#------------------------------------------------------------------------------ #$Date: 2022-03-11 23:18:23 +0200 (Fri, 11 Mar 2022) $ #$Revision: 273664 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/01/3500120.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500120 _cell_angle_alpha 90.000 _cell_angle_beta 95.852 _cell_angle_gamma 90.000 _cell_length_a 5.7306 _cell_length_b 30.3712 _cell_length_c 9.9232 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file 2c12so4_cod.fcf _cod_data_source_block 2c12so4 _shelx_title ' 2c12so4 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 181.50 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6063.90 5032.80 70.65 o 4 0 0 3099.22 3055.26 51.03 o 6 0 0 632.89 665.50 12.78 o 1 1 0 84.85 70.05 1.18 o 2 1 0 8419.13 7245.83 86.09 o 3 1 0 293.43 293.06 3.49 o 4 1 0 1300.09 1412.86 23.18 o 5 1 0 35.64 37.76 0.46 o 6 1 0 291.91 291.12 4.07 o 7 1 0 8.50 10.03 0.36 o 1 2 0 2538.90 3115.60 41.39 o 2 2 0 3915.92 3335.11 42.06 o 3 2 0 60.37 56.68 1.19 o 4 2 0 878.13 885.36 7.53 o 5 2 0 10.16 9.65 0.22 o 6 2 0 457.44 474.10 6.02 o 7 2 0 10.78 10.93 0.38 o 1 3 0 5515.47 4443.85 127.90 o 2 3 0 3660.69 3756.76 61.47 o 3 3 0 1718.76 2099.45 40.32 o 4 3 0 1278.50 1334.88 17.87 o 5 3 0 98.71 97.16 1.15 o 6 3 0 218.98 223.93 3.18 o 7 3 0 105.15 114.96 2.07 o 0 4 0 6061.27 5546.26 112.66 o 1 4 0 5924.37 4884.65 70.70 o 2 4 0 961.92 1122.91 24.47 o 3 4 0 202.62 175.12 3.19 o 4 4 0 65.14 57.25 0.56 o 5 4 0 110.85 117.41 1.36 o 6 4 0 41.68 43.47 0.72 o 7 4 0 73.23 76.53 1.44 o 1 5 0 15335.40 15760.15 177.45 o 2 5 0 477.98 479.94 12.30 o 3 5 0 658.41 695.73 7.23 o 4 5 0 490.99 502.13 4.28 o 5 5 0 1017.59 1059.23 11.04 o 6 5 0 0.67 0.54 0.08 o 7 5 0 367.26 395.30 6.62 o 0 6 0 361.34 425.77 22.59 o 1 6 0 7046.27 5620.97 104.01 o 2 6 0 69.84 62.81 1.35 o 3 6 0 1443.69 1429.77 31.26 o 4 6 0 10.32 7.42 0.17 o 5 6 0 33.54 34.63 0.53 o 6 6 0 12.54 14.34 0.35 o 7 6 0 137.66 139.79 2.46 o 1 7 0 1841.90 1827.85 34.03 o 2 7 0 560.26 587.36 19.40 o 3 7 0 15.38 18.11 0.34 o 4 7 0 130.29 128.83 1.62 o 5 7 0 1271.96 1326.78 14.52 o 6 7 0 26.43 24.32 0.48 o 7 7 0 842.38 891.70 14.67 o 0 8 0 1669.53 1243.88 47.92 o 1 8 0 4788.56 4837.18 68.05 o 2 8 0 48.52 63.25 