#------------------------------------------------------------------------------ #$Date: 2022-04-04 09:09:47 +0300 (Mon, 04 Apr 2022) $ #$Revision: 274296 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/00/01/3000196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3000196 _cell_angle_alpha 90.000 _cell_angle_beta 91.352 _cell_angle_gamma 90.000 _cell_length_a 7.5409 _cell_length_b 21.4401 _cell_length_c 11.7364 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7386 _cod_data_source_file zn7atpso4.fcf _cod_data_source_block zn7atpso4 _shelx_title ' [Zn(H2O)5(C5H5N5)](SO4).C5H5N5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 326.81 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3.39 -1.92 1.92 o 2 0 0 41246.77 38247.35 777.83 o 3 0 0 10702.49 10904.05 225.95 o 4 0 0 17317.03 16861.33 349.98 o 5 0 0 2830.96 2894.99 65.38 o 6 0 0 81.79 161.53 15.38 o 7 0 0 180.74 220.18 20.19 o 8 0 0 2258.13 2359.45 63.46 o 9 0 0 33.09 51.92 19.23 o 10 0 0 1566.53 1565.28 63.46 o 1 1 0 3944.07 3248.16 50.48 o 2 1 0 3557.87 3222.85 67.30 o 3 1 0 57.63 77.27 4.62 o 4 1 0 10265.34 9196.12 223.06 o 5 1 0 492.95 553.72 13.55 o 6 1 0 9508.50 8978.24 133.25 o 7 1 0 2193.10 2274.70 41.45 o 8 1 0 2355.26 2399.86 45.54 o 9 1 0 1199.15 1290.04 34.65 o 10 1 0 224.12 264.80 28.16 o 1 2 0 2179.85 1945.72 29.91 o 2 2 0 4872.74 4421.81 65.38 o 3 2 0 1012.30 1030.33 17.09 o 4 2 0 2820.54 2552.33 40.04 o 5 2 0 2467.64 2462.66 40.04 o 6 2 0 62.56 106.33 18.27 o 7 2 0 709.48 730.98 20.26 o 8 2 0 134.25 147.46 16.83 o 9 2 0 8.85 6.58 13.24 o 10 2 0 38.34 33.42 18.21 o 1 3 0 3564.81 3622.59 37.49 o 2 3 0 3091.70 2965.65 45.55 o 3 3 0 1099.30 1157.27 27.88 o 4 3 0 2192.93 2156.44 46.63 o 5 3 0 275.80 281.51 10.13 o 6 3 0 3824.30 3910.49 62.14 o 7 3 0 11.70 11.62 7.62 o 8 3 0 33.75 35.98 10.39 o 9 3 0 184.44 225.29 22.59 o 10 3 0 482.08 500.45 52.88 o 0 4 0 37603.55 35478.41 364.40 o 1 4 0 96.18 110.60 3.54 o 2 4 0 3822.29 3621.71 55.41 o 3 4 0 210.18 268.25 9.16 o 4 4 0 2840.66 2662.82 41.61 o 5 4 0 541.84 599.81 14.04 o 6 4 0 4808.36 4966.31 77.05 o 7 4 0 72.68 82.63 9.23 o 8 4 0 237.98 270.54 17.76 o 9 4 0 16.76 18.27 16.35 o 10 4 0 4.10 7.58 21.21 o 1 5 0 9078.98 8120.70 63.12 o 2 5 0 94.53 76.14 2.97 o 3 5 0 4490.48 4394.94 84.13 o 4 5 0 522.25 521.12 21.15 o 5 5 0 0.76 11.86 4.30 o 6 5 0 817.73 821.75 19.37 o 7 5 0 339.15 388.41 24.52 o 8 5 0 122.74 141.83 14.28 o 9 5 0 19.19 29.78 13.14 o 10 5 0 1011.68 