#------------------------------------------------------------------------------ #$Date: 2024-12-03 05:01:54 +0200 (Tue, 03 Dec 2024) $ #$Revision: 296198 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/31/27/2312719.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312719 loop_ _publ_author_name 'Xu, Mingyu' 'Wang, Haozhe' 'Vojvodin, Cameron' 'Yarava, Jayasubba Reddy' 'Wang, Tuo' 'Xie, Weiwei' _publ_section_title ; Polymorphism of Pb5(PO4)3OHδ within the LK-99 mixture. ; _journal_coeditor_code RM5078 _journal_issue 6 _journal_name_full 'Acta crystallographica Section B, Structural science, crystal engineering and materials' _journal_paper_doi 10.1107/S2052520624010023 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'H O13 P3 Pb5' _chemical_formula_sum 'Cu0 H O13 P3 Pb5' _chemical_formula_weight 1337.87 _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_Hall '-P 2ac 2n' _space_group_name_H-M_alt 'P n m a' _atom_sites_solution_hydrogens geom _audit_creation_date 2024-02-21 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.5137(4) _cell_length_b 10.2904(4) _cell_length_c 9.3838(3) _cell_measurement_reflns_used 15385 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 41.0250 _cell_measurement_theta_min 2.6200 _cell_volume 1304.92(8) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2019/1 (Sheldrick, 2019)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_device_type 'XtalLAB Synergy, Dualflex, Hypix' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1257 _diffrn_reflns_av_unetI/netI 0.0668 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 48595 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 41.236 _diffrn_reflns_theta_min 2.643 _exptl_absorpt_coefficient_mu 64.731 _exptl_absorpt_correction_T_max 0.177 _exptl_absorpt_correction_T_min 0.057 _exptl_absorpt_correction_type analytical _exptl_crystal_density_diffrn 6.810 _exptl_crystal_description rod-like _exptl_crystal_F_000 2240 _exptl_crystal_size_max 0.076 _exptl_crystal_size_mid 0.056 _exptl_crystal_size_min 0.049 _refine_diff_density_max 3.786 _refine_diff_density_min -5.989 _refine_diff_density_rms 0.511 _refine_ls_extinction_coef 0.00025(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2019/1 (Sheldrick 2019)' _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 114 _refine_ls_number_reflns 4458 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0811 _refine_ls_R_factor_gt 0.0402 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0195P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0681 _refine_ls_wR_factor_ref 0.0758 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2940 _reflns_number_total 4458 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file rm5078.cif _cod_data_source_block I _cod_original_cell_volume 1304.93(7) _cod_database_code 2312719 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.140 _shelx_estimated_absorpt_t_min 0.079 _olex2_refinement_description ; 1. Others Fixed Sof: Pb4(0.355) Pb5(0.145) H8(0.5) 2.a Tetrahedral OH refined with riding coordinates: O8(H8) ; _shelx_res_file ; TITL HW_MX_PbCuPO_081123_corr_ver2 in Pnma HW_MX_PbCuPO_081123_corr_ver2.res created by SHELXL-2019/1 at 12:18:34 on 14-Aug-2023 CELL 0.71073 13.51374 10.29039 9.38381 90.0000 90.0000 90.0000 ZERR 4.00 0.00044 0.00036 0.00029 0.0000 0.0000 0.0000 LATT 1 SYMM 0.5-X, -Y, 0.5+Z SYMM -X, 0.5+Y, -Z SYMM 0.5+X, 0.5-Y, 0.5-Z SFAC H O P CU PB UNIT 4 52 12 0 20 ACTA L.S. 10 WGHT 0.019500 EXTI 0.000246 FVAR 0.05218 0.99758 PB1 5 0.073773 0.555770 0.296299 11.00000 0.02213 0.01654 = 0.01823 0.00298 -0.00192 -0.00122 PB2 5 0.020426 0.750000 -0.028418 10.50000 0.01586 0.02079 = 0.01357 0.00000 -0.00303 0.00000 PB3 5 0.233500 0.750000 -0.303564 10.50000 0.02997 0.02127 = 0.02286 0.00000 0.00819 0.00000 PB4 5 0.274987 0.750000 0.155579 10.35500 0.01109 0.05244 = 0.02207 0.00000 0.00323 0.00000 PB5 5 0.270286 0.750000 0.127665 10.14500 0.01108 0.09802 = 0.03967 0.00000 0.00581 0.00000 P1 3 -0.163104 0.532434 0.070739 11.00000 0.01099 0.01048 = 0.01540 -0.00003 0.00135 0.00082 P2 3 0.002989 0.750000 -0.425174 10.50000 0.01417 0.02033 = 0.01150 0.00000 0.00105 0.00000 O1 2 -0.091262 0.750000 -0.346073 10.50000 0.02930 0.06552 = 0.02573 0.00000 0.01116 0.00000 O2 2 -0.017098 0.750000 0.417861 10.50000 0.02179 0.04063 = 0.01471 0.00000 0.00191 0.00000 O3 2 0.108903 0.750000 0.175308 10.50000 0.00976 0.01821 = 0.01222 0.00000 0.00014 0.00000 O4 2 -0.175054 0.385913 0.095466 11.00000 0.03851 0.01216 = 0.02374 -0.00068 0.00702 -0.00762 O5 2 -0.168535 0.558765 -0.090242 11.00000 0.03973 0.03343 = 0.01596 0.00312 -0.00503 0.01206 O6 2 -0.061800 0.579418 0.124904 11.00000 0.01752 0.04099 = 0.03492 0.00755 -0.00833 -0.01100 O7 2 -0.245117 0.605293 0.148817 11.00000 0.03072 0.02536 = 0.04373 -0.01158 0.01954 0.00489 O8 2 0.063524 0.867674 -0.391537 11.00000 0.02800 0.03298 = 0.06067 -0.01862 -0.01218 -0.00096 AFIX 83 H8 1 0.099291 0.852435 -0.322954 10.50000 -1.50000 AFIX 0 HKLF 4 REM HW_MX_PbCuPO_081123_corr_ver2 in Pnma REM wR2 = 0.0758, GooF = S = 1.047, Restrained GooF = 1.047 for all data REM R1 = 0.0402 for 2940 Fo > 4sig(Fo) and 0.0811 for all 4458 data REM 114 parameters refined using 0 restraints END WGHT 0.0195 0.0000 REM Highest difference peak 3.786, deepest hole -5.989, 1-sigma level 0.511 Q1 1 0.2020 0.7500 -0.3368 10.50000 0.05 2.95 Q2 1 0.0638 0.5923 0.3433 11.00000 0.05 2.90 Q3 1 0.2272 0.7943 -0.3643 11.00000 0.05 2.27 Q4 1 0.0987 0.4933 0.2383 11.00000 0.05 2.24 Q5 1 -0.0101 0.7960 -0.3620 11.00000 0.05 2.19 Q6 1 0.0698 0.5932 0.2338 11.00000 0.05 2.04 Q7 1 0.2589 0.8602 0.2029 11.00000 0.05 2.04 Q8 1 0.2561 0.7922 0.1439 11.00000 0.05 1.91 Q9 1 0.0327 0.7928 -0.0730 11.00000 0.05 1.90 Q10 1 -0.1466 0.2500 0.1539 10.50000 0.05 1.87 Q11 1 0.1033 0.5571 0.2954 11.00000 0.05 1.85 Q12 1 -0.0477 0.7500 0.0016 10.50000 0.05 1.85 Q13 1 -0.0979 0.7500 -0.1833 10.50000 0.05 1.85 Q14 1 0.0749 0.5179 0.3565 11.00000 0.05 1.82 Q15 1 0.2721 0.7844 0.2113 11.00000 0.05 1.81 Q16 1 -0.1434 0.4985 -0.1235 11.00000 0.05 1.80 Q17 1 0.1222 0.6037 