1.35 o 3 8 0 3082.63 2958.08 50.79 o 4 8 0 165.95 163.57 1.93 o 5 8 0 54.97 55.31 0.76 o 6 8 0 4.05 5.38 0.23 o 7 8 0 1.37 3.03 0.29 o 1 9 0 747.31 710.73 29.81 o 2 9 0 688.88 558.69 18.40 o 3 9 0 65.15 62.44 0.79 o 4 9 0 253.04 247.18 2.83 o 5 9 0 1204.49 1204.64 13.21 o 6 9 0 1.34 0.85 0.13 o 7 9 0 74.69 68.76 1.15 o 0 10 0 4083.64 3952.02 82.96 o 1 10 0 3550.90 3274.49 57.29 o 2 10 0 42.79 46.74 1.80 o 3 10 0 2968.16 2978.41 96.94 o 4 10 0 536.18 531.56 5.60 o 5 10 0 114.28 115.44 1.42 o 6 10 0 79.87 79.63 1.09 o 7 10 0 187.28 184.74 2.59 o 1 11 0 408.85 315.92 8.15 o 2 11 0 1511.42 1303.97 42.70 o 3 11 0 30.58 45.22 0.57 o 4 11 0 1257.65 1265.92 15.70 o 5 11 0 996.58 996.13 11.61 o 6 11 0 12.32 11.88 0.30 o 7 11 0 202.87 205.75 3.14 o 0 12 0 2861.56 2966.52 41.90 o 1 12 0 1670.99 1374.78 35.13 o 2 12 0 83.81 90.06 1.33 o 3 12 0 3313.46 3176.80 103.43 o 4 12 0 958.16 974.48 10.16 o 5 12 0 129.30 121.86 1.54 o 6 12 0 264.74 284.19 3.89 o 7 12 0 65.64 67.22 1.12 o 1 13 0 119.19 91.24 1.90 o 2 13 0 1717.97 1662.49 38.98 o 3 13 0 382.75 343.13 3.47 o 4 13 0 1555.60 1586.17 23.24 o 5 13 0 495.91 489.80 5.82 o 6 13 0 1.24 4.28 0.22 o 0 14 0 3258.21 3186.15 45.50 o 1 14 0 431.82 428.71 6.31 o 2 14 0 183.70 208.20 2.67 o 3 14 0 244.34 264.86 2.70 o 4 14 0 1425.77 1460.12 15.96 o 5 14 0 27.25 24.88 0.45 o 6 14 0 180.66 171.80 2.29 o 1 15 0 167.70 154.40 2.45 o 2 15 0 1542.15 1554.21 35.91 o 3 15 0 74.92 76.36 0.86 o 4 15 0 446.69 457.40 5.11 o 5 15 0 40.04 42.45 0.72 o 6 15 0 0.15 0.86 0.15 o 0 16 0 2797.80 2834.99 124.12 o 1 16 0 18.93 19.17 0.41 o 2 16 0 48.46 58.90 0.69 o 3 16 0 2.80 2.67 0.18 o 4 16 0 271.76 271.16 3.29 o 5 16 0 259.40 238.92 3.39 o 6 16 0 157.79 154.51 2.27 o 1 17 0 477.65 493.86 6.21 o 2 17 0 682.81 665.02 6.62 o 3 17 0 175.42 162.79 1.66 o 4 17 0 1625.36 1672.98 24.53 o 5 17 0 167.72 149.07 2.03 o 6 17 0 0.13 0.58 0.12 o 0 18 0 86.37 72.45 1.54 o 1 18 0 33.03 35.28 0.60 o 2 18 0 1.97 1.11 0.12 o 3 18 0 147.58 144.04 1.47 o 4 18 0 825.05 821.64 9.62 o 5 18 0 49.28 53.18 0.85 o 6 18 0 97.47 97.87 1.62 o 1 19 0 1.28 2.50 0.14 o 2 19 0 58.01 59.57 0.70 o 3 19 0 319.34 286.64 3.22 o 4 19 0 633.04 618.00 7.28 o 5 19 0 695.94 713.11 8.96 o 6 19 0 0.55 0.55 0.11 o 0 