#------------------------------------------------------------------------------ #$Date: 2024-12-03 04:59:07 +0200 (Tue, 03 Dec 2024) $ #$Revision: 296196 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/27/2312717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312717 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.1314 _cell_length_b 17.1314 _cell_length_c 35.1640 _exptl_crystal_F_000 4464.00 _reflns_d_resolution_high 0.7823 _cod_data_source_file aw5097dadsa_hmbc_2sup10.hkl _cod_data_source_block dadsa_hmbc_2 _shelx_title ' dadsa_hmbc_2_a.res in P-42(1)c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 763.90 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 31.98 23.39 10.12 o 0 2 0 32587.81 30362.10 837.77 o 1 2 0 3274.87 4894.48 102.90 o 2 2 0 225780.17 213225.55 4794.96 o 1 3 0 2029.49 2058.98 56.46 o 2 3 0 151383.19 152073.33 1984.81 o 3 3 0 53.26 197.02 17.45 o 0 4 0 115046.76 119908.92 3450.05 o 1 4 0 27530.31 26534.39 1401.00 o 2 4 0 583549.56 598377.81 8293.26 o 3 4 0 22700.54 22544.00 1159.89 o 4 4 0 164566.48 150035.14 2931.31 o 1 5 0 1055.19 6804.00 916.64 o 2 5 0 81193.61 87979.55 1404.78 o 3 5 0 8.70 874.10 157.17 o 4 5 0 0.51 145.35 23.12 o 5 5 0 23474.95 22567.19 448.69 o 0 6 0 21912.32 27597.43 852.87 o 1 6 0 630.72 1641.70 303.61 o 2 6 0 5879.91 5340.61 149.16 o 3 6 0 131.80 1357.58 290.28 o 4 6 0 12701.92 9815.72 395.36 o 5 6 0 1087.69 1870.79 50.65 o 6 6 0 96375.23 97686.97 1910.34 o 1 7 0 0.75 62.44 24.94 o 2 7 0 38358.16 36146.12 874.03 o 3 7 0 4092.21 2693.99 55.07 o 4 7 0 3895.32 4591.20 83.99 o 5 7 0 103.41 174.84 20.20 o 6 7 0 20948.53 23530.85 1190.80 o 7 7 0 3540.39 4557.51 152.86 o 0 8 0 7726.94 8176.90 281.97 o 1 8 0 3473.91 4335.97 274.86 o 2 8 0 256.06 811.73 76.53 o 3 8 0 804.40 2558.75 310.81 o 4 8 0 40152.20 42524.41 774.14 o 5 8 0 2865.91 2895.64 222.57 o 6 8 0 28771.47 29450.27 478.54 o 7 8 0 5.16 141.35 31.39 o 8 8 0 2195.59 2474.69 70.81 o 1 9 0 2244.22 2389.73 210.07 o 2 9 0 1361.91 1435.18 283.22 o 3 9 0 0.88 690.79 163.71 o 4 9 0 13296.88 13989.23 257.12 o 5 9 0 303.11 1543.45 377.88 o 6 9 0 27829.00 28640.33 510.10 o 7 9 0 265.27 358.81 38.66 o 8 9 0 3834.82 3114.20 65.83 o 9 9 0 460.71 447.81 19.72 o 0 10 0 2064.71 1595.52 57.90 o 1 10 0 19407.40 17499.14 356.01 o 2 10 0 12751.08 14771.63 273.07 o 3 10 0 1494.26 2849.35 353.06 o 4 10 0 15151.52 13512.16 210.38 o 5 10 0 4913.97 5394.01 192.95 o 6 10 0 16537.60 16773.71 238.63 o 7 10 0 523.68 