1035.75 45.49 o 0 6 0 12175.76 10737.65 110.09 o 1 6 0 15371.83 14751.12 260.89 o 2 6 0 4.43 6.19 1.67 o 3 6 0 6581.70 6065.50 86.20 o 4 6 0 2234.61 2259.71 53.84 o 5 6 0 9067.34 8943.63 132.13 o 6 6 0 422.92 418.64 13.83 o 7 6 0 2810.29 2898.90 75.48 o 8 6 0 321.83 354.82 18.48 o 9 6 0 611.81 626.37 24.07 o 1 7 0 9695.98 8396.05 65.77 o 2 7 0 3466.93 3406.44 33.57 o 3 7 0 10533.66 10075.96 184.02 o 4 7 0 212.22 193.88 7.00 o 5 7 0 27.60 32.71 4.44 o 6 7 0 274.72 256.91 11.74 o 7 7 0 10.39 21.81 7.54 o 8 7 0 32.01 25.96 11.54 o 9 7 0 890.02 883.52 28.54 o 0 8 0 6668.48 7078.21 74.39 o 1 8 0 2375.78 2440.89 21.26 o 2 8 0 8659.80 8226.26 77.11 o 3 8 0 11872.17 11248.77 143.11 o 4 8 0 1175.61 1174.38 15.67 o 5 8 0 1282.29 1215.85 23.98 o 6 8 0 3106.03 3214.06 53.25 o 7 8 0 2030.71 1992.35 37.88 o 8 8 0 1472.56 1493.80 37.54 o 9 8 0 313.18 335.56 21.38 o 1 9 0 1758.00 1362.46 12.58 o 2 9 0 2187.85 2083.85 18.47 o 3 9 0 5235.53 5042.98 49.37 o 4 9 0 1819.41 1858.09 21.11 o 5 9 0 503.51 488.47 12.49 o 6 9 0 3354.60 3370.46 57.23 o 7 9 0 878.13 906.39 32.57 o 8 9 0 184.46 186.87 18.21 o 9 9 0 229.23 216.14 17.08 o 0 10 0 163.50 149.09 6.60 o 1 10 0 23.70 45.91 2.97 o 2 10 0 2809.45 2683.64 23.41 o 3 10 0 7625.02 7489.82 71.75 o 4 10 0 6.30 13.36 4.89 o 5 10 0 3975.78 4168.12 75.95 o 6 10 0 507.81 541.93 22.58 o 7 10 0 3255.39 3260.18 75.88 o 8 10 0 684.00 685.44 30.84 o 9 10 0 690.30 703.68 25.21 o 1 11 0 10068.12 9762.86 72.65 o 2 11 0 10.44 28.22 2.81 o 3 11 0 8417.55 8502.62 81.30 o 4 11 0 52.97 53.09 4.49 o 5 11 0 1358.66 1359.52 24.32 o 6 11 0 825.77 833.66 18.89 o 7 11 0 295.86 342.72 23.92 o 8 11 0 36.62 42.86 10.38 o 9 11 0 169.91 187.41 16.32 o 0 12 0 9693.09 10312.41 108.89 o 1 12 0 1680.73 1822.08 17.99 o 2 12 0 1926.27 2076.10 19.57 o 3 12 0 1425.73 1468.39 19.01 o 4 12 0 119.18 112.80 6.85 o 5 12 0 2630.39 2680.90 47.76 o 6 12 0 523.15 489.15 17.16 o 7 12 0 4019.49 4119.35 84.89 o 8 12 0 958.03 957.65 26.75 o 9 12 0 1492.81 1558.96 51.33 o 1 13 0 118.29 168.95 6.17 o 2 13 0 220.07 219.44 6.18 o 3 13 0 3968.66 4139.44 43.34 o 4 13 0 2446.60 2539.18 29.47 o 5 13 0 1.13 7.25 6.88 o 6 13 0 6.22 7.23 11.45 o 7 13 0 16.57 16.84 10.09 o 8 13 0 80.82 75.76 12.28 o 9 13 0 7.68 2.88 31.73 o 0 14 0 1999.91 1987.05 26.68 o 1 14 0 57.76 54.98 4.18 o 2 14 0 1080.09 1060.56 12.88 o 3 14 0 937.40 1005.17 16.14 o 4 14 0 212.80 212.40 14.04 o 5 14 0 24.38 20.80 8.44 o 6 14 0 29.13 34.17 8.82 o 7 