0.2069 11.00000 0.05 1.78 Q18 1 -0.0417 0.7500 0.3003 10.50000 0.05 1.71 Q19 1 0.0108 0.7868 -0.0804 11.00000 0.05 1.71 Q20 1 -0.0920 0.6561 0.1374 11.00000 0.05 1.70 ; _shelx_res_checksum 61433 _shelx_hkl_file ; 0 0 2 404.19 41.07 0 0 2 437.84 41.06 0 0 2 406.21 41.09 0 0 -2 457.67 41.00 0 0 3 0.50 0.84 0 0 -3 -0.19 0.63 0 0 3 -0.67 0.80 0 0 -3 0.85 0.91 0 0 -3 -0.11 0.42 0 0 3 0.11 0.41 0 0 3 0.50 0.85 0 0 3 1.59 0.60 0 0 3 -0.22 0.81 0 0 3 0.46 0.39 0 0 -4 5.26 1.00 0 0 -4 4.02 1.31 0 0 4 6.87 1.25 0 0 4 4.51 1.28 0 0 4 4.38 0.76 0 0 4 4.38 1.00 0 0 4 3.60 1.33 0 0 -4 5.43 0.77 0 0 4 4.91 0.78 0 0 5 -0.47 0.80 0 0 -5 -0.72 1.33 0 0 -5 0.57 0.86 0 0 5 -0.37 1.34 0 0 -5 0.45 0.56 0 0 5 0.50 0.58 0 0 -6 196.94 18.61 0 0 6 194.71 18.84 0 0 -6 192.20 19.16 0 0 6 213.03 19.25 0 0 6 184.62 18.46 0 0 7 0.66 1.20 0 0 7 1.04 1.63 0 0 -7 1.53 1.89 0 0 -7 -3.01 1.96 0 0 -8 321.74 29.05 0 0 8 334.75 29.10 0 0 8 287.41 27.86 0 0 -8 272.02 28.83 0 0 -9 -1.29 2.52 0 0 -9 -2.03 2.54 0 0 -10 139.77 14.71 0 0 -10 123.45 14.73 0 0 10 153.99 14.89 0 0 -11 0.74 3.10 0 0 -11 -1.41 3.04 0 0 -11 -2.54 3.43 0 0 11 0.81 2.93 0 0 -12 112.76 12.79 0 0 12 139.86 13.29 0 0 -12 99.43 12.86 0 0 -12 112.73 12.79 0 0 -13 -1.63 3.70 0 0 13 2.93 3.63 0 0 -13 2.02 4.03 0 0 -13 2.18 3.68 0 0 13 0.95 3.59 0 0 -14 19.92 4.87 0 0 14 18.39 4.76 0 0 -14 12.85 4.93 0 0 14 11.33 4.79 0 0 15 -1.07 4.53 0 0 -15 -1.10 4.82 0 0 15 -3.18 4.96 0 0 16 11.20 4.74 0 0 -16 6.48 5.27 0 0 16 7.58 5.03 0 0 17 1.08 4.59 0 0 17 2.29 4.89 0 1 1 22.93 2.32 0 -1 1 19.81 2.23 0 -1 1 21.24 2.19 0 -1 -1 22.55 2.37 0 -1 1 22.98 2.15 0 1 1 19.73 2.21 0 1 1 22.47 2.27 0 -1 2 0.09 0.44 0 1 -2 1.10 0.44 0 -1 2 0.57 0.55 0 1 2 -0.32 0.97 0 1 2 -0.20 1.28 0 1 -2 -0.53 0.50 0 -1 2 0.26 0.55 0 -1 -2 0.08 0.61 0 1 2 -0.32 0.55 0 -1 3 23.96 2.51 0 -1 3 26.65 2.63 0 1 -3 27.59 2.61 0 1 3 22.50 2.73 0 -1 3 22.59 2.54 0 1 3 20.92 2.77 0 1 -3 22.28 2.54 0 -1 -3 21.05 2.76 0 -1 3 21.64 2.64 0 -1 3 20.97 2.70 0 -1 -3 24.55 2.51 0 1 3 24.97 2.47 0 -1 -4 -0.34 1.33 0 1 -4 -0.21 0.81 0 1 -4 -0.69 0.94 0 1 -4 0.28 0.79 0 -1 4 -0.50 0.73 0 1 4 0.50 1.12 0 -1 -4 0.67 1.27 0 -1 -4 0.25 1.26 0 -1 4 0.67 0.65 0 -1 4 0.28 0.90 0 1 4 0.09 0.59 0 -1 -5 327.65 32.63 0 1 -5 332.21 32.43 0 -1 5 320.73 32.08 0 1 -5 330.81 32.11 0 -1 5 370.18 32.27 0 -1 5 350.86 32.55 0 1 5 331.61 32.00 0 -1 -6 -0.84 1.09 0 -1 -6 0.94 1.52 0 -1 -6 -0.48 1.58 0 1 -6 -0.37 1.60 0 -1 6 -0.29 1.02 0 -1 6 2.23 0.95 0 1 6 -0.46 1.48 0 -1 6 -1.68 1.52 0 1 -6 -0.15 0.95 0 1 6 0.45 0.64 0 -1 6 0.44 0.68 0 -1 -7 79.21 7.86 0 1 -7 76.56 8.52 0 -1 -7 87.60 8.79 0 1 -7 76.82 8.48 0 -1 -7 79.72 8.72 0 1 -7 72.61 7.82 0 -1 7 75.33 8.08 0 -1 7 93.68 8.74 0 1 7 90.74 8.75 0 -1 7 80.89 7.78 0 1 7 77.41 7.64 0 1 -8 -0.56 1.69 0 -1 -8 0.63 2.24 0 -1 -8 1.26 2.20 0 1 -8 1.53 1.85 0 -1 8 -1.35 1.37 0 1 8 3.11 2.12 0 -1 8 -0.58 2.27 0 -1 8 0.94 0.90 0 1 -9 1.74 2.23 0 -1 -9 1.40 2.41 0 -1 9 -0.65 2.28 0 1 9 2.06 2.11 0 -1 -9 -0.71 2.57 0 1 -9 -1.96 2.48 0 -1 9 -0.67 1.89 0 1 9 1.25 2.06 0 -1 -10 1.52 2.75 0 1 -10 -0.62 2.87 0 1 10 -0.76 2.66 0 -1 10 2.15 2.80 0 1 -10 -1.10 2.54 0 1 -10 0.74 2.65 0 -1 -10 1.59 2.75 0 1 10 -2.80 2.42 0 -1 10 1.50 2.63 0 -1 -11 59.92 8.57 0 1 -11 68.31 8.35 0 -1 11 81.08 8.70 0 1 11 95.53 9.26 0 -1 -11 52.67 8.45 0 1 -11 69.32 8.24 0 1 -11 60.63 8.59 0 1 11 87.13 8.70 0 -1 -12 -4.23 3.71 0 1 -12 0.70 3.34 0 1 12 -0.92 3.62 0 -1 12 0.88 3.23 0 1 -12 0.93 3.48 0 -1 -12 -1.87 3.74 0 -1 -12 5.05 3.89 0 1 -12 -0.58 3.19 0 1 12 -1.72 3.31 0 1 -13 22.09 4.71 0 -1 -13 19.22 4.96 0 1 13 25.91 5.08 0 -1 13 28.67 5.17 0 -1 -13 19.02 5.21 0 -1 -13 17.10 4.95 0 1 -13 9.06 4.56 0 1 13 27.88 5.08 0 1 -14 -2.20 3.84 0 -1 -14 -1.80 4.10 0 1 14 6.30 4.20 0 -1 14 -1.01 4.11 0 1 -14 1.06 4.65 0 -1 -14 1.06 4.19 0 -1 -14 9.09 4.54 0 1 14 6.98 4.08 0 -1 -15 2.67 4.60 0 1 15 -5.40 4.95 0 -1 15 -3.14 4.42 0 1 -15 -1.07 4.34 0 -1 -15 3.29 5.03 0 1 15 2.10 4.19 0 -1 16 2.14 4.60 0 1 16 -1.10 4.45 0 -1 -16 5.51 4.92 0 1 16 2.19 4.67 0 1 17 -2.19 4.89 0 -1 17 -2.12 4.70 0 -1 -17 -4.20 4.90 0 -1 17 4.69 5.19 0 1 17 8.98 5.19 0 -2 0 402.00 38.37 0 2 -1 0.25 0.30 0 -2 -1 0.91 0.82 0 2 1 0.10 0.50 0 -2 1 -0.66 0.78 0 -2 1 0.40 0.28 0 -2 1 0.56 0.35 0 2 1 -0.32 0.66 0 2 2 224.92 20.22 0 -2 2 187.74 20.35 0 -2 -2 228.77 20.21 0 -2 2 189.33 20.25 0 2 -2 220.43 20.37 0 2 -2 207.98 20.22 0 -2 -2 223.59 20.60 0 -2 2 221.30 20.23 0 2 2 202.49 20.38 0 -2 -2 207.95 20.34 0 2 2 195.88 20.33 0 -2 3 0.72 0.64 0 -2 3 2.02 0.78 0 2 -3 -0.52 0.50 0 -2 3 1.17 0.77 0 -2 3 1.64 0.65 0 2 3 0.72 1.17 0 -2 -3 0.21 0.46 0 -2 3 0.81 0.67 0 2 -3 -0.20 0.94 0 2 3 -0.76 1.26 0 2 3 0.36 0.42 0 -2 3 -0.54 0.76 0 -2 -3 0.31 0.92 0 2 3 -0.42 0.78 0 -2 4 12.38 1.70 0 -2 -4 16.95 2.39 0 -2 4 11.24 1.80 0 2 -4 14.62 1.92 0 -2 4 18.27 1.90 0 2 -4 12.42 1.75 0 2 -4 14.09 1.76 0 -2 4 11.70 1.94 0 2 4 13.85 1.73 0 -2 -4 13.68 1.86 0 -2 5 1.49 0.88 0 -2 -5 1.87 1.62 0 2 -5 1.44 1.18 0 2 -5 -1.21 1.00 0 -2 5 -0.37 1.17 0 2 -5 -1.34 1.17 0 -2 -5 -1.90 1.64 0 -2 5 -0.65 1.17 0 -2 -5 -0.14 0.89 0 2 5 0.26 0.81 0 -2 -6 247.84 23.94 0 -2 -6 254.51 23.98 0 2 -6 211.55 23.40 0 2 -6 242.92 23.31 0 -2 6 266.77 23.38 0 -2 6 255.49 23.70 0 2 6 231.36 23.06 0 2 -7 1.49 1.49 0 -2 -7 -1.21 2.03 0 -2 7 -0.56 1.08 0 2 7 1.70 1.60 0 2 -7 -1.39 1.30 0 -2 7 -0.48 1.66 0 -2 -7 0.59 1.95 0 -2 -8 18.57 3.47 0 2 -8 18.65 3.39 0 -2 -8 25.23 2.60 0 2 -8 21.71 3.22 0 -2 -8 17.73 3.77 0 -2 8 21.45 3.46 0 -2 8 20.23 2.78 0 2 -8 15.51 2.57 0 -2 8 22.83 3.52 0 2 8 21.78 3.48 0 -2 8 20.68 2.43 0 2 -9 -0.37 1.98 0 2 -9 3.20 2.47 0 -2 -9 1.48 2.61 0 2 -9 -1.48 2.31 0 -2 -9 0.75 2.60 0 2 9 -1.22 2.04 0 -2 9 2.78 2.17 0 -2 9 -0.36 1.49 0 -2 9 4.37 2.38 0 2 9 -1.42 2.31 0 -2 9 1.01 1.13 0 2 -10 58.36 8.10 0 -2 -10 80.23 8.88 0 -2 10 73.87 8.66 0 2 10 84.62 8.68 0 -2 10 70.44 7.86 0 -2 10 82.24 8.75 0 2 10 91.13 8.98 0 2 -10 62.83 8.48 0 -2 -10 73.42 8.88 0 2 -10 69.95 8.00 0 -2 -11 1.72 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872.95 81.10 0 3 -1 824.89 81.17 0 -3 -1 841.02 81.44 0 -3 -1 897.24 81.29 0 -3 1 765.01 81.11 0 3 1 890.42 