709.79 17.39 o 8 10 0 405.09 599.64 17.55 o 9 10 0 1194.13 1290.96 102.42 o 10 10 0 55.37 65.94 18.58 o 1 11 0 2141.42 2575.41 44.36 o 2 11 0 847.87 1058.23 95.68 o 3 11 0 2927.52 2752.16 66.18 o 4 11 0 14543.03 13812.17 184.03 o 5 11 0 161.20 338.09 30.27 o 6 11 0 5268.44 5358.66 63.61 o 7 11 0 438.83 418.47 14.94 o 8 11 0 580.52 344.22 14.22 o 9 11 0 1252.57 1636.95 128.57 o 10 11 0 3852.84 3365.81 112.69 o 11 11 0 259.27 415.26 23.64 o 0 12 0 1308.40 1092.74 31.78 o 1 12 0 2.70 57.89 13.29 o 2 12 0 0.74 39.30 10.80 o 3 12 0 3376.27 2979.86 34.11 o 4 12 0 3018.50 2968.71 43.31 o 5 12 0 3.04 134.27 10.08 o 6 12 0 361.82 450.67 22.21 o 7 12 0 517.33 759.39 17.32 o 8 12 0 1064.00 884.43 54.71 o 9 12 0 314.56 553.13 35.01 o 10 12 0 1876.20 2033.07 33.26 o 11 12 0 851.94 904.55 22.43 o 12 12 0 373.41 308.25 22.38 o 1 13 0 778.20 1044.24 84.63 o 2 13 0 2466.11 2793.12 95.47 o 3 13 0 700.16 646.92 25.73 o 4 13 0 1549.13 1557.37 69.04 o 5 13 0 1586.67 1723.06 71.17 o 6 13 0 342.51 386.18 12.61 o 7 13 0 16.62 135.18 12.89 o 8 13 0 27849.15 27146.02 310.89 o 9 13 0 402.94 491.22 16.73 o 10 13 0 1029.80 938.28 28.31 o 11 13 0 25.91 49.28 13.68 o 12 13 0 1679.88 1463.77 32.05 o 13 13 0 50.04 78.18 19.76 o 0 14 0 3218.31 2695.08 66.75 o 1 14 0 5731.42 5704.02 83.26 o 2 14 0 254.91 323.09 18.32 o 3 14 0 491.42 434.37 19.44 o 4 14 0 65.92 110.96 11.41 o 5 14 0 6.06 395.47 12.79 o 6 14 0 334.55 540.03 14.81 o 7 14 0 120.67 325.53 28.84 o 8 14 0 1471.15 1413.43 22.54 o 9 14 0 361.26 344.48 25.23 o 10 14 0 1.28 177.79 17.54 o 11 14 0 1866.66 1586.20 28.05 o 12 14 0 831.95 869.37 26.41 o 13 14 0 6.56 118.46 24.66 o 14 14 0 23.24 43.89 32.88 o 1 15 0 388.14 338.33 25.17 o 2 15 0 236.98 842.90 187.18 o 3 15 0 16.26 29.93 16.02 o 4 15 0 50.15 85.67 13.05 o 5 15 0 2697.93 3020.85 79.97 o 6 15 0 2637.38 2280.06 30.31 o 7 15 0 347.00 467.56 14.94 o 8 15 0 26.63 35.26 12.91 o 9 15 0 79.20 53.16 13.26 o 10 15 0 175.52 212.50 23.14 o 11 15 0 185.54 271.63 25.04 o 12 15 0 2427.93 2354.37 87.94 o 13 15 0 147.04 156.09 15.30 o 14 15 0 17.08 168.38 28.80 o 15 15 0 117.47 146.77 13.84 o 0 16 0 3.09 36.29 29.84 o 1 16 0 812.43 863.72 67.21 o 2 16 0 7805.95 7316.46 135.27 o 3 16 0 387.81 284.56 21.98 o 4 16 0 14.41 70.43 23.18 o 5 16 0 289.13 588.19 43.16 o 6 16 0 200.11 354.33 43.26 o 7 16 0 670.52 709.71 37.65 o 8 16 0 131.26 256.14 15.85 o 9 16 0 54.67 182.48 19.65 o 10 16 0 2682.16 2792.27 53.47 o 11 16 0 208.04 286.69 38.66 o 12 16 0 