20 0 131.92 141.62 2.39 o 1 20 0 200.83 218.10 2.82 o 2 20 0 49.60 44.89 0.56 o 3 20 0 224.66 220.45 2.41 o 4 20 0 257.99 238.40 3.64 o 5 20 0 94.73 106.22 1.64 o 6 20 0 138.75 140.66 2.22 o 1 21 0 1914.21 1955.39 30.78 o 2 21 0 35.68 32.76 0.46 o 3 21 0 64.04 55.76 0.71 o 4 21 0 108.04 95.21 1.48 o 5 21 0 51.40 51.57 0.90 o 6 21 0 0.03 0.23 0.08 o 0 22 0 153.56 161.09 3.27 o 1 22 0 1015.02 1104.86 20.99 o 2 22 0 205.52 198.54 2.21 o 3 22 0 310.39 309.16 3.51 o 4 22 0 205.39 198.87 2.86 o 5 22 0 69.00 64.93 1.16 o 6 22 0 447.10 450.92 6.72 o 1 23 0 2129.47 2133.24 31.11 o 2 23 0 1.06 0.99 0.11 o 3 23 0 143.54 141.66 1.70 o 4 23 0 234.81 234.64 3.33 o 5 23 0 498.49 500.87 7.53 o 6 23 0 80.83 77.25 1.27 o 0 24 0 378.83 403.81 7.85 o 1 24 0 1114.39 1524.09 228.17 o 2 24 0 110.44 117.04 1.75 o 3 24 0 1792.33 1839.21 30.13 o 4 24 0 25.11 27.50 0.56 o 5 24 0 99.54 102.47 1.67 o 1 25 0 519.51 513.86 6.59 o 2 25 0 570.10 587.49 8.00 o 3 25 0 365.38 330.57 4.83 o 4 25 0 31.40 36.99 0.69 o 5 25 0 95.03 96.01 1.81 o 0 26 0 32.73 32.46 1.07 o 1 26 0 104.82 106.03 1.76 o 2 26 0 152.87 145.84 2.15 o 3 26 0 22.16 21.22 0.61 o 4 26 0 8.38 9.35 0.38 o 5 26 0 91.16 92.73 1.73 o 1 27 0 407.70 398.89 5.51 o 2 27 0 823.70 813.38 11.02 o 3 27 0 70.10 72.58 1.18 o 4 27 0 19.74 17.01 0.53 o 5 27 0 33.01 35.44 0.88 o 0 28 0 376.99 387.62 9.29 o 1 28 0 5.64 5.39 0.24 o 2 28 0 4.91 5.23 0.37 o 3 28 0 22.78 21.97 0.49 o 4 28 0 1.39 1.15 0.24 o 5 28 0 0.16 0.64 0.20 o 1 29 0 291.48 283.35 3.99 o 2 29 0 527.76 529.82 7.26 o 3 29 0 24.02 21.30 0.47 o 4 29 0 93.53 92.28 1.98 o 5 29 0 71.42 76.79 1.88 o 0 30 0 360.42 380.21 9.15 o 1 30 0 0.65 0.34 0.13 o 2 30 0 237.76 220.52 4.45 o 3 30 0 132.81 130.48 1.96 o 4 30 0 37.57 37.58 0.94 o 1 31 0 0.06 0.43 0.12 o 2 31 0 9.52 11.75 0.35 o 3 31 0 6.01 5.48 0.26 o 4 31 0 97.40 99.13 2.07 o 0 32 0 299.59 292.76 5.82 o 1 32 0 124.21 118.53 1.80 o 2 32 0 0.19 0.45 0.12 o 3 32 0 82.20 76.73 1.38 o 4 32 0 94.27 95.77 2.00 o 1 33 0 133.24 123.38 1.87 o 2 33 0 135.41 136.64 2.21 o 3 33 0 10.28 10.58 0.33 o 4 33 0 137.07 144.10 3.19 o 0 34 0 216.78 199.90 3.55 o 1 34 0 23.31 22.47 0.46 o 2 34 0 23.27 20.01 0.49 o 3 34 0 1.17 0.74 0.13 o 1 35 0 0.60 1.32 0.16 o 2 35 0 180.57 