81.34 0 -3 1 852.75 81.06 0 -3 1 893.05 81.20 0 3 -1 885.67 81.08 0 3 -1 840.08 81.13 0 3 1 806.86 81.21 0 -3 1 880.11 81.16 0 3 1 863.28 81.25 0 3 -2 0.84 0.65 0 3 -2 0.19 0.45 0 -3 -2 -0.93 1.16 0 3 2 0.70 0.79 0 -3 -2 0.13 0.75 0 -3 2 -0.60 1.05 0 -3 2 0.54 0.45 0 3 2 -0.41 0.82 0 -3 2 0.22 0.46 0 -3 2 0.55 0.44 0 -3 -2 -0.59 1.03 0 3 2 1.49 1.02 0 -3 -3 298.37 27.89 0 3 -3 289.26 27.67 0 -3 -3 303.01 27.33 0 3 3 286.15 27.32 0 -3 3 274.76 27.37 0 -3 3 258.70 27.36 0 -3 -3 281.50 27.53 0 -3 -3 320.07 27.91 0 -3 -4 0.35 0.66 0 3 -4 -0.59 1.23 0 3 -4 0.80 0.67 0 -3 4 -1.22 1.02 0 3 -4 0.41 0.64 0 -3 4 0.51 0.84 0 -3 4 -0.44 0.86 0 -3 -4 2.41 1.33 0 3 -5 302.97 28.18 0 3 -5 278.33 27.93 0 3 -5 283.67 27.87 0 -3 5 292.83 28.16 0 -3 5 296.30 28.07 0 -3 -5 305.33 28.79 0 3 -6 -0.38 0.68 0 -3 6 0.58 1.07 0 -3 -6 0.61 2.01 0 -3 -6 -2.44 2.23 0 3 -6 3.75 1.61 0 -3 -6 0.59 1.85 0 3 -6 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5 8 7.52 2.37 -10 -5 -8 0.68 3.34 10 5 -8 3.96 4.06 -10 5 8 5.68 2.45 -10 -5 8 8.72 3.38 -10 5 8 5.82 2.62 -10 -5 8 2.33 2.53 -10 -5 8 2.51 2.92 10 -5 8 3.99 2.73 10 -5 8 -1.52 3.51 10 5 8 5.93 3.69 -10 -5 -9 5.70 5.44 -10 5 -9 6.64 3.96 10 -5 -9 6.18 2.14 10 -5 -9 -4.29 3.62 10 5 -9 4.75 4.41 -10 -5 -9 -0.71 3.66 -10 5 9 4.44 2.63 -10 -5 9 6.59 3.98 -10 -5 9 11.68 3.84 -10 5 9 5.96 3.06 -10 -5 9 -0.64 2.65 10 5 9 -4.15 3.69 10 -5 9 3.90 3.44 10 -5 9 8.61 3.17 -10 -5 -10 17.93 6.18 10 -5 -10 13.85 4.92 10 5 -10 6.69 3.59 10 5 -10 12.49 4.70 -10 5 10 8.25 3.15 -10 -5 10 9.17 4.58 10 -5 10 10.41 4.00 -10 -5 10 7.78 4.01 -10 5 10 9.63 3.65 -10 -5 10 15.20 3.67 10 -5 10 7.90 3.88 10 5 10 15.23 4.24 -10 -5 -11 -10.96 6.67 10 -5 -11 2.75 5.03 10 5 -11 2.63 3.42 10 5 -11 0.82 4.27 -10 5 11 4.21 3.15 -10 -5 11 -4.42 4.71 10 -5 11 7.22 4.14 -10 -5 11 -2.11 4.07 -10 -5 11 -2.26 3.39 -10 5 11 1.63 3.58 10 -5 11 7.09 3.94 10 5 11 -0.75 3.88 -10 -5 -12 4.86 6.50 10 -5 -12 -2.87 5.63 10 5 -12 5.51 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4.39 -10 -6 2 30.98 3.59 -10 6 2 35.04 4.58 -10 -6 2 26.78 4.57 -10 -6 -2 36.51 3.66 10 6 2 22.83 5.10 10 6 -2 34.13 5.72 -10 6 -3 2.20 2.10 10 -6 3 0.45 1.78 10 -6 -3 -0.68 2.04 10 6 3 0.68 2.58 -10 -6 -3 2.21 1.22 -10 -6 3 1.67 1.03 10 -6 3 1.24 2.37 -10 6 3 -0.65 2.30 -10 -6 3 2.16 2.30 10 6 3 6.12 3.89 10 6 -3 1.02 3.32 -10 6 3 2.55 1.25 -10 6 -4 -0.60 2.14 10 -6 4 0.88 1.73 10 6 -4 0.30 1.33 10 6 -4 1.41 2.08 10 -6 -4 2.23 2.53 10 6 4 1.25 2.45 10 6 -4 -2.05 3.65 -10 -6 4 0.32 1.11 -10 6 4 0.72 2.20 -10 -6 4 2.21 2.43 10 -6 4 -2.53 2.50 10 6 -4 -0.95 3.39 10 6 4 -1.00 3.30 -10 6 -5 -2.00 2.35 10 -6 -5 1.01 1.53 10 6 -5 -0.30 1.40 10 6 -5 -1.45 2.65 10 -6 5 3.06 1.90 10 -6 -5 4.09 2.75 10 6 5 0.57 2.47 10 6 -5 -2.13 4.05 -10 -6 5 1.01 1.14 -10 6 5 -0.71 1.65 -10 6 5 4.80 2.77 10 -6 -5 0.50 2.43 10 6 5 0.98 3.38 10 6 -5 6.97 3.75 -10 -6 5 0.76 2.41 10 -6 5 3.23 2.81 -10 6 -6 -1.49 2.65 10 -6 -6 -0.80 1.56 -10 -6 -6 7.08 4.90 10 6 -6 2.21 2.63 10 -6 6 -0.43 1.74 10 -6 -6 -0.90 2.70 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40.44 9.09 10 7 -12 67.55 9.00 10 -7 12 36.66 7.82 -10 7 12 60.88 9.41 10 7 12 80.76 9.22 -10 -7 12 62.71 8.81 -10 7 12 65.22 7.74 10 -7 12 48.43 7.76 10 -7 -13 -1.48 6.00 -10 -7 13 1.37 5.80 10 -7 13 1.00 4.58 -10 7 13 7.01 5.85 10 7 13 4.68 5.13 -10 -7 13 3.84 5.61 -10 7 13 1.68 3.96 -10 -7 -13 1.65 6.75 10 -7 -14 -5.71 6.37 10 -7 14 6.39 5.61 -10 -7 14 1.44 6.02 10 -7 14 4.92 4.63 -10 7 14 2.78 5.44 10 7 14 -4.75 5.49 -10 -7 14 5.37 5.49 -10 7 14 -7.74 4.72 -10 -7 -14 -1.63 6.36 10 -8 0 3.73 1.98 10 8 0 6.56 3.49 10 -8 0 1.80 3.22 -10 8 0 -0.56 2.22 10 8 1 13.14 3.78 10 8 -1 3.01 3.42 10 -8 1 10.30 3.46 10 -8 -1 10.66 3.76 10 -8 1 6.76 3.19 10 -8 -1 12.78 3.97 -10 8 1 9.69 2.50 -10 8 -1 4.04 2.53 10 -8 -1 2.43 2.34 10 -8 1 7.39 2.17 10 8 1 12.20 4.51 -10 -8 -1 3.08 1.83 10 8 -1 6.09 4.00 10 8 2 12.06 3.79 10 8 -2 12.75 4.41 10 -8 2 10.81 3.33 10 -8 -2 9.92 4.19 10 -8 2 17.43 3.90 -10 8 -2 12.27 2.94 -10 8 2 12.76 3.25 10 -8 -2 11.98 4.32 10 -8 -2 15.03 3.28 10 -8 2 12.09 2.55 10 8 2 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10.20 3.82 10 -8 -7 17.75 3.30 -10 -8 -7 31.70 7.05 10 8 7 22.43 3.40 10 8 -7 14.27 5.73 -10 -8 -7 12.27 4.69 10 8 -7 9.12 3.71 10 -8 7 14.29 2.72 10 -8 -7 20.57 4.63 -10 8 7 19.42 4.79 -10 8 7 11.57 2.85 -10 -8 7 17.10 4.40 10 8 7 21.34 5.05 10 -8 7 16.46 4.63 10 -8 -7 20.64 3.58 10 -8 -8 -2.12 2.48 -10 8 -8 0.96 3.61 -10 -8 -8 6.35 5.49 10 8 -8 3.90 5.86 -10 -8 -8 1.00 4.48 10 8 -8 -5.19 3.04 -10 8 8 -2.33 4.16 -10 8 8 -2.60 2.60 10 -8 8 3.60 4.31 10 -8 8 -1.82 4.29 10 8 8 0.96 4.17 -10 -8 8 4.00 3.51 -10 8 -9 56.74 9.87 -10 -8 -9 75.77 11.51 -10 -8 -9 94.45 10.72 10 8 -9 76.98 11.16 10 -8 -9 63.82 10.72 -10 8 9 80.67 10.64 -10 8 9 74.96 8.79 10 -8 9 77.01 9.91 10 -8 9 80.51 9.54 10 8 9 81.25 9.86 -10 -8 9 84.46 10.05 -10 -8 -10 -3.19 5.85 10 -8 -10 1.47 5.51 10 8 -10 -0.75 3.15 -10 -8 -10 7.40 5.25 10 8 -10 6.13 5.47 10 8 10 2.10 4.14 -10 8 10 2.61 4.78 -10 8 10 -1.31 3.24 10 -8 10 -3.80 4.89 10 -8 10 -2.54 3.68 10 8 10 -0.83 4.15 -10 -8 10 3.35 4.52 -10 -8 -11 4.86 6.35 10 8 -11 7.92 6.01 10 -8 11 13.77 5.26 10 8 11 1.09 4.30 -10 8 11 4.06 5.97 -10 8 11 12.14 3.71 10 -8 11 1.93 4.65 -10 -8 11 5.87 4.52 -10 -8 -12 8.16 7.29 10 8 -12 1.01 5.30 10 -8 12 -4.20 4.66 -10 -8 12 7.44 5.02 -10 8 12 8.32 5.91 10 8 12 4.47 4.73 -10 8 12 3.80 3.67 10 -8 12 6.65 4.49 10 -8 -13 23.59 7.27 10 -8 13 23.98 6.06 -10 8 13 15.35 6.87 10 8 13 20.70 6.14 -10 8 13 32.35 5.44 -10 -8 13 29.91 6.88 -10 -8 -13 24.51 8.34 10 -9 0 45.63 6.13 10 -9 0 52.48 7.22 10 9 0 49.91 7.36 -10 9 0 56.25 6.41 10 -9 0 45.00 7.17 10 -9 1 -1.62 3.40 10 -9 -1 9.16 4.22 10 9 1 11.09 4.25 10 9 -1 5.30 3.84 10 -9 1 -0.96 3.47 10 -9 -1 11.83 4.59 -10 9 1 6.13 2.83 -10 9 -1 3.04 2.66 10 -9 1 1.49 2.16 10 -9 -1 3.86 2.47 10 9 1 6.39 4.50 -10 -9 -1 3.28 2.13 10 9 -2 14.76 4.96 10 -9 2 10.36 3.38 10 -9 -2 8.79 4.28 10 9 2 17.01 4.18 10 -9 2 15.22 4.50 -10 9 2 11.60 3.30 -10 9 -2 13.39 3.05 10 -9 -2 4.74 4.25 10 -9 -2 7.21 2.86 10 9 -2 14.06 4.99 10 9 2 