844.62 807.96 23.11 o 13 16 0 1018.83 1104.54 38.89 o 14 16 0 4.96 40.06 10.31 o 1 17 0 240.23 454.01 51.27 o 2 17 0 26.31 -1.56 22.97 o 3 17 0 9.95 9.60 26.46 o 4 17 0 914.50 947.68 35.33 o 5 17 0 34.43 135.43 24.79 o 6 17 0 1079.57 1191.56 37.51 o 7 17 0 26.84 14.11 18.92 o 8 17 0 445.57 380.60 19.78 o 9 17 0 680.25 685.53 19.77 o 10 17 0 4886.45 4862.44 90.39 o 11 17 0 265.23 762.77 76.41 o 12 17 0 88.95 68.12 20.18 o 13 17 0 51.80 89.89 11.84 o 0 18 0 7353.15 14558.24 579.12 o 1 18 0 26.95 233.01 84.40 o 2 18 0 44.53 171.49 29.99 o 3 18 0 2529.97 2298.31 52.39 o 4 18 0 135.03 157.41 21.31 o 5 18 0 136.85 144.83 20.55 o 6 18 0 1766.21 1888.76 43.29 o 7 18 0 0.13 32.72 14.22 o 8 18 0 750.67 800.85 20.16 o 9 18 0 0.40 116.81 17.11 o 10 18 0 981.83 961.15 52.93 o 11 18 0 1005.41 1146.54 49.72 o 12 18 0 1094.35 1036.22 45.52 o 1 19 0 60.10 131.87 37.34 o 2 19 0 84.48 124.99 36.28 o 3 19 0 56.60 24.72 26.23 o 4 19 0 110.68 244.85 31.61 o 5 19 0 140.58 168.40 15.05 o 6 19 0 315.41 249.25 16.50 o 7 19 0 77.71 128.56 20.30 o 8 19 0 49.59 190.82 25.10 o 9 19 0 168.24 230.27 16.58 o 10 19 0 448.47 412.87 17.28 o 0 20 0 959.90 859.53 39.04 o 1 20 0 245.29 196.25 18.65 o 2 20 0 676.96 780.08 25.87 o 3 20 0 5.80 11.60 16.14 o 4 20 0 4.30 28.37 18.31 o 5 20 0 51.59 186.54 19.96 o 6 20 0 38.89 87.30 11.86 o 7 20 0 1034.46 1028.51 42.10 o 8 20 0 4.15 2016.33 1055.50 o 1 21 0 71.20 56.13 10.27 o 2 21 0 4.78 21.17 11.38 o 3 21 0 62.47 115.33 10.55 o 4 21 0 280.25 145.98 11.50 o 5 21 0 40.20 42.65 11.79 o 0 1 1 1.50 12.57 4.94 o -1 2 1 1498.01 1960.82 63.15 o 0 2 1 6952.44 5507.50 110.15 o 1 2 1 1498.82 1921.85 40.82 o -2 3 1 42658.00 44326.14 707.12 o -1 3 1 18155.35 16608.04 325.50 o 0 3 1 446.19 485.79 22.52 o 1 3 1 18159.77 16878.23 291.33 o 2 3 1 42657.38 44638.42 612.88 o -3 4 1 18927.53 18147.02 477.80 o -2 4 1 1978.99 1879.77 69.12 o -1 4 1 78084.97 74244.56 1271.25 o 0 4 1 1448.30 1474.84 32.26 o 1 4 1 78091.14 72372.30 1271.98 o 2 4 1 1971.67 1805.07 123.33 o 3 4 1 18931.84 18383.39 341.66 o -4 5 1 3172.77 3618.86 145.44 o -3 5 1 49750.71 47502.82 759.53 o -2 5 1 1789.49 1543.12 76.89 o -1 5 1 95805.87 81350.81 1590.36 o 0 5 1 8725.77 7057.88 144.22 o 1 5 1 95895.80 81642.88 1590.91 o 2 5 1 1792.39 1613.33 79.74 o 3 5 1 49647.91 47245.46 706.66 o 4 5 1 3174.35 3476.76 116.59 o -5 6 1 2444.79 2012.70 46.15 o -4 6 1 3301.76 2812.06 47.50 o -3 6 1 27395.23 24650.79 423.98 o -2 6 1 2266.21 1816.99 34.58 o -1 6 1 40207.09 