(9) . . ? O8 Mo3 O3 108.37(9) . . ? O8 Mo3 O4 112.92(9) . . ? O9 Mo3 O3 108.57(10) . . ? O9 Mo3 O4 107.39(10) . . ? O9 Mo3 O8 106.80(11) . . ? O11 Mo4 O10 105.87(9) . . ? O11 Mo4 O12 105.89(10) . . ? O11 Mo4 O13 105.39(9) . . ? O12 Mo4 O10 113.08(9) . . ? O12 Mo4 O13 110.90(9) . . ? O13 Mo4 O10 114.86(9) . . ? N2 Cu1 N1 177.72(11) . 1_455 ? N4 Cu2 N3 176.48(11) . 1_655 ? Mo2 O2 Mo1 119.95(10) . . ? Mo3 O3 Mo2 147.63(12) . . ? Mo3 O4 Mo1 129.81(11) . 3_876 ? Mo2 O10 Mo1 89.34(7) 3_876 3_876 ? Mo4 O10 Mo1 136.33(10) . 3_876 ? Mo4 O10 Mo2 130.47(10) . 3_876 ? Mo4 O12 Mo2 118.97(10) . . ? Mo4 O13 Mo1 122.37(10) . . ? C3 N1 Cu1 120.0(2) . 1_655 ? C4 N1 Cu1 122.3(2) . 1_655 ? C4 N1 C3 117.6(2) . . ? C8 N2 Cu1 121.8(2) . . ? C9 N2 Cu1 120.5(2) . . ? C9 N2 C8 117.7(3) . . ? C13 N3 Cu2 122.5(2) . 1_455 ? C14 N3 Cu2 119.7(2) . 1_455 ? C14 N3 C13 117.8(2) . . ? C18 N4 Cu2 122.0(2) . . ? C18 N4 C19 117.4(2) . . ? C19 N4 Cu2 120.5(2) . . ? C2 C1 C5 117.5(3) . . ? C2 C1 C6 121.2(3) . . ? C5 C1 C6 121.3(3) . . ? C1 C2 H2 120.0 . . ? C3 C2 C1 120.1(3) . . ? C3 C2 H2 120.0 . . ? N1 C3 C2 122.4(3) . . ? N1 C3 H3 118.8 . . ? C2 C3 H3 118.8 . . ? N1 C4 H4 118.4 . . ? N1 C4 C5 123.1(3) . . ? C5 C4 H4 118.4 . . ? C1 C5 H5 120.4 . . ? C4 C5 C1 119.2(3) . . ? C4 C5 H5 120.4 . . ? C7 C6 C1 121.9(3) . . ? C7 C6 C10 117.7(3) . . ? C10 C6 C1 120.5(3) . . ? C6 C7 H7 120.3 . . ? C8 C7 C6 119.3(3) . . ? C8 C7 H7 120.3 . . ? N2 C8 C7 123.1(3) . . ? N2 C8 H8 118.5 . . ? C7 C8 H8 118.5 . . ? N2 C9 H9 118.7 . . ? N2 C9 C10 122.7(3) . . ? C10 C9 H9 118.7 . . ? C6 C10 H10 120.2 . . ? C9 C10 C6 119.6(3) . . ? C9 C10 H10 120.2 . . ? C12 C11 C15 117.6(3) . . ? C12 C11 C16 122.1(3) . . ? C15 C11 C16 120.3(3) . . ? C11 C12 H12 120.3 . . ? C13 C12 C11 119.5(3) . . ? C13 C12 H12 120.3 . . ? N3 C13 C12 122.8(3) . . ? N3 C13 H13 118.6 . . ? C12 C13 H13 118.6 . . ? N3 C14 H14 118.9 . . ? N3 C14 C15 122.3(3) . . ? C15 C14 H14 118.9 . . ? C11 C15 H15 120.0 . . ? C14 C15 C11 120.0(3) . . ? C14 C15 H15 120.0 . . ? C17 C16 C11 120.3(3) . . ? C20 C16 C11 121.7(3) . . ? C20 C16 C17 117.9(3) . . ? C16 C17 H17 120.1 . . ? C18 C17 C16 119.8(3) . . ? C18 C17 H17 120.1 . . ? N4 C18 C17 122.7(3) . . ? N4 C18 H18 118.7 . . ? C17 C18 H18 118.7 . . ? N4 C19 H19 118.5 . . ? N4 C19 C20 123.1(3) . . ? C20 C19 H19 118.5 . . ? C16 C20 H20 120.4 . . ? C19 C20 C16 119.1(3) . . ? C19 C20 H20 120.