15.14 5.22 -10 -9 -2 12.81 2.72 -10 9 -3 21.70 3.68 10 -9 -3 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207.92 19.98 -12 -5 -2 159.84 18.45 12 5 2 261.01 21.14 12 5 -2 234.29 21.09 -12 -5 -3 18.81 3.45 12 -5 3 13.65 2.20 12 -5 3 9.50 2.68 12 5 -3 11.43 2.47 -12 5 3 17.68 3.38 12 -5 3 11.76 3.29 -12 -5 3 14.11 2.19 -12 5 3 12.29 3.04 12 5 3 10.50 3.88 12 -5 3 7.00 3.17 12 -5 -3 15.18 3.78 12 5 -3 14.27 4.60 -12 -5 -4 11.13 3.25 -12 -5 -4 8.34 4.42 12 5 -4 9.10 2.15 12 -5 4 10.67 2.65 12 5 -4 8.92 4.26 12 -5 4 7.35 2.88 -12 -5 4 8.82 1.93 -12 5 4 9.09 2.96 -12 5 4 12.68 3.18 12 -5 4 11.28 3.26 12 -5 -4 15.80 3.59 -12 5 4 15.50 2.59 12 5 -4 5.22 3.95 12 5 4 14.46 4.15 -12 5 -5 10.55 3.31 -12 -5 -5 -1.22 4.74 12 5 -5 6.03 1.99 12 -5 5 6.72 2.43 12 -5 -5 9.84 3.26 12 5 5 10.31 3.20 12 5 -5 2.27 4.16 12 -5 5 3.78 2.65 -12 -5 5 8.02 1.79 -12 5 5 8.03 2.99 -12 5 5 6.44 2.33 -12 5 5 14.60 3.50 -12 -5 5 7.62 3.41 12 5 5 4.06 3.92 12 -5 5 15.80 3.90 12 -5 -5 3.63 2.71 12 5 -5 6.63 4.21 -12 5 -6 4.99 3.13 -12 -5 -6 1.25 4.35 12 -5 -6 4.79 3.20 12 5 6 6.94 3.10 -12 -5 -6 9.94 3.13 12 5 -6 2.30 4.92 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10.53 3.86 -12 7 -6 24.41 4.39 -12 -7 -6 35.84 7.27 12 7 -6 18.43 4.28 12 -7 6 8.98 3.03 12 -7 -6 13.69 4.56 -12 -7 -6 14.82 4.10 12 7 6 15.67 3.76 12 7 -6 11.73 5.40 12 -7 6 21.83 4.56 -12 7 6 22.86 4.72 -12 7 6 19.30 3.36 -12 -7 6 18.87 4.62 12 -7 6 27.41 5.14 12 -7 -6 20.51 3.91 12 7 6 10.30 4.86 -12 7 -7 4.78 3.84 -12 -7 -7 7.47 5.34 12 7 -7 1.81 3.22 12 -7 7 4.57 2.13 12 -7 -7 4.49 3.67 -12 -7 -7 4.96 3.94 12 7 7 3.35 2.91 12 7 -7 9.22 5.22 -12 7 7 7.93 4.60 -12 7 7 5.80 2.73 -12 -7 7 4.12 3.48 12 -7 7 1.58 3.60 12 -7 7 11.65 4.70 12 7 7 10.03 4.95 12 -7 -7 2.91 2.72 -12 7 -8 4.29 4.18 -12 -7 -8 10.54 5.81 12 7 -8 1.89 3.36 12 -7 8 0.49 2.19 12 -7 -8 3.57 4.42 12 7 -8 2.59 5.40 -12 -7 -8 -3.46 4.42 -12 7 8 -4.64 4.74 -12 7 8 9.78 4.60 -12 7 8 -0.60 2.92 12 -7 8 -1.59 3.77 12 -7 8 9.01 4.94 12 7 8 -1.07 4.67 -12 -7 8 3.22 3.77 -12 -7 -9 23.19 7.19 -12 7 -9 10.71 5.16 12 7 -9 29.33 7.20 12 -7 -9 15.19 5.65 -12 7 9 22.65 4.28 -12 7 9 26.02 6.20 12 -7 9 9.26 5.16 12 7 9 31.83 6.08 -12 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29.56 5.77 12 -8 -2 47.70 7.25 -12 8 2 25.50 4.70 -12 8 -2 28.32 5.03 12 -8 -2 28.57 4.79 12 -8 2 32.68 4.38 12 8 2 35.08 6.69 12 8 -2 20.20 6.28 12 -8 -3 70.77 8.19 12 8 3 71.53 8.44 12 8 -3 67.82 9.40 12 -8 3 58.36 8.18 -12 8 3 70.65 8.00 -12 8 -3 57.32 7.77 12 8 3 43.61 8.58 12 8 -3 63.66 9.40 -12 8 -4 4.72 3.20 12 -8 4 2.20 2.21 12 8 -4 4.29 1.91 12 8 -4 3.59 3.03 12 -8 -4 8.43 3.76 12 8 4 6.25 3.51 12 -8 4 6.16 3.91 -12 8 4 3.19 3.21 -12 8 4 9.00 3.49 12 8 -4 11.17 5.66 -12 -8 4 2.91 3.38 12 -8 -4 2.94 3.25 12 8 4 -2.57 4.39 -12 8 -5 40.09 6.27 12 -8 5 41.52 5.69 12 8 -5 42.77 5.25 12 8 -5 41.78 6.54 12 -8 -5 67.36 7.34 12 8 5 51.83 6.57 12 8 -5 40.81 7.83 -12 8 5 44.49 6.64 12 -8 5 43.82 7.04 -12 8 5 54.03 7.25 -12 -8 5 52.45 7.21 12 -8 -5 50.72 6.66 12 8 5 44.84 7.57 -12 8 -6 0.90 3.54 -12 -8 -6 1.56 5.25 12 -8 6 7.02 2.30 12 8 -6 5.51 3.53 12 -8 -6 7.64 3.87 12 8 -6 1.39 5.17 -12 -8 -6 2.63 4.20 12 8 6 7.67 3.54 12 -8 6 9.12 4.32 -12 8 6 8.27 2.38 -12 8 6 1.09 3.96 -12 -8 6 5.25 4.03 12 -8 6 3.96 4.37 12 -8 -6 3.73 3.24 12 8 6 3.62 5.06 -12 8 -7 4.83 3.87 -12 -8 -7 1.56 5.57 12 8 -7 5.60 5.91 -12 -8 -7 5.53 4.34 12 8 7 2.26 3.03 12 8 -7 2.80 3.34 12 -8 7 3.34 2.35 12 -8 -7 1.17 3.60 -12 8 7 3.40 2.55 -12 8 7 1.18 4.32 12 -8 7 7.13 4.56 12 -8 -7 2.11 2.92 -12 -8 7 2.19 3.96 12 8 7 1.16 4.47 12 -8 7 0.92 4.09 -12 8 -8 2.15 4.34 -12 -8 -8 3.10 5.95 12 8 -8 8.46 6.10 -12 -8 -8 14.56 5.14 12 8 -8 6.76 4.05 12 -8 -8 -1.25 4.24 -12 8 8 7.51 5.11 -12 8 8 11.12 3.40 -12 -8 8 12.54 4.95 12 -8 8 4.59 4.44 12 -8 8 6.25 4.74 12 8 8 14.35 5.02 -12 8 -9 67.30 9.81 -12 -8 -9 64.18 10.65 12 8 -9 60.59 10.54 -12 -8 -9 62.14 9.43 -12 8 9 70.39 8.08 -12 8 9 54.29 9.41 12 -8 9 65.15 9.47 -12 -8 9 70.03 9.39 12 8 9 76.73 9.54 -12 -8 -10 22.25 7.12 -12 8 -10 6.33 5.47 12 -8 -10 -1.56 5.43 12 8 -10 15.83 7.13 -12 8 10 8.20 3.58 -12 8 10 5.53 5.36 -12 -8 10 -1.23 4.73 12 -8 10 7.60 5.54 12 8 10 0.97 4.65 -12 -8 -11 12.84 7.36 12 8 -11 1.22 6.30 12 -8 11 2.34 5.54 12 8 11 -2.30 4.65 -12 8 11 -1.42 6.00 12 -8 11 3.27 5.34 -12 -8 11 3.85 4.84 -12 -8 -12 14.55 7.45 12 8 -12 3.27 6.03 12 -8 12 10.38 5.78 -12 -8 12 17.37 6.12 12 -8 12 5.28 5.26 12 8 12 4.64 5.19 -12 8 12 4.31 6.29 12 -8 13 8.00 5.37 12 8 13 5.76 5.62 -12 -8 13 4.15 5.53 12 -9 0 16.14 3.57 12 9 0 12.25 4.89 12 -9 0 25.63 5.64 -12 9 0 19.32 4.09 12 9 1 2.07 3.85 12 9 -1 2.36 4.14 12 -9 1 7.56 4.37 12 -9 -1 3.76 4.72 -12 9 -1 -0.72 2.95 -12 9 1 -2.14 2.95 12 -9 1 3.97 2.56 12 -9 -1 0.72 2.69 -12 -9 -1 0.74 2.14 12 9 1 -1.43 4.79 12 9 -1 4.30 5.39 12 9 2 43.24 6.58 12 9 -2 35.20 6.94 12 -9 2 48.42 7.10 12 -9 -2 35.91 7.30 -12 9 -2 36.45 5.54 -12 9 2 50.37 6.13 12 -9 -2 32.76 5.56 -12 -9 -2 27.08 4.79 12 9 2 47.80 8.00 12 -9 -3 -0.88 3.18 12 9 3 2.63 3.51 12 9 -3 2.66 5.07 12 -9 3 -3.02 3.98 -12 9 3 3.12 3.12 -12 9 -3 0.76 2.95 12 9 -3 5.51 5.05 12 9 3 8.25 5.10 12 9 -4 3.01 1.84 12 9 -4 -4.64 3.70 12 -9 -4 -1.92 3.43 12 9 4 -3.22 3.76 12 -9 4 -1.01 4.26 -12 9 4 3.38 3.22 -12 9 -4 9.73 3.78 12 9 4 1.33 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14.33 5.14 12 10 7 8.36 5.21 -12 10 -8 17.98 5.31 -12 -10 -8 22.66 7.73 12 -10 -8 4.67 6.50 12 10 -8 9.96 4.53 -12 -10 -8 17.38 6.19 12 10 -8 24.61 8.08 -12 10 8 16.66 6.39 -12 10 8 10.32 5.49 12 -10 8 4.58 5.29 12 -10 8 10.05 5.78 -12 -10 8 27.39 6.19 12 10 8 17.93 6.00 -12 10 -9 -2.28 5.00 -12 -10 -9 19.11 6.73 12 -10 -9 -4.80 6.62 -12 -10 -9 5.83 6.05 12 10 -9 1.59 7.45 -12 10 9 8.77 5.86 12 10 9 -0.99 4.49 -12 10 9 14.69 5.81 12 -10 9 4.58 5.53 12 10 9 2.09 4.98 -12 -10 9 6.46 5.23 -12 -10 -10 9.51 7.45 12 -10 -10 16.12 7.31 12 10 -10 36.25 8.26 -12 10 10 39.37 7.99 12 10 10 33.79 5.85 -12 10 10 24.53 6.71 -12 -10 10 13.34 6.49 12 10 10 41.29 6.54 12 -10 10 8.13 6.33 -12 -10 -11 15.71 7.59 12 -10 -11 17.39 7.39 12 10 -11 12.53 7.50 -12 10 11 10.41 6.19 12 10 11 