42195.55 732.10 o 0 6 1 1449.53 1238.11 34.22 o 1 6 1 40200.19 40718.34 731.99 o 2 6 1 2272.31 1900.47 43.49 o 3 6 1 27365.43 24610.76 346.94 o 4 6 1 3306.10 2806.67 50.56 o 5 6 1 2441.63 1949.82 38.94 o -6 7 1 4432.09 3864.79 73.21 o -5 7 1 41961.40 41201.50 668.95 o -4 7 1 125.93 291.27 22.05 o -3 7 1 5398.31 5973.62 103.80 o -2 7 1 1358.89 1164.72 30.08 o -1 7 1 3918.87 3887.48 100.86 o 0 7 1 7124.84 6154.74 138.89 o 1 7 1 3929.07 4081.84 90.59 o 2 7 1 1357.07 1162.82 44.60 o 3 7 1 5394.83 6155.83 127.00 o 4 7 1 126.13 286.52 24.61 o 5 7 1 41962.22 41718.64 668.78 o 6 7 1 4450.65 3723.68 81.38 o -7 8 1 1399.68 1723.85 140.44 o -6 8 1 155.82 545.16 33.98 o -5 8 1 18532.21 18306.29 329.11 o -4 8 1 2521.79 2473.11 141.23 o -3 8 1 8855.39 8480.95 171.02 o -2 8 1 4922.41 3979.20 75.16 o -1 8 1 361.15 305.33 27.52 o 0 8 1 5210.31 3753.43 105.58 o 1 8 1 359.62 328.16 29.82 o 2 8 1 4928.74 3919.97 75.49 o 3 8 1 8848.09 8150.21 184.30 o 4 8 1 2510.24 2400.36 131.82 o 5 8 1 18522.15 18167.16 329.06 o 6 8 1 157.43 608.92 57.33 o 7 8 1 1399.11 1794.61 70.70 o -8 9 1 688.26 648.02 21.57 o -7 9 1 1131.67 1496.23 40.62 o -6 9 1 1945.25 2189.42 102.31 o -5 9 1 25857.66 25170.34 593.67 o -4 9 1 225.15 309.45 29.79 o -3 9 1 19082.20 20495.97 408.29 o -2 9 1 2944.97 2960.74 160.71 o -1 9 1 1584.19 1389.45 46.47 o 0 9 1 5910.42 5067.64 102.90 o 1 9 1 1575.81 1402.40 48.34 o 2 9 1 2943.40 3034.95 115.79 o 3 9 1 19069.42 20142.06 408.45 o 4 9 1 226.91 302.41 27.38 o 5 9 1 25842.51 25857.73 514.50 o 6 9 1 1944.79 2153.24 135.79 o 7 9 1 1133.40 1416.12 89.98 o 8 9 1 688.36 620.84 25.18 o -9 10 1 72.47 88.83 13.82 o -8 10 1 527.58 471.49 16.92 o -7 10 1 40.21 140.34 15.29 o -6 10 1 654.31 775.79 18.02 o -5 10 1 20742.92 20769.42 275.63 o -4 10 1 17.37 74.33 18.63 o -3 10 1 6950.60 6708.02 196.01 o -2 10 1 6744.67 7547.92 407.36 o -1 10 1 5379.89 5373.20 145.41 o 0 10 1 2252.91 1645.01 41.45 o 1 10 1 5375.77 5338.95 123.20 o 2 10 1 6748.34 7562.92 280.91 o 3 10 1 6948.62 6652.49 188.99 o 4 10 1 16.74 76.63 28.17 o 5 10 1 20722.58 20619.79 313.83 o 6 10 1 655.58 696.78 26.03 o 7 10 1 40.58 123.43 18.91 o 8 10 1 527.11 457.11 17.87 o 9 10 1 72.33 87.35 17.07 o -10 11 1 198.31 232.78 15.87 o -9 11 1 5464.78 5624.28 78.44 o -8 11 1 2949.79 2875.07 41.11 o -7 11 1 1565.25 1610.06 37.82 o -6 11 1 44.94 85.02 11.36 o -5 11 1 1342.00 1434.10 23.73 o -4 11 1 1612.16 1258.71 25.38 o -3 11 1 1247.15 1030.88 20.23 o -2 11 1 2054.54 2056.45 