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Information card for entry 2312870
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| Coordinates | 2312870.cif |
|---|---|
| Structure factors | 2312870.hkl |
| Original IUCr paper | HTML |
| Chemical name | Carbonyl(4,4'-di-<i>tert</i>-butyl-2,2'-bypyridine)hydridobis(triphenylphosphane)ruthenium(II) hexaflurophosphate |
|---|---|
| Formula | C55 H55 F6 N2 O P3 Ru |
| Calculated formula | C55 H55 F6 N2 O P3 Ru |
| Title of publication | Synthesis and structural characterization of ruthenium(II) hydrido carbonyl triphenylphosphine α-diimine complexes with derivatives of 2,2'-bipyridine. |
| Authors of publication | Wysocki, Waldemar; Karczmarzyk, Zbigniew; Kamecka, Anna |
| Journal of publication | Acta crystallographica. Section C, Structural chemistry |
| Year of publication | 2025 |
| Journal volume | 81 |
| Journal issue | 7 |
| a | 29.96 ± 0.002 Å |
| b | 11.7394 ± 0.0005 Å |
| c | 31.263 ± 0.002 Å |
| α | 90° |
| β | 109.849 ± 0.008° |
| γ | 90° |
| Cell volume | 10342.3 ± 1.2 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/c 1 |
| Hall space group symbol | -I 2yc |
| Residual factor for all reflections | 0.1362 |
| Residual factor for significantly intense reflections | 0.0835 |
| Weighted residual factors for significantly intense reflections | 0.1976 |
| Weighted residual factors for all reflections included in the refinement | 0.2338 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 300208 (current) | 2025-06-26 | cif/ hkl/ Adding structures of 2312870, 2312871 via cif-deposit CGI script. |
2312870.cif 2312870.hkl |
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Users of the data should acknowledge the original authors of the
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