174.76 3.07 o 3 35 0 0.74 1.00 0.15 o 0 36 0 131.42 141.96 2.94 o 1 36 0 18.19 23.35 0.48 o 2 36 0 32.21 30.42 0.63 o 3 36 0 5.36 7.60 0.37 o 1 37 0 4.88 5.02 0.22 o 2 37 0 65.86 60.65 0.97 o 0 38 0 1.22 0.74 0.15 o 1 38 0 154.73 165.15 2.35 o 1 39 0 7.45 8.09 0.26 o -7 0 1 469.44 500.58 11.79 o -5 0 1 10.19 13.16 0.37 o -3 0 1 3250.97 2770.80 47.94 o -1 0 1 4850.83 5464.16 86.50 o 1 0 1 5922.28 5773.25 85.45 o 3 0 1 1.58 4.50 0.23 o 5 0 1 7716.60 8191.16 156.60 o 7 0 1 241.51 264.69 6.36 o -7 1 1 219.14 245.04 4.19 o -6 1 1 1.16 1.38 0.15 o -5 1 1 8.11 6.67 0.24 o -4 1 1 3954.18 3536.95 59.08 o -3 1 1 4033.40 3844.59 64.61 o -2 1 1 7.22 11.40 0.52 o -1 1 1 2698.17 1304.78 834.77 o 0 1 1 165.69 171.59 6.63 o 1 1 1 169.49 166.83 8.39 o 2 1 1 1.82 5.10 0.20 o 3 1 1 133.80 132.34 1.33 o 4 1 1 97.49 100.44 0.91 o 5 1 1 8.52 10.74 0.24 o 6 1 1 11.34 11.70 0.34 o 7 1 1 275.48 278.81 4.73 o -7 2 1 278.41 295.03 5.00 o -6 2 1 177.93 180.84 2.64 o -5 2 1 12.48 15.57 0.28 o -4 2 1 95.69 95.83 0.90 o -3 2 1 3740.26 3380.92 41.90 o -2 2 1 1.13 3.64 0.20 o -1 2 1 1914.84 2252.89 30.23 o 0 2 1 252.21 254.72 12.95 o 1 2 1 5115.74 5260.14 81.47 o 2 2 1 883.35 896.53 18.48 o 3 2 1 120.56 127.43 1.23 o 4 2 1 87.90 81.37 0.76 o 5 2 1 151.87 152.62 1.51 o 6 2 1 49.42 48.93 0.79 o 7 2 1 207.70 227.31 3.90 o -7 3 1 52.15 56.42 1.12 o -6 3 1 0.45 2.87 0.48 o -5 3 1 120.66 130.55 1.49 o -4 3 1 134.72 140.12 1.37 o -3 3 1 65.48 72.38 1.16 o -2 3 1 0.85 1.12 0.12 o -1 3 1 2478.10 1374.82 624.27 o 0 3 1 2351.68 2700.76 63.48 o 1 3 1 0.75 7.88 3.91 o 2 3 1 0.61 3.03 0.15 o 3 3 1 169.41 158.24 1.57 o 4 3 1 610.05 637.75 5.28 o 5 3 1 58.77 57.45 0.65 o 6 3 1 37.60 40.78 0.65 o 7 3 1 85.66 87.08 1.61 o -7 4 1 1.47 1.12 0.16 o -6 4 1 378.21 367.14 4.70 o -5 4 1 1145.57 1208.86 12.56 o -4 4 1 65.34 66.84 0.68 o -3 4 1 1998.66 2316.85 98.19 o -2 4 1 341.85 275.74 4.88 o -1 4 1 99.78 116.97 3.17 o 0 4 1 179.49 192.04 4.22 o 1 4 1 1932.27 1510.47 61.31 o 2 4 1 191.23 233.78 4.52 o 3 4 1 636.11 642.86 6.39 o 4 4 1 423.20 422.30 3.65 o 5 4 1 228.91 226.47 2.37 o 6 4 1 88.86 99.65 1.42 o 7 4 1 140.34 159.22 2.78 o -7 5 1 66.45 72.30 1.37 o -6 5 1 43.85 44.12 0.73 o -5 5 1 305.03 313.50 3.55 o -4 5 1 491.09 480.67 4.83 