14 0 1011.37 993.51 25.07 o 8 14 0 43.08 48.80 13.13 o 1 15 0 3729.79 3612.60 32.74 o 2 15 0 230.24 246.43 7.39 o 3 15 0 2.44 5.09 5.18 o 4 15 0 395.32 362.67 20.50 o 5 15 0 492.77 504.47 17.94 o 6 15 0 642.26 655.82 36.51 o 7 15 0 3968.31 3995.32 59.92 o 8 15 0 851.36 809.01 47.04 o 0 16 0 1723.88 1767.44 25.95 o 1 16 0 52.61 44.44 4.68 o 2 16 0 6066.81 6069.01 55.34 o 3 16 0 98.63 103.84 8.19 o 4 16 0 167.77 198.66 11.96 o 5 16 0 749.52 695.06 21.32 o 6 16 0 21.11 39.00 10.46 o 7 16 0 568.37 608.76 28.97 o 8 16 0 415.21 427.46 29.52 o 1 17 0 41.49 39.89 5.01 o 2 17 0 162.39 208.44 8.72 o 3 17 0 13.45 25.66 6.44 o 4 17 0 11672.77 11938.69 115.86 o 5 17 0 0.07 25.94 16.08 o 6 17 0 4081.97 4102.08 61.30 o 7 17 0 370.62 396.09 27.66 o 8 17 0 1649.20 1763.34 78.84 o 0 18 0 2566.14 2557.32 34.84 o 1 18 0 1126.57 1060.75 15.57 o 2 18 0 1767.02 1692.38 19.61 o 3 18 0 2501.27 2574.67 32.42 o 4 18 0 2695.89 2805.91 35.09 o 5 18 0 1248.19 1271.36 29.37 o 6 18 0 85.38 97.92 12.81 o 7 18 0 785.16 792.83 28.27 o 1 19 0 15.32 24.93 5.71 o 2 19 0 289.29 285.62 10.63 o 3 19 0 36.05 28.42 9.19 o 4 19 0 1622.20 1743.60 26.32 o 5 19 0 67.84 76.55 12.14 o 6 19 0 620.56 665.33 25.52 o 7 19 0 555.07 615.27 33.49 o 0 20 0 2956.96 3013.20 46.81 o 1 20 0 340.03 287.60 10.95 o 2 20 0 671.61 723.95 13.80 o 3 20 0 342.37 370.68 17.35 o 4 20 0 5.89 18.80 8.47 o 5 20 0 146.94 157.02 14.57 o 6 20 0 128.71 112.27 14.29 o 7 20 0 15.03 39.93 21.15 o 1 21 0 116.16 99.03 8.55 o 2 21 0 420.90 384.16 11.96 o 3 21 0 24.21 41.56 8.85 o 4 21 0 931.72 959.54 24.61 o 5 21 0 288.71 342.69 24.12 o 6 21 0 124.56 161.14 20.36 o 7 21 0 982.35 998.97 58.65 o 0 22 0 1215.82 1199.63 39.82 o 1 22 0 54.44 44.22 7.12 o 2 22 0 3863.58 3775.79 37.14 o 3 22 0 8.03 11.55 9.18 o 4 22 0 15.35 29.81 17.00 o 5 22 0 139.26 133.64 20.62 o 6 22 0 356.51 440.35 49.04 o 1 23 0 2865.41 2856.61 31.31 o 2 23 0 77.39 94.93 8.09 o 3 23 0 1296.58 1319.51 25.72 o 4 23 0 119.78 134.89 15.89 o 5 23 0 271.73 318.94 46.63 o 6 23 0 269.89 286.52 36.54 o 0 24 0 72.46 49.35 13.15 o 1 24 0 758.23 805.65 18.84 o 2 24 0 10.09 14.50 7.97 o 3 24 0 19.98 53.91 15.40 o 4 24 0 114.67 69.18 20.36 o 5 24 0 1439.60 1515.59 49.26 o 1 25 0 2509.26 2522.67 40.20 o 2 25 0 151.05 159.83 11.43 o 3 25 0 1653.94 1694.08 52.57 o 4 25 0 582.26 561.91 59.61 o 5 25 0 425.92 474.97 60.57 o 0 26 0 218.89 229.47 25.99 o 1 26 0 705.85 775.57 23.22 o 2 26 0 310.63 348.13 23.37 o 3 26 0 880.92 