#------------------------------------------------------------------------------ #$Date: 2024-12-03 04:59:07 +0200 (Tue, 03 Dec 2024) $ #$Revision: 296196 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/27/2312714.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312714 _cell_angle_alpha 92.859 _cell_angle_beta 94.838 _cell_angle_gamma 101.799 _cell_length_a 9.0744 _cell_length_b 17.4077 _cell_length_c 25.1209 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8204 _cod_data_source_file aw5097hmbvsup7.hkl _cod_data_source_block hmbv _shelx_title ' hmbv_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 465.42 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5462.96 9130.54 221.13 o 2 0 0 16045.28 25460.49 794.38 o 3 0 0 5148.01 9097.56 329.32 o 4 0 0 592.58 491.63 44.47 o 5 0 0 2392.78 2166.33 112.91 o 6 0 0 71.81 89.53 8.24 o 7 0 0 661.64 444.96 16.30 o 8 0 0 826.37 646.87 22.98 o 9 0 0 115.12 112.01 11.12 o 10 0 0 83.30 130.50 15.05 o -10 1 0 62.65 99.16 14.24 o -9 1 0 0.23 20.27 10.98 o -8 1 0 34.78 104.52 9.14 o -7 1 0 776.34 769.89 20.45 o -6 1 0 98.21 106.62 9.32 o -5 1 0 27.16 21.44 27.04 o -4 1 0 76.63 73.96 24.91 o -3 1 0 798.78 497.93 38.60 o -2 1 0 1651.20 1206.76 54.30 o -1 1 0 698.94 443.12 35.69 o 0 1 0 12.93 3.85 5.42 o 1 1 0 2450.58 1683.00 55.76 o 2 1 0 5340.27 6388.28 180.99 o 3 1 0 732.66 1074.05 70.19 o 4 1 0 2909.99 3881.23 163.99 o 5 1 0 24640.61 32410.71 1137.39 o 6 1 0 6018.16 7470.58 119.22 o 7 1 0 5733.50 7751.26 115.05 o 8 1 0 5262.67 6189.89 93.13 o 9 1 0 4908.08 4725.29 88.16 o 10 1 0 2726.27 2389.50 75.85 o -10 2 0 1744.36 1930.37 65.40 o -9 2 0 6070.06 7404.24 141.87 o -8 2 0 13597.80 17465.95 257.15 o -7 2 0 11815.92 15452.88 188.58 o -6 2 0 109.71 105.33 8.62 o -5 2 0 1073.93 1702.16 95.74 o -4 2 0 3832.18 3807.70 158.53 o -3 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45.33 o 8 8 0 22.70 10.86 11.16 o 9 8 0 4.72 26.49 9.54 o -10 9 0 38.12 31.35 12.86 o -9 9 0 36.38 55.51 13.32 o -8 9 0 1856.96 1752.51 42.07 o -7 9 0 1455.03 1317.40 36.72 o -6 9 0 3253.92 3588.56 91.07 o -5 9 0 1294.15 2001.52 67.96 o -4 9 0 9562.44 12176.12 459.96 o -3 9 0 625.50 1338.94 107.21 o -2 9 0 4478.61 8209.37 693.95 o -1 9 0 11371.35 15723.40 2758.30 o 0 9 0 262.47 349.24 68.79 o 1 9 0 8061.50 12333.12 517.79 o 2 9 0 2598.91 3180.71 129.79 o 3 9 0 4000.64 6617.15 220.20 o 4 9 0 490.38 239.26 20.19 o 5 9 0 2440.79 2075.52 57.20 o 6 9 0 2303.04 1890.80 83.05 o 7 9 0 46.94 33.34 19.19 o 8 9 0 1003.41 985.22 47.20 o -10 10 0 22.45 33.52 12.02 o -9 10 0 41.31 80.34 13.71 o -8 10 0 489.48 1003.36 32.10 o -7 10 0 20.94 10.99 12.76 o -6 10 0 14.92 95.92 13.17 o -5 10 0 2028.86 1332.43 80.38 o -4 10 0 1572.61 784.21 80.72 o -3 10 0 34.04 19.83 32.54 o -2 10 0 320.38 151.46 42.14 o -1 10 0 381.76 225.27 74.68 o 0 10 0 2501.95 3349.21 163.34 o 1 10 0 2382.27 2602.36 306.31 o 2 10 0 364.96 399.48 55.05 o 3 10 0 225.32 272.51 23.84 o 4 10 0 2701.57 3056.89 76.32 o 5 10 0 806.36 645.32 23.94 o 6 10 0 8773.70 9883.07 186.39 o 7 10 0 90.47 46.79 30.99 o 8 10 0 1043.18 936.95 40.96 o -10 11 0 726.57 939.68 34.94 o -9 11 0 2710.62 2574.99 58.95 o -8 11 0 541.70 639.72 25.82 o -7 11 0 402.48 429.97 20.84 o -6 11 0 2430.50 2263.49 62.05 o -5 11 0 227.92 223.97 18.07 o -4 11 0 1540.74 1827.72 111.31 o -3 11 0 1428.60 1561.12 129.22 o -2 11 0 46.66 37.14 27.81 o -1 11 0 254.27 248.70 45.23 o 0 11 0 1842.19 1493.32 99.73 o 1 11 0 3448.43 1818.54 114.48 o 2 11 0 330.43 209.21 35.42 o 3 11 0 57.82 29.98 16.20 o 4 11 0 17.32 8.07 14.64 o 5 11 0 74.68 132.92 18.06 o 6 11 0 37.74 95.21 15.69 o 7 11 0 1.52 24.02 18.54 o 8 11 0 131.48 106.48 10.35 o -10 12 0 362.50 261.34 20.66 o -9 12 0 2.53 18.80 12.21 o -8 12 0 2201.16 1969.03 77.68 o -7 12 0 5444.92 5012.22 117.45 o -6 12 0 6876.60 6817.97 151.48 o -5 12 0 328.04 364.97 20.31 o -4 12 0 6698.98 7541.00 359.13 o -3 12 0 8794.93 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