o -3 5 1 5345.35 4193.42 61.58 o -2 5 1 150.35 193.36 3.15 o -1 5 1 976.96 1315.72 40.90 o 0 5 1 6892.32 8030.86 183.36 o 1 5 1 555.00 505.73 20.35 o 2 5 1 184.41 251.51 4.85 o 3 5 1 52.56 51.44 0.59 o 4 5 1 1755.86 1736.01 28.42 o 5 5 1 48.13 50.64 0.67 o 6 5 1 310.70 311.38 4.35 o 7 5 1 2.47 2.54 0.20 o -7 6 1 5.69 7.18 0.31 o -6 6 1 375.19 375.83 4.80 o -5 6 1 8.02 7.97 0.23 o -4 6 1 315.30 327.79 3.19 o -3 6 1 61.89 60.49 0.76 o -2 6 1 2320.94 2732.01 57.48 o -1 6 1 477.52 519.25 15.00 o 0 6 1 527.28 504.64 43.68 o 1 6 1 570.05 401.59 23.83 o 2 6 1 380.79 335.75 19.71 o 3 6 1 320.14 349.38 3.89 o 4 6 1 2410.33 2581.54 84.21 o 5 6 1 52.16 53.26 0.70 o 6 6 1 18.39 18.72 0.53 o 7 6 1 41.40 51.01 0.90 o -7 7 1 43.01 47.38 0.96 o -6 7 1 120.47 133.82 1.83 o -5 7 1 66.29 65.55 0.92 o -4 7 1 1450.96 1469.42 19.63 o -3 7 1 926.94 977.37 24.56 o -2 7 1 2402.34 1912.90 44.23 o -1 7 1 1068.22 1062.89 36.15 o 0 7 1 5404.51 4754.36 88.65 o 1 7 1 231.51 249.76 8.69 o 2 7 1 185.81 224.83 5.10 o 3 7 1 67.02 54.17 0.60 o 4 7 1 34.05 35.14 0.43 o 5 7 1 58.92 59.27 0.81 o 6 7 1 170.58 159.37 2.03 o 7 7 1 28.23 27.14 0.51 o -7 8 1 1.07 1.44 0.17 o -6 8 1 4.85 7.48 0.26 o -5 8 1 72.44 74.61 1.10 o -4 8 1 556.94 575.06 5.75 o -3 8 1 39.56 42.36 0.51 o -2 8 1 75.41 102.58 3.11 o -1 8 1 1127.92 1306.00 36.05 o 0 8 1 338.71 336.15 7.00 o 1 8 1 455.74 1538.57 688.03 o 2 8 1 2721.53 2721.43 62.79 o 3 8 1 715.84 709.88 7.05 o 4 8 1 1563.56 1614.31 30.56 o 5 8 1 4.45 5.12 0.30 o 6 8 1 9.48 9.46 0.27 o 7 8 1 3.15 2.73 0.20 o -7 9 1 0.02 0.22 0.13 o -6 9 1 832.09 869.57 11.73 o -5 9 1 35.07 32.67 0.58 o -4 9 1 1917.82 1829.10 44.84 o -3 9 1 143.43 161.48 1.77 o -2 9 1 433.20 491.22 11.97 o -1 9 1 1500.55 1721.62 35.47 o 0 9 1 2404.77 2883.60 51.21 o 1 9 1 141.31 136.83 2.06 o 2 9 1 4.06 7.75 0.27 o 3 9 1 1199.05 1207.38 19.93 o 4 9 1 214.53 211.83 2.12 o 5 9 1 3.72 3.04 0.19 o 6 9 1 161.49 155.16 2.10 o 7 9 1 2.28 3.49 0.19 o -7 10 1 56.01 56.39 1.28 o -6 10 1 17.73 14.81 0.40 o -5 10 1 2.93 1.91 0.23 o -4 10 1 924.50 950.00 9.90 o -3 10 1 4.60 8.39 0.19 o -2 10 1 950.16 837.79 19.37 o -1 10 1 461.80 462.84 11.50 o 0 10 1 218.86 227.99 5.78 o 1 10 1 398.77 440.66 8.37 o 2 10 1 3907.46 3573.46 45.99 o 3 10 