36.41 o -1 11 1 37.91 130.98 20.47 o 0 11 1 2578.14 2190.64 35.22 o 1 11 1 38.13 110.40 15.80 o 2 11 1 2059.50 2067.16 34.51 o 3 11 1 1238.72 997.00 20.96 o 4 11 1 1618.36 1235.51 22.92 o 5 11 1 1347.75 1482.37 26.75 o 6 11 1 44.68 85.91 13.27 o 7 11 1 1566.54 1514.92 33.85 o 8 11 1 2951.17 2862.25 43.49 o 9 11 1 5463.88 5452.65 84.71 o 10 11 1 199.52 213.93 23.35 o -11 12 1 568.22 509.54 18.47 o -10 12 1 925.21 756.60 19.88 o -9 12 1 5544.60 5487.87 68.01 o -8 12 1 416.71 447.73 16.46 o -7 12 1 485.93 579.18 18.95 o -6 12 1 2725.72 2728.90 52.67 o -5 12 1 898.50 819.79 14.06 o -4 12 1 580.09 688.39 25.98 o -3 12 1 4313.19 4763.89 55.84 o -2 12 1 2768.64 2432.83 57.24 o -1 12 1 3310.52 3075.93 51.16 o 0 12 1 370.98 625.10 17.95 o 1 12 1 3310.43 3017.44 44.55 o 2 12 1 2770.39 2529.10 61.25 o 3 12 1 4312.97 4732.22 54.40 o 4 12 1 577.53 666.66 29.40 o 5 12 1 894.77 833.77 14.30 o 6 12 1 2731.11 2705.78 46.44 o 7 12 1 487.24 608.23 16.66 o 8 12 1 415.49 437.58 18.53 o 9 12 1 5536.82 5468.94 79.31 o 10 12 1 923.95 749.45 22.58 o 11 12 1 566.06 508.10 20.71 o -12 13 1 294.81 324.48 19.13 o -11 13 1 584.66 682.87 22.00 o -10 13 1 396.08 389.29 15.82 o -9 13 1 1014.00 1000.56 20.79 o -8 13 1 1992.18 2194.26 61.72 o -7 13 1 4923.80 4945.67 60.72 o -6 13 1 80.10 134.89 12.23 o -5 13 1 1487.23 1605.94 20.55 o -4 13 1 251.47 386.23 12.63 o -3 13 1 96.98 144.49 14.74 o -2 13 1 1604.98 1493.95 31.40 o -1 13 1 1941.70 1666.29 34.70 o 0 13 1 503.83 646.69 20.43 o 1 13 1 1952.00 1666.41 28.09 o 2 13 1 1607.49 1609.64 39.00 o 3 13 1 97.40 120.54 12.25 o 4 13 1 252.91 401.71 13.84 o 5 13 1 1485.87 1615.57 22.61 o 6 13 1 80.35 119.23 11.59 o 7 13 1 4926.90 4935.79 61.01 o 8 13 1 1991.38 2471.86 136.33 o 9 13 1 1014.75 999.29 21.67 o 10 13 1 400.83 413.53 23.00 o 11 13 1 585.34 677.82 23.97 o 12 13 1 293.44 393.28 51.39 o -13 14 1 504.83 476.19 22.27 o -12 14 1 431.76 438.19 34.75 o -11 14 1 184.22 196.66 16.15 o -10 14 1 747.95 652.64 16.49 o -9 14 1 1532.72 1502.46 23.74 o -8 14 1 150.06 117.33 12.94 o -7 14 1 5878.10 5765.76 68.35 o -6 14 1 131.15 120.83 11.06 o -5 14 1 2697.92 2504.10 29.41 o -4 14 1 1943.56 1889.99 25.92 o -3 14 1 1716.50 1465.46 37.62 o -2 14 1 4250.37 3996.43 69.64 o -1 14 1 1329.32 1216.09 36.71 o 0 14 1 56.50 173.29 16.49 o 1 14 1 1330.24 1246.40 29.09 o 2 14 1 4248.90 3958.67 61.32 o 3 14 1 1715.76 1484.87 47.09 o 4 14 1 1943.66 1880.25 32.00 o 5 14 1 2694.70 2420.95 34.22 o 6 14 1 131.29 167.27 18.35 