#------------------------------------------------------------------------------ #$Date: 2025-05-13 04:50:58 +0300 (Tue, 13 May 2025) $ #$Revision: 299628 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/31/28/2312844.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2312844 _cell_angle_alpha 76.672 _cell_angle_beta 87.948 _cell_angle_gamma 80.721 _cell_length_a 8.8588 _cell_length_b 18.8289 _cell_length_c 20.4271 _exptl_crystal_F_000 1368.00 _reflns_d_resolution_high 0.7467 _cod_data_source_file qf3068Ru2TPA2Ph2dhbqCl2sup7.hkl _cod_data_source_block Ru2TPA2Ph2dhbqCl2 _shelx_title ' shelxt_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.51 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1732.31 1058.01 30.76 o 2 0 0 14621.77 14852.42 143.81 o 3 0 0 285.34 141.89 6.30 o 4 0 0 3562.37 4145.07 48.34 o 5 0 0 554.04 542.38 13.94 o 6 0 0 10988.85 10476.53 124.84 o 7 0 0 1764.69 1735.53 35.89 o 8 0 0 2312.20 2223.32 74.06 o 9 0 0 2.78 30.76 13.67 o 10 0 0 64.61 20.30 16.39 o 11 0 0 362.82 361.84 39.87 o -11 1 0 1283.46 1117.61 64.31 o -10 1 0 2641.46 2784.01 68.06 o -9 1 0 1029.98 902.50 74.63 o -8 1 0 594.98 636.70 36.46 o -7 1 0 1016.15 1204.74 28.47 o -6 1 0 1507.61 1356.32 26.13 o -5 1 0 10793.61 11053.92 121.91 o -4 1 0 4478.19 4228.69 49.46 o -3 1 0 18068.40 18886.06 185.21 o -2 1 0 549.94 549.47 9.66 o -1 1 0 622.09 995.63 15.38 o 0 1 0 3525.23 2200.03 42.15 o 1 1 0 31794.18 37669.74 256.58 o 2 1 0 1732.09 1946.30 16.38 o 3 1 0 1580.34 2007.05 43.86 o 4 1 0 192.17 190.98 7.62 o 5 1 0 1297.79 1115.54 19.43 o 6 1 0 52.75 70.50 8.43 o 7 1 0 2377.25 2388.13 55.26 o 8 1 0 659.82 672.41 78.61 o 9 1 0 10207.52 10864.63 241.54 o 10 1 0 384.84 308.26 35.89 o 11 1 0 1306.90 1232.14 64.76 o -11 2 0 201.71 178.73 35.01 o -10 2 0 817.30 907.01 63.23 o -9 2 0 473.59 476.17 64.37 o -8 2 0 349.51 359.80 21.34 o -7 2 0 5763.30 5870.63 174.32 o -6 2 0 318.57 417.06 34.18 o -5 2 0 3505.03 3391.52 46.96 o -4 2 0 1773.15 1810.52 24.17 o -3 2 0 2960.73 3173.83 35.84 o -2 2 0 528.34 439.02 6.53 o -1 2 0 22000.88 22290.22 154.95 o 0 2 0 22808.69 24856.61 257.49 o 1 2 0 783.89 716.23 10.82 o 2 2 0 8683.82 10102.03 77.23 o 3 2 0 1253.66 1427.73 18.80 o 4 2 0 2409.94 2647.49 30.33 o 5 2 0 1863.92 1986.63 27.09 o 6 2 0 4263.59 4229.15 57.53 o 7 2 0 139.07 117.23 11.56 o 8 2 0 79.36 60.87 12.01 o 9 2 0 8.94 18.88 24.50 o 10 2 0 2190.92 2097.20 57.75 o 11 2 0 27.52 13.18 28.16 o -11 3 0 129.68 146.47 33.58 o -10 3 0 418.23 496.16 32.42 o -9 3 0 194.82 203.03 21.90 o -8 3 0 1735.53 1770.74 84.31 o -7 3 0 83.80 93.14 11.77 o -6 3 0 12259.35 11796.36 140.89 o -5 3 0 707.17 772.84 19.37 o -4 3 0 3118.06 3354.62 39.87 o -3 3 0 91.52 30.85 9.11 o -2 3 0 3284.27 2914.06 42.72 o -1 3 0 260.90 429.25 6.30 o 0 3 0 34761.48 34129.42 370.85 o 1 3 0 5626.82 7262.96 51.48 o 2 3 0 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322.99 325.86 34.77 o -8 8 0 335.11 364.65 33.05 o -7 8 0 2023.51 2216.19 59.01 o -6 8 0 8628.63 8644.47 132.21 o -5 8 0 1152.61 1291.46 27.37 o -4 8 0 1942.24 2187.80 33.08 o -3 8 0 707.95 918.44 19.33 o -2 8 0 595.47 532.88 16.52 o -1 8 0 6282.88 6302.42 56.79 o 0 8 0 3179.74 3445.44 54.69 o 1 8 0 750.06 615.73 25.63 o 2 8 0 1948.41 1829.23 22.56 o 3 8 0 3935.92 3984.31 63.23 o 4 8 0 240.42 56.87 6.53 o 5 8 0 5007.92 4767.30 57.05 o 6 8 0 1061.55 1001.27 22.51 o 7 8 0 2091.45 2020.02 36.33 o 8 8 0 225.99 255.97 22.70 o 9 8 0 1092.58 1031.42 82.60 o 10 8 0 0.15 -20.86 20.86 o 11 8 0 97.28 77.54 37.60 o -10 9 0 359.06 348.55 65.51 o -9 9 0 1627.40 1633.64 67.79 o -8 9 0 1234.23 1265.21 56.59 o -7 9 0 609.03 674.32 41.52 o -6 9 0 1158.43 1196.23 60.38 o -5 9 0 5464.82 5609.84 74.78 o -4 9 0 0.55 0.18 7.62 o -3 9 0 11381.12 11454.10 117.05 o -2 9 0 111.84 68.74 6.53 o -1 9 0 2118.79 2245.13 26.59 o 0 9 0 7376.51 7884.77 81.10 o 1 9 0 1073.25 995.31 18.61 o 2 9 0 6864.82 7406.96 74.26 o 3 9 0 8099.07 8626.00 82.23 o 4 9 0 2227.19 2253.21 28.87 o 5 9 0 5166.13 5221.57 72.49 o 6 9 0 86.87 99.24 10.94 o 7 9 0 1890.87 1729.00 38.74 o 8 9 0 1818.63 1651.49 49.57 o 9 9 0 577.56 451.24 40.71 o 10 9 0 487.98 460.14 44.16 o 11 9 0 92.48 57.36 26.94 o -9 10 0 134.24 178.07 32.30 o -8 10 0 1136.26 1153.35 58.22 o -7 10 0 2454.97 2510.11 67.53 o -6 10 0 2674.97 2659.49 63.80 o -5 10 0 955.33 762.31 50.70 o -4 10 0 45.09 51.75 13.10 o -3 10 0 582.72 647.01 46.14 o -2 10 0 9574.02 9028.00 88.80 o -1 10 0 3266.75 3606.75 41.20 o 0 10 0 9767.24 8610.50 96.27 o 1 10 0 197.27 195.82 20.51 o 2 10 0 1124.66 1243.19 22.95 o 3 10 0 49.05 28.56 11.39 o 4 10 0 4178.33 3880.96 109.37 o 5 10 0 701.46 633.67 20.53 o 6 10 0 2017.31 2055.83 39.73 o 7 10 0 32.57 50.00 11.19 o 8 10 0 1422.72 1290.69 62.09 o 9 10 0 4.13 -17.42 17.42 o 10 10 0 655.81 672.45 69.50 o 11 10 0 19.32 2.65 27.25 o -9 11 0 14.41 -27.91 27.91 o -8 11 0 141.47 121.29 27.89 o -7 11 0 93.20 50.48 22.99 o -6 11 0 2113.58 2301.80 118.49 o -5 11 0 6567.33 6644.87 169.76 o -4 11 0 6057.49 6168.25 85.45 o -3 11 0 5821.47 6152.55 78.84 o -2 11 0 58.76 39.08 11.96 o -1 11 0 778.88 869.25 30.19 o 0 11 0 1276.72 1251.74 22.95 o 1 11 0 8452.83 8739.10 137.86 o 2 11 0 1604.93 1512.10 33.61 o 3 11 0 9530.58 9872.42 97.93 o 4 11 0 795.42 838.16 19.97 o 5 11 0 338.36 304.91 15.87 o 6 11 0 83.57 69.73 12.47 o 7 11 0 3635.42 3926.70 66.79 o 8 11 0 677.78 803.07 45.19 o 9 11 0 2898.38 2770.67 80.18 o 10 11 0 173.27 125.51 46.71 o 11 11 0 191.63 274.50 58.11 o -9 12 0 1778.59 1602.78 71.71 o -8 12 0 160.04 199.98 32.77 o -7 12 0 3859.84 3898.70 103.49 o -6 12 0 8.76 37.02 22.22 o -5 12 0 49.62 31.97 21.08 o -4 12 0 2020.95 1883.19 36.65 o -3 12 0 7508.26 7695.41 96.15 o -2 12 0 257.27 302.90 13.41 o -1 12 0 6739.09 6885.98 72.98 o 0 12 0 61.40 104.93 9.67 o 1 12 0 371.31 287.09 38.17 o 2 12 0 1692.04 2027.38 30.20 o 3 12 0 810.15 1004.26 22.06 o 4 12 0 4616.58 4656.26 54.50 o 5 12 0 2894.67 2801.48 41.31 o 6 12 0 3815.03 3546.79 63.49 o 7 12 0 581.28 574.22 26.27 o 8 12 0 47.48 3.42 20.52 o 9 12 0 496.16 541.07 40.45 o 10 12 0 1055.83 1050.12 73.49 o 11 12 0 5.02 31.61 