1 136.46 134.25 1.39 o 4 10 1 1899.26 1970.12 45.59 o 5 10 1 109.98 108.84 1.36 o 6 10 1 3.12 3.72 0.21 o 7 10 1 12.77 11.95 0.29 o -7 11 1 1.43 0.95 0.15 o -6 11 1 299.03 293.60 4.26 o -5 11 1 19.61 22.62 0.45 o -4 11 1 1367.85 1372.43 20.08 o -3 11 1 17.29 12.94 0.23 o -2 11 1 1.55 2.67 0.31 o -1 11 1 1074.51 1304.80 80.47 o 0 11 1 2446.75 2625.66 92.38 o 1 11 1 1067.29 1357.43 64.37 o 2 11 1 74.58 65.26 1.39 o 3 11 1 316.55 307.33 2.98 o 4 11 1 357.45 355.15 3.82 o 5 11 1 88.04 92.87 1.29 o 6 11 1 222.94 229.83 2.82 o 7 11 1 6.46 8.04 0.26 o -7 12 1 103.50 113.26 2.06 o -6 12 1 2.12 3.46 0.22 o -5 12 1 261.70 266.63 4.08 o -4 12 1 864.99 874.20 9.61 o -3 12 1 184.06 162.22 1.62 o -2 12 1 557.90 503.51 8.46 o -1 12 1 3335.13 3992.10 212.62 o 0 12 1 1393.50 1706.97 76.19 o 1 12 1 15.69 37.89 213.76 o 2 12 1 1733.18 2375.90 113.68 o 3 12 1 251.54 210.97 2.08 o 4 12 1 976.98 1011.07 11.11 o 5 12 1 171.23 168.75 2.13 o 6 12 1 0.31 0.81 0.15 o -7 13 1 43.66 44.32 0.89 o -6 13 1 292.96 297.84 5.08 o -5 13 1 49.95 49.24 1.22 o -4 13 1 641.46 629.14 6.96 o -3 13 1 240.40 235.18 2.82 o -2 13 1 83.12 86.93 1.98 o -1 13 1 1234.09 1313.40 43.70 o 0 13 1 1986.99 2523.36 70.42 o 1 13 1 1145.71 1279.14 47.61 o 2 13 1 0.67 3.83 0.24 o 3 13 1 1410.47 1402.95 16.23 o 4 13 1 99.90 103.83 1.28 o 5 13 1 373.05 387.63 4.38 o 6 13 1 158.17 161.12 2.01 o -6 14 1 1.19 1.44 0.19 o -5 14 1 729.82 765.96 10.37 o -4 14 1 329.52 322.65 3.88 o -3 14 1 329.41 338.69 3.94 o -2 14 1 550.53 560.31 8.27 o -1 14 1 432.35 444.44 6.01 o 0 14 1 1736.62 2057.82 274.48 o 1 14 1 329.22 309.29 4.60 o 2 14 1 1448.42 1500.89 34.69 o 3 14 1 217.41 197.08 1.96 o 4 14 1 479.85 490.52 5.47 o 5 14 1 277.48 267.43 3.07 o 6 14 1 0.45 0.68 0.11 o -6 15 1 179.72 177.32 2.82 o -5 15 1 11.23 12.00 0.38 o -4 15 1 31.68 32.55 0.57 o -3 15 1 880.28 881.25 9.55 o -2 15 1 140.60 135.33 1.42 o -1 15 1 771.38 828.26 65.38 o 0 15 1 171.97 221.72 2.52 o 1 15 1 436.05 437.17 5.47 o 2 15 1 231.62 232.78 2.38 o 3 15 1 2009.58 1993.67 46.01 o 4 15 1 40.56 40.62 0.59 o 5 15 1 785.40 797.85 8.36 o 6 15 1 99.24 96.98 1.38 o -6 16 1 1.26 1.79 0.17 o -5 16 1 728.15 753.99 10.22 o -4 16 1 2.37 1.80 0.15 o -3 16 1 260.12 276.30 2.97 o -2 16 1 184.31 