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Mo1 O1 1.697(2) . ? Mo1 O2 1.929(2) . ? Mo1 O4 1.971(2) 3_876 ? Mo1 O5 1.698(2) . ? Mo1 O10 2.4256(19) 3_876 ? Mo1 O13 2.266(2) . ? Mo2 O2 1.9096(19) . ? Mo2 O3 1.963(2) . ? Mo2 O6 1.711(2) . ? Mo2 O7 1.714(2) . ? Mo2 O10 2.300(2) 3_876 ? Mo2 O12 2.269(2) . ? Mo3 O3 1.841(2) . ? Mo3 O4 1.841(2) . ? Mo3 O8 1.703(2) . ? Mo3 O9 1.701(2) . ? Mo4 O10 1.842(2) . ? Mo4 O11 1.712(2) . ? Mo4 O12 1.774(2) . ? Mo4 O13 1.7740(19) . ? Cu1 N1 1.894(2) 1_455 ? Cu1 N2 1.894(2) . ? Cu2 N3 1.900(2) 1_655 ? Cu2 N4 1.894(2) . ? N1 C3 1.351(4) . ? N1 C4 1.344(4) . ? N2 C8 1.350(4) . ? N2 C9 1.347(4) . ? N3 C13 1.349(4) . ? N3 C14 1.346(4) . ? N4 C18 1.351(4) . ? N4 C19 1.354(4) . ? C1 C2 1.392(4) . ? C1 C5 1.394(4) . ? C1 C6 1.482(4) . ? C2 H2 0.9500 . ? C2 C3 1.374(4) . ? C3 H3 0.9500 . ? C4 H4 0.9500 . ? C4 C5 1.380(4) . ? C5 H5 0.9500 . ? C6 C7 1.394(4) . ? C6 C10 1.398(4) . ? C7 H7 0.9500 . ? C7 C8 1.379(4) . ? C8 H8 0.9500 . ? C9 H9 0.9500 . ? C9 C10 1.380(4) . ? C10 H10 0.9500 . ? C11 C12 1.390(4) . ? C11 C15 1.391(4) . ? C11 C16 1.482(4) . ? C12 H12 0.9500 . ? C12 C13 1.377(4) . ? C13 H13 0.9500 . ? C14 H14 0.9500 . ? C14 C15 1.378(4) . ? C15 H15 0.9500 . ? C16 C17 1.397(4) . ? C16 C20 1.391(4) . ? C17 H17 0.9500 . ? C17 C18 1.376(4) . ? C18 H18 0.9500 . ? C19 H19 0.9500 . ? C19 C20 1.383(4) . ? C20 H20 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 N1 C3 C2 -177.9(2) 1_655 . . . ? Cu1 N1 C4 C5 178.1(2) 1_655 . . . ? Cu1 N2 C8 C7 178.5(2) . . . . ? Cu1 N2 C9 C10 -178.3(2) . . . . ? Cu2 N3 C13 C12 179.8(2) 1_455 . . . ? Cu2 N3 C14 C15 -178.8(2) 1_455 . . . ? Cu2 N4 C18 C17 -176.5(2) . . . . ? Cu2 N4 C19 C20 176.1(2) . . . . ? O3 Mo3 O4 Mo1 80.65(15) . . . 3_876 ? O4 Mo3 O3 Mo2 56.5(2) . . . . ? O8 Mo3 O3 Mo2 -177.9(2) . . . . ? O8 Mo3 O4 Mo1 -42.45(16) . . . 3_876 ? O9 Mo3 O3 Mo2 -62.2(2) . . . . ? O9 Mo3 O4 Mo1 -159.92(13) . . . 3_876 ? O10 Mo4 O12 Mo2 81.39(12) . . . . ? O10 Mo4 O13 Mo1 -85.34(13) . . . . ? O11 Mo4 O10 Mo1 -75.60(16) . . . 3_876 ? O11 Mo4 O10 Mo2 75.10(14) . . . 