38.17 o -8 13 0 563.70 465.79 44.45 o -7 13 0 11.95 25.33 25.44 o -6 13 0 3533.75 3489.41 309.33 o -5 13 0 360.52 362.47 24.09 o -4 13 0 4057.04 3780.79 67.31 o -3 13 0 908.59 828.21 44.43 o -2 13 0 912.91 840.32 23.81 o -1 13 0 135.87 80.51 9.24 o 0 13 0 4017.45 3977.33 49.87 o 1 13 0 2489.05 2531.09 35.52 o 2 13 0 5812.96 5680.89 128.74 o 3 13 0 288.22 337.80 15.24 o 4 13 0 0.00 11.39 9.27 o 5 13 0 401.14 388.89 37.03 o 6 13 0 1517.21 1660.08 42.42 o 7 13 0 2804.60 2541.53 54.20 o 8 13 0 861.63 818.58 75.76 o 9 13 0 258.57 269.43 67.22 o 10 13 0 13.30 23.33 27.59 o -8 14 0 31.91 52.68 30.19 o -7 14 0 76.20 89.04 52.41 o -6 14 0 209.77 218.92 39.31 o -5 14 0 4491.88 4813.97 124.76 o -4 14 0 551.30 629.39 29.20 o -3 14 0 13915.85 13658.27 382.24 o -2 14 0 20.29 44.46 29.05 o -1 14 0 771.45 865.73 72.92 o 0 14 0 1948.86 1919.53 62.66 o 1 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101.70 103.13 18.48 o -2 16 0 615.05 673.21 24.85 o -1 16 0 1549.19 1546.63 51.84 o 0 16 0 1458.26 1638.70 59.24 o 1 16 0 794.28 934.52 51.27 o 2 16 0 1015.25 1025.54 54.12 o 3 16 0 4959.83 5075.65 76.51 o 4 16 0 126.22 130.50 16.21 o 5 16 0 28.28 17.49 10.98 o 6 16 0 314.13 293.27 53.55 o 7 16 0 3346.63 3157.85 93.99 o 8 16 0 193.82 257.90 50.13 o 9 16 0 2010.20 2049.99 280.27 o 10 16 0 320.18 260.29 120.20 o -7 17 0 1687.95 1975.92 129.88 o -6 17 0 116.04 93.30 30.49 o -5 17 0 122.74 82.45 28.81 o -4 17 0 8.58 18.88 37.03 o -3 17 0 4951.72 5104.16 90.99 o -2 17 0 908.68 1003.54 30.77 o -1 17 0 2275.12 2367.16 59.81 o 0 17 0 295.92 425.68 23.51 o 1 17 0 0.45 -12.59 12.59 o 2 17 0 1253.18 1165.42 39.68 o 3 17 0 1656.84 1741.84 43.92 o 4 17 0 1101.30 1038.58 66.08 o 5 17 0 1177.96 1219.35 34.44 o 6 17 0 827.89 910.30 36.46 o 7 17 0 9.55 35.25 19.28 o 8 17 0 96.75 78.04 23.36 o 9 17 0 355.16 325.16 53.55 o -6 18 0 2345.14 2523.67 89.60 o -5 18 0 28.23 9.71 37.03 o -4 18 0 410.35 370.62 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864.40 751.19 41.87 o 2 20 0 89.23 43.24 46.71 o 3 20 0 377.73 330.93 34.77 o 4 20 0 898.67 946.63 45.87 o 5 20 0 58.24 71.06 43.86 o 6 20 0 3022.49 3065.92 71.21 o 7 20 0 10.24 17.16 37.60 o 8 20 0 10.52 -1.53 36.46 o -4 21 0 834.26 714.33 67.02 o -3 21 0 380.10 465.44 41.02 o -2 21 0 117.95 151.04 56.40 o -1 21 0 997.06 1041.72 40.88 o 0 21 0 874.35 925.35 37.72 o 1 21 0 2470.68 2660.72 71.69 o 2 21 0 1223.12 1186.04 89.44 o 3 21 0 721.16 780.53 48.18 o 4 21 0 498.95 414.46 38.17 o 5 21 0 0.85 -11.35 18.23 o 6 21 0 554.79 568.18 35.32 o 7 21 0 1036.19 990.56 70.89 o -3 22 0 642.98 597.64 51.24 o -2 22 0 159.11 211.48 84.88 o -1 22 0 281.09 288.30 34.18 o 0 22 0 33.05 52.62 20.00 o 1 22 0 77.14 110.69 28.74 o 2 22 0 296.73 296.75 36.02 o 3 22 0 1380.41 1350.17 63.20 o 4 22 0 850.99 824.31 52.43 o 5 22 0 119.97 119.84 21.59 o 6 22 0 872.21 859.39 41.35 o -2 23 0 406.16 327.67 44.99 o -1 23 0 11.84 22.00 19.32 o 0 23 0 2483.89 2565.22 65.62 o 1 23 0 45.14 5.85 41.59 o 2 23 0 844.20 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