18.71 5.61 -12 10 11 16.51 6.53 -12 -10 11 19.15 6.74 12 -10 11 10.50 6.21 12 10 12 10.58 5.54 12 10 -12 15.93 7.63 12 -10 12 6.45 6.58 12 11 0 -2.44 4.59 12 -11 0 2.81 5.22 -12 11 0 2.40 3.51 -12 -11 0 4.22 2.74 12 11 1 1.13 4.61 12 11 -1 -2.61 5.16 -12 11 -1 1.58 3.26 12 -11 1 -4.03 5.18 12 -11 -1 -4.50 6.13 -12 11 1 0.80 3.53 12 11 1 7.74 6.39 -12 -11 -1 0.98 2.76 -12 -11 1 5.16 3.13 12 11 2 48.60 8.68 12 11 -2 64.29 10.35 12 -11 2 80.99 10.34 12 -11 -2 77.14 11.03 -12 11 2 77.02 8.72 -12 11 -2 68.87 8.71 12 11 2 72.87 10.75 12 11 3 9.48 4.39 12 11 -3 7.41 6.11 12 -11 3 3.88 5.18 12 -11 -3 11.97 6.49 -12 11 3 6.89 3.69 -12 11 -3 17.21 4.44 12 11 3 1.47 6.01 12 11 -4 -0.97 3.65 12 11 4 0.86 3.97 12 -11 4 -3.93 5.29 -12 11 4 6.46 4.24 -12 11 -4 -1.70 3.81 12 11 4 -1.42 5.74 12 -11 -5 -5.59 5.59 12 11 -5 -2.94 3.51 12 11 5 1.53 3.67 12 -11 5 -9.28 5.87 -12 11 5 -1.99 4.61 -12 11 -5 -0.88 3.86 12 11 5 -4.08 5.86 -12 11 -6 -0.91 4.12 12 -11 -6 -4.45 5.86 12 11 -6 2.91 4.01 -12 -11 -6 1.17 4.99 12 11 6 -0.69 3.47 12 11 -6 -3.39 6.93 -12 11 6 -2.13 4.85 12 -11 6 2.67 5.63 -12 11 6 -2.28 4.87 12 -11 -6 0.72 3.88 12 11 6 -3.88 5.29 -12 11 -7 -0.97 4.32 -12 -11 -7 -3.31 6.38 12 11 -7 -2.93 3.82 12 -11 -7 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1.28 5.50 12 12 -7 -7.29 7.99 -12 12 7 1.12 4.90 12 -12 7 4.25 6.55 12 12 7 -3.95 3.66 -12 12 7 -2.37 5.10 -12 12 -7 2.87 4.31 -12 12 -8 -6.04 4.89 -12 -12 -8 1.64 6.79 12 -12 -8 -1.58 6.33 12 12 -8 -9.06 7.94 -12 -12 -8 6.50 6.27 -12 12 8 -1.16 5.58 12 -12 8 -1.33 5.88 12 12 8 -0.82 4.22 -12 12 8 1.24 5.24 12 -12 8 4.80 5.82 -12 -12 -9 35.06 8.53 12 -12 -9 17.26 7.51 12 12 -9 37.24 9.93 -12 -12 -9 9.05 6.59 -12 12 9 18.81 6.15 12 12 9 14.67 5.10 -12 12 9 16.60 6.33 -12 -12 9 17.25 6.36 12 -12 9 13.33 6.37 12 12 -10 -6.63 8.42 -12 12 10 4.70 5.62 12 12 10 4.47 4.45 -12 12 10 -1.28 5.87 12 -12 10 1.22 6.16 -12 -12 10 1.35 5.71 12 13 0 30.91 7.68 12 -13 0 30.27 7.49 12 -13 0 48.36 9.49 -12 13 0 37.90 6.03 -12 -13 0 28.01 5.46 12 13 -1 33.39 7.99 12 13 1 44.47 7.28 12 -13 -1 21.81 7.14 12 -13 1 14.97 7.25 12 -13 -1 39.54 9.03 -12 13 -1 24.69 5.27 -12 13 1 22.62 5.56 -12 -13 1 26.05 5.23 12 -13 -2 -1.18 5.21 12 13 -2 4.64 6.38 12 13 2 2.24 5.01 12 -13 2 3.27 6.83 12 -13 -2 7.59 7.58 -12 13 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6 -9 22.31 6.75 16 -6 -9 20.51 6.48 16 6 -9 34.28 7.69 16 -6 9 23.78 6.52 -16 6 9 30.58 6.72 -16 6 9 33.10 7.16 16 6 9 26.98 6.82 16 -6 9 26.58 7.25 16 -6 -10 11.81 5.88 16 6 -10 12.27 6.75 16 -6 10 14.50 5.80 -16 6 10 17.59 6.07 -16 -6 -10 7.36 6.56 -16 6 -10 14.94 6.89 16 6 10 13.53 6.00 16 -6 10 6.13 6.38 16 -6 -11 6.01 5.93 16 6 -11 1.12 4.92 16 6 -11 1.13 6.23 -16 -6 -11 1.50 6.44 16 6 11 4.22 5.68 16 -6 11 -1.16 5.72 16 -6 11 1.22 5.45 -16 6 11 -1.19 5.82 16 6 -12 -1.11 4.82 16 -6 12 1.08 5.54 16 -7 0 4.79 4.92 16 7 0 12.35 5.68 16 7 0 2.50 4.60 16 -7 1 10.94 4.96 16 -7 -1 11.62 5.60 16 7 -1 13.82 6.08 16 7 1 5.89 4.71 16 7 -1 14.37 5.43 16 -7 2 61.76 8.42 16 -7 -2 64.93 8.81 -16 -7 -2 69.68 10.02 -16 7 -2 70.77 8.95 16 -7 2 80.36 10.33 16 -7 -2 76.66 9.81 16 7 2 84.21 11.03 16 7 -2 88.89 11.27 16 7 2 52.09 9.05 16 7 -2 53.22 9.87 16 -7 3 3.35 3.01 16 7 -3 8.57 2.68 16 -7 -3 8.89 4.36 16 7 3 6.22 4.73 -16 7 -3 -2.84 4.06 -16 -7 -3 7.11 4.81 16 7 3 5.90 5.78 16 -7 -3 -2.15 4.73 16 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6.89 6.40 16 9 8 6.42 6.54 -16 -9 -9 -1.45 6.16 -16 9 -9 2.82 6.42 16 9 -9 -3.06 7.01 -16 9 9 8.70 6.12 -16 -9 9 14.28 6.26 16 -9 9 4.10 6.33 16 9 9 -7.22 6.19 -16 -9 -10 1.44 6.65 -16 9 -10 -1.46 7.21 16 9 -10 4.34 7.82 16 -9 10 15.08 6.69 -16 9 10 7.34 6.41 -16 -9 10 10.13 5.88 16 -9 10 8.06 7.22 16 9 10 9.89 6.42 16 10 0 -8.04 5.88 -16 10 0 1.95 4.33 16 -10 0 -5.50 6.04 16 10 0 -1.69 6.75 16 10 1 41.34 8.19 16 10 -1 29.80 8.27 16 -10 1 34.48 8.99 -16 10 -1 38.03 6.79 -16 10 1 56.15 7.48 16 -10 1 45.16 8.79 16 -10 -1 38.21 8.36 16 10 -1 52.02 9.45 16 -10 -2 2.97 3.95 16 10 2 -1.17 5.05 16 10 -2 10.52 6.36 16 -10 2 6.04 6.52 -16 10 2 11.96 4.95 -16 10 -2 7.13 4.63 16 10 -2 4.96 7.27 16 -10 2 5.71 6.28 16 -10 -2 7.47 5.88 16 10 2 11.56 7.47 16 10 -3 28.48 4.61 16 -10 -3 31.33 6.21 16 10 3 41.99 7.23 16 10 -3 32.87 8.51 -16 10 3 41.89 6.74 16 -10 3 15.61 7.30 -16 10 -3 32.93 6.92 16 10 -3 31.99 8.77 16 -10 -3 55.79 8.28 16 10 3 46.93 8.86 16 10 -4 5.72 4.77 16 -10 -4 9.45 4.67 16 10 4 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3.74 22 -5 4 -1.09 4.72 22 -5 -4 -1.46 5.70 22 5 4 3.47 5.70 22 5 -4 1.52 7.05 -22 5 4 -2.02 4.94 22 -5 4 1.15 5.16 -22 5 -4 2.44 5.35 22 5 4 -9.32 6.94 22 5 -4 3.88 6.52 22 -5 -4 2.23 5.89 22 5 -5 5.03 5.67 22 -5 5 -2.12 4.48 22 -5 -5 5.97 6.10 22 5 5 1.06 5.68 22 5 -5 -1.48 7.52 22 -5 5 -4.73 5.70 -22 5 5 -1.01 5.00 -22 5 -5 1.28 5.80 22 5 5 7.50 7.17 22 -5 5 -6.03 7.49 22 5 -5 1.13 6.30 22 -5 6 -1.02 4.39 22 5 6 7.64 5.70 22 5 -6 4.27 6.86 -22 5 6 2.05 4.93 22 -5 6 4.85 6.07 -22 5 -6 2.64 6.07 22 5 6 -7.18 6.98 22 -5 6 -1.48 6.85 22 6 0 -0.90 3.75 22 6 0 4.32 6.55 22 -6 0 -1.02 5.17 -22 6 0 1.08 4.75 22 6 0 -1.67 8.30 22 -6 0 -13.56 7.43 22 6 -1 3.45 3.82 22 6 1 -2.79 3.95 22 6 -1 -6.60 5.56 22 6 1 4.12 6.56 22 6 -1 20.87 7.62 22 -6 1 -2.15 5.37 -22 6 1 5.27 4.75 -22 6 -1 1.11 5.24 22 6 1 3.36 7.83 22 6 -1 3.25 7.59 22 -6 1 1.56 7.07 22 -6 -1 1.43 7.17 22 -6 2 -3.36 4.68 22 6 -2 10.08 4.12 22 6 -2 3.95 5.26 22 6 2 2.59 6.66 22 6 -2 -1.52 7.45 22 -6 2 -1.12 5.28 -22 6 2 4.15 4.76 -22 6 -2 -1.17 5.41 22 6 2 13.36 8.48 22 6 -2 1.55 7.55 22 -6 2 15.82 7.51 22 -6 -2 4.00 6.53 22 -6 3 4.43 4.53 22 6 -3 8.11 4.45 22 6 -3 -3.88 5.10 22 -6 -3 -2.87 5.80 22 6 3 6.03 6.42 22 -6 3 -1.16 5.57 -22 6 3 3.15 5.14 -22 6 -3 -6.00 5.56 22 6 -3 -4.33 7.22 22 -6 3 -11.13 7.72 22 6 -4 8.97 5.29 22 6 -4 15.44 4.49 22 -6 4 11.91 5.14 22 -6 -4 19.32 6.77 22 6 4 16.73 6.75 22 6 -4 15.28 8.34 -22 6 4 15.86 5.60 22 -6 4 14.27 6.30 -22 6 -4 11.22 6.51 22 6 4 22.13 8.13 22 6 -4 9.10 6.91 22 -6 5 1.04 4.36 22 -6 -5 13.65 6.53 22 6 5 -1.02 5.32 22 6 -5 2.99 7.33 22 -6 5 7.31 6.06 -22 6 5 2.12 5.01 -22 6 -5 1.29 5.87 