1009.93 87.11 o 4 26 0 2.61 20.65 24.81 o 1 27 0 3970.95 4156.25 52.12 o 2 27 0 394.15 322.80 26.92 o 3 27 0 836.31 958.59 69.23 o 0 28 0 14.83 46.15 26.51 o 1 28 0 196.25 236.34 24.42 o 2 28 0 8.36 -6.74 22.81 o -10 1 1 197.65 203.34 18.09 o -9 1 1 95.95 114.02 14.61 o -8 1 1 458.88 492.92 20.36 o -7 1 1 92.86 99.14 10.39 o -6 1 1 1019.70 1023.45 21.34 o -5 1 1 1606.42 1588.93 27.17 o -4 1 1 1754.85 1821.93 29.21 o -3 1 1 547.77 762.45 20.19 o -1 1 1 2100.71 1830.44 29.81 o 1 1 1 19004.55 18326.17 190.37 o 2 1 1 161.68 129.61 3.31 o 3 1 1 4300.99 4141.45 64.00 o 4 1 1 283.06 250.86 9.16 o 5 1 1 1030.47 990.38 20.36 o 6 1 1 2.25 3.24 6.43 o 7 1 1 34.63 45.13 8.84 o 8 1 1 6.36 14.64 10.52 o 9 1 1 410.90 442.29 25.81 o 10 1 1 199.02 199.02 30.77 o -10 2 1 133.61 162.69 21.03 o -9 2 1 435.63 441.45 23.96 o -8 2 1 73.47 83.08 11.08 o -7 2 1 1309.37 1322.89 27.38 o -6 2 1 313.37 304.65 12.01 o -5 2 1 3430.30 3309.45 51.25 o -4 2 1 9766.96 8999.38 186.53 o -3 2 1 827.32 893.21 23.08 o -1 2 1 1226.35 1146.88 18.69 o 0 2 1 9010.75 8032.67 291.83 o 1 2 1 4082.11 3745.51 71.22 o 2 2 1 23.77 30.28 3.88 o 3 2 1 221.78 202.65 5.62 o 4 2 1 106.74 90.84 5.62 o 5 2 1 423.70 413.03 13.14 o 6 2 1 1817.35 1791.82 33.23 o 7 2 1 521.22 567.09 19.30 o 8 2 1 2041.52 2107.50 42.45 o 9 2 1 7.87 12.72 13.14 o 10 2 1 174.69 204.06 21.72 o -10 3 1 8.13 14.28 20.36 o -9 3 1 15.03 23.07 10.89 o -8 3 1 1999.16 2024.30 39.56 o -7 3 1 22.23 31.23 7.62 o -6 3 1 1363.40 1365.69 25.59 o -5 3 1 350.98 326.60 9.60 o -4 3 1 5518.85 5410.20 115.38 o -3 3 1 14809.37 12430.87 254.79 o -2 3 1 428.17 356.87 8.84 o -1 3 1 7820.61 6815.30 98.11 o 0 3 1 11037.79 9950.41 186.38 o 1 3 1 570.52 478.51 5.98 o 2 3 1 2232.26 2074.53 26.99 o 3 3 1 2.43 9.41 2.66 o 4 3 1 5243.47 5137.21 103.58 o 5 3 1 1618.72 1669.31 30.11 o 6 3 1 185.92 193.43 12.01 o 7 3 1 723.57 777.50 25.48 o 8 3 1 253.42 255.78 18.71 o 9 3 1 99.15 104.80 21.15 o 10 3 1 67.64 83.66 23.08 o -10 4 1 1536.73 1528.06 47.90 o -9 4 1 2226.25 2245.18 38.85 o -8 4 1 12.05 28.51 9.43 o -7 4 1 2961.96 3014.43 50.77 o -6 4 1 2496.26 2476.39 41.20 o -5 4 1 4106.15 4044.91 91.34 o -4 4 1 14931.28 13184.66 272.10 o -3 4 1 2459.88 2666.16 60.57 o -2 4 1 20898.38 20119.23 296.42 o -1 4 1 7291.40 6545.23 104.36 o 0 4 1 2262.75 1987.55 17.92 o 1 4 1 13104.30 12105.17 115.02 o 2 4 1 665.64 870.91 13.40 o 3 4 1 3353.79 3128.37 39.91 o 4 4 1 1289.04 1213.07 18.58 o 5 4 1 1166.40 1174.32 23.27 