o 7 14 1 5875.03 5605.01 74.71 o 8 14 1 149.49 124.67 13.91 o 9 14 1 1529.45 1454.70 26.94 o 10 14 1 746.73 638.37 19.71 o 11 14 1 185.63 241.46 29.23 o 12 14 1 432.03 425.22 28.49 o 13 14 1 506.81 475.16 36.13 o -14 15 1 1081.96 975.05 24.74 o -13 15 1 329.30 364.30 16.28 o -12 15 1 359.94 661.71 130.04 o -11 15 1 279.57 315.42 16.93 o -10 15 1 481.25 563.20 39.15 o -9 15 1 361.45 441.95 15.18 o -8 15 1 787.33 741.62 26.20 o -7 15 1 372.91 423.43 14.50 o -6 15 1 1426.43 1565.37 25.40 o -5 15 1 3217.78 3265.82 52.69 o -4 15 1 325.10 262.74 15.11 o -3 15 1 210.81 248.15 20.86 o -2 15 1 65.56 582.69 212.31 o -1 15 1 1415.94 1314.63 38.35 o 0 15 1 329.61 351.30 25.45 o 1 15 1 1413.30 1340.43 40.36 o 2 15 1 65.53 788.89 215.94 o 3 15 1 210.07 244.47 18.03 o 4 15 1 322.57 282.85 14.45 o 5 15 1 3217.78 3235.11 57.88 o 6 15 1 1428.65 1534.47 24.61 o 7 15 1 373.80 441.40 15.52 o 8 15 1 788.07 722.27 24.90 o 9 15 1 361.08 443.81 16.31 o 10 15 1 481.98 554.06 37.11 o 11 15 1 280.67 320.90 17.27 o 12 15 1 359.28 477.16 76.85 o 13 15 1 331.69 391.94 22.36 o 14 15 1 1086.51 980.62 51.10 o -14 16 1 177.89 172.15 26.87 o -13 16 1 150.33 115.02 14.53 o -12 16 1 66.53 93.25 17.36 o -11 16 1 1590.83 1590.63 55.17 o -10 16 1 174.82 212.14 19.42 o -9 16 1 229.35 300.16 26.45 o -8 16 1 192.02 257.81 28.68 o -7 16 1 439.18 525.79 18.77 o -6 16 1 794.47 749.97 21.50 o -5 16 1 554.60 611.28 29.46 o -4 16 1 776.92 788.91 30.77 o -3 16 1 407.88 400.79 44.05 o -2 16 1 123.58 187.92 24.27 o -1 16 1 1167.77 977.19 40.12 o 0 16 1 373.24 339.99 22.53 o 1 16 1 1166.72 1400.55 161.27 o 2 16 1 124.21 165.01 24.17 o 3 16 1 409.59 414.44 30.51 o 4 16 1 776.68 764.33 35.62 o 5 16 1 554.64 578.21 25.99 o 6 16 1 791.86 751.52 23.94 o 7 16 1 437.03 511.37 21.10 o 8 16 1 192.69 253.43 29.57 o 9 16 1 227.59 324.82 52.06 o 10 16 1 174.80 274.70 36.59 o 11 16 1 1589.01 1562.83 49.68 o 12 16 1 66.89 135.20 27.10 o 13 16 1 150.43 121.18 19.96 o 14 16 1 177.81 225.07 21.50 o -13 17 1 501.79 579.77 32.88 o -12 17 1 213.37 263.60 18.51 o -11 17 1 2475.34 2366.60 55.40 o -10 17 1 39.09 125.78 17.64 o -9 17 1 594.53 514.95 19.84 o -8 17 1 353.38 345.52 19.45 o -7 17 1 230.46 257.63 19.09 o -6 17 1 662.69 655.42 26.84 o -5 17 1 196.89 147.75 22.68 o -4 17 1 202.22 202.03 25.60 o -3 17 1 157.17 144.87 23.54 o -2 17 1 621.30 642.18 57.16 o -1 17 1 944.46 1225.11 46.90 o 0 17 1 142.47 1310.88 395.61 o 1 17 1 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