22 6 5 9.13 7.04 22 6 -5 3.42 5.96 22 7 0 5.17 3.90 22 7 0 12.79 7.19 -22 7 0 4.47 5.16 22 7 0 8.44 8.10 22 -7 0 10.85 8.11 22 7 -1 4.12 4.01 22 7 1 -2.68 4.21 22 7 -1 19.96 6.08 22 7 1 1.35 6.52 22 7 -1 5.93 7.38 -22 7 1 6.54 5.07 -22 7 -1 9.16 5.63 22 7 1 1.70 7.82 22 7 -1 19.69 8.40 22 -7 1 32.22 8.53 22 -7 -1 2.93 6.96 22 7 -2 1.59 3.90 22 7 -2 -1.32 5.53 22 -7 -2 5.35 5.53 22 7 2 7.60 6.06 22 7 -2 4.56 7.66 -22 7 2 3.23 5.11 -22 7 -2 3.59 5.63 22 7 2 16.88 8.39 22 -7 2 -1.64 7.28 22 -7 -2 1.35 6.90 22 7 -2 -3.11 7.44 22 7 3 3.53 6.26 22 -7 3 13.28 6.42 -22 7 3 3.28 5.27 22 7 -3 0.76 3.75 22 7 -3 -3.95 5.27 22 -7 -3 1.41 5.52 22 -7 3 1.65 7.59 22 -7 -3 -2.42 6.06 22 7 -3 -8.66 7.58 22 7 4 4.33 5.74 22 7 -4 6.15 7.98 -22 7 4 7.70 5.48 22 -7 4 11.11 6.45 22 -7 -4 -2.95 6.24 22 7 4 1.60 8.15 22 -7 4 6.57 7.48 22 7 -4 3.90 7.23 22 7 -5 -8.03 6.33 22 7 5 6.87 5.58 22 8 0 0.82 4.04 22 -8 0 14.32 8.25 22 8 0 -1.68 8.22 22 8 0 8.42 6.66 22 8 -1 -4.67 3.89 22 8 1 0.85 3.91 22 8 1 9.28 7.40 22 8 -1 -7.32 6.83 -22 8 1 -1.12 5.15 22 -8 1 18.28 8.37 22 -8 -1 1.49 7.25 22 8 1 10.19 7.99 22 8 -1 4.89 7.60 22 8 2 12.40 6.97 22 8 -2 31.69 8.92 -22 8 2 28.91 6.15 22 8 -2 24.58 5.01 22 -8 2 20.40 8.74 22 8 2 35.41 9.58 22 -8 -2 20.47 7.95 22 8 -2 20.09 8.53 22 -8 -3 1.21 6.16 22 8 -3 -4.31 7.08 22 8 3 -2.29 6.43 23 0 0 -4.01 4.40 -23 0 0 0.92 4.39 23 0 0 -5.97 7.20 23 0 -1 10.01 4.68 23 0 -1 11.18 4.47 23 0 1 2.03 4.19 -23 0 1 5.32 4.23 -23 0 -1 3.85 4.69 23 0 -1 15.99 7.04 23 0 1 10.54 7.23 23 0 1 7.82 4.85 23 0 -2 34.41 6.44 23 0 -2 16.11 5.66 23 0 2 36.58 6.50 23 0 2 28.50 6.24 -23 0 -2 44.99 6.96 -23 0 2 39.30 6.52 23 0 -2 37.23 8.92 23 0 2 27.15 8.62 23 0 2 45.77 6.85 23 0 -3 8.19 4.52 23 0 -3 16.05 4.90 23 0 3 9.99 5.07 -23 0 -3 5.21 5.05 -23 0 3 8.23 4.45 23 0 -3 -1.28 6.43 23 0 3 13.41 7.17 23 0 3 8.90 4.80 23 0 4 19.38 5.29 -23 0 -4 9.88 5.44 23 0 -4 15.00 6.41 23 0 4 16.56 5.99 -23 0 4 20.52 4.89 23 0 5 -4.56 4.80 -23 0 5 -0.77 3.79 23 0 5 -3.22 5.26 -23 0 -5 4.63 5.58 23 0 5 5.77 6.78 23 0 -6 4.01 6.74 -23 0 -6 4.93 5.30 23 0 6 1.41 6.91 -23 0 6 2.30 4.19 23 0 6 -4.47 5.43 23 -1 0 2.80 4.13 23 1 0 -1.08 4.47 23 1 0 5.13 4.29 -23 1 0 -2.89 4.92 -23 -1 0 3.54 4.37 23 1 0 -3.02 6.98 23 -1 0 11.89 7.22 23 -1 -1 11.37 4.66 23 1 -1 6.42 4.40 23 1 -1 5.06 4.38 23 -1 1 4.27 4.48 23 1 1 3.28 4.82 -23 1 1 11.09 4.97 -23 -1 1 0.86 4.55 -23 1 -1 12.97 5.36 -23 -1 -1 0.92 4.48 23 1 1 13.71 7.63 23 1 -1 11.76 7.42 23 -1 1 4.51 6.97 23 -1 -1 -5.77 7.02 23 -1 1 0.87 4.76 23 -1 -2 3.86 4.03 23 1 -2 -2.12 4.43 23 -1 -2 1.02 4.26 23 1 -2 -0.99 4.10 23 -1 2 2.18 4.54 23 1 2 -1.11 4.61 -23 -1 2 -3.28 4.16 -23 1 -2 1.04 4.71 -23 -1 -2 -1.93 4.16 -23 1 2 -0.89 4.40 23 -1 -2 8.20 7.32 23 1 2 1.52 6.87 23 1 -2 -2.82 7.36 23 -1 2 4.52 7.04 23 -1 2 -0.93 4.74 23 1 -3 15.00 4.94 23 1 -3 7.90 4.64 23 -1 3 -1.10 4.18 23 1 3 4.49 4.90 23 -1 -3 3.96 4.03 -23 1 -3 8.62 4.97 -23 -1 -3 6.06 4.54 -23 -1 3 2.36 4.17 23 1 3 21.13 7.94 23 -1 -3 17.71 6.79 23 1 -3 5.21 6.63 23 -1 3 1.50 6.77 -23 1 3 2.58 4.36 23 -1 3 1.98 4.86 23 1 -4 7.62 4.56 23 -1 4 11.22 4.89 23 1 4 5.72 4.89 -23 1 4 15.01 4.80 23 -1 4 6.20 5.15 -23 1 -4 2.26 5.27 -23 -1 -4 5.34 4.87 -23 -1 4 9.08 4.42 23 -1 -4 6.83 6.21 23 1 -4 13.01 6.77 23 -1 5 -2.25 4.49 23 1 5 1.15 4.49 23 1 -5 -2.89 7.28 23 -1 5 3.24 5.33 -23 1 5 -0.83 4.09 -23 1 -5 3.55 5.34 -23 -1 -5 -1.14 5.11 23 1 5 -1.45 6.54 23 -1 5 1.46 6.68 23 1 -6 6.83 6.80 -23 1 -6 -2.52 6.03 -23 -1 -6 7.26 5.93 23 1 6 7.04 6.85 23 -1 6 7.13 6.93 -23 1 6 8.21 4.38 23 -1 6 -1.11 5.42 23 -2 0 4.21 4.25 23 2 0 -3.04 4.44 23 2 0 -1.15 4.55 -23 2 0 -1.98 4.47 -23 -2 0 -1.68 4.15 23 2 0 -6.15 7.69 23 -2 0 8.95 7.35 23 -2 1 5.37 4.79 23 2 -1 14.74 5.09 23 2 -1 18.96 5.01 23 2 1 15.61 4.98 23 2 1 4.65 4.76 -23 2 -1 12.38 6.28 -23 -2 1 12.17 4.39 -23 -2 -1 17.64 5.23 -23 2 1 10.54 4.96 23 2 1 10.90 7.67 23 2 -1 18.05 7.58 23 -2 1 22.72 8.16 23 -2 -1 30.28 8.34 23 -2 1 15.09 5.39 23 2 -2 -1.13 4.50 23 2 -2 5.87 4.41 23 -2 2 -2.19 4.48 23 2 2 -1.18 4.97 -23 -2 2 6.95 4.27 -23 2 -2 1.07 5.08 -23 -2 -2 -0.93 4.36 -23 2 2 -0.93 4.14 23 2 2 6.17 6.89 23 2 -2 12.91 7.48 23 -2 2 7.62 7.29 23 -2 -2 -6.81 7.39 23 -2 2 4.73 5.19 23 2 -3 -6.78 5.23 23 2 -3 -0.97 4.19 23 -2 3 -1.11 4.59 -23 2 3 0.89 4.50 23 -2 3 2.99 4.84 -23 2 -3 2.22 4.78 -23 -2 -3 6.90 4.82 23 2 3 1.53 7.12 23 2 -3 1.33 6.82 23 -2 3 1.52 7.15 23 -2 -3 -2.51 6.81 23 2 -4 -3.40 4.53 23 -2 4 -3.35 4.61 23 2 4 -3.44 4.73 23 2 -4 6.09 7.99 -23 2 4 -1.78 4.38 23 -2 4 14.68 5.54 -23 2 -4 -1.16 5.38 -23 -2 -4 -5.26 5.42 23 -2 -4 3.36 6.18 23 2 -4 -1.21 6.15 23 -2 5 1.10 4.47 23 2 -5 8.05 4.93 23 2 -5 8.81 7.52 -23 2 5 3.51 4.61 23 -2 5 14.21 5.69 -23 2 -5 -1.21 5.33 -23 -2 -5 4.50 5.49 23 2 5 11.65 7.56 23 -2 5 7.42 7.34 -23 -2 -6 8.34 5.62 23 2 -6 20.35 7.39 -23 2 6 12.22 4.83 23 -2 6 8.99 5.65 23 -3 0 1.07 4.36 23 3 0 -0.99 4.18 23 3 0 -2.43 4.79 -23 3 0 -1.02 4.63 23 3 0 -1.58 7.47 23 -3 -1 -1.06 4.19 23 -3 1 1.08 4.52 23 3 -1 0.98 4.13 23 3 -1 -3.60 4.96 23 3 1 -1.03 4.18 23 3 1 1.23 4.68 -23 3 -1 -4.28 5.04 -23 3 1 -5.92 5.08 23 3 1 -4.75 7.19 23 3 -1 -6.12 6.96 23 -3 -1 -2.91 6.95 23 -3 1 -1.84 4.57 23 3 -2 2.37 4.62 23 -3 2 4.41 4.36 23 3 -2 4.80 4.25 23 3 2 1.07 4.74 23 -3 2 -4.88 4.85 -23 3 -2 -2.21 4.97 -23 -3 -2 0.89 4.30 -23 3 2 1.91 4.45 23 3 2 -6.29 7.34 23 3 -2 1.46 7.13 23 -3 -2 -8.20 7.36 23 3 -3 8.26 4.82 23 3 -3 4.69 4.04 23 -3 3 1.12 4.42 23 3 -3 -3.11 7.51 23 -3 3 5.13 5.18 -23 3 3 -2.79 4.62 -23 3 -3 5.69 5.40 -23 -3 -3 4.83 4.73 23 3 -3 1.36 6.87 23 -3 -3 -7.50 6.57 23 3 -4 25.91 6.25 23 3 -4 23.01 5.36 23 -3 4 11.18 5.37 23 3 -4 38.06 9.16 23 -3 4 11.83 6.02 -23 3 4 26.10 5.68 -23 3 -4 29.72 6.50 -23 -3 -4 21.62 5.83 23 3 -4 29.73 7.37 23 -3 -4 34.36 7.49 23 3 -5 2.38 4.89 23 -3 5 2.19 4.32 23 3 -5 8.71 7.44 -23 3 5 15.78 5.21 23 -3 5 -1.12 5.20 -23 3 -5 8.62 5.42 -23 -3 -5 6.64 5.44 23 3 5 5.89 6.77 -23 -3 -6 1.16 5.54 23 -4 0 -2.18 4.50 23 4 0 -0.98 3.99 23 4 0 -3.79 4.99 23 4 0 5.97 7.25 -23 4 0 3.17 4.63 23 4 0 -8.00 7.53 23 -4 1 12.09 4.89 23 4 -1 13.35 4.57 23 4 -1 8.80 5.42 23 4 1 