193.94 2.11 o -1 16 1 31.13 37.78 0.58 o 0 16 1 2987.38 3918.44 114.68 o 1 16 1 987.64 991.12 35.16 o 2 16 1 294.24 273.13 2.92 o 3 16 1 192.64 178.61 1.79 o 4 16 1 201.70 196.68 2.17 o 5 16 1 686.41 703.97 7.39 o 6 16 1 0.24 0.47 0.09 o -6 17 1 32.37 30.64 0.58 o -5 17 1 1.03 1.15 0.14 o -4 17 1 267.87 258.09 3.63 o -3 17 1 1292.74 1259.36 15.60 o -2 17 1 100.80 95.48 1.16 o -1 17 1 734.76 733.74 19.99 o 0 17 1 1610.03 1703.83 47.73 o 1 17 1 1067.09 1177.00 33.16 o 2 17 1 245.58 258.86 2.64 o 3 17 1 1334.39 1396.89 18.70 o 4 17 1 242.63 225.78 2.47 o 5 17 1 172.56 171.36 2.04 o 6 17 1 110.02 103.30 1.43 o -6 18 1 5.57 7.23 0.39 o -5 18 1 675.04 695.92 8.74 o -4 18 1 19.59 16.98 0.37 o -3 18 1 514.34 523.66 5.26 o -2 18 1 9.74 9.60 0.35 o -1 18 1 209.55 204.01 2.86 o 0 18 1 76.18 75.56 0.95 o 1 18 1 5537.74 4403.89 164.02 o 2 18 1 4.13 3.27 0.12 o 3 18 1 194.67 167.27 1.70 o 4 18 1 4.80 6.29 0.24 o 5 18 1 294.67 306.21 3.71 o 6 18 1 0.33 0.18 0.07 o -6 19 1 3.18 2.87 0.23 o -5 19 1 18.10 18.13 0.44 o -4 19 1 315.52 311.98 4.02 o -3 19 1 1284.83 1313.05 16.29 o -2 19 1 15.57 11.97 0.24 o -1 19 1 676.55 687.87 9.29 o 0 19 1 1362.75 1408.21 26.78 o 1 19 1 2181.99 2345.83 76.48 o 2 19 1 179.19 184.58 1.93 o 3 19 1 504.23 522.36 5.04 o 4 19 1 2.85 2.29 0.15 o 5 19 1 31.41 32.32 0.55 o 6 19 1 95.97 88.66 1.34 o -6 20 1 23.88 30.21 0.62 o -5 20 1 1039.09 1076.92 14.56 o -4 20 1 138.16 127.45 1.92 o -3 20 1 218.29 210.33 2.43 o -2 20 1 389.42 366.10 4.65 o -1 20 1 1597.15 1946.33 30.38 o 0 20 1 948.11 961.36 14.22 o 1 20 1 6.48 5.77 0.18 o 2 20 1 50.89 57.69 0.69 o 3 20 1 27.81 22.59 0.39 o 4 20 1 281.29 281.34 3.67 o 5 20 1 2.12 2.66 0.23 o 6 20 1 8.05 8.19 0.27 o -6 21 1 37.58 36.63 0.71 o -5 21 1 122.28 123.25 2.05 o -4 21 1 27.77 30.92 0.61 o -3 21 1 995.46 1019.85 11.88 o -2 21 1 513.08 462.06 5.16 o -1 21 1 625.84 629.69 7.89 o 0 21 1 392.71 365.35 3.71 o 1 21 1 120.16 108.37 1.38 o 2 21 1 1.11 2.09 0.16 o 3 21 1 134.18 136.23 1.55 o 4 21 1 116.43 127.14 1.65 o 5 21 1 100.53 105.22 1.61 o 6 21 1 161.10 169.36 2.62 o -6 22 1 0.90 2.15 0.31 o -5 22 1 194.77 196.94 3.44 o -4 22 1 735.93 705.96 9.57 o -3 22 1 5.03 3.69 0.23 o -2 22 1 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