o 6 4 1 2022.85 1985.84 36.25 o 7 4 1 26.15 35.06 8.32 o 8 4 1 1005.81 1034.99 28.34 o 9 4 1 822.51 878.12 30.23 o 10 4 1 659.45 693.66 38.30 o -10 5 1 1386.63 1322.02 68.26 o -9 5 1 181.33 203.58 15.83 o -8 5 1 1556.63 1642.18 36.54 o -7 5 1 65.01 79.72 8.29 o -6 5 1 1505.39 1596.36 28.87 o -5 5 1 5072.67 5139.07 114.42 o -4 5 1 3333.83 3437.26 78.84 o -3 5 1 9285.61 8367.58 176.91 o -2 5 1 1451.02 1279.44 23.45 o -1 5 1 5148.97 4438.20 33.04 o 0 5 1 14324.47 12908.70 123.98 o 1 5 1 3599.15 3070.68 29.82 o 2 5 1 17547.96 16351.05 207.87 o 3 5 1 6889.25 6984.59 94.17 o 4 5 1 2888.99 2877.96 37.85 o 5 5 1 745.06 822.10 15.18 o 6 5 1 285.23 300.18 13.46 o 7 5 1 24.19 32.68 8.53 o 8 5 1 1389.27 1384.47 32.98 o 9 5 1 562.23 570.69 27.26 o 10 5 1 716.31 763.41 58.65 o -9 6 1 1014.41 1049.33 26.48 o -8 6 1 92.69 119.54 11.01 o -7 6 1 3050.98 3065.34 43.39 o -6 6 1 2798.92 2794.50 84.61 o -5 6 1 9.54 19.23 6.80 o -4 6 1 10890.34 10491.41 276.42 o -3 6 1 608.33 807.86 18.69 o -2 6 1 25478.43 25096.01 369.56 o -1 6 1 9777.69 8853.46 69.08 o 0 6 1 1655.08 1572.83 16.48 o 1 6 1 3457.57 3484.06 30.74 o 2 6 1 1786.64 1657.42 17.48 o 3 6 1 15890.81 15035.80 179.11 o 4 6 1 718.13 665.18 13.00 o 5 6 1 301.82 301.60 9.64 o 6 6 1 3317.27 3294.04 54.87 o 7 6 1 416.15 414.72 17.25 o 8 6 1 2115.79 2118.40 46.05 o 9 6 1 1360.25 1380.73 37.18 o -9 7 1 218.22 211.64 15.70 o -8 7 1 753.03 794.28 22.64 o -7 7 1 166.59 183.00 10.45 o -6 7 1 10.95 31.22 12.02 o -5 7 1 172.22 129.15 12.92 o -4 7 1 1746.60 1900.26 50.96 o -3 7 1 966.82 760.81 20.67 o -2 7 1 608.75 668.31 15.30 o -1 7 1 7.56 14.03 2.23 o 0 7 1 7.35 11.08 1.75 o 1 7 1 13617.30 12278.71 110.14 o 2 7 1 6582.39 6188.92 52.89 o 3 7 1 1472.80 1488.43 28.99 o 4 7 1 3811.88 3854.46 52.14 o 5 7 1 147.09 163.27 8.82 o 6 7 1 60.09 67.38 9.61 o 7 7 1 518.36 514.11 18.85 o 8 7 1 283.38 284.89 26.92 o 9 7 1 4.14 10.71 14.32 o -9 8 1 145.82 140.38 12.67 o -8 8 1 37.07 37.66 8.64 o -7 8 1 51.85 45.49 12.86 o -6 8 1 946.99 980.01 27.19 o -5 8 1 367.54 362.87 17.79 o -4 8 1 358.62 381.29 15.29 o -3 8 1 1055.75 1151.64 15.10 o -2 8 1 10446.50 10051.36 93.45 o -1 8 1 125.56 103.74 3.58 o 0 8 1 8.68 4.31 1.77 o 1 8 1 263.91 305.76 6.73 o 2 8 1 10754.45 10829.52 91.11 o 3 8 1 57.16 43.40 4.65 o 4 8 1 224.49 230.69 13.38 o 5 8 1 461.71 475.48 12.80 o 6 8 1 278.94 256.63 13.83 o 7 8 1 246.77 247.80 16.00 o 8 8 1 1027.84 985.02 28.60 o 9 8 1 4.49 -11.09 14.04 o -9 9 1 547.98 