14.21 4.81 23 4 1 8.60 7.23 23 4 -1 10.84 7.80 23 -4 1 10.53 5.53 -23 4 -1 1.09 5.17 -23 4 1 12.29 4.82 23 4 1 -1.61 7.50 23 4 -1 -3.12 7.51 23 -4 2 8.87 5.07 23 4 -2 14.97 4.69 23 4 -2 6.20 5.21 23 4 2 18.90 5.26 23 4 2 14.94 7.63 23 -4 2 17.31 5.70 -23 4 2 12.90 4.95 -23 4 -2 24.88 6.47 23 4 2 22.49 8.50 23 4 -2 25.49 8.68 23 -4 -2 13.79 7.56 23 4 -3 2.46 4.63 23 4 -3 5.44 4.34 23 -4 3 -4.47 4.72 23 4 3 2.18 4.51 23 4 3 11.49 6.71 23 -4 3 -1.07 5.22 -23 4 3 4.86 4.69 -23 4 -3 7.02 5.42 23 4 -3 1.39 6.92 23 -4 -3 2.50 6.49 23 4 -4 9.77 4.99 23 4 -4 0.88 3.98 23 -4 4 1.11 4.55 23 4 4 4.76 6.65 23 4 -4 -3.02 7.21 23 -4 4 5.54 5.55 -23 4 4 0.98 4.61 -23 4 -4 4.85 5.17 23 4 4 -4.61 7.41 23 4 -4 2.52 6.56 23 4 5 -1.09 6.16 23 4 -5 1.46 7.29 -23 4 5 2.92 4.81 23 -4 5 6.88 5.40 23 5 0 -0.95 4.14 23 5 0 1.31 5.16 23 5 0 -1.47 7.03 23 -5 0 2.82 4.90 -23 5 0 -1.08 4.81 23 5 0 -1.64 7.73 23 -5 1 11.20 4.90 23 5 -1 3.68 4.05 23 5 -1 3.89 5.02 23 5 1 4.92 4.33 23 5 1 7.04 7.30 23 5 -1 4.52 7.20 23 -5 1 21.03 6.24 -23 5 -1 19.15 5.70 -23 5 1 13.61 5.16 23 5 1 13.22 8.43 23 5 -1 14.41 8.18 23 -5 2 1.13 4.50 23 5 -2 0.90 4.16 23 5 -2 1.29 4.85 23 5 2 -5.11 4.40 23 5 2 -2.66 6.76 23 5 -2 -1.53 7.54 -23 5 2 -2.03 4.71 23 -5 2 4.24 5.22 -23 5 -2 4.65 5.38 23 5 2 -8.17 7.63 23 5 -2 -7.60 8.34 23 -5 2 -4.62 6.81 23 -5 3 19.05 5.55 23 5 -3 3.77 5.26 23 5 -3 9.54 4.27 23 5 3 11.22 7.01 -23 5 3 10.19 5.28 23 -5 3 20.99 6.30 -23 5 -3 2.38 5.48 23 5 -3 -2.82 7.10 23 -5 3 12.34 8.25 23 -5 -3 3.77 6.74 23 5 -4 2.50 3.75 23 5 4 5.77 6.03 23 5 -4 6.03 7.50 23 -5 4 6.89 5.59 -23 5 4 10.24 5.35 -23 5 -4 9.90 5.59 23 5 4 -7.81 8.11 23 5 -4 -1.26 6.32 23 -5 4 1.54 6.81 23 6 0 1.83 4.23 23 6 0 -5.32 5.43 23 6 0 -4.30 7.07 23 -6 0 1.00 5.70 -23 6 0 -1.11 5.34 23 6 0 8.31 8.07 23 -6 0 -1.50 7.18 23 6 -1 2.64 3.88 23 6 -1 7.88 5.55 23 6 1 -3.79 4.37 23 6 1 1.37 6.54 23 6 -1 5.95 7.45 23 -6 1 9.51 5.67 -23 6 -1 5.78 5.41 -23 6 1 8.66 5.47 23 6 1 15.09 8.28 23 6 -1 19.33 8.47 23 -6 1 1.56 7.45 23 6 -2 9.41 4.07 23 6 2 0.99 4.45 23 -6 -2 2.76 5.53 23 6 2 6.43 6.42 23 6 -2 27.27 8.18 -23 6 2 6.33 4.83 23 -6 2 9.93 5.82 -23 6 -2 -2.38 5.62 23 6 2 20.03 8.84 23 6 -2 6.11 7.99 23 -6 2 3.17 7.95 23 6 3 -4.80 6.54 23 6 -3 0.82 3.88 23 -6 -3 -4.29 5.97 23 6 -3 9.84 7.99 23 -6 3 9.17 5.74 23 6 -4 6.31 6.91 23 -7 0 -1.53 7.33 23 -7 0 -2.12 5.31 23 -7 -1 -5.76 7.71 23 -7 1 3.35 5.58 24 0 0 24.04 5.64 24 0 0 25.70 8.62 -24 0 0 25.61 6.18 24 0 -1 20.14 5.28 24 0 -1 13.58 4.98 24 0 1 4.61 7.08 24 0 -1 22.00 8.65 -24 0 1 8.26 4.99 -24 0 -1 9.80 5.08 24 0 -2 -2.03 4.20 24 0 -2 -1.03 4.37 24 0 2 4.50 4.60 -24 0 2 5.28 4.44 -24 0 -2 7.13 5.28 24 0 2 4.58 7.01 24 0 -2 8.41 8.05 24 0 -3 -1.03 4.52 -24 0 -3 4.26 5.05 -24 0 3 4.22 4.47 24 0 -3 1.29 6.70 24 0 3 -6.06 7.25 24 0 3 -0.99 5.11 -24 0 -4 1.12 5.34 -24 0 4 1.62 4.12 24 0 -4 5.78 6.07 24 0 4 3.10 5.14 24 1 0 11.86 4.68 24 1 0 10.64 4.62 24 1 0 3.05 7.32 24 -1 0 6.00 7.80 -24 1 0 6.95 4.86 -24 -1 0 -0.90 4.68 24 1 -1 11.76 4.91 24 1 -1 -1.04 4.24 24 -1 1 3.31 4.46 24 1 1 3.29 4.58 -24 1 1 -5.66 4.99 -24 -1 1 0.87 4.39 -24 1 -1 1.02 5.07 -24 -1 -1 6.61 4.69 24 -1 -1 1.46 6.90 24 1 1 7.74 7.29 24 1 -1 -1.50 7.33 24 -1 1 9.16 7.64 24 1 -2 5.35 4.55 24 -1 -2 9.40 4.74 24 1 -2 12.21 4.75 24 -1 2 9.03 5.21 24 1 2 -2.21 4.80 -24 1 2 9.09 4.84 -24 -1 2 10.02 4.51 -24 1 -2 6.34 5.01 -24 -1 -2 3.94 4.85 24 -1 -2 1.38 7.14 24 1 2 1.54 7.83 24 1 -2 9.92 7.21 24 -1 2 6.10 7.71 24 -1 2 4.68 5.04 24 1 -3 2.15 4.77 24 1 -3 2.01 4.33 -24 1 -3 5.48 5.11 -24 -1 -3 3.08 4.99 -24 1 3 2.66 4.46 24 1 3 -4.57 7.28 24 -1 -3 3.80 6.78 24 1 -3 -5.24 6.75 24 -1 3 1.52 7.31 24 -1 3 -2.97 5.23 -24 1 -4 5.73 5.43 -24 -1 -4 2.17 5.14 24 1 -4 -5.88 6.46 24 -1 4 -4.15 5.15 -24 1 4 -1.70 4.34 24 -2 0 36.78 6.80 24 2 0 33.69 7.07 24 2 0 26.23 6.34 24 -2 0 37.49 9.32 -24 2 0 40.04 7.11 24 2 -1 6.85 5.07 24 -2 1 8.83 4.86 24 2 -1 3.07 4.21 24 2 1 1.07 4.36 24 2 1 7.02 5.00 -24 2 1 8.79 4.91 -24 2 -1 4.23 5.39 -24 -2 -1 9.86 4.45 24 2 1 1.57 7.59 24 2 -1 1.52 7.39 24 -2 1 -1.53 7.21 24 -2 -1 1.45 7.21 24 2 -2 9.00 4.99 24 2 -2 5.99 4.59 24 -2 2 -2.26 4.78 24 2 2 4.43 4.72 24 2 2 -1.18 5.03 24 -2 2 5.65 5.05 -24 2 -2 -1.09 5.45 -24 -2 -2 2.84 4.57 -24 2 2 0.94 4.44 24 2 2 14.04 7.81 24 2 -2 4.31 7.24 24 -2 2 3.07 7.35 24 -2 -2 1.37 7.01 24 2 -3 11.25 5.10 24 2 3 7.15 5.81 24 2 -3 -4.67 7.41 24 -2 3 1.99 5.01 24 -2 -3 2.51 6.52 24 2 3 7.70 7.73 24 2 -3 1.33 6.83 24 -2 3 12.25 7.46 -24 2 -3 11.27 5.59 -24 -2 -3 9.01 4.97 -24 2 3 4.61 4.51 -24 2 4 -0.89 4.41 24 -2 4 2.10 5.10 -24 -2 -4 -2.12 5.42 24 2 -4 -3.60 6.82 24 -3 0 1.09 4.57 24 3 0 4.11 4.71 24 3 0 -6.12 5.85 -24 3 0 -5.27 5.35 24 3 0 15.77 8.06 24 -3 0 -1.51 7.88 24 3 0 10.55 7.43 24 3 -1 2.40 4.91 24 3 -1 1.00 4.37 24 3 1 2.10 4.56 24 3 1 3.71 5.00 24 3 -1 -1.54 7.56 -24 3 1 11.19 5.82 -24 3 -1 6.54 5.38 24 3 1 1.59 7.44 24 3 -1 -6.14 7.63 24 -3 1 6.18 7.45 24 -3 -1 2.90 7.16 24 3 -2 2.37 4.80 24 3 -2 1.95 4.37 24 3 2 -2.49 4.99 24 -3 2 5.82 5.33 24 3 2 12.62 8.45 24 3 -2 5.83 7.71 24 -3 2 3.12 7.82 24 -3 -2 9.55 7.03 -24 3 -2 7.82 5.56 -24 3 2 -0.99 5.11 24 -3 3 3.06 5.40 -24 3 3 -0.95 4.66 24 3 -3 -4.07 6.68 24 -3 -3 4.98 6.79 24 3 -4 3.65 6.80 24 4 0 22.47 8.26 24 4 0 28.81 8.80 -24 4 0 12.89 5.73 24 4 1 1.44 7.20 24 4 -1 3.05 7.63 24 4 1 9.66 7.94 24 4 -1 -1.56 7.39 24 -4 -1 4.39 7.37 -24 4 -1 1.11 5.49 -24 4 1 4.17 4.87 24 -4 2 3.01 5.24 24 4 -2 13.40 7.61 24 -4 -2 -6.81 6.91 24 -4 3 -1.05 5.60 24 4 -3 -1.37 6.90 24 -4 -3 -2.47 6.43 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 32103 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.07377(2) 0.55577(2) 0.29630(2) 0.01897(6) Uani 1 1 d . . . . . Pb2 Pb 0.02043(2) 0.750000 -0.02842(3) 0.01674(6) Uani 1 2 d S T P . . Pb3 Pb 0.23350(3) 0.750000 -0.30356(4) 0.02470(8) Uani 1 2 d S T P . . Pb4 Pb 0.27499(19) 0.750000 0.1556(2) 0.0285(2) Uani 0.71 2 d S T P . . Pb5 Pb 0.2703(5) 0.750000 0.1277(6) 0.0496(14) Uani 0.29 2 d S T P . . P1 P -0.16310(10) 0.53243(13) 0.07074(14) 0.0123(2) Uani 1 1 d . . . . . P2 P 0.00299(15) 0.750000 -0.4252(2) 0.0153(4) Uani 1 2 