3_876 ? O11 Mo4 O12 Mo2 -163.12(10) . . . . ? O11 Mo4 O13 Mo1 158.55(11) . . . . ? O12 Mo4 O10 Mo1 39.90(17) . . . 3_876 ? O12 Mo4 O10 Mo2 -169.40(11) . . . 3_876 ? O12 Mo4 O13 Mo1 44.41(14) . . . . ? O13 Mo4 O10 Mo1 168.57(13) . . . 3_876 ? O13 Mo4 O10 Mo2 -40.73(16) . . . 3_876 ? O13 Mo4 O12 Mo2 -49.29(13) . . . . ? N1 C4 C5 C1 0.0(5) . . . . ? N2 C9 C10 C6 -0.4(5) . . . . ? N3 C14 C15 C11 -1.1(5) . . . . ? N4 C19 C20 C16 1.0(5) . . . . ? C1 C2 C3 N1 -0.5(5) . . . . ? C1 C6 C7 C8 179.2(3) . . . . ? C1 C6 C10 C9 -179.0(3) . . . . ? C2 C1 C5 C4 -0.4(4) . . . . ? C2 C1 C6 C7 -146.2(3) . . . . ? C2 C1 C6 C10 34.1(4) . . . . ? C3 N1 C4 C5 0.1(4) . . . . ? C4 N1 C3 C2 0.1(4) . . . . ? C5 C1 C2 C3 0.6(4) . . . . ? C5 C1 C6 C7 35.2(4) . . . . ? C5 C1 C6 C10 -144.6(3) . . . . ? C6 C1 C2 C3 -178.1(3) . . . . ? C6 C1 C5 C4 178.3(3) . . . . ? C6 C7 C8 N2 0.0(5) . . . . ? C7 C6 C10 C9 1.2(4) . . . . ? C8 N2 C9 C10 -0.6(4) . . . . ? C9 N2 C8 C7 0.8(5) . . . . ? C10 C6 C7 C8 -1.0(4) . . . . ? C11 C12 C13 N3 -0.8(4) . . . . ? C11 C16 C17 C18 178.8(3) . . . . ? C11 C16 C20 C19 -179.2(3) . . . . ? C12 C11 C15 C14 0.6(4) . . . . ? C12 C11 C16 C17 -143.3(3) . . . . ? C12 C11 C16 C20 35.4(4) . . . . ? C13 N3 C14 C15 0.6(4) . . . . ? C14 N3 C13 C12 0.3(4) . . . . ? C15 C11 C12 C13 0.3(4) . . . . ? C15 C11 C16 C17 35.9(4) . . . . ? C15 C11 C16 C20 -145.4(3) . . . . ? C16 C11 C12 C13 179.5(3) . . . . ? C16 C11 C15 C14 -178.6(3) . . . . ? C16 C17 C18 N4 -0.1(5) . . . . ? C17 C16 C20 C19 -0.4(4) . . . . ? C18 N4 C19 C20 -1.1(5) . . . . ? C19 N4 C18 C17 0.7(5) . . . . ? C20 C16 C17 C18 0.0(4) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 14.9316 2.4018 2.8211 0.1277 0.5221 0.8433 1.6564 -4.8935 -29.3944 -0.2073 -0.8660 0.4551 -1.9174 4.8593 29.3894 0.2054 0.8582 -0.4704 -14.7566 -2.6356 -4.2963 -0.1375 -0.5629 -0.8150 -9.2876 -4.8805 -21.2524 -0.2248 -0.9311 -0.2872 -1.2358 -3.9207 29.9657 -0.3480 0.8389 -0.4185 0.0637 4.0904 -29.8111 0.3591 -0.8663 0.3471 13.5662 -3.6470 10.4395 -0.2767 0.6735 0.6854 -7.3150 -2.6169 27.6901 -0.2530 0.6070 -0.7533 -3.3110 -13.9697 13.4380 -0.9197 0.2206 -0.3248 -0.5889 14.8947 -10.3897 0.9707 -0.2335 0.0566 11.8394 -9.9881 -3.9742 -0.6234 0.1520 0.7670 13.3655 3.5212 -15.3672 0.2619 -0.0606 0.9632