509.78 36.21 o -8 9 1 96.09 97.90 9.42 o -7 9 1 14.52 18.27 11.56 o -6 9 1 191.16 161.53 17.00 o -5 9 1 0.21 1.88 7.80 o -4 9 1 2716.49 2959.60 42.88 o -3 9 1 191.72 220.51 8.42 o -2 9 1 4.80 1.37 2.84 o -1 9 1 1362.08 1327.30 13.09 o 0 9 1 683.93 694.86 8.07 o 1 9 1 5681.64 5443.70 44.48 o 2 9 1 3133.97 3402.10 28.84 o 3 9 1 19.63 25.51 4.78 o 4 9 1 22.53 24.54 5.00 o 5 9 1 1333.44 1204.04 21.63 o 6 9 1 63.60 60.00 10.10 o 7 9 1 126.49 123.07 13.46 o 8 9 1 145.69 146.76 13.52 o 9 9 1 187.64 173.27 17.54 o -9 10 1 16.73 21.76 11.12 o -8 10 1 398.74 400.96 31.04 o -7 10 1 176.26 166.18 12.88 o -6 10 1 176.93 163.45 25.96 o -5 10 1 21.42 26.56 3.73 o -4 10 1 131.23 125.27 8.88 o -3 10 1 526.32 560.09 9.63 o -2 10 1 1454.38 1408.84 17.10 o -1 10 1 1383.49 1350.54 12.91 o 0 10 1 2224.34 2486.83 22.43 o 1 10 1 7024.69 7088.31 57.20 o 2 10 1 2544.92 2837.72 25.00 o 3 10 1 473.56 449.02 10.86 o 4 10 1 226.89 248.50 10.37 o 5 10 1 1101.88 1080.91 20.65 o 6 10 1 67.02 67.51 8.88 o 7 10 1 128.04 123.49 13.92 o 8 10 1 339.76 338.63 38.46 o 9 10 1 4.40 -5.29 13.29 o -9 11 1 3.79 12.31 21.04 o -8 11 1 618.24 581.57 31.19 o -7 11 1 1.57 5.54 7.05 o -6 11 1 1780.39 1756.20 29.04 o -5 11 1 884.65 906.29 14.71 o -4 11 1 218.88 209.73 8.46 o -3 11 1 2401.03 2637.02 28.75 o -2 11 1 657.14 722.65 8.62 o -1 11 1 4267.05 4043.62 32.23 o 0 11 1 4116.81 4060.37 32.46 o 1 11 1 576.13 582.43 8.62 o 2 11 1 2712.05 2462.25 22.50 o 3 11 1 1088.05 1181.77 18.74 o 4 11 1 538.16 503.99 12.71 o 5 11 1 1839.98 1794.71 26.08 o 6 11 1 6.05 10.84 7.20 o 7 11 1 4156.17 4058.50 75.89 o 8 11 1 98.93 108.68 12.96 o 9 11 1 38.03 32.19 14.34 o -9 12 1 799.55 795.66 71.63 o -8 12 1 321.12 275.37 26.20 o -7 12 1 2743.56 2796.43 43.13 o -6 12 1 1849.94 1859.94 36.42 o -5 12 1 1018.68 1073.33 18.86 o -4 12 1 723.73 643.07 12.83 o -3 12 1 870.98 1019.98 14.91 o -2 12 1 988.25 843.03 10.10 o -1 12 1 5196.50 5215.78 40.86 o 0 12 1 2245.02 2280.38 20.31 o 1 12 1 741.45 595.08 9.46 o 2 12 1 55.04 80.41 4.35 o 3 12 1 985.85 931.38 14.52 o 4 12 1 702.49 775.34 15.85 o 5 12 1 1416.86 1412.65 23.22 o 6 12 1 1496.91 1576.85 29.14 o 7 12 1 264.63 258.60 19.03 o 8 12 1 419.99 437.92 21.46 o 9 12 1 49.93 24.57 22.09 o -9 13 1 37.96 37.40 28.28 o -8 13 1 761.05 720.81 44.49 o -7 13 1 189.52 194.56 16.62 o -6 13 1 3665.41 3681.44 53.13 o -5 13 1 1317.94 1359.90 20.89 o -4 13 1 17.87 33.49 5.38 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