d S T P . . O1 O -0.0913(6) 0.750000 -0.3461(8) 0.0402(19) Uani 1 2 d S T P . . O2 O -0.0171(5) 0.750000 0.4179(6) 0.0257(13) Uani 1 2 d S T P . . O3 O 0.1089(4) 0.750000 0.1753(5) 0.0134(10) Uani 1 2 d S T P . . O4 O -0.1751(4) 0.3859(4) 0.0955(4) 0.0248(9) Uani 1 1 d . . . . . O5 O -0.1685(4) 0.5588(5) -0.0902(5) 0.0297(11) Uani 1 1 d . . . . . O6 O -0.0618(3) 0.5794(5) 0.1249(6) 0.0311(11) Uani 1 1 d . . . . . O7 O -0.2451(4) 0.6053(5) 0.1488(6) 0.0333(12) Uani 1 1 d . . . . . O8 O 0.0635(4) 0.8677(5) -0.3915(7) 0.0406(14) Uani 1 1 d . . . . . H8 H 0.099291 0.852435 -0.322954 0.061 Uiso 0.5 1 calc R U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.02213(10) 0.01654(10) 0.01823(9) 0.00298(7) -0.00192(8) -0.00122(8) Pb2 0.01586(12) 0.02079(14) 0.01357(11) 0.000 -0.00303(10) 0.000 Pb3 0.02997(17) 0.02127(15) 0.02286(15) 0.000 0.00819(13) 0.000 Pb4 0.0111(3) 0.0524(5) 0.0221(5) 0.000 0.0032(3) 0.000 Pb5 0.0111(9) 0.098(2) 0.040(3) 0.000 0.0058(15) 0.000 P1 0.0110(5) 0.0105(5) 0.0154(6) 0.0000(4) 0.0014(5) 0.0008(5) P2 0.0142(8) 0.0203(9) 0.0115(8) 0.000 0.0010(7) 0.000 O1 0.029(4) 0.066(6) 0.026(4) 0.000 0.011(3) 0.000 O2 0.022(3) 0.041(4) 0.015(3) 0.000 0.002(2) 0.000 O3 0.010(2) 0.018(3) 0.012(2) 0.000 0.0001(17) 0.000 O4 0.039(3) 0.0122(18) 0.024(2) -0.0007(15) 0.007(2) -0.0076(19) O5 0.040(3) 0.033(2) 0.0160(19) 0.0031(18) -0.0050(19) 0.012(2) O6 0.018(2) 0.041(3) 0.035(3) 0.008(2) -0.0083(19) -0.011(2) O7 0.031(3) 0.025(2) 0.044(3) -0.012(2) 0.020(2) 0.005(2) O8 0.028(3) 0.033(3) 0.061(4) -0.019(3) -0.012(3) -0.001(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Pb4 Pb1 Pb5 4.13(11) . . ? O2 Pb1 Pb4 95.16(11) . . ? O2 Pb1 Pb5 96.41(12) . . ? O3 Pb1 Pb4 37.09(13) . . ? O3 Pb1 Pb5 35.30(14) . . ? O3 Pb1 O2 69.77(15) . . ? O3 Pb1 O5 85.80(15) . 5_565 ? O3 Pb1 O6 75.47(17) . . ? O3 Pb1 O7 74.55(17) . 6_656 ? O5 Pb1 Pb4 67.03(12) 5_565 . ? O5 Pb1 Pb5 64.62(13) 5_565 . ? O5 Pb1 O2 154.68(15) 5_565 . ? O6 Pb1 Pb4 105.49(12) . . ? O6 Pb1 Pb5 101.73(14) . . ? O6 Pb1 O2 81.89(19) . . ? O6 Pb1 O5 85.71(17) . 5_565 ? O6 Pb1 O7 146.06(16) . 6_656 ? O7 Pb1 Pb4 40.88(12) 6_656 . ? O7 Pb1 Pb5 44.49(14) 6_656 . ? O7 Pb1 O2 102.13(18) 6_656 . ? O7 Pb1 O5 76.61(17) 6_656 5_565 ? O3 Pb2 Pb5 34.53(16) . . ? O3 Pb2 O4 77.19(15) . 5_565 ? O3 Pb2 O4 77.19(15) . 3 ? O3 Pb2 O6 75.55(14) . 7_575 ? O3 Pb2 O6 75.55(14) . . ? O4 Pb2 Pb5 49.98(12) 3 . ? O4 Pb2 Pb5 49.98(12) 5_565 . ? O4 Pb2 O4 65.31(18) 3 5_565 ? O6 Pb2 Pb5 100.19(12) . . ? O6 Pb2 Pb5 100.19(12) 7_575 . ? O6 Pb2 O4 150.17(14) . 3 ? O6 Pb2 O4 150.17(14) 7_575 5_565 ? O6 Pb2 O4 96.77(15) 7_575 3 ? O6 Pb2 O4 96.77(15) . 5_565 ? O6 Pb2 O6 88.0(3) 7_575 . ? O4 Pb3 O1 82.81(18) 3 6_655 ? O4 Pb3 O1 82.81(18) 5_565 6_655 ? O4 Pb3 O4 67.17(19) 3 5_565 ? O4 Pb3 O5 92.11(15) 5_565 6_655 ? O4 Pb3 O5 92.11(14) 3 4_564 ? O4 Pb3 O5 152.01(14) 5_565 4_564 ? O4 Pb3 O5 152.01(14) 3 6_655 ? O4 Pb3 O8 74.03(16) 3 . ? O4 Pb3 O8 74.03(16) 5_565 7_575 ? O4 Pb3 O8 102.50(18) 3 7_575 ? O4 Pb3 O8 102.50(18) 5_565 . ? O5 Pb3 O1 75.81(15) 6_655 6_655 ? O5 Pb3 O1 75.81(15) 4_564 6_655 ? O5 Pb3 O5 99.8(2) 4_564 6_655 ? O5 Pb3 O8 131.03(16) 6_655 . ? O5 Pb3 O8 88.65(17) 6_655 7_575 ? O5 Pb3 O8 131.03(16) 4_564 7_575 ? O5 Pb3 O8 88.65(17) 4_564 . ? O8 Pb3 O1 151.60(12) 7_575 6_655 ? O8 Pb3 O1 151.60(12) . 6_655 ? O8 Pb3 O8 52.8(2) . 7_575 ? Pb1 Pb4 Pb1 66.95(4) 7_575 . ? O3 Pb4 Pb1 38.94(7) . . ? O3 Pb4 Pb1 38.94(7) . 7_575 ? O3 Pb4 O7 79.79(17) . 4_565 ? O3 Pb4 O7 79.79(17) . 6_656 ? O7 Pb4 Pb1 88.76(15) 4_565 . ? O7 Pb4 Pb1 88.76(15) 6_656 7_575 ? O7 Pb4 Pb1 44.60(13) 6_656 . ? O7 Pb4 Pb1 44.60(13) 4_565 7_575 ? O7 Pb4 O7 77.5(3) 4_565 6_656 ? Pb1 Pb5 Pb1 65.77(11) 7_575 . ? Pb2 Pb5 Pb1 60.61(10) . . ? Pb2 Pb5 Pb1 60.61(10) . 7_575 ? O3 Pb5 Pb1 37.53(9) . . ? O3 Pb5 Pb1 37.53(9) . 7_575 ? O3 Pb5 Pb2 35.03(16) . . ? O3 Pb5 O7 76.0(2) . 4_565 ? O3 Pb5 O7 76.0(2) . 6_656 ? O7 Pb5 Pb1 84.6(2) 4_565 . ? O7 Pb5 Pb1 43.88(14) 6_656 . ? O7 Pb5 Pb1 43.88(14) 4_565 7_575 ? O7 Pb5 Pb1 84.6(2) 6_656 7_575 ? O7 Pb5 Pb2 104.4(2) 6_656 . ? O7 Pb5 Pb2 104.4(2) 4_565 . ? O7 Pb5 O7 70.5(3) 4_565 6_656 ? O4 P1 O5 108.5(2) . . ? O4 P1 O6 110.6(3) . . ? O5 P1 O6 108.2(3) . . ? O7 P1 O4 109.5(3) . . ? O7 P1 O5 110.5(3) . . ? O7 P1 O6 109.5(3) . . ? O1 P2 O2 109.8(4) . 1_554 ? O1 P2 O8 111.5(3) . . ? O1 P2 O8 111.5(3) . 7_575 ? O8 P2 O2 107.9(3) . 1_554 ? O8 P2 O2 107.9(3) 7_575 1_554 ? O8 P2 O8 108.2(4) 7_575 . ? P2 O1 Pb3 179.6(5) . 6 ? Pb1 O2 Pb1 100.0(2) . 7_575 ? P2 O2 Pb1 110.2(2) 1_556 7_575 ? P2 O2 Pb1 110.2(2) 1_556 . ? Pb1 O3 Pb1 116.8(2) 7_575 . ? Pb2 O3 Pb1 107.63(14) . 7_575 ? Pb2 O3 Pb1 107.63(14) . . ? Pb4 O3 Pb1 103.97(15) . . ? Pb4 O3 Pb1 103.96(15) . 7_575 ? Pb4 O3 Pb2 117.3(2) . . ? Pb5 O3 Pb1 107.17(16) . 7_575 ? Pb5 O3 Pb1 107.17(16) . . ? Pb5 O3 Pb2 110.4(3) . . ? Pb5 O3 Pb4 6.87(18) . . ? Pb3 O4 Pb2 98.09(15) 5_565 5_565 ? P1 O4 Pb2 114.1(2) . 5_565 ? P1 O4 Pb3 133.9(2) . 5_565 ? Pb3 O5 Pb1 108.18(15) 6 5_565 ? P1 O5 Pb1 128.9(3) . 5_565 ? P1 O5 Pb3 122.7(3) . 6 ? Pb1 O6 Pb2 96.54(15) . . ? P1 O6 Pb1 148.3(3) . . ? P1 O6 Pb2 114.9(3) . . ? Pb1 O7 Pb5 91.6(2) 6_556 6_556 ? Pb4 O7 Pb1 94.52(17) 6_556 6_556 ? Pb4 O7 Pb5 4.14(13) 6_556 6_556 ? P1 O7 Pb1 134.1(3) . 6_556 ? P1 O7 Pb4 126.5(3) . 6_556 ? P1 O7 Pb5 128.0(3) . 6_556 ? P2 O8 Pb3 99.5(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 Pb4 3.624(2) . ? Pb1 Pb5 3.681(6) . ? Pb1 O2 2.608(4) . ? Pb1 O3 2.347(3) . ? Pb1 O5 2.601(5) 5_565 ? Pb1 O6 2.450(5) . ? Pb1 O7 2.552(5) 6_656 ? Pb2 Pb5 3.681(6) . ? Pb2 O3 2.255(5) . ? Pb2 O4 2.592(5) 5_565 ? Pb2 O4 2.592(5) 3 ? Pb2 O6 2.527(5) . ? Pb2 O6 2.527(5) 7_575 ? Pb3 O1 2.753(7) 6_655 ? Pb3 O4 2.528(4) 5_565 ? Pb3 O4 2.528(4) 3 ? Pb3 O5 2.573(4) 6_655 ? Pb3 O5 2.573(4) 4_564 ? Pb3 O8 2.725(5) 7_575 ? Pb3 O8 2.725(5) . ? Pb4 O3 2.252(6) . ? Pb4 O7 2.379(5) 6_656 ? Pb4 O7 2.379(5) 4_565 ? Pb5 O3 2.226(9) . ? Pb5 O7 2.581(7) 4_565 ? Pb5 O7 2.581(7) 6_656 ? P1 O4 1.534(4) . ? P1 O5 1.536(4) . ? P1 O6 1.538(5) . ? P1 O7 1.526(5) . ? P2 O1 1.474(7) . ? P2 O2 1.498(6) 1_554 ? P2 O8 1.495(5) . ? P2 O8 1.495(5) 7_575 ?